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Information card for entry 7160651
Preview
| Coordinates | 7160651.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C26 H24 N3 O2 S |
|---|---|
| Calculated formula | C26 H25 N3 O2 S |
| Title of publication | Diastereoselective construction of structurally diverse polycyclic spiroindolenines via Yb(OTf)3-catalyzed cascade [1,5]-hydride transfer/cyclization |
| Authors of publication | Hu, Song; Hu, Dan; Xu, Jianming; Wang, Jian; Yin, Heng; Xie, Ying; Li, Yu-Long; Li, Chenyi |
| Journal of publication | Organic & Biomolecular Chemistry |
| Year of publication | 2025 |
| a | 12.891 ± 0.0006 Å |
| b | 8.2439 ± 0.0003 Å |
| c | 21.5146 ± 0.001 Å |
| α | 90° |
| β | 93.477 ± 0.002° |
| γ | 90° |
| Cell volume | 2282.19 ± 0.17 Å3 |
| Cell temperature | 273.15 K |
| Ambient diffraction temperature | 273.15 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.069 |
| Residual factor for significantly intense reflections | 0.0529 |
| Weighted residual factors for significantly intense reflections | 0.1511 |
| Weighted residual factors for all reflections included in the refinement | 0.1636 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.026 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 301406 (current) | 2025-07-30 | cif/ Adding structures of 7160651 via cif-deposit CGI script. |
7160651.cif |
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Users of the data should acknowledge the original authors of the
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