Crystallography Open Database

Information card for entry 7224532

Preview

Coordinates	7224532.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H76 Co8 N14 O76 Si2 W18
Calculated formula	C14 H42 Co8 N14 O76 Si2 W18
Title of publication	Extended hybrid architectures based on tetra-CoIIsandwiched polyoxotungstates
Authors of publication	Zhu, Yu; Fang, Wei-Hui; Wei, Qi; Yang, Guo-Yu
Journal of publication	CrystEngComm
Year of publication	2016
Journal volume	18
Journal issue	15
Pages of publication	2712
a	12.7068 ± 0.0018 Å
b	13.1565 ± 0.0016 Å
c	17.082 ± 0.003 Å
α	73.022 ± 0.004°
β	83.299 ± 0.005°
γ	63.09 ± 0.004°
Cell volume	2435.1 ± 0.6 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0509
Residual factor for significantly intense reflections	0.0444
Weighted residual factors for significantly intense reflections	0.1342
Weighted residual factors for all reflections included in the refinement	0.1455
Goodness-of-fit parameter for all reflections included in the refinement	1.077
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
182639 (current)	2016-05-06	cif/ Updating files of 7224532, 7224533, 7224534 Original log message: Adding full bibliography for 7224532--7224534.cif.	7224532.cif
178008	2016-03-08	cif/ Adding structures of 7224532, 7224533, 7224534 via cif-deposit CGI script.	7224532.cif