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Information card for entry 7234157
Preview
| Coordinates | 7234157.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C29 H25 N O2 |
|---|---|
| Calculated formula | C29 H25 N O2 |
| Title of publication | Copper-Catalyzed Diastereoselective O-Transfer Reaction of N-Vinyl-α,β-Unsaturated Nitrones with Ketenes into γ-Lactones through [5+2] Cycloaddition and N-O Bond Cleavage |
| Authors of publication | Liao, Jun-Yi; Wu, Qing-Yan; Lu, Xiuqiang; Zou, Ning; Pan, Cheng-Xue; Liang, Cui; SU, Guifa; Mo, Dong-Liang |
| Journal of publication | Green Chemistry |
| Year of publication | 2019 |
| a | 13.123 ± 0.014 Å |
| b | 11.404 ± 0.012 Å |
| c | 16.76 ± 0.018 Å |
| α | 90° |
| β | 109.759 ± 0.017° |
| γ | 90° |
| Cell volume | 2361 ± 4 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296.15 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0826 |
| Residual factor for significantly intense reflections | 0.0656 |
| Weighted residual factors for significantly intense reflections | 0.1798 |
| Weighted residual factors for all reflections included in the refinement | 0.1981 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.035 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 218849 (current) | 2019-09-25 | cif/ Adding structures of 7234157 via cif-deposit CGI script. |
7234157.cif |
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