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Information card for entry 7234164
Preview
| Coordinates | 7234164.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | 11-(2-fluorophenyl)-2,3,5,6-tetraoxa-11-azaspiro[bicyclo[5.3.1]undecane-4,1'-cyclohexane] |
|---|---|
| Formula | C17 H22 F N O4 |
| Calculated formula | C17 H22 F N O4 |
| Title of publication | New synthesis of tetraoxaspirododecane-diamines and tetraoxazaspirobicycloalkanes |
| Authors of publication | Makhmudiyarova, Nataliya N.; Shangaraev, Kamil R.; Dzhemileva, Lilya U.; Tyumkina, Tatyana V.; Mescheryakova, Ekaterina S.; D'yakonov, Vladimir A.; Ibragimov, Askhat G.; Dzhemilev, Usein M. |
| Journal of publication | RSC Advances |
| Year of publication | 2019 |
| Journal volume | 9 |
| Journal issue | 51 |
| Pages of publication | 29949 |
| a | 6.4738 ± 0.0003 Å |
| b | 10.2056 ± 0.0009 Å |
| c | 12.4931 ± 0.001 Å |
| α | 75.029 ± 0.007° |
| β | 80.67 ± 0.006° |
| γ | 88.09 ± 0.006° |
| Cell volume | 786.81 ± 0.1 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0764 |
| Residual factor for significantly intense reflections | 0.0503 |
| Weighted residual factors for significantly intense reflections | 0.1115 |
| Weighted residual factors for all reflections included in the refinement | 0.1303 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.061 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 218855 (current) | 2019-09-25 | cif/ Adding structures of 7234163, 7234164, 7234165, 7234166, 7234167, 7234168 via cif-deposit CGI script. |
7234164.cif |
All data in the COD and the database itself are dedicated to the
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Users of the data should acknowledge the original authors of the
structural data.