Crystallography Open Database

Information card for entry 7234166

Preview

Coordinates	7234166.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	7,8,11-trioxaspiro[5.6]dodecane-9,10-diol
Formula	C8 H14 O6
Calculated formula	C8 H14 O6
Title of publication	New synthesis of tetraoxaspirododecane-diamines and tetraoxazaspirobicycloalkanes
Authors of publication	Makhmudiyarova, Nataliya N.; Shangaraev, Kamil R.; Dzhemileva, Lilya U.; Tyumkina, Tatyana V.; Mescheryakova, Ekaterina S.; D'yakonov, Vladimir A.; Ibragimov, Askhat G.; Dzhemilev, Usein M.
Journal of publication	RSC Advances
Year of publication	2019
Journal volume	9
Journal issue	51
Pages of publication	29949
a	6.5986 ± 0.0006 Å
b	9.8591 ± 0.0008 Å
c	29.604 ± 0.002 Å
α	90°
β	90°
γ	90°
Cell volume	1925.9 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	3
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.1975
Residual factor for significantly intense reflections	0.0921
Weighted residual factors for significantly intense reflections	0.2133
Weighted residual factors for all reflections included in the refinement	0.2743
Goodness-of-fit parameter for all reflections included in the refinement	0.975
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
218855 (current)	2019-09-25	cif/ Adding structures of 7234163, 7234164, 7234165, 7234166, 7234167, 7234168 via cif-deposit CGI script.	7234166.cif