#------------------------------------------------------------------------------ #$Date: 2019-10-07 10:14:40 +0300 (Mon, 07 Oct 2019) $ #$Revision: 219119 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/23/44/7234403.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7234403 loop_ _publ_author_name 'Min Ren' 'Carlos D. S. Brites' 'Song-Song Bao' 'Rute A. S. Ferreira' 'Li-Min Zheng' 'Luis D. Carlos' _publ_section_title ; A cryogenic luminescent ratiometric thermometer based on a lanthanide phosphonate dimer ; _journal_name_full 'Journal of Materials Chemistry C' _journal_page_first 8480 _journal_page_last 8484 _journal_paper_doi 10.1039/C5TC01468A _journal_volume 3 _journal_year 2015 _chemical_formula_moiety 'C18 H48 N8 O26 P6 Tb2, 8(H2 O)' _chemical_formula_sum 'C18 H64 N8 O34 P6 Tb2' _chemical_formula_weight 1440.43 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _cell_angle_alpha 90 _cell_angle_beta 108.512(2) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 10.8448(8) _cell_length_b 13.1903(10) _cell_length_c 16.9763(15) _cell_measurement_reflns_used 2950 _cell_measurement_temperature 173(2) _cell_measurement_theta_max 25.90 _cell_measurement_theta_min 2.96 _cell_volume 2302.7(3) _computing_cell_refinement SMART _computing_data_collection 'SMART (Bruker, 2000)' _computing_data_reduction 'SAINT (Bruker, 2000)' _computing_molecular_graphics SHELXTL _computing_publication_material SHELXTL _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_structure_solution 'SHELXTL (Bruker, 2000)' _diffrn_ambient_temperature 173(2) _diffrn_measured_fraction_theta_full 0.986 _diffrn_measured_fraction_theta_max 0.976 _diffrn_measurement_device_type 'CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0923 _diffrn_reflns_av_unetI/netI 0.0937 _diffrn_reflns_Laue_measured_fraction_full 0.986 _diffrn_reflns_Laue_measured_fraction_max 0.976 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 13397 _diffrn_reflns_point_group_measured_fraction_full 0.986 _diffrn_reflns_point_group_measured_fraction_max 0.976 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.994 _diffrn_reflns_theta_min 2.965 _diffrn_source 'sealed tube' _exptl_absorpt_coefficient_mu 3.367 _exptl_absorpt_correction_T_max 0.761 _exptl_absorpt_correction_T_min 0.420 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS(Bruker, 2000)' _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 2.077 _exptl_crystal_description sheet-like _exptl_crystal_F_000 1440 _exptl_crystal_size_max 0.25 _exptl_crystal_size_mid 0.22 _exptl_crystal_size_min 0.08 _refine_diff_density_max 0.985 _refine_diff_density_min -1.082 _refine_diff_density_rms 0.203 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.012 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 307 _refine_ls_number_reflns 4421 _refine_ls_number_restraints 38 _refine_ls_restrained_S_all 1.014 _refine_ls_R_factor_all 0.0854 _refine_ls_R_factor_gt 0.0412 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0226P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0623 _refine_ls_wR_factor_ref 0.0722 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 3064 _reflns_number_total 4421 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file J-Mater-Chem-C-2015-3-8480.cif _cod_data_source_block 1 _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 7234403 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelxl_version_number 2013-4 _shelx_res_file ; TITL 1 in P2(1)/c CELL 0.71073 10.8448 13.1903 16.9763 90.000 108.512 90.000 ZERR 2.00 0.0008 0.0010 0.0015 0.000 0.002 0.000 LATT 1 SYMM -X, 0.5+Y, 0.5-Z SFAC C H N O P Tb UNIT 36 128 16 68 12 4 OMIT -2.00 52.00 L.S. 4 ACTA BOND $H FMAP 2 PLAN 5 HTAB O5W O9_$3 HTAB O5W O11_$3 HTAB O4W O5W HTAB O4W O3_$1 HTAB O3W O5_$7 EQIV $7 x, -y+3/2, z+1/2 HTAB O3W O2W HTAB O2W O12_$6 HTAB O2W O10_$6 HTAB O2W N4_$6 EQIV $6 -x+1, y-1/2, -z+1/2 HTAB O2W O9 HTAB O1W O3W_$4 HTAB O1W O4W_$4 HTAB O8 O2W_$5 EQIV $5 -x+1, -y+2, -z+1 HTAB O5 O3_$2 HTAB N3 O4 HTAB N1 O4 HTAB C9 O3W HTAB C6 O11_$1 HTAB C6 O8 HTAB C6 O2 HTAB C5 O8 HTAB C4 O5W_$4 EQIV $4 -x+1, y+1/2, -z+1/2 HTAB C3 O12_$3 EQIV $3 x, y-1, z HTAB C2 O10_$2 EQIV $2 -x, -y+2, -z HTAB C1 O2_$1 EQIV $1 -x, y-1/2, -z+1/2 isor 0.002 0.005 O12 simu 0.002 0.005 O12 N4 delu 0.002 0.005 O12 N4 simu 0.005 0.01 N1 C1 C6 C7 delu 0.005 0.01 N1 c1 C6 C7 delu 0.01 0.02 C5 N3 CONF HTAB FREE Tb1 P1 TEMP -100.150 WGHT 0.022600 FVAR 0.07217 TB1 6 0.126076 1.056450 0.103880 11.00000 0.01135 0.00740 = 0.00693 -0.00011 0.00339 -0.00002 P1 5 -0.133155 0.970946 0.114022 11.00000 0.01182 0.00792 = 0.00861 0.00088 0.00436 0.00014 P2 5 0.169388 0.811664 0.024746 11.00000 0.01323 0.00793 = 0.00889 -0.00001 0.00435 0.00055 P3 5 0.339846 0.976466 0.320789 11.00000 0.01589 0.01209 = 0.00981 -0.00038 0.00130 -0.00088 C1 1 -0.049777 0.668732 0.164374 11.00000 0.01349 0.00743 = 0.01538 0.00270 -0.00085 -0.00626 AFIX 23 H1A 2 -0.013563 0.633949 0.218508 11.00000 -1.20000 H1B 2 -0.144559 0.655743 0.143589 11.00000 -1.20000 AFIX 0 C2 1 0.013060 0.627294 0.103369 11.00000 0.02410 0.00794 = 0.01167 0.00296 0.00348 0.00147 AFIX 23 H2A 2 0.006882 0.552394 0.101920 11.00000 -1.20000 H2B 2 -0.033276 0.653262 0.047004 11.00000 -1.20000 AFIX 0 C3 1 0.238801 0.601650 0.195913 11.00000 0.01540 0.00853 = 0.01311 0.00188 0.00220 0.00567 AFIX 23 H3A 2 0.281904 0.547808 0.173529 11.00000 -1.20000 H3B 2 0.190432 0.569018 0.229685 11.00000 -1.20000 AFIX 0 C4 1 0.341204 0.673660 0.250350 11.00000 0.01633 0.01122 = 0.01840 -0.00242 0.00177 0.00378 AFIX 23 H4A 2 0.382339 0.642031 0.305340 11.00000 -1.20000 H4B 2 0.409768 0.685358 0.224341 11.00000 -1.20000 AFIX 0 C5 1 0.178181 0.758405 0.302804 11.00000 0.02147 0.00934 = 0.00424 0.00333 0.00177 -0.00069 AFIX 23 H5A 2 0.159288 0.684939 0.302356 11.00000 -1.20000 H5B 2 0.213907 0.779738 0.361603 11.00000 -1.20000 AFIX 0 C6 1 0.052185 0.813815 0.263841 11.00000 0.01311 0.01209 = 0.01241 0.00311 0.00578 -0.00335 AFIX 23 H6A 2 0.071396 0.887160 0.263521 11.00000 -1.20000 H6B 2 -0.003481 0.804191 0.299538 11.00000 -1.20000 AFIX 0 C7 1 -0.149960 0.841225 0.146916 11.00000 0.01203 0.00899 = 0.01561 0.00138 0.00527 -0.00360 AFIX 23 H7A 2 -0.188189 0.843488 0.192655 11.00000 -1.20000 H7B 2 -0.211786 0.804576 0.099919 11.00000 -1.20000 AFIX 0 C8 1 0.199924 0.680127 0.058838 11.00000 0.02785 0.00783 = 0.01523 0.00248 0.01301 0.00197 AFIX 23 H8A 2 0.158344 0.634481 0.011564 11.00000 -1.20000 H8B 2 0.294706 0.667040 0.077125 11.00000 -1.20000 AFIX 0 C9 1 0.387575 0.847394 0.307325 11.00000 0.01101 0.01376 = 0.01129 -0.00389 0.00075 -0.00471 AFIX 3 H9A 2 0.453075 0.850023 0.277925 11.00000 -1.20000 H9B 2 0.431035 0.818493 0.363085 11.00000 -1.20000 AFIX 0 N1 3 -0.025113 0.782162 0.175722 11.00000 0.01293 0.00762 = 0.01423 0.00232 0.00539 -0.00205 AFIX 3 H1C 2 0.022007 0.800153 0.142842 11.00000 -1.20000 AFIX 0 N2 3 0.148799 0.657628 0.127628 11.00000 0.02105 0.01147 = 0.01126 0.00267 0.00818 -0.00273 N3 3 0.281557 0.774398 0.261757 11.00000 0.01099 0.01315 = 0.01107 0.00250 0.00130 0.00152 AFIX 13 H3C 2 0.237912 0.803156 0.205243 11.00000 -1.20000 AFIX 0 N4 3 0.196557 1.277414 0.120987 11.00000 0.03550 0.01220 = 0.03071 -0.00302 0.01350 -0.00486 O1 4 -0.090867 0.962307 0.036265 11.00000 0.01014 0.01195 = 0.00631 -0.00131 0.00393 0.00448 O2 4 -0.020505 1.022092 0.179091 11.00000 0.01309 0.01335 = 0.00805 -0.00189 0.00372 -0.00371 O3 4 -0.265387 1.017703 0.099424 11.00000 0.01642 0.01581 = 0.01436 0.00157 0.00980 0.00235 O4 4 0.169128 0.873397 0.100842 11.00000 0.01807 0.00668 = 0.00873 0.00237 0.00357 0.00524 O5 4 0.295534 0.833368 0.000927 11.00000 0.01309 0.01221 = 0.01746 0.00296 0.00474 0.00410 AFIX 83 H5C 2 0.282197 0.882591 -0.032115 11.00000 -1.50000 AFIX 0 O6 4 0.048220 0.821881 -0.048985 11.00000 0.01276 0.00706 = 0.00980 -0.00483 -0.00112 0.00086 O7 4 0.254692 1.014643 0.238226 11.00000 0.01788 0.01891 = 0.00983 -0.00388 0.00152 -0.00069 O8 4 0.255706 0.967966 0.381429 11.00000 0.02206 0.01415 = 0.01411 -0.00556 0.00572 -0.00749 AFIX 83 H8C 2 0.283495 1.009451 0.420622 11.00000 -1.50000 AFIX 0 O9 4 0.465066 1.031070 0.362332 11.00000 0.01648 0.01152 = 0.01990 0.00019 0.00228 -0.00337 O10 4 0.197711 1.238336 0.054347 11.00000 0.02023 0.02479 = 0.01508 -0.00331 0.00786 0.00067 O11 4 0.189053 1.219305 0.179496 11.00000 0.03106 0.01132 = 0.01305 0.00143 0.01051 -0.00379 O12 4 0.199062 1.371178 0.130265 11.00000 0.05399 0.01528 = 0.04109 -0.00440 0.01980 -0.00731 O1W 4 0.343721 1.064534 0.100785 11.00000 0.01344 0.02381 = 0.02294 0.01431 0.00668 0.00788 AFIX 3 H1WA 2 0.403638 1.020639 0.118193 11.00000 -1.20000 H1WB 2 0.354705 1.099051 0.061187 11.00000 -1.20000 AFIX 0 O2W 4 0.654505 0.934219 0.479445 11.00000 0.03210 0.02533 = 0.01598 -0.00580 0.00288 0.00618 AFIX 3 H2WA 2 0.605458 0.979194 0.449476 11.00000 -1.20000 H2WB 2 0.674771 0.889579 0.449484 11.00000 -1.20000 AFIX 0 O3W 4 0.550785 0.714093 0.481352 11.00000 0.02821 0.03220 = 0.04315 -0.00097 0.01846 0.00109 AFIX 3 H3WA 2 0.581438 0.772407 0.498536 11.00000 -1.20000 H3WB 2 0.481203 0.703285 0.492467 11.00000 -1.20000 AFIX 0 O4W 4 0.452724 0.440179 0.338149 11.00000 0.01965 0.02526 = 0.04164 0.00045 0.01978 0.00082 AFIX 3 H4WA 2 0.393632 0.463363 0.356158 11.00000 -1.20000 H4WB 2 0.478967 0.385450 0.364550 11.00000 -1.20000 AFIX 0 O5W 4 0.416501 0.230936 0.327927 11.00000 0.03416 0.02033 = 0.04825 -0.00816 0.00057 0.00134 AFIX 3 H5WA 2 0.371315 0.223795 0.277110 11.00000 -1.20000 H5WB 2 0.449201 0.174152 0.348545 11.00000 -1.20000 AFIX 0 HKLF 4 REM 1 in P2(1)/c REM R1 = 0.0412 for 3064 Fo > 4sig(Fo) and 0.0854 for all 4421 data REM 307 parameters refined using 38 restraints END WGHT 0.0227 0.0000 REM Instructions for potential hydrogen bonds HTAB C1 O2_$1 HTAB C2 O10_$2 HTAB C3 O12_$3 HTAB C4 O5W_$4 HTAB C5 O8 HTAB C6 O2 HTAB C6 O8 HTAB C6 O11_$1 HTAB C9 O3W HTAB N1 O4 HTAB N3 O4 HTAB O5 O3_$2 HTAB O8 O2W_$5 HTAB O1W O4W_$4 HTAB O1W O3W_$4 HTAB O2W O9 HTAB O2W N4_$6 HTAB O2W O10_$6 HTAB O2W O12_$6 HTAB O3W O2W HTAB O3W O5_$7 HTAB O4W O3_$1 HTAB O4W O5W HTAB O5W O11_$3 HTAB O5W O9_$3 REM Highest difference peak 0.985, deepest hole -1.082, 1-sigma level 0.203 Q1 1 -0.0002 1.0608 0.0867 11.00000 0.05 0.98 Q2 1 0.2550 1.0578 0.1601 11.00000 0.05 0.92 Q3 1 0.1409 0.8231 0.1121 11.00000 0.05 0.84 Q4 1 0.0857 1.0165 0.0651 11.00000 0.05 0.80 Q5 1 0.1235 0.9031 0.0439 11.00000 0.05 0.79 ; _shelx_res_checksum 67961 _shelx_hkl_file ; -2 0 2 404.47 3.40 2 0 -2 399.54 3.33 -3 0 3 0.47 0.94 3 0 -3 -0.04 0.87 4 0 -4 78.65 2.57 -4 0 4 78.66 2.63 -5 0 5 -0.27 1.25 5 0 -5 -0.06 1.20 6 0 -6 42.67 2.87 -6 0 6 41.73 2.96 7 0 -7 2.79 1.79 -7 0 7 1.15 1.93 -8 0 8 96.52 4.66 8 0 -8 98.58 4.58 9 0 -9 0.44 2.61 -9 0 9 -1.34 2.38 -10 0 10 1.80 3.16 10 0 -10 2.92 3.40 -11 0 11 -0.39 3.83 11 0 -11 4.10 4.06 12 0 -12 8.39 5.24 -12 0 12 -3.74 4.68 2 1 -2 2.09 0.85 -2 1 2 3.14 0.69 2 -1 -2 2.50 0.68 -2 -1 2 2.62 0.86 3 1 -3 189.11 3.34 -3 1 3 188.00 2.89 3 -1 -3 181.50 2.97 -3 -1 3 189.99 3.37 -4 1 4 0.80 0.99 4 1 -4 1.30 1.14 -4 -1 4 -0.25 1.09 4 -1 -4 1.17 1.10 5 1 -5 175.85 4.07 -5 1 5 173.85 3.71 -5 -1 5 172.78 4.11 5 -1 -5 176.80 3.77 -6 1 6 10.61 1.82 6 1 -6 8.65 1.75 -6 -1 6 11.91 1.89 6 -1 -6 9.04 1.74 -7 1 7 72.91 3.65 7 1 -7 73.83 3.90 -7 -1 7 71.78 3.90 7 -1 -7 76.38 3.71 -8 1 8 0.53 2.03 8 1 -8 -0.52 2.39 8 -1 -8 1.56 2.21 -8 -1 8 -1.07 2.17 9 1 -9 19.83 3.28 -9 1 9 16.45 3.00 -9 -1 9 18.07 3.33 9 -1 -9 21.42 3.09 10 1 -10 19.91 3.82 -10 1 10 12.72 3.41 -10 -1 10 11.64 3.60 10 -1 -10 13.31 3.31 -11 1 11 3.50 3.54 11 1 -11 3.60 4.23 11 -1 -11 -2.56 3.71 -11 -1 11 4.70 4.06 -12 1 12 2.70 4.45 12 1 -12 5.60 5.60 12 -1 -12 6.75 4.83 -12 -1 12 6.83 5.13 0 2 0 126.30 2.38 0 -2 0 130.58 2.40 1 2 -1 -0.44 0.84 -1 -2 1 0.14 0.79 2 2 -2 69.70 2.44 -2 2 2 70.83 1.75 2 -2 -2 71.14 1.77 -2 -2 2 72.27 2.41 -3 2 3 3.71 0.91 3 2 -3 3.35 1.29 3 -2 -3 4.75 0.95 -3 -2 3 3.85 1.18 4 2 -4 184.65 4.09 -4 2 4 191.97 3.21 4 -2 -4 185.63 3.42 -4 -2 4 187.56 4.09 -5 2 5 49.85 2.38 5 2 -5 49.16 2.97 5 -2 -5 46.55 2.55 -5 -2 5 48.80 2.89 -6 2 6 34.61 2.50 6 2 -6 34.52 3.15 6 -2 -6 34.64 2.74 -6 -2 6 35.83 3.07 -7 2 7 28.70 2.91 7 2 -7 32.35 3.73 -7 -2 7 28.54 3.68 7 -2 -7 31.50 3.28 8 2 -8 74.52 4.83 -8 2 8 67.10 3.93 -8 -2 8 69.78 4.67 8 -2 -8 67.16 4.15 9 2 -9 74.13 5.49 -9 2 9 59.42 4.40 9 -2 -9 66.11 4.65 -9 -2 9 63.70 5.42 -10 2 10 -1.65 2.81 10 2 -10 3.12 3.75 10 -2 -10 4.53 3.14 -10 -2 10 -3.14 3.45 11 2 -11 39.80 5.50 -11 2 11 28.03 4.14 -11 -2 11 28.27 4.90 11 -2 -11 46.03 6.10 -12 2 12 3.03 4.17 12 2 -12 -3.44 5.82 12 -2 -12 4.02 4.37 -12 -2 12 7.08 5.33 0 3 0 -0.37 0.99 0 -3 0 0.25 1.01 1 3 -1 256.59 4.09 1 -3 -1 255.77 3.60 -1 -3 1 253.24 4.07 2 3 -2 16.72 2.08 -2 -3 2 17.66 2.10 2 -3 -2 19.06 1.53 -3 3 3 70.19 2.18 3 3 -3 70.41 2.91 3 -3 -3 72.71 2.22 -3 -3 3 71.02 2.94 -4 3 4 74.97 2.31 4 3 -4 71.57 3.16 -4 -3 4 76.84 3.16 4 -3 -4 75.21 2.45 5 3 -5 103.99 3.88 -5 3 5 99.75 2.91 5 -3 -5 100.35 3.14 -5 -3 5 103.39 3.96 -6 3 6 19.61 2.27 6 3 -6 16.83 2.32 6 -3 -6 16.84 2.01 -6 -3 6 14.00 2.36 -7 3 7 0.77 1.63 7 3 -7 3.32 2.39 7 -3 -7 0.01 1.76 -7 -3 7 -0.58 2.14 -8 3 8 57.78 3.73 8 3 -8 57.80 5.08 -8 -3 8 55.81 4.93 8 -3 -8 57.73 4.16 -9 3 9 12.77 2.69 9 3 -9 16.25 3.71 9 -3 -9 10.28 2.88 -9 -3 9 13.14 3.36 -10 3 10 80.39 5.15 10 3 -10 80.36 7.08 -10 -3 10 67.70 6.93 10 -3 -10 77.47 5.48 -11 3 11 4.35 3.23 11 3 -11 -3.90 4.93 11 -3 -11 2.50 3.49 -11 -3 11 -0.23 4.81 12 3 -12 26.97 6.59 12 -3 -12 26.38 4.51 -12 -3 12 28.57 6.36 0 4 0 217.50 4.10 0 -4 0 227.01 4.24 1 4 -1 23.43 2.23 1 -4 -1 24.47 2.02 -1 -4 1 22.65 2.27 2 4 -2 9.71 1.67 -2 -4 2 10.95 1.73 2 -4 -2 11.05 1.38 3 4 -3 21.74 2.59 3 -4 -3 24.14 1.90 -3 -4 3 22.53 2.46 4 4 -4 5.94 1.77 -4 -4 4 3.65 1.49 4 -4 -4 5.46 1.30 5 4 -5 85.27 4.02 -5 4 5 91.24 2.98 5 -4 -5 91.44 3.06 -5 -4 5 89.30 3.98 6 4 -6 17.67 2.56 -6 4 6 18.02 2.33 -6 -4 6 19.81 2.73 6 -4 -6 18.35 2.08 -7 4 7 23.01 2.20 7 4 -7 21.66 3.09 7 -4 -7 19.48 2.42 -7 -4 7 16.48 2.98 -8 4 8 41.85 3.34 8 4 -8 51.48 5.21 -8 -4 8 46.43 4.97 8 -4 -8 50.23 4.01 -9 4 9 123.71 4.65 9 4 -9 130.89 7.22 -9 -4 9 139.98 7.32 9 -4 -9 132.78 5.53 10 4 -10 -2.80 4.28 -10 4 10 -1.60 2.51 10 -4 -10 -2.10 2.95 11 4 -11 17.87 5.65 -11 4 11 20.69 3.51 -11 -4 11 29.90 5.62 11 -4 -11 27.92 3.98 -12 4 12 3.27 3.74 12 4 -12 11.66 6.78 -12 -4 12 -12.73 6.20 12 -4 -12 5.01 4.49 0 5 0 -0.78 1.23 0 -5 0 -1.34 1.17 1 5 -1 45.66 2.88 -1 -5 1 45.40 2.92 1 -5 -1 45.95 2.57 2 5 -2 241.76 5.26 2 -5 -2 251.08 4.59 -2 -5 2 243.60 5.23 3 5 -3 1.87 1.67 3 -5 -3 2.28 1.13 -3 -5 3 0.11 1.35 4 5 -4 99.18 4.18 -4 -5 4 107.52 4.17 4 -5 -4 105.40 3.29 5 5 -5 -0.62 1.79 5 -5 -5 -0.69 1.36 -5 -5 5 2.46 1.67 6 5 -6 4.42 2.46 6 -5 -6 5.29 1.78 -6 -5 6 3.47 2.32 7 5 -7 6.42 2.94 7 -5 -7 6.18 2.15 -7 -5 7 2.68 2.55 8 5 -8 59.65 5.82 8 -5 -8 66.47 4.38 -8 -5 8 54.73 5.61 9 5 -9 1.71 4.11 9 -5 -9 4.99 2.94 10 5 -10 88.57 8.30 -10 -5 10 96.06 8.67 10 -5 -10 95.17 5.88 11 5 -11 12.11 5.80 11 -5 -11 3.42 3.55 -11 -5 11 0.28 5.38 -12 -5 12 24.50 7.51 0 6 0 7.99 1.71 0 -6 0 6.69 1.72 1 6 -1 60.49 3.27 1 -6 -1 61.38 3.00 -1 -6 1 59.01 3.28 2 6 -2 71.61 3.48 -2 -6 2 72.51 3.64 2 -6 -2 73.84 3.25 3 6 -3 26.10 3.03 3 -6 -3 33.44 2.66 -3 -6 3 29.23 3.00 3 -6 -3 33.03 2.59 4 6 -4 26.53 3.00 -4 -6 4 20.07 2.36 4 -6 -4 18.79 1.96 5 6 -5 117.68 5.09 -5 -6 5 111.75 4.87 5 -6 -5 118.66 3.87 6 6 -6 9.90 2.81 -6 -6 6 11.34 2.71 6 -6 -6 9.05 2.14 7 6 -7 5.70 3.14 -7 -6 7 6.57 2.90 7 -6 -7 5.72 2.17 8 6 -8 0.80 3.44 8 -6 -8 0.69 2.49 9 6 -9 39.92 5.19 -9 -6 9 36.38 5.09 9 -6 -9 37.25 4.91 10 6 -10 9.45 5.24 -10 -6 10 3.56 5.33 10 -6 -10 0.79 3.26 -11 -6 11 18.62 6.40 11 -6 -11 17.43 3.96 0 7 0 0.17 1.46 0 -7 0 0.76 1.46 1 7 -1 149.22 4.73 -1 -7 1 148.32 4.74 1 -7 -1 147.35 4.62 2 7 -2 0.34 1.61 -2 -7 2 0.05 1.80 2 -7 -2 0.46 1.58 3 7 -3 26.37 3.30 -3 -7 3 26.71 3.25 3 -7 -3 28.61 2.89 3 -7 -3 24.63 2.89 4 7 -4 11.66 2.38 4 -7 -4 14.84 2.31 -4 -7 4 12.40 2.19 4 -7 -4 12.92 2.11 5 7 -5 96.49 5.08 5 -7 -5 90.78 4.15 5 -7 -5 86.24 3.89 -5 -7 5 89.27 5.01 6 7 -6 33.66 4.05 -6 -7 6 34.95 4.58 6 -7 -6 33.76 3.58 7 7 -7 36.85 4.36 7 -7 -7 30.15 3.75 -7 -7 7 36.79 4.34 8 7 -8 6.31 4.12 -8 -7 8 8.29 3.85 8 -7 -8 12.16 2.95 9 7 -9 17.57 5.04 9 -7 -9 6.29 3.38 -9 -7 9 2.80 4.92 -10 -7 10 36.50 6.22 10 -7 -10 23.72 4.06 11 7 -11 -5.75 6.93 11 -7 -11 -0.37 4.06 -11 -7 11 4.52 6.99 0 -8 0 184.74 5.43 1 8 -1 -1.26 1.66 -1 -8 1 -1.52 1.52 1 -8 -1 -1.21 1.74 2 8 -2 32.16 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8 -2 -7 75.88 4.63 7 2 -6 52.92 3.97 -7 2 6 58.28 3.56 7 -2 -6 56.25 3.72 -7 -2 6 57.07 4.02 6 2 -5 94.38 4.09 -6 2 5 96.83 3.53 -6 -2 5 102.87 4.11 6 -2 -5 94.99 3.69 -5 2 4 9.30 1.56 5 2 -4 10.40 1.75 5 -2 -4 9.66 1.60 -5 -2 4 11.31 1.79 -4 2 3 27.62 1.99 4 2 -3 25.85 2.28 -4 -2 3 28.26 2.37 4 -2 -3 29.33 2.11 -3 2 2 146.39 2.89 3 2 -2 146.28 3.52 3 -2 -2 148.13 2.97 -3 -2 2 150.27 3.52 -2 2 1 46.02 1.80 2 2 -1 45.76 2.20 -2 -2 1 48.76 2.24 2 -2 -1 47.41 1.83 1 2 0 11.09 1.43 1 -2 0 9.80 1.22 -1 -2 0 11.29 1.44 0 2 1 28.94 1.38 0 -2 -1 28.80 1.36 0 -2 1 29.39 1.52 1 2 -2 6.16 1.05 -1 -2 2 6.49 1.03 1 -2 -2 7.41 0.74 2 2 -3 68.33 2.43 -2 -2 3 67.61 2.37 2 -2 -3 69.02 1.46 -3 2 4 197.86 2.40 3 2 -4 194.96 3.77 -3 -2 4 197.36 3.76 3 -2 -4 192.05 2.49 -4 2 5 44.50 1.70 4 2 -5 43.66 2.55 -4 -2 5 40.55 2.40 4 -2 -5 40.29 1.86 -5 2 6 128.63 2.76 5 2 -6 134.69 3.95 5 -2 -6 134.95 3.05 -5 -2 6 132.26 3.87 -6 2 7 5.09 1.33 6 2 -7 6.25 1.84 -6 -2 7 3.28 1.80 6 -2 -7 6.31 1.44 7 2 -8 19.87 2.54 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3.72 -5 -3 4 154.79 4.51 4 3 -3 5.34 1.52 -4 3 3 4.53 1.23 4 -3 -3 5.62 1.28 -4 -3 3 3.82 1.38 -3 3 2 15.38 1.67 3 3 -2 15.58 1.82 -3 -3 2 17.35 2.14 3 -3 -2 20.16 1.74 2 3 -1 5.81 1.48 2 -3 -1 6.12 1.21 -2 -3 1 5.75 1.38 1 3 0 110.44 2.97 -1 -3 0 112.50 2.98 0 3 1 21.69 1.74 0 -3 -1 22.82 1.72 0 -3 1 22.54 1.92 -1 3 2 2.10 0.95 1 3 -2 3.14 1.33 -1 -3 2 1.65 1.18 1 -3 -2 2.77 0.94 2 3 -3 30.19 2.24 2 -3 -3 34.40 1.60 2 -3 -3 30.93 1.61 -2 -3 3 31.90 2.27 3 3 -4 12.80 1.64 -3 -3 4 13.97 1.68 3 -3 -4 17.27 1.39 4 3 -5 162.80 4.23 -4 3 5 162.95 2.79 -4 -3 5 162.41 4.16 4 -3 -5 162.42 2.86 5 3 -6 -0.39 1.52 -5 3 6 0.02 0.89 5 -3 -6 -0.04 1.19 -5 -3 6 1.23 1.47 6 3 -7 15.16 2.41 -6 3 7 17.65 2.05 6 -3 -7 14.53 1.81 -6 -3 7 18.39 2.45 7 3 -8 6.01 2.45 -7 3 8 5.88 1.53 -7 -3 8 6.20 2.46 7 -3 -8 8.97 1.88 8 3 -9 55.03 4.95 -8 3 9 65.58 3.35 8 -3 -9 61.14 3.54 -8 -3 9 64.33 5.06 9 3 -10 25.78 3.94 -9 3 10 35.04 3.58 -9 -3 10 33.27 3.98 9 -3 -10 31.36 3.67 10 3 -11 8.09 4.09 -10 3 11 9.22 2.68 10 -3 -11 12.96 2.83 -10 -3 11 10.14 3.94 -11 3 12 17.93 3.13 11 -3 -12 21.93 3.41 12 3 -13 10.55 6.38 -12 -3 13 13.73 5.98 12 4 -11 1.05 6.92 -12 4 11 5.33 4.15 12 -4 -11 17.13 4.87 -12 -4 11 6.12 6.31 11 4 -10 10.21 5.64 -11 4 10 1.12 3.49 11 -4 -10 4.14 3.99 -11 -4 10 11.06 5.46 10 4 -9 61.07 7.37 -10 4 9 56.29 5.18 -10 -4 9 64.87 6.92 10 -4 -9 74.39 6.33 9 4 -8 3.25 3.51 -9 4 8 0.77 2.41 9 -4 -8 -0.40 2.72 -9 -4 8 5.02 3.38 -8 4 7 76.10 4.19 8 4 -7 75.02 5.53 8 -4 -7 70.26 4.57 -8 -4 7 69.67 5.59 -7 4 6 4.41 1.86 7 4 -6 7.41 2.72 7 -4 -6 1.42 1.99 -7 -4 6 3.80 2.53 -6 4 5 103.01 3.63 6 4 -5 103.79 4.56 6 -4 -5 102.87 3.84 -6 -4 5 101.95 4.56 5 4 -4 10.98 2.12 -5 4 4 11.48 1.67 -5 -4 4 12.57 2.09 5 -4 -4 10.23 1.65 -4 4 3 213.86 4.14 4 4 -3 208.22 5.02 -4 -4 3 211.93 5.00 4 -4 -3 216.14 4.22 3 4 -2 11.93 1.96 3 -4 -2 9.39 1.43 -3 -4 2 10.57 1.70 2 4 -1 270.35 5.04 2 -4 -1 276.03 4.44 -2 -4 1 271.59 4.98 1 4 0 1.08 1.19 1 -4 0 0.97 1.22 -1 -4 0 -0.38 1.20 0 4 1 80.23 2.77 0 -4 1 78.26 2.93 0 -4 -1 76.84 2.80 1 4 -2 56.30 2.77 -1 4 2 62.36 2.45 1 -4 -2 58.39 2.39 -1 -4 2 61.70 2.80 2 4 -3 16.09 1.84 2 -4 -3 14.11 1.69 -2 -4 3 17.11 2.18 3 4 -4 1.35 1.39 3 -4 -4 -0.26 0.95 -3 -4 4 0.06 1.28 4 4 -5 1.60 1.46 4 -4 -5 0.41 1.00 -4 -4 5 -0.07 1.43 5 4 -6 34.74 3.26 5 -4 -6 37.65 2.24 -5 -4 6 35.25 3.06 6 4 -7 0.54 1.99 6 -4 -7 0.73 1.54 -6 -4 7 -0.82 2.02 -7 4 8 15.75 1.91 7 4 -8 11.75 2.94 7 -4 -8 10.89 2.03 -7 -4 8 12.87 2.81 8 4 -9 65.28 5.52 -8 4 9 66.50 3.33 -8 -4 9 60.57 5.43 8 -4 -9 66.28 3.82 -9 4 10 4.26 1.98 9 4 -10 4.05 3.42 -9 -4 10 8.37 3.78 9 -4 -10 4.27 2.32 10 -4 -11 34.27 4.18 11 4 -12 8.72 5.72 11 -4 -12 8.37 2.98 -11 -4 12 14.22 5.42 12 4 -13 33.62 7.21 -12 -4 13 18.13 6.62 12 5 -11 -7.96 7.07 12 -5 -11 0.51 4.61 -12 -5 11 -11.95 6.55 11 5 -10 32.19 6.54 -11 5 10 30.32 4.25 11 -5 -10 29.04 4.88 -11 -5 10 29.89 6.08 -10 5 9 8.92 3.15 10 5 -9 11.16 5.14 -10 -5 9 4.42 4.37 10 -5 -9 10.02 3.75 9 5 -8 135.21 7.57 -9 5 8 134.07 5.37 -9 -5 8 131.53 7.78 9 -5 -8 128.82 6.03 -8 5 7 7.49 2.30 8 5 -7 6.52 3.44 8 -5 -7 5.40 2.72 -8 -5 7 0.91 2.90 -7 5 6 83.89 3.98 7 5 -6 84.51 5.44 7 -5 -6 81.69 4.22 -7 -5 6 81.27 5.13 6 5 -5 -1.24 2.13 -6 5 5 0.33 1.66 -6 -5 5 3.37 2.19 6 -5 -5 -0.12 1.55 5 5 -4 129.14 4.77 -5 -5 4 132.24 4.73 5 -5 -4 128.27 3.92 4 5 -3 38.23 3.01 4 -5 -3 39.14 2.67 -4 -5 3 39.78 2.97 3 5 -2 96.59 3.83 3 -5 -2 98.78 3.31 -3 -5 2 99.63 3.82 2 5 -1 23.30 2.58 -2 -5 1 23.53 2.52 2 -5 -1 23.46 2.23 1 5 0 400.21 6.16 1 -5 0 408.21 6.01 -1 -5 0 402.79 6.16 0 5 1 19.93 2.18 0 -5 1 20.87 2.35 0 -5 -1 25.31 2.40 1 5 -2 20.19 2.54 -1 -5 2 20.43 2.38 1 -5 -2 20.16 2.14 2 5 -3 26.02 2.53 2 -5 -3 26.69 2.08 -2 -5 3 25.40 2.65 3 5 -4 25.98 2.68 -3 -5 4 27.14 2.70 3 -5 -4 24.04 2.15 3 -5 -4 25.17 2.05 4 5 -5 1.33 1.71 -4 -5 5 2.05 1.68 4 -5 -5 2.53 1.25 5 5 -6 13.78 2.44 -5 -5 6 10.50 2.21 5 -5 -6 13.42 1.67 6 5 -7 4.01 2.47 -6 -5 7 -0.07 2.20 6 -5 -7 2.10 1.47 7 5 -8 39.89 4.73 -7 -5 8 35.55 4.59 7 -5 -8 34.21 3.32 8 5 -9 12.21 3.43 -8 -5 9 0.49 3.15 8 -5 -9 2.06 2.22 9 -5 -10 58.10 4.29 10 5 -11 -2.07 4.71 10 -5 -11 5.85 2.64 -10 -5 11 0.64 4.77 11 5 -12 15.96 6.29 -11 -5 12 11.62 5.67 11 -5 -12 10.35 2.87 -11 -6 10 2.71 6.01 11 -6 -10 7.36 4.57 10 6 -9 63.74 6.73 10 -6 -9 62.20 6.30 -10 -6 9 74.73 8.84 9 6 -8 -2.21 4.10 -9 -6 8 3.83 3.85 9 -6 -8 -1.08 3.11 8 6 -7 30.19 4.28 8 -6 -7 43.11 4.65 -8 -6 7 38.30 4.71 7 6 -6 -1.00 2.91 -7 -6 6 -1.97 2.56 7 -6 -6 -1.74 2.08 6 6 -5 96.56 5.37 6 -6 -5 95.33 4.23 -6 -6 5 97.81 5.02 5 6 -4 9.16 2.40 5 -6 -4 11.05 1.95 -5 -6 4 6.75 2.12 4 6 -3 53.76 3.72 4 -6 -3 58.89 3.19 -4 -6 3 57.29 3.45 3 6 -2 58.07 3.50 -3 -6 2 63.46 3.55 3 -6 -2 61.28 3.12 2 6 -1 133.02 4.44 2 -6 -1 133.30 4.06 -2 -6 1 129.41 4.42 2 -6 -1 134.03 4.08 1 6 0 -1.04 1.37 1 -6 0 0.17 1.22 -1 -6 0 0.10 1.25 0 6 1 34.14 2.70 0 -6 1 35.64 2.83 0 -6 -1 35.82 2.70 1 6 -2 90.28 3.80 -1 -6 2 91.47 3.87 1 -6 -2 90.16 3.42 2 6 -3 28.17 2.94 2 -6 -3 27.06 2.56 -2 -6 3 26.73 2.80 3 6 -4 23.03 2.74 3 -6 -4 21.96 2.38 -3 -6 4 25.63 2.77 3 -6 -4 24.86 2.49 4 6 -5 2.12 1.79 4 -6 -5 -0.41 1.26 -4 -6 5 -1.41 1.67 4 -6 -5 2.49 1.42 5 6 -6 65.65 4.54 5 -6 -6 69.36 3.18 5 -6 -6 68.64 3.21 -5 -6 6 62.95 4.12 6 6 -7 13.67 3.12 6 -6 -7 11.87 1.97 -6 -6 7 13.37 2.92 7 6 -8 5.96 3.30 -7 -6 8 4.42 2.92 7 -6 -8 5.06 2.10 8 6 -9 32.52 4.61 8 -6 -9 31.71 3.97 9 6 -10 15.44 4.61 -9 -6 10 7.95 4.66 9 -6 -10 18.35 2.84 10 6 -11 19.17 5.59 10 -6 -11 18.84 3.11 -10 -6 11 27.38 5.87 11 -6 -12 7.37 2.82 -11 -6 12 11.09 6.65 11 -6 -12 4.47 2.55 11 7 -10 23.54 7.22 11 -7 -10 13.99 4.62 -11 -7 10 14.07 7.34 -10 -7 9 13.84 5.57 10 -7 -9 5.01 4.00 9 7 -8 21.65 5.12 9 -7 -8 19.92 3.89 -9 -7 8 17.96 4.68 8 7 -7 -1.95 3.63 -8 -7 7 -4.48 3.52 8 -7 -7 6.28 2.84 7 7 -6 23.99 3.90 7 -7 -6 20.71 2.93 -7 -7 6 27.92 3.96 6 7 -5 -3.34 2.56 6 -7 -5 0.35 2.05 -6 -7 5 -1.08 2.44 5 7 -4 132.09 5.46 5 -7 -4 138.27 4.77 -5 -7 4 136.84 5.45 4 7 -3 11.46 2.25 4 -7 -3 9.13 2.00 -4 -7 3 12.45 2.30 3 7 -2 5.80 2.04 -3 -7 2 7.00 2.02 3 -7 -2 6.42 1.82 3 -7 -2 5.27 1.97 2 7 -1 119.15 4.47 2 -7 -1 116.42 4.29 -2 -7 1 124.59 4.58 1 7 0 0.93 1.42 -1 -7 0 -0.85 1.36 1 -7 0 -0.03 1.39 0 7 1 122.34 4.21 0 -7 -1 126.80 4.35 0 -7 1 118.52 4.34 1 7 -2 21.40 2.82 1 -7 -2 21.59 2.68 -1 -7 2 22.30 2.77 2 7 -3 94.76 4.28 -2 -7 3 93.98 4.26 2 -7 -3 89.92 3.76 3 7 -4 37.33 3.32 -3 -7 4 42.00 3.44 3 -7 -4 37.92 3.00 3 -7 -4 35.81 2.99 4 7 -5 84.99 4.42 4 -7 -5 87.14 3.70 -4 -7 5 84.81 4.63 4 -7 -5 83.59 3.72 5 7 -6 36.31 4.01 -5 -7 6 34.39 4.22 5 -7 -6 34.68 3.12 5 -7 -6 32.48 3.09 6 7 -7 66.67 5.39 6 -7 -7 73.36 3.81 -6 -7 7 66.42 5.23 6 -7 -7 67.25 3.78 7 7 -8 6.18 3.51 7 -7 -8 8.99 2.27 -7 -7 8 2.99 3.14 7 -7 -8 8.09 2.19 8 7 -9 75.60 7.00 8 -7 -9 72.96 4.09 8 -7 -9 82.03 4.85 -8 -7 9 76.29 6.99 9 7 -10 14.35 4.95 9 -7 -10 14.54 2.63 9 -7 -10 12.06 3.15 -9 -7 10 13.74 5.21 10 -7 -11 17.18 2.91 10 -7 -11 23.47 3.43 -10 -7 11 25.81 6.28 11 7 -12 1.03 7.01 -11 -7 12 3.46 7.49 11 8 -10 13.03 7.97 11 -8 -10 16.60 5.16 -11 -8 10 36.15 8.42 10 8 -9 22.38 6.68 10 -8 -9 11.72 4.79 -10 -8 9 23.69 6.42 -9 -8 8 2.57 4.96 9 -8 -8 6.24 3.76 8 8 -7 11.47 4.25 8 -8 -7 2.67 2.92 -8 -8 7 -0.05 3.79 7 8 -6 23.51 4.04 7 -8 -6 20.78 3.22 -7 -8 6 29.20 4.38 6 8 -5 20.81 3.42 6 -8 -5 18.48 2.71 -6 -8 5 18.03 3.23 5 -8 -4 12.79 2.70 5 -8 -4 16.84 2.63 -5 -8 4 19.32 2.92 4 8 -3 6.76 2.48 4 -8 -3 7.84 2.30 4 -8 -3 8.43 2.46 -4 -8 3 7.15 2.44 3 8 -2 25.45 3.14 3 -8 -2 24.09 3.19 -3 -8 2 22.27 2.75 3 -8 -2 19.75 2.63 2 8 -1 11.52 2.37 2 -8 -1 8.27 2.03 -2 -8 1 5.77 2.07 1 8 0 66.20 3.85 1 -8 0 67.54 3.94 -1 -8 0 63.61 3.82 0 8 1 1.54 1.71 0 -8 1 1.91 1.79 0 -8 -1 1.66 1.73 1 8 -2 134.53 4.98 -1 -8 2 139.67 5.18 1 -8 -2 141.25 4.91 2 8 -3 0.98 1.79 2 -8 -3 1.86 1.71 -2 -8 3 1.70 1.98 3 8 -4 69.65 4.30 -3 -8 4 75.38 4.36 3 -8 -4 72.14 3.80 3 -8 -4 69.64 3.94 4 8 -5 11.90 2.44 4 -8 -5 12.10 2.27 4 -8 -5 11.27 2.08 -4 -8 5 6.45 2.45 5 -8 -6 51.80 3.71 -5 -8 6 52.20 5.30 5 -8 -6 52.05 3.80 6 8 -7 0.83 3.26 6 -8 -7 -1.94 2.12 -6 -8 7 -2.54 3.04 6 -8 -7 -0.45 2.05 7 8 -8 87.17 6.98 7 -8 -8 86.38 4.67 -7 -8 8 95.20 6.91 7 -8 -8 101.23 4.66 8 8 -9 9.94 4.68 8 -8 -9 10.92 2.64 -8 -8 9 22.60 4.90 8 -8 -9 13.77 3.14 -9 -8 10 49.93 6.55 9 -8 -10 50.73 4.65 9 -8 -10 43.03 5.52 10 8 -11 0.48 6.11 -10 -8 11 -2.92 6.33 10 -8 -11 -0.87 3.02 10 -8 -11 2.72 3.26 10 9 -9 0.66 6.70 10 -9 -9 7.33 4.81 10 -9 -9 1.53 4.05 -10 -9 9 5.89 6.96 9 9 -8 3.26 5.75 9 -9 -8 -0.88 3.57 9 -9 -8 7.80 4.01 -9 -9 8 9.81 5.89 8 -9 -7 -1.32 3.27 -8 -9 7 -1.40 4.30 8 -9 -7 -2.95 3.25 7 9 -6 12.05 4.25 7 -9 -6 10.47 2.95 -7 -9 6 14.13 3.93 7 -9 -6 12.68 3.35 6 9 -5 2.63 3.19 6 -9 -5 -2.03 2.72 6 -9 -5 7.13 2.83 -6 -9 5 2.35 2.93 5 9 -4 0.21 2.47 5 -9 -4 0.24 2.52 5 -9 -4 -1.64 2.43 -5 -9 4 -1.37 2.51 4 9 -3 33.98 4.21 4 -9 -3 35.10 4.14 4 -9 -3 30.26 3.90 3 9 -2 5.01 2.59 3 -9 -2 3.97 2.31 3 -9 -2 6.86 2.35 -3 -9 2 6.15 2.41 2 9 -1 55.48 4.23 -2 -9 1 55.02 4.21 2 -9 -1 53.52 4.20 1 9 0 2.63 2.10 -1 -9 0 0.69 1.93 1 -9 0 -0.57 2.00 0 9 1 110.09 4.98 0 -9 -1 109.75 4.96 0 -9 1 122.63 5.13 -1 -9 2 17.83 2.46 1 -9 -2 18.12 2.77 2 9 -3 86.52 4.91 -2 -9 3 83.18 4.89 2 -9 -3 89.13 4.63 3 -9 -4 7.47 2.21 3 -9 -4 5.24 2.24 -3 -9 4 4.39 2.24 4 9 -5 67.54 4.94 4 -9 -5 64.01 4.30 4 -9 -5 66.07 4.18 -4 -9 5 68.21 5.06 5 9 -6 -1.84 2.70 -5 -9 6 2.78 2.79 5 -9 -6 2.28 2.29 5 -9 -6 -2.78 2.04 6 9 -7 85.25 6.75 6 -9 -7 93.14 4.98 -6 -9 7 78.71 6.32 6 -9 -7 91.54 4.79 7 9 -8 -3.16 3.92 7 -9 -8 3.07 2.68 7 -9 -8 1.30 2.74 -7 -9 8 -0.63 3.82 8 -9 -9 49.32 5.03 8 -9 -9 47.37 5.14 -8 -9 9 56.90 6.38 9 9 -10 18.60 6.34 9 -9 -10 12.44 3.86 -9 -9 10 12.49 6.07 9 -9 -10 7.59 3.48 10 9 -11 25.33 7.79 -10 -9 11 12.87 7.59 10 10 -9 8.32 7.53 10 -10 -9 -0.46 4.62 -10 -10 9 2.59 7.85 10 -10 -9 1.94 5.14 9 10 -8 4.62 6.35 -9 -10 8 -14.22 6.05 9 -10 -8 -5.00 4.06 9 -10 -8 5.60 4.30 8 10 -7 9.87 5.45 8 -10 -7 -0.46 4.03 8 -10 -7 4.18 3.91 -8 -10 7 6.46 5.21 7 10 -6 4.21 4.03 -7 -10 6 0.71 4.10 7 -10 -6 -0.67 3.09 7 -10 -6 -4.05 3.15 6 10 -5 20.83 4.02 -6 -10 5 14.05 3.63 6 -10 -5 10.91 3.24 6 -10 -5 19.49 3.61 5 10 -4 8.26 2.90 5 -10 -4 -2.47 2.64 5 -10 -4 3.08 2.88 -5 -10 4 -2.04 2.98 4 10 -3 71.56 5.25 -4 -10 3 78.15 5.25 4 -10 -3 72.33 5.48 4 -10 -3 74.83 5.18 3 10 -2 34.59 4.41 3 -10 -2 40.54 4.57 -3 -10 2 31.71 3.45 3 -10 -2 33.58 4.29 2 -10 -1 20.85 3.11 1 10 0 39.91 4.10 1 -10 0 35.53 4.23 -1 -10 0 37.48 3.95 0 -10 -1 32.69 4.19 0 -10 1 38.12 3.92 1 -10 -2 79.86 5.08 2 10 -3 1.80 2.52 2 -10 -3 4.55 2.55 -2 -10 3 0.80 2.44 3 10 -4 155.33 6.61 3 -10 -4 150.41 5.98 -3 -10 4 145.10 6.31 3 -10 -4 143.83 5.76 4 10 -5 2.36 2.79 -4 -10 5 2.68 2.96 4 -10 -5 -1.00 2.64 4 -10 -5 1.64 2.39 5 10 -6 69.12 6.15 5 -10 -6 70.17 4.97 5 -10 -6 80.46 5.33 -5 -10 6 85.32 6.02 6 10 -7 8.89 4.11 6 -10 -7 9.91 3.00 -6 -10 7 4.67 3.93 6 -10 -7 9.38 3.14 7 10 -8 43.12 6.03 7 -10 -8 38.33 4.07 7 -10 -8 42.56 5.33 -7 -10 8 48.92 6.07 8 10 -9 6.70 5.82 8 -10 -9 -1.24 3.18 8 -10 -9 0.84 3.20 -8 -10 9 -3.94 5.41 9 10 -10 17.83 6.90 9 -10 -10 22.52 4.38 9 -10 -10 20.92 4.00 -9 -10 10 30.76 7.50 9 11 -8 27.97 7.72 -9 -11 8 15.16 7.44 8 11 -7 3.02 5.68 -8 -11 7 2.84 6.12 7 11 -6 49.02 5.78 -7 -11 6 45.96 5.81 6 11 -5 0.09 3.71 6 -11 -5 -2.74 3.49 -6 -11 5 -0.80 3.54 -5 -11 4 16.48 3.80 5 -11 -4 13.90 3.87 4 11 -3 12.52 3.48 -4 -11 3 17.90 3.53 3 11 -2 40.70 5.10 -3 -11 2 37.69 4.97 2 11 -1 15.59 3.20 -2 -11 1 10.56 2.97 1 11 0 38.94 5.00 -1 -11 0 42.06 4.73 1 -11 0 38.13 4.88 0 -11 1 21.99 3.54 0 -11 -1 23.21 3.65 -1 -11 2 15.81 3.05 2 -11 -3 38.41 4.09 -2 -11 3 38.89 4.20 3 11 -4 7.72 3.39 3 -11 -4 1.13 2.76 3 -11 -4 0.36 2.87 -3 -11 4 1.78 2.84 4 11 -5 111.75 6.46 4 -11 -5 118.75 6.32 4 -11 -5 108.11 5.96 -4 -11 5 109.75 6.60 5 -11 -6 12.78 3.27 5 -11 -6 11.92 3.39 -5 -11 6 13.58 3.65 6 11 -7 34.71 5.44 -6 -11 7 41.08 5.22 6 -11 -7 42.54 5.63 6 -11 -7 52.02 5.92 7 11 -8 10.21 5.51 7 -11 -8 4.22 3.60 7 -11 -8 4.51 3.57 -7 -11 8 -3.01 5.10 8 11 -9 27.03 6.79 8 -11 -9 22.38 4.54 -8 -11 9 30.16 7.08 8 -11 -9 30.64 4.42 9 11 -10 4.96 7.84 -9 -11 10 20.65 8.22 9 -11 -10 8.78 4.77 8 12 -7 69.55 8.40 8 -12 -7 80.73 8.73 -8 -12 7 102.20 11.63 8 -12 -7 74.68 8.58 7 12 -6 10.43 5.32 -7 -12 6 -4.64 5.17 7 -12 -6 9.33 4.56 7 -12 -6 17.28 4.75 6 12 -5 39.02 5.63 -6 -12 5 34.69 4.96 6 -12 -5 39.39 5.06 6 -12 -5 36.81 5.34 5 12 -4 1.06 3.84 -5 -12 4 -4.68 3.73 5 -12 -4 0.06 3.66 5 -12 -4 -1.97 4.01 4 12 -3 78.70 6.44 4 -12 -3 58.36 6.57 -4 -12 3 71.85 6.42 4 -12 -3 80.61 6.44 3 12 -2 3.18 3.61 3 -12 -2 1.66 3.30 -3 -12 2 8.07 3.06 3 -12 -2 1.68 3.45 2 12 -1 73.72 6.29 2 -12 -1 72.99 5.74 2 -12 -1 76.51 6.43 -2 -12 1 60.87 6.00 1 -12 0 15.39 3.63 -1 -12 0 20.22 3.86 0 -12 1 24.35 4.05 0 -12 -1 29.56 4.30 -1 -12 2 8.72 3.30 1 -12 -2 20.02 4.04 2 -12 -3 -1.94 3.22 -2 -12 3 -3.21 2.73 -3 -12 4 16.75 3.99 3 -12 -4 18.73 4.24 3 -12 -4 21.28 3.88 4 12 -5 34.82 4.58 4 -12 -5 22.99 4.46 -4 -12 5 29.59 4.60 4 -12 -5 26.63 4.08 5 12 -6 17.45 4.48 -5 -12 6 21.77 4.48 6 12 -7 7.14 5.19 -6 -12 7 -6.24 4.85 7 12 -8 19.50 6.14 7 -12 -8 11.37 4.52 7 -12 -8 9.75 4.76 -7 -12 8 2.45 5.98 8 12 -9 12.77 7.61 -8 -12 9 2.47 7.28 8 -12 -9 1.25 4.80 8 -12 -9 4.39 4.77 7 13 -6 61.36 7.47 7 -13 -6 54.26 6.51 7 -13 -6 91.25 9.12 -7 -13 6 81.73 10.26 6 13 -5 0.95 4.79 -6 -13 5 -1.17 4.70 6 -13 -5 7.49 4.80 6 -13 -5 -8.05 4.68 5 13 -4 46.64 5.74 5 -13 -4 44.05 5.86 -5 -13 4 38.52 5.32 5 -13 -4 43.31 5.47 4 13 -3 10.73 4.06 4 -13 -3 3.96 4.60 4 -13 -3 2.37 3.93 -4 -13 3 -0.19 3.96 3 13 -2 113.83 7.73 3 -13 -2 123.65 8.22 -3 -13 2 125.99 7.84 3 -13 -2 117.42 7.71 2 -13 -1 -1.20 3.83 -2 -13 1 -3.32 3.44 2 -13 -1 5.91 3.65 -1 -13 0 103.68 7.49 1 -13 0 115.45 7.90 0 -13 -1 7.82 3.93 0 -13 1 1.04 3.79 -1 -13 2 24.95 4.49 1 -13 -2 21.27 4.24 -2 -13 3 8.57 3.67 2 -13 -3 -2.86 3.71 3 -13 -4 3.22 4.08 -3 -13 4 -3.00 3.86 3 -13 -4 -6.18 3.62 4 -13 -5 4.00 4.11 4 -13 -5 2.45 3.85 -4 -13 5 -3.30 4.09 5 13 -6 3.94 4.53 -5 -13 6 3.70 4.55 5 -13 -6 2.54 4.44 5 -13 -6 3.17 4.51 6 13 -7 11.24 5.56 6 -13 -7 -0.11 4.43 -6 -13 7 -10.58 5.59 6 -13 -7 0.72 4.59 7 -13 -8 -0.02 5.04 7 -13 -8 7.69 5.07 6 -14 -5 45.64 7.00 6 -14 -5 53.80 6.91 5 14 -4 0.74 5.30 -5 -14 4 -4.64 5.48 5 -14 -4 -0.13 5.27 5 -14 -4 1.92 5.27 4 14 -3 68.37 7.90 4 -14 -3 51.44 6.31 4 -14 -3 87.02 8.50 -4 -14 3 58.43 7.72 -3 -14 2 16.57 4.56 3 -14 -2 17.44 4.88 3 -14 -2 21.87 5.73 -2 -14 1 26.18 5.29 2 -14 -1 24.14 5.15 2 -14 -1 14.21 5.20 -1 -14 0 -6.57 4.41 1 -14 0 -4.44 4.52 0 -14 1 25.24 5.38 0 -14 -1 18.25 4.94 -1 -14 2 2.14 4.09 1 -14 -2 5.43 4.43 -2 -14 3 19.48 4.76 2 -14 -3 21.29 5.31 3 -14 -4 6.82 4.97 -3 -14 4 -2.17 4.82 -4 -14 5 12.82 5.09 4 -14 -5 -1.85 4.81 4 -14 -5 15.11 4.71 5 -14 -6 11.09 5.39 -5 -14 6 10.16 5.63 5 -14 -6 8.09 5.39 6 -14 -7 -0.79 5.40 6 -14 -7 -3.55 5.37 5 -15 -4 33.35 6.92 5 -15 -4 29.93 7.24 4 -15 -3 2.79 5.52 4 -15 -3 -9.50 6.28 3 -15 -2 32.12 6.19 -3 -15 2 27.26 5.85 3 -15 -2 30.71 6.43 2 -15 -1 21.39 5.85 -2 -15 1 24.46 5.78 2 -15 -1 18.67 6.54 1 -15 0 3.09 6.00 -1 -15 0 1.54 5.91 0 -15 -1 13.31 6.31 0 -15 1 15.80 6.13 1 -15 -2 24.83 6.20 -1 -15 2 30.27 6.05 -2 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1.66 -2 -1 0 13.79 1.66 2 -1 0 11.78 1.51 -1 1 -1 38.11 1.48 -1 -1 -1 38.30 1.63 0 1 -2 10.15 1.15 1 -1 -3 0.39 0.34 -1 -1 3 0.07 0.68 2 1 -4 182.64 2.78 -2 -1 4 183.41 2.81 3 1 -5 20.48 1.71 -3 1 5 20.38 1.01 -3 -1 5 18.94 1.67 3 -1 -5 20.50 0.97 -4 1 6 5.86 0.93 4 1 -6 4.97 1.19 -4 -1 6 5.76 1.19 4 -1 -6 5.23 0.86 5 1 -7 10.15 1.60 -5 1 7 12.25 1.32 -5 -1 7 9.00 1.59 5 -1 -7 11.17 1.22 6 1 -8 -0.61 1.52 -6 1 8 0.04 1.32 -6 -1 8 1.10 1.57 6 -1 -8 -0.39 1.17 7 1 -9 93.03 4.06 -7 1 9 99.22 3.49 -7 -1 9 97.59 4.08 7 -1 -9 92.04 3.17 -8 1 10 2.99 1.95 8 1 -10 -1.18 2.22 -8 -1 10 3.34 2.34 8 -1 -10 3.98 1.92 9 1 -11 29.78 3.38 -9 1 11 33.16 3.97 9 -1 -11 35.30 3.92 -9 -1 11 33.59 3.61 -10 1 12 0.45 2.68 10 1 -12 5.21 3.35 10 -1 -12 -1.31 2.74 -10 -1 12 -1.20 3.04 11 1 -13 31.18 4.79 -11 1 13 26.91 3.72 -11 -1 13 27.19 4.30 11 -1 -13 33.38 3.96 12 1 -14 4.61 5.03 -12 -1 14 2.85 5.03 -12 2 10 19.98 5.00 12 2 -10 21.08 6.46 12 -2 -10 23.04 5.61 -12 -2 10 28.81 5.71 -11 2 9 2.18 3.78 11 2 -9 6.21 5.07 11 -2 -9 3.55 4.39 -11 -2 9 -3.76 4.42 -10 2 8 15.71 3.59 10 2 -8 10.90 4.34 10 -2 -8 10.64 3.86 -10 -2 8 10.06 3.78 -9 2 7 42.45 4.55 9 2 -7 44.87 5.53 -9 -2 7 37.72 4.16 9 -2 -7 46.14 5.12 -8 2 6 18.63 2.91 8 2 -6 25.77 3.41 8 -2 -6 19.12 3.00 -8 -2 6 26.23 3.43 -7 2 5 35.13 3.38 7 2 -5 39.23 3.91 -7 -2 5 32.83 3.74 7 -2 -5 39.64 3.75 6 2 -4 37.88 3.23 -6 2 4 35.74 3.03 -6 -2 4 39.54 3.30 6 -2 -4 28.52 3.03 5 2 -3 153.63 4.35 -5 2 3 152.27 3.97 5 -2 -3 147.65 4.05 -5 -2 3 150.44 4.38 4 2 -2 9.32 1.63 -4 2 2 9.94 1.48 4 -2 -2 8.08 1.43 -4 -2 2 9.93 1.61 3 2 -1 73.32 2.91 -3 2 1 76.85 2.55 -3 -2 1 74.66 2.90 3 -2 -1 76.83 2.61 -2 2 0 -0.24 0.87 2 2 0 0.05 1.05 -2 -2 0 -0.93 1.04 2 -2 0 0.08 0.88 1 2 1 100.03 2.42 -1 2 -1 94.72 2.33 -1 -2 -1 100.87 2.48 1 -2 1 97.67 2.43 0 2 2 4.45 0.83 0 -2 -2 5.10 0.84 -1 2 3 377.81 2.86 -1 -2 3 363.17 4.29 1 -2 -3 367.57 2.83 2 2 -4 -1.12 0.98 -2 -2 4 0.28 1.03 2 -2 -4 0.60 0.45 2 -2 -4 0.56 0.47 3 2 -5 63.91 2.50 3 -2 -5 61.25 1.27 -3 -2 5 59.95 2.49 -4 2 6 70.53 1.51 4 2 -6 70.05 2.82 4 -2 -6 69.76 1.60 -4 -2 6 64.59 2.75 5 2 -7 38.92 2.85 -5 2 7 42.69 1.70 -5 -2 7 37.86 2.69 5 -2 -7 39.96 1.70 6 2 -8 29.61 3.05 -6 2 8 30.81 1.97 6 -2 -8 35.44 1.99 -6 -2 8 29.45 3.07 7 2 -9 16.40 2.57 -7 2 9 17.46 2.21 7 -2 -9 18.83 2.17 -7 -2 9 18.91 2.53 -8 2 10 38.89 2.98 8 2 -10 40.80 4.22 8 -2 -10 36.91 2.92 -8 -2 10 44.34 4.22 9 2 -11 5.35 3.02 -9 2 11 1.25 1.95 9 -2 -11 0.60 2.02 -9 -2 11 -0.54 2.73 10 2 -12 38.81 4.43 -10 2 12 37.94 3.85 -10 -2 12 31.82 4.42 10 -2 -12 29.63 3.08 -11 2 13 3.40 2.78 11 2 -13 -0.66 4.52 11 -2 -13 4.39 3.04 -11 -2 13 -3.25 4.01 12 2 -14 18.64 5.55 -12 -2 14 18.06 5.28 12 3 -10 4.76 6.70 -12 3 10 2.81 4.70 12 -3 -10 3.78 5.16 -12 -3 10 -2.65 5.45 11 3 -9 25.01 5.64 -11 3 9 17.07 4.28 11 -3 -9 15.46 4.60 -11 -3 9 13.22 5.14 -10 3 8 21.26 3.84 10 -3 -8 29.81 4.30 -9 3 7 -0.28 2.53 9 3 -7 4.74 3.36 9 -3 -7 1.66 2.95 -9 -3 7 5.59 3.30 -8 3 6 20.79 2.76 8 3 -6 20.89 3.41 -8 -3 6 22.66 3.33 8 -3 -6 17.57 3.05 -7 3 5 55.54 3.69 7 3 -5 48.70 4.27 7 -3 -5 52.14 3.93 -7 -3 5 58.21 4.43 6 3 -4 124.37 4.76 -6 3 4 130.92 4.15 6 -3 -4 120.55 4.15 -6 -3 4 132.18 4.82 5 3 -3 4.03 1.60 -5 3 3 2.11 1.39 5 -3 -3 0.56 1.33 -5 -3 3 -0.06 1.42 -4 3 2 254.56 4.49 4 3 -2 264.72 5.31 -4 -3 2 254.73 5.25 4 -3 -2 251.38 4.54 3 3 -1 37.49 2.59 -3 3 1 39.61 2.22 -3 -3 1 42.39 2.69 3 -3 -1 43.64 2.29 -2 3 0 198.36 3.62 2 3 0 195.12 4.03 2 -3 0 195.37 3.65 -2 -3 0 193.96 4.04 1 3 1 1.13 1.23 -1 -3 -1 0.92 1.07 1 -3 1 -0.22 1.14 0 3 2 114.78 2.70 0 -3 -2 114.47 2.69 -1 3 3 7.68 1.04 1 -3 -3 7.52 1.06 -1 -3 3 5.88 1.35 2 3 -4 22.11 2.08 -2 -3 4 21.97 2.21 2 -3 -4 22.39 1.35 3 3 -5 30.75 2.42 -3 -3 5 33.05 2.37 3 -3 -5 35.78 1.35 3 -3 -5 34.73 1.38 4 3 -6 68.60 3.22 4 -3 -6 70.06 1.87 -4 -3 6 77.61 3.26 5 3 -7 22.83 2.80 5 -3 -7 17.97 1.67 -5 -3 7 22.35 2.69 6 3 -8 52.01 3.63 -6 3 8 41.46 1.98 6 -3 -8 48.26 2.13 -6 -3 8 45.73 3.61 7 3 -9 9.96 2.62 -7 3 9 8.82 1.38 -7 -3 9 6.89 2.47 7 -3 -9 11.58 1.50 -8 3 10 0.61 1.49 8 3 -10 1.87 2.81 8 -3 -10 2.44 1.53 -8 -3 10 5.83 2.71 -9 3 11 2.67 1.67 9 3 -11 2.85 3.20 9 -3 -11 5.51 1.95 -9 -3 11 6.08 3.31 -10 3 12 2.69 1.98 10 3 -12 0.95 4.11 -10 -3 12 5.13 3.98 10 -3 -12 0.55 2.20 11 3 -13 21.95 5.44 11 -3 -13 19.04 2.70 -11 -3 13 15.91 5.14 12 4 -10 -0.42 7.00 -12 4 10 -0.60 4.57 -12 -4 10 1.88 6.18 12 -4 -10 12.16 5.32 11 4 -9 19.14 5.94 -11 4 9 18.59 4.16 11 -4 -9 14.52 4.75 -11 -4 9 10.66 5.26 -10 4 8 9.88 3.37 10 4 -8 12.57 4.73 -10 -4 8 16.37 4.50 10 -4 -8 15.73 3.76 -9 4 7 31.20 3.43 -9 -4 7 30.55 4.20 9 -4 -7 27.57 3.77 -8 4 6 5.87 2.34 8 4 -6 5.41 3.06 -8 -4 6 5.66 3.15 8 -4 -6 2.75 2.52 -7 4 5 46.32 3.54 7 4 -5 47.20 4.56 -7 -4 5 50.13 4.53 7 -4 -5 42.10 3.76 6 4 -4 6.49 2.32 -6 4 4 3.69 1.64 -6 -4 4 0.71 1.96 6 -4 -4 1.54 1.69 5 4 -3 103.35 4.27 -5 4 3 106.20 3.63 5 -4 -3 104.87 3.66 -5 -4 3 103.01 4.14 -4 4 2 10.42 1.60 4 4 -2 10.63 1.86 -4 -4 2 10.96 1.86 4 -4 -2 9.07 1.58 -3 4 1 213.43 4.21 3 4 -1 217.06 4.95 3 -4 -1 213.61 4.29 -3 -4 1 220.75 4.91 2 4 0 5.64 1.63 2 -4 0 3.34 1.19 -2 -4 0 2.35 1.37 1 4 1 535.35 6.35 1 -4 1 551.64 6.52 -1 -4 -1 547.07 6.40 0 4 2 13.56 1.56 0 -4 2 11.94 1.65 0 -4 -2 12.50 1.46 1 4 -3 77.68 3.07 -1 4 3 83.06 2.57 1 -4 -3 79.82 2.51 -1 -4 3 81.55 3.17 2 4 -4 7.29 1.50 2 -4 -4 8.67 1.18 -2 -4 4 7.30 1.57 3 4 -5 107.44 3.67 -3 -4 5 108.41 3.74 3 -4 -5 111.47 2.41 3 -4 -5 109.79 2.43 4 4 -6 20.38 2.66 -4 -4 6 18.95 2.24 4 -4 -6 20.04 1.60 4 -4 -6 19.57 1.57 5 4 -7 58.65 3.72 -5 -4 7 59.29 3.65 5 -4 -7 65.87 2.36 6 4 -8 30.06 3.25 6 -4 -8 28.41 2.27 -6 -4 8 30.77 3.63 7 4 -9 27.05 3.36 7 -4 -9 30.40 2.46 -7 -4 9 28.25 3.23 8 4 -10 -0.34 2.86 -8 -4 10 -3.25 2.68 8 -4 -10 2.87 1.58 9 4 -11 2.73 3.70 -9 -4 11 5.18 3.68 9 -4 -11 0.85 1.69 -10 -4 12 5.39 4.25 11 4 -13 9.66 5.42 -11 -4 13 7.39 5.26 12 5 -10 -3.13 7.55 -12 5 10 -2.07 4.47 -12 -5 10 -6.78 6.70 12 -5 -10 -11.68 5.31 -11 5 9 0.05 3.81 11 5 -9 -0.23 6.09 11 -5 -9 5.27 4.42 -11 -5 9 6.52 5.59 10 5 -8 40.10 5.80 -10 5 8 32.52 3.94 10 -5 -8 32.38 4.45 -10 -5 8 37.92 5.24 -9 5 7 -2.12 2.50 9 5 -7 0.68 3.72 -9 -5 7 2.48 3.66 9 -5 -7 2.12 3.07 8 5 -6 80.45 6.01 -8 5 6 74.77 4.58 -8 -5 6 84.00 5.80 8 -5 -6 75.60 4.99 -7 5 5 1.10 1.98 7 5 -5 2.36 2.67 -7 -5 5 -1.62 2.51 7 -5 -5 2.37 2.14 -6 5 4 171.71 4.85 6 5 -4 176.85 5.80 -6 -5 4 164.86 5.76 6 -5 -4 169.17 4.97 -5 5 3 3.47 1.60 5 5 -3 2.66 1.81 5 -5 -3 2.92 1.62 -5 -5 3 4.15 1.74 4 5 -2 193.38 5.24 -4 -5 2 192.13 5.20 4 -5 -2 194.79 4.60 3 5 -1 13.18 2.18 -3 -5 1 13.20 1.95 3 -5 -1 11.43 1.67 2 5 0 248.71 5.24 2 -5 0 234.47 4.78 -2 -5 0 244.17 5.24 1 5 1 0.69 1.33 -1 -5 -1 0.13 1.34 1 -5 1 -0.76 1.28 0 5 2 402.82 5.73 0 -5 -2 410.26 5.81 0 -5 2 415.80 6.37 -1 5 3 162.67 3.74 1 -5 -3 159.72 3.71 -1 -5 3 166.17 4.41 2 5 -4 181.04 4.65 -2 -5 4 180.29 4.73 2 -5 -4 180.96 3.65 3 5 -5 53.91 3.26 3 -5 -5 52.37 2.34 -3 -5 5 50.36 3.17 3 -5 -5 53.46 2.35 4 5 -6 118.78 4.35 4 -5 -6 121.41 2.98 -4 -5 6 125.40 4.68 4 -5 -6 123.58 2.99 5 5 -7 87.63 4.34 -5 -5 7 79.76 4.29 5 -5 -7 79.53 2.66 5 -5 -7 87.35 2.71 6 5 -8 110.67 5.30 -6 -5 8 114.40 5.25 6 -5 -8 117.43 3.37 6 -5 -8 116.75 3.02 7 5 -9 0.01 2.76 -7 -5 9 6.09 2.75 7 -5 -9 0.86 1.69 8 5 -10 -0.45 3.29 8 -5 -10 0.37 1.69 -8 -5 10 -2.00 3.13 9 -5 -11 6.31 1.76 10 5 -12 4.57 4.72 -10 -5 12 9.04 5.20 11 5 -13 9.42 5.93 -11 -5 13 15.25 5.89 12 6 -10 5.13 7.91 -12 -6 10 15.95 7.99 12 -6 -10 13.93 5.69 11 6 -9 0.70 6.58 11 -6 -9 10.78 4.64 -11 -6 9 7.87 5.76 -10 6 8 1.34 3.28 10 6 -8 -1.39 5.19 -10 -6 8 11.94 5.16 10 -6 -8 5.68 3.91 -9 6 7 28.53 3.67 9 6 -7 27.53 5.16 -9 -6 7 31.74 4.82 9 -6 -7 30.16 4.10 -8 6 6 23.17 3.19 8 6 -6 15.34 3.95 -8 -6 6 17.24 3.82 8 -6 -6 18.49 3.23 7 6 -5 78.14 5.82 7 -6 -5 70.52 4.50 -7 -6 5 68.48 5.44 6 6 -4 21.87 3.10 6 -6 -4 21.10 2.69 -6 -6 4 21.32 3.01 5 6 -3 198.08 5.88 5 -6 -3 209.58 5.31 -5 -6 3 200.14 5.90 4 6 -2 0.27 1.82 -4 -6 2 1.24 1.61 4 -6 -2 1.78 1.57 3 6 -1 224.73 5.73 -3 -6 1 225.22 5.64 3 -6 -1 224.66 5.15 2 6 0 0.75 1.41 -2 -6 0 1.64 1.57 2 -6 0 -1.35 1.34 1 6 1 187.75 4.77 1 -6 1 189.45 4.84 -1 -6 -1 188.96 4.86 0 6 2 3.23 1.36 0 -6 -2 1.80 1.32 0 -6 2 -0.87 1.32 -1 6 3 200.99 4.53 1 -6 -3 197.77 4.51 -1 -6 3 190.91 5.06 2 6 -4 12.17 2.02 2 -6 -4 12.75 1.75 -2 -6 4 10.37 1.89 3 6 -5 98.98 4.13 -3 -6 5 100.05 4.16 3 -6 -5 104.42 3.32 3 -6 -5 102.11 3.32 4 6 -6 78.04 4.11 4 -6 -6 79.06 2.99 4 -6 -6 84.08 3.04 -4 -6 6 80.37 4.30 5 6 -7 24.52 3.06 5 -6 -7 26.34 2.45 -5 -6 7 34.53 3.89 5 -6 -7 23.49 2.43 6 6 -8 47.51 4.79 -6 -6 8 44.67 4.60 6 -6 -8 41.90 2.73 6 -6 -8 42.12 2.84 7 6 -9 17.49 3.64 7 -6 -9 15.91 2.23 -7 -6 9 13.32 3.34 7 -6 -9 16.23 1.93 8 6 -10 6.89 4.19 8 -6 -10 6.18 1.78 8 -6 -10 6.69 2.02 9 6 -11 1.85 4.26 9 -6 -11 1.27 1.88 -9 -6 11 -8.64 4.29 9 -6 -11 -0.35 1.71 10 6 -12 30.52 6.09 -10 -6 12 28.43 5.86 11 6 -13 -3.33 6.80 -11 -6 13 2.25 6.70 11 7 -9 36.55 7.89 -11 -7 9 52.07 8.04 11 -7 -9 39.21 5.62 10 -7 -8 8.06 4.38 -10 -7 8 17.01 5.95 9 7 -7 75.05 8.15 9 -7 -7 73.79 6.36 -9 -7 7 82.75 7.80 8 7 -6 -0.62 3.87 -8 -7 6 1.30 3.53 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23.20 2.86 -1 -9 -1 22.07 2.88 0 9 2 -0.32 2.02 0 -9 -2 0.17 1.94 0 -9 2 -1.52 1.90 -1 -9 3 113.01 5.14 1 -9 -3 104.94 4.89 2 -9 -4 5.05 2.33 -2 -9 4 5.40 2.39 -3 -9 5 41.44 4.77 3 -9 -5 40.24 3.93 4 9 -6 3.72 2.63 4 -9 -6 0.45 1.88 -4 -9 6 -1.01 2.37 4 -9 -6 3.30 2.18 5 9 -7 77.94 5.85 5 -9 -7 74.36 4.41 5 -9 -7 80.26 4.59 -5 -9 7 83.70 6.03 6 9 -8 29.48 4.44 -6 -9 8 21.85 4.52 6 -9 -8 27.85 3.07 6 -9 -8 24.38 2.93 7 9 -9 82.18 7.73 7 -9 -9 92.64 4.91 7 -9 -9 78.67 5.00 -7 -9 9 90.09 7.91 8 9 -10 2.24 5.70 -8 -9 10 -2.80 5.01 8 -9 -10 2.07 2.91 8 -9 -10 1.89 2.73 9 9 -11 74.96 8.05 9 -9 -11 67.92 5.34 -9 -9 11 86.14 10.54 9 -9 -11 72.63 5.00 10 9 -12 8.62 7.93 -10 -9 12 -15.53 7.40 10 10 -8 29.36 8.30 -10 -10 8 10.18 7.27 9 10 -7 2.55 6.20 -9 -10 7 -0.03 5.70 8 10 -6 40.60 6.53 -8 -10 6 28.80 5.57 8 -10 -6 36.01 5.11 8 -10 -6 34.03 4.89 7 10 -5 3.69 4.13 -7 -10 5 6.75 4.15 7 -10 -5 -1.90 3.33 7 -10 -5 8.65 3.68 6 10 -4 25.97 3.94 -6 -10 4 26.88 4.04 6 -10 -4 25.58 3.74 6 -10 -4 20.99 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6.12 3.96 6 -12 -8 0.32 3.78 7 12 -9 12.65 6.57 -7 -12 9 15.13 6.74 7 -12 -9 15.46 4.38 7 -12 -9 11.16 4.57 8 12 -10 14.64 8.40 8 -12 -10 7.99 4.64 8 -12 -10 10.65 5.01 -8 -12 10 2.23 8.23 7 13 -5 -3.55 5.96 7 -13 -5 2.86 5.47 -7 -13 5 -4.84 5.72 7 -13 -5 7.16 5.27 6 13 -4 9.21 5.22 -6 -13 4 5.46 4.68 6 -13 -4 5.08 5.20 6 -13 -4 10.39 5.10 5 13 -3 3.91 4.48 -5 -13 3 3.95 4.11 5 -13 -3 -3.17 4.27 5 -13 -3 0.03 4.68 4 13 -2 95.21 7.57 4 -13 -2 104.74 7.93 4 -13 -2 90.01 8.22 -4 -13 2 83.23 7.26 3 13 -1 12.83 3.97 3 -13 -1 11.72 4.53 3 -13 -1 11.75 4.14 -3 -13 1 6.90 4.00 2 13 0 41.40 5.36 2 -13 0 35.96 4.88 2 -13 0 61.92 7.19 -2 -13 0 60.32 6.75 -1 -13 -1 10.88 4.35 1 -13 1 19.41 4.52 0 -13 -2 70.08 7.13 0 -13 2 63.37 6.84 -1 -13 3 -0.64 3.48 1 -13 -3 0.81 3.89 -2 -13 4 33.72 4.46 2 -13 -4 37.23 4.98 -3 -13 5 3.74 4.09 3 -13 -5 0.07 3.79 3 -13 -5 4.67 3.77 4 -13 -6 57.92 7.04 4 -13 -6 49.13 5.41 -4 -13 6 56.45 5.88 5 -13 -7 -0.79 4.30 -5 -13 7 8.27 4.92 5 -13 -7 -4.18 4.11 6 -13 -8 4.25 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1.95 8 0 -11 0.36 1.92 9 0 -12 50.79 4.09 -9 0 12 51.22 4.19 10 0 -13 3.05 2.96 -10 0 13 2.03 2.98 -11 0 14 14.29 3.72 11 0 -14 20.61 3.74 -13 1 10 -1.41 6.02 13 1 -10 2.96 7.55 -13 -1 10 13.47 6.74 13 -1 -10 -1.18 6.72 12 1 -9 43.87 6.99 -12 -1 9 33.45 5.94 12 -1 -9 43.98 6.51 -11 1 8 -1.86 3.88 11 1 -8 4.76 5.14 11 -1 -8 1.68 4.55 -10 1 7 37.41 4.30 10 1 -7 40.83 4.92 10 -1 -7 33.43 4.71 -10 -1 7 40.53 4.59 -9 1 6 2.40 2.81 9 1 -6 1.93 3.27 9 -1 -6 2.20 3.28 -9 -1 6 -1.68 2.70 -8 1 5 72.76 4.57 8 1 -5 62.90 5.01 -8 -1 5 63.99 4.77 8 -1 -5 75.94 4.98 -7 1 4 8.33 2.12 7 1 -4 2.21 2.27 -7 -1 4 3.78 2.16 7 -1 -4 5.16 2.22 6 1 -3 115.56 4.49 -6 1 3 110.28 4.14 6 -1 -3 113.31 4.25 -6 -1 3 110.78 4.34 -5 1 2 3.42 1.52 5 1 -2 4.58 1.64 -5 -1 2 5.75 1.73 5 -1 -2 2.75 1.56 4 1 -1 131.20 3.86 -4 1 1 130.48 3.68 4 -1 -1 134.57 3.82 -4 -1 1 134.82 3.86 -3 1 0 66.25 2.65 3 1 0 62.17 2.90 -3 -1 0 66.43 2.82 3 -1 0 67.79 2.76 2 1 1 1.57 1.19 -2 1 -1 1.53 1.08 -2 -1 -1 3.56 1.27 2 -1 1 1.19 1.04 -1 1 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24.83 5.03 -10 2 7 1.00 3.17 10 2 -7 7.77 4.27 -10 -2 7 3.99 3.62 10 -2 -7 4.12 3.88 9 2 -6 1.51 3.46 -9 2 6 -0.40 2.68 -9 -2 6 2.11 2.96 9 -2 -6 -1.38 2.96 8 2 -5 0.03 2.62 -8 2 5 0.01 2.19 8 -2 -5 -0.62 2.53 -8 -2 5 0.04 2.66 7 2 -4 96.36 4.82 -7 2 4 89.29 4.39 -7 -2 4 98.67 4.74 7 -2 -4 93.48 4.60 6 2 -3 29.17 3.12 -6 2 3 26.95 3.01 6 -2 -3 27.45 3.17 -6 -2 3 25.50 3.14 5 2 -2 107.18 3.96 -5 2 2 110.92 3.75 -5 -2 2 112.66 4.04 5 -2 -2 106.58 3.80 4 2 -1 5.72 1.71 -4 2 1 6.24 1.34 4 -2 -1 5.46 1.37 -4 -2 1 7.05 1.47 -3 2 0 -0.18 1.03 3 2 0 -0.88 1.37 3 -2 0 1.19 1.13 -3 -2 0 -0.06 1.26 2 2 1 67.95 2.72 -2 2 -1 70.69 2.61 -2 -2 -1 68.36 2.71 2 -2 1 67.68 2.52 -1 2 -2 28.88 1.84 1 2 2 27.44 1.93 1 -2 2 27.63 1.95 -1 -2 -2 26.97 1.92 0 2 3 93.85 2.16 0 -2 -3 92.39 2.18 0 -2 3 92.74 2.62 -1 2 4 23.20 1.23 -1 -2 4 21.87 1.92 1 -2 -4 22.36 1.23 -2 -2 5 66.52 2.47 3 2 -6 16.64 1.94 -3 -2 6 17.03 1.96 4 2 -7 175.25 3.85 -4 -2 7 171.61 3.83 5 2 -8 35.50 2.73 -5 -2 8 33.63 2.62 6 2 -9 33.25 3.11 -6 -2 9 33.30 3.15 6 -2 -9 34.67 1.53 7 2 -10 34.14 3.55 -7 2 10 33.67 1.87 -7 -2 10 35.04 3.57 7 -2 -10 35.19 1.94 -8 2 11 64.68 2.51 8 2 -11 63.67 4.52 -8 -2 11 71.12 4.67 8 -2 -11 63.00 2.60 -9 2 12 14.08 1.76 9 2 -12 11.96 3.15 9 -2 -12 9.73 1.77 -9 -2 12 10.51 3.05 10 2 -13 23.85 4.08 -10 -2 13 19.72 4.00 11 2 -14 45.14 5.17 -11 -2 14 48.74 5.31 12 3 -9 18.49 6.71 -12 3 9 18.68 5.24 -12 -3 9 20.12 6.18 12 -3 -9 23.08 6.37 -11 3 8 -2.55 3.84 11 3 -8 3.03 5.50 -11 -3 8 -6.39 4.50 11 -3 -8 8.61 4.85 -10 3 7 -2.53 3.12 10 3 -7 6.63 4.34 -10 -3 7 1.72 3.78 10 -3 -7 3.39 3.48 -9 3 6 0.46 2.47 9 3 -6 -4.36 3.24 9 -3 -6 3.04 3.19 -9 -3 6 0.01 3.02 8 3 -5 10.25 3.18 -8 3 5 9.81 2.55 8 -3 -5 9.04 2.86 -8 -3 5 12.75 3.03 7 3 -4 7.17 2.64 -7 3 4 7.08 2.17 -7 -3 4 10.02 2.36 7 -3 -4 5.18 2.31 -6 3 3 3.73 1.74 6 3 -3 3.63 1.79 6 -3 -3 5.96 1.85 -6 -3 3 3.43 2.06 5 3 -2 7.62 1.78 -5 3 2 8.48 1.71 5 -3 -2 6.25 1.65 -5 -3 2 7.14 1.73 -4 3 1 35.60 2.46 4 3 -1 35.11 2.74 -4 -3 1 30.83 2.64 4 -3 -1 37.22 2.53 -3 3 0 163.23 3.79 3 3 0 163.51 4.18 3 -3 0 160.94 3.77 -3 -3 0 167.18 4.25 -2 3 -1 1.13 1.09 2 3 1 1.69 1.29 2 -3 1 0.39 1.14 -2 -3 -1 -0.24 1.19 1 3 2 109.12 3.10 -1 -3 -2 111.51 3.11 1 -3 2 110.33 3.12 0 3 3 162.82 3.15 0 -3 -3 160.01 3.10 -1 3 4 44.65 1.73 1 -3 -4 43.17 1.73 -1 -3 4 45.73 2.40 -2 -3 5 12.61 1.65 2 -3 -5 12.93 1.11 3 3 -6 196.91 4.29 -3 -3 6 194.13 4.29 4 3 -7 7.18 1.63 -4 -3 7 5.99 1.68 5 3 -8 203.03 4.91 -5 -3 8 198.57 4.88 6 3 -9 18.07 2.43 -6 -3 9 18.07 2.49 7 3 -10 44.73 4.15 -7 -3 10 35.49 3.97 8 3 -11 15.81 3.11 -8 -3 11 19.51 3.32 9 3 -12 24.97 3.85 -9 -3 12 29.54 4.03 10 3 -13 18.50 4.56 -10 -3 13 20.40 4.36 11 3 -14 0.80 5.10 -11 -3 14 -0.15 4.64 -12 4 9 16.71 5.29 -12 -4 9 10.05 6.24 12 -4 -9 3.39 5.89 -11 4 8 5.33 4.15 11 4 -8 6.06 5.72 -11 -4 8 0.50 5.02 11 -4 -8 5.14 4.68 10 4 -7 7.99 4.87 -10 4 7 13.05 3.62 10 -4 -7 11.56 4.02 -10 -4 7 17.89 4.61 -9 4 6 11.11 3.06 9 -4 -6 5.24 3.24 -8 4 5 3.09 2.41 8 4 -5 3.60 3.18 -8 -4 5 7.40 3.06 8 -4 -5 3.69 2.70 -7 4 4 2.77 2.08 7 4 -4 5.78 2.49 -7 -4 4 2.02 2.36 7 -4 -4 0.88 2.12 6 4 -3 -0.46 1.87 -6 4 3 2.59 1.79 -6 -4 3 1.37 1.82 6 -4 -3 1.69 1.79 -5 4 2 4.23 1.65 5 4 -2 3.50 1.75 5 -4 -2 1.38 1.58 -5 -4 2 1.11 1.55 4 4 -1 36.95 2.92 -4 4 1 34.81 2.49 -4 -4 1 36.44 2.92 4 -4 -1 39.04 2.72 3 4 0 1.42 1.43 -3 4 0 4.69 1.41 -3 -4 0 1.71 1.51 3 -4 0 1.83 1.23 2 4 1 242.14 4.86 -2 -4 -1 254.43 4.98 2 -4 1 243.54 4.69 1 4 2 47.05 2.63 -1 -4 -2 47.14 2.63 1 -4 2 47.05 2.70 0 4 3 91.80 2.91 0 -4 -3 92.38 2.89 -1 4 4 8.65 1.28 1 -4 -4 10.28 1.33 -1 -4 4 8.19 1.54 2 -4 -5 118.15 2.55 -2 -4 5 115.47 3.71 3 4 -6 0.73 1.50 -3 -4 6 1.83 1.46 3 -4 -6 1.12 0.78 3 -4 -6 0.52 0.82 4 4 -7 157.26 4.65 4 -4 -7 155.58 2.28 4 -4 -7 162.41 2.29 -4 -4 7 158.28 4.62 5 4 -8 15.07 2.28 -5 -4 8 14.29 2.32 6 4 -9 156.47 5.41 -6 -4 9 155.02 5.29 7 4 -10 10.38 2.81 -7 -4 10 11.35 2.83 8 4 -11 24.47 3.56 -8 -4 11 20.35 3.65 9 4 -12 2.38 3.61 -9 -4 12 3.51 3.50 10 4 -13 26.72 5.08 -10 -4 13 31.47 4.92 11 4 -14 6.70 5.87 -11 -4 14 5.11 5.59 12 5 -9 4.40 7.36 -12 5 9 3.20 4.91 -12 -5 9 -1.53 6.42 12 -5 -9 19.40 6.29 -11 5 8 1.99 4.06 11 5 -8 6.28 6.26 11 -5 -8 0.94 4.48 -11 -5 8 8.95 5.44 -10 5 7 -3.07 3.34 10 5 -7 1.19 4.84 10 -5 -7 1.52 3.91 -10 -5 7 -3.88 4.13 -9 5 6 13.68 3.31 9 5 -6 13.91 4.21 9 -5 -6 16.38 3.55 -9 -5 6 20.22 4.23 -8 5 5 12.14 2.90 8 -5 -5 9.97 2.83 -8 -5 5 15.29 3.77 -7 5 4 1.05 2.09 7 5 -4 3.65 2.68 7 -5 -4 -0.78 2.14 -7 -5 4 0.90 2.24 6 5 -3 15.64 2.65 -6 5 3 19.10 2.42 6 -5 -3 18.80 2.47 -6 -5 3 15.31 2.45 -5 5 2 3.72 1.67 5 5 -2 0.89 1.78 5 -5 -2 0.03 1.60 -5 -5 2 0.29 1.57 -4 5 1 1.95 1.53 4 5 -1 2.48 1.60 -4 -5 1 4.45 1.60 4 -5 -1 2.16 1.36 3 5 0 305.78 6.13 3 -5 0 312.69 5.70 -3 -5 0 321.34 6.33 2 5 1 27.18 2.62 -2 -5 -1 25.50 2.58 2 -5 1 26.63 2.46 1 5 2 554.53 7.11 1 -5 2 562.68 7.45 -1 -5 -2 566.04 7.19 0 5 3 54.10 2.72 0 -5 3 56.37 3.03 0 -5 -3 57.55 2.72 -1 5 4 29.25 2.22 -1 -5 4 25.51 2.50 1 -5 -4 27.80 2.19 2 -5 -5 2.98 1.12 -2 -5 5 -1.17 1.33 3 5 -6 103.65 4.03 3 -5 -6 104.27 2.71 3 -5 -6 103.99 2.66 -3 -5 6 105.02 4.18 4 5 -7 60.84 3.82 -4 -5 7 65.35 3.80 4 -5 -7 65.47 2.20 4 -5 -7 68.97 2.29 5 5 -8 259.13 6.52 5 -5 -8 263.39 3.45 -5 -5 8 263.34 6.53 5 -5 -8 266.01 3.38 6 5 -9 5.10 2.52 -6 -5 9 3.87 2.45 6 -5 -9 4.60 1.03 6 -5 -9 2.90 1.20 7 5 -10 119.30 6.01 -7 -5 10 121.56 5.97 8 5 -11 -1.73 3.26 -8 -5 11 -1.43 3.32 -9 -5 12 54.88 5.67 10 5 -13 5.84 5.14 -10 -5 13 9.72 5.15 11 5 -14 12.48 6.45 -11 -5 14 7.01 5.93 -12 6 9 5.56 5.63 12 6 -9 18.03 8.82 -12 -6 9 6.53 7.42 -11 6 8 13.36 4.68 11 6 -8 6.56 6.68 -11 -6 8 6.90 5.69 11 -6 -8 6.80 5.11 -10 6 7 2.89 3.74 10 6 -7 8.22 5.50 -10 -6 7 6.43 4.90 10 -6 -7 0.69 4.09 9 6 -6 20.63 4.66 -9 6 6 20.22 3.48 9 -6 -6 26.34 3.97 -9 -6 6 16.76 4.75 -8 6 5 11.93 2.82 8 6 -5 8.86 3.58 8 -6 -5 12.53 3.18 -8 -6 5 12.21 3.54 -7 6 4 25.72 3.13 -7 -6 4 21.43 3.43 7 -6 -4 22.71 3.12 -6 6 3 1.44 1.95 6 6 -3 4.22 2.25 -6 -6 3 -3.46 1.97 6 -6 -3 4.55 2.28 5 6 -2 40.26 3.54 5 -6 -2 35.17 3.27 -5 -6 2 38.74 3.45 4 6 -1 29.63 3.35 4 -6 -1 30.91 3.00 -4 -6 1 30.13 3.22 3 6 0 43.49 3.29 -3 -6 0 45.78 3.22 3 -6 0 42.50 3.11 2 6 1 118.72 4.29 -2 -6 -1 114.10 4.15 2 -6 1 119.15 4.14 1 6 2 125.77 4.20 1 -6 2 135.10 4.32 1 -6 2 128.63 4.32 -1 -6 -2 131.96 4.20 0 6 3 118.01 3.88 0 -6 -3 121.64 3.87 0 -6 3 114.31 4.16 -1 6 4 0.66 1.37 1 -6 -4 -0.69 1.23 -1 -6 4 0.74 1.41 -2 -6 5 207.51 5.45 2 -6 -5 199.97 4.24 3 6 -6 2.95 1.86 3 -6 -6 1.34 1.31 -3 -6 6 -0.22 1.74 4 6 -7 129.79 5.15 4 -6 -7 131.29 3.39 -4 -6 7 127.20 5.15 4 -6 -7 131.92 3.32 5 6 -8 7.76 2.59 -5 -6 8 5.57 2.58 5 -6 -8 10.25 1.50 5 -6 -8 8.82 1.50 6 6 -9 101.55 5.77 -6 -6 9 91.53 5.55 6 -6 -9 94.84 2.79 6 -6 -9 98.70 3.03 7 6 -10 2.56 3.17 -7 -6 10 1.57 3.16 7 -6 -10 1.07 1.23 8 6 -11 29.59 5.18 9 6 -12 23.25 5.27 -9 -6 12 17.18 5.04 10 6 -13 24.70 6.13 -10 -6 13 29.03 6.12 11 6 -14 11.09 7.12 -11 -6 14 12.96 7.31 11 7 -8 -1.52 6.89 -11 -7 8 7.00 6.68 11 -7 -8 -0.97 5.09 10 7 -7 83.78 9.81 10 -7 -7 84.71 7.90 -10 -7 7 97.44 9.49 9 7 -6 5.29 4.79 9 -7 -6 7.91 3.76 -9 -7 6 11.27 4.58 8 7 -5 84.56 6.70 8 -7 -5 83.86 5.59 -8 -7 5 78.28 6.64 7 7 -4 14.15 3.41 7 -7 -4 11.68 2.98 -7 -7 4 6.35 3.06 6 -7 -3 105.04 5.17 -6 -7 3 99.08 5.25 5 7 -2 0.19 2.04 -5 -7 2 5.08 2.08 5 -7 -2 0.61 1.98 4 7 -1 70.85 4.49 4 -7 -1 62.78 3.88 -4 -7 1 68.29 4.10 3 7 0 71.32 4.20 3 -7 0 74.59 3.80 -3 -7 0 73.62 4.06 2 7 1 45.96 3.35 2 -7 1 45.52 3.33 -2 -7 -1 45.53 3.29 2 -7 1 45.04 3.31 1 7 2 4.60 1.86 -1 -7 -2 3.97 1.70 1 -7 2 1.78 1.48 0 7 3 37.08 2.98 0 -7 -3 37.11 3.06 0 -7 3 39.38 3.11 -1 7 4 79.06 3.57 -1 -7 4 81.61 4.01 1 -7 -4 75.92 3.55 2 -7 -5 6.61 1.77 -2 -7 5 6.75 2.09 3 7 -6 77.04 4.32 3 -7 -6 75.09 3.42 -3 -7 6 77.35 4.33 4 7 -7 9.44 2.55 -4 -7 7 8.27 2.50 4 -7 -7 6.63 1.68 4 -7 -7 7.39 1.55 5 7 -8 50.89 4.92 5 -7 -8 49.60 2.95 -5 -7 8 46.53 4.89 5 -7 -8 50.06 3.03 6 7 -9 6.56 3.65 6 -7 -9 5.48 1.80 6 -7 -9 6.80 1.76 -6 -7 9 6.78 3.19 7 7 -10 0.99 3.65 7 -7 -10 2.99 1.86 7 -7 -10 2.56 1.65 -7 -7 10 5.05 3.52 8 7 -11 25.12 4.99 -8 -7 11 24.91 4.87 9 7 -12 36.51 6.16 -9 -7 12 38.56 6.11 -10 -7 13 10.11 6.55 11 8 -8 53.59 8.89 -11 -8 8 63.23 9.05 10 8 -7 -9.73 5.89 -10 -8 7 7.37 6.26 10 -8 -7 0.75 4.54 9 8 -6 110.29 9.24 -9 -8 6 117.87 8.80 9 -8 -6 122.66 7.38 8 8 -5 9.63 4.22 8 -8 -5 11.35 3.55 -8 -8 5 10.46 4.10 7 8 -4 77.18 6.52 -7 -8 4 76.03 6.04 7 -8 -4 82.10 5.69 6 8 -3 6.45 2.94 6 -8 -3 8.80 2.78 -6 -8 3 13.58 2.99 5 -8 -2 128.60 5.42 -5 -8 2 118.58 5.96 4 8 -1 9.03 2.48 -4 -8 1 13.22 2.55 4 -8 -1 12.14 2.56 3 8 0 55.26 4.00 3 -8 0 62.86 4.17 -3 -8 0 48.70 3.84 3 -8 0 61.19 3.88 2 8 1 63.10 4.02 2 -8 1 56.54 3.90 2 -8 1 58.08 3.74 -2 -8 -1 57.78 3.94 1 8 2 34.56 3.39 1 -8 2 36.29 3.34 -1 -8 -2 36.86 3.42 0 8 3 3.02 1.94 0 -8 3 0.29 1.72 0 -8 -3 -0.96 1.82 -1 8 4 0.44 1.74 1 -8 -4 0.24 1.66 -1 -8 4 -3.34 1.64 2 -8 -5 17.75 2.30 -2 -8 5 18.44 2.62 3 -8 -6 8.75 2.12 -3 -8 6 9.73 2.56 4 8 -7 23.81 3.28 -4 -8 7 20.68 3.13 4 -8 -7 24.08 2.56 4 -8 -7 24.86 3.04 5 8 -8 5.30 3.17 5 -8 -8 -1.51 1.73 5 -8 -8 2.53 1.99 6 8 -9 8.55 3.68 6 -8 -9 6.54 2.01 -6 -8 9 6.71 3.55 6 -8 -9 7.83 2.06 7 8 -10 36.68 5.12 7 -8 -10 36.72 3.46 -7 -8 10 32.99 4.99 7 -8 -10 34.88 3.35 8 8 -11 13.53 5.13 8 -8 -11 1.57 2.14 8 -8 -11 4.57 1.79 -8 -8 11 2.90 4.69 -9 -8 12 53.63 6.96 10 8 -13 9.86 7.12 -10 -8 13 -5.24 6.93 11 9 -8 18.64 8.49 -11 -9 8 -2.27 8.25 11 -9 -8 3.03 6.28 10 9 -7 43.38 7.62 -10 -9 7 35.47 7.19 10 -9 -7 42.84 6.22 9 9 -6 -2.66 5.31 -9 -9 6 3.79 5.12 8 9 -5 69.60 7.41 -8 -9 5 59.90 7.42 8 -9 -5 54.68 6.32 7 9 -4 -3.22 3.39 -7 -9 4 -3.93 3.18 7 -9 -4 1.77 3.17 6 9 -3 84.94 5.73 6 -9 -3 100.21 5.74 -6 -9 3 88.43 6.03 5 9 -2 27.19 3.85 5 -9 -2 21.07 3.25 -5 -9 2 22.05 3.34 4 9 -1 65.89 4.92 4 -9 -1 56.77 4.80 4 -9 -1 59.93 4.93 3 9 0 4.33 2.35 -3 -9 0 -0.93 2.00 3 -9 0 -1.55 2.37 3 -9 0 -0.35 2.12 2 9 1 62.12 4.44 2 -9 1 60.27 4.36 2 -9 1 61.71 4.36 -2 -9 -1 64.48 4.30 1 9 2 1.85 2.18 -1 -9 -2 1.51 2.13 1 -9 2 -1.44 1.80 0 9 3 14.34 2.59 0 -9 -3 13.78 2.71 0 -9 3 17.00 2.78 -1 9 4 11.93 2.55 -1 -9 4 6.82 2.27 1 -9 -4 16.15 2.59 -2 -9 5 13.96 2.62 2 -9 -5 15.62 2.47 3 -9 -6 5.97 2.29 4 9 -7 12.28 3.13 -4 -9 7 6.84 3.22 4 -9 -7 9.53 2.35 4 -9 -7 8.60 2.32 5 9 -8 20.74 3.99 -5 -9 8 15.08 3.94 5 -9 -8 16.99 2.53 5 -9 -8 18.34 2.73 6 9 -9 60.75 6.97 6 -9 -9 48.73 3.97 -6 -9 9 48.65 6.24 6 -9 -9 51.78 4.10 7 9 -10 4.00 4.62 7 -9 -10 4.76 2.50 -7 -9 10 7.42 4.59 7 -9 -10 4.39 2.45 8 9 -11 33.22 6.28 8 -9 -11 30.14 2.87 8 -9 -11 30.51 3.18 -8 -9 11 29.79 6.07 9 9 -12 8.87 6.60 -9 -9 12 0.33 6.56 10 10 -7 12.12 7.96 -10 -10 7 -0.91 7.11 10 -10 -7 4.26 5.66 9 10 -6 58.78 7.29 -9 -10 6 48.34 7.37 9 -10 -6 59.58 7.80 8 10 -5 16.28 5.05 8 -10 -5 9.33 4.23 -8 -10 5 -5.22 4.40 7 10 -4 98.47 6.96 -7 -10 4 104.24 7.18 6 10 -3 12.26 3.33 -6 -10 3 7.04 3.09 5 10 -2 113.56 6.76 5 -10 -2 102.64 6.38 -5 -10 2 101.81 5.94 5 -10 -2 94.08 6.39 4 10 -1 7.90 3.36 -4 -10 1 8.25 2.88 4 -10 -1 10.50 3.29 4 -10 -1 10.93 3.08 3 10 0 57.25 4.79 -3 -10 0 41.54 4.43 3 -10 0 53.19 4.58 3 -10 0 50.99 4.83 2 -10 1 1.85 2.43 2 -10 1 0.29 2.52 1 10 2 13.82 2.95 -1 -10 -2 10.70 2.82 0 10 3 51.35 4.77 0 -10 -3 36.15 4.56 -1 -10 4 4.76 2.53 1 -10 -4 1.65 2.43 -2 -10 5 32.79 3.75 2 -10 -5 35.39 4.27 3 -10 -6 1.18 2.35 -3 -10 6 4.08 2.62 4 -10 -7 55.64 4.54 -4 -10 7 61.37 5.69 4 -10 -7 64.28 4.67 -5 -10 8 1.16 3.75 5 -10 -8 2.52 2.58 5 -10 -8 2.62 2.61 6 -10 -9 11.44 3.06 6 -10 -9 15.31 2.94 -6 -10 9 5.55 4.57 7 10 -10 20.27 5.55 7 -10 -10 18.18 3.21 7 -10 -10 11.56 3.05 -7 -10 10 14.47 5.79 8 10 -11 0.71 5.85 8 -10 -11 9.51 3.18 -8 -10 11 0.70 6.05 8 -10 -11 1.98 2.89 9 10 -12 38.01 7.93 -9 -10 12 36.65 8.46 9 11 -6 13.71 7.17 -9 -11 6 7.64 6.99 9 -11 -6 11.82 5.53 9 -11 -6 6.36 5.09 8 11 -5 24.90 5.90 8 -11 -5 38.31 5.44 8 -11 -5 30.33 5.41 -8 -11 5 20.36 5.49 7 11 -4 3.92 4.31 7 -11 -4 5.21 4.18 7 -11 -4 2.97 4.39 -7 -11 4 6.90 4.10 6 11 -3 51.72 5.30 6 -11 -3 50.30 6.46 -6 -11 3 48.78 6.14 6 -11 -3 42.26 4.78 5 -11 -2 -0.08 3.37 -5 -11 2 -1.65 3.19 5 -11 -2 -4.20 3.08 4 11 -1 63.09 5.35 -4 -11 1 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4.45 11 -2 -7 10.69 4.92 10 2 -6 16.45 4.52 -10 2 6 12.69 3.63 10 -2 -6 16.48 4.14 9 2 -5 38.15 4.54 -9 2 5 49.33 5.11 9 -2 -5 45.65 5.22 -9 -2 5 43.24 5.35 -8 2 4 115.23 5.39 8 2 -4 126.24 6.05 8 -2 -4 115.52 5.63 -8 -2 4 114.12 5.63 -7 2 3 21.60 2.87 7 2 -3 19.03 2.97 -7 -2 3 15.97 2.67 7 -2 -3 12.44 2.66 6 2 -2 62.77 3.90 -6 2 2 58.16 3.56 -6 -2 2 63.57 3.86 6 -2 -2 63.58 3.77 5 2 -1 2.38 1.59 -5 2 1 3.08 1.54 5 -2 -1 1.54 1.58 -5 -2 1 0.33 1.49 4 2 0 134.77 4.12 -4 2 0 137.21 3.89 -4 -2 0 137.35 4.13 4 -2 0 138.67 3.92 -3 2 -1 40.19 2.51 3 2 1 39.60 2.73 3 -2 1 41.31 2.57 -3 -2 -1 42.94 2.70 2 2 2 37.00 2.46 -2 2 -2 36.84 2.36 -2 -2 -2 38.71 2.51 2 -2 2 37.06 2.37 1 2 3 15.01 1.59 -1 2 -3 8.61 1.39 1 -2 3 11.05 1.41 -1 -2 -3 15.10 2.01 0 2 -4 493.14 5.43 0 2 4 484.48 4.56 0 -2 4 492.19 5.48 0 -2 -4 495.85 4.85 -1 2 5 30.82 1.38 -1 -2 5 31.52 2.11 1 -2 -5 29.30 1.57 -2 -2 6 22.65 2.00 -3 -2 7 0.29 1.15 -4 -2 8 -0.16 1.29 5 2 -9 20.24 2.65 -5 -2 9 18.68 1.98 6 2 -10 6.75 1.98 -6 -2 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4 -3 2.25 2.41 -7 4 3 4.71 2.32 -7 -4 3 7.83 2.54 7 -4 -3 2.42 2.39 -6 4 2 3.21 1.92 6 4 -2 2.67 1.88 6 -4 -2 1.39 1.74 -6 -4 2 3.50 2.11 -5 4 1 22.53 2.84 5 4 -1 28.31 2.98 -5 -4 1 23.98 2.80 5 -4 -1 22.21 2.78 -4 4 0 0.54 1.28 4 4 0 1.57 1.48 -4 -4 0 -0.79 1.36 4 -4 0 -0.37 1.30 -3 4 -1 21.27 2.32 3 4 1 22.13 2.61 3 -4 1 22.69 2.38 -3 -4 -1 23.83 2.61 2 4 2 -0.05 1.29 -2 4 -2 0.36 1.25 2 -4 2 0.91 1.25 -2 -4 -2 -0.04 1.24 1 4 3 0.52 1.17 -1 -4 -3 0.47 1.19 1 -4 3 1.13 1.30 0 4 4 8.16 1.42 0 -4 4 5.90 1.51 0 -4 -4 5.09 1.25 -1 4 5 62.56 2.34 -1 -4 5 62.30 2.96 1 -4 -5 66.25 2.33 -2 4 6 62.05 2.02 -2 -4 6 57.00 2.96 2 -4 -6 57.59 1.93 3 -4 -7 79.50 1.67 3 -4 -7 81.14 1.76 -3 -4 7 86.05 3.74 4 4 -8 0.39 1.71 -4 -4 8 0.99 1.74 5 4 -9 259.21 6.08 -5 -4 9 265.75 6.14 6 4 -10 6.62 2.53 -6 -4 10 5.50 2.30 7 4 -11 53.98 4.87 -7 -4 11 52.67 4.68 8 4 -12 2.93 3.22 -8 -4 12 -1.35 3.03 9 4 -13 39.19 4.75 -9 -4 13 37.28 4.60 10 4 -14 6.05 4.73 -10 -4 14 11.75 4.88 -12 5 8 27.30 5.66 12 5 -8 50.83 8.24 12 -5 -8 41.92 6.47 -12 -5 8 28.80 7.31 -11 5 7 1.37 4.76 -11 -5 7 1.24 5.21 10 5 -6 74.94 8.52 -10 5 6 79.37 6.80 10 -5 -6 65.98 6.95 -10 -5 6 74.18 7.68 9 5 -5 4.85 4.05 -9 5 5 -1.91 3.05 -9 -5 5 5.95 3.57 9 -5 -5 2.90 3.48 8 5 -4 31.52 4.71 -8 5 4 34.03 3.64 8 -5 -4 32.01 3.77 7 5 -3 9.69 2.78 -7 5 3 4.26 2.54 -7 -5 3 7.87 2.68 7 -5 -3 5.63 2.39 -6 5 2 63.20 3.90 6 5 -2 65.84 4.20 -6 -5 2 70.20 4.33 6 -5 -2 58.83 4.00 5 5 -1 29.78 3.09 -5 5 1 32.96 3.02 5 -5 -1 32.35 3.15 -5 -5 1 33.98 3.39 -4 5 0 24.86 2.67 4 5 0 27.09 2.94 -4 -5 0 22.23 2.93 4 -5 0 25.81 2.75 -3 5 -1 10.94 1.71 3 5 1 14.60 2.06 -3 -5 -1 14.21 2.16 3 -5 1 12.38 1.90 2 5 2 0.11 1.51 2 -5 2 0.49 1.39 -2 -5 -2 1.20 1.38 1 5 3 8.02 1.62 -1 -5 -3 8.76 1.58 1 -5 3 10.01 1.85 0 5 4 82.05 3.13 0 -5 4 81.03 3.48 0 -5 -4 81.97 3.05 -1 5 5 15.97 2.10 -1 -5 5 18.85 2.47 1 -5 -5 16.61 1.66 -2 5 6 139.81 3.21 2 -5 -6 138.40 3.14 -2 -5 6 135.87 4.34 -3 -5 7 0.82 1.67 3 -5 -7 2.26 1.02 4 5 -8 31.80 3.47 4 -5 -8 29.27 1.56 4 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5.69 8 -5 -2 80.24 5.94 -8 -5 2 86.70 6.02 -7 5 1 7.42 2.67 7 -5 -1 4.79 2.66 -7 -5 1 6.76 2.59 -6 5 0 168.51 5.84 6 5 0 159.57 6.01 -6 -5 0 165.11 6.01 6 -5 0 162.54 5.81 -5 5 -1 0.99 1.66 5 5 1 5.92 2.16 -5 -5 -1 2.06 2.00 5 -5 1 4.67 2.00 4 5 2 84.97 4.08 -4 5 -2 82.73 3.78 -4 -5 -2 86.62 4.20 4 -5 2 81.99 3.88 3 5 3 2.70 1.60 -3 5 -3 1.66 1.47 -3 -5 -3 0.84 1.55 3 -5 3 1.38 1.51 2 5 4 198.87 5.01 -2 -5 -4 194.87 5.07 2 -5 4 190.88 5.16 1 5 5 2.46 1.45 -1 -5 -5 3.23 1.51 1 -5 5 4.50 1.71 0 5 6 63.06 3.10 0 -5 6 63.22 3.34 0 -5 -6 62.62 3.05 -1 5 7 91.32 3.14 -1 -5 7 87.00 3.87 -1 -5 7 88.69 3.92 1 -5 -7 84.96 3.09 -2 5 8 45.29 2.28 2 -5 -8 41.56 2.36 -2 -5 8 42.44 3.28 3 -5 -9 2.92 1.10 -3 -5 9 1.83 2.10 -4 -5 10 1.73 2.19 -5 -5 11 3.93 2.49 -6 -5 12 10.09 3.02 -7 -5 13 8.21 3.32 -8 -5 14 27.13 4.47 -9 -5 15 6.01 4.75 -12 6 6 8.99 6.43 12 6 -6 12.36 8.26 -12 -6 6 -6.54 6.98 12 -6 -6 -1.36 6.78 -11 6 5 0.53 5.14 11 6 -5 2.42 6.59 -11 -6 5 8.74 5.80 11 -6 -5 -8.15 5.55 -10 6 4 2.24 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185.74 5.23 3 4 4 0.85 1.60 -3 4 -4 -1.93 1.46 -3 -4 -4 2.37 1.55 3 -4 4 3.39 1.54 -2 4 -5 244.14 5.57 2 4 5 243.65 5.40 2 -4 5 239.86 5.60 -2 -4 -5 243.35 5.55 1 4 6 15.54 1.99 -1 4 -6 12.22 1.94 -1 -4 -6 15.31 2.10 1 -4 6 14.97 2.03 0 4 7 317.72 5.19 0 -4 7 322.01 6.23 0 -4 -7 324.42 5.58 -1 4 8 0.20 1.22 1 -4 -8 -0.19 1.31 -1 -4 8 0.58 1.51 -2 4 9 282.52 3.74 -2 -4 9 281.86 6.02 2 -4 -9 292.40 4.05 -2 -4 9 284.29 6.08 -3 -4 10 0.12 1.80 -3 -4 10 -1.47 1.76 -4 -4 11 78.86 4.32 -5 -4 12 0.77 2.31 -6 -4 13 31.09 3.52 -7 -4 14 9.47 3.23 -8 -4 15 11.42 3.73 -9 -4 16 1.54 4.07 -10 -4 17 3.08 4.93 -12 5 5 1.99 6.38 12 5 -5 23.82 7.97 -12 -5 5 -5.05 6.77 12 -5 -5 -6.07 6.64 -11 5 4 16.08 5.72 11 5 -4 -0.92 6.45 11 -5 -4 9.04 5.77 -11 -5 4 8.77 6.03 -10 5 3 16.07 4.69 10 -5 -3 18.61 5.32 -10 -5 3 8.00 4.73 9 5 -2 19.85 4.59 -9 5 2 18.72 4.01 9 -5 -2 19.22 4.44 -9 -5 2 12.74 3.67 -8 5 1 14.85 3.65 8 5 -1 12.91 3.50 8 -5 -1 15.35 3.52 -8 -5 1 17.22 3.74 7 5 0 21.96 3.52 -7 5 0 31.59 3.70 7 -5 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9.82 2.52 -5 5 -3 6.07 2.19 5 -5 3 11.58 2.40 -5 -5 -3 3.65 2.02 4 5 4 3.27 2.14 -4 5 -4 2.89 1.74 4 -5 4 2.00 1.68 -4 -5 -4 2.62 1.80 3 5 5 7.95 2.00 -3 5 -5 10.06 2.07 -3 -5 -5 11.65 2.34 3 -5 5 7.44 2.09 -2 5 -6 161.60 5.14 2 5 6 170.68 5.12 -2 -5 -6 177.95 5.40 2 -5 6 172.56 5.31 1 5 7 50.10 3.37 -1 -5 -7 57.08 3.61 1 -5 7 50.96 3.50 0 5 8 145.02 4.34 0 -5 8 152.12 5.21 0 -5 -8 148.77 4.61 -1 5 9 3.02 1.55 1 -5 -9 1.04 1.72 -1 -5 9 2.93 2.03 -2 5 10 148.55 3.44 2 -5 -10 153.22 3.92 -2 -5 10 153.93 5.49 -2 -5 10 158.49 5.55 -3 -5 11 0.80 2.25 -3 -5 11 1.65 2.30 -4 -5 12 85.83 5.15 -4 -5 12 74.22 4.90 -5 -5 13 -0.30 2.87 -5 -5 13 4.31 2.78 -6 -5 14 59.86 5.87 -6 -5 14 71.80 5.80 -7 -5 15 -5.97 3.75 -8 -5 16 65.17 7.46 -8 -5 16 77.61 7.40 -9 -5 17 3.33 5.15 -9 -5 17 11.52 5.16 -12 6 4 -2.49 6.71 12 6 -4 20.53 8.96 -12 -6 4 4.38 7.65 12 -6 -4 9.02 7.46 11 6 -3 16.54 7.07 -11 6 3 13.58 5.93 -11 -6 3 6.59 5.57 10 6 -2 16.75 5.48 -10 6 2 10.16 4.81 -10 -6 2 10.92 5.32 10 -6 -2 11.76 5.44 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6.62 0 -6 -18 7.37 5.29 0 -6 18 2.46 6.93 7 7 11 15.41 8.97 -7 -7 -11 22.28 7.59 6 7 12 3.66 7.45 -6 -7 -12 2.36 6.36 5 7 13 24.26 7.11 5 -7 13 16.54 7.53 -5 -7 -13 25.96 7.06 4 7 14 11.35 6.33 -4 -7 -14 11.03 6.40 4 -7 14 3.10 7.30 3 7 15 35.00 6.94 -3 -7 -15 24.57 7.02 3 -7 15 12.83 7.68 2 7 16 5.75 5.69 -2 -7 -16 -5.90 6.05 2 -7 16 1.06 7.46 1 7 17 20.45 6.05 -1 -7 -17 23.89 6.27 1 -7 17 26.03 7.72 5 8 13 -1.11 7.30 -5 -8 -13 2.03 6.65 4 8 14 48.64 7.83 -4 -8 -14 59.76 8.33 3 8 15 -8.43 6.55 -3 -8 -15 4.97 6.49 -2 -8 -16 17.59 6.89 2 -8 16 30.83 8.81 8 0 11 -12.77 6.84 -8 0 -11 -13.98 6.35 7 0 12 -4.01 6.82 -7 0 -12 6.79 6.61 6 0 13 -0.56 6.24 -6 0 -13 1.41 6.46 -5 0 -14 75.12 8.47 5 0 14 77.02 8.44 4 0 15 -10.96 6.05 -4 0 -15 10.34 6.26 -3 0 -16 49.75 6.72 3 0 16 30.61 7.49 2 0 17 -3.38 6.24 -2 0 -17 -4.40 5.24 -1 0 -18 86.54 9.14 1 0 18 80.07 10.16 0 0 19 -4.93 6.29 -1 0 20 32.86 6.80 -8 1 -11 8.96 7.46 8 1 11 15.85 7.53 8 -1 11 1.03 7.20 -8 -1 -11 1.74 6.62 -7 1 -12 -0.18 6.74 7 1 12 1.25 6.81 -7 -1 -12 -2.87 6.04 7 -1 12 -6.36 6.84 6 1 13 4.16 6.86 -6 1 -13 21.31 7.07 -6 -1 -13 18.05 7.03 6 -1 13 16.16 7.03 5 1 14 -4.87 6.03 -5 1 -14 19.01 6.40 -5 -1 -14 4.69 6.31 5 -1 14 9.61 7.10 4 1 15 53.94 7.51 -4 1 -15 64.19 7.55 -4 -1 -15 66.38 7.84 4 -1 15 59.68 7.78 -3 1 -16 4.13 5.58 -3 -1 -16 6.13 6.02 3 -1 16 7.85 6.35 2 1 17 59.84 7.28 -2 1 -17 71.26 9.23 -2 -1 -17 71.27 9.31 1 1 18 -7.56 6.01 -1 1 -18 7.36 5.54 -1 -1 -18 -1.82 5.01 1 -1 18 9.48 6.24 0 1 19 79.08 10.10 0 -1 19 92.55 10.65 0 -1 -19 96.64 8.74 -1 -1 20 1.92 6.65 8 2 11 9.27 7.63 -8 -2 -11 -1.36 6.69 -7 2 -12 10.16 6.77 7 2 12 -7.61 6.63 -7 -2 -12 15.52 6.83 7 -2 12 13.00 7.29 6 2 13 -6.78 6.80 -6 2 -13 4.27 6.61 -6 -2 -13 -3.14 5.97 6 -2 13 6.58 7.29 -5 2 -14 38.11 6.98 5 2 14 49.17 7.93 -5 -2 -14 44.63 7.19 5 -2 14 49.83 8.17 -4 2 -15 0.59 5.86 4 2 15 -2.71 6.14 4 -2 15 6.07 6.52 -4 -2 -15 -1.92 5.89 -3 2 -16 43.81 6.74 3 -2 16 35.48 6.98 -3 -2 -16 33.89 6.82 2 2 17 -8.73 5.89 -2 2 -17 2.03 5.84 2 -2 17 6.23 6.40 -2 -2 -17 11.89 5.74 1 2 18 60.87 7.27 -1 -2 -18 76.74 8.87 0 2 19 -3.08 5.98 0 -2 -19 4.53 4.98 0 -2 19 3.45 6.56 -1 2 20 21.48 6.14 -1 -2 20 24.62 6.92 7 3 12 18.44 7.55 -7 3 -12 6.96 6.52 -7 -3 -12 3.28 6.17 7 -3 12 30.93 7.76 -6 3 -13 17.16 6.84 6 3 13 9.34 7.05 6 -3 13 1.69 7.26 -6 -3 -13 10.00 6.38 -5 3 -14 32.97 7.02 5 3 14 31.58 7.09 -5 -3 -14 25.63 6.71 5 -3 14 19.35 6.91 -4 3 -15 11.61 6.27 4 3 15 9.55 6.44 -4 -3 -15 -5.78 6.16 4 -3 15 2.55 6.83 -3 3 -16 -0.77 5.80 3 -3 16 8.24 6.53 -3 -3 -16 -9.43 5.82 -2 3 -17 7.57 6.07 2 3 17 20.53 6.30 -2 -3 -17 19.09 6.20 2 -3 17 28.53 6.91 1 3 18 6.01 6.24 -1 -3 -18 5.85 5.35 1 -3 18 13.95 6.71 0 3 19 30.43 6.46 7 4 12 15.20 8.36 -7 -4 -12 -10.89 6.32 6 4 13 41.10 8.05 -6 4 -13 10.46 6.79 6 -4 13 18.04 8.07 -6 -4 -13 21.91 7.24 -5 4 -14 -0.06 6.12 5 4 14 4.38 6.85 5 -4 14 1.74 7.24 -5 -4 -14 9.20 6.52 -4 4 -15 11.62 6.55 4 4 15 -0.64 6.67 -4 -4 -15 -4.06 6.15 4 -4 15 12.50 6.75 -3 4 -16 1.83 6.04 -3 -4 -16 -8.11 5.94 3 -4 16 -1.68 6.45 2 4 17 5.01 6.11 -2 -4 -17 -6.16 6.08 2 -4 17 -4.88 6.47 1 4 18 -1.15 6.03 1 -4 18 3.55 6.44 -1 -4 -18 8.63 5.95 0 -4 19 5.96 6.97 7 5 12 9.35 8.63 -7 -5 -12 0.93 6.98 6 5 13 4.42 8.11 -6 5 -13 13.79 7.42 6 -5 13 13.96 8.45 -6 -5 -13 -1.51 7.17 -5 5 -14 23.18 7.04 5 5 14 5.71 7.64 -5 -5 -14 7.29 6.73 5 -5 14 20.99 8.02 4 5 15 1.01 6.60 -4 5 -15 -8.16 6.56 -4 -5 -15 5.68 6.28 4 -5 15 6.74 7.60 3 5 16 -10.91 6.06 -3 -5 -16 -2.42 6.46 3 -5 16 2.03 6.97 2 5 17 2.12 5.94 2 -5 17 4.86 7.03 -2 -5 -17 -5.96 6.18 1 5 18 1.25 5.71 1 -5 18 -2.62 6.61 -1 -5 -18 -0.90 6.07 6 6 13 3.70 7.75 -6 -6 -13 14.44 7.74 5 6 14 11.51 7.62 -5 -6 -14 12.20 7.18 4 6 15 7.29 6.36 4 -6 15 8.38 7.74 -4 -6 -15 -4.27 6.96 3 6 16 7.84 6.35 -3 -6 -16 3.79 6.62 3 -6 16 2.35 7.30 2 6 17 13.74 6.65 2 -6 17 5.74 8.08 -2 -6 -17 11.00 6.70 -7 0 -13 11.49 8.28 7 0 13 -8.08 7.90 6 0 14 0.19 7.26 -6 0 -14 2.75 8.02 -5 0 -15 11.79 7.67 5 0 15 2.11 7.15 -4 0 -16 3.63 7.14 4 0 16 -4.74 6.79 3 0 17 -10.91 6.70 -3 0 -17 9.38 6.92 -2 0 -18 16.08 6.59 2 0 18 16.45 7.34 -1 0 -19 14.45 6.36 7 1 13 0.20 7.75 -7 -1 -13 4.18 7.68 -6 1 -14 11.91 7.81 6 1 14 1.21 7.31 -6 -1 -14 -1.12 7.23 6 -1 14 -9.50 7.73 -5 1 -15 12.84 7.03 5 1 15 -10.91 7.34 -5 -1 -15 -5.23 7.49 5 -1 15 -6.32 7.53 -4 1 -16 7.45 6.88 4 1 16 -6.28 7.21 -4 -1 -16 2.88 7.14 4 -1 16 1.54 7.39 3 1 17 7.03 7.18 -3 1 -17 -10.63 6.46 3 -1 17 12.78 7.60 -3 -1 -17 9.39 6.96 -2 1 -18 2.08 6.59 2 -1 18 11.71 7.52 -2 -1 -18 8.78 6.59 1 1 19 13.62 7.41 -1 1 -19 12.21 6.43 -1 -1 -19 7.46 6.31 1 -1 19 10.50 7.85 7 2 13 19.18 8.52 -7 -2 -13 16.63 7.75 -6 2 -14 1.62 7.58 6 2 14 -7.54 7.29 6 -2 14 6.30 8.52 -6 -2 -14 -1.35 7.33 -5 2 -15 18.02 7.63 5 2 15 0.37 7.30 -5 -2 -15 3.67 7.29 5 -2 15 16.52 7.81 -4 2 -16 -7.31 6.68 4 2 16 -2.13 7.14 -4 -2 -16 10.55 7.63 4 -2 16 16.92 7.72 3 2 17 1.54 7.07 -3 2 -17 6.32 6.83 -3 -2 -17 16.13 7.28 3 -2 17 11.22 7.41 -2 2 -18 9.05 6.66 -2 -2 -18 14.27 6.87 2 -2 18 18.92 7.48 1 2 19 6.79 6.69 1 -2 19 9.66 7.89 -1 -2 -19 1.68 6.13 -6 3 -14 62.18 9.42 6 3 14 78.01 9.44 -6 -3 -14 66.85 8.73 6 -3 14 63.08 9.97 -5 3 -15 -2.33 7.27 5 3 15 20.47 7.72 5 -3 15 13.77 8.17 -5 -3 -15 -2.57 7.30 -4 3 -16 22.32 7.35 4 3 16 29.81 7.60 -4 -3 -16 7.32 7.51 4 -3 16 18.07 8.23 -3 3 -17 11.34 7.24 3 3 17 5.28 7.18 -3 -3 -17 7.40 7.36 3 -3 17 9.86 7.84 -2 3 -18 18.57 7.19 -2 -3 -18 27.47 7.24 2 -3 18 21.51 7.92 6 4 14 22.42 8.98 -6 -4 -14 -1.29 6.96 -5 4 -15 57.31 8.92 5 4 15 78.08 9.73 -5 -4 -15 44.42 8.34 5 -4 15 50.50 9.50 4 4 16 12.23 7.71 -4 4 -16 4.51 7.37 -4 -4 -16 -8.58 7.09 4 -4 16 10.56 8.30 3 4 17 25.80 7.97 -3 4 -17 -0.16 7.08 -3 -4 -17 15.55 7.23 3 -4 17 30.63 8.49 -2 -4 -18 5.26 7.26 2 -4 18 18.78 8.26 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 41075 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Tb1 Tb 0.12608(3) 1.05645(2) 0.10388(2) 0.00845(9) Uani 1 1 d . . . . . P1 P -0.13316(16) 0.97095(12) 0.11402(10) 0.0092(4) Uani 1 1 d . . . . . P2 P 0.16939(16) 0.81166(12) 0.02475(10) 0.0098(4) Uani 1 1 d . . . . . P3 P 0.33985(17) 0.97647(13) 0.32079(10) 0.0133(4) Uani 1 1 d . . . . . C1 C -0.0498(6) 0.6687(4) 0.1644(4) 0.0134(13) Uani 1 1 d . U . . . H1A H -0.0136 0.6339 0.2185 0.016 Uiso 1 1 calc R U . . . H1B H -0.1446 0.6557 0.1436 0.016 Uiso 1 1 calc R U . . . C2 C 0.0131(6) 0.6273(5) 0.1034(4) 0.0151(15) Uani 1 1 d . . . . . H2A H 0.0069 0.5524 0.1019 0.018 Uiso 1 1 calc R U . . . H2B H -0.0333 0.6533 0.0470 0.018 Uiso 1 1 calc R U . . . C3 C 0.2388(6) 0.6017(4) 0.1959(4) 0.0129(14) Uani 1 1 d . . . . . H3A H 0.2819 0.5478 0.1735 0.015 Uiso 1 1 calc R U . . . H3B H 0.1904 0.5690 0.2297 0.015 Uiso 1 1 calc R U . . . C4 C 0.3412(6) 0.6737(5) 0.2503(4) 0.0162(15) Uani 1 1 d . . . . . H4A H 0.3823 0.6420 0.3053 0.019 Uiso 1 1 calc R U . . . H4B H 0.4098 0.6854 0.2243 0.019 Uiso 1 1 calc R U . . . C5 C 0.1782(6) 0.7584(5) 0.3028(4) 0.0122(14) Uani 1 1 d . U . . . H5A H 0.1593 0.6849 0.3024 0.015 Uiso 1 1 calc R U . . . H5B H 0.2139 0.7797 0.3616 0.015 Uiso 1 1 calc R U . . . C6 C 0.0522(6) 0.8138(5) 0.2638(4) 0.0121(13) Uani 1 1 d . U . . . H6A H 0.0714 0.8872 0.2635 0.015 Uiso 1 1 calc R U . . . H6B H -0.0035 0.8042 0.2995 0.015 Uiso 1 1 calc R U . . . C7 C -0.1500(6) 0.8412(4) 0.1469(4) 0.0120(13) Uani 1 1 d . U . . . H7A H -0.1882 0.8435 0.1927 0.014 Uiso 1 1 calc R U . . . H7B H -0.2118 0.8046 0.0999 0.014 Uiso 1 1 calc R U . . . C8 C 0.1999(6) 0.6801(5) 0.0588(4) 0.0155(15) Uani 1 1 d . . . . . H8A H 0.1583 0.6345 0.0116 0.019 Uiso 1 1 calc R U . . . H8B H 0.2947 0.6670 0.0771 0.019 Uiso 1 1 calc R U . . . C9 C 0.3876(6) 0.8474(4) 0.3073(4) 0.0127(14) Uani 1 1 d . . . . . H9A H 0.4531 0.8500 0.2779 0.015 Uiso 1 1 d R U . . . H9B H 0.4310 0.8185 0.3631 0.015 Uiso 1 1 d R U . . . N1 N -0.0251(5) 0.7822(4) 0.1757(3) 0.0113(10) Uani 1 1 d . U . . . H1C H 0.0220 0.8002 0.1428 0.014 Uiso 1 1 d R U . . . N2 N 0.1488(5) 0.6576(4) 0.1276(3) 0.0139(13) Uani 1 1 d . . . . . N3 N 0.2816(5) 0.7744(4) 0.2618(3) 0.0123(12) Uani 1 1 d . U . . . H3C H 0.2379 0.8032 0.2052 0.015 Uiso 1 1 calc R U . . . N4 N 0.1966(6) 1.2774(4) 0.1210(4) 0.0254(13) Uani 1 1 d . U . . . O1 O -0.0909(4) 0.9623(3) 0.0363(2) 0.0092(9) Uani 1 1 d . . . . . O2 O -0.0205(4) 1.0221(3) 0.1791(2) 0.0114(10) Uani 1 1 d . . . . . O3 O -0.2654(4) 1.0177(3) 0.0994(2) 0.0144(10) Uani 1 1 d . . . . . O4 O 0.1691(4) 0.8734(3) 0.1008(2) 0.0113(10) Uani 1 1 d . . . . . O5 O 0.2955(4) 0.8334(3) 0.0009(2) 0.0143(10) Uani 1 1 d . . . . . H5C H 0.2822 0.8826 -0.0321 0.021 Uiso 1 1 calc R U . . . O6 O 0.0482(4) 0.8219(3) -0.0490(2) 0.0110(10) Uani 1 1 d . . . . . O7 O 0.2547(4) 1.0146(3) 0.2382(2) 0.0162(10) Uani 1 1 d . . . . . O8 O 0.2557(4) 0.9680(3) 0.3814(2) 0.0168(11) Uani 1 1 d . . . . . H8C H 0.2835 1.0095 0.4206 0.025 Uiso 1 1 calc R U . . . O9 O 0.4651(4) 1.0311(3) 0.3623(3) 0.0168(11) Uani 1 1 d . . . . . O10 O 0.1977(4) 1.2383(3) 0.0543(3) 0.0195(11) Uani 1 1 d . . . . . O11 O 0.1891(4) 1.2193(3) 0.1795(3) 0.0177(11) Uani 1 1 d . . . . . O12 O 0.1991(5) 1.3712(4) 0.1303(3) 0.0357(12) Uani 1 1 d . U . . . O1W O 0.3437(4) 1.0645(3) 0.1008(2) 0.0198(10) Uani 1 1 d . . . . . H1WA H 0.4036 1.0206 0.1182 0.024 Uiso 1 1 d R U . . . H1WB H 0.3547 1.0991 0.0612 0.024 Uiso 1 1 d R U . . . O2W O 0.6545(4) 0.9342(4) 0.4794(2) 0.0256(11) Uani 1 1 d . . . . . H2WA H 0.6055 0.9792 0.4495 0.031 Uiso 1 1 d R U . . . H2WB H 0.6748 0.8896 0.4495 0.031 Uiso 1 1 d R U . . . O3W O 0.5508(5) 0.7141(4) 0.4814(3) 0.0328(13) Uani 1 1 d . . . . . H3WA H 0.5814 0.7724 0.4985 0.039 Uiso 1 1 d R U . . . H3WB H 0.4812 0.7033 0.4925 0.039 Uiso 1 1 d R U . . . O4W O 0.4527(4) 0.4402(4) 0.3381(3) 0.0265(11) Uani 1 1 d . . . . . H4WA H 0.3936 0.4634 0.3562 0.032 Uiso 1 1 d R U . . . H4WB H 0.4790 0.3854 0.3645 0.032 Uiso 1 1 d R U . . . O5W O 0.4165(5) 0.2309(4) 0.3279(3) 0.0372(14) Uani 1 1 d . . . . . H5WA H 0.3713 0.2238 0.2771 0.045 Uiso 1 1 d R U . . . H5WB H 0.4492 0.1742 0.3485 0.045 Uiso 1 1 d R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Tb1 0.01135(15) 0.00740(15) 0.00693(14) -0.00011(15) 0.00339(11) -0.00002(16) P1 0.0118(9) 0.0079(9) 0.0086(8) 0.0009(6) 0.0044(7) 0.0001(7) P2 0.0132(9) 0.0079(9) 0.0089(8) 0.0000(7) 0.0044(7) 0.0006(7) P3 0.0159(10) 0.0121(9) 0.0098(9) -0.0004(7) 0.0013(8) -0.0009(7) C1 0.013(3) 0.007(3) 0.015(3) 0.003(2) -0.001(3) -0.006(2) C2 0.024(4) 0.008(3) 0.012(4) 0.003(3) 0.003(3) 0.001(3) C3 0.015(4) 0.009(3) 0.013(3) 0.002(3) 0.002(3) 0.006(3) C4 0.016(4) 0.011(4) 0.018(4) -0.002(3) 0.002(3) 0.004(3) C5 0.021(4) 0.009(3) 0.004(3) 0.003(3) 0.002(3) -0.001(3) C6 0.013(3) 0.012(3) 0.012(3) 0.003(2) 0.006(2) -0.003(2) C7 0.012(3) 0.009(3) 0.016(3) 0.001(2) 0.005(2) -0.004(2) C8 0.028(4) 0.008(3) 0.015(4) 0.002(3) 0.013(3) 0.002(3) C9 0.011(3) 0.014(4) 0.011(3) -0.004(3) 0.001(3) -0.005(3) N1 0.013(2) 0.008(2) 0.014(2) 0.0023(18) 0.0054(19) -0.0021(18) N2 0.021(3) 0.011(3) 0.011(3) 0.003(2) 0.008(3) -0.003(2) N3 0.011(3) 0.013(3) 0.011(3) 0.002(2) 0.001(2) 0.002(2) N4 0.036(3) 0.012(2) 0.031(3) -0.003(3) 0.014(3) -0.005(3) O1 0.010(2) 0.012(3) 0.006(2) -0.0013(18) 0.0039(18) 0.0045(18) O2 0.013(2) 0.013(2) 0.008(2) -0.0019(18) 0.004(2) -0.0037(19) O3 0.016(3) 0.016(2) 0.014(2) 0.0016(19) 0.010(2) 0.002(2) O4 0.018(3) 0.007(2) 0.009(2) 0.0024(18) 0.004(2) 0.0052(19) O5 0.013(2) 0.012(2) 0.017(3) 0.0030(19) 0.005(2) 0.0041(19) O6 0.013(2) 0.007(2) 0.010(2) -0.0048(18) -0.0011(19) 0.0009(19) O7 0.018(3) 0.019(3) 0.010(2) -0.0039(19) 0.002(2) -0.001(2) O8 0.022(3) 0.014(3) 0.014(2) -0.0056(19) 0.006(2) -0.007(2) O9 0.016(3) 0.012(3) 0.020(2) 0.0002(19) 0.002(2) -0.0034(19) O10 0.020(3) 0.025(3) 0.015(3) -0.003(2) 0.008(2) 0.001(2) O11 0.031(3) 0.011(2) 0.013(2) 0.001(2) 0.011(2) -0.004(2) O12 0.054(3) 0.015(2) 0.041(3) -0.004(2) 0.020(2) -0.007(2) O1W 0.013(2) 0.024(3) 0.023(2) 0.014(2) 0.007(2) 0.008(2) O2W 0.032(3) 0.025(3) 0.016(2) -0.006(2) 0.003(2) 0.006(3) O3W 0.028(3) 0.032(3) 0.043(3) -0.001(3) 0.018(3) 0.001(3) O4W 0.020(3) 0.025(3) 0.042(3) 0.000(3) 0.020(2) 0.001(2) O5W 0.034(3) 0.020(3) 0.048(4) -0.008(3) 0.001(3) 0.001(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Tb Tb -0.1723 4.1537 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 O1 Tb1 O7 146.93(14) 3_575 . O1 Tb1 O2 127.97(13) 3_575 . O7 Tb1 O2 73.96(14) . . O1 Tb1 O1W 79.75(14) 3_575 . O7 Tb1 O1W 75.08(14) . . O2 Tb1 O1W 149.02(14) . . O1 Tb1 O6 79.68(13) 3_575 3_575 O7 Tb1 O6 133.07(13) . 3_575 O2 Tb1 O6 76.13(13) . 3_575 O1W Tb1 O6 128.20(14) . 3_575 O1 Tb1 O4 80.98(13) 3_575 . O7 Tb1 O4 74.33(14) . . O2 Tb1 O4 89.31(13) . . O1W Tb1 O4 81.23(14) . . O6 Tb1 O4 140.30(13) 3_575 . O1 Tb1 O11 123.75(14) 3_575 . O7 Tb1 O11 73.62(14) . . O2 Tb1 O11 90.48(13) . . O1W Tb1 O11 82.00(14) . . O6 Tb1 O11 71.32(14) 3_575 . O4 Tb1 O11 146.68(14) . . O1 Tb1 O1 70.13(14) 3_575 . O7 Tb1 O1 119.90(13) . . O2 Tb1 O1 58.49(12) . . O1W Tb1 O1 141.36(13) . . O6 Tb1 O1 70.08(13) 3_575 . O4 Tb1 O1 70.83(13) . . O11 Tb1 O1 135.00(13) . . O1 Tb1 O10 75.31(13) 3_575 . O7 Tb1 O10 111.61(14) . . O2 Tb1 O10 129.49(13) . . O1W Tb1 O10 64.75(14) . . O6 Tb1 O10 64.21(13) 3_575 . O4 Tb1 O10 141.19(13) . . O11 Tb1 O10 48.86(13) . . O1 Tb1 O10 126.32(13) . . O1 Tb1 Tb1 37.41(9) 3_575 3_575 O7 Tb1 Tb1 143.49(10) . 3_575 O2 Tb1 Tb1 90.92(10) . 3_575 O1W Tb1 Tb1 113.72(10) . 3_575 O6 Tb1 Tb1 71.15(9) 3_575 3_575 O4 Tb1 Tb1 72.41(9) . 3_575 O11 Tb1 Tb1 140.90(10) . 3_575 O1 Tb1 Tb1 32.73(8) . 3_575 O10 Tb1 Tb1 103.70(9) . 3_575 O3 P1 O2 116.2(2) . . O3 P1 O1 114.7(2) . . O2 P1 O1 105.5(2) . . O3 P1 C7 104.6(2) . . O2 P1 C7 109.2(3) . . O1 P1 C7 106.2(2) . . O6 P2 O4 114.8(2) . . O6 P2 O5 111.8(2) . . O4 P2 O5 110.9(2) . . O6 P2 C8 111.8(3) . . O4 P2 C8 106.7(3) . . O5 P2 C8 99.8(3) . . O7 P3 O9 118.4(3) . . O7 P3 O8 108.7(2) . . O9 P3 O8 110.6(2) . . O7 P3 C9 108.2(3) . . O9 P3 C9 104.9(3) . . O8 P3 C9 105.2(3) . . C2 C1 N1 110.1(5) . . C2 C1 H1A 109.6 . . N1 C1 H1A 109.6 . . C2 C1 H1B 109.6 . . N1 C1 H1B 109.6 . . H1A C1 H1B 108.2 . . N2 C2 C1 110.0(5) . . N2 C2 H2A 109.7 . . C1 C2 H2A 109.7 . . N2 C2 H2B 109.7 . . C1 C2 H2B 109.7 . . H2A C2 H2B 108.2 . . N2 C3 C4 109.9(5) . . N2 C3 H3A 109.7 . . C4 C3 H3A 109.7 . . N2 C3 H3B 109.7 . . C4 C3 H3B 109.7 . . H3A C3 H3B 108.2 . . N3 C4 C3 111.3(5) . . N3 C4 H4A 109.4 . . C3 C4 H4A 109.4 . . N3 C4 H4B 109.4 . . C3 C4 H4B 109.4 . . H4A C4 H4B 108.0 . . C6 C5 N3 115.6(5) . . C6 C5 H5A 108.4 . . N3 C5 H5A 108.4 . . C6 C5 H5B 108.4 . . N3 C5 H5B 108.4 . . H5A C5 H5B 107.4 . . C5 C6 N1 116.0(5) . . C5 C6 H6A 108.3 . . N1 C6 H6A 108.3 . . C5 C6 H6B 108.3 . . N1 C6 H6B 108.3 . . H6A C6 H6B 107.4 . . N1 C7 P1 114.7(4) . . N1 C7 H7A 108.6 . . P1 C7 H7A 108.6 . . N1 C7 H7B 108.6 . . P1 C7 H7B 108.6 . . H7A C7 H7B 107.6 . . N2 C8 P2 111.5(4) . . N2 C8 H8A 109.3 . . P2 C8 H8A 109.3 . . N2 C8 H8B 109.3 . . P2 C8 H8B 109.3 . . H8A C8 H8B 108.0 . . N3 C9 P3 117.5(4) . . N3 C9 H9A 108.4 . . P3 C9 H9A 108.0 . . N3 C9 H9B 107.3 . . P3 C9 H9B 108.0 . . H9A C9 H9B 107.2 . . C7 N1 C1 111.4(4) . . C7 N1 C6 109.6(5) . . C1 N1 C6 114.4(5) . . C7 N1 H1C 107.0 . . C1 N1 H1C 107.0 . . C6 N1 H1C 107.0 . . C2 N2 C3 116.6(5) . . C2 N2 C8 115.7(5) . . C3 N2 C8 114.0(5) . . C9 N3 C5 114.1(5) . . C9 N3 C4 109.7(4) . . C5 N3 C4 110.2(4) . . C9 N3 H3C 107.5 . . C5 N3 H3C 107.5 . . C4 N3 H3C 107.5 . . O12 N4 O10 121.3(6) . . O12 N4 O11 120.1(6) . . O10 N4 O11 118.6(6) . . P1 O1 Tb1 154.4(2) . 3_575 P1 O1 Tb1 93.49(18) . . Tb1 O1 Tb1 109.87(14) 3_575 . P1 O2 Tb1 102.38(19) . . P2 O4 Tb1 126.3(2) . . P2 O5 H5C 109.5 . . P2 O6 Tb1 138.2(2) . 3_575 P3 O7 Tb1 173.6(3) . . P3 O8 H8C 109.5 . . N4 O10 Tb1 89.9(4) . . N4 O11 Tb1 101.1(4) . . Tb1 O1W H1WA 128.0 . . Tb1 O1W H1WB 115.5 . . H1WA O1W H1WB 110.8 . . H2WA O2W H2WB 110.9 . . H3WA O3W H3WB 110.8 . . H4WA O4W H4WB 106.3 . . H5WA O5W H5WB 110.4 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Tb1 O1 2.300(4) 3_575 Tb1 O7 2.330(4) . Tb1 O2 2.377(4) . Tb1 O1W 2.380(4) . Tb1 O6 2.429(4) 3_575 Tb1 O4 2.463(4) . Tb1 O11 2.484(4) . Tb1 O1 2.585(4) . Tb1 O10 2.735(4) . Tb1 Tb1 4.0013(7) 3_575 P1 O3 1.507(4) . P1 O2 1.520(4) . P1 O1 1.533(4) . P1 C7 1.827(6) . P2 O6 1.506(4) . P2 O4 1.528(4) . P2 O5 1.571(4) . P2 C8 1.826(6) . P3 O7 1.500(4) . P3 O9 1.501(4) . P3 O8 1.582(4) . P3 C9 1.815(6) . C1 C2 1.511(8) . C1 N1 1.521(7) . C1 H1A 0.9900 . C1 H1B 0.9900 . C2 N2 1.453(7) . C2 H2A 0.9900 . C2 H2B 0.9900 . C3 N2 1.457(7) . C3 C4 1.529(8) . C3 H3A 0.9900 . C3 H3B 0.9900 . C4 N3 1.517(7) . C4 H4A 0.9900 . C4 H4B 0.9900 . C5 C6 1.505(8) . C5 N3 1.511(7) . C5 H5A 0.9900 . C5 H5B 0.9900 . C6 N1 1.523(7) . C6 H6A 0.9900 . C6 H6B 0.9900 . C7 N1 1.503(7) . C7 H7A 0.9900 . C7 H7B 0.9900 . C8 N2 1.473(7) . C8 H8A 0.9900 . C8 H8B 0.9900 . C9 N3 1.511(7) . C9 H9A 0.9900 . C9 H9B 0.9901 . N1 H1C 0.9001 . N3 H3C 1.0000 . N4 O12 1.246(7) . N4 O10 1.247(6) . N4 O11 1.277(6) . O1 Tb1 2.300(4) 3_575 O5 H5C 0.8400 . O6 Tb1 2.429(4) 3_575 O8 H8C 0.8400 . O1W H1WA 0.8502 . O1W H1WB 0.8510 . O2W H2WA 0.8496 . O2W H2WB 0.8513 . O3W H3WA 0.8519 . O3W H3WB 0.8460 . O4W H4WA 0.8497 . O4W H4WB 0.8497 . O5W H5WA 0.8513 . O5W H5WB 0.8547 . loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A O5W H5WB O9 0.85 1.90 2.715(6) 158.3 1_545 O5W H5WA O11 0.85 2.14 2.917(7) 151.8 1_545 O4W H4WB O5W 0.85 2.18 2.785(7) 128.6 . O4W H4WA O3 0.85 1.92 2.768(6) 177.8 2_545 O3W H3WB O5 0.85 2.12 2.958(6) 170.9 4_576 O3W H3WA O2W 0.85 2.33 3.118(7) 152.9 . O2W H2WB O12 0.85 2.22 2.926(6) 139.9 2_645 O2W H2WB O10 0.85 2.44 3.187(6) 146.9 2_645 O2W H2WB N4 0.85 2.57 3.397(7) 162.9 2_645 O2W H2WA O9 0.85 1.88 2.685(6) 157.0 . O1W H1WB O3W 0.85 2.08 2.856(6) 150.5 2_655 O1W H1WA O4W 0.85 1.84 2.681(6) 172.3 2_655 O8 H8C O2W 0.84 1.78 2.594(6) 163.8 3_676 O5 H5C O3 0.84 1.71 2.552(6) 176.2 3_575 N3 H3C O4 1.00 1.93 2.922(6) 172.5 . N1 H1C O4 0.90 2.17 3.033(6) 160.5 . C9 H9B O3W 0.99 2.44 3.411(8) 166.2 . C6 H6B O11 0.99 2.43 3.305(7) 147.6 2_545 C6 H6A O8 0.99 2.57 3.193(7) 120.9 . C6 H6A O2 0.99 2.30 3.085(7) 135.1 . C5 H5B O8 0.99 2.53 3.069(7) 114.2 . C4 H4B O5W 0.99 2.40 3.385(8) 173.1 2_655 C3 H3A O12 0.99 2.52 3.219(8) 127.4 1_545 C2 H2B O10 0.99 2.50 3.413(8) 153.7 3_575 C1 H1A O2 0.99 2.22 3.178(7) 162.4 2_545 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 N1 C1 C2 N2 51.8(7) . . . . N2 C3 C4 N3 39.9(7) . . . . N3 C5 C6 N1 64.7(7) . . . . O3 P1 C7 N1 -172.7(4) . . . . O2 P1 C7 N1 -47.7(5) . . . . O1 P1 C7 N1 65.6(5) . . . . O6 P2 C8 N2 -96.1(5) . . . . O4 P2 C8 N2 30.2(5) . . . . O5 P2 C8 N2 145.6(4) . . . . O7 P3 C9 N3 -49.1(5) . . . . O9 P3 C9 N3 -176.4(4) . . . . O8 P3 C9 N3 66.9(5) . . . . P1 C7 N1 C1 -154.0(4) . . . . P1 C7 N1 C6 78.3(5) . . . . C2 C1 N1 C7 116.9(5) . . . . C2 C1 N1 C6 -118.1(5) . . . . C5 C6 N1 C7 177.9(5) . . . . C5 C6 N1 C1 51.9(7) . . . . C1 C2 N2 C3 77.5(6) . . . . C1 C2 N2 C8 -144.2(5) . . . . C4 C3 N2 C2 -142.4(5) . . . . C4 C3 N2 C8 78.7(6) . . . . P2 C8 N2 C2 86.4(6) . . . . P2 C8 N2 C3 -134.2(5) . . . . P3 C9 N3 C5 -60.5(6) . . . . P3 C9 N3 C4 175.2(4) . . . . C6 C5 N3 C9 102.4(6) . . . . C6 C5 N3 C4 -133.7(5) . . . . C3 C4 N3 C9 -173.5(5) . . . . C3 C4 N3 C5 60.0(6) . . . . O3 P1 O1 Tb1 -30.1(6) . . . 3_575 O2 P1 O1 Tb1 -159.2(5) . . . 3_575 C7 P1 O1 Tb1 84.9(6) . . . 3_575 O3 P1 O1 Tb1 126.2(2) . . . . O2 P1 O1 Tb1 -3.0(2) . . . . C7 P1 O1 Tb1 -118.8(2) . . . . O3 P1 O2 Tb1 -125.0(2) . . . . O1 P1 O2 Tb1 3.3(2) . . . . C7 P1 O2 Tb1 117.1(2) . . . . O6 P2 O4 Tb1 -53.1(3) . . . . O5 P2 O4 Tb1 74.8(3) . . . . C8 P2 O4 Tb1 -177.5(3) . . . . O4 P2 O6 Tb1 24.4(4) . . . 3_575 O5 P2 O6 Tb1 -103.0(3) . . . 3_575 C8 P2 O6 Tb1 146.1(3) . . . 3_575 O12 N4 O10 Tb1 -166.1(6) . . . . O11 N4 O10 Tb1 12.0(6) . . . . O12 N4 O11 Tb1 164.6(5) . . . . O10 N4 O11 Tb1 -13.5(6) . . . .