#------------------------------------------------------------------------------ #$Date: 2019-10-07 12:07:06 +0300 (Mon, 07 Oct 2019) $ #$Revision: 219127 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/23/44/7234416.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7234416 loop_ _publ_author_name 'Rawad K. Hallani' 'Karl J. Thorley' 'Anna K. Hailey' 'Sean R. Parkin' 'Yueh-Lin Loo' 'John E. Anthony' _publ_section_title ; The effect of regioisomerism on the crystal packing and device performance of desymmetrized anthradithiophenes ; _journal_name_full 'Journal of Materials Chemistry C' _journal_page_first 8956 _journal_page_last 8962 _journal_paper_doi 10.1039/C5TC02145F _journal_volume 3 _journal_year 2015 _chemical_formula_moiety 'C32 H36 S2 Si' _chemical_formula_sum 'C32 H36 S2 Si' _chemical_formula_weight 512.82 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _cell_angle_alpha 90 _cell_angle_beta 105.8296(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 13.9118(1) _cell_length_b 8.7857(1) _cell_length_c 23.9007(2) _cell_measurement_reflns_used 70811 _cell_measurement_temperature 90.0(2) _cell_measurement_theta_max 27.48 _cell_measurement_theta_min 1.00 _cell_volume 2810.48(4) _computing_cell_refinement 'SCALEPACK (Otwinowski & Minor, 2006)' _computing_data_collection 'COLLECT (Nonius, 1998)' _computing_data_reduction 'DENZO-SMN (Otwinowski & Minor, 2006)' _computing_molecular_graphics 'XP in SHELXTL (Sheldrick, 2008)' _computing_publication_material 'SHELX (Sheldrick, 2008) and CIFFIX (Parkin, 2013)' _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2008)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 2008)' _diffrn_ambient_temperature 90.0(2) _diffrn_detector_area_resol_mean 9.1 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Nonius KappaCCD diffractometer' _diffrn_measurement_method '\f and \w scans at fixed \c = 55\%' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0435 _diffrn_reflns_av_unetI/netI 0.0246 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 30 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_number 77455 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.487 _diffrn_reflns_theta_min 1.521 _diffrn_source 'fine-focus sealed-tube' _exptl_absorpt_coefficient_mu 0.251 _exptl_absorpt_correction_T_max 0.956 _exptl_absorpt_correction_T_min 0.826 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS (Sheldrick, 2008)' _exptl_crystal_colour red _exptl_crystal_density_diffrn 1.212 _exptl_crystal_density_meas . _exptl_crystal_density_method . _exptl_crystal_description slab _exptl_crystal_F_000 1096 _exptl_crystal_size_max 0.250 _exptl_crystal_size_mid 0.220 _exptl_crystal_size_min 0.140 _exptl_transmission_factor_max . _exptl_transmission_factor_min . _refine_diff_density_max 0.614 _refine_diff_density_min -0.489 _refine_diff_density_rms 0.071 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.085 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 348 _refine_ls_number_reflns 6430 _refine_ls_number_restraints 70 _refine_ls_restrained_S_all 1.090 _refine_ls_R_factor_all 0.0993 _refine_ls_R_factor_gt 0.0743 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1425P)^2^+1.5728P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2189 _refine_ls_wR_factor_ref 0.2438 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 4634 _reflns_number_total 6430 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL k13120s in P2(1)/c CELL 0.71073 13.9118 8.7857 23.9007 90.000 105.8296 90.000 ZERR 4.00 0.0001 0.0001 0.0002 0.000 0.0003 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H SI S UNIT 128 144 4 8 TEMP -183 SIZE 0.25 0.22 0.14 REM FORM slab REM COLR red REM Cell: 70811, 1.00, 27.48 L.S. 8 BOND $H ACTA CONF LIST 4 FMAP 2 PLAN 5 REM EXTI 0.000000 not needed. WGHT 0.142500 1.572800 FVAR 0.49485 0.59131 0.50741 SI1 3 0.266380 0.195506 0.286525 11.00000 0.07414 0.08281 = 0.06634 -0.02964 0.01216 -0.02629 C1 1 0.421310 0.552827 0.413366 11.00000 0.03134 0.03529 = 0.04017 0.00289 0.00874 0.00300 C2 1 0.358106 0.651008 0.434515 11.00000 0.02814 0.03582 = 0.04653 0.00569 0.01056 0.00364 C3 1 0.252492 0.637850 0.415175 11.00000 0.02882 0.04053 = 0.05655 0.00412 0.00789 0.00128 AFIX 43 H3 2 0.222832 0.560774 0.388076 11.00000 -1.20000 AFIX 0 C4 1 0.192915 0.736477 0.435577 11.00000 0.02999 0.04153 = 0.06759 0.01141 0.01685 0.00517 C5 1 0.082956 0.743192 0.419963 11.00000 0.03383 0.04527 = 0.08934 0.01203 0.02181 0.00486 AFIX 43 H5 2 0.039903 0.676734 0.393081 11.00000 -1.20000 AFIX 0 C6 1 0.051814 0.855082 0.448604 11.00000 0.03566 0.05494 = 0.12054 0.01503 0.03369 0.00939 AFIX 43 H6 2 -0.017016 0.875903 0.443647 11.00000 -1.20000 AFIX 0 S7 4 0.146137 0.960181 0.495674 11.00000 0.04538 0.04713 = 0.10538 0.00510 0.03822 0.01096 C8 1 0.237475 0.850640 0.476984 11.00000 0.03679 0.03719 = 0.06934 0.01034 0.02617 0.00880 C9 1 0.338807 0.866485 0.497625 11.00000 0.03863 0.03529 = 0.05712 0.00110 0.01976 0.00569 AFIX 43 H9 2 0.366644 0.942558 0.525602 11.00000 -1.20000 AFIX 0 C10 1 0.402329 0.766606 0.476412 11.00000 0.03152 0.03367 = 0.04409 0.00401 0.01336 0.00469 C11 1 0.506125 0.780993 0.495094 11.00000 0.03332 0.03162 = 0.04387 0.00095 0.01031 0.00093 AFIX 43 H11 2 0.534711 0.857089 0.522897 11.00000 -1.20000 AFIX 0 C12 1 0.569023 0.686591 0.474025 11.00000 0.02812 0.03335 = 0.04282 0.00386 0.00964 0.00356 C13 1 0.674871 0.704399 0.493268 11.00000 0.02990 0.03389 = 0.04984 0.00309 0.00801 0.00016 AFIX 43 H13 2 0.703827 0.780491 0.520987 11.00000 -1.20000 AFIX 0 C14 1 0.734288 0.610395 0.471281 11.00000 0.02784 0.03855 = 0.05661 0.00900 0.01356 0.00280 S15 4 0.864125 0.612346 0.488195 11.00000 0.02820 0.04879 = 0.08672 0.00626 0.01667 0.00419 C16 1 0.862950 0.459672 0.442005 11.00000 0.03745 0.05590 = 0.08446 0.00971 0.02829 0.01217 AFIX 43 H16 2 0.922360 0.416356 0.436622 11.00000 -1.20000 AFIX 0 C17 1 0.771554 0.407392 0.414427 11.00000 0.04049 0.04912 = 0.06402 0.00594 0.02224 0.01131 AFIX 43 H17 2 0.759566 0.324737 0.387791 11.00000 -1.20000 AFIX 0 C18 1 0.693078 0.492550 0.430241 11.00000 0.03538 0.03941 = 0.05135 0.00754 0.01833 0.00828 C19 1 0.591271 0.473059 0.410951 11.00000 0.03516 0.03669 = 0.04411 0.00070 0.01380 0.00555 AFIX 43 H19 2 0.564132 0.395126 0.383659 11.00000 -1.20000 AFIX 0 C20 1 0.526396 0.569900 0.431931 11.00000 0.03097 0.03643 = 0.04061 0.00547 0.01159 0.00452 C21 1 0.376832 0.435874 0.372778 11.00000 0.03458 0.04522 = 0.04677 0.00089 0.00882 0.00280 C22 1 0.335371 0.338330 0.338956 11.00000 0.04881 0.05888 = 0.05222 -0.00689 0.00914 -0.00428 C23 1 0.132648 0.206504 0.291561 11.00000 0.08143 0.11513 = 0.08274 -0.00995 -0.00407 -0.03367 AFIX 13 H23 2 0.110859 0.313965 0.281677 11.00000 -1.20000 AFIX 0 C24 1 0.059204 0.104401 0.244328 11.00000 0.11359 0.24058 = 0.14043 -0.06662 -0.00189 -0.05816 AFIX 137 H24A 2 0.068769 -0.002793 0.255841 11.00000 -1.50000 H24B 2 0.073220 0.118455 0.206642 11.00000 -1.50000 H24C 2 -0.009956 0.134180 0.241189 11.00000 -1.50000 AFIX 0 C25 1 0.120530 0.179180 0.350174 11.00000 0.07060 0.11332 = 0.09717 0.00060 0.01159 -0.02281 AFIX 23 H25A 2 0.171699 0.239119 0.378527 11.00000 -1.20000 H25B 2 0.133866 0.070266 0.359847 11.00000 -1.20000 AFIX 0 C26 1 0.016528 0.219787 0.357915 11.00000 0.07835 0.12092 = 0.11206 -0.01409 0.01244 0.00556 AFIX 137 H26A 2 0.000695 0.326034 0.346609 11.00000 -1.50000 H26B 2 0.017283 0.205929 0.398718 11.00000 -1.50000 H26C 2 -0.034172 0.153081 0.333315 11.00000 -1.50000 AFIX 0 EADP C27 C27' EADP C28 C28' EADP C29 C29' EADP C30 C30' SAME 0.020 C27' C28' C29' C30' RIGU 0.01 C27 > C30' PART 1 C27 1 0.333413 0.005027 0.308430 21.00000 0.15145 0.07437 = 0.12729 -0.04683 -0.02259 0.01132 AFIX 13 H27 2 0.294916 -0.036362 0.334788 21.00000 -1.20000 AFIX 0 C28 1 0.439282 0.002799 0.348977 21.00000 0.11340 0.07490 = 0.09147 -0.01281 0.03397 0.01321 AFIX 137 H28A 2 0.457013 -0.101474 0.362445 21.00000 -1.50000 H28B 2 0.442580 0.068823 0.382498 21.00000 -1.50000 H28C 2 0.486222 0.039619 0.328020 21.00000 -1.50000 AFIX 0 C29 1 0.318211 -0.119060 0.264065 21.00000 0.25726 0.10419 = 0.18603 -0.08926 -0.03109 0.01145 AFIX 23 H29A 2 0.252087 -0.159262 0.264801 21.00000 -1.20000 H29B 2 0.304923 -0.059938 0.227487 21.00000 -1.20000 AFIX 0 C30 1 0.358093 -0.232663 0.251496 21.00000 0.26369 0.11293 = 0.16740 -0.08263 -0.02359 0.01003 AFIX 137 H30A 2 0.421283 -0.204489 0.243590 21.00000 -1.50000 H30B 2 0.313876 -0.280034 0.216819 21.00000 -1.50000 H30C 2 0.371192 -0.304818 0.283972 21.00000 -1.50000 AFIX 0 PART 2 C27' 1 0.326344 0.030495 0.289539 -21.00000 0.15145 0.07437 = 0.12729 -0.04683 -0.02259 0.01132 AFIX 13 H27' 2 0.388904 0.053274 0.278186 -21.00000 -1.20000 AFIX 0 C28' 1 0.359328 -0.021533 0.352015 -21.00000 0.11340 0.07490 = 0.09147 -0.01281 0.03397 0.01321 AFIX 33 H28D 2 0.394866 0.061442 0.376497 -21.00000 -1.50000 H28E 2 0.403882 -0.109451 0.355309 -21.00000 -1.50000 H28F 2 0.300667 -0.050389 0.364828 -21.00000 -1.50000 AFIX 0 C29' 1 0.275455 -0.096971 0.250432 -21.00000 0.25726 0.10419 = 0.18603 -0.08926 -0.03109 0.01145 AFIX 23 H29C 2 0.225529 -0.044972 0.218658 -21.00000 -1.20000 H29D 2 0.327230 -0.135303 0.232642 -21.00000 -1.20000 AFIX 0 C30' 1 0.232420 -0.212287 0.259796 -21.00000 0.26369 0.11293 = 0.16740 -0.08263 -0.02359 0.01003 AFIX 33 H30D 2 0.201589 -0.263903 0.222914 -21.00000 -1.50000 H30E 2 0.180604 -0.184324 0.278654 -21.00000 -1.50000 H30F 2 0.280725 -0.280661 0.285293 -21.00000 -1.50000 AFIX 0 PART 0 EADP C31 C31' EADP C32 C32' EADP C33 C33' EADP C34 C34' SAmE 0.02 C31' c32' c33' c34' RIGU 0.005 C31 > C34' PART 1 C31 1 0.286565 0.230203 0.214757 31.00000 0.12327 0.08382 = 0.07172 -0.02758 0.01789 -0.02706 AFIX 13 H31 2 0.249071 0.153261 0.186226 31.00000 -1.20000 AFIX 0 C32 1 0.396156 0.233914 0.213785 31.00000 0.14928 0.14495 = 0.12362 -0.02247 0.04562 -0.01403 AFIX 137 H32A 2 0.399695 0.245737 0.173623 31.00000 -1.50000 H32B 2 0.428864 0.138637 0.229893 31.00000 -1.50000 H32C 2 0.430037 0.319743 0.237216 31.00000 -1.50000 AFIX 0 C33 1 0.246849 0.382948 0.197503 31.00000 0.15781 0.11878 = 0.07841 -0.00206 0.05131 -0.00613 AFIX 23 H33A 2 0.287534 0.456651 0.225471 31.00000 -1.20000 H33B 2 0.178115 0.387288 0.201809 31.00000 -1.20000 AFIX 0 C34 1 0.243139 0.437042 0.136540 31.00000 0.18387 0.13300 = 0.06952 -0.00979 0.04318 -0.04624 AFIX 137 H34A 2 0.307878 0.480920 0.136486 31.00000 -1.50000 H34B 2 0.190890 0.514417 0.124221 31.00000 -1.50000 H34C 2 0.228256 0.350664 0.109609 31.00000 -1.50000 AFIX 0 PARt 2 C31' 1 0.248736 0.293591 0.210513 -31.00000 0.12327 0.08382 = 0.07172 -0.02758 0.01789 -0.02706 AFIX 13 H31' 2 0.220667 0.213158 0.180970 -31.00000 -1.20000 AFIX 0 C32' 1 0.176487 0.426711 0.195276 -31.00000 0.14928 0.14495 = 0.12362 -0.02247 0.04562 -0.01403 AFIX 33 H32D 2 0.109884 0.393648 0.196637 -31.00000 -1.50000 H32E 2 0.173413 0.463062 0.156061 -31.00000 -1.50000 H32F 2 0.199588 0.509239 0.223307 -31.00000 -1.50000 AFIX 0 C33' 1 0.344968 0.340170 0.199787 -31.00000 0.15781 0.11878 = 0.07841 -0.00206 0.05131 -0.00613 AFIX 23 H33C 2 0.388266 0.248897 0.205196 -31.00000 -1.20000 H33D 2 0.377407 0.413344 0.230672 -31.00000 -1.20000 AFIX 0 C34' 1 0.345254 0.410930 0.142061 -31.00000 0.18387 0.13300 = 0.06952 -0.00979 0.04318 -0.04624 AFIX 33 H34D 2 0.409801 0.460322 0.145595 -31.00000 -1.50000 H34E 2 0.291733 0.486741 0.131038 -31.00000 -1.50000 H34F 2 0.334413 0.331522 0.112192 -31.00000 -1.50000 PART 0 AFIX 0 HKLF 4 REM k13120s in P2(1)/c REM R1 = 0.0743 for 4634 Fo > 4sig(Fo) and 0.0993 for all 6430 data REM 348 parameters refined using 70 restraints END WGHT 0.1420 1.5779 REM Highest difference peak 0.614, deepest hole -0.489, 1-sigma level 0.071 Q1 1 0.0992 0.2812 0.3266 11.00000 0.05 0.61 Q2 1 0.1802 0.2441 0.1631 11.00000 0.05 0.61 Q3 1 0.1596 0.1230 0.3191 11.00000 0.05 0.56 Q4 1 0.1695 0.9451 0.5331 11.00000 0.05 0.52 Q5 1 0.0821 0.3955 0.2799 11.00000 0.05 0.45 ; _cod_data_source_file J-Mater-Chem-C-2015-3-8956.cif _cod_data_source_block k13120u _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 7234416 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.940 _shelx_estimated_absorpt_t_max 0.966 _shelxl_version_number 2013-4 _shelx_res_checksum 57448 _shelx_hkl_file ; 1 0 0 359.78 16.28 1 0 0 379.09 16.28 -1 0 0 396.73 13.96 -1 0 0 369.55 17.72 1 0 0 396.15 10.82 1 0 0 377.15 15.12 -1 0 0 372.27 17.29 -1 0 0 404.25 10.55 1 0 0 367.15 13.73 1 0 0 393.55 10.74 -1 0 0 370.09 17.33 1 0 0 392.78 12.17 1 0 0 385.56 15.04 -1 0 0 376.10 12.56 -1 0 0 406.62 13.76 1 0 0 366.35 26.48 1 0 0 388.42 24.26 -1 0 0 399.34 24.33 -1 0 0 381.34 25.98 2 0 0 6181.84 398.27 -2 0 0 6134.64 424.62 -2 0 0 6015.23 392.41 2 0 0 6033.04 399.68 -3 0 0 51.957 3.102 -3 0 0 55.679 1.939 3 0 0 52.461 2.210 -3 0 0 57.424 2.830 3 0 0 53.469 2.171 3 0 0 53.159 1.784 3 0 0 54.516 2.598 -3 0 0 59.052 2.404 3 0 0 53.624 1.861 3 0 0 56.687 2.094 -3 0 0 49.979 1.861 3 0 0 58.005 2.016 -3 0 0 52.034 1.900 3 0 0 57.113 2.210 -3 0 0 51.879 1.939 3 0 0 53.875 4.400 3 0 0 53.216 4.787 -3 0 0 56.881 4.739 -3 0 0 50.911 4.642 -4 0 0 1566.92 42.50 4 0 0 1620.39 56.07 -4 0 0 1524.69 54.67 -4 0 0 1553.89 39.94 -4 0 0 1590.26 50.25 4 0 0 1563.78 42.53 4 0 0 1549.82 41.26 -4 0 0 1664.98 53.86 4 0 0 1608.06 45.56 4 0 0 1519.11 47.03 -4 0 0 1598.67 52.31 4 0 0 1589.56 54.86 4 0 0 1575.68 42.50 4 0 0 1531.28 63.39 -4 0 0 1549.20 38.23 -4 0 0 1676.27 102.73 4 0 0 1631.47 103.03 4 0 0 1678.14 102.72 -4 0 0 1728.36 103.79 5 0 0 354.93 12.21 -5 0 0 367.57 9.42 -5 0 0 375.56 11.09 5 0 0 380.14 10.70 5 0 0 360.17 12.56 5 0 0 356.45 10.55 -5 0 0 358.00 13.84 -5 0 0 360.32 12.21 -5 0 0 375.33 11.71 5 0 0 384.21 12.37 5 0 0 378.20 10.97 5 0 0 364.20 14.23 -5 0 0 374.55 10.93 5 0 0 361.80 13.45 -5 0 0 383.70 11.21 -5 0 0 393.83 25.08 -5 0 0 373.49 24.79 5 0 0 360.83 25.23 5 0 0 368.44 24.25 6 0 0 0.1939 0.8918 -6 0 0 1.2020 1.0857 6 0 0 0.5041 1.0081 6 0 0 0.1551 1.0857 6 0 0 0.4653 0.8918 -6 0 0 0.0775 1.0469 6 0 0 -0.2714 0.9693 -6 0 0 2.0162 1.0081 -6 0 0 0.3490 1.0081 -6 0 0 1.2408 1.1632 -6 0 0 0.0000 0.9306 6 0 0 1.9294 4.1098 6 0 0 4.6502 5.3610 -6 0 0 -4.690 2.915 -6 0 0 1.6618 3.5026 -7 0 0 911.84 43.74 -7 0 0 893.89 27.99 7 0 0 839.80 37.38 -7 0 0 878.92 27.53 7 0 0 880.20 48.82 7 0 0 874.96 25.32 7 0 0 894.04 29.00 7 0 0 912.54 23.54 -7 0 0 896.02 24.97 -7 0 0 868.30 25.86 -7 0 0 911.80 47.73 8 0 0 947.97 29.43 8 0 0 925.95 72.04 8 0 0 952.24 25.32 -8 0 0 950.96 27.88 -8 0 0 916.99 26.79 -8 0 0 966.66 89.88 -8 0 0 957.98 29.70 -8 0 0 952.32 26.91 -8 0 0 990.28 43.35 8 0 0 948.36 32.41 -9 0 0 5.9711 1.4734 -9 0 0 5.0793 1.5897 9 0 0 4.0712 1.6285 9 0 0 2.6754 2.2876 9 0 0 4.8079 2.4427 9 0 0 5.6997 1.7448 -9 0 0 2.5203 1.4734 9 0 0 3.9937 2.2876 -9 0 0 4.0712 1.6673 -10 0 0 683.35 20.05 -10 0 0 689.51 19.58 10 0 0 681.41 19.12 10 0 0 688.81 22.68 10 0 0 660.12 21.29 -10 0 0 691.33 19.58 -10 0 0 668.38 23.73 10 0 0 666.09 23.88 -11 0 0 640.85 20.63 11 0 0 623.01 29.74 -11 0 0 628.09 26.21 11 0 0 644.73 31.48 -11 0 0 648.37 21.79 11 0 0 636.62 21.67 11 0 0 616.27 25.24 -11 0 0 629.80 19.15 -12 0 0 14.114 2.133 12 0 0 11.787 3.218 12 0 0 12.912 2.908 12 0 0 11.903 3.102 -12 0 0 11.089 2.133 12 0 0 11.128 2.792 -12 0 0 13.454 2.792 -12 0 0 12.950 2.482 -13 0 0 2.3652 3.4121 13 0 0 5.5058 3.1407 -13 0 0 1.6673 3.1019 -13 0 0 1.5897 3.3733 -13 0 0 0.1551 2.4427 13 0 0 1.5509 2.4427 13 0 0 1.9387 2.2101 13 0 0 -2.249 2.675 14 0 0 130.32 8.18 14 0 0 130.28 8.10 14 0 0 142.49 10.31 -14 0 0 127.68 9.11 -14 0 0 137.22 9.03 -14 0 0 150.17 9.11 14 0 0 154.55 8.45 -14 0 0 152.85 8.45 -15 0 0 187.00 12.14 15 0 0 201.43 11.67 -15 0 0 179.87 12.91 15 0 0 185.30 15.32 -15 0 0 206.59 13.49 -15 0 0 215.04 13.80 16 0 0 11.903 4.381 -16 0 0 14.850 5.351 -16 0 0 19.232 5.932 -16 0 0 18.417 5.700 -16 0 0 16.905 5.312 -17 0 0 23.807 5.932 17 0 0 32.609 8.375 -17 0 0 29.003 7.871 -17 0 0 17.254 5.351 -17 0 0 29.313 4.692 0 -1 0 0.1939 0.2326 0 -1 0 -0.1551 0.2326 0 -1 0 -0.1939 0.3490 0 -1 0 -1.241 0.349 0 -1 0 -0.4653 0.2714 0 -1 0 -0.0388 0.3490 0 -1 0 -0.7755 0.2326 0 -1 0 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1.8224 -9 -2 0 2.6754 1.3571 9 2 0 3.1019 2.4040 9 2 0 2.2101 1.1632 -9 2 0 4.4590 2.7141 9 2 0 2.8692 0.8142 9 2 0 0.8530 2.5203 -9 2 0 2.8305 1.3183 -9 2 0 4.1875 2.0938 -9 2 0 2.5203 1.2020 9 2 0 0.2326 2.2101 -9 2 0 7.7159 2.9080 -10 -2 0 107.17 5.43 10 -2 0 104.15 6.16 -10 -2 0 105.43 4.54 10 -2 0 100.38 5.47 10 -2 0 93.444 4.537 -10 -2 0 109.07 5.62 -10 -2 0 93.677 4.381 -10 2 0 104.15 4.89 10 2 0 103.06 5.31 -10 2 0 98.717 5.855 -10 2 0 113.02 6.44 10 2 0 100.93 6.09 10 2 0 99.338 3.761 -10 2 0 96.314 4.769 10 2 0 107.52 5.20 10 2 0 95.189 5.041 11 -2 0 138.38 5.54 -11 -2 0 159.40 5.31 11 -2 0 144.39 7.68 11 -2 0 148.08 7.25 -11 -2 0 156.26 9.00 -11 -2 0 151.10 5.16 -11 -2 0 155.91 5.16 -11 2 0 147.88 6.86 -11 2 0 146.60 6.40 -11 2 0 145.59 7.52 11 2 0 144.39 6.48 11 2 0 131.02 6.01 11 2 0 143.97 7.95 11 2 0 149.36 8.65 -11 2 0 149.94 6.75 -12 -2 0 47.847 4.498 -12 -2 0 40.673 3.606 -12 -2 0 57.230 5.312 -12 -2 0 54.981 4.149 12 -2 0 48.816 4.498 12 2 0 45.481 4.188 -12 2 0 41.643 4.653 12 2 0 49.553 4.420 -12 2 0 50.600 3.955 -12 2 0 48.777 4.653 -12 2 0 46.722 4.730 12 2 0 38.463 3.955 12 2 0 52.267 5.118 -13 -2 0 161.30 6.55 -13 -2 0 178.32 6.71 13 -2 0 153.04 10.00 -13 -2 0 160.29 6.63 -13 -2 0 161.07 9.34 -13 2 0 173.05 8.49 13 2 0 152.85 9.96 13 2 0 162.15 11.52 -13 2 0 165.95 7.60 -13 2 0 164.24 7.10 -13 2 0 160.02 8.45 13 2 0 155.40 9.77 13 2 0 147.34 9.15 -14 -2 0 44.163 5.234 -14 -2 0 41.333 5.234 -14 -2 0 54.244 6.204 14 -2 0 42.806 4.459 -14 -2 0 39.200 4.071 -14 2 0 49.863 6.824 14 2 0 41.061 5.545 -14 2 0 41.139 4.575 14 2 0 53.701 4.381 -14 2 0 47.149 5.273 -15 -2 0 0.1939 3.6447 15 -2 0 2.0550 4.9242 -15 -2 0 1.3571 3.3733 -15 -2 0 4.1488 3.0631 -15 -2 0 -0.1551 3.2182 15 -2 0 1.9775 2.6754 15 2 0 -0.4653 4.3814 -15 2 0 -2.675 2.482 15 2 0 4.1100 3.1019 -15 2 0 -1.551 4.692 -15 2 0 -1.706 4.885 -15 2 0 -1.435 4.808 16 -2 0 15.005 4.498 16 -2 0 6.7078 4.5365 -16 -2 0 12.679 5.583 -16 -2 0 8.9955 4.9630 -16 -2 0 11.865 5.234 -16 -2 0 11.128 6.087 16 2 0 15.122 6.669 -16 2 0 3.8774 6.0875 -16 2 0 6.3589 5.2732 16 2 0 17.409 5.428 -16 2 0 17.448 5.661 -17 -2 0 -2.986 3.645 -17 -2 0 0.1163 4.0712 -17 -2 0 1.2795 3.9161 -17 -2 0 -5.273 4.188 17 -2 0 3.5284 5.1181 -17 2 0 6.2038 6.6303 -17 2 0 1.1244 6.9792 -17 2 0 4.1100 6.3976 17 2 0 2.0938 5.3895 -17 2 0 1.5897 5.8160 -17 2 0 1.3958 7.2894 0 -3 0 0.1939 0.9693 0 -3 0 0.1163 0.6592 0 -3 0 0.3102 0.6979 0 -3 0 -1.396 1.124 0 -3 0 0.3877 0.6592 0 -3 0 -0.3877 0.6979 0 -3 0 1.0469 0.8530 0 -3 0 1.7836 0.8530 0 -3 0 -1.202 1.202 0 -3 0 -0.8142 1.2795 0 -3 0 -0.6979 0.6204 0 -3 0 0.0388 0.4265 0 3 0 -1.124 0.969 0 3 0 -0.4265 0.6592 0 3 0 -1.124 0.892 0 3 0 -0.2714 0.8142 0 3 0 0.3877 0.7755 0 3 0 0.5041 0.8530 0 3 0 1.4346 0.9693 -1 -3 0 330.04 10.74 1 -3 0 339.46 12.06 -1 -3 0 326.55 9.93 1 -3 0 348.38 9.96 1 -3 0 331.55 9.62 1 -3 0 336.63 10.16 -1 -3 0 324.81 9.00 -1 -3 0 328.02 11.24 -1 -3 0 327.56 12.33 -1 -3 0 309.96 9.89 -1 -3 0 316.78 8.65 -1 -3 0 324.19 10.12 1 -3 0 336.75 11.67 1 -3 0 332.75 10.39 1 -3 0 308.83 9.46 1 -3 0 332.13 11.40 1 -3 0 332.68 9.34 -1 -3 0 331.28 12.37 -1 -3 0 326.71 11.71 -1 -3 0 329.81 10.39 -1 3 0 324.15 10.47 -1 3 0 326.71 10.47 -1 3 0 318.02 11.48 1 3 0 317.21 10.78 -1 3 0 319.88 12.06 1 3 0 325.66 11.44 -1 3 0 305.57 8.76 -1 3 0 329.23 12.14 -1 3 0 312.32 11.44 -1 3 0 325.08 9.77 1 3 0 328.22 11.01 1 3 0 326.51 10.12 1 -3 0 360.70 21.29 1 -3 0 334.68 22.60 -1 3 0 343.26 21.39 -1 3 0 331.95 22.49 -2 -3 0 90.342 4.381 -2 -3 0 89.102 3.179 2 -3 0 88.598 3.722 2 -3 0 90.614 4.188 -2 -3 0 90.459 4.188 -2 -3 0 88.249 3.800 -2 -3 0 83.984 2.637 2 -3 0 90.071 3.451 -2 -3 0 94.995 4.149 2 -3 0 97.516 4.265 2 -3 0 92.126 3.451 2 -3 0 88.016 3.451 -2 -3 0 84.759 3.335 2 -3 0 90.846 3.451 -2 -3 0 91.699 2.753 2 -3 0 88.636 4.343 2 -3 0 88.985 3.839 2 3 0 99.299 4.692 -2 3 0 87.589 3.451 2 3 0 90.846 3.296 2 3 0 92.785 4.149 -2 3 0 93.328 3.335 -2 3 0 87.589 3.722 2 3 0 85.302 3.179 2 3 0 93.987 3.490 -2 3 0 90.691 3.141 -2 3 0 91.195 3.335 -2 3 0 87.434 3.373 2 3 0 91.855 4.110 -2 3 0 83.402 2.986 2 3 0 85.030 3.179 -2 -3 0 89.606 6.655 2 -3 0 98.634 6.824 -2 -3 0 95.850 6.396 2 -3 0 89.640 6.581 -2 3 0 87.793 6.830 -2 3 0 95.066 6.914 2 3 0 86.594 6.107 2 3 0 93.243 6.792 -3 -3 0 317.79 12.10 -3 -3 0 318.60 11.52 3 -3 0 319.34 11.05 -3 -3 0 327.75 10.04 3 -3 0 308.37 9.65 3 -3 0 318.87 10.90 -3 -3 0 312.55 9.38 -3 -3 0 306.54 8.22 -3 -3 0 310.58 8.96 -3 -3 0 317.90 10.66 3 -3 0 322.09 9.81 3 -3 0 322.87 11.28 3 -3 0 315.00 8.18 -3 -3 0 317.17 10.90 3 -3 0 318.18 10.24 3 -3 0 320.08 11.13 3 -3 0 308.02 10.39 -3 3 0 307.51 8.80 3 3 0 322.56 13.57 3 3 0 322.05 9.31 3 3 0 315.50 8.84 -3 3 0 304.92 10.35 -3 3 0 304.53 9.23 3 3 0 315.77 10.59 -3 3 0 314.30 9.54 -3 3 0 302.78 11.09 -3 3 0 310.81 9.46 3 3 0 303.56 11.52 -3 3 0 297.04 9.31 -3 -3 0 312.25 20.38 -3 -3 0 326.13 20.58 3 -3 0 324.87 20.83 3 -3 0 327.63 20.72 -3 3 0 332.83 21.31 3 3 0 338.16 20.25 -3 3 0 320.49 20.91 3 3 0 322.67 20.37 4 -3 0 12.330 2.094 4 -3 0 13.803 1.822 -4 -3 0 11.244 1.667 -4 -3 0 11.826 1.318 -4 -3 0 9.9260 1.7448 -4 -3 0 14.307 1.939 4 -3 0 10.895 1.590 4 -3 0 12.640 0.698 -4 -3 0 12.485 0.969 4 -3 0 11.593 0.892 4 -3 0 11.787 0.969 4 -3 0 14.424 2.133 -4 -3 0 10.314 1.357 4 3 0 13.454 2.016 4 3 0 14.850 1.357 -4 3 0 14.307 1.822 -4 3 0 13.842 1.551 -4 3 0 15.354 1.628 4 3 0 12.524 0.969 4 3 0 11.516 1.241 -4 3 0 9.9260 1.3571 -4 3 0 10.934 0.892 -4 3 0 13.144 1.435 4 3 0 13.958 1.667 -4 3 0 12.912 1.628 -4 -3 0 12.497 3.270 -4 -3 0 10.644 3.050 4 -3 0 9.2021 3.8365 4 -3 0 4.5723 3.5447 -4 3 0 7.3361 4.5118 4 3 0 10.452 2.630 4 3 0 19.079 3.710 -4 3 0 7.2772 4.2151 -5 -3 0 55.563 2.869 5 -3 0 55.214 2.947 -5 -3 0 55.407 2.947 -5 -3 0 56.920 2.947 5 -3 0 48.583 3.179 5 -3 0 56.920 2.094 -5 3 0 63.240 2.365 -5 3 0 54.012 2.249 -5 3 0 59.401 2.986 5 3 0 54.244 3.994 5 3 0 46.722 3.063 -5 3 0 57.075 2.675 -5 3 0 61.844 2.869 5 3 0 56.842 2.792 5 3 0 59.130 2.792 -5 3 0 56.609 2.482 5 3 0 54.012 1.900 -6 -3 0 23.691 2.365 6 -3 0 24.505 1.357 -6 -3 0 26.715 1.086 6 -3 0 25.203 1.202 6 -3 0 25.319 2.404 -6 -3 0 27.219 1.822 6 -3 0 22.527 2.133 6 3 0 26.366 1.241 -6 3 0 24.350 1.977 6 3 0 22.683 2.249 6 3 0 23.342 3.063 6 3 0 26.599 1.861 -6 3 0 25.474 2.598 -6 3 0 24.970 2.055 -6 3 0 24.931 1.861 6 3 0 27.025 1.822 -6 3 0 26.250 2.326 -6 3 0 23.536 2.016 7 -3 0 -0.9693 1.2408 7 -3 0 -0.1163 0.5428 -7 -3 0 -1.202 0.969 7 -3 0 0.2326 1.1244 -7 -3 0 0.2326 0.8142 7 -3 0 -1.318 0.737 -7 -3 0 1.5509 0.5816 -7 3 0 0.4265 1.8611 -7 3 0 0.5816 1.2020 7 3 0 -0.5816 0.5816 -7 3 0 -1.086 0.698 7 3 0 0.8142 1.1244 -7 3 0 -1.163 1.706 -7 3 0 1.1632 1.2408 7 3 0 -4.459 2.365 7 3 0 1.6285 2.4040 7 3 0 0.4653 0.5428 -7 3 0 0.1163 1.0857 8 -3 0 29.739 2.443 -8 -3 0 29.119 2.055 -8 -3 0 21.946 2.404 -8 -3 0 36.719 3.683 -8 -3 0 21.248 1.784 8 -3 0 27.801 1.551 8 -3 0 26.172 1.628 -8 3 0 28.615 2.675 -8 3 0 25.397 2.365 8 3 0 26.250 2.443 8 3 0 28.188 3.024 8 3 0 31.135 2.016 -8 3 0 30.670 1.745 8 3 0 27.490 1.086 -8 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6.79 11 3 0 145.83 9.07 11 3 0 131.44 8.03 11 3 0 137.84 6.82 -11 3 0 146.18 6.71 11 3 0 153.54 7.21 -11 3 0 157.27 7.33 -11 3 0 150.87 6.63 -11 3 0 154.44 6.32 -11 3 0 145.48 7.79 -12 -3 0 -2.210 3.296 -12 -3 0 -0.7367 2.2101 -12 -3 0 1.8999 2.2489 -12 -3 0 -1.628 2.016 12 -3 0 -0.3877 2.6366 -12 3 0 1.0469 2.2876 -12 3 0 7.7935 3.3345 -12 3 0 -0.9306 3.4896 12 3 0 -3.645 2.559 -12 3 0 -0.9306 1.9775 12 3 0 0.5816 2.5978 12 3 0 -0.3102 4.0325 -12 3 0 -0.6979 2.2876 -12 3 0 0.0000 1.1632 12 3 0 -2.675 1.590 -13 -3 0 17.332 3.141 13 -3 0 15.432 4.265 -13 -3 0 19.581 4.071 -13 -3 0 16.362 3.179 -13 -3 0 10.934 3.063 -13 3 0 16.091 3.102 13 3 0 8.4914 4.1100 -13 3 0 16.905 3.141 -13 3 0 16.750 2.869 13 3 0 10.314 3.490 -13 3 0 10.120 3.218 -13 3 0 10.895 3.373 -13 3 0 14.307 2.947 -14 -3 0 5.7773 3.1019 14 -3 0 8.9955 4.8079 -14 -3 0 6.8629 2.8305 -14 -3 0 4.7691 2.6754 -14 -3 0 8.3751 2.5978 14 3 0 2.7141 4.6916 -14 3 0 6.9017 5.1569 -14 3 0 11.903 4.692 -14 3 0 4.4977 3.7610 -14 3 0 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223.68 7.21 -1 -4 0 232.64 9.27 -1 -4 0 218.95 6.94 -1 -4 0 228.49 7.13 1 -4 0 225.24 10.90 -1 -4 0 226.17 7.41 1 -4 0 221.78 8.03 1 -4 0 233.46 7.68 1 -4 0 245.48 9.11 1 -4 0 215.19 8.84 -1 -4 0 223.18 9.27 1 -4 0 217.40 7.41 -1 -4 0 223.57 9.34 -1 -4 0 220.62 7.25 -1 -4 0 218.18 9.34 -1 -4 0 232.45 11.01 -1 -4 0 238.81 8.30 -1 -4 0 232.18 8.22 -1 -4 0 228.80 9.00 1 -4 0 244.04 8.53 -1 4 0 247.30 8.41 1 4 0 226.63 7.83 1 4 0 228.69 7.37 -1 4 0 223.88 7.56 -1 4 0 221.28 6.75 -1 4 0 231.01 6.63 1 4 0 228.73 6.82 -1 4 0 232.14 6.05 1 4 0 228.84 8.38 -1 4 0 214.53 9.27 -1 4 0 230.82 6.32 -1 4 0 233.18 8.18 1 -4 0 247.80 15.11 1 -4 0 235.45 15.23 -1 4 0 233.88 15.13 -1 4 0 236.05 15.06 2 -4 0 200.38 7.72 -2 -4 0 206.59 7.52 2 -4 0 204.92 8.80 2 -4 0 215.04 8.61 -2 -4 0 211.90 7.79 -2 -4 0 231.83 9.31 2 -4 0 213.76 7.68 2 -4 0 206.28 6.55 -2 -4 0 214.73 9.54 -2 -4 0 218.92 8.92 2 -4 0 217.21 7.75 2 -4 0 202.44 8.57 -2 -4 0 203.52 6.86 -2 -4 0 209.73 9.03 -2 -4 0 222.06 9.19 -2 -4 0 206.86 6.05 2 -4 0 203.21 7.95 2 4 0 205.77 6.63 2 4 0 213.02 7.25 -2 4 0 211.12 6.75 2 4 0 218.49 6.28 2 4 0 215.70 6.59 2 4 0 217.05 7.41 -2 4 0 208.49 6.79 -2 4 0 203.21 7.13 -2 4 0 207.05 6.20 -2 4 0 217.52 6.71 -2 4 0 206.47 7.44 -2 4 0 191.58 11.24 2 -4 0 208.49 14.24 -2 -4 0 218.85 13.90 2 -4 0 214.82 14.57 -2 4 0 227.49 14.76 2 4 0 223.14 13.86 -2 4 0 212.92 13.86 2 4 0 203.86 13.82 3 -4 0 16.440 1.512 3 -4 0 18.883 1.435 3 -4 0 19.542 2.133 -3 -4 0 15.432 2.171 -3 -4 0 17.758 1.667 -3 -4 0 16.634 1.745 -3 -4 0 21.597 1.512 3 -4 0 19.387 1.667 -3 -4 0 20.783 2.210 -3 -4 0 18.107 2.016 -3 4 0 24.233 2.171 -3 4 0 16.867 1.900 3 4 0 18.534 2.133 -3 4 0 20.744 1.900 -3 4 0 20.821 2.016 3 4 0 21.791 1.861 -3 4 0 19.077 2.094 -3 4 0 19.736 1.822 -3 4 0 19.930 1.667 3 4 0 21.636 2.055 -4 -4 0 90.071 4.304 -4 -4 0 83.557 4.459 4 -4 0 90.498 4.188 4 -4 0 86.465 6.436 4 -4 0 87.396 3.412 -4 -4 0 88.442 5.390 -4 -4 0 86.581 3.645 4 4 0 89.024 3.296 4 4 0 88.249 3.994 -4 4 0 84.449 4.188 -4 4 0 83.751 3.877 -4 4 0 93.289 3.567 4 4 0 95.771 4.304 -4 4 0 90.265 3.722 -4 4 0 84.100 3.645 4 4 0 85.806 3.567 5 -4 0 50.212 4.885 -5 -4 0 54.787 3.335 5 -4 0 52.810 2.520 -5 -4 0 56.299 2.133 -5 -4 0 51.918 2.520 5 -4 0 57.811 1.861 5 -4 0 55.989 2.792 -5 4 0 59.091 3.606 5 4 0 54.012 3.683 -5 4 0 54.516 2.792 -5 4 0 55.563 2.986 -5 4 0 58.975 3.761 -5 4 0 55.020 3.141 5 4 0 55.950 4.498 5 4 0 54.942 2.947 5 4 0 58.277 2.675 6 -4 0 5.3508 1.2408 6 -4 0 6.3976 2.1325 6 -4 0 7.7547 0.9693 6 -4 0 4.4590 0.8530 -6 -4 0 5.7385 0.8918 -6 -4 0 4.2651 1.5122 -6 -4 0 5.2344 1.7060 -6 4 0 10.197 1.667 6 4 0 7.4058 2.0938 6 4 0 8.8791 1.3958 -6 4 0 8.3363 1.1632 6 4 0 7.0180 1.2020 -6 4 0 4.9630 1.4346 -6 4 0 6.8629 2.2101 6 4 0 8.2588 2.4040 -6 4 0 6.2425 1.8611 -6 4 0 7.9098 2.4815 7 -4 0 17.215 1.163 -7 -4 0 15.703 1.008 7 -4 0 15.858 1.861 -7 -4 0 18.301 3.063 -7 -4 0 12.252 1.900 7 -4 0 15.044 1.163 7 -4 0 16.518 2.094 7 -4 0 14.656 1.124 7 4 0 14.695 2.520 -7 4 0 18.456 2.171 -7 4 0 15.393 1.977 -7 4 0 18.844 2.482 -7 4 0 18.573 1.977 -7 4 0 17.875 2.171 7 4 0 16.867 1.900 7 4 0 16.130 2.482 -7 4 0 13.765 2.559 7 4 0 18.766 1.628 -8 -4 0 191.70 6.75 -8 -4 0 160.41 9.50 -8 -4 0 195.96 7.10 8 -4 0 188.87 7.25 8 -4 0 190.42 6.55 8 -4 0 181.11 8.61 -8 4 0 188.94 6.71 -8 4 0 181.46 6.20 -8 4 0 194.37 6.82 -8 4 0 192.51 7.33 -8 4 0 184.72 8.69 8 4 0 175.18 7.25 -8 4 0 175.37 7.02 8 4 0 192.32 8.49 8 4 0 193.29 8.76 8 4 0 191.08 10.31 -9 -4 0 74.484 5.506 9 -4 0 63.356 4.653 9 4 0 78.439 3.800 -9 4 0 68.319 3.645 -9 4 0 63.123 4.498 9 4 0 74.639 5.079 -9 4 0 74.058 4.226 -9 4 0 80.184 4.924 -9 4 0 72.274 4.537 9 4 0 59.362 5.816 9 4 0 73.553 3.528 -9 4 0 67.078 4.149 -10 -4 0 539.92 15.70 -10 -4 0 509.99 21.05 10 -4 0 477.96 20.28 -10 -4 0 483.58 20.16 -10 -4 0 484.79 19.43 10 4 0 479.01 34.74 -10 4 0 496.34 14.81 10 4 0 484.94 24.78 -10 4 0 456.09 28.46 -10 4 0 481.30 15.04 10 4 0 499.64 15.04 -10 4 0 482.07 14.93 -10 4 0 472.92 15.04 10 4 0 502.43 17.22 -10 4 0 484.05 16.63 11 -4 0 2.9856 3.4121 -11 -4 0 -0.1551 2.7141 -11 -4 0 8.9179 2.5591 -11 -4 0 0.6979 2.4040 -11 -4 0 4.1875 2.3652 -11 4 0 6.6303 2.7141 -11 4 0 2.1325 2.3652 -11 4 0 1.8611 2.1713 11 4 0 4.4590 2.0938 -11 4 0 0.8142 2.3264 11 4 0 6.8629 4.7304 11 4 0 -0.4653 2.7141 -11 4 0 0.4653 2.4427 -11 4 0 2.3264 1.7836 11 4 0 3.2182 1.7448 12 -4 0 48.157 5.273 -12 -4 0 54.903 4.692 -12 -4 0 38.347 4.459 -12 -4 0 40.247 4.730 -12 -4 0 42.031 4.692 -12 4 0 41.875 3.683 -12 4 0 57.811 5.118 -12 4 0 47.343 4.847 -12 4 0 41.875 3.761 -12 4 0 54.826 5.855 12 4 0 39.549 5.971 -12 4 0 44.086 5.196 -13 -4 0 5.9711 2.6366 -13 -4 0 15.936 3.683 13 -4 0 11.710 3.645 -13 -4 0 16.595 4.963 -13 -4 0 11.050 3.412 -13 4 0 17.642 4.614 13 4 0 9.1118 4.5753 -13 4 0 15.277 4.692 -13 4 0 13.493 3.994 -13 4 0 14.540 4.537 -13 4 0 13.920 4.304 -14 -4 0 2.7529 2.7141 14 -4 0 3.8774 3.5284 -14 -4 0 4.4590 3.4508 -14 -4 0 8.2975 3.1407 14 -4 0 4.3426 3.6059 -14 -4 0 5.7385 3.0631 -14 4 0 -5.777 5.816 -14 4 0 6.7078 3.3733 -14 4 0 3.0243 3.4121 -14 4 0 -0.0775 4.1100 -14 4 0 7.0568 3.4508 14 4 0 2.1713 3.4896 -15 -4 0 18.960 6.475 15 -4 0 12.640 3.761 -15 -4 0 5.4671 4.4590 -15 -4 0 14.230 4.265 15 -4 0 6.9792 5.1569 -15 -4 0 7.0568 3.6835 -15 4 0 9.9648 5.1569 15 4 0 9.6158 5.9324 -15 4 0 19.387 5.816 -15 4 0 14.152 4.614 -15 4 0 13.067 4.459 -15 4 0 16.440 5.700 16 -4 0 4.4977 4.9630 -16 -4 0 7.2119 4.9630 -16 -4 0 11.089 4.808 -16 -4 0 3.6447 4.4202 -16 -4 0 6.0099 5.0793 -16 4 0 10.857 4.459 -16 4 0 2.9080 4.3426 -16 4 0 -0.7367 4.6528 16 4 0 6.0099 6.2038 -16 4 0 10.740 6.436 -16 4 0 3.9161 6.7466 0 -5 0 0.2714 0.7755 0 -5 0 0.0388 1.0469 0 -5 0 0.8918 0.8918 0 -5 0 -0.6592 1.9387 0 -5 0 -2.598 1.861 0 5 0 2.4815 1.2408 0 5 0 1.0469 1.2408 0 5 0 -0.8142 1.1244 0 5 0 0.5816 1.0857 1 -5 0 250.98 9.81 1 -5 0 245.17 9.15 1 -5 0 238.11 7.52 -1 -5 0 223.65 6.75 -1 -5 0 234.93 8.10 1 -5 0 229.31 8.26 1 -5 0 230.47 8.06 -1 -5 0 234.77 6.98 -1 5 0 229.77 8.10 -1 5 0 251.68 8.38 1 5 0 243.58 8.26 1 5 0 248.77 8.10 -1 5 0 242.92 8.38 -1 5 0 238.92 8.22 -1 5 0 244.04 8.18 -1 5 0 246.33 7.64 -1 5 0 243.34 7.13 1 5 0 241.91 8.18 1 5 0 241.83 7.56 2 -5 0 405.96 10.74 2 -5 0 413.64 13.45 -2 -5 0 424.69 12.72 -2 -5 0 406.42 13.80 2 -5 0 418.06 20.51 2 -5 0 402.90 13.92 -2 -5 0 408.98 11.13 -2 5 0 428.45 14.93 2 5 0 422.83 13.57 -2 5 0 418.83 13.42 -2 5 0 405.77 14.54 2 5 0 413.40 14.70 -2 5 0 400.22 14.54 -2 5 0 407.70 12.80 -2 5 0 415.42 12.60 2 5 0 408.01 15.86 -2 5 0 443.88 20.74 2 5 0 415.65 12.64 -3 -5 0 425.27 26.13 3 -5 0 416.85 19.66 3 -5 0 433.72 20.43 3 -5 0 450.28 16.60 3 -5 0 441.05 12.52 -3 -5 0 426.43 14.07 -3 -5 0 449.85 14.62 -3 -5 0 429.84 26.91 -3 5 0 425.58 11.79 3 5 0 438.68 13.76 -3 5 0 442.02 19.74 3 5 0 418.56 16.75 -3 5 0 449.77 12.95 -3 5 0 426.01 16.91 -3 5 0 444.19 16.60 -3 5 0 449.81 17.29 -4 -5 0 311.62 10.24 4 -5 0 303.91 30.44 -4 -5 0 315.23 8.30 4 -5 0 322.79 12.60 -4 -5 0 292.66 19.23 4 -5 0 313.02 11.86 -4 -5 0 298.63 20.63 4 -5 0 307.09 9.03 4 5 0 315.62 15.08 -4 5 0 308.75 11.17 4 5 0 320.77 9.27 -4 5 0 312.83 11.09 4 5 0 313.02 12.33 -4 5 0 327.09 11.94 -4 5 0 311.12 10.31 -4 5 0 308.37 9.38 -4 5 0 309.10 10.12 -5 -5 0 324.73 15.70 5 -5 0 338.45 21.02 -5 -5 0 357.69 11.90 5 -5 0 341.63 19.31 5 -5 0 349.27 11.32 5 -5 0 349.27 12.80 -5 -5 0 325.23 25.71 5 -5 0 349.70 12.02 -5 5 0 341.98 10.70 5 5 0 365.91 12.99 5 5 0 341.94 18.30 -5 5 0 330.20 9.31 -5 5 0 348.61 10.86 -5 5 0 335.86 10.74 -5 5 0 348.73 10.00 5 5 0 340.43 16.52 6 -5 0 341.01 10.51 -6 -5 0 327.48 10.70 6 -5 0 337.25 15.28 6 -5 0 323.18 10.55 -6 -5 0 329.92 15.94 6 -5 0 315.23 21.52 6 -5 0 322.52 9.00 -6 5 0 323.53 11.94 -6 5 0 315.85 9.34 6 5 0 326.74 10.24 -6 5 0 320.39 11.55 -6 5 0 317.13 9.65 -6 5 0 326.59 10.31 6 5 0 325.85 15.28 6 5 0 315.19 11.01 7 -5 0 9.0730 0.8530 7 -5 0 4.8855 1.8999 7 -5 0 6.7078 0.7755 -7 -5 0 12.252 2.249 -7 -5 0 9.1118 1.0469 7 5 0 9.7322 3.3345 -7 5 0 11.477 3.141 -7 5 0 13.648 3.257 7 5 0 6.3976 1.5509 -7 5 0 9.6158 3.0243 7 5 0 7.7547 1.7060 -7 5 0 13.958 2.482 -7 5 0 7.2507 2.5978 8 -5 0 338.61 14.35 -8 -5 0 323.91 15.24 -8 5 0 343.22 13.26 8 5 0 340.20 13.22 -8 5 0 323.95 13.61 8 5 0 320.89 19.31 8 5 0 340.39 12.99 -8 5 0 329.65 12.91 -8 5 0 330.39 11.94 -8 5 0 330.66 14.19 -9 -5 0 59.052 4.188 9 -5 0 59.013 4.692 -9 5 0 49.746 4.381 9 5 0 60.099 4.188 -9 5 0 63.356 3.567 -9 5 0 62.891 5.312 -9 5 0 49.126 4.575 -9 5 0 54.205 3.916 9 5 0 64.170 3.528 9 5 0 53.120 5.894 -9 5 0 58.315 4.769 10 -5 0 94.026 5.467 -10 -5 0 102.75 6.67 -10 5 0 100.04 7.29 10 5 0 83.984 6.087 -10 5 0 103.02 7.17 -10 5 0 96.934 6.204 -10 5 0 86.232 5.467 10 5 0 98.446 7.173 -10 5 0 92.591 6.010 -10 5 0 100.42 7.52 10 5 0 102.32 5.54 11 -5 0 0.3490 2.6754 -11 -5 0 1.8999 2.9468 -11 -5 0 3.6447 2.7917 -11 -5 0 0.6204 2.7529 -11 -5 0 0.3490 3.1019 -11 5 0 2.7917 2.4815 -11 5 0 0.6204 2.4040 -11 5 0 5.5834 3.0243 -11 5 0 2.1713 2.8692 11 5 0 -2.016 2.869 -11 5 0 5.0793 2.9080 12 -5 0 19.697 3.412 -12 -5 0 13.416 3.373 -12 -5 0 16.091 3.877 12 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12.95 -3 6 0 345.82 16.09 3 6 0 374.24 13.22 3 6 0 378.35 13.69 3 6 0 344.66 14.73 3 6 0 343.03 10.66 4 -6 0 -0.6204 1.0469 4 -6 0 2.3264 1.5897 -4 -6 0 1.3571 1.3958 -4 -6 0 3.2958 1.7836 4 -6 0 -0.3102 1.1632 4 -6 0 2.0162 1.2795 -4 6 0 6.4364 2.2489 -4 6 0 0.4653 2.1713 -4 6 0 0.8918 1.7836 4 6 0 6.0487 2.1713 -4 6 0 -1.280 2.249 4 6 0 -1.861 2.792 -4 6 0 2.9468 2.1325 -5 -6 0 11.942 1.435 -5 -6 0 12.873 2.094 5 -6 0 15.471 2.986 5 -6 0 10.585 2.598 5 6 0 13.532 2.482 5 6 0 8.9955 2.2101 -5 6 0 11.516 2.016 -5 6 0 9.0342 1.9775 -5 6 0 10.120 2.288 -5 6 0 11.632 2.326 -5 6 0 11.128 2.443 5 6 0 12.408 2.714 6 -6 0 1.6673 2.4040 -6 -6 0 4.3039 2.0938 -6 -6 0 5.8548 1.3571 6 -6 0 4.1100 2.2101 6 6 0 9.3057 2.0938 -6 6 0 2.5203 2.2101 -6 6 0 3.8774 1.8999 -6 6 0 2.7529 2.8692 -6 6 0 8.1037 3.1407 -6 6 0 9.3444 2.9856 6 6 0 6.5527 3.4121 6 6 0 5.2344 1.3958 -7 -6 0 6.2813 2.2489 7 -6 0 10.740 2.559 -7 6 0 5.0018 2.5591 -7 6 0 4.0325 2.2876 -7 6 0 8.8016 2.0550 7 6 0 8.1812 2.5978 -7 6 0 10.081 2.830 -7 6 0 11.981 3.257 7 6 0 5.3120 1.7448 7 6 0 8.9955 2.3652 8 -6 0 30.941 3.335 -8 -6 0 34.547 3.567 8 -6 0 38.812 3.994 -8 6 0 34.315 5.002 -8 6 0 28.576 3.761 8 6 0 41.255 5.002 -8 6 0 42.108 4.963 8 6 0 42.031 3.606 -8 6 0 33.617 3.606 8 6 0 39.316 3.218 -8 6 0 35.943 4.032 -9 -6 0 18.030 3.839 9 -6 0 19.115 4.769 9 -6 0 14.967 3.412 9 6 0 13.028 2.753 -9 6 0 11.516 2.792 9 6 0 20.899 2.947 -9 6 0 16.556 4.071 9 6 0 16.789 2.753 -9 6 0 16.905 3.955 -9 6 0 14.075 3.683 -9 6 0 20.279 3.800 10 -6 0 28.615 5.157 -10 -6 0 40.829 5.700 10 -6 0 33.888 5.312 -10 6 0 25.474 4.304 -10 6 0 27.568 5.583 -10 6 0 34.702 4.924 -10 6 0 36.408 4.343 10 6 0 27.723 4.498 -10 6 0 28.886 3.296 11 -6 0 -6.320 3.645 -11 -6 0 -1.124 2.908 -11 -6 0 -3.063 3.412 -11 -6 0 -0.9306 3.1407 11 -6 0 -1.900 4.459 -11 -6 0 0.3102 2.9468 11 6 0 -0.0775 4.1100 -11 6 0 -3.024 2.520 -11 6 0 -1.590 2.792 -11 6 0 0.4653 2.8305 -11 6 0 1.6673 2.6754 -11 6 0 -1.900 2.675 12 -6 0 4.1100 2.6754 -12 -6 0 13.571 3.839 -12 -6 0 5.9324 4.3814 -12 -6 0 0.8918 3.6447 12 -6 0 5.7385 3.9161 -12 -6 0 -0.2714 3.6447 -12 6 0 1.3958 4.2263 -12 6 0 3.6447 3.8386 12 6 0 0.5816 5.1957 -12 6 0 8.8791 4.8855 -12 6 0 6.2425 3.7223 -12 6 0 3.2958 4.7691 -13 -6 0 11.050 4.420 -13 -6 0 6.6303 3.3345 13 -6 0 15.587 5.777 13 -6 0 -6.126 5.041 -13 -6 0 8.4914 3.3733 -13 -6 0 4.8079 3.6059 -13 6 0 10.275 5.041 -13 6 0 -1.900 4.071 13 6 0 8.1037 6.0487 -13 6 0 8.2588 3.7610 -13 6 0 3.4508 5.2344 -13 6 0 10.081 3.761 14 -6 0 4.2263 5.6609 -14 -6 0 2.4040 4.5365 -14 -6 0 -6.436 4.343 14 -6 0 -1.202 4.459 -14 -6 0 8.3751 5.1957 -14 -6 0 4.3426 5.6609 -14 6 0 4.2651 4.0325 -14 6 0 -5.079 5.467 -14 6 0 -4.885 5.661 -14 6 0 0.0388 4.6528 -14 6 0 -0.3490 6.6303 14 6 0 -0.7367 6.3201 0 -7 0 1.6285 2.2101 0 -7 0 -1.280 1.357 0 -7 0 -1.086 1.512 0 7 0 -0.4265 1.5897 0 7 0 -1.512 3.102 0 7 0 0.0775 2.0550 0 7 0 -1.939 2.210 -1 -7 0 34.508 3.296 -1 -7 0 30.282 2.675 -1 -7 0 26.676 3.141 1 -7 0 30.088 2.637 1 -7 0 34.508 2.986 1 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86.077 5.118 4 7 0 88.947 4.730 5 -7 0 230.74 10.35 5 -7 0 236.05 7.75 -5 -7 0 227.68 13.65 -5 -7 0 228.45 9.65 -5 7 0 227.87 9.73 5 7 0 220.08 11.75 -5 7 0 222.64 10.27 -5 7 0 219.11 8.14 -5 7 0 227.72 10.43 5 7 0 228.57 14.11 -5 7 0 226.71 10.16 6 -7 0 101.20 6.67 6 -7 0 93.522 6.630 -6 -7 0 107.09 6.98 -6 -7 0 110.00 6.28 -6 7 0 115.27 6.01 -6 7 0 99.881 5.777 6 7 0 107.91 5.97 -6 7 0 104.84 5.58 -6 7 0 117.52 7.17 6 7 0 120.31 5.74 -6 7 0 107.98 5.70 -7 -7 0 0.3102 2.4040 7 -7 0 1.7448 2.7141 7 -7 0 2.8305 2.0162 -7 7 0 2.5978 3.4121 -7 7 0 4.7691 3.0631 -7 7 0 3.2182 2.7529 7 7 0 3.7998 4.3814 -7 7 0 6.7466 3.2958 -7 7 0 4.6916 3.2570 7 7 0 3.1407 2.4815 8 -7 0 193.01 12.91 8 -7 0 200.54 9.54 -8 -7 0 177.62 10.86 -8 7 0 187.70 8.72 8 7 0 192.63 11.48 -8 7 0 194.14 10.86 8 7 0 198.91 10.47 -8 7 0 209.65 9.34 -8 7 0 187.82 11.13 -8 7 0 205.93 11.17 9 -7 0 193.52 11.63 -9 -7 0 191.66 9.85 9 -7 0 176.85 12.29 -9 7 0 187.00 11.90 -9 7 0 182.74 10.78 -9 7 0 191.85 10.04 9 7 0 191.85 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12.795 0.969 2 1 -6 15.936 0.814 2 1 -6 13.299 0.775 2 1 -6 12.795 1.008 2 1 -6 13.067 1.396 -2 1 6 13.803 1.008 -2 1 6 11.671 1.047 -2 1 6 14.346 0.775 -2 -1 6 8.7473 2.7015 -2 -1 6 9.5176 2.6694 2 -1 -6 10.429 2.752 2 -1 -6 10.422 2.446 -2 1 6 11.000 3.254 -2 1 6 11.125 2.446 2 1 -6 6.2754 2.5450 2 1 -6 7.0941 2.7690 1 -1 -6 3698.03 129.27 1 -1 -6 3722.49 169.94 1 -1 -6 3729.51 136.25 -1 1 6 3761.69 155.06 -1 1 6 3710.28 114.73 1 1 -6 3694.66 121.40 1 1 -6 3636.11 120.62 -1 1 6 3877.36 136.02 1 1 -6 3648.75 188.71 -1 -1 6 3807.25 237.17 1 -1 -6 3873.00 232.85 1 -1 -6 3790.27 241.63 -1 -1 6 3924.38 233.80 -1 1 6 3861.58 242.08 1 1 -6 3779.46 240.19 1 1 -6 3823.58 243.68 -1 1 6 3824.09 238.38 0 -1 -6 3390.46 208.03 0 -1 6 3500.68 211.35 0 1 6 3338.49 215.90 0 1 6 3325.52 213.80 0 1 -6 3487.72 219.03 0 1 -6 3434.87 205.04 -1 -1 -6 1927.51 70.30 1 -1 6 1940.00 70.45 1 -1 6 2063.80 46.10 1 -1 6 2031.50 53.93 -1 -1 -6 2030.07 95.62 1 -1 6 2082.49 45.95 -1 -1 -6 2055.50 94.65 -1 -1 -6 1942.48 46.64 1 -1 6 1953.02 69.79 -1 -1 -6 2013.71 82.08 -1 -1 -6 2018.82 82.20 -1 1 -6 1890.09 53.24 -1 1 -6 1892.85 51.57 1 1 6 1934.45 53.24 -1 1 -6 1930.23 53.74 1 1 6 1927.36 53.90 -1 1 -6 1997.15 64.64 1 1 6 1933.09 70.96 -1 1 -6 1945.85 58.51 -1 1 -6 1982.45 53.93 -1 1 -6 1959.07 97.79 -1 -1 -6 2153.31 149.53 1 -1 6 2176.27 127.73 1 -1 6 2111.28 129.28 -1 -1 -6 2041.70 140.41 1 1 6 2055.70 141.61 -1 1 -6 2176.74 133.24 1 1 6 2212.92 141.26 -1 1 -6 2017.60 127.42 2 -1 6 367.81 11.24 -2 -1 -6 356.76 11.32 2 -1 6 355.94 11.55 -2 -1 -6 368.47 11.55 -2 -1 -6 369.74 10.55 2 -1 6 380.83 14.85 2 -1 6 374.20 10.47 -2 -1 -6 369.40 11.36 -2 -1 -6 359.28 12.21 2 -1 6 370.99 13.49 -2 1 -6 346.17 10.31 2 1 6 352.30 15.94 -2 1 -6 364.70 10.74 -2 1 -6 350.13 10.59 -2 1 -6 354.31 14.27 -2 1 -6 353.54 11.55 -2 1 -6 376.76 10.74 -2 1 -6 361.49 12.02 2 1 6 349.04 10.35 -2 1 -6 343.84 14.77 2 1 6 374.75 10.16 -2 1 -6 354.20 11.75 2 1 6 358.69 11.98 2 1 6 360.48 8.57 -2 -1 -6 387.17 24.87 -2 -1 -6 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7.8323 4.2651 1 -1 -29 7.7547 4.6141 1 1 -29 10.818 6.708 -1 1 29 13.416 4.575 0 -1 -29 -2.598 5.932 0 -1 29 -4.032 7.289 0 1 29 20.744 7.832 0 1 -29 7.4833 4.6141 1 -1 29 3.1794 6.0487 -1 -1 -29 8.4914 5.2344 1 1 29 8.0649 4.6916 -1 1 -29 0.4265 5.2732 -9 -2 29 -1.667 4.459 9 -2 -29 -3.257 5.234 -9 -2 29 3.1019 6.5915 9 -2 -29 -1.008 6.243 9 -2 -29 2.2101 5.6609 9 2 -29 -1.551 8.026 -9 2 29 2.4815 6.3201 9 2 -29 -0.8142 5.0406 -9 2 29 2.3652 6.4364 -8 -2 29 3.5284 4.3039 8 -2 -29 -0.9306 6.9405 8 -2 -29 10.081 4.149 -8 -2 29 2.7529 6.0099 8 -2 -29 0.4265 6.2038 8 2 -29 3.4508 7.6384 8 2 -29 12.136 6.049 -8 2 29 12.059 5.932 -7 -2 29 1.7448 5.7385 7 -2 -29 6.0487 6.5140 -7 -2 29 2.8305 4.1488 7 -2 -29 -0.7367 3.2570 7 -2 -29 -0.6592 6.0875 7 2 -29 -1.357 4.653 7 2 -29 -0.9306 4.2263 7 2 -29 1.5122 6.3201 -7 2 29 5.4283 5.2732 -6 -2 29 -10.12 6.59 6 -2 -29 -2.520 4.963 6 -2 -29 -12.49 5.00 6 -2 -29 0.0775 4.1488 6 2 -29 -4.692 6.087 6 2 -29 -4.226 5.777 -6 2 29 -2.210 5.079 6 2 -29 -0.6979 5.7385 -5 -2 29 9.7709 6.3589 5 -2 -29 5.5058 6.5915 5 2 -29 4.7691 5.7773 5 2 -29 10.779 6.049 -5 2 29 10.585 5.661 5 2 -29 -0.2714 6.0099 -4 -2 29 5.0018 3.7610 4 -2 -29 4.5753 5.1569 -4 2 29 3.2182 3.9161 4 2 -29 1.4346 4.1875 4 2 -29 -4.692 6.553 4 2 -29 -0.8530 5.3895 -3 -2 29 -9.771 4.498 3 -2 -29 3.7998 4.8855 3 2 -29 -0.8142 3.9161 -3 2 29 5.5058 4.5365 3 2 -29 2.3652 6.0875 3 2 -29 -4.459 3.451 -2 -2 29 -1.512 6.359 2 -2 -29 3.8774 5.6609 2 2 -29 -0.6979 4.7691 -2 2 29 0.3490 4.6528 2 2 -29 1.8611 4.1488 2 2 -29 1.8999 4.5753 -1 -2 29 -0.5428 5.0793 1 -2 -29 8.7628 5.5058 1 2 -29 5.6222 7.0956 -1 2 29 0.3102 5.3895 0 -2 29 -3.257 4.343 0 -2 -29 2.8305 5.0793 0 2 29 5.8936 5.0793 0 2 -29 5.8936 4.2651 -8 -3 29 3.1794 4.6141 8 -3 -29 -1.667 3.761 8 -3 -29 4.4202 7.8710 8 3 -29 1.0857 4.0712 8 3 -29 0.1939 4.3039 8 3 -29 0.0000 5.3508 7 -3 -29 -2.869 3.994 -7 -3 29 1.5897 4.6528 7 -3 -29 -4.381 4.071 7 -3 -29 -2.326 5.894 -7 3 29 1.9775 5.6222 7 3 -29 5.2344 7.2119 7 3 -29 -4.420 3.528 7 3 -29 0.3102 3.7998 -6 -3 29 -4.730 5.157 6 -3 -29 5.5058 3.2182 -6 3 29 -4.071 4.149 6 3 -29 -1.318 3.761 6 3 -29 1.2795 4.0712 6 3 -29 2.0938 4.4202 5 -3 -29 -8.530 5.777 -5 -3 29 0.0000 5.5446 5 3 -29 -0.9693 6.2813 -5 3 29 4.7691 5.7385 5 3 -29 0.2326 5.4283 5 3 -29 3.0631 6.2813 4 -3 -29 2.2489 3.8386 -4 -3 29 9.3444 6.9405 4 3 -29 -13.73 5.70 -4 3 29 0.8142 4.1100 4 3 -29 5.5446 7.1731 4 3 -29 5.5446 5.8160 -3 -3 29 2.0550 5.3508 3 -3 -29 -1.706 4.847 3 3 -29 7.7159 6.0875 3 3 -29 -2.210 3.955 -3 3 29 -1.357 7.057 3 3 -29 3.5284 5.1569 -2 -3 29 4.0325 7.7935 2 -3 -29 9.7322 6.7466 2 3 -29 -3.567 7.445 -2 3 29 0.6204 4.6528 2 3 -29 -2.986 6.281 2 3 -29 0.9306 6.5140 -2 3 29 9.1893 6.1262 -1 -3 29 1.2795 4.6141 1 -3 -29 5.8936 5.6222 -1 3 29 -2.171 5.041 1 3 -29 5.6609 5.5446 1 3 -29 1.6285 5.0793 -1 3 29 6.4364 5.1569 1 3 -29 4.7304 5.9324 -8 0 30 6.3201 3.7223 8 0 -30 7.5996 6.2813 8 0 -30 5.2732 4.8079 -8 0 30 3.9549 4.6528 8 0 -30 7.2119 5.0018 7 0 -30 4.6528 7.2119 7 0 -30 2.3264 4.5753 -7 0 30 -0.3102 4.1875 7 0 -30 10.275 6.630 -7 0 30 -0.6592 7.4058 -6 0 30 68.823 6.049 6 0 -30 46.877 7.483 6 0 -30 47.730 8.259 6 0 -30 62.038 7.987 5 0 -30 6.7854 4.4590 5 0 -30 10.314 4.769 -5 0 30 9.1506 4.7691 5 0 -30 5.1181 4.2263 4 0 -30 -3.451 4.769 4 0 -30 6.3589 6.8629 -4 0 30 2.4040 3.7223 4 0 -30 1.3183 7.0956 -3 0 30 -8.259 7.251 3 0 -30 4.3814 4.4590 2 0 -30 5.1181 4.7304 -2 0 30 9.4608 7.2119 1 0 -30 -2.210 6.902 -1 0 30 3.8774 4.4202 -8 -1 30 1.0857 5.6609 8 -1 -30 -4.730 6.243 -8 -1 30 2.5591 4.0325 8 -1 -30 -1.939 6.320 8 -1 -30 -3.645 5.273 8 1 -30 1.2020 3.9549 8 1 -30 0.3877 4.5365 -8 1 30 -2.288 3.955 8 1 -30 -3.839 4.769 7 -1 -30 12.795 7.367 -7 -1 30 -5.157 4.265 7 -1 -30 3.5672 5.0793 -7 -1 30 5.2344 4.7304 7 -1 -30 -0.1939 6.0875 7 1 -30 7.5221 6.4364 -7 1 30 0.3877 5.8936 7 1 -30 8.0649 4.3426 7 1 -30 17.332 6.863 6 -1 -30 7.6772 6.0487 -6 -1 30 17.332 4.963 6 -1 -30 12.679 4.963 6 -1 -30 22.217 5.390 -6 1 30 19.038 5.661 6 1 -30 13.997 6.436 6 1 -30 11.283 4.653 6 1 -30 6.7854 5.2344 5 -1 -30 16.556 5.700 -5 -1 30 15.897 4.343 5 -1 -30 31.445 8.026 -5 1 30 14.075 5.428 5 1 -30 14.152 6.514 5 1 -30 8.5302 4.4202 -4 -1 30 -4.847 4.847 4 -1 -30 3.7223 4.6141 4 1 -30 3.7998 4.5753 -4 1 30 -1.047 5.428 4 1 -30 7.2119 5.6609 4 1 -30 1.5897 4.7304 3 -1 -30 6.4364 6.4364 -3 -1 30 0.6204 4.7304 -3 1 30 -0.5428 4.7304 3 1 -30 -2.869 3.877 3 1 -30 -2.598 3.683 3 1 -30 1.6673 4.1488 -2 -1 30 0.2326 7.3670 2 -1 -30 -8.685 7.522 -2 1 30 1.3183 4.7304 2 1 -30 -8.259 6.320 -1 -1 30 3.6059 3.9549 1 -1 -30 2.7529 5.0406 -1 1 30 -1.008 5.894 1 1 -30 -1.977 6.398 7 -2 -30 3.1794 4.9630 7 -2 -30 2.5591 7.5608 7 -2 -30 0.8530 4.0712 -7 -2 30 0.5428 4.6141 7 2 -30 4.6141 5.3895 7 2 -30 -8.414 6.785 7 2 -30 -8.840 6.165 6 -2 -30 8.6465 6.3976 -6 -2 30 5.4283 5.0018 6 2 -30 2.0938 4.3426 -6 2 30 3.8774 4.8855 6 2 -30 -2.094 5.894 6 2 -30 -2.171 3.877 5 -2 -30 -7.483 4.226 -5 -2 30 -1.008 5.273 5 2 -30 2.4815 4.1875 5 2 -30 -1.435 7.096 5 2 -30 -0.8918 4.4977 -5 2 30 2.4040 7.3670 -4 -2 30 -1.590 6.398 4 -2 -30 1.7836 6.1650 4 2 -30 3.9549 6.0487 4 2 -30 1.6285 4.6528 -4 2 30 -4.575 4.614 4 2 -30 4.9242 4.9630 3 -2 -30 -6.863 6.514 -3 -2 30 -1.745 6.514 3 2 -30 -0.0388 7.3282 3 2 -30 2.8305 5.5058 -3 2 30 -8.491 3.296 3 2 -30 2.1713 6.3201 2 -2 -30 1.8611 4.3814 -2 -2 30 0.0388 5.5446 2 2 -30 -4.420 5.816 2 2 -30 1.8611 5.0793 2 2 -30 -3.645 5.273 -2 2 30 3.5284 4.8855 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 40932 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Si1 Si 0.26638(9) 0.19551(14) 0.28652(5) 0.0758(4) Uani 1 1 d . . . . . C1 C 0.42131(17) 0.5528(3) 0.41337(10) 0.0358(5) Uani 1 1 d . . . . . C2 C 0.35811(17) 0.6510(3) 0.43452(11) 0.0368(5) Uani 1 1 d . . . . . C3 C 0.25249(18) 0.6379(3) 0.41517(12) 0.0427(6) Uani 1 1 d . . . . . H3 H 0.2228 0.5608 0.3881 0.051 Uiso 1 1 calc R U . . . C4 C 0.19292(18) 0.7365(3) 0.43558(13) 0.0457(6) Uani 1 1 d . . . . . C5 C 0.0830(2) 0.7432(3) 0.41996(16) 0.0552(8) Uani 1 1 d . . . . . H5 H 0.0399 0.6767 0.3931 0.066 Uiso 1 1 calc R U . . . C6 C 0.0518(2) 0.8551(4) 0.44860(18) 0.0679(10) Uani 1 1 d . . . . . H6 H -0.0170 0.8759 0.4436 0.082 Uiso 1 1 calc R U . . . S7 S 0.14614(6) 0.96018(9) 0.49567(4) 0.0625(3) Uani 1 1 d . . . . . C8 C 0.2375(2) 0.8506(3) 0.47698(13) 0.0455(6) Uani 1 1 d . . . . . C9 C 0.33881(19) 0.8665(3) 0.49763(12) 0.0424(6) Uani 1 1 d . . . . . H9 H 0.3666 0.9426 0.5256 0.051 Uiso 1 1 calc R U . . . C10 C 0.40233(17) 0.7666(3) 0.47641(11) 0.0358(5) Uani 1 1 d . . . . . C11 C 0.50612(17) 0.7810(3) 0.49509(11) 0.0363(5) Uani 1 1 d . . . . . H11 H 0.5347 0.8571 0.5229 0.044 Uiso 1 1 calc R U . . . C12 C 0.56902(17) 0.6866(3) 0.47402(11) 0.0348(5) Uani 1 1 d . . . . . C13 C 0.67487(18) 0.7044(3) 0.49327(12) 0.0384(5) Uani 1 1 d . . . . . H13 H 0.7038 0.7805 0.5210 0.046 Uiso 1 1 calc R U . . . C14 C 0.73429(17) 0.6104(3) 0.47128(12) 0.0406(6) Uani 1 1 d . . . . . S15 S 0.86412(5) 0.61235(9) 0.48820(4) 0.0544(3) Uani 1 1 d . . . . . C16 C 0.8630(2) 0.4597(4) 0.44201(16) 0.0570(8) Uani 1 1 d . . . . . H16 H 0.9224 0.4164 0.4366 0.068 Uiso 1 1 calc R U . . . C17 C 0.7716(2) 0.4074(3) 0.41443(14) 0.0496(7) Uani 1 1 d . . . . . H17 H 0.7596 0.3247 0.3878 0.060 Uiso 1 1 calc R U . . . C18 C 0.69308(18) 0.4926(3) 0.43024(12) 0.0408(6) Uani 1 1 d . . . . . C19 C 0.59127(18) 0.4731(3) 0.41095(11) 0.0381(5) Uani 1 1 d . . . . . H19 H 0.5641 0.3951 0.3837 0.046 Uiso 1 1 calc R U . . . C20 C 0.52640(17) 0.5699(3) 0.43193(11) 0.0356(5) Uani 1 1 d . . . . . C21 C 0.37683(19) 0.4359(3) 0.37278(12) 0.0426(6) Uani 1 1 d . . . . . C22 C 0.3354(2) 0.3383(4) 0.33896(13) 0.0542(7) Uani 1 1 d . . . . . C23 C 0.1326(4) 0.2065(6) 0.2916(2) 0.0983(15) Uani 1 1 d . . . . . H23 H 0.1109 0.3140 0.2817 0.118 Uiso 1 1 calc R U . . . C24 C 0.0592(5) 0.1044(11) 0.2443(3) 0.172(3) Uani 1 1 d . . . . . H24A H 0.0688 -0.0028 0.2558 0.258 Uiso 1 1 calc R U . . . H24B H 0.0732 0.1185 0.2066 0.258 Uiso 1 1 calc R U . . . H24C H -0.0100 0.1342 0.2412 0.258 Uiso 1 1 calc R U . . . C25 C 0.1205(3) 0.1792(6) 0.3502(2) 0.0959(14) Uani 1 1 d . . . . . H25A H 0.1717 0.2391 0.3785 0.115 Uiso 1 1 calc R U . . . H25B H 0.1339 0.0703 0.3598 0.115 Uiso 1 1 calc R U . . . C26 C 0.0165(4) 0.2198(7) 0.3579(2) 0.1064(16) Uani 1 1 d . . . . . H26A H 0.0007 0.3260 0.3466 0.160 Uiso 1 1 calc R U . . . H26B H 0.0173 0.2059 0.3987 0.160 Uiso 1 1 calc R U . . . H26C H -0.0342 0.1531 0.3333 0.160 Uiso 1 1 calc R U . . . C27 C 0.333(2) 0.0050(17) 0.3084(8) 0.130(5) Uani 0.591(6) 1 d D U P A 1 H27 H 0.2949 -0.0364 0.3348 0.156 Uiso 0.591(6) 1 calc R U P A 1 C28 C 0.4393(7) 0.0028(9) 0.3490(4) 0.0921(19) Uani 0.591(6) 1 d D U P A 1 H28A H 0.4570 -0.1015 0.3624 0.138 Uiso 0.591(6) 1 calc R U P A 1 H28B H 0.4426 0.0688 0.3825 0.138 Uiso 0.591(6) 1 calc R U P A 1 H28C H 0.4862 0.0396 0.3280 0.138 Uiso 0.591(6) 1 calc R U P A 1 C29 C 0.318(2) -0.1191(19) 0.2641(9) 0.200(7) Uani 0.591(6) 1 d D U P A 1 H29A H 0.2521 -0.1593 0.2648 0.241 Uiso 0.591(6) 1 calc R U P A 1 H29B H 0.3049 -0.0599 0.2275 0.241 Uiso 0.591(6) 1 calc R U P A 1 C30 C 0.3581(12) -0.2327(13) 0.2515(6) 0.198(6) Uani 0.591(6) 1 d D U P A 1 H30A H 0.4213 -0.2045 0.2436 0.296 Uiso 0.591(6) 1 calc R U P A 1 H30B H 0.3139 -0.2800 0.2168 0.296 Uiso 0.591(6) 1 calc R U P A 1 H30C H 0.3712 -0.3048 0.2840 0.296 Uiso 0.591(6) 1 calc R U P A 1 C27' C 0.326(4) 0.030(2) 0.2895(11) 0.130(5) Uani 0.409(6) 1 d D U P A 2 H27' H 0.3889 0.0533 0.2782 0.156 Uiso 0.409(6) 1 calc R U P A 2 C28' C 0.3593(11) -0.0215(13) 0.3520(6) 0.0921(19) Uani 0.409(6) 1 d D U P A 2 H28D H 0.3949 0.0614 0.3765 0.138 Uiso 0.409(6) 1 calc R U P A 2 H28E H 0.4039 -0.1095 0.3553 0.138 Uiso 0.409(6) 1 calc R U P A 2 H28F H 0.3007 -0.0504 0.3648 0.138 Uiso 0.409(6) 1 calc R U P A 2 C29' C 0.275(3) -0.097(3) 0.2504(12) 0.200(7) Uani 0.409(6) 1 d D U P A 2 H29C H 0.2255 -0.0450 0.2187 0.241 Uiso 0.409(6) 1 calc R U P A 2 H29D H 0.3272 -0.1353 0.2326 0.241 Uiso 0.409(6) 1 calc R U P A 2 C30' C 0.2324(19) -0.212(2) 0.2598(9) 0.198(6) Uani 0.409(6) 1 d D U P A 2 H30D H 0.2016 -0.2639 0.2229 0.296 Uiso 0.409(6) 1 calc R U P A 2 H30E H 0.1806 -0.1843 0.2787 0.296 Uiso 0.409(6) 1 calc R U P A 2 H30F H 0.2807 -0.2807 0.2853 0.296 Uiso 0.409(6) 1 calc R U P A 2 C31 C 0.2866(10) 0.2302(12) 0.2148(5) 0.095(3) Uani 0.507(6) 1 d D U P A 1 H31 H 0.2491 0.1533 0.1862 0.114 Uiso 0.507(6) 1 calc R U P A 1 C32 C 0.3962(11) 0.2339(18) 0.2138(6) 0.138(3) Uani 0.507(6) 1 d D U P A 1 H32A H 0.3997 0.2457 0.1736 0.206 Uiso 0.507(6) 1 calc R U P A 1 H32B H 0.4289 0.1386 0.2299 0.206 Uiso 0.507(6) 1 calc R U P A 1 H32C H 0.4300 0.3197 0.2372 0.206 Uiso 0.507(6) 1 calc R U P A 1 C33 C 0.2468(12) 0.3829(15) 0.1975(5) 0.115(3) Uani 0.507(6) 1 d D U P A 1 H33A H 0.2875 0.4567 0.2255 0.137 Uiso 0.507(6) 1 calc R U P A 1 H33B H 0.1781 0.3873 0.2018 0.137 Uiso 0.507(6) 1 calc R U P A 1 C34 C 0.2431(11) 0.4370(14) 0.1365(4) 0.127(3) Uani 0.507(6) 1 d D U P A 1 H34A H 0.3079 0.4809 0.1365 0.191 Uiso 0.507(6) 1 calc R U P A 1 H34B H 0.1909 0.5144 0.1242 0.191 Uiso 0.507(6) 1 calc R U P A 1 H34C H 0.2283 0.3507 0.1096 0.191 Uiso 0.507(6) 1 calc R U P A 1 C31' C 0.2487(10) 0.2936(14) 0.2105(6) 0.095(3) Uani 0.493(6) 1 d D U P A 2 H31' H 0.2207 0.2132 0.1810 0.114 Uiso 0.493(6) 1 calc R U P A 2 C32' C 0.1765(12) 0.4267(17) 0.1953(7) 0.138(3) Uani 0.493(6) 1 d D U P A 2 H32D H 0.1099 0.3936 0.1966 0.206 Uiso 0.493(6) 1 calc R U P A 2 H32E H 0.1734 0.4631 0.1561 0.206 Uiso 0.493(6) 1 calc R U P A 2 H32F H 0.1996 0.5092 0.2233 0.206 Uiso 0.493(6) 1 calc R U P A 2 C33' C 0.3450(10) 0.3402(16) 0.1998(4) 0.115(3) Uani 0.493(6) 1 d D U P A 2 H33C H 0.3883 0.2489 0.2052 0.137 Uiso 0.493(6) 1 calc R U P A 2 H33D H 0.3774 0.4133 0.2307 0.137 Uiso 0.493(6) 1 calc R U P A 2 C34' C 0.3453(12) 0.4109(15) 0.1421(4) 0.127(3) Uani 0.493(6) 1 d D U P A 2 H34D H 0.4098 0.4603 0.1456 0.191 Uiso 0.493(6) 1 calc R U P A 2 H34E H 0.2917 0.4867 0.1310 0.191 Uiso 0.493(6) 1 calc R U P A 2 H34F H 0.3344 0.3315 0.1122 0.191 Uiso 0.493(6) 1 calc R U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Si1 0.0741(7) 0.0828(8) 0.0663(6) -0.0296(5) 0.0122(5) -0.0263(5) C1 0.0313(11) 0.0353(12) 0.0402(13) 0.0029(10) 0.0087(9) 0.0030(9) C2 0.0281(11) 0.0358(12) 0.0465(13) 0.0057(10) 0.0106(9) 0.0036(9) C3 0.0288(11) 0.0405(13) 0.0566(15) 0.0041(12) 0.0079(10) 0.0013(10) C4 0.0300(12) 0.0415(14) 0.0676(18) 0.0114(13) 0.0169(11) 0.0052(10) C5 0.0338(13) 0.0453(15) 0.089(2) 0.0120(15) 0.0218(14) 0.0049(11) C6 0.0357(15) 0.0549(18) 0.121(3) 0.0150(19) 0.0337(17) 0.0094(13) S7 0.0454(4) 0.0471(4) 0.1054(7) 0.0051(4) 0.0382(4) 0.0110(3) C8 0.0368(13) 0.0372(13) 0.0693(17) 0.0103(13) 0.0262(12) 0.0088(10) C9 0.0386(13) 0.0353(12) 0.0571(16) 0.0011(11) 0.0198(11) 0.0057(10) C10 0.0315(11) 0.0337(12) 0.0441(13) 0.0040(10) 0.0134(10) 0.0047(9) C11 0.0333(11) 0.0316(12) 0.0439(13) 0.0010(10) 0.0103(10) 0.0009(9) C12 0.0281(11) 0.0334(12) 0.0428(13) 0.0039(10) 0.0096(9) 0.0036(9) C13 0.0299(11) 0.0339(12) 0.0498(14) 0.0031(11) 0.0080(10) 0.0002(9) C14 0.0278(11) 0.0386(13) 0.0566(15) 0.0090(11) 0.0136(10) 0.0028(9) S15 0.0282(3) 0.0488(4) 0.0867(6) 0.0063(4) 0.0167(3) 0.0042(3) C16 0.0375(14) 0.0559(18) 0.084(2) 0.0097(16) 0.0283(14) 0.0122(12) C17 0.0405(14) 0.0491(16) 0.0640(18) 0.0059(13) 0.0222(13) 0.0113(12) C18 0.0354(12) 0.0394(13) 0.0514(15) 0.0075(11) 0.0183(11) 0.0083(10) C19 0.0352(12) 0.0367(12) 0.0441(13) 0.0007(10) 0.0138(10) 0.0056(10) C20 0.0310(11) 0.0364(12) 0.0406(13) 0.0055(10) 0.0116(9) 0.0045(9) C21 0.0346(12) 0.0452(14) 0.0468(14) 0.0009(12) 0.0088(10) 0.0028(11) C22 0.0488(16) 0.0589(18) 0.0522(16) -0.0069(14) 0.0091(13) -0.0043(14) C23 0.081(3) 0.115(4) 0.083(3) -0.010(3) -0.004(2) -0.034(3) C24 0.114(5) 0.241(9) 0.140(6) -0.067(6) -0.002(4) -0.058(6) C25 0.071(3) 0.113(4) 0.097(3) 0.001(3) 0.012(2) -0.023(2) C26 0.078(3) 0.121(4) 0.112(4) -0.014(3) 0.012(3) 0.006(3) C27 0.151(6) 0.074(6) 0.127(12) -0.047(7) -0.023(9) 0.011(6) C28 0.113(5) 0.075(4) 0.091(4) -0.013(3) 0.034(4) 0.013(4) C29 0.257(19) 0.104(7) 0.186(10) -0.089(7) -0.031(9) 0.011(9) C30 0.264(14) 0.113(6) 0.167(9) -0.083(7) -0.024(9) 0.010(8) C27' 0.151(6) 0.074(6) 0.127(12) -0.047(7) -0.023(9) 0.011(6) C28' 0.113(5) 0.075(4) 0.091(4) -0.013(3) 0.034(4) 0.013(4) C29' 0.257(19) 0.104(7) 0.186(10) -0.089(7) -0.031(9) 0.011(9) C30' 0.264(14) 0.113(6) 0.167(9) -0.083(7) -0.024(9) 0.010(8) C31 0.123(7) 0.084(6) 0.072(3) -0.028(5) 0.018(5) -0.027(4) C32 0.149(7) 0.145(8) 0.124(7) -0.022(6) 0.046(6) -0.014(6) C33 0.158(7) 0.119(6) 0.078(4) -0.002(4) 0.051(5) -0.006(5) C34 0.184(9) 0.133(6) 0.070(4) -0.010(4) 0.043(5) -0.046(7) C31' 0.123(7) 0.084(6) 0.072(3) -0.028(5) 0.018(5) -0.027(4) C32' 0.149(7) 0.145(8) 0.124(7) -0.022(6) 0.046(6) -0.014(6) C33' 0.158(7) 0.119(6) 0.078(4) -0.002(4) 0.051(5) -0.006(5) C34' 0.184(9) 0.133(6) 0.070(4) -0.010(4) 0.043(5) -0.046(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C27' Si1 C22 113.6(8) . . C31 Si1 C22 109.7(4) . . C27' Si1 C23 122.0(18) . . C31 Si1 C23 116.9(4) . . C22 Si1 C23 105.02(18) . . C31 Si1 C27 102.3(9) . . C22 Si1 C27 106.5(4) . . C23 Si1 C27 116.0(10) . . C27' Si1 C31' 110.9(14) . . C22 Si1 C31' 103.9(4) . . C23 Si1 C31' 99.1(4) . . C20 C1 C2 120.7(2) . . C20 C1 C21 120.4(2) . . C2 C1 C21 118.8(2) . . C1 C2 C3 121.4(2) . . C1 C2 C10 119.2(2) . . C3 C2 C10 119.4(2) . . C4 C3 C2 120.2(2) . . C4 C3 H3 119.9 . . C2 C3 H3 119.9 . . C3 C4 C8 119.9(2) . . C3 C4 C5 128.2(3) . . C8 C4 C5 111.9(2) . . C6 C5 C4 111.0(3) . . C6 C5 H5 124.5 . . C4 C5 H5 124.5 . . C5 C6 S7 115.4(2) . . C5 C6 H6 122.3 . . S7 C6 H6 122.3 . . C6 S7 C8 90.87(15) . . C9 C8 C4 122.1(2) . . C9 C8 S7 127.0(2) . . C4 C8 S7 110.86(19) . . C8 C9 C10 119.0(3) . . C8 C9 H9 120.5 . . C10 C9 H9 120.5 . . C11 C10 C9 121.0(2) . . C11 C10 C2 119.6(2) . . C9 C10 C2 119.3(2) . . C12 C11 C10 121.8(2) . . C12 C11 H11 119.1 . . C10 C11 H11 119.1 . . C11 C12 C13 120.8(2) . . C11 C12 C20 119.6(2) . . C13 C12 C20 119.6(2) . . C14 C13 C12 119.2(2) . . C14 C13 H13 120.4 . . C12 C13 H13 120.4 . . C13 C14 C18 121.8(2) . . C13 C14 S15 127.0(2) . . C18 C14 S15 111.23(18) . . C16 S15 C14 90.89(13) . . C17 C16 S15 114.8(2) . . C17 C16 H16 122.6 . . S15 C16 H16 122.6 . . C16 C17 C18 111.9(3) . . C16 C17 H17 124.0 . . C18 C17 H17 124.0 . . C19 C18 C14 120.1(2) . . C19 C18 C17 128.7(3) . . C14 C18 C17 111.1(2) . . C18 C19 C20 120.0(2) . . C18 C19 H19 120.0 . . C20 C19 H19 120.0 . . C1 C20 C19 121.7(2) . . C1 C20 C12 119.1(2) . . C19 C20 C12 119.3(2) . . C22 C21 C1 177.2(3) . . C21 C22 Si1 177.1(3) . . C25 C23 C24 111.5(5) . . C25 C23 Si1 114.8(3) . . C24 C23 Si1 112.3(4) . . C25 C23 H23 105.8 . . C24 C23 H23 105.8 . . Si1 C23 H23 105.8 . . C23 C24 H24A 109.5 . . C23 C24 H24B 109.5 . . H24A C24 H24B 109.5 . . C23 C24 H24C 109.5 . . H24A C24 H24C 109.5 . . H24B C24 H24C 109.5 . . C23 C25 C26 115.3(4) . . C23 C25 H25A 108.4 . . C26 C25 H25A 108.4 . . C23 C25 H25B 108.4 . . C26 C25 H25B 108.4 . . H25A C25 H25B 107.5 . . C25 C26 H26A 109.5 . . C25 C26 H26B 109.5 . . H26A C26 H26B 109.5 . . C25 C26 H26C 109.5 . . H26A C26 H26C 109.5 . . H26B C26 H26C 109.5 . . C29 C27 C28 111.5(19) . . C29 C27 Si1 118.6(10) . . C28 C27 Si1 119.8(10) . . C29 C27 H27 100.7 . . C28 C27 H27 100.7 . . Si1 C27 H27 100.7 . . C27 C28 H28A 109.5 . . C27 C28 H28B 109.5 . . H28A C28 H28B 109.5 . . C27 C28 H28C 109.5 . . H28A C28 H28C 109.5 . . H28B C28 H28C 109.5 . . C30 C29 C27 141.8(18) . . C30 C29 H29A 101.5 . . C27 C29 H29A 101.5 . . C30 C29 H29B 101.5 . . C27 C29 H29B 101.5 . . H29A C29 H29B 104.6 . . C29 C30 H30A 109.5 . . C29 C30 H30B 109.5 . . H30A C30 H30B 109.5 . . C29 C30 H30C 109.5 . . H30A C30 H30C 109.5 . . H30B C30 H30C 109.5 . . C29' C27' C28' 111(2) . . C29' C27' Si1 118(2) . . C28' C27' Si1 109(2) . . C29' C27' H27' 106.1 . . C28' C27' H27' 106.1 . . Si1 C27' H27' 106.1 . . C27' C28' H28D 109.5 . . C27' C28' H28E 109.5 . . H28D C28' H28E 109.5 . . C27' C28' H28F 109.5 . . H28D C28' H28F 109.5 . . H28E C28' H28F 109.5 . . C30' C29' C27' 132(3) . . C30' C29' H29C 104.2 . . C27' C29' H29C 104.2 . . C30' C29' H29D 104.2 . . C27' C29' H29D 104.2 . . H29C C29' H29D 105.5 . . C29' C30' H30D 109.5 . . C29' C30' H30E 109.5 . . H30D C30' H30E 109.5 . . C29' C30' H30F 109.5 . . H30D C30' H30F 109.5 . . H30E C30' H30F 109.5 . . C33 C31 C32 106.0(10) . . C33 C31 Si1 105.8(8) . . C32 C31 Si1 115.1(9) . . C33 C31 H31 109.9 . . C32 C31 H31 109.9 . . Si1 C31 H31 109.9 . . C31 C32 H32A 109.5 . . C31 C32 H32B 109.5 . . H32A C32 H32B 109.5 . . C31 C32 H32C 109.5 . . H32A C32 H32C 109.5 . . H32B C32 H32C 109.5 . . C31 C33 C34 117.9(11) . . C31 C33 H33A 107.8 . . C34 C33 H33A 107.8 . . C31 C33 H33B 107.8 . . C34 C33 H33B 107.8 . . H33A C33 H33B 107.2 . . C33 C34 H34A 109.5 . . C33 C34 H34B 109.5 . . H34A C34 H34B 109.5 . . C33 C34 H34C 109.5 . . H34A C34 H34C 109.5 . . H34B C34 H34C 109.5 . . C33' C31' C32' 108.3(11) . . C33' C31' Si1 112.9(9) . . C32' C31' Si1 117.8(9) . . C33' C31' H31' 105.6 . . C32' C31' H31' 105.6 . . Si1 C31' H31' 105.6 . . C31' C32' H32D 109.5 . . C31' C32' H32E 109.5 . . H32D C32' H32E 109.5 . . C31' C32' H32F 109.5 . . H32D C32' H32F 109.5 . . H32E C32' H32F 109.5 . . C31' C33' C34' 119.7(12) . . C31' C33' H33C 107.4 . . C34' C33' H33C 107.4 . . C31' C33' H33D 107.4 . . C34' C33' H33D 107.4 . . H33C C33' H33D 106.9 . . C33' C34' H34D 109.5 . . C33' C34' H34E 109.5 . . H34D C34' H34E 109.5 . . C33' C34' H34F 109.5 . . H34D C34' H34F 109.5 . . H34E C34' H34F 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Si1 C27' 1.66(3) . Si1 C31 1.838(12) . Si1 C22 1.847(3) . Si1 C23 1.899(5) . Si1 C27 1.918(17) . Si1 C31' 1.965(13) . C1 C20 1.415(3) . C1 C2 1.420(3) . C1 C21 1.433(4) . C2 C3 1.420(3) . C2 C10 1.441(4) . C3 C4 1.377(4) . C3 H3 0.9500 . C4 C8 1.427(4) . C4 C5 1.474(3) . C5 C6 1.336(5) . C5 H5 0.9500 . C6 S7 1.742(4) . C6 H6 0.9500 . S7 C8 1.746(3) . C8 C9 1.368(4) . C9 C10 1.433(3) . C9 H9 0.9500 . C10 C11 1.396(3) . C11 C12 1.396(3) . C11 H11 0.9500 . C12 C13 1.427(3) . C12 C20 1.445(4) . C13 C14 1.371(4) . C13 H13 0.9500 . C14 C18 1.434(4) . C14 S15 1.740(2) . S15 C16 1.734(4) . C16 C17 1.343(4) . C16 H16 0.9500 . C17 C18 1.456(3) . C17 H17 0.9500 . C18 C19 1.375(3) . C19 C20 1.427(3) . C19 H19 0.9500 . C21 C22 1.211(4) . C23 C25 1.476(7) . C23 C24 1.579(7) . C23 H23 1.0000 . C24 H24A 0.9800 . C24 H24B 0.9800 . C24 H24C 0.9800 . C25 C26 1.550(7) . C25 H25A 0.9900 . C25 H25B 0.9900 . C26 H26A 0.9800 . C26 H26B 0.9800 . C26 H26C 0.9800 . C27 C29 1.495(15) . C27 C28 1.53(2) . C27 H27 1.0000 . C28 H28A 0.9800 . C28 H28B 0.9800 . C28 H28C 0.9800 . C29 C30 1.22(2) . C29 H29A 0.9900 . C29 H29B 0.9900 . C30 H30A 0.9800 . C30 H30B 0.9800 . C30 H30C 0.9800 . C27' C29' 1.506(16) . C27' C28' 1.51(2) . C27' H27' 1.0000 . C28' H28D 0.9800 . C28' H28E 0.9800 . C28' H28F 0.9800 . C29' C30' 1.23(3) . C29' H29C 0.9900 . C29' H29D 0.9900 . C30' H30D 0.9800 . C30' H30E 0.9800 . C30' H30F 0.9800 . C31 C33 1.467(13) . C31 C32 1.531(15) . C31 H31 1.0000 . C32 H32A 0.9800 . C32 H32B 0.9800 . C32 H32C 0.9800 . C33 C34 1.520(12) . C33 H33A 0.9900 . C33 H33B 0.9900 . C34 H34A 0.9800 . C34 H34B 0.9800 . C34 H34C 0.9800 . C31' C33' 1.488(14) . C31' C32' 1.520(16) . C31' H31' 1.0000 . C32' H32D 0.9800 . C32' H32E 0.9800 . C32' H32F 0.9800 . C33' C34' 1.514(12) . C33' H33C 0.9900 . C33' H33D 0.9900 . C34' H34D 0.9800 . C34' H34E 0.9800 . C34' H34F 0.9800 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 C20 C1 C2 C3 178.4(2) . . . . C21 C1 C2 C3 -1.6(4) . . . . C20 C1 C2 C10 -1.5(4) . . . . C21 C1 C2 C10 178.5(2) . . . . C1 C2 C3 C4 -178.8(2) . . . . C10 C2 C3 C4 1.1(4) . . . . C2 C3 C4 C8 -1.0(4) . . . . C2 C3 C4 C5 178.6(3) . . . . C3 C4 C5 C6 -179.7(3) . . . . C8 C4 C5 C6 0.0(4) . . . . C4 C5 C6 S7 -0.2(4) . . . . C5 C6 S7 C8 0.4(3) . . . . C3 C4 C8 C9 0.0(4) . . . . C5 C4 C8 C9 -179.7(3) . . . . C3 C4 C8 S7 180.0(2) . . . . C5 C4 C8 S7 0.3(3) . . . . C6 S7 C8 C9 179.6(3) . . . . C6 S7 C8 C4 -0.4(2) . . . . C4 C8 C9 C10 0.9(4) . . . . S7 C8 C9 C10 -179.1(2) . . . . C8 C9 C10 C11 178.4(2) . . . . C8 C9 C10 C2 -0.8(4) . . . . C1 C2 C10 C11 0.5(4) . . . . C3 C2 C10 C11 -179.3(2) . . . . C1 C2 C10 C9 179.7(2) . . . . C3 C2 C10 C9 -0.2(4) . . . . C9 C10 C11 C12 -178.7(2) . . . . C2 C10 C11 C12 0.4(4) . . . . C10 C11 C12 C13 179.3(2) . . . . C10 C11 C12 C20 -0.3(4) . . . . C11 C12 C13 C14 -179.5(2) . . . . C20 C12 C13 C14 0.2(4) . . . . C12 C13 C14 C18 -1.2(4) . . . . C12 C13 C14 S15 179.69(19) . . . . C13 C14 S15 C16 178.9(3) . . . . C18 C14 S15 C16 -0.3(2) . . . . C14 S15 C16 C17 0.3(3) . . . . S15 C16 C17 C18 -0.2(4) . . . . C13 C14 C18 C19 1.3(4) . . . . S15 C14 C18 C19 -179.5(2) . . . . C13 C14 C18 C17 -179.0(2) . . . . S15 C14 C18 C17 0.2(3) . . . . C16 C17 C18 C19 179.7(3) . . . . C16 C17 C18 C14 0.0(4) . . . . C14 C18 C19 C20 -0.2(4) . . . . C17 C18 C19 C20 -179.8(3) . . . . C2 C1 C20 C19 -179.6(2) . . . . C21 C1 C20 C19 0.4(4) . . . . C2 C1 C20 C12 1.6(4) . . . . C21 C1 C20 C12 -178.5(2) . . . . C18 C19 C20 C1 -179.6(2) . . . . C18 C19 C20 C12 -0.8(4) . . . . C11 C12 C20 C1 -0.7(3) . . . . C13 C12 C20 C1 179.7(2) . . . . C11 C12 C20 C19 -179.5(2) . . . . C13 C12 C20 C19 0.9(3) . . . . C27' Si1 C23 C25 73.5(10) . . . . C31 Si1 C23 C25 -179.5(5) . . . . C22 Si1 C23 C25 -57.6(4) . . . . C27 Si1 C23 C25 59.6(6) . . . . C31' Si1 C23 C25 -164.8(5) . . . . C27' Si1 C23 C24 -55.4(10) . . . . C31 Si1 C23 C24 51.7(6) . . . . C22 Si1 C23 C24 173.6(5) . . . . C27 Si1 C23 C24 -69.2(7) . . . . C31' Si1 C23 C24 66.4(6) . . . . C24 C23 C25 C26 -62.8(7) . . . . Si1 C23 C25 C26 168.0(4) . . . . C28 C27 C29 C30 9(6) . . . . Si1 C27 C29 C30 155(4) . . . . C31 Si1 C27' C29' -71(3) . . . . C22 Si1 C27' C29' 178(3) . . . . C23 Si1 C27' C29' 50(4) . . . . C27 Si1 C27' C29' 117(12) . . . . C31' Si1 C27' C29' -66(4) . . . . C31 Si1 C27' C28' 161(3) . . . . C22 Si1 C27' C28' 50(3) . . . . C23 Si1 C27' C28' -77(2) . . . . C27 Si1 C27' C28' -10(7) . . . . C31' Si1 C27' C28' 167(2) . . . . C28' C27' C29' C30' 24(7) . . . . Si1 C27' C29' C30' -103(4) . . . . C27' Si1 C31 C33 -176.0(16) . . . . C22 Si1 C31 C33 -61.2(9) . . . . C23 Si1 C31 C33 58.2(10) . . . . C27 Si1 C31 C33 -173.9(11) . . . . C31' Si1 C31 C33 17.4(14) . . . . C27' Si1 C31 C32 -59.3(15) . . . . C22 Si1 C31 C32 55.5(9) . . . . C23 Si1 C31 C32 174.9(8) . . . . C27 Si1 C31 C32 -57.2(11) . . . . C31' Si1 C31 C32 134(2) . . . . C32 C31 C33 C34 63.7(15) . . . . Si1 C31 C33 C34 -173.6(11) . . . . C32' C31' C33' C34' -50.5(15) . . . . Si1 C31' C33' C34' 177.2(10) . . . .