#------------------------------------------------------------------------------ #$Date: 2019-10-07 12:07:06 +0300 (Mon, 07 Oct 2019) $ #$Revision: 219127 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/23/44/7234417.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7234417 loop_ _publ_author_name 'Rawad K. Hallani' 'Karl J. Thorley' 'Anna K. Hailey' 'Sean R. Parkin' 'Yueh-Lin Loo' 'John E. Anthony' _publ_section_title ; The effect of regioisomerism on the crystal packing and device performance of desymmetrized anthradithiophenes ; _journal_name_full 'Journal of Materials Chemistry C' _journal_page_first 8956 _journal_page_last 8962 _journal_paper_doi 10.1039/C5TC02145F _journal_volume 3 _journal_year 2015 _chemical_formula_moiety 'C32 H36 S2 Si, C31 H33 S2 Si, C H3' _chemical_formula_sum 'C32 H36 S2 Si' _chemical_formula_weight 512.82 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _cell_angle_alpha 90 _cell_angle_beta 106.356(2) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 18.6511(5) _cell_length_b 19.2711(5) _cell_length_c 16.3771(4) _cell_measurement_reflns_used 9773 _cell_measurement_temperature 90.0(2) _cell_measurement_theta_max 67.90 _cell_measurement_theta_min 2.47 _cell_volume 5648.2(3) _computing_cell_refinement 'APEX2 (Bruker-AXS, 2006)' _computing_data_collection 'APEX2 (Bruker-AXS, 2006)' _computing_data_reduction 'APEX2 (Bruker-AXS, 2006)' _computing_molecular_graphics 'XP in SHELXTL (Sheldrick, 2008)' _computing_publication_material 'SHELX (Sheldrick, 2008) and CIFFIX (Parkin, 2013)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2015b)' _computing_structure_solution 'SHELXT (Sheldrick, 2015a)' _diffrn_ambient_temperature 90.0(2) _diffrn_detector_area_resol_mean 5.6 _diffrn_measured_fraction_theta_full 0.961 _diffrn_measured_fraction_theta_max 0.958 _diffrn_measurement_device_type 'Bruker X8 Proteum diffractometer' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0496 _diffrn_reflns_av_unetI/netI 0.0383 _diffrn_reflns_Laue_measured_fraction_full 0.961 _diffrn_reflns_Laue_measured_fraction_max 0.958 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -22 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -7 _diffrn_reflns_number 59932 _diffrn_reflns_point_group_measured_fraction_full 0.961 _diffrn_reflns_point_group_measured_fraction_max 0.958 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 67.933 _diffrn_reflns_theta_min 2.469 _diffrn_source 'fine-focus rotating anode' _exptl_absorpt_coefficient_mu 2.239 _exptl_absorpt_correction_T_max 0.942 _exptl_absorpt_correction_T_min 0.658 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS (Krause et al., 2015)' _exptl_crystal_colour red _exptl_crystal_density_diffrn 1.206 _exptl_crystal_description block _exptl_crystal_F_000 2192 _exptl_crystal_size_max 0.280 _exptl_crystal_size_mid 0.240 _exptl_crystal_size_min 0.115 _refine_diff_density_max 0.925 _refine_diff_density_min -0.488 _refine_diff_density_rms 0.092 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.164 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 717 _refine_ls_number_reflns 9853 _refine_ls_number_restraints 498 _refine_ls_restrained_S_all 1.173 _refine_ls_R_factor_all 0.1265 _refine_ls_R_factor_gt 0.0866 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1580P)^2^+6.2276P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2408 _refine_ls_wR_factor_ref 0.2837 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 6868 _reflns_number_total 9853 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file J-Mater-Chem-C-2015-3-8956.cif _cod_data_source_block x13371x _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 7234417 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.573 _shelx_estimated_absorpt_t_max 0.783 _exptl_absorpt_special_details ; In addition to absorption, multi-scan techniques also correct other slowly varying changes in scale factor over reciprocal space, such as those caused by x-ray beam inhomogeneity, goniometer imperfection, crystal decomposition, crystal longer than the x-ray beam cross section, absorption by the crystal mount etc. These account, by and large, for much of the difference between estimated values of Tmin and Tmax and the _exptl_absorpt_correction_ values. ; _shelx_res_file ; x13371x.res created by SHELXL-2014/7 TITL x13371 in P2(1)/c CELL 1.54178 18.6511 19.2711 16.3771 90.000 106.356 90.000 ZERR 8.00 0.0005 0.0005 0.0004 0.000 0.002 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H SI S UNIT 256 288 8 16 TEMP -183.000 SIZE 0.28 0.24 0.115 REM COLR red REM FORM block REM The very weakest data were systematically too low, presumably as a result REM of bad backgrounds and poorly shaped reflection profiles. Hence the 0 on REM the MERG line. Fresh crystals are unlikely to result in a better dataset REM in this case. Part of the problem is likely to do with the sec-butyl REM groups. These are not enantiomerically pure, so there is an unholy mix REM of isomers in the crystal, which naturally leads to extensive disorder. OMIT 0 136 L.S. 16 BOND $H CONF ACTA LIST 4 FMAP 2 PLAN 10 WGHT 0.158000 6.227600 FVAR 0.27826 0.63776 0.53890 SI1A 3 0.802565 0.925685 0.466206 11.00000 0.04523 0.08663 = 0.05966 0.00848 0.01761 0.01588 C1A 1 0.561439 0.983669 0.376124 11.00000 0.04319 0.03102 = 0.02890 0.00431 0.01703 0.00276 C2A 1 0.534131 1.037323 0.418605 11.00000 0.04939 0.02806 = 0.02871 0.00455 0.02076 0.00101 C3A 1 0.580131 1.071493 0.490564 11.00000 0.03900 0.03337 = 0.02915 0.00637 0.01239 0.00412 AFIX 43 H3A 2 0.631035 1.058435 0.512763 11.00000 -1.20000 AFIX 0 C4A 1 0.551150 1.123230 0.527943 11.00000 0.04818 0.03271 = 0.02913 0.00258 0.01386 -0.00490 S5A 4 0.598379 1.171723 0.616944 11.00000 0.06126 0.03583 = 0.03267 -0.00014 0.01454 -0.00056 C6A 1 0.517672 1.218769 0.612279 11.00000 0.06713 0.03818 = 0.03462 -0.00197 0.02273 0.00354 AFIX 43 H6A 2 0.516492 1.254631 0.651681 11.00000 -1.20000 AFIX 0 C7A 1 0.456897 1.200813 0.548861 11.00000 0.06524 0.02169 = 0.02723 0.00137 0.01870 0.00096 AFIX 43 H7A 2 0.408999 1.221542 0.539000 11.00000 -1.20000 AFIX 0 C8A 1 0.475103 1.144505 0.496906 11.00000 0.05481 0.02998 = 0.02825 0.00207 0.02190 -0.00006 C9A 1 0.428898 1.112214 0.426994 11.00000 0.04308 0.03207 = 0.02885 0.00106 0.01628 0.00195 AFIX 43 H9A 2 0.378173 1.126232 0.406213 11.00000 -1.20000 AFIX 0 C10A 1 0.456751 1.057641 0.385368 11.00000 0.04601 0.03150 = 0.02709 0.00312 0.01739 0.00283 C11A 1 0.412136 1.024562 0.313880 11.00000 0.04281 0.03137 = 0.03014 0.00306 0.01471 0.00478 AFIX 43 H11A 2 0.361272 1.038136 0.293048 11.00000 -1.20000 AFIX 0 C12A 1 0.438707 0.972059 0.271044 11.00000 0.04589 0.02864 = 0.02547 0.00412 0.01592 0.00153 C13A 1 0.392295 0.939488 0.197158 11.00000 0.04152 0.03963 = 0.02537 0.00531 0.01100 0.00261 AFIX 43 H13A 2 0.341422 0.952922 0.175899 11.00000 -1.20000 AFIX 0 C14A 1 0.420599 0.888774 0.156422 11.00000 0.05735 0.03059 = 0.02460 0.00219 0.01460 -0.00336 C15A 1 0.383717 0.849863 0.080478 11.00000 0.06487 0.04234 = 0.02568 0.00106 0.01427 0.00036 AFIX 43 H15A 2 0.332376 0.855024 0.050578 11.00000 -1.20000 AFIX 0 C16A 1 0.429694 0.805983 0.057089 11.00000 0.07775 0.03390 = 0.03440 -0.00161 0.02347 -0.00502 AFIX 43 H16A 2 0.414060 0.777373 0.008034 11.00000 -1.20000 AFIX 0 S17A 4 0.520453 0.805520 0.123744 11.00000 0.06554 0.03218 = 0.03872 -0.00186 0.02700 0.00119 C18A 1 0.496595 0.868969 0.188291 11.00000 0.05442 0.03036 = 0.02608 0.00312 0.02060 0.00353 C19A 1 0.543557 0.898199 0.259568 11.00000 0.05071 0.02382 = 0.03368 0.00318 0.02065 0.00394 AFIX 43 H19A 2 0.594110 0.883529 0.279682 11.00000 -1.20000 AFIX 0 C20A 1 0.515409 0.951103 0.303262 11.00000 0.04655 0.02902 = 0.02634 0.00440 0.01778 0.00203 C21A 1 0.637637 0.963650 0.407355 11.00000 0.04599 0.03858 = 0.03964 -0.00211 0.02015 0.00035 C22A 1 0.703407 0.947522 0.433237 11.00000 0.05059 0.04764 = 0.04910 -0.00222 0.01781 0.00478 EADP C23A C23C EADP C24A C25C EADP C25A C24C SAME 0.010 C23C C24C C25C C26C RIGU 0.005 C23A > C26C ISOR 0.010 C23A > C26C PART 1 C23A 1 0.834896 0.931888 0.366837 10.50000 0.06235 0.08206 = 0.06706 0.00046 0.03434 0.00653 AFIX 13 H23A 2 0.886997 0.913596 0.378676 10.50000 -1.20000 AFIX 0 C24A 1 0.833922 1.009004 0.347091 10.50000 0.08414 0.09275 = 0.08985 0.01689 0.03491 -0.00681 AFIX 33 H24A 2 0.867157 1.033575 0.395509 10.50000 -1.50000 H24B 2 0.851047 1.016301 0.296397 10.50000 -1.50000 H24C 2 0.782932 1.026857 0.336634 10.50000 -1.50000 AFIX 0 C25A 1 0.782512 0.892011 0.290792 10.50000 0.10258 0.11144 = 0.08257 -0.00753 0.03856 -0.00408 AFIX 23 H25A 2 0.730185 0.908548 0.276444 10.50000 -1.20000 H25B 2 0.784382 0.841126 0.299439 10.50000 -1.20000 AFIX 0 C26A 1 0.827130 0.917808 0.219720 10.50000 0.15549 0.13275 = 0.08593 -0.00006 0.05637 0.04139 AFIX 33 H26A 2 0.802368 0.897763 0.163901 10.50000 -1.50000 H26B 2 0.825782 0.968551 0.215634 10.50000 -1.50000 H26C 2 0.879188 0.902111 0.238294 10.50000 -1.50000 AFIX 0 PART 2 C23C 1 0.840557 0.957958 0.375237 10.50000 0.06235 0.08206 = 0.06706 0.00046 0.03434 0.00653 AFIX 13 H23C 2 0.893497 0.941755 0.387952 10.50000 -1.20000 AFIX 0 C24C 1 0.797134 0.923418 0.292390 10.50000 0.10258 0.11144 = 0.08257 -0.00753 0.03856 -0.00408 AFIX 33 H24D 2 0.797209 0.873021 0.300407 10.50000 -1.50000 H24E 2 0.745542 0.940464 0.275907 10.50000 -1.50000 H24F 2 0.820720 0.934551 0.247562 10.50000 -1.50000 AFIX 0 C25C 1 0.841140 1.037837 0.363953 10.50000 0.08414 0.09275 = 0.08985 0.01689 0.03491 -0.00681 AFIX 23 H25C 2 0.877489 1.061597 0.411594 10.50000 -1.20000 H25D 2 0.791001 1.058999 0.353552 10.50000 -1.20000 AFIX 0 C26C 1 0.870208 1.032635 0.274829 10.50000 0.11934 0.20550 = 0.13611 0.04828 0.05860 -0.00684 AFIX 33 H26D 2 0.875224 1.079472 0.253783 10.50000 -1.50000 H26E 2 0.918649 1.008992 0.288178 10.50000 -1.50000 H26F 2 0.833537 1.006435 0.231060 10.50000 -1.50000 AFIX 0 PART 0 EXYZ C27A C27C EADP C27A C27C EADP C28A C28C EADP C29A C29C EADP C30A C30C SAME 0.010 C27C C28C C29C C30C RIGU 0.005 C27A > C30C ISOR 0.010 C27A > C30C PART 1 C27A 1 0.810012 0.830259 0.492475 21.00000 0.09844 0.10101 = 0.12056 0.01845 0.04945 0.03878 AFIX 13 H27A 2 0.767276 0.815376 0.443545 21.00000 -1.20000 AFIX 0 C28A 1 0.868667 0.787477 0.468280 21.00000 0.11218 0.12715 = 0.15946 0.00198 0.06954 0.03641 AFIX 137 H28A 2 0.918266 0.800285 0.504582 21.00000 -1.50000 H28B 2 0.866167 0.796238 0.408597 21.00000 -1.50000 H28C 2 0.859655 0.738126 0.475950 21.00000 -1.50000 AFIX 0 C29A 1 0.777923 0.805958 0.559333 21.00000 0.07971 0.07278 = 0.07207 -0.01071 0.02097 0.01084 AFIX 23 H29A 2 0.729119 0.829420 0.550592 21.00000 -1.20000 H29B 2 0.810759 0.822651 0.614371 21.00000 -1.20000 AFIX 0 C30A 1 0.765438 0.729846 0.568728 21.00000 0.10454 0.07247 = 0.07429 -0.01347 0.02181 0.01504 AFIX 137 H30A 2 0.716490 0.716655 0.531148 21.00000 -1.50000 H30B 2 0.767075 0.719734 0.627870 21.00000 -1.50000 H30C 2 0.804592 0.703416 0.553304 21.00000 -1.50000 AFIX 0 PART 2 C27C 1 0.810012 0.830259 0.492475 -21.00000 0.09844 0.10101 = 0.12056 0.01845 0.04945 0.03878 AFIX 13 H27C 2 0.799478 0.810163 0.433991 -21.00000 -1.20000 AFIX 0 C28C 1 0.891842 0.810854 0.528058 -21.00000 0.11218 0.12715 = 0.15946 0.00198 0.06954 0.03641 AFIX 33 H28D 2 0.922085 0.839016 0.500469 -21.00000 -1.50000 H28E 2 0.907744 0.819417 0.589525 -21.00000 -1.50000 H28F 2 0.898484 0.761610 0.517133 -21.00000 -1.50000 AFIX 0 C29C 1 0.751492 0.797152 0.521201 -21.00000 0.07971 0.07278 = 0.07207 -0.01071 0.02097 0.01084 AFIX 23 H29C 2 0.709136 0.788155 0.470203 -21.00000 -1.20000 H29D 2 0.733906 0.831391 0.556326 -21.00000 -1.20000 AFIX 0 C30C 1 0.767282 0.730784 0.571113 -21.00000 0.10454 0.07247 = 0.07429 -0.01347 0.02181 0.01504 AFIX 33 H30D 2 0.722095 0.715620 0.585330 -21.00000 -1.50000 H30E 2 0.782566 0.694960 0.536966 -21.00000 -1.50000 H30F 2 0.807488 0.738461 0.623615 -21.00000 -1.50000 AFIX 0 PART 0 EADP C31A C31C EADP C32A C33C EADP C33A C32C SAME 0.010 C31C C32C C33C C34C RIGU 0.005 C31A > C34C ISOR 0.010 C31A > C34C PART 1 C31A 1 0.846053 0.989845 0.559001 21.00000 0.07751 0.08331 = 0.07439 0.00980 -0.00467 -0.00879 AFIX 13 H31A 2 0.843365 1.038356 0.536662 21.00000 -1.20000 AFIX 0 C32A 1 0.925695 0.968453 0.593957 21.00000 0.08656 0.14027 = 0.12215 0.02080 0.00576 -0.02055 AFIX 137 H32A 2 0.951615 1.001605 0.637720 21.00000 -1.50000 H32B 2 0.949856 0.967625 0.548014 21.00000 -1.50000 H32C 2 0.927937 0.922076 0.619102 21.00000 -1.50000 AFIX 0 C33A 1 0.792749 0.982675 0.630337 21.00000 0.09629 0.10578 = 0.07111 0.00621 -0.00076 -0.01707 AFIX 23 H33A 2 0.739233 0.989285 0.599989 21.00000 -1.20000 H33B 2 0.799023 0.935831 0.656200 21.00000 -1.20000 AFIX 0 C34A 1 0.816283 1.034219 0.695525 21.00000 0.25569 0.22251 = 0.17051 -0.06289 0.05340 -0.02972 AFIX 137 H34A 2 0.807946 1.017069 0.748444 21.00000 -1.50000 H34B 2 0.787437 1.076848 0.677848 21.00000 -1.50000 H34C 2 0.869554 1.043977 0.704847 21.00000 -1.50000 AFIX 0 PART 2 C31C 1 0.850662 0.968772 0.556667 -21.00000 0.07751 0.08331 = 0.07439 0.00980 -0.00467 -0.00879 AFIX 13 H31C 2 0.828368 1.014592 0.534423 -21.00000 -1.20000 AFIX 0 C32C 1 0.831955 0.977572 0.639209 -21.00000 0.09629 0.10578 = 0.07111 0.00621 -0.00076 -0.01707 AFIX 33 H32D 2 0.870993 1.005110 0.678392 -21.00000 -1.50000 H32E 2 0.783847 1.001463 0.628958 -21.00000 -1.50000 H32F 2 0.828785 0.931901 0.664282 -21.00000 -1.50000 AFIX 0 C33C 1 0.941670 0.997540 0.567888 -21.00000 0.08656 0.14027 = 0.12215 0.02080 0.00576 -0.02055 AFIX 23 H33C 2 0.974513 0.957797 0.565036 -21.00000 -1.20000 H33D 2 0.942426 1.030441 0.521712 -21.00000 -1.20000 AFIX 0 C34C 1 0.967403 1.031525 0.649777 -21.00000 0.13440 0.20020 = 0.16009 -0.02376 0.02009 -0.04088 AFIX 33 H34D 2 1.018546 1.048334 0.658038 -21.00000 -1.50000 H34E 2 0.934565 1.070798 0.651794 -21.00000 -1.50000 H34F 2 0.966521 0.998453 0.694940 -21.00000 -1.50000 AFIX 0 PART 0 SI1B 3 0.917212 1.161546 0.019208 11.00000 0.06968 0.07536 = 0.14898 0.01113 0.06079 -0.00926 C1B 1 0.731026 1.022139 0.037828 11.00000 0.04385 0.04380 = 0.03686 0.00581 0.01083 0.00066 C2B 1 0.707198 0.966040 -0.017291 11.00000 0.04147 0.04070 = 0.03194 0.00841 0.01256 0.00274 C3B 1 0.749259 0.940178 -0.071441 11.00000 0.04896 0.04328 = 0.04140 0.00819 0.01877 0.00910 AFIX 43 H3B 2 0.796622 0.959659 -0.068929 11.00000 -1.20000 AFIX 0 C4B 1 0.721382 0.887799 -0.126363 11.00000 0.04382 0.04969 = 0.03692 0.00565 0.01849 0.00801 S5B 4 0.763195 0.849655 -0.198409 11.00000 0.06051 0.06495 = 0.05298 -0.00436 0.03031 0.00634 C6B 1 0.688627 0.793935 -0.234450 11.00000 0.07641 0.05282 = 0.04234 -0.00215 0.02796 0.01453 AFIX 43 H6B 2 0.686013 0.760870 -0.278217 11.00000 -1.20000 AFIX 0 C7B 1 0.634699 0.801100 -0.195676 11.00000 0.05509 0.04317 = 0.03750 0.00113 0.02033 -0.00052 AFIX 43 H7B 2 0.590411 0.773935 -0.208847 11.00000 -1.20000 AFIX 0 C8B 1 0.651512 0.854856 -0.131505 11.00000 0.04723 0.04184 = 0.03274 0.00339 0.01489 0.00393 C9B 1 0.610022 0.878441 -0.078875 11.00000 0.05042 0.03773 = 0.03632 0.00482 0.01693 -0.00363 AFIX 43 H9B 2 0.563059 0.857818 -0.082007 11.00000 -1.20000 AFIX 0 C10B 1 0.637234 0.933135 -0.020420 11.00000 0.04953 0.03843 = 0.02791 0.00382 0.01713 0.00369 C11B 1 0.595215 0.957468 0.032293 11.00000 0.04900 0.02971 = 0.03449 0.00838 0.01911 0.00110 AFIX 43 H11B 2 0.548937 0.935771 0.029925 11.00000 -1.20000 AFIX 0 C12B 1 0.619614 1.012836 0.088275 11.00000 0.05128 0.03503 = 0.03038 0.00798 0.01746 0.00604 C13B 1 0.575112 1.037555 0.140686 11.00000 0.04830 0.03585 = 0.03201 0.01062 0.01820 -0.00001 AFIX 43 H13B 2 0.529080 1.015464 0.138525 11.00000 -1.20000 AFIX 0 C14B 1 0.598728 1.092879 0.193831 11.00000 0.05868 0.03344 = 0.03333 0.00587 0.01963 0.00366 C15B 1 0.563507 1.125329 0.252546 11.00000 0.06084 0.03622 = 0.03794 0.00835 0.02250 0.00711 AFIX 43 H15B 2 0.516700 1.111165 0.259237 11.00000 -1.20000 AFIX 0 C16B 1 0.603513 1.176533 0.295513 11.00000 0.08652 0.03897 = 0.04022 0.00244 0.02125 0.01518 AFIX 43 H16B 2 0.588518 1.202207 0.337435 11.00000 -1.20000 AFIX 0 S17B 4 0.686762 1.193701 0.269323 11.00000 0.06725 0.04710 = 0.04511 -0.00759 0.01433 -0.00148 C18B 1 0.668506 1.125802 0.196090 11.00000 0.06001 0.03825 = 0.02981 0.00055 0.00890 0.00216 C19B 1 0.711818 1.104131 0.146495 11.00000 0.04753 0.04388 = 0.03680 0.00326 0.01289 -0.00279 AFIX 43 H19B 2 0.757362 1.127318 0.149120 11.00000 -1.20000 AFIX 0 C20B 1 0.688724 1.046908 0.090997 11.00000 0.04092 0.03845 = 0.03170 0.00648 0.01105 0.00402 C21B 1 0.795940 1.060824 0.035088 11.00000 0.05092 0.04727 = 0.05181 -0.00541 0.02179 0.00091 C22B 1 0.847719 1.097303 0.030721 11.00000 0.05483 0.05987 = 0.07353 -0.00427 0.02880 -0.00588 EADP C23B C23D EADP C24B C24D EADP C25B C25D EADP C26B C26D SAME 0.010 C23d c24d c25d c26d RIGU 0.005 C23B > C26D ISOR 0.010 C23B > C26D PART 1 C23B 1 0.857739 1.247621 -0.016807 31.00000 0.08401 0.08256 = 0.10276 0.00881 0.03605 0.00049 AFIX 13 H23B 2 0.850673 1.253378 -0.079263 31.00000 -1.20000 AFIX 0 C24B 1 0.931179 1.312250 0.039843 31.00000 0.10964 0.11443 = 0.15990 0.02003 0.04518 -0.00606 AFIX 33 H24G 2 0.978890 1.300889 0.028994 31.00000 -1.50000 H24H 2 0.915744 1.359072 0.018745 31.00000 -1.50000 H24I 2 0.936981 1.310298 0.101162 31.00000 -1.50000 AFIX 0 C25B 1 0.797547 1.262183 -0.002914 31.00000 0.08446 0.08249 = 0.09307 -0.00454 0.02542 0.00413 AFIX 23 H25E 2 0.789477 1.221791 0.030793 31.00000 -1.20000 H25F 2 0.761410 1.255841 -0.059660 31.00000 -1.20000 AFIX 0 C26B 1 0.761917 1.321847 0.034856 31.00000 0.09601 0.10504 = 0.10907 -0.00306 0.03533 0.00817 AFIX 33 H26G 2 0.710363 1.309614 0.032454 31.00000 -1.50000 H26H 2 0.790685 1.329560 0.094184 31.00000 -1.50000 H26I 2 0.762061 1.364287 0.001935 31.00000 -1.50000 AFIX 0 PART 2 C23D 1 0.880805 1.248932 0.048035 -31.00000 0.08401 0.08256 = 0.10276 0.00881 0.03605 0.00049 AFIX 13 H23D 2 0.914986 1.261962 0.104803 -31.00000 -1.20000 AFIX 0 C24D 1 0.910697 1.303769 -0.032371 -31.00000 0.10964 0.11443 = 0.15990 0.02003 0.04518 -0.00606 AFIX 33 H24J 2 0.960631 1.289446 -0.034226 -31.00000 -1.50000 H24K 2 0.875150 1.297560 -0.088699 -31.00000 -1.50000 H24L 2 0.911803 1.352723 -0.015862 -31.00000 -1.50000 AFIX 0 C25D 1 0.817546 1.268046 0.049174 -31.00000 0.08446 0.08249 = 0.09307 -0.00454 0.02542 0.00413 AFIX 23 H25G 2 0.825725 1.279879 0.109939 -31.00000 -1.20000 H25H 2 0.789855 1.223585 0.041511 -31.00000 -1.20000 AFIX 0 C26D 1 0.755783 1.319705 0.005103 -31.00000 0.09601 0.10504 = 0.10907 -0.00306 0.03533 0.00817 AFIX 33 H26J 2 0.713611 1.315265 0.029390 -31.00000 -1.50000 H26K 2 0.775520 1.367095 0.013857 -31.00000 -1.50000 H26L 2 0.738906 1.309634 -0.055990 -31.00000 -1.50000 AFIX 0 PART 0 EXYZ C27B C27D EADP C27b C27d EADP C28B C28d EADP C29B C29D EADP C30B C30D SAME 0.010 C27D C28D C29D C30D RIGU 0.005 C27B > C30D ISOR 0.010 C27B > C30D PART 1 C27B 1 1.007444 1.149087 0.106167 31.00000 0.10459 0.11410 = 0.14122 0.00214 0.04390 -0.01826 AFIX 13 H27B 2 1.046809 1.178634 0.092923 31.00000 -1.20000 AFIX 0 C28B 1 1.036421 1.071553 0.117721 31.00000 0.08498 0.11870 = 0.13752 0.01483 0.03178 0.00022 AFIX 33 H28G 2 1.050709 1.057048 0.067116 31.00000 -1.50000 H28H 2 1.079876 1.068374 0.167878 31.00000 -1.50000 H28I 2 0.996627 1.041208 0.125328 31.00000 -1.50000 AFIX 0 C29B 1 0.983022 1.182407 0.172427 31.00000 0.12308 0.13844 = 0.13688 0.00312 0.05347 0.00640 AFIX 23 H29E 2 1.025840 1.210091 0.206251 31.00000 -1.20000 H29F 2 0.943748 1.215973 0.143948 31.00000 -1.20000 AFIX 0 C30B 1 0.955120 1.145461 0.231144 31.00000 0.16168 0.18238 = 0.14748 -0.01186 0.05318 -0.02562 AFIX 33 H30G 2 0.941863 1.178121 0.270411 31.00000 -1.50000 H30H 2 0.910651 1.119245 0.200520 31.00000 -1.50000 H30I 2 0.993436 1.113314 0.263349 31.00000 -1.50000 AFIX 0 PART 2 C27D 1 1.007444 1.149087 0.106167 -31.00000 0.10459 0.11410 = 0.14122 0.00214 0.04390 -0.01826 AFIX 13 H27D 2 1.042098 1.183048 0.090871 -31.00000 -1.20000 AFIX 0 C28D 1 1.034706 1.076538 0.079883 -31.00000 0.08498 0.11870 = 0.13752 0.01483 0.03178 0.00022 AFIX 33 H28J 2 1.024768 1.074567 0.017896 -31.00000 -1.50000 H28K 2 1.088450 1.071321 0.106814 -31.00000 -1.50000 H28L 2 1.007724 1.038955 0.098720 -31.00000 -1.50000 AFIX 0 C29D 1 1.017002 1.162826 0.195607 -31.00000 0.12308 0.13844 = 0.13688 0.00312 0.05347 0.00640 AFIX 23 H29G 2 0.966276 1.165622 0.203229 -31.00000 -1.20000 H29H 2 1.040970 1.121180 0.227101 -31.00000 -1.20000 AFIX 0 C30D 1 1.056666 1.220277 0.237449 -31.00000 0.16168 0.18238 = 0.14748 -0.01186 0.05318 -0.02562 AFIX 33 H30J 2 1.056467 1.219909 0.297223 -31.00000 -1.50000 H30K 2 1.108305 1.218185 0.234250 -31.00000 -1.50000 H30L 2 1.033011 1.262984 0.210185 -31.00000 -1.50000 AFIX 0 PART 0 EADP C31B C31d EADP C32B C33D EADP C33B C32D EADP C34B C34D SAME 0.005 C31d C32d C33d C34d RIGU C31b > C34d ISOR 0.010 C31b > C34d PART 1 C31B 1 0.927736 1.132602 -0.100147 21.00000 0.12860 0.12568 = 0.12843 -0.00543 0.07097 -0.00326 AFIX 13 H31B 2 0.929723 1.080773 -0.101537 21.00000 -1.20000 AFIX 0 C32B 1 0.852945 1.157697 -0.177106 21.00000 0.17370 0.20302 = 0.18843 0.01174 0.04935 0.00028 AFIX 137 H32G 2 0.868279 1.171566 -0.227266 21.00000 -1.50000 H32H 2 0.829223 1.197111 -0.157187 21.00000 -1.50000 H32I 2 0.817357 1.119167 -0.192114 21.00000 -1.50000 AFIX 0 C33B 1 1.000177 1.159430 -0.110653 21.00000 0.14861 0.15062 = 0.14993 -0.00880 0.07130 -0.00003 AFIX 23 H33E 2 0.999041 1.210784 -0.111989 21.00000 -1.20000 H33F 2 1.041771 1.144812 -0.061364 21.00000 -1.20000 AFIX 0 C34B 1 1.013419 1.132874 -0.190409 21.00000 0.20377 0.23624 = 0.19894 -0.03988 0.10282 -0.02238 AFIX 137 H34G 2 1.045813 1.091927 -0.177555 21.00000 -1.50000 H34H 2 1.037590 1.168991 -0.215474 21.00000 -1.50000 H34I 2 0.965581 1.120201 -0.230765 21.00000 -1.50000 AFIX 0 PART 2 C31D 1 0.937327 1.167338 -0.073630 -21.00000 0.12860 0.12568 = 0.12843 -0.00543 0.07097 -0.00326 AFIX 13 H31D 2 0.963918 1.212926 -0.067652 -21.00000 -1.20000 AFIX 0 C32D 1 1.005856 1.112067 -0.074291 -21.00000 0.14861 0.15062 = 0.14993 -0.00880 0.07130 -0.00003 AFIX 33 H32J 2 1.040934 1.109496 -0.017191 -21.00000 -1.50000 H32K 2 0.984707 1.065981 -0.091363 -21.00000 -1.50000 H32L 2 1.032233 1.128214 -0.114708 -21.00000 -1.50000 AFIX 0 C33D 1 0.879873 1.175695 -0.157894 -21.00000 0.17370 0.20302 = 0.18843 0.01174 0.04935 0.00028 AFIX 23 H33G 2 0.861352 1.224102 -0.163571 -21.00000 -1.20000 H33H 2 0.903493 1.166976 -0.204010 -21.00000 -1.20000 AFIX 0 C34D 1 0.815649 1.127624 -0.167917 -21.00000 0.20377 0.23624 = 0.19894 -0.03988 0.10282 -0.02238 AFIX 33 H34J 2 0.779631 1.134896 -0.223723 -21.00000 -1.50000 H34K 2 0.833554 1.079580 -0.163537 -21.00000 -1.50000 H34L 2 0.791416 1.136701 -0.123101 -21.00000 -1.50000 PART 0 AFIX 0 HKLF 4 1 0 0 1 0 -1 0 1 0 0 REM x13371 in P2(1)/c REM R1 = 0.0866 for 6868 Fo > 4sig(Fo) and 0.1265 for all 9853 data REM 717 parameters refined using 498 restraints END WGHT 0.1604 6.2977 REM Highest difference peak 0.925, deepest hole -0.488, 1-sigma level 0.092 Q1 1 1.0325 1.2338 0.1552 11.00000 0.05 0.71 Q2 1 0.7671 1.0058 0.6470 11.00000 0.05 0.64 Q3 1 0.9017 1.1890 0.0539 11.00000 0.05 0.55 Q4 1 1.0568 1.1714 0.2494 11.00000 0.05 0.55 Q5 1 1.0672 1.0843 -0.1004 11.00000 0.05 0.54 Q6 1 0.8032 0.9653 0.6280 11.00000 0.05 0.48 Q7 1 0.8206 0.8469 0.5449 11.00000 0.05 0.47 Q8 1 1.0013 1.1173 0.0063 11.00000 0.05 0.47 Q9 1 0.8879 1.2231 -0.0525 11.00000 0.05 0.46 Q10 1 0.8611 1.1975 -0.2346 11.00000 0.05 0.46 ; _shelx_res_checksum 95621 _shelx_hkl_file ; -1 0 0 -2.9375 0.2535 1 1 0 0 -2.7331 0.2953 1 1 0 0 -2.8673 0.2508 2 1 0 0 -2.9481 0.2325 3 -1 0 0 -2.7924 0.2807 1 2 0 0 2215.51 109.25 4 2 0 0 2321.16 111.06 5 3 0 0 0.38304 0.76655 2 -3 0 0 0.65220 0.82423 1 -3 0 0 0.16923 0.73443 1 3 0 0 0.40695 0.88650 1 3 0 0 0.48710 0.63485 2 3 0 0 -0.1804 0.6668 3 3 0 0 0.49752 1.61554 5 3 0 0 0.32522 0.71022 3 3 0 0 0.14044 0.80589 1 3 0 0 -0.6279 1.3670 4 4 0 0 219.846 11.052 3 4 0 0 214.310 12.362 1 4 0 0 192.807 11.114 4 4 0 0 222.089 11.307 1 4 0 0 222.845 10.424 2 4 0 0 196.543 11.396 2 -4 0 0 219.792 11.703 1 4 0 0 213.657 11.597 3 -4 0 0 219.913 11.351 1 4 0 0 201.977 11.585 5 -5 0 0 -0.6410 0.6600 1 5 0 0 -0.0184 0.8099 1 -5 0 0 -0.7078 0.6539 1 5 0 0 -0.7791 0.8098 1 5 0 0 -1.2574 2.6614 5 5 0 0 -0.3372 1.6513 4 6 0 0 100.069 6.791 5 6 0 0 94.3021 5.8809 4 7 0 0 0.59236 2.16895 4 7 0 0 -1.7951 2.5609 5 8 0 0 123.553 7.904 5 9 0 0 -0.6958 2.8661 5 10 0 0 208.026 12.820 5 10 0 0 223.882 13.630 13 10 0 0 223.323 14.767 14 10 0 0 220.332 13.444 12 11 0 0 -1.6848 2.0689 16 11 0 0 2.52079 3.26101 5 11 0 0 -2.7342 1.6701 12 11 0 0 -2.3474 2.2062 13 11 0 0 -3.0137 3.2042 14 11 0 0 -4.3792 3.3110 15 11 0 0 -2.7754 2.0805 11 12 0 0 490.909 29.721 13 12 0 0 478.290 31.649 15 12 0 0 505.997 30.881 11 12 0 0 518.308 31.736 14 12 0 0 506.025 29.438 12 13 0 0 -2.3817 2.2036 11 13 0 0 -3.6847 2.4463 13 13 0 0 -3.1808 3.4301 15 13 0 0 -3.3562 2.9850 14 14 0 0 4.20362 3.10624 13 14 0 0 6.48407 2.18253 12 14 0 0 10.0173 3.2752 15 15 0 0 -3.3351 1.8936 12 15 0 0 -4.3488 2.7564 13 15 0 0 -2.8705 3.0817 15 16 0 0 111.489 7.632 13 16 0 0 108.919 9.070 15 17 0 0 2.44914 2.34205 15 0 -1 0 0.24804 0.43069 1 0 -1 0 0.30856 0.33541 3 0 -1 0 0.50851 0.58614 1 0 -1 0 0.36326 0.42635 2 0 1 0 0.69488 0.38169 3 0 1 0 0.08088 0.47634 1 0 1 0 0.41499 0.27766 2 0 1 0 0.61654 0.50826 1 1 -1 0 6.04663 0.67313 2 1 -1 0 7.05019 0.96742 1 -1 -1 0 6.96358 1.01022 1 1 -1 0 6.04476 0.85605 2 1 -1 0 6.80067 0.87185 5 1 -1 0 7.59111 0.89206 3 -1 -1 0 6.04366 0.67330 3 1 -1 0 6.19267 0.91726 3 -1 -1 0 6.16661 0.90633 1 1 -1 0 6.80640 0.88648 1 -1 1 0 7.22700 1.02233 1 1 1 0 5.50112 0.62478 3 -1 1 0 7.15962 1.06542 1 1 1 0 6.55228 0.89299 3 1 1 0 6.04828 0.63116 2 1 1 0 6.07530 0.89144 1 -1 1 0 7.15593 0.85974 3 1 1 0 6.87394 0.80183 2 1 1 0 7.25663 0.74848 4 1 1 0 6.51579 1.00372 1 2 -1 0 630.891 35.707 1 2 -1 0 646.403 32.119 2 2 -1 0 630.869 34.186 3 -2 -1 0 630.884 34.229 1 2 -1 0 671.230 32.806 3 2 -1 0 630.902 32.799 5 2 -1 0 709.640 34.701 1 2 -1 0 630.562 34.137 2 -2 -1 0 668.762 34.100 1 2 1 0 630.891 33.830 3 2 1 0 624.656 35.796 2 2 1 0 655.843 34.060 1 -2 1 0 698.707 34.716 1 2 1 0 630.859 33.626 3 2 1 0 630.894 35.699 1 2 1 0 629.963 31.987 5 2 1 0 630.654 32.914 4 2 1 0 629.903 32.132 2 -2 1 0 645.127 34.692 1 3 -1 0 96.3070 6.0126 1 3 -1 0 95.9797 5.5345 3 3 -1 0 87.4351 5.3117 4 3 -1 0 110.457 5.652 3 3 -1 0 94.1236 6.0650 5 -3 -1 0 100.765 6.0623 1 3 -1 0 106.634 5.4923 2 3 -1 0 117.924 6.023 1 3 -1 0 97.9189 5.5604 2 3 1 0 93.3885 5.7721 5 3 1 0 108.850 5.670 3 3 1 0 89.6417 5.6246 4 -3 1 0 95.8770 5.9576 1 3 1 0 100.504 5.6724 3 3 1 0 88.5721 5.6113 2 3 1 0 112.512 5.533 2 3 1 0 95.1210 6.1543 1 -3 1 0 117.049 6.029 1 3 1 0 119.824 6.070 1 4 -1 0 0.81552 1.53979 4 4 -1 0 0.32725 1.13595 1 4 -1 0 0.28940 1.17289 1 -4 -1 0 0.78069 1.23870 1 4 -1 0 0.73169 0.95320 3 -4 -1 0 0.50548 1.30312 1 4 -1 0 -1.7891 2.2439 5 4 -1 0 0.16113 0.99574 2 4 -1 0 0.59886 1.11494 2 4 1 0 0.85782 1.08511 2 4 1 0 -0.7123 1.2654 1 4 1 0 0.15392 1.13017 2 4 1 0 0.20069 1.82994 4 4 1 0 -1.2227 2.0337 5 4 1 0 0.17309 1.07848 3 4 1 0 -0.1260 1.1021 1 -4 1 0 0.43811 1.11947 1 -4 1 0 -0.3114 0.9612 1 4 1 0 0.52400 1.16885 3 5 -1 0 60.7189 4.0544 1 5 -1 0 68.2817 5.2560 5 5 -1 0 61.7270 4.1895 4 -5 -1 0 64.4935 4.2027 1 5 -1 0 73.4787 4.0423 1 5 -1 0 71.5470 3.7170 2 -5 -1 0 71.0804 4.1816 1 -5 1 0 74.2514 3.9483 1 5 1 0 66.8931 3.8932 3 -5 1 0 65.0462 3.9818 1 5 1 0 56.7515 4.2219 1 5 1 0 69.7487 4.2738 1 5 1 0 56.7107 3.9674 2 5 1 0 61.1210 4.6137 4 5 1 0 66.7640 4.9865 5 5 1 0 61.5793 3.9753 3 5 1 0 69.5645 3.9660 2 -6 -1 0 189.294 10.841 1 6 -1 0 196.368 10.967 5 6 -1 0 187.156 10.06 4 -6 -1 0 195.262 10.653 1 6 1 0 194.216 10.26 4 6 1 0 178.241 10.869 1 6 1 0 191.297 10.810 5 6 1 0 202.620 10.311 1 7 -1 0 11.5989 2.9058 5 7 -1 0 9.48941 2.09293 4 7 1 0 11.0647 2.7383 5 7 1 0 12.0856 2.2555 4 8 -1 0 95.2793 7.3673 5 8 1 0 93.8317 6.8408 5 8 1 0 99.7774 6.110 4 9 -1 0 152.513 9.995 5 9 1 0 153.007 9.446 5 10 -1 0 105.038 7.1369 12 10 -1 0 113.314 8.497 14 10 -1 0 103.397 7.6621 13 10 -1 0 109.811 8.193 5 10 1 0 113.710 8.464 14 10 1 0 97.6296 7.9617 5 10 1 0 111.681 7.930 13 10 1 0 102.639 7.4898 12 11 -1 0 44.4060 6.0653 13 11 -1 0 40.5753 4.8165 11 11 -1 0 35.5770 6.0216 15 11 -1 0 39.6916 4.8818 16 11 -1 0 44.8683 7.0203 14 11 -1 0 43.8986 4.7738 12 11 -1 0 46.5151 5.5093 5 11 1 0 40.1027 4.6906 10 11 1 0 51.8473 4.8216 13 11 1 0 41.9509 6.7491 14 11 1 0 43.0535 5.2048 5 11 1 0 50.3533 4.9300 12 11 1 0 39.0538 6.1992 15 11 1 0 50.6632 4.7799 11 12 -1 0 258.918 15.474 13 12 -1 0 254.305 17.008 14 12 -1 0 255.204 15.329 12 12 -1 0 253.129 15.820 11 12 -1 0 242.168 15.917 16 12 -1 0 219.048 14.852 5 12 -1 0 250.110 16.521 15 12 1 0 263.224 15.974 11 12 1 0 243.136 16.870 15 12 1 0 264.587 15.382 12 12 1 0 244.071 15.481 13 12 1 0 269.986 17.349 14 13 -1 0 5.44582 3.29752 13 13 -1 0 6.54125 3.90836 15 13 -1 0 6.04918 2.86102 16 13 -1 0 5.81546 2.58577 11 13 -1 0 8.89439 3.83138 14 13 -1 0 8.01166 1.94187 12 13 1 0 7.90052 2.91515 11 13 1 0 8.44198 3.81988 14 13 1 0 8.53214 3.40136 15 13 1 0 5.79591 2.36025 12 13 1 0 8.80659 2.57265 13 14 -1 0 42.8143 6.4937 13 14 -1 0 47.5466 6.7482 15 14 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446.837 24.805 1 -2 -1 -3 411.479 22.554 2 -2 1 -3 496.798 24.800 1 2 1 3 411.297 25.942 1 -2 1 -3 467.117 24.763 1 2 1 3 474.525 22.635 2 2 1 3 411.285 24.129 3 2 1 3 446.655 24.745 1 -2 1 -3 412.181 23.010 3 2 1 3 439.173 23.027 3 -2 1 -3 411.255 23.001 2 3 -1 3 529.692 26.020 2 3 -1 3 457.858 26.711 3 -3 -1 -3 515.112 28.628 1 3 -1 3 529.767 28.801 1 3 -1 3 494.397 26.775 3 3 -1 3 494.074 28.718 1 3 -1 3 513.183 25.435 5 -3 -1 -3 529.662 28.409 1 3 1 3 492.320 26.311 2 3 1 3 529.644 28.641 1 3 1 3 455.036 26.268 2 3 1 3 529.676 26.167 3 3 1 3 486.490 28.666 1 -3 1 -3 512.271 28.747 1 -4 -1 -3 170.623 9.9635 1 4 -1 3 159.312 10.202 1 4 -1 3 171.121 9.197 2 -4 -1 -3 154.998 9.8816 1 4 -1 3 143.804 9.035 3 4 -1 3 155.211 9.117 5 4 1 3 144.859 10.009 1 4 1 3 160.068 9.069 3 4 1 3 145.203 8.939 2 4 1 3 155.015 9.020 2 4 1 3 158.221 10.086 1 4 1 3 161.659 9.019 5 -4 1 -3 177.002 9.9124 1 -4 1 -3 142.444 9.9038 1 5 -1 3 7.70082 2.07748 2 -5 -1 -3 7.12946 2.20625 1 -5 -1 -3 8.90051 2.40693 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2.7281 13 13 2 -3 12.8467 2.6975 14 13 2 -3 18.5896 3.1781 11 13 2 -3 16.3091 2.2253 12 12 -2 -3 89.4665 6.4295 12 12 -2 -3 75.5016 6.8311 13 12 -2 -3 87.3324 7.4858 5 12 -2 -3 78.3419 7.4257 9 12 -2 -3 81.4447 7.4695 10 12 -2 -3 87.3120 6.9609 16 12 -2 -3 90.1974 7.4836 14 12 -2 -3 79.0731 6.8175 11 12 -2 -3 89.6313 7.7913 15 12 2 -3 90.1757 6.8160 4 12 2 -3 88.8077 6.5072 9 12 2 -3 86.9282 7.5219 10 12 2 -3 88.4074 7.3392 13 12 2 -3 85.4348 6.6326 12 12 2 -3 89.2506 7.0153 11 12 2 -3 78.9426 7.6351 14 11 -2 -3 338.278 20.399 16 11 -2 -3 351.285 21.998 14 11 -2 -3 346.738 21.539 15 11 -2 -3 338.782 20.597 9 11 -2 -3 324.325 20.819 11 11 -2 -3 339.259 20.140 12 11 -2 -3 308.566 20.240 13 11 -2 -3 336.489 18.817 5 11 -2 -3 321.352 22.682 10 11 2 -3 320.559 21.917 14 11 2 -3 351.360 20.036 13 11 2 -3 346.996 22.852 10 11 2 -3 355.014 18.183 4 11 2 -3 317.702 20.465 9 11 2 -3 336.744 20.089 12 11 2 -3 351.304 20.983 11 10 -2 -3 424.232 22.435 5 10 -2 -3 423.487 22.936 4 10 2 -3 448.616 21.494 4 9 -2 -3 23.8066 3.6384 5 9 -2 -3 23.2075 2.7854 4 9 2 -3 21.4366 3.0575 5 9 2 -3 21.7643 3.5750 4 8 -2 -3 29.9648 3.7432 4 8 -2 -3 33.9904 4.3137 5 8 2 -3 32.9769 4.3728 4 8 2 -3 27.9590 3.0622 5 7 -2 -3 149.602 8.379 4 7 -2 -3 152.980 9.435 5 7 2 -3 160.486 8.886 4 7 2 -3 143.977 8.416 5 6 -2 -3 355.584 18.480 4 -6 -2 3 353.126 21.782 1 -6 -2 3 371.011 20.821 1 6 -2 -3 361.602 19.115 5 6 2 -3 415.410 19.197 2 6 2 -3 414.115 20.851 1 6 2 -3 354.455 20.902 1 6 2 -3 379.575 18.876 4 6 2 -3 380.289 19.128 2 6 2 -3 367.556 19.539 3 6 2 -3 408.440 19.576 3 6 2 -3 353.971 19.398 5 5 -2 -3 241.809 11.656 2 5 -2 -3 236.472 11.884 3 5 -2 -3 222.939 11.891 3 5 -2 -3 212.808 12.018 5 -5 -2 3 214.276 12.925 1 5 -2 -3 199.564 12.642 1 5 -2 -3 211.044 11.420 4 5 -2 -3 204.585 11.601 2 5 -2 -3 239.631 12.689 1 -5 -2 3 244.765 12.339 1 -5 2 3 213.672 12.798 1 5 2 -3 210.530 11.951 3 5 2 -3 211.467 11.564 4 5 2 -3 234.238 11.766 2 5 2 -3 201.616 11.387 5 -5 2 3 238.735 12.717 1 5 2 -3 213.004 11.684 2 5 2 -3 244.763 12.586 1 5 2 -3 244.755 11.963 3 5 2 -3 197.551 12.767 1 4 -2 -3 813.886 43.645 3 4 -2 -3 768.252 42.751 2 4 -2 -3 795.499 40.577 4 4 -2 -3 799.110 46.312 1 -4 -2 3 799.272 46.232 1 4 -2 -3 822.033 41.435 5 -4 -2 3 912.160 44.341 1 -4 2 3 819.035 46.424 1 4 2 -3 758.237 43.448 3 4 2 -3 797.782 42.571 2 4 2 -3 905.173 44.377 1 -4 2 3 891.275 43.143 1 4 2 -3 773.248 46.125 1 4 2 -3 816.678 40.574 4 4 2 -3 860.145 42.628 2 4 2 -3 895.378 42.525 3 3 -2 -3 833.595 44.042 3 -3 -2 3 974.920 48.687 1 3 -2 -3 757.914 43.145 2 3 -2 -3 945.297 46.856 1 3 -2 -3 845.425 41.673 5 3 -2 -3 832.778 40.871 4 3 -2 -3 864.513 43.178 2 -3 -2 3 851.604 48.684 1 3 -2 -3 835.660 46.771 1 3 -2 -3 816.075 44.009 3 3 2 -3 917.175 45.769 3 -3 2 3 944.738 46.807 1 3 2 -3 788.501 45.777 3 3 2 -3 848.972 48.643 1 3 2 -3 875.430 44.899 2 3 2 -3 870.587 44.872 2 -3 2 3 833.830 46.849 1 3 2 -3 925.863 48.679 1 3 2 -3 814.951 42.574 4 -2 -2 3 1999.89 108.26 1 2 -2 -3 1999.96 102.08 3 -2 -2 3 1919.10 107.73 3 2 -2 -3 2148.08 106.73 1 -2 -2 3 2100.72 107.99 1 2 -2 -3 1795.22 105.43 2 2 -2 -3 1938.76 113.93 1 2 -2 -3 2017.89 99.240 2 -2 2 3 1847.45 107.54 3 2 2 -3 1999.79 102.60 3 2 2 -3 1917.76 100.9 4 2 2 -3 2021.19 100.99 2 2 2 -3 2059.72 108.29 1 -2 2 3 1997.00 109.17 1 -2 2 3 2154.46 106.32 1 -1 -2 3 4489.56 243.03 1 -1 -2 3 4086.04 229.54 3 1 -2 -3 4811.77 242.80 1 1 -2 -3 4173.50 229.13 3 1 -2 -3 4260.86 224.57 2 -1 -2 3 4717.78 243.10 1 1 -2 -3 4696.95 242.70 1 -1 -2 3 4154.31 225.05 2 -1 2 3 4783.89 242.16 1 -1 2 3 4102.36 228.78 3 -1 2 3 4463.48 242.30 1 1 2 -3 4173.61 229.84 3 1 2 -3 4278.41 225.41 2 1 2 -3 4439.86 242.81 1 1 2 -3 4271.59 213.08 4 -1 2 3 4356.53 224.27 2 1 2 -3 4692.12 243.44 1 0 -2 -3 130.435 7.944 1 0 -2 3 129.388 7.716 2 0 -2 -3 135.164 8.280 1 0 -2 -3 117.027 7.170 3 0 -2 3 140.204 8.388 1 0 -2 3 119.072 7.495 3 0 -2 -3 120.078 6.991 2 0 -2 3 134.380 8.740 1 0 2 3 132.711 8.060 1 0 2 3 127.849 8.162 1 0 2 -3 118.401 7.292 2 0 2 3 121.375 7.134 3 0 2 -3 137.021 8.250 1 0 2 -3 129.057 8.389 1 0 2 3 123.353 7.049 2 0 2 -3 116.529 7.434 3 -1 -2 -3 2801.64 143.02 1 1 -2 3 2739.61 142.03 1 1 -2 3 2676.79 132.40 2 -1 -2 -3 2381.98 136.58 3 -1 -2 -3 2701.57 142.10 1 1 -2 3 2735.67 141.98 1 1 -2 3 2625.20 135.18 3 -1 -2 -3 2468.47 132.49 2 -1 2 -3 2590.10 142.77 1 1 2 3 2633.24 141.91 1 1 2 3 2734.86 142.15 1 1 2 3 2483.27 133.84 3 -1 2 -3 2381.96 136.37 2 -1 2 -3 2658.01 143.15 1 1 2 3 2580.32 132.20 2 -1 2 -3 2381.99 140.03 3 2 -2 3 3317.69 170.39 3 2 -2 3 3396.86 178.85 1 2 -2 3 3076.96 168.74 3 2 -2 3 3417.89 166.54 2 -2 -2 -3 3413.44 180.99 1 2 -2 3 3243.43 160.32 5 -2 -2 -3 3038.18 180.60 3 2 -2 3 3328.25 179.53 1 2 2 3 3268.98 179.19 1 2 2 3 3623.35 167.62 2 -2 2 -3 3025.92 181.95 3 -2 2 -3 3350.24 180.21 1 2 2 3 3558.82 179.66 1 -2 2 -3 3309.50 179.53 1 2 2 3 3351.05 170.92 3 -2 2 -3 3037.78 172.70 2 3 -2 3 -0.6810 1.5266 3 3 -2 3 -0.8125 2.0142 2 3 -2 3 -1.8961 2.2990 1 3 -2 3 -3.9027 2.6140 1 -3 -2 -3 -0.8288 1.8484 1 3 -2 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5 2 3 203.635 10.856 3 5 2 3 171.191 10.879 3 5 2 3 214.100 10.675 5 -5 2 -3 175.928 11.940 1 5 2 3 176.866 12.064 1 5 2 3 202.368 10.643 2 6 -2 3 742.298 35.677 3 6 -2 3 676.785 34.983 2 6 -2 3 625.517 35.469 3 6 -2 3 699.598 34.961 2 6 -2 3 661.911 34.121 5 6 -2 3 684.979 38.397 1 6 2 3 588.743 36.409 3 6 2 3 684.232 33.848 5 6 2 3 715.129 34.853 2 6 2 3 680.502 35.410 3 7 -2 3 271.079 14.345 3 7 -2 3 252.177 14.081 2 7 -2 3 250.440 14.489 5 7 2 3 281.002 14.148 2 7 2 3 247.206 14.002 5 7 2 3 243.284 14.107 3 8 -2 3 5.57645 1.96281 2 8 -2 3 7.38287 1.97287 3 8 -2 3 7.48304 3.86453 5 8 2 3 8.55254 3.64804 5 8 2 3 5.09605 1.93333 3 8 2 3 6.42513 2.42928 2 9 -2 3 179.443 12.024 8 9 -2 3 186.229 11.460 5 9 -2 3 172.888 12.014 15 9 -2 3 172.814 11.006 13 9 -2 3 165.998 12.229 14 9 -2 3 178.890 10.948 12 9 2 3 170.847 10.961 5 9 2 3 198.254 9.682 2 9 2 3 178.815 11.188 11 9 2 3 168.504 10.960 13 9 2 3 174.762 10.869 12 9 2 3 169.229 9.529 3 9 2 3 162.045 13.003 14 9 2 3 164.637 12.160 7 9 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49.9234 7.6210 15 13 -2 3 44.5106 5.3066 13 13 2 3 37.9272 4.9333 13 13 2 3 38.3859 6.6128 15 13 2 3 50.2620 4.8453 12 13 2 3 34.3128 4.8585 14 14 -2 3 -1.1624 2.2586 13 14 -2 3 -3.2667 3.2854 15 14 -2 3 -2.0059 3.8763 14 14 2 3 -2.2713 3.0867 15 14 2 3 -1.7402 1.9831 12 15 -2 3 22.4646 4.4915 14 15 -2 3 23.7715 3.5054 13 15 -2 3 24.1829 4.2688 15 15 2 3 28.9195 4.1142 15 16 -2 3 8.96909 3.58435 14 16 -2 3 6.90004 2.30675 13 16 -2 3 14.4848 3.2710 15 17 -2 3 2.47552 2.96281 15 17 -2 3 5.14940 3.00215 14 18 -3 -3 3.50167 2.03117 15 18 3 -3 1.51147 1.67607 12 17 -3 -3 10.3638 2.6534 14 17 -3 -3 2.87575 2.76069 16 17 3 -3 8.41919 2.14885 12 17 3 -3 6.17775 2.64300 14 16 -3 -3 -0.6790 2.0735 13 16 -3 -3 2.33598 2.51550 16 16 -3 -3 3.23511 2.93983 14 16 3 -3 1.53126 2.90954 14 16 3 -3 0.22601 2.13222 12 16 3 -3 0.58627 2.49033 11 15 -3 -3 32.2069 4.9081 16 15 -3 -3 33.7126 4.9942 9 15 -3 -3 33.7812 5.7783 14 15 -3 -3 23.4688 4.5314 15 15 -3 -3 29.9341 4.6209 12 15 -3 -3 30.8819 5.0113 13 15 3 -3 39.3224 5.4348 13 15 3 -3 38.2628 4.2253 12 15 3 -3 33.7121 5.0098 10 15 3 -3 25.8033 3.8120 14 14 -3 -3 55.5853 6.7689 9 14 -3 -3 62.8083 6.3431 16 14 -3 -3 68.9379 7.0993 14 14 -3 -3 60.6543 6.9204 13 14 -3 -3 68.8207 6.6362 15 14 -3 -3 63.9182 5.1609 12 14 3 -3 46.9703 6.8314 14 14 3 -3 49.0304 6.2892 13 14 3 -3 60.9760 6.3462 10 14 3 -3 73.6333 5.7410 11 14 3 -3 70.3807 5.5499 12 13 -3 -3 31.3712 4.9725 13 13 -3 -3 34.8328 5.4898 9 13 -3 -3 23.9969 5.5747 5 13 -3 -3 28.5389 3.9951 14 13 -3 -3 41.5896 5.0138 16 13 -3 -3 46.9722 6.5475 15 13 -3 -3 35.8565 4.1582 12 13 3 -3 33.3980 4.9424 13 13 3 -3 34.7411 5.2316 10 13 3 -3 37.1471 4.7285 12 13 3 -3 32.6526 4.8775 9 13 3 -3 35.9522 4.8918 11 12 -3 -3 30.9375 5.0634 10 12 -3 -3 26.0300 3.3803 13 12 -3 -3 37.5910 5.0890 16 12 -3 -3 45.7774 5.8848 15 12 -3 -3 34.2240 4.1950 12 12 -3 -3 40.0747 6.4905 14 12 -3 -3 33.8605 4.7699 9 12 -3 -3 45.7785 5.5503 5 12 3 -3 33.4987 5.3914 10 12 3 -3 38.9617 5.4851 13 12 3 -3 40.9683 5.4377 4 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506.077 29.850 1 4 3 -3 574.635 29.894 1 -4 3 3 520.722 30.026 1 4 3 -3 528.896 26.146 4 4 3 -3 496.240 29.751 1 4 3 -3 478.019 27.902 3 4 3 -3 576.539 27.904 3 4 3 -3 505.721 27.319 2 -4 3 3 596.557 29.924 1 4 3 -3 516.311 27.390 2 3 -3 -3 4500.54 234.50 3 3 -3 -3 4685.22 229.90 2 3 -3 -3 4525.02 247.32 1 3 -3 -3 4343.28 246.06 2 3 -3 -3 4724.60 220.89 5 -3 -3 3 4418.94 255.36 1 -3 -3 3 5202.63 256.20 1 3 -3 -3 4437.15 234.04 3 3 -3 -3 4823.70 247.80 1 3 3 -3 4298.22 249.43 3 3 3 -3 5076.15 242.59 3 -3 3 3 4961.34 247.73 1 3 3 -3 4352.57 258.30 1 3 3 -3 4928.98 256.70 1 3 3 -3 4382.76 224.61 4 3 3 -3 4447.38 237.45 2 3 3 -3 4381.42 237.22 2 -3 3 3 4344.26 246.85 1 2 -3 -3 33.3595 3.4651 1 -2 -3 3 35.7356 4.4483 1 2 -3 -3 32.0540 3.2324 2 2 -3 -3 32.9509 3.2528 3 -2 -3 3 31.6362 3.2440 3 2 -3 -3 29.1303 2.7072 3 -2 -3 3 34.3822 3.5145 1 -2 -3 3 31.4567 3.6809 2 2 3 -3 37.5208 3.4599 2 2 3 -3 31.7176 3.2898 4 2 3 -3 36.1751 3.5927 1 2 3 -3 32.7256 3.5832 1 -2 3 3 26.4873 3.0748 3 2 3 -3 32.5217 3.1396 3 -2 3 3 31.8584 4.2156 1 2 3 -3 29.9554 3.4265 3 -2 3 3 33.4536 3.3625 1 -1 -3 3 9.38522 1.53758 3 -1 -3 3 9.52921 3.14767 1 -1 -3 3 7.93273 2.02318 2 1 -3 -3 11.4845 2.6766 1 1 -3 -3 9.27118 2.38327 1 1 -3 -3 9.27230 1.63127 3 -1 -3 3 9.98702 2.2593 1 1 -3 -3 8.82374 1.69164 2 1 3 -3 10.6943 2.3321 1 1 3 -3 12.0225 2.8617 1 -1 3 3 8.58782 2.65051 1 1 3 -3 9.27282 1.71236 2 1 3 -3 10.3350 1.4165 3 1 3 -3 10.8512 1.6126 4 -1 3 3 8.98818 1.53411 2 -1 3 3 8.13496 1.57876 3 -1 3 3 9.59161 2.4719 1 0 -3 -3 238.556 13.116 2 0 -3 3 253.703 14.963 1 0 -3 3 244.218 12.778 5 0 -3 3 239.269 13.703 3 0 -3 3 253.677 14.198 1 0 -3 -3 246.380 14.769 1 0 -3 -3 253.668 13.855 1 0 -3 -3 244.885 13.582 3 0 -3 3 243.716 13.736 2 0 3 3 242.022 13.023 2 0 3 3 238.587 13.503 3 0 3 -3 253.858 14.929 1 0 3 -3 238.694 13.654 3 0 3 -3 253.685 14.521 1 0 3 3 233.753 14.738 1 0 3 -3 251.992 12.578 4 0 3 -3 245.851 13.582 2 0 3 3 253.665 13.838 1 1 -3 3 4.78015 2.12169 1 1 -3 3 4.33830 2.59719 1 -1 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12.359 2 3 3 3 230.057 13.172 1 3 3 3 227.986 12.611 3 3 3 3 237.976 11.677 2 -3 3 -3 221.875 13.346 1 -3 3 -3 183.205 12.110 3 -3 3 -3 212.968 13.667 1 4 -3 3 155.831 10.574 1 4 -3 3 149.659 9.070 3 4 -3 3 149.980 8.881 2 -4 -3 -3 162.735 10.355 1 4 -3 3 171.417 10.254 1 4 -3 3 175.694 9.412 3 4 -3 3 164.950 9.161 5 4 -3 3 165.102 9.358 2 -4 3 -3 153.760 10.392 1 4 3 3 184.438 8.965 2 4 3 3 142.371 10.352 1 4 3 3 168.230 10.165 1 4 3 3 140.409 9.232 3 4 3 3 135.261 9.287 2 4 3 3 167.878 9.200 3 -4 3 -3 175.807 10.311 1 -5 -3 -3 207.353 12.425 1 5 -3 3 189.059 11.346 3 5 -3 3 180.629 11.189 2 -5 -3 -3 186.991 12.534 1 5 -3 3 215.190 11.640 2 5 -3 3 194.842 12.778 1 5 -3 3 195.714 12.500 1 5 -3 3 212.003 11.360 5 5 -3 3 221.293 11.651 3 -5 3 -3 187.486 12.556 1 5 3 3 202.910 12.448 1 5 3 3 211.160 11.489 3 5 3 3 173.010 12.630 1 5 3 3 216.362 11.260 5 -5 3 -3 210.832 12.532 1 5 3 3 227.991 11.186 2 6 -3 3 489.539 24.132 3 6 -3 3 444.600 23.681 2 6 -3 3 442.243 23.368 5 6 3 3 445.723 22.929 5 6 3 3 435.085 23.890 3 6 3 3 431.446 23.459 2 7 -3 3 507.407 27.292 2 7 -3 3 515.045 27.122 5 7 -3 3 576.227 27.952 3 7 3 3 491.167 27.620 3 7 3 3 537.623 27.254 2 7 3 3 503.751 26.581 5 8 -3 3 104.659 8.332 5 8 -3 3 116.177 6.805 3 8 -3 3 101.902 6.704 2 8 3 3 98.8489 7.8995 5 8 3 3 100.380 6.611 3 8 3 3 111.004 7.000 2 9 -3 3 123.605 9.850 14 9 -3 3 128.239 8.043 12 9 -3 3 113.075 8.346 16 9 -3 3 120.068 8.836 8 9 -3 3 122.603 9.135 15 9 -3 3 119.133 8.705 13 9 -3 3 126.362 9.399 5 9 3 3 123.163 7.943 12 9 3 3 124.081 8.207 11 9 3 3 133.749 7.460 2 9 3 3 123.782 8.625 8 9 3 3 112.772 10.12 14 9 3 3 113.659 9.157 7 9 3 3 122.140 8.066 13 9 3 3 114.753 8.073 5 9 3 3 116.723 7.082 3 10 -3 3 61.4712 7.7635 14 10 -3 3 64.1823 6.5079 13 10 -3 3 67.3230 7.6299 5 10 -3 3 63.0417 5.6265 8 10 -3 3 62.8584 6.1678 16 10 -3 3 66.3045 6.9313 15 10 3 3 54.1527 6.1774 15 10 3 3 59.5667 7.7780 14 10 3 3 65.1525 4.8624 12 10 3 3 68.0059 5.6608 8 10 3 3 58.0779 5.8479 13 11 -3 3 143.168 9.9785 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1.11372 2.11297 11 5 -4 -21 0.04960 1.71876 7 5 4 -21 -0.0457 0.6133 11 5 4 -21 0.31008 1.88493 7 4 -4 -21 5.47077 1.2028 11 4 4 -21 5.47232 1.1510 7 3 -4 -21 0.53927 1.85343 7 3 -4 -21 1.49204 1.97834 11 3 4 -21 1.26670 1.81429 7 -2 -4 21 -0.7131 0.6577 6 2 4 -21 -0.6982 0.4082 6 1 -4 -21 31.1488 3.3659 6 1 4 -21 31.1153 2.8868 6 0 -4 21 2.86608 2.19944 6 0 -4 -21 1.38212 1.59472 6 0 4 21 4.07089 2.08032 6 0 4 -21 5.17255 1.76563 6 10 -5 -21 22.4825 2.2421 8 10 5 -21 22.5148 1.9083 8 9 -5 -21 35.3995 3.0505 8 9 -5 -21 35.4050 2.9996 11 9 5 -21 35.4013 2.6236 8 8 -5 -21 24.0088 2.2234 7 8 -5 -21 23.9337 2.1896 11 8 -5 -21 24.0255 2.3759 8 8 5 -21 24.0411 2.0305 7 8 5 -21 24.0229 2.5328 8 7 -5 -21 1.43250 1.31640 11 7 -5 -21 -0.4997 0.6067 7 7 -5 -21 -0.4258 0.7652 8 7 5 -21 -0.2872 0.5399 7 6 -5 -21 1.49781 0.83758 11 6 -5 -21 1.44903 1.29014 7 6 5 -21 1.47779 1.05556 7 5 -5 -21 2.53617 1.69075 7 5 -5 -21 4.35845 1.95452 11 5 5 -21 3.07220 1.94493 7 4 -5 -21 8.65546 1.88994 7 4 5 -21 11.0527 2.0140 7 3 -5 -21 0.97313 1.46799 7 -3 -5 21 0.87403 2.92751 6 3 -5 -21 1.09262 1.88659 11 3 5 -21 -0.2691 0.2615 6 3 5 -21 1.25152 1.31353 7 2 -5 -21 -0.2630 0.5493 11 2 -5 -21 -0.5163 0.4023 6 -2 -5 21 -0.2306 0.5565 6 -2 5 21 -0.4036 0.6825 6 2 5 -21 -0.1983 0.3231 6 1 -5 -21 14.7163 1.9304 6 -1 -5 21 14.7827 1.8646 6 -1 5 21 14.7662 3.4498 6 9 -6 -21 -0.3282 0.7189 8 8 -6 -21 2.97240 1.50113 8 8 -6 -21 0.20236 1.80683 11 8 6 -21 5.33538 1.19735 7 8 6 -21 4.51531 1.53885 8 7 -6 -21 -0.5112 0.5691 7 7 -6 -21 -0.2500 0.7225 8 7 -6 -21 -0.2023 0.8458 11 7 6 -21 -0.6313 0.4356 7 6 -6 -21 0.65794 0.57823 7 6 -6 -21 0.45837 1.65294 11 5 -6 -21 -0.0068 0.6746 11 5 -6 -21 0.25840 0.57767 7 5 6 -21 0.53077 0.48466 7 4 -6 -21 -0.3080 0.7243 11 4 -6 -21 -0.9183 0.5564 7 4 6 -21 0.20550 0.39538 7 3 -6 -21 1.62634 1.85814 11 3 -6 -21 1.99662 1.39930 7 2 -6 -21 0.99719 1.77115 11 -2 -6 21 -0.1577 0.4548 6 2 6 -21 0.97136 0.30850 6 7 -7 -21 0.52617 0.44702 7 7 7 -21 0.08329 1.21857 7 6 -7 -21 27.0141 2.6993 11 6 -7 -21 26.9504 2.4105 7 6 7 -21 27.0057 2.5443 7 5 -7 -21 21.0972 2.6142 7 5 7 -21 19.7969 2.6068 7 4 -7 -21 3.16820 1.47870 7 4 -7 -21 6.32504 1.76926 11 4 7 -21 6.01553 1.83433 7 3 -7 -21 8.18099 1.86416 11 6 -8 -21 32.6637 2.9403 7 6 8 -21 32.6069 2.7159 7 5 -8 -21 17.0689 2.0045 7 8 0 -22 3.64408 1.62223 11 7 0 -22 0.01506 0.50961 11 6 0 -22 7.08550 2.11015 11 5 0 -22 0.14946 0.43634 11 4 0 -22 35.3298 2.9161 11 8 -1 -22 0.16113 1.06546 11 8 1 -22 -0.2143 0.5855 11 7 -1 -22 -0.1805 0.6026 11 7 1 -22 0.32761 0.50363 11 6 -1 -22 2.09594 1.06526 11 6 1 -22 2.13456 1.34477 11 5 -1 -22 0.38079 2.06281 11 5 1 -22 0.93459 0.43632 11 4 -1 -22 3.90737 1.86289 11 4 1 -22 3.90973 1.19426 11 8 -2 -22 2.39490 1.11076 11 7 -2 -22 5.00659 1.34874 11 6 -2 -22 8.56601 1.88115 11 5 -2 -22 14.5381 2.3936 11 4 -2 -22 0.19530 0.39047 11 3 -2 -22 -0.3701 0.3292 11 7 -3 -22 2.65796 1.60929 11 7 -3 -22 2.09815 0.99853 7 6 -3 -22 1.14714 0.52056 11 6 3 -22 0.83210 0.31716 7 5 -3 -22 27.7355 2.4112 11 4 -3 -22 7.31364 2.06384 11 6 -4 -22 0.11836 1.24424 7 6 -4 -22 2.88265 1.67045 11 6 4 -22 0.34666 1.25539 7 5 -4 -22 4.02989 1.37307 7 5 4 -22 4.03127 1.00891 7 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 53579 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Si1A Si 0.80257(8) 0.92568(9) 0.46621(9) 0.0633(4) Uani 1 1 d . . . . . C1A C 0.5614(2) 0.98367(19) 0.3761(2) 0.0330(8) Uani 1 1 d . . . . . C2A C 0.5341(2) 1.03732(19) 0.4186(2) 0.0334(8) Uani 1 1 d . . . . . C3A C 0.5801(2) 1.0715(2) 0.4906(2) 0.0333(8) Uani 1 1 d . . . . . H3A H 0.6310 1.0584 0.5128 0.040 Uiso 1 1 calc R U . . . C4A C 0.5512(2) 1.1232(2) 0.5279(2) 0.0361(9) Uani 1 1 d . . . . . S5A S 0.59838(7) 1.17172(5) 0.61694(6) 0.0430(3) Uani 1 1 d . . . . . C6A C 0.5177(3) 1.2188(2) 0.6123(3) 0.0449(10) Uani 1 1 d . . . . . H6A H 0.5165 1.2546 0.6517 0.054 Uiso 1 1 calc R U . . . C7A C 0.4569(3) 1.20081(19) 0.5489(2) 0.0369(9) Uani 1 1 d . . . . . H7A H 0.4090 1.2215 0.5390 0.044 Uiso 1 1 calc R U . . . C8A C 0.4751(2) 1.1445(2) 0.4969(2) 0.0356(9) Uani 1 1 d . . . . . C9A C 0.4289(2) 1.1122(2) 0.4270(2) 0.0334(8) Uani 1 1 d . . . . . H9A H 0.3782 1.1262 0.4062 0.040 Uiso 1 1 calc R U . . . C10A C 0.4568(2) 1.0576(2) 0.3854(2) 0.0334(8) Uani 1 1 d . . . . . C11A C 0.4121(2) 1.0246(2) 0.3139(2) 0.0339(8) Uani 1 1 d . . . . . H11A H 0.3613 1.0381 0.2930 0.041 Uiso 1 1 calc R U . . . C12A C 0.4387(2) 0.97206(19) 0.2710(2) 0.0321(8) Uani 1 1 d . . . . . C13A C 0.3923(2) 0.9395(2) 0.1972(2) 0.0352(8) Uani 1 1 d . . . . . H13A H 0.3414 0.9529 0.1759 0.042 Uiso 1 1 calc R U . . . C14A C 0.4206(2) 0.8888(2) 0.1564(2) 0.0369(9) Uani 1 1 d . . . . . C15A C 0.3837(3) 0.8499(2) 0.0805(2) 0.044(1) Uani 1 1 d . . . . . H15A H 0.3324 0.8550 0.0506 0.053 Uiso 1 1 calc R U . . . C16A C 0.4297(3) 0.8060(2) 0.0571(3) 0.0471(11) Uani 1 1 d . . . . . H16A H 0.4141 0.7774 0.0080 0.057 Uiso 1 1 calc R U . . . S17A S 0.52045(7) 0.80552(5) 0.12374(6) 0.0430(3) Uani 1 1 d . . . . . C18A C 0.4966(2) 0.8690(2) 0.1883(2) 0.0351(9) Uani 1 1 d . . . . . C19A C 0.5436(2) 0.89820(19) 0.2596(2) 0.0343(8) Uani 1 1 d . . . . . H19A H 0.5941 0.8835 0.2797 0.041 Uiso 1 1 calc R U . . . C20A C 0.5154(2) 0.95110(19) 0.3033(2) 0.0324(8) Uani 1 1 d . . . . . C21A C 0.6376(2) 0.9636(2) 0.4074(3) 0.0398(9) Uani 1 1 d . . . . . C22A C 0.7034(3) 0.9475(2) 0.4332(3) 0.0483(10) Uani 1 1 d . . . . . C23A C 0.8349(10) 0.9319(7) 0.3668(8) 0.067(3) Uani 0.5 1 d D U P A 1 H23A H 0.8870 0.9136 0.3787 0.081 Uiso 0.5 1 calc R U P A 1 C24A C 0.8339(11) 1.0090(8) 0.3471(12) 0.087(3) Uani 0.5 1 d D U P A 1 H24A H 0.8672 1.0336 0.3955 0.130 Uiso 0.5 1 calc R U P A 1 H24B H 0.8510 1.0163 0.2964 0.130 Uiso 0.5 1 calc R U P A 1 H24C H 0.7829 1.0269 0.3366 0.130 Uiso 0.5 1 calc R U P A 1 C25A C 0.7825(11) 0.892(1) 0.2908(11) 0.096(3) Uani 0.5 1 d D U P A 1 H25A H 0.7302 0.9085 0.2764 0.116 Uiso 0.5 1 calc R U P A 1 H25B H 0.7844 0.8411 0.2994 0.116 Uiso 0.5 1 calc R U P A 1 C26A C 0.8271(11) 0.9178(10) 0.2197(10) 0.120(6) Uani 0.5 1 d D U P A 1 H26A H 0.8024 0.8978 0.1639 0.180 Uiso 0.5 1 calc R U P A 1 H26B H 0.8258 0.9686 0.2156 0.180 Uiso 0.5 1 calc R U P A 1 H26C H 0.8792 0.9021 0.2383 0.180 Uiso 0.5 1 calc R U P A 1 C23C C 0.8406(10) 0.9580(7) 0.3752(8) 0.067(3) Uani 0.5 1 d D U P A 2 H23C H 0.8935 0.9418 0.3880 0.081 Uiso 0.5 1 calc R U P A 2 C24C C 0.7971(11) 0.9234(9) 0.2924(11) 0.096(3) Uani 0.5 1 d D U P A 2 H24D H 0.7972 0.8730 0.3004 0.144 Uiso 0.5 1 calc R U P A 2 H24E H 0.7455 0.9405 0.2759 0.144 Uiso 0.5 1 calc R U P A 2 H24F H 0.8207 0.9346 0.2476 0.144 Uiso 0.5 1 calc R U P A 2 C25C C 0.8411(11) 1.0378(8) 0.3640(11) 0.087(3) Uani 0.5 1 d D U P A 2 H25C H 0.8775 1.0616 0.4116 0.104 Uiso 0.5 1 calc R U P A 2 H25D H 0.7910 1.0590 0.3536 0.104 Uiso 0.5 1 calc R U P A 2 C26C C 0.8702(12) 1.0326(13) 0.2748(13) 0.149(7) Uani 0.5 1 d D U P A 2 H26D H 0.8752 1.0795 0.2538 0.224 Uiso 0.5 1 calc R U P A 2 H26E H 0.9186 1.0090 0.2882 0.224 Uiso 0.5 1 calc R U P A 2 H26F H 0.8335 1.0064 0.2311 0.224 Uiso 0.5 1 calc R U P A 2 C27A C 0.8100(5) 0.8303(5) 0.4925(6) 0.103(2) Uani 0.638(7) 1 d D U P A 1 H27A H 0.7673 0.8154 0.4435 0.123 Uiso 0.638(7) 1 calc R U P A 1 C28A C 0.8687(9) 0.7875(8) 0.4683(12) 0.127(4) Uani 0.638(7) 1 d D U P A 1 H28A H 0.9183 0.8003 0.5046 0.190 Uiso 0.638(7) 1 calc R U P A 1 H28B H 0.8662 0.7962 0.4086 0.190 Uiso 0.638(7) 1 calc R U P A 1 H28C H 0.8597 0.7381 0.4759 0.190 Uiso 0.638(7) 1 calc R U P A 1 C29A C 0.7779(7) 0.8060(5) 0.5593(7) 0.075(2) Uani 0.638(7) 1 d D U P A 1 H29A H 0.7291 0.8294 0.5506 0.090 Uiso 0.638(7) 1 calc R U P A 1 H29B H 0.8108 0.8227 0.6144 0.090 Uiso 0.638(7) 1 calc R U P A 1 C30A C 0.765(2) 0.7298(13) 0.569(4) 0.084(2) Uani 0.638(7) 1 d D U P A 1 H30A H 0.7165 0.7167 0.5311 0.127 Uiso 0.638(7) 1 calc R U P A 1 H30B H 0.7671 0.7197 0.6279 0.127 Uiso 0.638(7) 1 calc R U P A 1 H30C H 0.8046 0.7034 0.5533 0.127 Uiso 0.638(7) 1 calc R U P A 1 C27C C 0.8100(5) 0.8303(5) 0.4925(6) 0.103(2) Uani 0.362(7) 1 d D U P A 2 H27C H 0.7995 0.8102 0.4340 0.123 Uiso 0.362(7) 1 calc R U P A 2 C28C C 0.8918(8) 0.8109(14) 0.5281(18) 0.127(4) Uani 0.362(7) 1 d D U P A 2 H28D H 0.9221 0.8390 0.5005 0.190 Uiso 0.362(7) 1 calc R U P A 2 H28E H 0.9077 0.8194 0.5895 0.190 Uiso 0.362(7) 1 calc R U P A 2 H28F H 0.8985 0.7616 0.5171 0.190 Uiso 0.362(7) 1 calc R U P A 2 C29C C 0.7515(9) 0.7972(9) 0.5212(13) 0.075(2) Uani 0.362(7) 1 d D U P A 2 H29C H 0.7091 0.7882 0.4702 0.090 Uiso 0.362(7) 1 calc R U P A 2 H29D H 0.7339 0.8314 0.5563 0.090 Uiso 0.362(7) 1 calc R U P A 2 C30C C 0.767(4) 0.731(2) 0.571(7) 0.084(2) Uani 0.362(7) 1 d D U P A 2 H30D H 0.7221 0.7156 0.5853 0.127 Uiso 0.362(7) 1 calc R U P A 2 H30E H 0.7826 0.6950 0.5370 0.127 Uiso 0.362(7) 1 calc R U P A 2 H30F H 0.8075 0.7385 0.6236 0.127 Uiso 0.362(7) 1 calc R U P A 2 C31A C 0.8461(11) 0.9898(8) 0.5590(8) 0.084(3) Uani 0.638(7) 1 d D U P A 1 H31A H 0.8434 1.0384 0.5367 0.100 Uiso 0.638(7) 1 calc R U P A 1 C32A C 0.9257(8) 0.9685(9) 0.594(1) 0.121(4) Uani 0.638(7) 1 d D U P A 1 H32A H 0.9516 1.0016 0.6377 0.182 Uiso 0.638(7) 1 calc R U P A 1 H32B H 0.9499 0.9676 0.5480 0.182 Uiso 0.638(7) 1 calc R U P A 1 H32C H 0.9279 0.9221 0.6191 0.182 Uiso 0.638(7) 1 calc R U P A 1 C33A C 0.7927(8) 0.9827(8) 0.6303(8) 0.096(3) Uani 0.638(7) 1 d D U P A 1 H33A H 0.7392 0.9893 0.6000 0.115 Uiso 0.638(7) 1 calc R U P A 1 H33B H 0.7990 0.9358 0.6562 0.115 Uiso 0.638(7) 1 calc R U P A 1 C34A C 0.8163(15) 1.0342(14) 0.6955(14) 0.218(10) Uani 0.638(7) 1 d D U P A 1 H34A H 0.8079 1.0171 0.7484 0.326 Uiso 0.638(7) 1 calc R U P A 1 H34B H 0.7874 1.0768 0.6778 0.326 Uiso 0.638(7) 1 calc R U P A 1 H34C H 0.8696 1.0440 0.7048 0.326 Uiso 0.638(7) 1 calc R U P A 1 C31C C 0.8507(17) 0.9688(16) 0.5567(13) 0.084(3) Uani 0.362(7) 1 d D U P A 2 H31C H 0.8284 1.0146 0.5344 0.100 Uiso 0.362(7) 1 calc R U P A 2 C32C C 0.8320(13) 0.9776(15) 0.6392(13) 0.096(3) Uani 0.362(7) 1 d D U P A 2 H32D H 0.8710 1.0051 0.6784 0.144 Uiso 0.362(7) 1 calc R U P A 2 H32E H 0.7838 1.0015 0.6290 0.144 Uiso 0.362(7) 1 calc R U P A 2 H32F H 0.8288 0.9319 0.6643 0.144 Uiso 0.362(7) 1 calc R U P A 2 C33C C 0.9417(12) 0.9975(17) 0.5679(16) 0.121(4) Uani 0.362(7) 1 d D U P A 2 H33C H 0.9745 0.9578 0.5650 0.145 Uiso 0.362(7) 1 calc R U P A 2 H33D H 0.9424 1.0304 0.5217 0.145 Uiso 0.362(7) 1 calc R U P A 2 C34C C 0.9674(17) 1.032(2) 0.650(2) 0.169(11) Uani 0.362(7) 1 d D U P A 2 H34D H 1.0185 1.0483 0.6580 0.254 Uiso 0.362(7) 1 calc R U P A 2 H34E H 0.9346 1.0708 0.6518 0.254 Uiso 0.362(7) 1 calc R U P A 2 H34F H 0.9665 0.9985 0.6949 0.254 Uiso 0.362(7) 1 calc R U P A 2 Si1B Si 0.91721(11) 1.16155(11) 0.01921(17) 0.0919(7) Uani 1 1 d . . . . . C1B C 0.7310(2) 1.0221(2) 0.0378(3) 0.0416(9) Uani 1 1 d . . . . . C2B C 0.7072(2) 0.9660(2) -0.0173(2) 0.0376(9) Uani 1 1 d . . . . . C3B C 0.7493(3) 0.9402(2) -0.0714(3) 0.0433(10) Uani 1 1 d . . . . . H3B H 0.7966 0.9597 -0.0689 0.052 Uiso 1 1 calc R U . . . C4B C 0.7214(2) 0.8878(2) -0.1264(3) 0.042(1) Uani 1 1 d . . . . . S5B S 0.76319(7) 0.84965(7) -0.19841(8) 0.0566(4) Uani 1 1 d . . . . . C6B C 0.6886(3) 0.7939(3) -0.2344(3) 0.0549(12) Uani 1 1 d . . . . . H6B H 0.6860 0.7609 -0.2782 0.066 Uiso 1 1 calc R U . . . C7B C 0.6347(3) 0.8011(2) -0.1957(3) 0.0438(10) Uani 1 1 d . . . . . H7B H 0.5904 0.7739 -0.2088 0.053 Uiso 1 1 calc R U . . . C8B C 0.6515(2) 0.8549(2) -0.1315(2) 0.0399(9) Uani 1 1 d . . . . . C9B C 0.6100(3) 0.8784(2) -0.0789(2) 0.0405(9) Uani 1 1 d . . . . . H9B H 0.5631 0.8578 -0.0820 0.049 Uiso 1 1 calc R U . . . C10B C 0.6372(2) 0.9331(2) -0.0204(2) 0.0374(9) Uani 1 1 d . . . . . C11B C 0.5952(2) 0.9575(2) 0.0323(2) 0.0362(9) Uani 1 1 d . . . . . H11B H 0.5489 0.9358 0.0299 0.043 Uiso 1 1 calc R U . . . C12B C 0.6196(2) 1.0128(2) 0.0883(2) 0.0377(9) Uani 1 1 d . . . . . C13B C 0.5751(2) 1.0376(2) 0.1407(2) 0.0373(9) Uani 1 1 d . . . . . H13B H 0.5291 1.0155 0.1385 0.045 Uiso 1 1 calc R U . . . C14B C 0.5987(3) 1.0929(2) 0.1938(2) 0.0405(9) Uani 1 1 d . . . . . C15B C 0.5635(3) 1.1253(2) 0.2525(3) 0.0432(10) Uani 1 1 d . . . . . H15B H 0.5167 1.1112 0.2592 0.052 Uiso 1 1 calc R U . . . C16B C 0.6035(3) 1.1765(2) 0.2955(3) 0.0545(12) Uani 1 1 d . . . . . H16B H 0.5885 1.2022 0.3374 0.065 Uiso 1 1 calc R U . . . S17B S 0.68676(8) 1.19370(6) 0.26932(7) 0.0535(3) Uani 1 1 d . . . . . C18B C 0.6685(3) 1.1258(2) 0.1961(2) 0.0435(10) Uani 1 1 d . . . . . C19B C 0.7118(3) 1.1041(2) 0.1465(3) 0.0425(9) Uani 1 1 d . . . . . H19B H 0.7574 1.1273 0.1491 0.051 Uiso 1 1 calc R U . . . C20B C 0.6887(2) 1.0469(2) 0.0910(2) 0.0369(9) Uani 1 1 d . . . . . C21B C 0.7959(3) 1.0608(2) 0.0351(3) 0.0485(11) Uani 1 1 d . . . . . C22B C 0.8477(3) 1.0973(3) 0.0307(4) 0.0606(13) Uani 1 1 d . . . . . C23B C 0.8577(7) 1.2476(7) -0.0168(10) 0.088(3) Uani 0.539(7) 1 d D U P A 1 H23B H 0.8507 1.2534 -0.0793 0.105 Uiso 0.539(7) 1 calc R U P A 1 C24B C 0.9312(9) 1.3122(10) 0.0398(13) 0.127(4) Uani 0.539(7) 1 d D U P A 1 H24G H 0.9789 1.3009 0.0290 0.190 Uiso 0.539(7) 1 calc R U P A 1 H24H H 0.9157 1.3591 0.0187 0.190 Uiso 0.539(7) 1 calc R U P A 1 H24I H 0.9370 1.3103 0.1012 0.190 Uiso 0.539(7) 1 calc R U P A 1 C25B C 0.7975(7) 1.2622(7) -0.0029(10) 0.087(3) Uani 0.539(7) 1 d D U P A 1 H25E H 0.7895 1.2218 0.0308 0.104 Uiso 0.539(7) 1 calc R U P A 1 H25F H 0.7614 1.2558 -0.0597 0.104 Uiso 0.539(7) 1 calc R U P A 1 C26B C 0.7619(13) 1.3218(13) 0.0349(15) 0.102(5) Uani 0.539(7) 1 d D U P A 1 H26G H 0.7104 1.3096 0.0325 0.153 Uiso 0.539(7) 1 calc R U P A 1 H26H H 0.7907 1.3296 0.0942 0.153 Uiso 0.539(7) 1 calc R U P A 1 H26I H 0.7621 1.3643 0.0019 0.153 Uiso 0.539(7) 1 calc R U P A 1 C23D C 0.8808(9) 1.2489(8) 0.0480(11) 0.088(3) Uani 0.461(7) 1 d D U P A 2 H23D H 0.9150 1.2620 0.1048 0.105 Uiso 0.461(7) 1 calc R U P A 2 C24D C 0.9107(12) 1.3038(12) -0.0324(15) 0.127(4) Uani 0.461(7) 1 d D U P A 2 H24J H 0.9606 1.2894 -0.0342 0.190 Uiso 0.461(7) 1 calc R U P A 2 H24K H 0.8752 1.2976 -0.0887 0.190 Uiso 0.461(7) 1 calc R U P A 2 H24L H 0.9118 1.3527 -0.0159 0.190 Uiso 0.461(7) 1 calc R U P A 2 C25D C 0.8175(9) 1.2680(9) 0.0492(11) 0.087(3) Uani 0.461(7) 1 d D U P A 2 H25G H 0.8257 1.2799 0.1099 0.104 Uiso 0.461(7) 1 calc R U P A 2 H25H H 0.7899 1.2236 0.0415 0.104 Uiso 0.461(7) 1 calc R U P A 2 C26D C 0.7558(15) 1.3197(15) 0.0051(18) 0.102(5) Uani 0.461(7) 1 d D U P A 2 H26J H 0.7136 1.3153 0.0294 0.153 Uiso 0.461(7) 1 calc R U P A 2 H26K H 0.7755 1.3671 0.0139 0.153 Uiso 0.461(7) 1 calc R U P A 2 H26L H 0.7389 1.3096 -0.0560 0.153 Uiso 0.461(7) 1 calc R U P A 2 C27B C 1.0074(5) 1.1491(5) 0.1062(7) 0.118(3) Uani 0.539(7) 1 d D U P A 1 H27B H 1.0468 1.1786 0.0929 0.142 Uiso 0.539(7) 1 calc R U P A 1 C28B C 1.0364(15) 1.0716(8) 0.1177(13) 0.114(5) Uani 0.539(7) 1 d D U P A 1 H28G H 1.0507 1.0570 0.0671 0.170 Uiso 0.539(7) 1 calc R U P A 1 H28H H 1.0799 1.0684 0.1679 0.170 Uiso 0.539(7) 1 calc R U P A 1 H28I H 0.9966 1.0412 0.1253 0.170 Uiso 0.539(7) 1 calc R U P A 1 C29B C 0.9830(13) 1.1824(10) 0.1724(12) 0.129(5) Uani 0.539(7) 1 d D U P A 1 H29E H 1.0258 1.2101 0.2063 0.155 Uiso 0.539(7) 1 calc R U P A 1 H29F H 0.9437 1.2160 0.1439 0.155 Uiso 0.539(7) 1 calc R U P A 1 C30B C 0.9551(13) 1.1455(13) 0.2311(13) 0.162(6) Uani 0.539(7) 1 d D U P A 1 H30G H 0.9419 1.1781 0.2704 0.243 Uiso 0.539(7) 1 calc R U P A 1 H30H H 0.9107 1.1192 0.2005 0.243 Uiso 0.539(7) 1 calc R U P A 1 H30I H 0.9934 1.1133 0.2633 0.243 Uiso 0.539(7) 1 calc R U P A 1 C27D C 1.0074(5) 1.1491(5) 0.1062(7) 0.118(3) Uani 0.461(7) 1 d D U P A 2 H27D H 1.0421 1.1830 0.0909 0.142 Uiso 0.461(7) 1 calc R U P A 2 C28D C 1.0347(18) 1.0765(9) 0.0799(16) 0.114(5) Uani 0.461(7) 1 d D U P A 2 H28J H 1.0248 1.0746 0.0179 0.170 Uiso 0.461(7) 1 calc R U P A 2 H28K H 1.0884 1.0713 0.1068 0.170 Uiso 0.461(7) 1 calc R U P A 2 H28L H 1.0077 1.0390 0.0987 0.170 Uiso 0.461(7) 1 calc R U P A 2 C29D C 1.0170(15) 1.1628(12) 0.1956(10) 0.129(5) Uani 0.461(7) 1 d D U P A 2 H29G H 0.9663 1.1656 0.2032 0.155 Uiso 0.461(7) 1 calc R U P A 2 H29H H 1.0410 1.1212 0.2271 0.155 Uiso 0.461(7) 1 calc R U P A 2 C30D C 1.0567(16) 1.2203(14) 0.2374(14) 0.162(6) Uani 0.461(7) 1 d D U P A 2 H30J H 1.0565 1.2199 0.2972 0.243 Uiso 0.461(7) 1 calc R U P A 2 H30K H 1.1083 1.2182 0.2342 0.243 Uiso 0.461(7) 1 calc R U P A 2 H30L H 1.0330 1.2630 0.2102 0.243 Uiso 0.461(7) 1 calc R U P A 2 C31B C 0.9277(10) 1.1326(9) -0.1001(11) 0.120(4) Uani 0.638(7) 1 d D U P A 1 H31B H 0.9297 1.0808 -0.1015 0.145 Uiso 0.638(7) 1 calc R U P A 1 C32B C 0.8529(12) 1.1577(16) -0.1771(17) 0.189(6) Uani 0.638(7) 1 d D U P A 1 H32G H 0.8683 1.1716 -0.2273 0.283 Uiso 0.638(7) 1 calc R U P A 1 H32H H 0.8292 1.1971 -0.1572 0.283 Uiso 0.638(7) 1 calc R U P A 1 H32I H 0.8174 1.1192 -0.1921 0.283 Uiso 0.638(7) 1 calc R U P A 1 C33B C 1.0002(10) 1.1594(11) -0.1107(12) 0.144(5) Uani 0.638(7) 1 d D U P A 1 H33E H 0.9990 1.2108 -0.1120 0.173 Uiso 0.638(7) 1 calc R U P A 1 H33F H 1.0418 1.1448 -0.0614 0.173 Uiso 0.638(7) 1 calc R U P A 1 C34B C 1.0134(13) 1.1329(14) -0.1904(15) 0.204(7) Uani 0.638(7) 1 d D U P A 1 H34G H 1.0458 1.0919 -0.1776 0.305 Uiso 0.638(7) 1 calc R U P A 1 H34H H 1.0376 1.1690 -0.2155 0.305 Uiso 0.638(7) 1 calc R U P A 1 H34I H 0.9656 1.1202 -0.2308 0.305 Uiso 0.638(7) 1 calc R U P A 1 C31D C 0.9373(14) 1.1673(16) -0.0736(16) 0.120(4) Uani 0.362(7) 1 d D U P A 2 H31D H 0.9639 1.2129 -0.0677 0.145 Uiso 0.362(7) 1 calc R U P A 2 C32D C 1.0059(17) 1.1121(17) -0.074(2) 0.144(5) Uani 0.362(7) 1 d D U P A 2 H32J H 1.0409 1.1095 -0.0172 0.216 Uiso 0.362(7) 1 calc R U P A 2 H32K H 0.9847 1.0660 -0.0914 0.216 Uiso 0.362(7) 1 calc R U P A 2 H32L H 1.0322 1.1282 -0.1147 0.216 Uiso 0.362(7) 1 calc R U P A 2 C33D C 0.8799(17) 1.176(2) -0.158(2) 0.189(6) Uani 0.362(7) 1 d D U P A 2 H33G H 0.8614 1.2241 -0.1636 0.226 Uiso 0.362(7) 1 calc R U P A 2 H33H H 0.9035 1.1670 -0.2040 0.226 Uiso 0.362(7) 1 calc R U P A 2 C34D C 0.8156(18) 1.128(3) -0.168(3) 0.204(7) Uani 0.362(7) 1 d D U P A 2 H34J H 0.7796 1.1349 -0.2237 0.305 Uiso 0.362(7) 1 calc R U P A 2 H34K H 0.8336 1.0796 -0.1635 0.305 Uiso 0.362(7) 1 calc R U P A 2 H34L H 0.7914 1.1367 -0.1231 0.305 Uiso 0.362(7) 1 calc R U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Si1A 0.0452(8) 0.0866(11) 0.0597(8) 0.0085(7) 0.0176(6) 0.0159(7) C1A 0.043(2) 0.031(2) 0.0289(18) 0.0043(14) 0.0170(16) 0.0028(16) C2A 0.049(2) 0.0281(19) 0.0287(18) 0.0045(14) 0.0208(16) 0.0010(16) C3A 0.039(2) 0.033(2) 0.0291(18) 0.0064(14) 0.0124(15) 0.0041(16) C4A 0.048(2) 0.033(2) 0.0291(18) 0.0026(14) 0.0139(16) -0.0049(17) S5A 0.0613(7) 0.0358(6) 0.0327(5) -0.0001(4) 0.0145(4) -0.0006(5) C6A 0.067(3) 0.038(2) 0.035(2) -0.0020(16) 0.023(2) 0.004(2) C7A 0.065(3) 0.0217(18) 0.0272(18) 0.0014(13) 0.0187(18) 0.0010(17) C8A 0.055(2) 0.030(2) 0.0283(18) 0.0021(14) 0.0219(17) -0.0001(17) C9A 0.043(2) 0.032(2) 0.0289(18) 0.0011(14) 0.0163(16) 0.0019(16) C10A 0.046(2) 0.031(2) 0.0271(18) 0.0031(14) 0.0174(16) 0.0028(16) C11A 0.043(2) 0.031(2) 0.0301(18) 0.0031(14) 0.0147(15) 0.0048(16) C12A 0.046(2) 0.0286(19) 0.0255(17) 0.0041(13) 0.0159(15) 0.0015(16) C13A 0.042(2) 0.040(2) 0.0254(18) 0.0053(14) 0.0110(15) 0.0026(16) C14A 0.057(3) 0.031(2) 0.0246(18) 0.0022(14) 0.0146(16) -0.0034(17) C15A 0.065(3) 0.042(2) 0.0257(19) 0.0011(16) 0.0143(18) 0.000(2) C16A 0.078(3) 0.034(2) 0.034(2) -0.0016(16) 0.023(2) -0.005(2) S17A 0.0655(7) 0.0322(5) 0.0387(5) -0.0019(4) 0.0270(5) 0.0012(4) C18A 0.054(2) 0.030(2) 0.0261(18) 0.0031(14) 0.0206(17) 0.0035(17) C19A 0.051(2) 0.0238(18) 0.0337(19) 0.0032(14) 0.0206(17) 0.0039(16) C20A 0.047(2) 0.0290(19) 0.0263(17) 0.0044(13) 0.0178(16) 0.0020(15) C21A 0.046(2) 0.039(2) 0.040(2) -0.0021(16) 0.0202(18) 0.0003(18) C22A 0.051(3) 0.048(3) 0.049(2) -0.0022(19) 0.018(2) 0.005(2) C23A 0.062(4) 0.082(6) 0.067(3) 0.000(4) 0.034(3) 0.007(5) C24A 0.084(5) 0.093(6) 0.090(5) 0.017(5) 0.035(4) -0.007(5) C25A 0.103(6) 0.111(7) 0.083(4) -0.008(5) 0.039(4) -0.004(5) C26A 0.155(12) 0.133(12) 0.086(8) 0.000(7) 0.056(8) 0.041(10) C23C 0.062(4) 0.082(6) 0.067(3) 0.000(4) 0.034(3) 0.007(5) C24C 0.103(6) 0.111(7) 0.083(4) -0.008(5) 0.039(4) -0.004(5) C25C 0.084(5) 0.093(6) 0.090(5) 0.017(5) 0.035(4) -0.007(5) C26C 0.119(13) 0.205(15) 0.136(10) 0.048(10) 0.059(10) -0.007(11) C27A 0.098(4) 0.101(4) 0.121(5) 0.018(4) 0.049(4) 0.039(3) C28A 0.112(6) 0.127(9) 0.159(10) 0.002(7) 0.070(6) 0.036(6) C29A 0.080(5) 0.073(4) 0.072(5) -0.011(4) 0.021(4) 0.011(3) C30A 0.105(5) 0.072(4) 0.074(5) -0.013(3) 0.022(3) 0.015(3) C27C 0.098(4) 0.101(4) 0.121(5) 0.018(4) 0.049(4) 0.039(3) C28C 0.112(6) 0.127(9) 0.159(10) 0.002(7) 0.070(6) 0.036(6) C29C 0.080(5) 0.073(4) 0.072(5) -0.011(4) 0.021(4) 0.011(3) C30C 0.105(5) 0.072(4) 0.074(5) -0.013(3) 0.022(3) 0.015(3) C31A 0.078(4) 0.083(7) 0.074(3) 0.010(4) -0.005(3) -0.009(5) C32A 0.087(5) 0.140(8) 0.122(7) 0.021(6) 0.006(4) -0.021(5) C33A 0.096(7) 0.106(6) 0.071(4) 0.006(4) -0.001(5) -0.017(6) C34A 0.256(18) 0.223(16) 0.171(12) -0.063(11) 0.053(11) -0.030(13) C31C 0.078(4) 0.083(7) 0.074(3) 0.010(4) -0.005(3) -0.009(5) C32C 0.096(7) 0.106(6) 0.071(4) 0.006(4) -0.001(5) -0.017(6) C33C 0.087(5) 0.140(8) 0.122(7) 0.021(6) 0.006(4) -0.021(5) C34C 0.134(15) 0.200(19) 0.160(13) -0.024(12) 0.02(1) -0.041(14) Si1B 0.0697(12) 0.0754(13) 0.1490(19) 0.0111(11) 0.0608(12) -0.0093(9) C1B 0.044(2) 0.044(2) 0.037(2) 0.0058(17) 0.0108(17) 0.0007(18) C2B 0.041(2) 0.041(2) 0.0319(19) 0.0084(16) 0.0126(16) 0.0027(17) C3B 0.049(3) 0.043(2) 0.041(2) 0.0082(17) 0.0188(19) 0.0091(19) C4B 0.044(2) 0.050(3) 0.037(2) 0.0056(17) 0.0185(17) 0.0080(19) S5B 0.0605(8) 0.0649(8) 0.0530(7) -0.0044(5) 0.0303(6) 0.0063(6) C6B 0.076(4) 0.053(3) 0.042(2) -0.0022(19) 0.028(2) 0.015(2) C7B 0.055(3) 0.043(2) 0.037(2) 0.0011(17) 0.0203(19) -0.0005(19) C8B 0.047(2) 0.042(2) 0.033(2) 0.0034(16) 0.0149(17) 0.0039(18) C9B 0.050(3) 0.038(2) 0.036(2) 0.0048(16) 0.0169(18) -0.0036(18) C10B 0.050(2) 0.038(2) 0.0279(18) 0.0038(15) 0.0171(16) 0.0037(17) C11B 0.049(2) 0.030(2) 0.0345(19) 0.0084(15) 0.0191(17) 0.0011(16) C12B 0.051(2) 0.035(2) 0.0304(19) 0.0080(15) 0.0175(17) 0.0060(17) C13B 0.048(2) 0.036(2) 0.0320(19) 0.0106(15) 0.0182(17) 0.0000(17) C14B 0.059(3) 0.033(2) 0.033(2) 0.0059(15) 0.0196(18) 0.0037(18) C15B 0.061(3) 0.036(2) 0.038(2) 0.0083(17) 0.0225(19) 0.0071(19) C16B 0.087(4) 0.039(3) 0.040(2) 0.0024(18) 0.021(2) 0.015(2) S17B 0.0672(8) 0.0471(7) 0.0451(6) -0.0076(5) 0.0143(5) -0.0015(5) C18B 0.060(3) 0.038(2) 0.030(2) 0.0006(16) 0.0089(18) 0.0022(19) C19B 0.048(2) 0.044(2) 0.037(2) 0.0033(17) 0.0129(18) -0.0028(18) C20B 0.041(2) 0.038(2) 0.0317(19) 0.0065(15) 0.0111(16) 0.0040(16) C21B 0.051(3) 0.047(3) 0.052(3) -0.0054(19) 0.022(2) 0.001(2) C22B 0.055(3) 0.060(3) 0.074(3) -0.004(2) 0.029(3) -0.006(2) C23B 0.084(4) 0.083(5) 0.103(6) 0.009(5) 0.036(4) 0.000(4) C24B 0.110(7) 0.114(8) 0.160(9) 0.020(8) 0.045(7) -0.006(6) C25B 0.084(4) 0.082(5) 0.093(6) -0.005(5) 0.025(4) 0.004(4) C26B 0.096(6) 0.105(6) 0.109(12) -0.003(7) 0.035(7) 0.008(5) C23D 0.084(4) 0.083(5) 0.103(6) 0.009(5) 0.036(4) 0.000(4) C24D 0.110(7) 0.114(8) 0.160(9) 0.020(8) 0.045(7) -0.006(6) C25D 0.084(4) 0.082(5) 0.093(6) -0.005(5) 0.025(4) 0.004(4) C26D 0.096(6) 0.105(6) 0.109(12) -0.003(7) 0.035(7) 0.008(5) C27B 0.105(5) 0.114(5) 0.141(5) 0.002(4) 0.044(4) -0.018(4) C28B 0.085(6) 0.119(6) 0.138(12) 0.015(6) 0.032(9) 0.000(5) C29B 0.123(8) 0.138(7) 0.137(6) 0.003(5) 0.053(5) 0.006(5) C30B 0.162(10) 0.182(10) 0.147(8) -0.012(7) 0.053(7) -0.026(8) C27D 0.105(5) 0.114(5) 0.141(5) 0.002(4) 0.044(4) -0.018(4) C28D 0.085(6) 0.119(6) 0.138(12) 0.015(6) 0.032(9) 0.000(5) C29D 0.123(8) 0.138(7) 0.137(6) 0.003(5) 0.053(5) 0.006(5) C30D 0.162(10) 0.182(10) 0.147(8) -0.012(7) 0.053(7) -0.026(8) C31B 0.129(5) 0.126(7) 0.128(6) -0.005(5) 0.071(4) -0.003(5) C32B 0.174(7) 0.203(9) 0.188(8) 0.012(6) 0.049(6) 0.000(6) C33B 0.149(6) 0.151(8) 0.150(7) -0.009(6) 0.071(5) 0.000(6) C34B 0.204(10) 0.236(13) 0.199(10) -0.040(8) 0.103(8) -0.022(9) C31D 0.129(5) 0.126(7) 0.128(6) -0.005(5) 0.071(4) -0.003(5) C32D 0.149(6) 0.151(8) 0.150(7) -0.009(6) 0.071(5) 0.000(6) C33D 0.174(7) 0.203(9) 0.188(8) 0.012(6) 0.049(6) 0.000(6) C34D 0.204(10) 0.236(13) 0.199(10) -0.040(8) 0.103(8) -0.022(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.2541 0.3302 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C31C Si1A C22A 112.6(12) . . C31C Si1A C27C 106.8(11) . . C22A Si1A C27C 107.2(3) . . C22A Si1A C27A 107.2(3) . . C22A Si1A C23A 105.8(5) . . C27A Si1A C23A 103.7(5) . . C31C Si1A C23C 107.2(12) . . C22A Si1A C23C 105.1(5) . . C27C Si1A C23C 118.2(5) . . C22A Si1A C31A 104.4(6) . . C27A Si1A C31A 116.9(5) . . C23A Si1A C31A 117.8(8) . . C20A C1A C2A 121.6(4) . . C20A C1A C21A 119.6(3) . . C2A C1A C21A 118.8(4) . . C3A C2A C1A 122.2(4) . . C3A C2A C10A 119.7(3) . . C1A C2A C10A 118.1(4) . . C4A C3A C2A 119.6(4) . . C4A C3A H3A 120.2 . . C2A C3A H3A 120.2 . . C3A C4A C8A 122.2(4) . . C3A C4A S5A 126.7(3) . . C8A C4A S5A 111.2(3) . . C6A S5A C4A 90.9(2) . . C7A C6A S5A 115.4(3) . . C7A C6A H6A 122.3 . . S5A C6A H6A 122.3 . . C6A C7A C8A 110.6(4) . . C6A C7A H7A 124.7 . . C8A C7A H7A 124.7 . . C9A C8A C4A 119.7(4) . . C9A C8A C7A 128.4(4) . . C4A C8A C7A 111.9(4) . . C8A C9A C10A 120.3(4) . . C8A C9A H9A 119.9 . . C10A C9A H9A 119.9 . . C11A C10A C9A 122.0(4) . . C11A C10A C2A 119.5(3) . . C9A C10A C2A 118.6(4) . . C10A C11A C12A 122.9(4) . . C10A C11A H11A 118.6 . . C12A C11A H11A 118.6 . . C11A C12A C13A 122.0(4) . . C11A C12A C20A 118.4(4) . . C13A C12A C20A 119.6(3) . . C14A C13A C12A 120.3(4) . . C14A C13A H13A 119.9 . . C12A C13A H13A 119.9 . . C13A C14A C18A 119.7(4) . . C13A C14A C15A 129.2(4) . . C18A C14A C15A 111.1(4) . . C16A C15A C14A 112.7(4) . . C16A C15A H15A 123.6 . . C14A C15A H15A 123.6 . . C15A C16A S17A 114.5(3) . . C15A C16A H16A 122.8 . . S17A C16A H16A 122.8 . . C16A S17A C18A 90.4(2) . . C19A C18A C14A 122.5(3) . . C19A C18A S17A 126.2(3) . . C14A C18A S17A 111.3(3) . . C18A C19A C20A 119.0(4) . . C18A C19A H19A 120.5 . . C20A C19A H19A 120.5 . . C1A C20A C19A 121.4(4) . . C1A C20A C12A 119.5(3) . . C19A C20A C12A 119.0(4) . . C22A C21A C1A 178.7(5) . . C21A C22A Si1A 176.6(4) . . C24A C23A C25A 110.3(10) . . C24A C23A Si1A 104.9(10) . . C25A C23A Si1A 112.2(11) . . C24A C23A H23A 109.8 . . C25A C23A H23A 109.8 . . Si1A C23A H23A 109.8 . . C23A C24A H24A 109.5 . . C23A C24A H24B 109.5 . . H24A C24A H24B 109.5 . . C23A C24A H24C 109.5 . . H24A C24A H24C 109.5 . . H24B C24A H24C 109.5 . . C23A C25A C26A 95.(1) . . C23A C25A H25A 112.7 . . C26A C25A H25A 112.7 . . C23A C25A H25B 112.7 . . C26A C25A H25B 112.7 . . H25A C25A H25B 110.2 . . C25A C26A H26A 109.5 . . C25A C26A H26B 109.5 . . H26A C26A H26B 109.5 . . C25A C26A H26C 109.5 . . H26A C26A H26C 109.5 . . H26B C26A H26C 109.5 . . C24C C23C C25C 110.3(10) . . C24C C23C Si1A 109.2(11) . . C25C C23C Si1A 115.4(10) . . C24C C23C H23C 107.2 . . C25C C23C H23C 107.2 . . Si1A C23C H23C 107.2 . . C23C C24C H24D 109.5 . . C23C C24C H24E 109.5 . . H24D C24C H24E 109.5 . . C23C C24C H24F 109.5 . . H24D C24C H24F 109.5 . . H24E C24C H24F 109.5 . . C23C C25C C26C 93.4(10) . . C23C C25C H25C 113.0 . . C26C C25C H25C 113.0 . . C23C C25C H25D 113.0 . . C26C C25C H25D 113.0 . . H25C C25C H25D 110.4 . . C25C C26C H26D 109.5 . . C25C C26C H26E 109.5 . . H26D C26C H26E 109.5 . . C25C C26C H26F 109.5 . . H26D C26C H26F 109.5 . . H26E C26C H26F 109.5 . . C29A C27A C28A 120.0(9) . . C29A C27A Si1A 117.6(6) . . C28A C27A Si1A 119.0(8) . . C29A C27A H27A 96.1 . . C28A C27A H27A 96.1 . . Si1A C27A H27A 96.1 . . C27A C28A H28A 109.5 . . C27A C28A H28B 109.5 . . H28A C28A H28B 109.5 . . C27A C28A H28C 109.5 . . H28A C28A H28C 109.5 . . H28B C28A H28C 109.5 . . C27A C29A C30A 119.8(16) . . C27A C29A H29A 107.4 . . C30A C29A H29A 107.4 . . C27A C29A H29B 107.4 . . C30A C29A H29B 107.4 . . H29A C29A H29B 106.9 . . C29A C30A H30A 109.5 . . C29A C30A H30B 109.5 . . H30A C30A H30B 109.5 . . C29A C30A H30C 109.5 . . H30A C30A H30C 109.5 . . H30B C30A H30C 109.5 . . C29C C27C C28C 122.2(13) . . C29C C27C Si1A 119.3(9) . . C28C C27C Si1A 109.2(12) . . C29C C27C H27C 100.2 . . C28C C27C H27C 100.2 . . Si1A C27C H27C 100.2 . . C27C C28C H28D 109.5 . . C27C C28C H28E 109.5 . . H28D C28C H28E 109.5 . . C27C C28C H28F 109.5 . . H28D C28C H28F 109.5 . . H28E C28C H28F 109.5 . . C27C C29C C30C 120.0(19) . . C27C C29C H29C 107.3 . . C30C C29C H29C 107.3 . . C27C C29C H29D 107.3 . . C30C C29C H29D 107.3 . . H29C C29C H29D 106.9 . . C29C C30C H30D 109.5 . . C29C C30C H30E 109.5 . . H30D C30C H30E 109.5 . . C29C C30C H30F 109.5 . . H30D C30C H30F 109.5 . . H30E C30C H30F 109.5 . . C32A C31A C33A 114.6(10) . . C32A C31A Si1A 105.9(12) . . C33A C31A Si1A 106.4(10) . . C32A C31A H31A 109.9 . . C33A C31A H31A 109.9 . . Si1A C31A H31A 109.9 . . C31A C32A H32A 109.5 . . C31A C32A H32B 109.5 . . H32A C32A H32B 109.5 . . C31A C32A H32C 109.5 . . H32A C32A H32C 109.5 . . H32B C32A H32C 109.5 . . C34A C33A C31A 109.4(14) . . C34A C33A H33A 109.8 . . C31A C33A H33A 109.8 . . C34A C33A H33B 109.8 . . C31A C33A H33B 109.8 . . H33A C33A H33B 108.2 . . C33A C34A H34A 109.5 . . C33A C34A H34B 109.5 . . H34A C34A H34B 109.5 . . C33A C34A H34C 109.5 . . H34A C34A H34C 109.5 . . H34B C34A H34C 109.5 . . C32C C31C Si1A 130(2) . . C32C C31C C33C 109.6(12) . . Si1A C31C C33C 120.1(19) . . C32C C31C H31C 92.9 . . Si1A C31C H31C 92.9 . . C33C C31C H31C 92.9 . . C31C C32C H32D 109.5 . . C31C C32C H32E 109.5 . . H32D C32C H32E 109.5 . . C31C C32C H32F 109.5 . . H32D C32C H32F 109.5 . . H32E C32C H32F 109.5 . . C34C C33C C31C 107.5(15) . . C34C C33C H33C 110.2 . . C31C C33C H33C 110.2 . . C34C C33C H33D 110.2 . . C31C C33C H33D 110.2 . . H33C C33C H33D 108.5 . . C33C C34C H34D 109.5 . . C33C C34C H34E 109.5 . . H34D C34C H34E 109.5 . . C33C C34C H34F 109.5 . . H34D C34C H34F 109.5 . . H34E C34C H34F 109.5 . . C31D Si1B C22B 118.9(11) . . C31D Si1B C27D 108.3(9) . . C22B Si1B C27D 109.9(4) . . C22B Si1B C27B 109.9(4) . . C31D Si1B C23D 110.5(11) . . C22B Si1B C23D 104.9(5) . . C27D Si1B C23D 103.1(6) . . C22B Si1B C23B 104.0(4) . . C27B Si1B C23B 129.3(5) . . C22B Si1B C31B 99.8(5) . . C27B Si1B C31B 111.8(6) . . C23B Si1B C31B 97.8(7) . . C2B C1B C20B 121.9(4) . . C2B C1B C21B 120.0(4) . . C20B C1B C21B 117.8(4) . . C1B C2B C3B 122.7(4) . . C1B C2B C10B 118.9(4) . . C3B C2B C10B 118.4(4) . . C4B C3B C2B 119.8(4) . . C4B C3B H3B 120.1 . . C2B C3B H3B 120.1 . . C3B C4B C8B 122.9(4) . . C3B C4B S5B 126.9(4) . . C8B C4B S5B 110.2(3) . . C6B S5B C4B 91.3(2) . . C7B C6B S5B 114.5(4) . . C7B C6B H6B 122.8 . . S5B C6B H6B 122.8 . . C6B C7B C8B 112.4(4) . . C6B C7B H7B 123.8 . . C8B C7B H7B 123.8 . . C9B C8B C4B 118.4(4) . . C9B C8B C7B 129.9(4) . . C4B C8B C7B 111.6(4) . . C8B C9B C10B 120.4(4) . . C8B C9B H9B 119.8 . . C10B C9B H9B 119.8 . . C11B C10B C9B 120.6(4) . . C11B C10B C2B 119.3(4) . . C9B C10B C2B 120.0(4) . . C12B C11B C10B 121.7(4) . . C12B C11B H11B 119.2 . . C10B C11B H11B 119.2 . . C11B C12B C13B 120.7(4) . . C11B C12B C20B 119.6(4) . . C13B C12B C20B 119.7(4) . . C14B C13B C12B 120.2(4) . . C14B C13B H13B 119.9 . . C12B C13B H13B 119.9 . . C13B C14B C18B 119.1(4) . . C13B C14B C15B 129.3(4) . . C18B C14B C15B 111.6(4) . . C16B C15B C14B 112.6(4) . . C16B C15B H15B 123.7 . . C14B C15B H15B 123.7 . . C15B C16B S17B 114.7(4) . . C15B C16B H16B 122.6 . . S17B C16B H16B 122.6 . . C18B S17B C16B 90.7(2) . . C19B C18B C14B 122.2(4) . . C19B C18B S17B 127.4(4) . . C14B C18B S17B 110.4(3) . . C18B C19B C20B 119.8(4) . . C18B C19B H19B 120.1 . . C20B C19B H19B 120.1 . . C1B C20B C19B 122.5(4) . . C1B C20B C12B 118.6(4) . . C19B C20B C12B 118.9(4) . . C22B C21B C1B 175.6(6) . . C21B C22B Si1B 172.6(5) . . C25B C23B C24B 109.2(11) . . C25B C23B Si1B 126.3(12) . . C24B C23B Si1B 97.9(9) . . C25B C23B H23B 107.3 . . C24B C23B H23B 107.3 . . Si1B C23B H23B 107.3 . . C23B C24B H24G 109.5 . . C23B C24B H24H 109.5 . . H24G C24B H24H 109.5 . . C23B C24B H24I 109.5 . . H24G C24B H24I 109.5 . . H24H C24B H24I 109.5 . . C23B C25B C26B 139.3(14) . . C23B C25B H25E 102.3 . . C26B C25B H25E 102.3 . . C23B C25B H25F 102.3 . . C26B C25B H25F 102.3 . . H25E C25B H25F 104.8 . . C25B C26B H26G 109.5 . . C25B C26B H26H 109.5 . . H26G C26B H26H 109.5 . . C25B C26B H26I 109.5 . . H26G C26B H26I 109.5 . . H26H C26B H26I 109.5 . . C25D C23D C24D 108.2(11) . . C25D C23D Si1B 131.8(15) . . C24D C23D Si1B 97.2(10) . . C25D C23D H23D 105.7 . . C24D C23D H23D 105.7 . . Si1B C23D H23D 105.7 . . C23D C24D H24J 109.5 . . C23D C24D H24K 109.5 . . H24J C24D H24K 109.5 . . C23D C24D H24L 109.5 . . H24J C24D H24L 109.5 . . H24K C24D H24L 109.5 . . C23D C25D C26D 140.7(16) . . C23D C25D H25G 101.9 . . C26D C25D H25G 101.9 . . C23D C25D H25H 101.9 . . C26D C25D H25H 101.9 . . H25G C25D H25H 104.7 . . C25D C26D H26J 109.5 . . C25D C26D H26K 109.5 . . H26J C26D H26K 109.5 . . C25D C26D H26L 109.5 . . H26J C26D H26L 109.5 . . H26K C26D H26L 109.5 . . C29B C27B C28B 120.0(12) . . C29B C27B Si1B 96.2(11) . . C28B C27B Si1B 114.3(11) . . C29B C27B H27B 108.5 . . C28B C27B H27B 108.5 . . Si1B C27B H27B 108.5 . . C27B C28B H28G 109.5 . . C27B C28B H28H 109.5 . . H28G C28B H28H 109.5 . . C27B C28B H28I 109.5 . . H28G C28B H28I 109.5 . . H28H C28B H28I 109.5 . . C30B C29B C27B 123.0(16) . . C30B C29B H29E 106.6 . . C27B C29B H29E 106.6 . . C30B C29B H29F 106.6 . . C27B C29B H29F 106.6 . . H29E C29B H29F 106.5 . . C29B C30B H30G 109.5 . . C29B C30B H30H 109.5 . . H30G C30B H30H 109.5 . . C29B C30B H30I 109.5 . . H30G C30B H30I 109.5 . . H30H C30B H30I 109.5 . . C29D C27D C28D 118.5(13) . . C29D C27D Si1B 124.7(12) . . C28D C27D Si1B 101.1(13) . . C29D C27D H27D 103.3 . . C28D C27D H27D 103.3 . . Si1B C27D H27D 103.3 . . C27D C28D H28J 109.5 . . C27D C28D H28K 109.5 . . H28J C28D H28K 109.5 . . C27D C28D H28L 109.5 . . H28J C28D H28L 109.5 . . H28K C28D H28L 109.5 . . C30D C29D C27D 122.5(18) . . C30D C29D H29G 106.7 . . C27D C29D H29G 106.7 . . C30D C29D H29H 106.7 . . C27D C29D H29H 106.7 . . H29G C29D H29H 106.6 . . C29D C30D H30J 109.5 . . C29D C30D H30K 109.5 . . H30J C30D H30K 109.5 . . C29D C30D H30L 109.5 . . H30J C30D H30L 109.5 . . H30K C30D H30L 109.5 . . C33B C31B C32B 113.7(15) . . C33B C31B Si1B 109.8(12) . . C32B C31B Si1B 110.5(14) . . C33B C31B H31B 107.5 . . C32B C31B H31B 107.5 . . Si1B C31B H31B 107.5 . . C31B C32B H32G 109.5 . . C31B C32B H32H 109.5 . . H32G C32B H32H 109.5 . . C31B C32B H32I 109.5 . . H32G C32B H32I 109.5 . . H32H C32B H32I 109.5 . . C34B C33B C31B 111.1(17) . . C34B C33B H33E 109.4 . . C31B C33B H33E 109.4 . . C34B C33B H33F 109.4 . . C31B C33B H33F 109.4 . . H33E C33B H33F 108.0 . . C33B C34B H34G 109.5 . . C33B C34B H34H 109.5 . . H34G C34B H34H 109.5 . . C33B C34B H34I 109.5 . . H34G C34B H34I 109.5 . . H34H C34B H34I 109.5 . . C33D C31D C32D 114.4(16) . . C33D C31D Si1B 124.1(19) . . C32D C31D Si1B 109(2) . . C33D C31D H31D 101.7 . . C32D C31D H31D 101.7 . . Si1B C31D H31D 101.7 . . C31D C32D H32J 109.5 . . C31D C32D H32K 109.5 . . H32J C32D H32K 109.5 . . C31D C32D H32L 109.5 . . H32J C32D H32L 109.5 . . H32K C32D H32L 109.5 . . C34D C33D C31D 112.3(19) . . C34D C33D H33G 109.1 . . C31D C33D H33G 109.1 . . C34D C33D H33H 109.1 . . C31D C33D H33H 109.1 . . H33G C33D H33H 107.9 . . C33D C34D H34J 109.5 . . C33D C34D H34K 109.5 . . H34J C34D H34K 109.5 . . C33D C34D H34L 109.5 . . H34J C34D H34L 109.5 . . H34K C34D H34L 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Si1A C31C 1.715(19) . Si1A C22A 1.824(5) . Si1A C27C 1.885(9) . Si1A C27A 1.885(9) . Si1A C23A 1.892(14) . Si1A C23C 1.924(14) . Si1A C31A 1.950(13) . C1A C20A 1.406(5) . C1A C2A 1.418(5) . C1A C21A 1.422(6) . C2A C3A 1.410(6) . C2A C10A 1.446(6) . C3A C4A 1.359(6) . C3A H3A 0.9500 . C4A C8A 1.426(6) . C4A S5A 1.747(4) . S5A C6A 1.740(5) . C6A C7A 1.349(6) . C6A H6A 0.9500 . C7A C8A 1.476(5) . C7A H7A 0.9500 . C8A C9A 1.373(6) . C9A C10A 1.428(5) . C9A H9A 0.9500 . C10A C11A 1.386(6) . C11A C12A 1.399(5) . C11A H11A 0.9500 . C12A C13A 1.420(6) . C12A C20A 1.436(6) . C13A C14A 1.370(6) . C13A H13A 0.9500 . C14A C18A 1.418(6) . C14A C15A 1.449(6) . C15A C16A 1.335(6) . C15A H15A 0.9500 . C16A S17A 1.737(5) . C16A H16A 0.9500 . S17A C18A 1.754(4) . C18A C19A 1.368(6) . C19A C20A 1.428(5) . C19A H19A 0.9500 . C21A C22A 1.220(6) . C23A C24A 1.520(15) . C23A C25A 1.553(16) . C23A H23A 1.0000 . C24A H24A 0.9800 . C24A H24B 0.9800 . C24A H24C 0.9800 . C25A C26A 1.685(19) . C25A H25A 0.9900 . C25A H25B 0.9900 . C26A H26A 0.9800 . C26A H26B 0.9800 . C26A H26C 0.9800 . C23C C24C 1.523(16) . C23C C25C 1.551(16) . C23C H23C 1.0000 . C24C H24D 0.9800 . C24C H24E 0.9800 . C24C H24F 0.9800 . C25C C26C 1.697(19) . C25C H25C 0.9900 . C25C H25D 0.9900 . C26C H26D 0.9800 . C26C H26E 0.9800 . C26C H26F 0.9800 . C27A C29A 1.465(11) . C27A C28A 1.509(12) . C27A H27A 1.0000 . C28A H28A 0.9800 . C28A H28B 0.9800 . C28A H28C 0.9800 . C29A C30A 1.50(2) . C29A H29A 0.9900 . C29A H29B 0.9900 . C30A H30A 0.9800 . C30A H30B 0.9800 . C30A H30C 0.9800 . C27C C29C 1.452(13) . C27C C28C 1.519(14) . C27C H27C 1.0000 . C28C H28D 0.9800 . C28C H28E 0.9800 . C28C H28F 0.9800 . C29C C30C 1.50(2) . C29C H29C 0.9900 . C29C H29D 0.9900 . C30C H30D 0.9800 . C30C H30E 0.9800 . C30C H30F 0.9800 . C31A C32A 1.49(2) . C31A C33A 1.74(2) . C31A H31A 1.0000 . C32A H32A 0.9800 . C32A H32B 0.9800 . C32A H32C 0.9800 . C33A C34A 1.43(2) . C33A H33A 0.9900 . C33A H33B 0.9900 . C34A H34A 0.9800 . C34A H34B 0.9800 . C34A H34C 0.9800 . C31C C32C 1.50(2) . C31C C33C 1.75(3) . C31C H31C 1.0000 . C32C H32D 0.9800 . C32C H32E 0.9800 . C32C H32F 0.9800 . C33C C34C 1.45(2) . C33C H33C 0.9900 . C33C H33D 0.9900 . C34C H34D 0.9800 . C34C H34E 0.9800 . C34C H34F 0.9800 . Si1B C31D 1.67(2) . Si1B C22B 1.840(6) . Si1B C27D 1.889(10) . Si1B C27B 1.889(10) . Si1B C23D 1.924(16) . Si1B C23B 1.990(14) . Si1B C31B 2.094(16) . C1B C2B 1.398(6) . C1B C20B 1.413(6) . C1B C21B 1.433(6) . C2B C3B 1.429(6) . C2B C10B 1.439(6) . C3B C4B 1.355(6) . C3B H3B 0.9500 . C4B C8B 1.431(6) . C4B S5B 1.749(4) . S5B C6B 1.724(6) . C6B C7B 1.339(6) . C6B H6B 0.9500 . C7B C8B 1.446(6) . C7B H7B 0.9500 . C8B C9B 1.387(6) . C9B C10B 1.418(6) . C9B H9B 0.9500 . C10B C11B 1.400(5) . C11B C12B 1.397(6) . C11B H11B 0.9500 . C12B C13B 1.433(6) . C12B C20B 1.436(6) . C13B C14B 1.368(6) . C13B H13B 0.9500 . C14B C18B 1.439(6) . C14B C15B 1.450(6) . C15B C16B 1.315(7) . C15B H15B 0.9500 . C16B S17B 1.755(6) . C16B H16B 0.9500 . S17B C18B 1.743(4) . C18B C19B 1.362(6) . C19B C20B 1.417(6) . C19B H19B 0.9500 . C21B C22B 1.213(7) . C23B C25B 1.239(13) . C23B C24B 1.890(16) . C23B H23B 1.0000 . C24B H24G 0.9800 . C24B H24H 0.9800 . C24B H24I 0.9800 . C25B C26B 1.542(15) . C25B H25E 0.9900 . C25B H25F 0.9900 . C26B H26G 0.9800 . C26B H26H 0.9800 . C26B H26I 0.9800 . C23D C25D 1.241(14) . C23D C24D 1.891(16) . C23D H23D 1.0000 . C24D H24J 0.9800 . C24D H24K 0.9800 . C24D H24L 0.9800 . C25D C26D 1.540(16) . C25D H25G 0.9900 . C25D H25H 0.9900 . C26D H26J 0.9800 . C26D H26K 0.9800 . C26D H26L 0.9800 . C27B C29B 1.441(15) . C27B C28B 1.582(14) . C27B H27B 1.0000 . C28B H28G 0.9800 . C28B H28H 0.9800 . C28B H28I 0.9800 . C29B C30B 1.41(2) . C29B H29E 0.9900 . C29B H29F 0.9900 . C30B H30G 0.9800 . C30B H30H 0.9800 . C30B H30I 0.9800 . C27D C29D 1.449(15) . C27D C28D 1.588(15) . C27D H27D 1.0000 . C28D H28J 0.9800 . C28D H28K 0.9800 . C28D H28L 0.9800 . C29D C30D 1.40(2) . C29D H29G 0.9900 . C29D H29H 0.9900 . C30D H30J 0.9800 . C30D H30K 0.9800 . C30D H30L 0.9800 . C31B C33B 1.50(2) . C31B C32B 1.67(3) . C31B H31B 1.0000 . C32B H32G 0.9800 . C32B H32H 0.9800 . C32B H32I 0.9800 . C33B C34B 1.49(2) . C33B H33E 0.9900 . C33B H33F 0.9900 . C34B H34G 0.9800 . C34B H34H 0.9800 . C34B H34I 0.9800 . C31D C33D 1.50(2) . C31D C32D 1.67(3) . C31D H31D 1.0000 . C32D H32J 0.9800 . C32D H32K 0.9800 . C32D H32L 0.9800 . C33D C34D 1.49(2) . C33D H33G 0.9900 . C33D H33H 0.9900 . C34D H34J 0.9800 . C34D H34K 0.9800 . C34D H34L 0.9800 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 C20A C1A C2A C3A -178.5(3) . . . . C21A C1A C2A C3A 0.2(5) . . . . C20A C1A C2A C10A 0.5(5) . . . . C21A C1A C2A C10A 179.2(3) . . . . C1A C2A C3A C4A 179.1(3) . . . . C10A C2A C3A C4A 0.0(5) . . . . C2A C3A C4A C8A 0.1(5) . . . . C2A C3A C4A S5A -180.0(3) . . . . C3A C4A S5A C6A -179.7(4) . . . . C8A C4A S5A C6A 0.2(3) . . . . C4A S5A C6A C7A 0.4(3) . . . . S5A C6A C7A C8A -0.8(4) . . . . C3A C4A C8A C9A 0.0(6) . . . . S5A C4A C8A C9A -180.0(3) . . . . C3A C4A C8A C7A 179.2(3) . . . . S5A C4A C8A C7A -0.7(4) . . . . C6A C7A C8A C9A -179.8(4) . . . . C6A C7A C8A C4A 1.0(5) . . . . C4A C8A C9A C10A -0.1(5) . . . . C7A C8A C9A C10A -179.2(3) . . . . C8A C9A C10A C11A -179.0(3) . . . . C8A C9A C10A C2A 0.2(5) . . . . C3A C2A C10A C11A 179.0(3) . . . . C1A C2A C10A C11A 0.0(5) . . . . C3A C2A C10A C9A -0.1(5) . . . . C1A C2A C10A C9A -179.2(3) . . . . C9A C10A C11A C12A 178.6(3) . . . . C2A C10A C11A C12A -0.6(6) . . . . C10A C11A C12A C13A -179.1(3) . . . . C10A C11A C12A C20A 0.7(5) . . . . C11A C12A C13A C14A 179.3(3) . . . . C20A C12A C13A C14A -0.5(5) . . . . C12A C13A C14A C18A -0.1(5) . . . . C12A C13A C14A C15A -179.2(4) . . . . C13A C14A C15A C16A 177.7(4) . . . . C18A C14A C15A C16A -1.5(5) . . . . C14A C15A C16A S17A 1.1(5) . . . . C15A C16A S17A C18A -0.3(3) . . . . C13A C14A C18A C19A 0.7(6) . . . . C15A C14A C18A C19A 179.9(3) . . . . C13A C14A C18A S17A -178.0(3) . . . . C15A C14A C18A S17A 1.2(4) . . . . C16A S17A C18A C19A -179.2(4) . . . . C16A S17A C18A C14A -0.6(3) . . . . C14A C18A C19A C20A -0.6(5) . . . . S17A C18A C19A C20A 177.9(3) . . . . C2A C1A C20A C19A 178.6(3) . . . . C21A C1A C20A C19A -0.1(5) . . . . C2A C1A C20A C12A -0.4(5) . . . . C21A C1A C20A C12A -179.1(3) . . . . C18A C19A C20A C1A -179.1(3) . . . . C18A C19A C20A C12A -0.1(5) . . . . C11A C12A C20A C1A -0.2(5) . . . . C13A C12A C20A C1A 179.6(3) . . . . C11A C12A C20A C19A -179.2(3) . . . . C13A C12A C20A C19A 0.6(5) . . . . C22A Si1A C23A C24A 70.6(10) . . . . C27A Si1A C23A C24A -176.7(9) . . . . C31A Si1A C23A C24A -45.7(12) . . . . C22A Si1A C23A C25A -49.1(11) . . . . C27A Si1A C23A C25A 63.6(11) . . . . C31A Si1A C23A C25A -165.4(11) . . . . C24A C23A C25A C26A 58.6(16) . . . . Si1A C23A C25A C26A 175.1(11) . . . . C24C C23C C25C C26C -50.6(16) . . . . Si1A C23C C25C C26C -175.0(12) . . . . C22A Si1A C27A C29A -59.0(9) . . . . C23A Si1A C27A C29A -170.7(10) . . . . C31A Si1A C27A C29A 57.7(12) . . . . C22A Si1A C27A C28A 141.6(10) . . . . C23A Si1A C27A C28A 29.9(12) . . . . C31A Si1A C27A C28A -101.7(13) . . . . C28A C27A C29A C30A -36(3) . . . . Si1A C27A C29A C30A 165(3) . . . . C31C Si1A C27C C29C 93.4(17) . . . . C22A Si1A C27C C29C -27.5(12) . . . . C23C Si1A C27C C29C -145.8(12) . . . . C31C Si1A C27C C28C -54.0(18) . . . . C22A Si1A C27C C28C -174.9(12) . . . . C23C Si1A C27C C28C 66.8(14) . . . . C28C C27C C29C C30C -15(6) . . . . Si1A C27C C29C C30C -158(5) . . . . C32A C31A C33A C34A 69.9(19) . . . . Si1A C31A C33A C34A -173.5(15) . . . . C22A Si1A C31C C32C 48(3) . . . . C27C Si1A C31C C32C -70(3) . . . . C23C Si1A C31C C32C 163(3) . . . . C22A Si1A C31C C33C -143(2) . . . . C27C Si1A C31C C33C 99(2) . . . . C23C Si1A C31C C33C -28(3) . . . . C32C C31C C33C C34C -9(4) . . . . Si1A C31C C33C C34C -180(3) . . . . C20B C1B C2B C3B -179.9(4) . . . . C21B C1B C2B C3B 6.7(6) . . . . C20B C1B C2B C10B 0.6(6) . . . . C21B C1B C2B C10B -172.8(4) . . . . C1B C2B C3B C4B -176.8(4) . . . . C10B C2B C3B C4B 2.7(6) . . . . C2B C3B C4B C8B -1.9(6) . . . . C2B C3B C4B S5B 179.2(3) . . . . C3B C4B S5B C6B -179.7(4) . . . . C8B C4B S5B C6B 1.2(3) . . . . C4B S5B C6B C7B -0.8(4) . . . . S5B C6B C7B C8B 0.1(5) . . . . C3B C4B C8B C9B 1.1(6) . . . . S5B C4B C8B C9B -179.8(3) . . . . C3B C4B C8B C7B 179.5(4) . . . . S5B C4B C8B C7B -1.4(5) . . . . C6B C7B C8B C9B 179.1(4) . . . . C6B C7B C8B C4B 0.9(6) . . . . C4B C8B C9B C10B -1.1(6) . . . . C7B C8B C9B C10B -179.2(4) . . . . C8B C9B C10B C11B 179.5(4) . . . . C8B C9B C10B C2B 2.0(6) . . . . C1B C2B C10B C11B -0.7(6) . . . . C3B C2B C10B C11B 179.8(4) . . . . C1B C2B C10B C9B 176.8(4) . . . . C3B C2B C10B C9B -2.7(6) . . . . C9B C10B C11B C12B -177.8(4) . . . . C2B C10B C11B C12B -0.3(6) . . . . C10B C11B C12B C13B 179.0(4) . . . . C10B C11B C12B C20B 1.3(6) . . . . C11B C12B C13B C14B -178.5(4) . . . . C20B C12B C13B C14B -0.7(6) . . . . C12B C13B C14B C18B 0.2(6) . . . . C12B C13B C14B C15B -179.0(4) . . . . C13B C14B C15B C16B 178.1(4) . . . . C18B C14B C15B C16B -1.1(5) . . . . C14B C15B C16B S17B 1.5(5) . . . . C15B C16B S17B C18B -1.3(4) . . . . C13B C14B C18B C19B 0.5(6) . . . . C15B C14B C18B C19B 179.8(4) . . . . C13B C14B C18B S17B -179.2(3) . . . . C15B C14B C18B S17B 0.1(4) . . . . C16B S17B C18B C19B -179.1(4) . . . . C16B S17B C18B C14B 0.6(3) . . . . C14B C18B C19B C20B -0.6(6) . . . . S17B C18B C19B C20B 179.0(3) . . . . C2B C1B C20B C19B -179.3(4) . . . . C21B C1B C20B C19B -5.8(6) . . . . C2B C1B C20B C12B 0.4(6) . . . . C21B C1B C20B C12B 174.0(4) . . . . C18B C19B C20B C1B 179.8(4) . . . . C18B C19B C20B C12B 0.0(6) . . . . C11B C12B C20B C1B -1.4(6) . . . . C13B C12B C20B C1B -179.1(4) . . . . C11B C12B C20B C19B 178.4(4) . . . . C13B C12B C20B C19B 0.6(6) . . . . C24B C23B C25B C26B 12(3) . . . . Si1B C23B C25B C26B 128(2) . . . . C24D C23D C25D C26D 2(4) . . . . Si1B C23D C25D C26D -116(3) . . . . C22B Si1B C27B C29B -77.9(10) . . . . C23B Si1B C27B C29B 51.0(11) . . . . C31B Si1B C27B C29B 172.2(10) . . . . C22B Si1B C27B C28B 49.0(11) . . . . C23B Si1B C27B C28B 178.(1) . . . . C31B Si1B C27B C28B -60.9(12) . . . . C28B C27B C29B C30B -26(3) . . . . Si1B C27B C29B C30B 97(2) . . . . C31D Si1B C27D C29D 160.2(17) . . . . C22B Si1B C27D C29D -68.4(13) . . . . C23D Si1B C27D C29D 43.0(14) . . . . C31D Si1B C27D C28D -63.2(16) . . . . C22B Si1B C27D C28D 68.3(12) . . . . C23D Si1B C27D C28D 179.6(12) . . . . C28D C27D C29D C30D 123(3) . . . . Si1B C27D C29D C30D -107(3) . . . . C32B C31B C33B C34B -62(3) . . . . Si1B C31B C33B C34B 173.4(16) . . . . C22B Si1B C31D C33D 52(3) . . . . C27D Si1B C31D C33D 178(3) . . . . C23D Si1B C31D C33D -69(3) . . . . C22B Si1B C31D C32D -88(2) . . . . C27D Si1B C31D C32D 38(2) . . . . C23D Si1B C31D C32D 150.5(18) . . . . C32D C31D C33D C34D 93(4) . . . . Si1B C31D C33D C34D -46(4) . . . .