#------------------------------------------------------------------------------ #$Date: 2019-10-11 11:54:38 +0300 (Fri, 11 Oct 2019) $ #$Revision: 219290 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/23/45/7234557.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7234557 loop_ _publ_author_name 'Maciej Ptak' 'Miroslaw Maczka' 'Anna Gagor' 'Pawel Gluchowski' 'Lucyna Macalik' _publ_section_title ; Synthesis, structure and optical properties of two novel luminescent polar dysprosium metal-organic frameworks: [(CH3)2NH2][Dy(HCOO)4] and [N2H5][Dy(HCOO)4] ; _journal_name_full 'Journal of Materials Chemistry C' _journal_page_first 1019 _journal_page_last 1028 _journal_paper_doi 10.1039/C5TC04264J _journal_volume 4 _journal_year 2016 _chemical_formula_sum 'C4 H9 Dy N2 O8' _chemical_formula_weight 375.63 _space_group_crystal_system orthorhombic _space_group_IT_number 29 _space_group_name_Hall 'P 2c -2ac' _space_group_name_H-M_alt 'P c a 21' _atom_sites_solution_hydrogens mixed _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 18.3359(5) _cell_length_b 6.60183(17) _cell_length_c 7.6049(2) _cell_measurement_reflns_used 7306 _cell_measurement_temperature 298(2) _cell_measurement_theta_max 27.6961 _cell_measurement_theta_min 2.8939 _cell_volume 920.58(4) _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _diffrn_ambient_temperature 298(2) _diffrn_detector_area_resol_mean 8.4350 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Xcalibur, Sapphire1, long nozzle' _diffrn_radiation_monochromator graphite _diffrn_radiation_source 'Enhance (Mo) X-ray Source' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.7107 _diffrn_reflns_av_R_equivalents 0.0254 _diffrn_reflns_av_unetI/netI 0.0181 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_k_max 8 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_l_max 9 _diffrn_reflns_limit_l_min -9 _diffrn_reflns_number 7972 _diffrn_reflns_point_group_measured_fraction_full 0.986 _diffrn_reflns_point_group_measured_fraction_max 0.986 _diffrn_reflns_theta_full 25.674 _diffrn_reflns_theta_max 25.674 _diffrn_reflns_theta_min 3.086 _exptl_absorpt_coefficient_mu 8.147 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.31586 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro, Oxford Diffraction Ltd., Version 1.171.34.44 (release 25-10-2010 CrysAlis171 .NET) (compiled Oct 25 2010,18:11:34) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_density_diffrn 2.710 _exptl_crystal_description prism _exptl_crystal_F_000 708 _exptl_crystal_size_max 0.18 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.14 _refine_diff_density_max 0.507 _refine_diff_density_min -0.528 _refine_diff_density_rms 0.093 _refine_ls_abs_structure_details ; Flack x determined using 745 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.032(11) _refine_ls_extinction_coef 0.0087(4) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2014/7 (Sheldrick 2014' _refine_ls_goodness_of_fit_ref 1.116 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 143 _refine_ls_number_reflns 1715 _refine_ls_number_restraints 6 _refine_ls_restrained_S_all 1.114 _refine_ls_R_factor_all 0.0151 _refine_ls_R_factor_gt 0.0147 _refine_ls_shift/su_max 0.039 _refine_ls_shift/su_mean 0.002 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0230P)^2^+0.0900P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0375 _refine_ls_wR_factor_ref 0.0377 _reflns_Friedel_coverage 0.823 _reflns_Friedel_fraction_full 0.971 _reflns_Friedel_fraction_max 0.971 _reflns_number_gt 1689 _reflns_number_total 1715 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file J-Mater-Chem-C-2016-4-1019.cif _cod_data_source_block nc2 _cod_original_cell_volume 920.57(4) _cod_database_code 7234557 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; nc.res created by SHELXL-2014/7 TITL hydrazyna_Y_k1a in Pca2(1) REM Pca2(1) (#29 in standard setting) CELL 0.71073 18.335873 6.601833 7.604884 90.0000 90.0000 90.0000 ZERR 4.00 0.000535 0.000168 0.000207 0.0000 0.0000 0.0000 LATT -1 SYMM -x,-y, z+1/2 SYMM x+1/2,-y, z SYMM -x+1/2, y, z+1/2 SFAC C H N O Dy UNIT 16 36 8 32 4 L.S. 16 BOND FMAP 2 PLAN 20 shel 10 0.82 acta 56 WGHT 0.023000 0.090000 EXTI 0.008710 FVAR 1.31907 MOLE 1 DY1 5 0.601978 0.204057 0.444670 11.00000 0.01121 0.01051 = 0.01452 0.00027 0.00049 0.00079 O1 4 0.719249 0.195022 0.583929 11.00000 0.01623 0.02911 = 0.05989 0.01429 -0.01510 0.00030 O2 4 0.585731 0.176460 0.752568 11.00000 0.02492 0.02141 = 0.01850 0.00143 0.00312 -0.00603 O3 4 0.652788 0.532067 0.490867 11.00000 0.02861 0.01039 = 0.03758 -0.00124 -0.00671 -0.00027 O4 4 0.572804 0.406276 0.187184 11.00000 0.01857 0.02205 = 0.02177 0.00529 -0.00371 0.00336 O5 4 0.677813 0.116867 0.217569 11.00000 0.01983 0.04159 = 0.03195 -0.00171 0.01061 0.00458 O6 4 0.494346 0.394219 0.518814 11.00000 0.02103 0.02888 = 0.02172 -0.00710 0.00002 0.00913 O7 4 0.624669 -0.143750 0.517100 11.00000 0.03592 0.01108 = 0.03409 0.00100 0.00150 0.00187 O8 4 0.490821 -0.024257 0.803400 11.00000 0.02666 0.02429 = 0.03005 0.00275 -0.00003 -0.00939 C1 1 0.638397 0.705693 0.427899 11.00000 0.02698 0.01819 = 0.02007 -0.00119 -0.00553 -0.00173 AFIX 43 H1 2 0.638235 0.719894 0.306233 11.00000 -1.20000 AFIX 0 C2 1 0.512958 0.477179 0.136593 11.00000 0.01729 0.02588 = 0.01747 0.00247 0.00069 0.00257 AFIX 43 H2 2 0.470915 0.429945 0.191348 11.00000 -1.20000 AFIX 0 C3 1 0.736072 0.077693 0.145806 11.00000 0.02047 0.01990 = 0.03770 0.00204 0.00783 0.00489 AFIX 43 H3 2 0.747728 -0.059068 0.137435 11.00000 -1.20000 AFIX 0 C4 1 0.543607 0.076136 0.851169 11.00000 0.02645 0.01775 = 0.01561 0.00092 0.00252 -0.00087 AFIX 43 H4 2 0.553513 0.078574 0.971085 11.00000 -1.20000 AFIX 0 MOLE 2 N1 3 0.679906 0.470369 0.927756 11.00000 0.03099 0.03267 = 0.03060 -0.00728 -0.00532 -0.00087 AFIX 133 H1A 2 0.727888 0.452506 0.936211 11.00000 -1.50000 H1B 2 0.662600 0.395636 0.839744 11.00000 -1.50000 H1C 2 0.658695 0.432879 1.027863 11.00000 -1.50000 AFIX 0 DFIX 0.91 0.002 N2 H2A N2 H2B dfix 1.49 0.001 H2a H2b dfix 2.0 0.001 H1b H2b dfix 2.0 0.001 H2a H1c N2 3 0.664753 0.678595 0.894862 11.00000 0.03909 0.03897 = 0.03898 0.01315 -0.00469 0.00012 H2A 2 0.622252 0.704803 0.952260 11.00000 -1.20000 H2B 2 0.657942 0.689471 0.776743 11.00000 -1.20000 HKLF 4 REM hydrazyna_Y_k1a in Pca2(1) REM R1 = 0.0147 for 1689 Fo > 4sig(Fo) and 0.0151 for all 1715 data REM 143 parameters refined using 6 restraints END WGHT 0.0227 0.0000 REM Highest difference peak 0.507, deepest hole -0.528, 1-sigma level 0.093 Q1 1 0.6015 0.1180 0.5779 11.00000 0.05 0.51 Q2 1 0.6007 0.2799 0.3077 11.00000 0.05 0.50 Q3 1 0.6024 0.1182 0.3117 11.00000 0.05 0.48 Q4 1 0.6009 0.2826 0.5831 11.00000 0.05 0.47 Q5 1 0.6113 0.0238 0.4485 11.00000 0.05 0.35 Q6 1 0.5767 0.3644 0.4418 11.00000 0.05 0.33 Q7 1 0.6256 0.3561 0.4418 11.00000 0.05 0.33 Q8 1 0.4580 -0.1174 0.8468 11.00000 0.05 0.33 Q9 1 0.4888 -0.1085 0.9397 11.00000 0.05 0.28 Q10 1 0.6941 0.6548 1.0594 11.00000 0.05 0.27 Q11 1 0.7017 0.6716 0.8591 11.00000 0.05 0.27 Q12 1 0.6289 0.8791 0.8861 11.00000 0.05 0.27 Q13 1 0.6589 0.6068 0.9401 11.00000 0.05 0.27 Q14 1 0.7007 0.7199 0.9504 11.00000 0.05 0.26 Q15 1 0.5451 0.0971 0.5447 11.00000 0.05 0.26 Q16 1 0.6135 0.0800 0.9435 11.00000 0.05 0.25 Q17 1 0.6583 0.1217 0.3445 11.00000 0.05 0.24 Q18 1 0.5982 0.2826 0.1523 11.00000 0.05 0.24 Q19 1 0.6069 0.5314 0.8747 11.00000 0.05 0.23 Q20 1 0.5943 0.3262 0.7346 11.00000 0.05 0.23 ; _shelx_res_checksum 89447 _shelx_hkl_file ; 0 0 -9-163.826 80.3392 8 0 0 -9 4.01549 27.7353 4 0 0 -8 17271.4 631.541 8 0 0 -8 16727.0 453.724 4 0 0 -7 30.6392 52.5665 8 0 0 -7 26.2752 28.1037 4 0 0 -6 29043.4 776.542 8 0 0 -6 29371.4 611.165 4 0 0 -5 6.44941 18.6029 4 0 0 -5 1468.56 135.256 8 0 0 -4 64751.3 1059.51 9 0 0 -4 63728.6 1108.66 4 0 0 -3 33.4737 11.3575 9 0 0 -3 35.8410 33.0381 8 0 0 -3 37.6905 17.2676 4 0 0 -2 68056.9 1263.59 8 0 0 -2 74234.7 1190.31 4 0 0 2 82317.3 1257.60 10 0 0 2 71549.9 1262.90 1 0 0 3 25.9125 15.4210 1 0 0 3 172.269 23.1246 10 0 0 4 69725.3 1162.31 10 0 0 4 66844.4 1174.02 1 0 0 5 123.528 25.7598 10 0 0 6 29292.8 591.917 10 0 0 7 39.1217 27.4925 10 0 0 8 15881.3 412.476 10 0 0 9 18.0966 40.8100 10 0 -1 -9 10.3898 75.8388 8 0 1 -9 8.94314 29.1300 4 0 1 -9 82.9663 79.4167 8 0 -1 -8 1866.01 204.837 8 0 1 -8 1800.73 127.990 4 0 1 -8 2039.52 203.983 8 0 -1 -7 32.5132 29.0406 4 0 1 -7 9.57886 25.6753 4 0 1 -7-15.1951 45.5841 8 0 -1 -7 8.94496 55.4376 8 0 1 -6 3466.75 228.973 8 0 -1 -6 3230.58 147.485 4 0 -1 -6 3326.96 229.216 8 0 1 -6 3370.14 147.521 4 0 -1 -5 9.89740 18.5729 4 0 1 -5-9.92560 18.5086 4 0 1 -5 68.6740 29.9102 3 0 -1 -5 18.0699 40.2732 8 0 1 -5-7.61176 18.1815 9 0 1 -4 146.328 22.4287 9 0 1 -4 159.708 27.6418 4 0 1 -4 130.473 25.6070 3 0 -1 -4 155.369 52.9681 8 0 -1 -3 38.4874 44.1348 7 0 1 -3 15.2118 14.3089 4 0 1 -3 16.1066 11.9280 1 0 1 -3 39.6258 18.6661 3 0 -1 -3 5.39991 11.9315 4 0 -1 -3 54.2656 37.4193 8 0 1 -3 13.6389 12.8461 9 0 -1 -2 5568.81 185.735 8 0 1 -2 5414.46 122.597 9 0 1 -2 5359.93 130.520 4 0 1 -2 5431.96 130.035 1 0 1 -2 5411.10 128.386 3 0 -1 -2 5156.94 181.796 7 0 1 -1 48.3893 11.2140 9 0 1 -1 40.4456 11.3303 3 0 -1 -1 96.7557 25.3226 7 0 -1 -1 59.4500 12.5081 6 0 -1 0 4852.34 76.8467 6 0 -1 0 3133.97 81.2331 2 0 1 1 31.1129 10.6946 6 0 1 2 3538.38 94.3321 10 0 -1 2 3548.17 85.6902 10 0 1 3 13.4400 14.9269 10 0 -1 3 25.4169 12.6636 10 0 -1 3 20.0326 16.5013 1 0 1 4 534.233 43.8414 10 0 -1 4 500.652 45.7987 1 0 -1 4 449.909 37.5476 10 0 -1 5 23.0079 19.0990 10 0 1 5 39.7001 22.1101 10 0 1 6 2943.39 131.827 10 0 -1 6 2994.67 124.960 10 0 -1 7-11.0663 26.3265 10 0 1 7-17.5390 31.5632 10 0 -1 8 1930.81 120.357 10 0 1 8 2014.58 128.377 10 0 -1 9 33.0529 39.7992 10 0 1 9 28.3956 43.1978 10 0 2 -9 53.1567 36.2796 4 0 2 -9 35.5422 61.0771 8 0 -2 -9 57.9360 70.1068 8 0 -2 -8 11357.3 534.133 8 0 2 -8 12084.8 370.774 4 0 2 -7-14.1813 30.7416 4 0 -2 -7 12.1077 64.7243 8 0 2 -6 26321.0 574.819 4 0 2 -6 27263.1 595.556 3 0 2 -6 27376.4 541.718 9 0 2 -5 20.6518 21.0366 4 0 2 -5 37.3028 23.2796 3 0 2 -5 7.82574 18.2232 9 0 -2 -5 27.3911 45.5762 7 0 -2 -5 21.1208 51.7680 8 0 2 -4 30544.6 562.284 9 0 2 -4 31172.2 585.191 4 0 -2 -4 28109.5 714.853 8 0 -2 -4 27862.5 712.992 7 0 2 -4 30422.5 581.379 3 0 2 -3 11.3050 14.6372 4 0 2 -3 18.5572 13.6564 1 0 2 -3 15.7725 15.6315 9 0 2 -3 15.8769 16.0418 3 0 -2 -3 32.0971 33.0609 8 0 -2 -3 49.6659 38.4622 7 0 2 -2 47408.8 800.275 4 0 2 -2 47307.8 796.698 9 0 2 -2 47802.5 803.580 3 0 2 -1 46.3620 16.7188 3 0 -2 -1 21.7607 24.4352 7 0 2 -1 20.8181 13.2241 9 0 -2 -1 25.4842 15.4856 6 0 2 0 29421.6 508.420 6 0 2 0 29798.5 486.296 9 0 -2 0 24524.4 560.369 7 0 -2 0 27110.8 497.950 6 0 -2 0 25806.6 531.073 2 0 2 0 29420.9 497.663 3 0 -2 1 31.2075 18.5241 6 0 2 1 27.1998 16.9235 2 0 2 1 72.4712 17.2102 6 0 2 1 22.2234 8.54902 9 0 2 2 48129.0 836.168 6 0 -2 2 48258.3 802.860 10 0 2 3 4.05198 13.5349 10 0 2 3 22.5682 13.4069 6 0 -2 4 28970.5 536.114 10 0 2 4 30003.8 562.605 10 0 2 5 16.6881 21.4219 10 0 -2 5 2.99056 16.0326 10 0 2 6 23927.9 513.671 10 0 -2 6 23178.1 483.722 10 0 2 7 38.5100 32.7259 10 0 2 8 12448.2 367.372 10 0 2 9 6.22954 45.1125 10 0 -3 -8 6277.53 392.060 8 0 3 -8 6191.76 252.456 4 0 3 -7-1.77590 24.0048 4 0 3 -7 66.9074 30.0541 9 0 -3 -7 63.7384 72.9243 8 0 3 -6 17278.9 422.171 4 0 3 -6 16907.3 397.882 9 0 3 -6 17325.7 430.111 3 0 3 -5 101.058 30.1590 4 0 3 -5-9.18823 24.1531 9 0 -3 -5 36.1598 49.6586 7 0 3 -5 38.1305 22.6624 3 0 3 -4 28720.2 568.151 4 0 3 -4 29171.4 574.637 3 0 -3 -4 26887.1 710.653 7 0 3 -4 28727.2 559.904 9 0 3 -3 14.0849 14.7101 4 0 3 -3 7.54184 15.4134 9 0 3 -3 17.5281 15.3841 1 0 -3 -3 26.0379 33.0431 7 0 3 -3 8.50441 15.6003 3 0 3 -2 28135.5 530.606 9 0 -3 -2 29419.8 552.473 6 0 3 -2 29440.3 544.607 3 0 -3 -1 8.25452 14.6355 6 0 3 -1 18.2932 14.5885 3 0 3 -1 5.93682 14.1458 9 0 -3 0 58028.8 932.886 5 0 3 0 58274.8 956.489 9 0 3 0 59098.5 974.865 3 0 3 0 60529.8 1001.77 6 0 3 1 7.15223 8.46057 9 0 3 1 13.4434 12.1327 3 0 -3 1 18.6981 8.47529 10 0 -3 1 17.8447 10.0365 5 0 3 1 1.75797 13.8273 6 0 -3 1 51.8167 18.0197 6 0 -3 1 1.97332 30.2008 7 0 -3 2 29731.3 572.608 10 0 -3 2 30765.6 609.847 6 0 3 2 33964.1 622.271 2 0 -3 2 31154.1 580.475 5 0 3 2 32118.0 539.838 9 0 3 2 33382.6 603.266 6 0 -3 3-3.58634 14.5324 10 0 3 3-2.10258 14.3234 10 0 3 4 30071.7 581.574 10 0 3 5 28.2754 27.5636 10 0 3 6 16018.7 390.219 10 0 3 7-20.3435 32.7813 10 0 3 8 7254.92 270.615 10 0 4 -8 2520.22 157.065 4 0 4 -7-20.1786 36.3585 9 0 4 -7-12.7412 29.0038 4 0 4 -6 9719.36 288.174 9 0 4 -6 9800.72 306.337 3 0 4 -6 9687.58 296.799 4 0 -4 -6 9082.94 437.324 7 0 4 -5-3.53094 20.8231 4 0 -4 -5 11.7662 59.8940 7 0 4 -5 12.4079 27.8950 9 0 4 -5 7.82994 22.4767 3 0 -4 -4 5629.10 289.133 7 0 4 -4 5866.29 190.955 4 0 4 -4 5685.12 188.843 9 0 4 -4 5620.34 196.306 3 0 4 -3 6.07430 15.6427 4 0 4 -3 8.17107 20.8760 9 0 -4 -3 43.1643 52.1252 7 0 4 -3 66.7935 26.5282 3 0 4 -2 12622.2 301.533 3 0 4 -2 12293.9 290.364 9 0 -4 -2 13049.0 415.390 7 0 -4 -1 15.9438 37.5931 7 0 4 -1 3.02294 15.5316 3 0 4 -1 14.6330 15.7359 9 0 4 0 4991.60 143.245 9 0 -4 0 5516.92 189.514 2 0 4 0 5051.54 157.343 3 0 4 0 5567.51 183.975 6 0 -4 0 5010.43 121.649 5 0 -4 0 5125.11 236.820 7 0 -4 0 5060.22 162.058 6 0 4 1 11.0911 13.4998 9 0 -4 1 31.2887 40.6167 7 0 4 1 1.11017 17.1385 3 0 -4 1 18.7306 15.2673 6 0 -4 2 11374.8 291.645 6 0 4 2 11959.2 335.333 2 0 -4 2 10860.2 376.290 7 0 4 2 11922.5 240.017 9 0 4 3 5.41584 15.0091 10 0 4 4 4905.19 164.170 10 0 4 5 5.50799 22.1526 10 0 4 6 9400.09 280.436 10 0 4 7 24.7461 35.4459 10 0 4 8 2702.25 162.696 10 0 5 -8 11328.5 363.230 9 0 5 -8 10619.1 364.901 4 0 -5 -7-17.1946 79.2087 7 0 5 -7-34.0947 45.8858 9 0 5 -7 43.4128 32.2318 4 0 5 -7 87.3533 34.1979 3 0 -5 -6 18347.8 680.033 7 0 5 -6 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5 24629.8 500.072 10 -2 -2 5 23467.4 480.611 10 2 -2 5 24121.5 465.305 10 2 2 6 1916.59 107.829 10 -2 2 6 1891.15 107.390 10 -2 -2 6 1788.38 97.1086 10 2 2 7 17076.7 424.583 10 -2 2 7 17423.7 431.788 10 -2 -2 7 16765.3 408.314 10 -2 2 8 841.239 89.7476 10 2 2 8 784.369 82.9825 10 2 2 9 9674.22 333.762 10 -2 2 9 9677.63 335.423 10 2 3 -9 5029.42 237.440 4 2 -3 -8 246.445 104.629 8 2 3 -8 228.810 50.1925 4 -2 -3 -8 229.366 107.446 8 -2 3 -8 141.759 39.7980 4 -2 3 -7 8254.73 252.675 9 2 3 -7 8252.35 300.865 3 2 3 -7 8330.85 275.470 4 2 3 -7 7915.92 252.853 9 -2 3 -7 7990.37 279.893 4 -2 3 -6 1778.87 108.613 3 2 -3 -6 1598.26 172.393 7 -2 3 -6 1683.97 110.372 4 2 3 -6 1703.95 105.217 4 2 3 -6 1614.13 112.169 3 2 3 -6 1627.87 99.2091 9 -2 3 -6 1550.62 94.1639 9 -2 -3 -6 1819.16 180.265 7 -2 -3 -5 12337.8 454.799 7 2 3 -5 12384.5 314.191 4 -2 3 -5 12657.3 307.929 9 2 3 -5 12307.2 308.647 9 -2 3 -5 12154.2 312.321 3 2 -3 -5 12433.6 454.032 7 -2 3 -5 12243.7 323.711 4 2 3 -5 12437.7 331.574 3 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481.166 7 8 5 -6 2002.67 137.387 9 -8 5 -6 1967.46 130.896 9 -8 5 -6 2279.86 162.919 4 8 -5 -6 1955.42 184.072 7 -8 -5 -6 1998.33 188.579 7 8 5 -6 1863.34 145.686 3 8 5 -5 15701.8 425.999 9 -8 5 -5 15461.8 416.455 9 -8 5 -5 16405.7 477.085 4 8 -5 -5 16525.8 542.820 7 -8 -5 -5 16120.2 542.502 7 8 5 -5 16266.3 461.824 3 8 5 -4 2396.71 146.378 3 8 5 -4 2115.51 126.168 9 -8 5 -4 2218.10 128.512 9 -8 5 -4 2041.16 124.381 3 8 -5 -4 2373.52 177.430 7 -8 -5 -4 2141.01 169.749 7 8 5 -3 22679.0 517.164 9 -8 5 -3 22741.6 523.111 9 -8 5 -3 22879.5 526.376 3 8 -5 -3 22370.5 522.425 5 8 -5 -3 24628.5 638.500 7 -8 -5 -3 24313.6 642.195 7 8 5 -3 23362.0 547.266 3 8 5 -2 6988.38 225.234 9 -8 5 -2 6892.18 231.012 9 8 -5 -2 7603.14 302.299 7 -8 -5 -2 7387.52 300.413 7 8 -5 -2 6996.36 233.924 5 -8 5 -2 6936.46 234.459 3 8 5 -2 7257.61 241.931 3 8 5 -1 27467.2 574.179 3 8 -5 -1 28509.2 674.367 7 -8 5 -1 26132.6 583.779 3 8 5 -1 26202.8 554.843 9 -8 5 -1 25633.1 563.530 9 8 -5 -1 26203.1 577.874 5 -8 -5 -1 27644.6 579.577 10 -8 -5 -1 26816.2 666.950 7 8 5 0 5192.15 181.032 3 8 5 0 5210.47 176.443 9 -8 5 0 4793.46 181.040 9 -8 -5 0 5503.56 197.986 10 8 -5 0 5128.82 199.518 5 -8 -5 0 5397.48 241.072 7 8 -5 0 5365.81 237.793 7 8 5 1 27636.3 554.722 3 -8 5 1 26587.8 569.296 9 -8 -5 1 27747.1 602.495 10 8 -5 1 25970.5 610.405 5 -8 -5 1 27176.7 671.190 7 -8 5 2 6628.74 212.584 9 8 -5 2 6472.28 256.175 5 8 -5 2 7608.44 296.770 7 -8 -5 2 6928.35 287.194 7 8 -5 3 25036.2 657.052 7 -8 -5 3 25050.9 657.228 7 8 -5 4 2799.72 192.684 7 -8 -5 4 2446.21 178.405 7 8 -6 -6 43.5414 50.8421 7 -8 -6 -6-18.2044 71.9345 7 8 -6 -5 686.199 117.488 7 -8 -6 -5 508.711 102.834 7 8 6 -5 597.541 77.8550 9 -8 6 -5 585.458 79.9303 9 -8 6 -5 633.391 89.4609 4 8 6 -5 626.559 86.4968 3 -8 -6 -4 49.9633 42.0788 7 8 -6 -4 32.8090 40.8496 7 8 6 -4 157.300 46.5183 3 8 6 -4 10.9779 29.7528 9 -8 6 -4 14.5115 29.6213 9 -8 6 -4 37.3091 26.5150 3 -8 -6 -3 790.181 115.142 7 8 6 -3 555.597 67.9797 9 -8 6 -3 557.678 69.5619 9 8 -6 -3 796.050 112.801 7 8 6 -3 538.193 70.3162 3 -8 6 -3 607.584 71.9883 3 8 -6 -3 760.994 75.5907 5 -8 6 -2 95.1514 36.9782 3 8 -6 -2-14.5788 43.9681 7 -8 -6 -2 38.1613 39.4111 7 8 6 -2 36.8295 23.4658 3 -8 6 -2 22.8276 29.4561 9 8 6 -1 747.274 77.0954 3 8 6 -1 594.033 62.6693 9 -8 6 -1 743.367 75.1436 9 8 -6 -1 817.435 107.750 7 -8 -6 -1 607.263 96.1872 7 -8 6 -1 727.421 77.9136 3 8 -6 0 293.614 67.7016 7 -8 -6 0 253.905 63.6843 7 -8 6 0 308.026 51.2697 9 8 6 0 301.750 47.2022 3 -8 6 0 310.642 55.2588 3 -8 6 1 821.666 74.7945 9 8 -6 1 1045.61 117.040 7 -8 -6 1 1059.77 117.149 7 8 -6 2-13.4992 36.8503 7 -8 -6 2 1.31674 41.3908 7 8 -6 3 555.199 95.1342 7 -8 -6 3 639.493 97.1310 7 8 -6 4 108.532 52.4666 7 -8 -6 4 49.2580 53.8560 7 8 -6 5 645.149 113.253 7 -8 -6 5 492.755 95.6162 7 8 -6 6 2.61290 49.2055 7 -8 -6 6 34.2980 48.0343 7 8 7 -4 2259.55 147.667 9 -8 7 -4 2317.58 160.238 3 8 -7 -4 2679.01 221.792 7 -8 -7 -4 2496.95 219.690 7 -8 -7 -3 10568.7 452.652 7 8 7 -3 9157.56 312.936 9 -8 7 -3 9860.34 329.617 9 -8 7 -3 9795.90 342.450 3 8 -7 -3 10894.5 456.541 7 8 7 -3 10693.6 359.625 3 8 7 -2 977.260 97.2232 3 8 7 -2 830.945 83.4085 9 -8 7 -2 946.125 92.9369 9 8 -7 -2 1283.22 146.943 7 -8 -7 -2 948.411 126.216 7 -8 7 -2 902.232 94.5970 3 8 7 -1 14439.3 408.109 3 -8 7 -1 13267.8 386.216 9 8 -7 -1 15331.5 523.976 7 -8 7 -1 13822.3 417.245 3 -8 -7 -1 14686.7 521.853 7 -8 -7 0 1731.25 169.284 7 8 7 0 1803.59 120.505 3 -8 7 0 1684.35 116.401 9 8 -7 0 1917.99 174.202 7 -8 7 0 1639.54 127.324 3 -8 7 1 14126.0 425.533 3 8 -7 1 14083.8 494.790 7 -8 -7 1 13916.6 498.577 7 -8 7 2 1091.04 110.365 3 8 -7 2 1040.88 130.494 7 -8 -7 2 1002.05 127.292 7 8 -7 3 10472.9 440.743 7 -8 -7 3 9854.82 428.087 7 8 -7 4 2394.43 211.593 7 -8 -7 4 1998.46 188.887 7 8 8 -1 5553.11 246.566 3 -8 8 -1 5094.94 226.864 9 -8 -8 -1 5505.54 327.591 7 8 -8 0 627.053 118.576 7 -8 -8 0 667.096 120.154 7 -8 -8 1 4829.94 301.045 7 -9 0 -9 66.8934 36.6009 4 9 0 -9-14.1442 54.2772 8 -9 0 -8-3.08713 31.9358 4 9 0 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16.8791 5 -9 0 4 5.53473 22.7381 10 9 0 4 20.4595 22.3960 5 -9 0 5 39.0541 34.9142 10 -9 0 6 41.0397 34.3447 10 -9 0 7 12.1662 28.9361 10 9 0 7 29.2534 25.6840 10 -9 0 8 41.3466 39.6752 10 9 0 8 44.0697 37.4919 10 -9 -1 -8 3171.87 185.247 4 -9 1 -8 3173.48 189.845 4 9 -1 -8 3350.27 241.198 8 9 1 -8 3217.12 225.424 8 -9 -1 -7 15406.4 431.344 4 -9 1 -7 15377.3 442.484 4 9 -1 -7 15817.9 522.566 8 9 1 -7 15380.7 498.559 8 -9 -1 -6 6607.16 236.422 4 9 1 -6 6501.84 235.625 9 -9 1 -6 6430.86 243.980 4 9 -1 -6 6994.44 300.433 8 9 1 -6 6586.23 282.301 8 -9 1 -6 7027.79 292.737 8 -9 -1 -5 19822.1 454.946 4 9 1 -5 19203.7 461.600 9 -9 1 -5 19053.2 468.127 4 9 -1 -5 19412.6 528.172 8 9 1 -5 19962.1 514.945 8 9 1 -4 13001.2 335.945 9 -9 1 -4 12932.1 298.428 9 -9 1 -4 12818.9 337.290 4 9 -1 -4 13426.6 377.878 8 9 1 -4 13443.8 366.393 8 -9 -1 -4 13413.1 318.249 4 9 -1 -4 12473.8 319.090 5 9 1 -3 29152.2 591.981 9 -9 -1 -3 28593.6 549.305 6 -9 -1 -3 29580.6 551.805 4 -9 1 -3 28836.2 556.521 9 -9 -1 -3 29594.4 546.451 9 -9 -1 -3 27641.9 543.295 1 9 -1 -3 29102.6 608.969 8 9 1 -3 29582.8 599.385 8 9 -1 -3 29070.8 577.191 5 9 1 -3 27902.1 540.672 5 9 1 -2 11346.8 290.751 9 -9 -1 -2 11538.1 258.069 6 -9 -1 -2 10954.5 245.388 4 -9 -1 -2 10740.3 280.626 10 -9 1 -2 11270.1 274.087 9 9 -1 -2 11556.5 288.176 5 9 1 -2 11210.1 268.649 8 9 1 -2 11224.6 254.215 5 -9 -1 -2 11329.1 243.587 1 -9 1 -2 10863.6 255.172 10 9 1 -1 42197.7 815.884 9 -9 1 -1 45941.1 717.613 6 -9 -1 -1 44771.6 793.181 6 -9 1 -1 43244.6 816.109 9 9 1 -1 42016.5 791.196 5 9 -1 -1 43838.6 834.401 5 9 -1 -1 42960.9 750.192 7 -9 -1 -1 42392.2 752.476 7 -9 -1 -1 42123.2 825.118 10 -9 1 -1 42340.1 799.415 10 9 1 0 35990.1 674.621 5 9 -1 0 34396.1 689.561 2 9 -1 0 35825.2 708.965 5 -9 -1 0 34426.5 702.518 10 -9 1 0 34561.1 673.737 10 9 -1 1 44809.2 752.441 7 -9 -1 1 43267.7 755.493 7 -9 1 1 43401.5 802.343 10 9 1 1 43264.5 804.839 5 -9 -1 1 44577.5 863.166 10 -9 -1 1 44028.5 763.184 2 9 -1 1 43223.2 861.202 5 9 1 2 11325.9 246.655 6 9 1 2 11160.7 264.826 5 9 -1 2 10918.3 292.836 5 -9 1 2 10373.8 270.201 2 -9 -1 2 10657.0 291.977 10 -9 1 2 10527.9 261.795 10 9 1 3 26946.6 522.089 6 9 1 3 28802.3 561.913 5 9 -1 3 29690.4 591.427 5 -9 1 3 28966.8 563.185 10 -9 -1 3 27642.9 578.719 10 9 -1 4 13852.0 350.981 5 -9 -1 4 13502.1 346.356 10 -9 1 4 14103.0 340.563 10 9 -1 5 18587.0 452.000 5 -9 -1 5 19334.2 453.189 10 -9 1 5 19261.0 445.689 10 9 -1 6 5847.68 224.178 5 -9 -1 6 5919.73 223.532 10 -9 1 6 5966.12 219.366 10 9 1 7 14541.8 393.444 10 -9 -1 7 14975.5 416.775 10 -9 1 7 15168.6 413.875 10 9 1 8 2952.72 162.700 10 -9 -1 8 3289.95 183.526 10 -9 1 8 2918.94 172.702 10 9 1 9 7339.64 283.782 10 -9 2 -8 518.839 85.6865 4 9 -2 -8 609.602 116.361 8 9 2 -8 567.628 111.353 8 9 2 -7 6060.42 238.569 9 -9 2 -7 6020.90 260.987 4 9 -2 -7 6613.05 325.940 8 9 2 -7 6499.47 306.239 8 -9 2 -7 7131.04 331.420 8 9 2 -6 2540.20 141.325 9 -9 2 -6 2840.62 161.565 4 9 -2 -6 2804.97 193.497 8 9 2 -6 2840.94 183.805 8 9 2 -5 6623.94 226.405 9 -9 2 -5 6331.53 199.000 9 -9 2 -5 6764.50 247.575 4 9 -2 -5 6963.82 286.290 8 9 2 -5 6759.34 268.828 8 9 2 -4 2149.69 115.373 9 -9 2 -4 2040.13 100.016 9 -9 2 -4 2069.49 122.120 4 9 -2 -4 2134.35 135.634 7 -9 -2 -4 2244.34 140.531 7 9 -2 -4 1938.66 108.338 5 9 2 -3 10068.4 273.717 9 -9 2 -3 10072.9 260.106 9 9 2 -3 9873.00 292.900 3 9 -2 -3 9760.28 271.769 5 9 -2 -3 9939.29 290.503 7 -9 -2 -3 10617.8 300.850 7 9 2 -2 2240.65 108.178 9 -9 -2 -2 2356.18 109.377 6 -9 2 -2 2430.65 108.472 9 9 -2 -2 2439.83 118.668 5 9 2 -2 2226.12 113.338 3 9 -2 -2 2404.01 111.818 7 -9 -2 -2 2333.35 111.737 7 -9 -2 -2 2179.64 112.165 10 9 2 -1 10355.0 264.321 9 -9 -2 -1 10272.9 275.022 6 -9 2 -1 10290.6 269.515 9 9 2 -1 10380.6 231.193 5 9 -2 -1 11048.4 297.232 5 9 2 -1 10297.5 262.295 3 -9 -2 -1 10249.4 284.094 10 9 -2 -1 10490.3 251.436 7 -9 -2 -1 10366.6 253.180 7 -9 2 -1 9877.65 240.124 10 -9 -2 0 3077.23 141.206 6 9 2 0 3022.21 122.101 9 -9 2 0 3360.28 92.3561 6 -9 2 0 3151.11 134.845 9 9 2 0 3413.23 122.652 5 -9 -2 0 2910.96 108.117 7 9 -2 0 3308.26 155.341 5 9 2 0 2994.23 112.293 3 -9 -2 0 2934.98 143.953 10 -9 2 0 3043.56 120.416 10 9 -2 0 3068.10 109.297 7 9 2 1 9370.84 247.015 9 9 2 1 9184.99 227.797 5 -9 -2 1 10206.8 300.510 10 9 -2 1 10121.3 300.779 5 -9 2 1 9693.99 276.408 9 9 2 1 9623.31 217.994 3 -9 2 1 8907.54 225.807 10 9 -2 1 9830.73 239.703 7 -9 -2 1 9501.45 240.076 7 -9 -2 2 2209.75 130.186 10 9 2 2 2174.27 99.4465 6 9 2 2 2354.88 95.3755 5 9 -2 2 2224.65 128.463 5 -9 2 2 2232.66 96.2378 10 9 2 3 8129.85 220.611 6 9 -2 3 8488.19 265.534 5 -9 -2 3 8384.91 262.268 10 -9 2 3 8595.25 230.097 10 9 -2 4 2520.30 134.709 5 -9 -2 4 2416.35 129.850 10 -9 2 4 2607.38 119.897 10 9 -2 5 5725.03 217.506 5 -9 -2 5 5638.03 213.112 10 -9 2 5 5762.20 200.709 10 9 -2 6 2284.78 139.238 5 -9 -2 6 2361.06 138.503 10 -9 2 6 2392.09 132.872 10 9 2 7 6071.32 234.583 10 9 -2 7 5901.23 246.055 5 -9 -2 7 5646.46 236.936 10 -9 2 7 6100.33 237.217 10 9 2 8 471.678 72.7658 10 9 -2 8 549.414 81.1272 5 -9 -2 8 547.543 80.2633 10 -9 2 8 536.176 77.9371 10 9 3 -8 946.470 99.1491 9 -9 3 -8 1166.04 120.669 4 9 3 -8 939.928 131.211 8 9 3 -7 5294.91 225.395 9 -9 3 -7 5387.72 251.526 4 9 3 -7 5716.46 294.944 8 9 3 -6 3347.52 167.538 9 -9 3 -6 3865.10 198.980 4 -9 3 -6 3341.73 150.397 9 9 3 -6 3410.50 197.433 3 9 3 -5 11951.3 335.523 9 -9 3 -5 11441.7 312.837 9 -9 3 -5 12267.6 371.802 4 9 3 -5 11858.6 371.341 3 9 -3 -5 12616.1 408.941 7 -9 -3 -5 12850.2 418.736 7 9 3 -4 2402.22 126.576 9 -9 3 -4 2447.92 118.936 9 9 3 -4 2495.31 141.217 3 9 -3 -4 2649.37 158.005 7 -9 -3 -4 2623.42 159.516 7 9 -3 -4 2359.64 126.036 5 9 3 -3 8543.57 248.717 9 -9 3 -3 8031.71 236.863 9 9 -3 -3 8025.51 250.412 5 9 3 -3 8292.44 260.233 3 9 -3 -3 8346.93 274.483 7 -9 -3 -3 8405.59 278.514 7 -9 3 -3 8186.56 224.047 3 9 3 -2 5277.91 180.110 9 -9 3 -2 5256.64 171.199 3 -9 3 -2 5215.02 178.823 9 9 -3 -2 5492.10 198.268 7 9 -3 -2 5114.02 189.630 5 -9 -3 -2 5155.87 189.197 10 9 3 -2 5200.10 183.600 3 -9 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9 -4 4 6116.22 261.989 5 -9 -4 4 6115.91 258.879 10 -9 4 4 5993.41 196.607 10 9 -4 5 15912.2 462.679 5 -9 -4 5 15116.4 451.270 10 -9 4 5 15680.2 388.595 10 9 -4 6 3085.32 184.742 5 -9 4 6 3024.45 153.331 10 9 4 7 8690.40 311.294 10 -9 4 7 8304.66 292.313 10 9 -5 -7 374.290 100.480 7 -9 -5 -7 303.197 96.3711 7 -9 5 -7 168.036 50.1257 9 9 -5 -6 144.948 64.3963 7 -9 -5 -6 32.4643 54.7351 7 9 5 -6 66.5960 43.6130 3 9 5 -6 141.207 47.0280 9 -9 5 -6 105.896 44.1419 9 -9 5 -6 48.8885 29.1770 4 9 -5 -5 180.836 68.3352 7 -9 -5 -5 146.896 64.9179 7 9 5 -5 72.0356 38.0966 3 9 5 -5 187.653 50.9607 9 -9 5 -5 136.963 40.6681 9 -9 5 -5 175.515 48.9253 4 9 -5 -4 294.050 67.1679 7 -9 -5 -4 300.831 65.1163 7 9 5 -4 303.750 59.3335 3 9 5 -4 257.592 52.2770 9 -9 5 -4 290.080 52.8237 9 -9 5 -4 296.095 48.1768 3 9 -5 -4 351.762 56.0968 5 9 5 -3 692.289 71.4213 9 -9 5 -3 661.430 71.4724 9 9 -5 -3 742.771 96.2447 7 -9 5 -3 898.631 76.8126 3 9 -5 -3 696.012 72.6362 5 -9 -5 -3 860.161 104.552 7 9 5 -3 761.570 85.2974 3 9 -5 -2 466.508 73.9801 7 9 5 -2 484.301 58.7062 9 -9 5 -2 512.018 63.2349 9 9 5 -2 465.422 60.9254 3 -9 -5 -2 814.248 94.2759 7 9 -5 -2 455.442 60.3124 5 -9 5 -2 578.615 65.4761 3 -9 5 -1 2103.27 124.816 3 9 5 -1 2005.01 109.906 9 -9 5 -1 2018.54 116.218 9 9 -5 -1 1874.50 119.479 5 -9 -5 -1 2012.50 121.116 10 9 -5 -1 2129.03 146.432 7 -9 -5 -1 2168.33 148.784 7 9 5 -1 1851.18 110.211 3 9 -5 0 48.9661 29.1256 5 -9 -5 0 41.2770 29.7598 10 9 -5 0 19.2632 31.9019 7 -9 -5 0 30.8915 36.8986 7 9 5 0 31.2849 22.6607 3 9 5 0 71.6608 29.9008 9 -9 5 0 52.9170 30.1478 9 -9 5 1 1988.04 112.921 9 -9 -5 1 1897.53 122.798 10 9 -5 1 1917.65 129.142 5 9 -5 1 1930.95 137.441 7 -9 -5 1 1786.81 135.472 7 -9 -5 2 362.412 60.7837 10 -9 -5 2 462.966 74.4019 7 -9 5 2 483.217 57.3912 9 9 -5 2 507.374 71.0493 5 9 -5 2 461.598 74.2380 7 9 -5 3 618.244 81.8661 5 9 -5 3 863.353 101.093 7 -9 -5 3 727.335 92.7583 7 9 -5 4 302.534 68.0816 7 -9 -5 4 253.885 63.7930 7 9 -5 5 221.697 65.8641 7 9 -6 -6 2421.50 214.611 7 -9 -6 -6 2612.53 225.081 7 9 6 -5 9287.00 323.709 9 -9 6 -5 9955.61 331.152 9 -9 6 -5 9965.69 378.653 4 9 -6 -5 9797.77 423.536 7 -9 -6 -5 9773.42 424.864 7 9 6 -5 9567.82 355.510 3 9 6 -4 3351.09 173.854 9 -9 6 -4 3311.54 173.681 9 -9 6 -4 3225.34 176.096 3 9 6 -4 3686.23 197.250 3 9 -6 -4 3533.51 231.876 7 -9 -6 -4 3277.19 226.328 7 -9 -6 -3 11498.3 428.324 7 9 6 -3 10279.1 319.489 9 -9 6 -3 10259.8 325.644 9 -9 6 -3 10159.4 332.907 3 9 -6 -3 10548.4 325.200 5 9 -6 -3 11897.6 428.696 7 9 6 -3 10487.5 344.147 3 9 6 -2 2842.90 146.689 9 -9 6 -2 2917.71 155.053 9 9 -6 -2 3052.70 155.713 5 9 -6 -2 3362.59 210.486 7 -9 6 -2 2978.34 161.181 3 -9 -6 -2 3175.44 207.008 7 9 6 -2 2943.58 159.145 3 9 6 -1 19204.6 473.974 3 9 6 -1 18716.8 453.567 9 -9 6 -1 18572.1 466.871 9 -9 -6 -1 20037.6 479.048 10 9 -6 -1 20243.5 569.325 7 -9 -6 -1 19986.9 572.353 7 -9 6 -1 19240.1 494.809 3 9 6 0 3458.47 157.666 3 -9 6 0 3659.91 183.775 3 -9 6 0 3287.16 158.039 9 9 -6 0 3716.08 214.200 7 -9 -6 0 3408.99 207.043 7 -9 6 1 18532.1 452.533 9 -9 -6 1 19169.5 553.817 7 9 -6 1 20207.4 557.456 7 9 -6 2 3226.70 204.619 7 -9 -6 2 3009.83 199.628 7 9 -6 3 11602.5 422.587 7 -9 -6 3 11109.6 414.961 7 9 -6 4 3460.91 229.815 7 -9 -6 4 3258.96 219.463 7 9 -6 5 10299.2 434.691 7 -9 -6 5 8899.86 395.609 7 9 -6 6 2844.90 231.410 7 -9 -6 6 2550.60 210.066 7 9 -7 -4 707.515 112.590 7 -9 7 -4 792.349 96.4120 3 -9 -7 -4 1057.76 145.723 7 9 7 -3 1842.65 130.383 9 -9 7 -3 1815.98 132.209 9 -9 7 -3 1827.32 139.056 3 9 -7 -3 2122.51 193.067 7 -9 -7 -3 2135.08 195.026 7 9 7 -3 2006.88 145.328 3 9 7 -2 1280.65 105.647 9 -9 7 -2 1481.37 117.664 9 -9 7 -2 1690.38 130.930 3 9 -7 -2 1547.33 158.107 7 -9 -7 -2 1546.47 157.240 7 9 7 -2 1215.32 109.105 3 9 7 -1 2726.05 157.137 3 -9 7 -1 2716.66 155.357 9 9 -7 -1 2971.08 211.145 7 -9 7 -1 2874.77 172.642 3 -9 -7 -1 2837.01 209.970 7 -9 7 0 1241.36 103.677 9 9 -7 0 1608.13 157.074 7 -9 -7 0 1550.27 154.467 7 -9 7 0 1270.07 115.264 3 -9 7 1 2835.58 176.501 3 9 -7 1 2776.96 201.869 7 -9 -7 1 2517.34 195.349 7 9 -7 2 1547.66 154.037 7 -9 -7 2 1507.71 155.564 7 9 -7 3 2127.57 188.308 7 -9 -7 3 1935.98 178.284 7 9 -7 4 1011.21 136.584 7 -9 -7 4 881.228 124.705 7 -9 -8 0 936.037 136.086 7 -10 0 -8 12638.2 410.016 4 10 0 -8 12562.1 475.664 8 -10 0 -7 1780.49 130.034 4 10 0 -7 2287.97 174.945 8 10 0 -6 27567.3 646.736 9 -10 0 -6 28121.9 632.538 4 10 0 -6 27696.8 693.110 8 10 0 -5 533.271 70.3772 9 -10 0 -5 609.436 65.4625 4 10 0 -5 549.171 72.7763 8 10 0 -4 29339.2 638.329 9 -10 0 -4 28624.7 592.825 4 10 0 -4 29081.6 628.195 8 10 0 -4 27971.3 577.460 5 10 0 -3 1440.43 104.677 9 -10 0 -3 1364.78 81.3309 4 -10 0 -3 1453.42 80.3327 9 10 0 -3 1457.62 89.0952 8 10 0 -3 1341.80 80.3990 5 -10 0 -3 1356.68 80.8926 10 10 0 -2 37479.7 764.410 9 -10 0 -2 36341.5 707.218 9 10 0 -2 35869.1 672.389 8 10 0 -2 37634.8 704.463 5 -10 0 -2 36436.8 702.141 10 -10 0 -1 7411.63 178.164 6 -10 0 -1 6759.05 218.177 10 10 0 -1 6970.40 219.720 5 -10 0 0 60397.0 1088.85 10 10 0 0 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10 -1 1 204.387 37.4267 2 10 1 1 203.068 27.9419 2 -10 -1 1 276.501 47.9962 10 -10 1 1 166.023 33.5898 10 -10 1 1 299.247 46.2823 2 -10 -1 1 203.736 27.0184 2 10 1 1 226.543 34.5478 5 10 -1 1 223.279 45.5081 5 10 1 2 4520.06 155.516 5 10 -1 2 4471.78 176.563 5 -10 -1 2 4320.28 174.622 10 -10 1 2 4533.51 156.515 10 10 1 3 1014.58 71.0939 5 10 -1 3 982.201 79.4624 5 -10 -1 3 926.170 78.0128 10 -10 1 3 999.129 72.5244 10 10 1 4 3893.67 153.742 5 10 -1 4 3814.07 163.310 5 -10 -1 4 3829.67 163.856 10 -10 1 4 3833.51 156.465 10 -10 -1 5 201.089 44.6910 10 -10 1 5 234.474 44.8981 10 10 -1 5 229.422 45.1438 5 10 -1 6 2720.05 152.491 5 -10 -1 6 2988.03 157.961 10 -10 1 6 3000.10 154.893 10 -10 1 7 61.4085 37.6107 10 10 1 7 36.1079 34.1991 10 10 -1 7 70.7292 36.6884 5 -10 -1 7 87.4219 47.0383 10 10 1 8 1422.87 114.544 10 10 -1 8 1693.10 136.773 5 -10 -1 8 1631.88 133.120 10 -10 1 8 1622.80 131.288 10 -10 2 -8 8515.89 339.519 4 10 -2 -8 8452.07 396.250 8 10 2 -8 7881.09 361.947 8 10 2 -7 29.0953 37.3718 9 -10 2 -7 31.7469 22.0656 4 10 -2 -7-6.25884 52.0779 8 10 2 -7 65.3123 45.2342 8 10 2 -6 13377.5 379.079 9 -10 2 -6 13057.8 399.808 4 10 -2 -6 14003.3 457.551 8 10 2 -6 13580.4 433.887 8 10 2 -5 879.569 81.3504 9 -10 2 -5 1000.92 73.3726 9 -10 2 -5 910.154 89.6019 4 10 2 -5 897.208 94.1549 8 10 2 -4 24818.9 532.715 9 -10 2 -4 23502.8 496.059 9 -10 2 -4 23589.9 548.410 4 -10 -2 -3 205.690 40.9028 7 10 2 -3 145.526 37.0637 9 -10 2 -3 165.303 33.5246 9 10 2 -3 176.764 43.1355 3 -10 -2 -3 178.383 36.9334 10 10 -2 -3 175.306 37.8137 5 10 2 -2 30257.2 611.097 9 -10 -2 -2 29676.7 601.780 6 -10 2 -2 29627.0 599.331 9 10 2 -2 29359.9 619.010 3 10 -2 -2 30405.8 630.603 5 -10 -2 -2 29893.7 622.232 10 10 2 -1 1793.18 98.3794 9 -10 -2 -1 1848.23 103.334 6 -10 2 -1 1863.04 103.200 9 -10 -2 -1 1816.18 110.866 10 10 2 -1 1804.98 83.0874 5 10 -2 -1 1836.33 113.598 5 10 2 -1 1972.59 101.653 3 -10 2 -1 1963.14 92.3971 10 -10 -2 0 32223.2 707.877 10 10 2 0 32937.4 660.711 9 -10 -2 0 34054.0 697.518 6 -10 2 0 33467.8 688.164 9 10 2 0 35913.0 657.585 5 10 -2 0 35099.8 725.560 5 10 2 0 33726.0 642.978 3 -10 2 0 34210.4 659.035 10 10 2 1 1820.94 100.899 9 10 2 1 1845.03 89.7105 5 10 -2 1 1955.92 123.876 5 -10 2 1 1896.80 116.372 9 10 2 1 1996.09 84.4287 3 -10 -2 1 1899.28 121.843 10 -10 2 1 1840.78 89.9821 10 10 2 2 29347.9 586.755 6 10 2 2 30063.4 580.157 5 10 -2 2 30864.1 672.397 5 -10 -2 2 30546.7 664.110 10 -10 2 2 30200.6 585.128 10 -10 -2 3 241.570 48.6667 10 10 2 3 286.099 38.2920 5 -10 2 3 366.224 45.2211 10 10 -2 3 329.359 52.3933 5 10 -2 4 23818.4 553.102 5 -10 -2 4 23504.4 546.916 10 -10 2 4 24624.2 522.748 10 10 -2 5 780.939 80.2928 5 -10 -2 5 756.177 79.6379 10 -10 2 5 698.404 69.9200 10 10 -2 6 12594.6 380.653 5 -10 -2 6 12909.0 377.276 10 -10 2 6 13356.9 366.444 10 -10 -2 7 34.8649 36.6496 10 -10 2 7 107.594 40.2067 10 10 -2 7 58.8068 32.4677 5 10 2 8 8723.78 310.718 10 10 -2 8 8817.39 334.018 5 -10 -2 8 8211.94 320.313 10 -10 2 8 9233.09 325.100 10 10 3 -8 5726.82 252.861 9 10 3 -8 5518.88 304.892 8 10 3 -7 115.649 47.5930 9 -10 3 -7 113.931 39.1939 4 10 3 -7 173.490 63.6926 8 10 3 -6 14037.9 396.695 9 -10 3 -6 14738.1 440.011 4 -10 3 -6 13543.9 359.684 9 10 -3 -5 160.797 52.0192 7 -10 -3 -5 113.965 53.9152 7 10 3 -5 49.2245 41.0084 3 10 3 -5 66.0271 38.9514 9 -10 3 -5 76.5272 32.0456 9 -10 3 -5 106.166 42.5055 4 10 3 -4 21651.1 490.314 9 -10 3 -4 20116.9 459.981 9 10 3 -4 21210.7 519.483 3 10 -3 -4 20472.6 523.207 7 -10 -3 -4 21478.7 537.078 7 10 -3 -4 19455.5 482.976 5 10 3 -3 805.046 73.2266 9 -10 3 -3 799.354 70.5058 9 10 -3 -3 837.857 77.1982 5 10 3 -3 764.454 74.4462 3 10 -3 -3 797.141 77.9923 7 -10 -3 -3 745.874 76.5542 7 -10 3 -3 830.527 62.5356 3 10 3 -2 19761.7 445.034 9 -10 3 -2 19394.9 442.483 9 -10 -3 -2 19172.3 451.901 7 10 -3 -2 19232.2 466.238 5 10 3 -2 19936.2 452.924 3 -10 -3 -2 19545.8 460.920 10 10 3 -1 1039.38 76.1858 9 -10 3 -1 981.773 76.1395 9 10 -3 -1 1060.72 89.7162 5 10 3 -1 1040.81 74.3561 3 -10 -3 -1 1081.12 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176.821 50.2533 10 -12 3 2 268.568 54.3333 9 12 -3 2 221.557 53.3816 5 12 -3 3 18665.8 518.351 5 -12 3 3 18902.1 506.359 9 -12 -3 3 19324.1 514.001 10 -12 3 3 20157.9 447.297 10 12 -3 4 1545.65 127.185 5 -12 3 4 1754.31 132.472 9 -12 -3 4 1680.15 130.715 10 -12 3 4 1755.75 109.610 10 12 -3 5 10840.5 373.492 5 -12 -3 5 10873.7 365.617 10 -12 3 5 11629.2 334.893 10 12 -3 6 740.207 94.1179 5 -12 -3 6 944.160 105.570 10 -12 3 6 809.916 85.9932 10 12 -3 7 7504.69 317.624 5 -12 -3 7 6676.93 293.903 10 -12 3 7 7504.24 284.361 10 12 4 -6 165.822 56.2164 9 -12 4 -6 145.931 41.2666 9 -12 4 -6 238.244 61.8471 4 12 4 -5 1594.02 122.216 9 -12 4 -5 1470.02 111.523 9 -12 4 -5 1660.54 145.799 4 12 4 -5 1645.66 139.292 3 12 -4 -5 1563.90 125.562 5 12 4 -4 17.9845 33.7764 3 12 4 -4-6.13064 28.7264 9 -12 4 -4 76.9452 41.2951 9 12 -4 -4 1.49976 36.5472 5 12 4 -3 3643.71 174.230 9 -12 4 -3 3689.14 173.577 9 12 -4 -3 3556.08 183.325 5 12 4 -3 3676.69 181.432 3 12 4 -2 564.064 68.7727 9 -12 4 -2 609.095 66.8627 3 -12 4 -2 601.904 72.9193 9 12 -4 -2 579.270 75.8739 5 12 4 -2 549.691 65.7834 3 -12 -4 -2 798.832 87.2279 10 12 4 -1 3939.78 170.684 9 -12 4 -1 3961.44 180.704 9 12 -4 -1 3720.88 191.759 5 12 4 -1 4013.58 169.853 3 -12 -4 -1 3795.41 188.586 10 -12 -4 0 108.617 45.2258 10 12 4 0 152.712 31.4482 3 12 4 0 154.370 40.5105 9 -12 4 0 111.762 39.1170 9 12 -4 0 118.602 48.2779 5 -12 4 1 3656.49 176.206 9 12 -4 1 3570.39 192.508 5 -12 -4 1 3500.36 188.648 10 -12 4 2 629.536 77.8284 9 12 -4 2 544.891 79.4484 5 -12 -4 2 616.652 84.8720 10 -12 4 3 3985.41 192.615 9 12 -4 3 4068.95 215.788 5 -12 -4 3 4013.82 208.906 10 -12 -4 4-15.2627 43.1427 10 12 -4 4 160.432 59.1650 5 12 -4 5 1633.49 146.020 5 -12 -4 5 1652.43 144.512 10 -12 -4 6 266.109 71.7641 10 12 -4 6 146.862 55.4115 5 12 -4 7 2036.88 165.743 5 -12 4 7 2252.78 149.893 10 -12 5 -6 146.652 44.9588 9 12 5 -5 15201.7 444.683 9 -12 5 -5 15626.3 441.304 9 -12 5 -5 16165.9 521.851 4 12 5 -5 15867.3 487.875 3 12 5 -4 301.998 57.3222 3 -12 5 -4 563.870 75.3049 9 12 5 -4 421.640 67.9214 9 12 -5 -4 437.780 68.0815 5 12 5 -3 22417.2 544.764 9 -12 5 -3 22866.6 551.543 9 12 -5 -3 22694.4 577.190 5 12 5 -3 22453.0 565.747 3 -12 5 -2 904.923 87.7263 3 12 5 -2 921.927 88.8024 9 -12 5 -2 802.365 84.8754 9 12 -5 -2 970.574 98.1523 5 12 5 -2 937.331 88.2338 3 -12 -5 -2 995.898 99.9665 10 12 5 -1 25060.1 566.445 9 -12 5 -1 25419.6 591.191 9 12 -5 -1 23974.5 609.856 5 -12 -5 -1 24710.9 606.046 10 12 5 -1 24958.8 565.462 3 -12 5 0 1259.10 105.178 9 12 -5 0 1416.21 115.619 5 -12 -5 0 1276.27 111.565 10 12 -5 1 23042.5 613.401 5 -12 -5 1 23683.0 606.221 10 -12 5 2 742.026 81.1526 9 12 -5 2 772.490 96.2532 5 -12 -5 2 824.627 96.1988 10 12 -5 3 22701.3 623.151 5 -12 -5 3 23396.4 613.472 10 12 -5 4 439.731 74.3744 5 12 6 -4 74.9265 42.7400 3 12 6 -4 135.405 53.7592 9 -12 6 -4 34.7837 37.1251 9 12 -6 -4 151.625 52.7710 5 12 6 -3 545.384 74.8550 9 -12 6 -3 550.792 79.3050 9 -12 6 -3 602.989 79.9950 3 12 6 -3 614.728 83.6824 3 12 -6 -3 504.253 73.2881 5 12 6 -2 483.884 71.3468 9 -12 6 -2 428.923 69.6733 9 12 6 -2 491.034 70.8530 3 -12 6 -2 380.705 64.0037 3 12 -6 -2 455.741 72.9685 5 -12 -6 -1 478.171 74.9177 10 -12 6 -1 480.531 70.1307 3 12 6 -1 524.824 68.7065 3 12 6 -1 381.371 60.1513 9 -12 6 -1 378.689 64.6423 9 12 -6 -1 582.244 79.6576 5 -12 -6 0 11.0397 39.1582 10 -12 6 0 37.9726 40.2860 9 12 -6 0 78.1103 31.8051 5 -12 6 1 274.144 55.1805 9 -12 6 2 478.643 70.8816 9 12 7 -2 505.501 74.2496 9 -12 7 -2 592.411 83.6330 3 12 7 -2 441.793 72.7933 3 -12 7 -1 10907.0 365.187 9 -12 7 -1 11606.2 400.264 3 -12 7 0 391.591 71.8456 9 -12 7 0 291.760 64.6244 3 -12 7 1 10675.0 348.996 9 13 0 -6 24.7265 46.8986 9 13 0 -5 23.8656 42.1440 9 -13 0 -5-5.03812 18.1991 4 13 0 -4 30.0499 42.4692 9 13 0 -4-1.94581 22.4806 5 -13 0 -3 18.6179 29.6422 10 -13 0 -3 5.48142 21.5269 9 -13 0 -3 66.6174 23.8677 4 13 0 -3 7.73181 21.3951 5 -13 0 -2 7.29886 27.0678 10 -13 0 -2 52.5082 33.4366 9 13 0 -2-10.6756 18.9063 5 -13 0 -1 8.19198 26.8297 10 13 0 -1-3.95978 27.3514 5 13 0 0 270.494 52.2980 5 13 0 0 116.647 29.8198 2 -13 0 1 11.9824 36.3983 10 13 0 1 42.6226 37.7060 5 13 0 1 48.2738 25.7456 2 -13 0 2 10.4982 28.5465 10 13 0 2-12.9840 30.3043 5 -13 0 3 81.7852 42.9893 10 13 0 3 12.4651 26.1569 5 -13 0 4 22.6165 31.3769 10 13 0 4 4.70680 29.8400 5 -13 0 5-8.10881 39.3470 10 13 0 5 49.1356 33.5974 5 -13 0 6 12.6523 39.7881 10 13 0 6-19.4968 31.7577 5 -13 0 7-9.14489 44.3420 10 13 0 7-5.66682 27.7402 5 -13 1 -8 8480.33 349.309 4 13 1 -7 2660.74 179.223 9 -13 1 -7 2803.20 179.143 4 13 1 -6 14566.4 444.890 9 -13 1 -6 15250.6 444.308 4 13 1 -5 8120.04 300.769 9 -13 1 -5 8436.56 294.868 4 13 -1 -5 8095.94 277.715 5 13 1 -4 25224.2 603.470 9 -13 1 -4 25952.4 548.561 9 -13 1 -4 24022.9 576.648 4 13 -1 -4 24647.4 572.989 5 13 1 -3 5484.67 229.079 9 -13 1 -3 5834.57 209.217 9 13 -1 -3 5594.86 217.129 5 13 1 -3 6217.28 201.295 5 -13 1 -3 5582.09 194.652 10 -13 -1 -3 5555.13 216.861 10 13 1 -2 25045.1 597.163 9 -13 1 -2 25929.2 578.235 9 13 -1 -2 25546.1 589.227 5 13 1 -2 26340.5 550.612 5 -13 -1 -2 25771.2 588.111 10 -13 1 -2 25129.1 551.434 10 13 1 -1 5301.13 221.620 9 -13 1 -1 5730.75 223.422 9 13 1 -1 5819.61 205.652 5 13 -1 -1 5603.19 224.383 5 -13 -1 -1 5343.16 218.612 10 -13 1 -1 5814.54 209.308 10 -13 -1 0 36657.5 717.921 6 13 1 0 35180.1 727.716 5 13 -1 0 35150.3 759.643 5 -13 -1 0 35803.2 762.534 10 -13 1 0 35476.5 729.856 10 13 1 1 5237.44 198.527 5 13 -1 1 5081.18 211.698 5 -13 -1 1 5456.13 219.035 10 -13 1 1 5125.21 197.871 10 13 1 2 24558.0 540.354 5 13 -1 2 23656.7 573.213 5 -13 -1 2 24161.4 571.190 10 -13 1 2 24140.2 538.024 10 13 1 3 4939.58 193.460 5 13 -1 3 5122.52 213.101 5 -13 -1 3 5145.36 213.199 10 -13 1 3 5232.94 198.183 10 13 1 4 24665.7 559.480 5 -13 -1 4 25033.9 586.293 10 -13 1 4 25989.0 573.211 10 13 1 5 7856.78 270.374 5 13 -1 5 8106.30 291.730 5 -13 -1 5 8131.84 291.303 10 -13 1 5 8441.03 283.877 10 13 1 6 14207.6 409.964 5 13 -1 6 14329.4 432.355 5 -13 -1 6 14829.0 434.343 10 -13 1 6 15457.7 432.484 10 13 1 7 2599.70 162.372 5 13 -1 7 2656.14 172.638 5 -13 -1 7 2647.26 173.858 10 -13 1 7 2927.88 177.487 10 13 1 8 7396.68 289.157 10 13 2 -7 520.219 84.2790 9 -13 2 -7 453.533 77.1523 4 13 2 -6 2932.44 177.502 9 -13 2 -6 2882.66 181.886 4 13 2 -5 2760.68 165.345 9 -13 2 -5 2606.02 164.366 4 13 -2 -5 2539.83 153.566 5 13 2 -4 8232.33 288.303 9 -13 2 -4 8212.21 260.024 9 13 -2 -4 7580.62 277.448 5 13 2 -3 1632.81 117.121 9 -13 2 -3 1580.92 107.259 9 13 -2 -3 1523.57 113.800 5 -13 -2 -3 1806.72 123.597 10 13 2 -2 5695.82 224.203 9 -13 2 -2 6158.00 224.438 9 13 -2 -2 5750.83 234.292 5 -13 -2 -2 5658.04 228.931 10 13 2 -1 2175.53 129.741 9 -13 2 -1 2321.83 137.386 9 13 -2 -1 2167.75 140.662 5 -13 -2 -1 2142.22 138.518 10 13 2 0 14205.7 390.026 9 -13 2 0 14877.9 416.096 9 13 -2 0 14810.6 420.154 5 -13 -2 0 15407.2 426.107 10 -13 2 0 15533.3 376.229 10 13 2 1 1988.00 111.860 5 -13 2 1 1984.65 138.111 9 13 -2 1 2127.09 137.872 5 -13 -2 1 2185.25 141.738 10 -13 2 1 1933.27 111.308 10 13 2 2 5558.67 197.022 5 13 -2 2 5843.29 240.836 5 -13 -2 2 5707.40 236.150 10 -13 2 2 5355.26 194.407 10 13 2 3 1907.30 110.397 5 13 -2 3 1799.32 132.459 5 -13 -2 3 1846.17 133.528 10 -13 2 3 1905.12 112.610 10 13 2 4 8067.70 258.924 5 13 -2 4 7680.56 291.076 5 -13 -2 4 7987.58 293.178 10 -13 2 4 8707.97 272.880 10 13 2 5 2295.49 132.657 5 13 -2 5 2322.68 154.939 5 -13 -2 5 2216.39 149.775 10 -13 2 5 2474.52 143.910 10 13 2 6 2361.86 144.092 5 13 -2 6 2672.98 172.631 5 -13 -2 6 2587.78 167.025 10 -13 2 6 2810.39 161.813 10 13 2 7 473.029 70.3111 5 13 -2 7 448.369 79.2116 5 -13 -2 7 594.303 88.4747 10 -13 2 7 605.612 85.8063 10 13 3 -7 1247.13 122.910 9 -13 3 -7 1227.72 129.765 4 13 3 -6 4897.13 233.455 9 -13 3 -6 5199.05 264.049 4 13 3 -5 784.963 90.2955 9 -13 3 -5 791.602 80.5156 9 -13 3 -5 831.352 99.6772 4 13 -3 -5 723.373 87.3513 5 13 3 -4 7978.96 284.408 9 -13 3 -4 7666.92 262.017 9 13 -3 -4 7445.85 284.163 5 13 3 -3 3450.57 172.137 9 -13 3 -3 3215.81 161.699 9 13 -3 -3 3138.01 172.793 5 -13 -3 -3 3276.56 176.697 10 13 3 -2 13222.1 368.092 9 -13 3 -2 13168.0 367.803 9 13 3 -2 12588.8 363.971 3 13 -3 -2 12159.9 381.988 5 -13 -3 -2 13317.2 389.215 10 13 3 -1 5204.71 204.593 9 -13 3 -1 5503.52 219.217 9 13 -3 -1 4541.53 216.339 5 13 3 -1 5213.73 197.301 3 -13 -3 -1 4748.74 218.182 10 13 3 0 8566.91 274.267 9 -13 3 0 9115.11 303.576 9 13 -3 0 8734.35 312.249 5 13 3 0 9115.47 262.072 3 -13 -3 0 8984.25 313.100 10 13 3 1 4143.98 177.460 9 -13 3 1 4492.56 209.137 9 13 -3 1 4483.61 216.034 5 -13 -3 1 4710.37 216.592 10 -13 3 2 12248.8 383.319 9 13 -3 2 12193.4 388.364 5 -13 -3 2 12762.8 391.146 10 -13 -3 3 3258.99 184.734 10 13 -3 3 3361.41 191.658 5 -13 3 3 3189.77 184.410 9 -13 3 3 3357.71 151.087 10 13 -3 4 7414.20 304.018 5 -13 3 4 7244.94 294.375 9 -13 -3 4 7424.91 295.388 10 -13 3 4 7975.33 258.758 10 13 -3 5 615.817 83.5694 5 -13 -3 5 644.819 90.7561 10 -13 3 5 865.487 86.7672 10 13 3 6 4483.25 199.630 5 13 -3 6 4867.59 247.485 5 -13 -3 6 4698.93 237.626 10 -13 3 6 4966.28 217.984 10 13 -3 7 1251.44 128.811 5 -13 -3 7 1095.18 122.099 10 -13 3 7 1225.39 117.151 10 13 4 -6 9076.97 333.579 9 -13 4 -6 8480.99 300.579 9 -13 4 -6 9494.73 385.098 4 13 4 -5 3114.41 177.719 9 -13 4 -5 2927.49 162.685 9 -13 4 -5 3176.38 207.190 4 13 4 -5 3089.06 196.180 3 13 -4 -5 3146.84 187.114 5 13 4 -4 13106.3 392.691 9 -13 4 -4 13046.5 376.720 9 13 4 -4 13018.2 413.122 3 13 -4 -4 13471.1 412.985 5 13 4 -3 4123.53 194.170 9 -13 4 -3 4243.43 193.404 9 13 4 -3 3973.29 196.253 3 13 -4 -3 3905.01 202.118 5 -13 -4 -3 3990.23 201.031 10 13 4 -2 19834.2 487.706 9 -13 4 -2 19821.9 495.689 9 13 -4 -2 18009.3 506.844 5 13 4 -2 19188.6 484.889 3 -13 -4 -2 19245.4 511.094 10 13 4 -1 6221.52 229.093 9 -13 4 -1 6031.63 237.573 9 13 -4 -1 5669.51 249.940 5 13 4 -1 5955.34 219.760 3 -13 -4 -1 5863.12 248.270 10 13 4 0 18965.4 453.703 9 -13 4 0 18277.4 477.029 9 13 -4 0 17865.6 504.101 5 -13 -4 0 17616.0 496.275 10 -13 4 1 5474.40 232.221 9 13 -4 1 5399.03 247.510 5 -13 -4 1 5611.93 248.405 10 -13 4 2 18510.5 501.914 9 13 -4 2 19281.6 536.854 5 -13 -4 2 19876.4 533.471 10 -13 4 3 3419.60 185.446 9 13 -4 3 3658.68 206.530 5 -13 -4 3 3747.29 204.752 10 13 -4 4 13267.6 445.471 5 -13 -4 4 13735.1 435.442 10 13 -4 5 3375.29 213.233 5 -13 -4 5 3155.81 198.450 10 13 -4 6 8822.04 364.127 5 -13 -4 6 8085.71 342.518 10 13 5 -5 188.153 62.2963 3 13 5 -5 21.4793 38.5960 9 -13 5 -5 93.5490 43.8730 9 -13 5 -5 130.299 52.5725 4 13 5 -4 273.928 58.9653 3 -13 5 -4 414.241 70.5858 9 13 5 -4 268.742 55.4352 9 13 -5 -4 300.010 60.7485 5 13 5 -3 257.034 52.9097 3 13 5 -3 288.407 57.8494 9 -13 5 -3 328.352 63.6833 9 13 -5 -3 292.271 62.8371 5 -13 -5 -2 458.745 77.7472 10 13 5 -2 420.458 61.8189 3 13 5 -2 342.836 59.1245 9 -13 5 -2 415.273 67.6699 9 13 -5 -2 465.909 75.2965 5 -13 5 -2 388.153 63.2853 3 -13 -5 -1 548.656 80.7200 10 13 5 -1 691.507 75.8721 9 -13 5 -1 758.606 89.5757 9 13 -5 -1 661.753 85.9800 5 13 5 -1 769.885 77.6807 3 -13 -5 0 387.678 71.4672 10 -13 5 0 456.870 69.8439 9 13 -5 0 415.168 72.8501 5 -13 5 1 798.156 90.1521 9 13 -5 1 817.693 98.5123 5 -13 -5 1 699.876 89.1830 10 -13 -5 2 315.036 63.3157 10 -13 5 2 307.661 54.3438 9 13 -5 2 411.268 75.5829 5 -13 -5 3 461.843 83.3217 10 13 -5 3 390.815 74.2731 5 -13 -5 4 297.822 75.6519 10 13 -5 4 240.491 58.4280 5 13 -5 5 136.252 49.9430 5 13 6 -4 8882.57 348.067 3 13 -6 -4 9073.16 346.048 5 13 6 -3 3198.46 178.560 9 -13 6 -3 3570.53 196.011 9 13 -6 -3 3533.53 201.793 5 13 6 -3 3500.13 197.607 3 13 6 -2 11907.9 366.692 9 -13 6 -2 11823.3 380.758 9 13 -6 -2 11891.0 397.548 5 13 6 -2 11987.5 376.667 3 -13 6 -2 12202.1 392.502 3 -13 6 -1 2676.53 172.778 3 -13 6 -1 2724.83 165.476 9 13 -6 -1 2672.01 174.389 5 -13 -6 -1 2636.70 172.647 10 -13 6 0 8954.82 318.577 9 13 -6 0 9010.29 341.024 5 -13 -6 0 8785.44 331.156 10 -13 6 1 2810.97 168.798 9 13 -6 1 2576.18 175.667 5 -13 6 2 11207.4 363.571 9 13 7 -2 2187.92 153.474 3 -13 7 0 2729.12 171.808 9 -13 7 1 570.713 80.4271 9 14 0 -4 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10500.5 409.223 10 -18 5 0 4187.86 248.350 9 18 -5 0 4325.75 249.601 5 -18 -5 0 4431.48 251.232 10 -18 5 1 9882.69 400.950 9 18 -5 1 10949.8 412.287 5 -18 -5 1 10996.6 409.823 10 -18 5 2 4289.19 254.838 9 18 -5 2 5107.68 268.984 5 -18 -5 2 4992.15 263.374 10 -18 5 3 8695.04 374.086 9 19 0 -3 24.2996 27.0923 5 -19 0 -2 137.628 67.5641 10 -19 0 -2 23.7294 40.7135 9 19 0 -2 37.8950 53.4815 5 -19 0 -1 118.120 50.8742 10 19 0 -1 138.140 51.7153 5 -19 0 0 320.233 65.3163 10 19 0 0 240.914 53.8743 5 -19 0 1 156.476 54.8430 10 19 0 1 191.064 52.1962 5 -19 0 2 87.3156 52.9630 10 19 0 2 15.4852 44.5542 5 -19 0 3-19.3814 44.5709 10 19 0 3 130.308 52.5770 5 -19 0 4-30.5146 48.6971 10 19 0 4 13.4863 34.8629 5 -19 0 5-2.13777 40.9688 10 19 0 5-5.11920 48.3666 5 19 -1 -5 10609.6 396.123 5 19 -1 -4 1526.28 137.752 5 -19 1 -3 14461.4 441.003 9 -19 -1 -3 14004.1 450.791 10 -19 1 -2 3892.20 212.144 9 19 -1 -2 3390.30 200.131 5 -19 -1 -2 3709.19 210.371 10 19 -1 -1 21113.6 574.748 5 -19 -1 -1 21641.5 583.129 10 19 -1 0 2610.06 166.589 5 -19 -1 0 2722.63 170.933 10 -19 1 0 2794.67 159.522 10 19 1 1 21296.3 532.768 5 19 -1 1 20223.0 551.191 5 -19 -1 1 21250.2 557.458 10 -19 1 1 20615.7 529.509 10 19 1 2 3361.84 181.698 5 19 -1 2 2938.77 180.539 5 -19 -1 2 3332.90 188.539 10 -19 1 2 3147.18 178.742 10 19 1 3 12999.7 414.879 5 19 -1 3 12333.0 419.686 5 -19 -1 3 13121.4 423.620 10 -19 1 3 12595.2 412.092 10 19 1 4 1637.06 139.715 5 19 -1 4 1791.76 154.297 5 -19 -1 4 1903.02 157.079 10 -19 1 4 1740.01 144.545 10 19 1 5 10395.9 388.016 5 19 -1 5 10696.2 414.265 5 -19 -1 5 11218.0 417.761 10 -19 1 5 11355.3 407.674 10 19 -2 -5 3333.59 219.240 5 19 2 -4 930.004 124.747 9 -19 2 -4 934.576 107.135 9 19 -2 -4 835.045 108.928 5 19 2 -3 3345.20 220.178 9 -19 2 -3 3305.99 201.600 9 19 -2 -3 3073.86 200.569 5 -19 -2 -3 3495.38 215.573 10 -19 2 -2 1132.98 123.626 9 19 -2 -2 873.510 106.398 5 -19 -2 -2 922.899 109.447 10 -19 2 -1 5022.44 256.001 9 19 -2 -1 4596.11 239.129 5 -19 -2 -1 5187.81 252.409 10 -19 2 0 1442.20 135.229 9 19 -2 0 1154.06 116.897 5 -19 -2 0 1404.11 126.459 10 19 -2 1 4712.15 238.094 5 -19 -2 1 4894.07 239.146 10 19 -2 2 771.418 96.6364 5 -19 -2 2 1048.72 113.269 10 19 -2 3 3308.28 202.785 5 -19 -2 3 3250.86 196.153 10 19 -2 4 956.142 115.545 5 -19 -2 4 822.779 109.147 10 -19 2 4 937.220 106.164 10 -19 2 5 3290.93 206.070 10 19 3 -4 1325.08 149.498 9 -19 3 -4 1484.57 141.877 9 19 -3 -4 1235.34 135.110 5 19 3 -3 6105.35 300.113 9 -19 3 -3 5770.37 278.364 9 19 -3 -3 5416.97 281.995 5 -19 -3 -3 5823.39 293.678 10 -19 -3 -2 415.339 80.6252 10 19 3 -2 500.739 93.6554 9 -19 3 -2 382.408 81.1064 9 19 -3 -2 411.807 77.5713 5 19 3 -1 6444.99 296.879 9 -19 3 -1 6945.68 314.262 9 19 -3 -1 6694.93 302.638 5 -19 -3 -1 7249.92 316.222 10 -19 3 0 1284.62 134.638 9 19 -3 0 1330.98 129.273 5 -19 -3 0 1289.20 128.531 10 -19 3 1 6910.54 318.097 9 19 -3 1 6182.32 284.260 5 -19 -3 1 6490.11 290.976 10 -19 -3 2 496.589 85.4119 10 -19 3 2 452.004 86.3637 9 19 -3 2 493.064 84.5961 5 -19 3 3 6757.53 316.981 9 19 -3 3 5983.02 286.955 5 -19 -3 3 6107.20 284.422 10 -19 3 4 1476.73 150.160 9 19 -3 4 1249.95 130.497 5 -19 -3 4 1386.48 133.436 10 19 4 -3 8910.13 372.576 9 -19 4 -3 9427.61 376.428 9 19 4 -2 1890.08 163.337 9 -19 4 -2 1924.17 164.239 9 19 -4 -2 1872.68 160.753 5 -19 -4 -2 2016.09 172.542 10 19 4 -1 10983.7 407.103 9 -19 4 -1 11215.1 424.284 9 19 -4 -1 12102.4 436.101 5 -19 -4 -1 11733.2 427.339 10 -19 4 0 1588.99 151.575 9 19 -4 0 1542.44 146.174 5 -19 -4 0 1661.21 151.491 10 -19 4 1 11002.8 428.221 9 19 -4 1 11733.1 422.376 5 -19 -4 1 12096.3 424.782 10 -19 4 2 1831.24 168.870 9 19 -4 2 1872.69 156.065 5 -19 -4 2 1739.98 150.170 10 -19 4 3 9036.31 388.287 9 -19 4 4 1837.12 167.444 9 -20 0 -2 24656.5 623.183 9 20 0 -2 22494.1 601.677 5 -20 0 -2 23178.8 608.487 10 20 0 -1 1972.25 138.000 5 -20 0 -1 1645.14 133.359 10 20 0 0 15644.4 455.197 5 -20 0 0 16006.0 458.567 10 20 0 1 1450.78 123.196 5 -20 0 1 1374.00 119.191 10 20 0 2 19742.8 541.791 5 -20 0 2 19985.7 540.087 10 -20 0 3 304.672 64.8101 10 20 0 3 369.305 70.4533 5 20 0 4 10794.9 403.306 5 -20 0 4 10939.0 401.811 10 20 0 5 753.391 105.805 5 20 -1 -5 46.1862 36.0708 5 20 -1 -4 1358.58 134.765 5 -20 -1 -3 280.740 76.4162 10 -20 1 -3 149.065 60.1078 9 20 -1 -3 176.483 57.7610 5 -20 1 -2 1496.45 137.503 9 20 -1 -2 1565.14 136.006 5 -20 -1 -2 1539.02 139.389 10 -20 1 -1 692.453 100.011 9 20 -1 -1 569.284 86.5607 5 -20 -1 -1 591.201 94.1795 10 20 -1 0 1227.69 116.125 5 -20 -1 0 1225.15 117.591 10 20 -1 1 566.386 83.4826 5 -20 -1 1 654.179 90.5552 10 -20 1 1 738.891 91.2739 10 20 1 2 1180.29 109.184 5 20 -1 2 1139.91 113.019 5 -20 -1 2 1167.34 117.522 10 -20 1 2 1270.98 119.138 10 -20 -1 3 22.5776 34.6068 10 -20 1 3 121.208 58.3062 10 20 1 3 137.493 53.5224 5 20 -1 3 97.5965 40.8162 5 20 1 4 1297.80 129.702 5 20 -1 4 1482.33 141.755 5 -20 -1 4 1342.08 134.067 10 -20 1 4 1292.58 135.119 10 -20 1 5 64.8813 50.9299 10 20 1 5-89.4647 40.3436 5 20 -2 -4 10484.1 409.186 5 -20 -2 -3 307.819 82.4535 10 -20 2 -3 209.002 63.0863 9 20 -2 -3 430.129 84.7270 5 -20 2 -2 11528.8 408.599 9 20 -2 -2 10442.4 394.190 5 -20 -2 -2 11223.9 407.271 10 -20 2 -1 441.335 82.8978 9 -20 -2 -1 712.467 99.2513 10 20 -2 -1 496.068 82.4117 5 -20 2 0 11682.1 418.346 9 20 -2 0 10619.6 383.758 5 -20 -2 0 11214.9 391.731 10 -20 -2 1 496.317 85.4146 10 -20 2 1 738.787 105.083 9 20 -2 1 525.891 81.5035 5 20 -2 2 9879.96 372.183 5 -20 -2 2 10514.4 377.018 10 -20 -2 3 356.468 69.3815 10 20 -2 3 275.467 60.3214 5 20 -2 4 10519.1 402.673 5 -20 -2 4 10177.2 389.609 10 -20 2 5 587.669 95.1521 10 -20 3 -4 7303.10 325.460 9 20 3 -3 975.853 134.286 9 -20 3 -3 951.352 114.416 9 20 -3 -3 912.401 116.544 5 -20 -3 -3 945.254 122.901 10 20 3 -2 8308.97 362.890 9 -20 3 -2 8643.10 359.836 9 20 -3 -2 8888.43 365.667 5 -20 -3 -2 9084.85 371.513 10 -20 3 -1 1300.31 141.741 9 20 -3 -1 1078.55 122.805 5 -20 -3 -1 1234.10 127.022 10 -20 3 0 7788.26 344.965 9 20 -3 0 7276.53 317.920 5 -20 -3 0 7751.70 327.480 10 -20 3 1 1031.20 132.168 9 20 -3 1 1062.46 116.341 5 -20 -3 1 1083.89 115.797 10 20 -3 2 8148.95 343.160 5 -20 -3 2 8661.19 346.571 10 -20 3 3 1135.57 133.443 9 20 -3 3 1046.32 119.014 5 -20 -3 3 989.341 117.581 10 -20 3 4 8060.61 359.804 9 20 4 -2 1574.41 159.314 9 20 4 -1 413.408 90.5682 9 20 -4 0 3505.56 219.391 5 -20 -4 0 3399.48 219.967 10 -20 4 1 406.648 87.8862 9 -21 0 -2-21.5132 40.9562 9 -21 0 -1 249.921 66.1366 10 21 0 -1 368.776 70.8021 5 -21 0 0 76.2364 46.9399 10 21 0 0 90.8586 38.0047 5 -21 0 1 251.255 67.3693 10 21 0 1 227.946 53.7376 5 -21 0 2 114.384 52.6255 10 21 0 2 70.9922 37.3383 5 -21 0 3 0.00000 38.9174 10 21 0 3 71.1752 51.6736 5 -21 0 4 28.0662 45.2643 10 21 0 4 106.856 54.1233 5 21 -1 -4 6828.30 315.462 5 -21 1 -3 5623.98 270.267 9 21 -1 -3 5303.01 268.604 5 -21 -1 -3 5804.05 282.868 10 -21 1 -2 10989.6 393.445 9 21 -1 -2 10241.6 381.486 5 -21 -1 -2 11058.7 394.565 10 -21 1 -1 6239.76 283.935 9 21 -1 -1 5373.55 259.031 5 -21 -1 -1 5494.09 262.629 10 21 -1 0 7186.23 300.213 5 -21 -1 0 7219.61 298.938 10 21 -1 1 5297.63 252.015 5 -21 -1 1 5373.38 250.247 10 21 -1 2 9367.17 353.458 5 -21 -1 2 10093.6 362.572 10 -21 1 2 9012.22 331.031 10 21 -1 3 5350.24 264.789 5 -21 -1 3 4954.27 252.288 10 -21 1 3 5232.18 254.587 10 21 1 4 6225.48 294.974 5 -21 1 4 6408.42 301.632 10 -21 2 -3 2308.72 179.658 9 21 -2 -3 2323.44 181.393 5 -21 -2 -3 2512.18 191.245 10 -21 2 -2 4488.55 249.525 9 21 -2 -2 4127.58 238.434 5 -21 -2 -2 4296.26 242.910 10 -21 2 -1 2609.08 191.196 9 21 -2 -1 2127.28 166.073 5 -21 -2 -1 2304.15 173.568 10 -21 2 0 2861.82 196.910 9 21 -2 0 2565.06 178.320 5 -21 -2 0 2613.45 179.061 10 -21 2 1 2180.43 174.197 9 21 -2 1 1758.98 147.037 5 -21 -2 1 1925.97 152.877 10 -21 2 2 5090.94 269.381 9 21 -2 2 4320.07 237.182 5 -21 -2 2 4370.99 235.495 10 21 -2 3 2449.95 178.350 5 -21 -2 3 2432.39 177.614 10 -21 3 -2 4142.50 245.823 9 -21 3 -1 2593.84 198.947 9 21 -3 -1 2336.20 181.224 5 -21 -3 -1 2685.92 193.351 10 -21 3 0 5460.81 290.622 9 21 -3 0 5104.71 265.265 5 -21 -3 0 5366.02 271.083 10 -21 3 1 2100.12 177.851 9 21 -3 1 2006.36 159.736 5 -21 -3 1 1910.01 156.984 10 -21 3 2 4604.13 267.853 9 -22 0 -2 72.5645 47.2081 9 -22 0 -1 18082.1 526.434 9 -22 0 -1 16840.0 499.690 10 -22 0 0 583.080 80.3477 10 22 0 0 504.241 74.1943 5 22 0 1 14405.9 444.954 5 -22 0 1 14364.8 440.859 10 -22 0 2 103.529 47.1861 10 22 0 2 106.053 38.6865 5 22 0 3 14030.6 460.178 5 -22 0 3 13655.7 452.022 10 22 -1 -3 692.864 100.188 5 -22 -1 -3 772.505 110.841 10 -22 -1 -2 212.834 69.2958 10 -22 1 -2 176.837 62.3303 9 22 -1 -2 154.064 51.3353 5 -22 1 -1 1390.89 135.897 9 22 -1 -1 1477.69 135.729 5 -22 -1 -1 1324.04 133.767 10 -22 -1 0 313.551 74.2609 10 22 -1 0 213.811 61.6370 5 22 -1 1 1063.10 112.733 5 -22 -1 1 1054.82 113.535 10 -22 -1 2 138.166 56.2408 10 22 -1 2 180.408 57.3270 5 -22 1 3 543.750 86.5104 10 -22 -2 -2-44.6624 57.3417 10 22 -2 -2-35.4594 33.0553 5 -22 2 -1 10788.2 407.443 9 22 -2 -1 9496.42 374.417 5 -22 -2 -1 9836.53 380.674 10 -22 -2 0 42.7829 43.6527 10 -22 2 0-37.8367 60.9596 9 22 -2 0 64.6589 41.5048 5 22 -2 1 9303.20 363.210 5 -22 -2 1 9195.78 359.755 10 -23 0 -2-36.1810 47.7299 9 -23 0 -1 104.916 61.7646 9 -23 0 0 56.5582 42.7550 10 -23 0 1 165.562 56.3961 10 23 0 1 89.6112 41.5522 5 -23 0 2 57.7238 54.3053 10 23 0 2 257.810 62.7480 5 -23 1 -2 8944.98 360.770 9 23 -1 -2 8412.04 345.660 5 -23 -1 -2 8063.60 340.705 10 -23 1 -1 4694.46 255.033 9 23 -1 -1 4055.21 228.136 5 -23 -1 -1 4355.00 237.265 10 23 -1 0 8878.94 347.098 5 -23 -1 0 8875.78 344.208 10 23 -1 1 3582.81 210.502 5 -23 -1 1 3797.31 214.868 10 ; _shelx_hkl_checksum 19223 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y, z' '-x+1/2, y, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Dy1 Dy 0.60198(2) 0.20406(2) 0.44467(9) 0.01208(11) Uani 1 1 d . . . . . O1 O 0.7192(2) 0.1950(6) 0.5839(7) 0.0351(12) Uani 1 1 d . . . . . O2 O 0.5857(2) 0.1765(6) 0.7526(6) 0.0216(9) Uani 1 1 d . . . . . O3 O 0.65279(19) 0.5321(5) 0.4909(5) 0.0255(11) Uani 1 1 d . . . . . O4 O 0.5728(2) 0.4063(5) 0.1872(5) 0.0208(8) Uani 1 1 d . . . . . O5 O 0.6778(2) 0.1169(7) 0.2176(5) 0.0311(10) Uani 1 1 d . . . . . O6 O 0.4943(2) 0.3942(6) 0.5188(5) 0.0239(8) Uani 1 1 d . . . . . O7 O 0.6247(3) -0.1437(6) 0.5171(6) 0.0270(9) Uani 1 1 d . . . . . O8 O 0.4908(2) -0.0243(6) 0.8034(5) 0.0270(9) Uani 1 1 d . . . . . C1 C 0.6384(3) 0.7057(7) 0.4279(14) 0.0217(14) Uani 1 1 d . . . . . H1 H 0.6382 0.7199 0.3062 0.026 Uiso 1 1 calc R U . . . C2 C 0.5130(3) 0.4772(8) 0.1366(7) 0.0202(11) Uani 1 1 d . . . . . H2 H 0.4709 0.4299 0.1913 0.024 Uiso 1 1 calc R U . . . C3 C 0.7361(3) 0.0777(8) 0.1458(7) 0.0260(13) Uani 1 1 d . . . . . H3 H 0.7477 -0.0591 0.1374 0.031 Uiso 1 1 calc R U . . . C4 C 0.5436(3) 0.0761(7) 0.8512(7) 0.0199(11) Uani 1 1 d . . . . . H4 H 0.5535 0.0786 0.9711 0.024 Uiso 1 1 calc R U . . . N1 N 0.6799(2) 0.4704(7) 0.9278(9) 0.0314(11) Uani 1 1 d . . . . . H1A H 0.7279 0.4525 0.9362 0.047 Uiso 1 1 calc R U . . . H1B H 0.6626 0.3956 0.8397 0.047 Uiso 1 1 calc DR U . . . H1C H 0.6587 0.4329 1.0279 0.047 Uiso 1 1 calc DR U . . . N2 N 0.6648(4) 0.6786(8) 0.8949(7) 0.0390(16) Uani 1 1 d D . . . . H2A H 0.6223(14) 0.705(3) 0.952(4) 0.047 Uiso 1 1 d D U . . . H2B H 0.658(2) 0.6895(8) 0.7767(10) 0.047 Uiso 1 1 d D U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Dy1 0.01121(14) 0.01051(15) 0.01452(14) 0.00027(18) 0.00049(17) 0.00079(6) O1 0.016(2) 0.029(2) 0.060(3) 0.014(2) -0.015(2) 0.0003(16) O2 0.025(2) 0.021(2) 0.018(2) 0.0014(16) 0.0031(19) -0.0060(16) O3 0.029(2) 0.0104(16) 0.038(3) -0.0012(15) -0.0067(15) -0.0003(15) O4 0.019(2) 0.022(2) 0.0218(19) 0.0053(16) -0.0037(16) 0.0034(16) O5 0.020(2) 0.042(3) 0.032(2) -0.002(2) 0.0106(18) 0.005(2) O6 0.021(2) 0.029(2) 0.0217(16) -0.0071(18) 0.0000(15) 0.0091(16) O7 0.036(2) 0.0111(18) 0.034(2) 0.0010(18) 0.001(2) 0.002(2) O8 0.027(2) 0.0243(19) 0.030(2) 0.0028(18) 0.0000(18) -0.0094(17) C1 0.027(3) 0.018(3) 0.020(4) -0.001(3) -0.006(4) -0.0017(18) C2 0.017(3) 0.026(3) 0.017(2) 0.002(2) 0.001(2) 0.003(2) C3 0.020(3) 0.020(3) 0.038(4) 0.002(2) 0.008(2) 0.005(2) C4 0.026(3) 0.018(2) 0.016(3) 0.001(2) 0.003(2) -0.001(2) N1 0.031(2) 0.033(2) 0.031(3) -0.007(3) -0.005(3) -0.0009(19) N2 0.039(3) 0.039(3) 0.039(4) 0.013(2) -0.005(2) 0.000(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 O5 Dy1 O8 88.15(15) . 2_654 O5 Dy1 O2 143.39(16) . . O8 Dy1 O2 108.91(15) 2_654 . O5 Dy1 O3 95.86(15) . . O8 Dy1 O3 144.50(13) 2_654 . O2 Dy1 O3 88.47(14) . . O5 Dy1 O7 80.05(15) . . O8 Dy1 O7 75.25(15) 2_654 . O2 Dy1 O7 73.79(14) . . O3 Dy1 O7 140.21(14) . . O5 Dy1 O1 77.43(18) . . O8 Dy1 O1 147.52(14) 2_654 . O2 Dy1 O1 70.98(17) . . O3 Dy1 O1 66.86(12) . . O7 Dy1 O1 73.69(14) . . O5 Dy1 O6 143.68(14) . . O8 Dy1 O6 77.03(14) 2_654 . O2 Dy1 O6 72.85(14) . . O3 Dy1 O6 79.16(12) . . O7 Dy1 O6 126.03(14) . . O1 Dy1 O6 130.17(15) . . O5 Dy1 O4 70.37(14) . . O8 Dy1 O4 75.42(13) 2_654 . O2 Dy1 O4 144.27(13) . . O3 Dy1 O4 72.88(12) . . O7 Dy1 O4 138.55(14) . . O1 Dy1 O4 124.55(15) . . O6 Dy1 O4 73.83(13) . . C3 O1 Dy1 141.9(4) 4_655 . C4 O2 Dy1 134.7(4) . . C1 O3 Dy1 133.1(4) . . C2 O4 Dy1 130.2(4) . . C3 O5 Dy1 156.4(4) . . C2 O6 Dy1 127.9(4) 2_665 . C1 O7 Dy1 133.1(5) 1_545 . C4 O8 Dy1 135.4(3) . 2_655 O7 C1 O3 124.3(9) 1_565 . O6 C2 O4 124.8(5) 2_664 . O1 C3 O5 128.4(5) 4_654 . O8 C4 O2 126.1(5) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Dy1 O5 2.291(4) . Dy1 O8 2.336(4) 2_654 Dy1 O2 2.367(4) . Dy1 O3 2.383(4) . Dy1 O7 2.398(4) . Dy1 O1 2.398(4) . Dy1 O6 2.406(4) . Dy1 O4 2.430(3) . O1 C3 1.222(7) 4_655 O2 C4 1.264(7) . O3 C1 1.270(7) . O4 C2 1.254(7) . O5 C3 1.227(7) . O6 C2 1.241(6) 2_665 O7 C1 1.229(8) 1_545 O8 C4 1.228(6) . O8 Dy1 2.336(4) 2_655 C1 O7 1.229(8) 1_565 C2 O6 1.241(6) 2_664 C3 O1 1.222(7) 4_654 N1 N2 1.425(7) .