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Information card for entry 7240262
Preview
Coordinates | 7240262.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C10 H10 N2 |
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Calculated formula | C10 H10 N2 |
Title of publication | Novel synthesis of divergent aryl imidazoles from ketones involving copper-catalyzed α-amination and oxidative C‒C bond cleavage |
Authors of publication | Huang, Jiangkun; Luo, Lan; Xing, Naiguo; Gu, Linghui; Li, Chen; Han, Qiao; Zheng, Shilong; He, Ling |
Journal of publication | RSC Advances |
Year of publication | 2020 |
Journal volume | 10 |
Journal issue | 23 |
Pages of publication | 13815 - 13819 |
a | 9.612 ± 0.003 Å |
b | 7.441 ± 0.002 Å |
c | 24.001 ± 0.007 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1716.6 ± 0.9 Å3 |
Cell temperature | 296 K |
Ambient diffraction temperature | 296 K |
Number of distinct elements | 3 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.1112 |
Residual factor for significantly intense reflections | 0.0565 |
Weighted residual factors for significantly intense reflections | 0.11 |
Weighted residual factors for all reflections included in the refinement | 0.1333 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.103 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
258114 (current) | 2020-10-06 | cif/ Updating files of 7240260, 7240261, 7240262 Original log message: Adding full bibliography for 7240260--7240262.cif. |
7240262.cif |
250395 | 2020-04-06 | cif/ Adding structures of 7240260, 7240261, 7240262 via cif-deposit CGI script. |
7240262.cif |
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Users of the data should acknowledge the original authors of the
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