#------------------------------------------------------------------------------ #$Date: 2020-04-21 02:36:04 +0300 (Tue, 21 Apr 2020) $ #$Revision: 250963 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/03/7240345.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7240345 loop_ _publ_author_name 'Pereira Copetti, Jo\~ao Pedro' 'Salbego, Paulo Roberto dos Santos' 'Orlando, Tain\'ara' 'Rosa, J\'essica Maria Luis' 'Fiss, Gabriela Fehn' 'Gomes de Oliveira, Jo\~ao Paulo' 'de Almeida Vasconcellos, M\'ario Luiz Ara\'ujo' 'Zanatta, Nilo' 'Bonacorso, Helio Gauze' 'Martins, Marcos A. P.' _publ_section_title ; Substituent Effects in the Crystallization Mechanisms of 7-chloro-4-substituted-Quinolines ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D0CE00214C _journal_year 2020 _chemical_absolute_configuration none _chemical_formula_moiety 'C12 H12 Cl N O2' _chemical_formula_sum 'C12 H12 Cl N O2' _chemical_formula_weight 237.68 _chemical_melting_point ? _chemical_name_common Chloroquinolin _chemical_name_systematic 3-((7-chloroquinolin-4-yl)oxy)propan-1-ol _space_group_crystal_system orthorhombic _space_group_IT_number 33 _space_group_name_Hall 'P 2c -2n' _space_group_name_H-M_alt 'P n a 21' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2020-04-10 deposited with the CCDC. 2020-04-20 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 17.4385(6) _cell_length_b 4.8748(2) _cell_length_c 25.7168(9) _cell_measurement_reflns_used 9130 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 30.616 _cell_measurement_theta_min 3.873 _cell_volume 2186.16(14) _computing_cell_refinement 'BRUKER SANT' _computing_data_collection 'BRUKER APEX-III' _computing_data_reduction 'BRUKER SOFTWARE' _computing_molecular_graphics 'ORTEP-3 (Farrugia, 2000)' _computing_publication_material 'SHELXL-97 (Sheldrick, 1997)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' _diffrn_ambient_temperature 293(2) _diffrn_detector_area_resol_mean none _diffrn_measured_fraction_theta_full 0.989 _diffrn_measured_fraction_theta_max 0.883 _diffrn_measurement_device_type 'D8 Venture' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0189 _diffrn_reflns_av_unetI/netI 0.0183 _diffrn_reflns_Laue_measured_fraction_full 0.989 _diffrn_reflns_Laue_measured_fraction_max 0.883 _diffrn_reflns_limit_h_max 23 _diffrn_reflns_limit_h_min -23 _diffrn_reflns_limit_k_max 6 _diffrn_reflns_limit_k_min -7 _diffrn_reflns_limit_l_max 32 _diffrn_reflns_limit_l_min -35 _diffrn_reflns_number 26505 _diffrn_reflns_point_group_measured_fraction_full 0.989 _diffrn_reflns_point_group_measured_fraction_max 0.830 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.939 _diffrn_reflns_theta_min 2.336 _diffrn_source 'Fine-focus sealed tube' _exptl_absorpt_coefficient_mu 0.332 _exptl_absorpt_correction_T_max 0.7455 _exptl_absorpt_correction_T_min 0.7091 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction. Reference: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10. ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.444 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 992 _exptl_crystal_size_max 0.375 _exptl_crystal_size_mid 0.262 _exptl_crystal_size_min 0.140 _exptl_transmission_factor_max none _exptl_transmission_factor_min none _refine_diff_density_max 0.268 _refine_diff_density_min -0.226 _refine_diff_density_rms 0.043 _refine_ls_abs_structure_details ; Flack x determined using 2368 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.033(13) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.040 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 289 _refine_ls_number_reflns 5734 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.040 _refine_ls_R_factor_all 0.0292 _refine_ls_R_factor_gt 0.0266 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0393P)^2^+0.5525P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0682 _refine_ls_wR_factor_ref 0.0696 _reflns_Friedel_coverage 0.843 _reflns_Friedel_fraction_full 0.990 _reflns_Friedel_fraction_max 0.775 _reflns_number_gt 5430 _reflns_number_total 5734 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d0ce00214c2.cif _cod_data_source_block shelx _cod_depositor_comments ; The following automatic conversions were performed: data item '_chemical_melting_point' value 'none' was changed to '?' -- the value is undefined or not given. data item '_exptl_crystal_density_meas' value 'none' was changed to '?' -- the value is perceived as not measured. Automatic conversion script Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas ; _cod_database_code 7240345 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.7127 _shelx_estimated_absorpt_t_max 0.7461 _exptl_absorpt_special_details none _shelx_res_file ; TITL mo_MMV0312_0ma_a.res in Pna2(1) shelx.res created by SHELXL-2018/3 at 05:08:27 on 10-Apr-2020 CELL 0.71073 17.4385 4.8748 25.7168 90.000 90.000 90.000 ZERR 8.00 0.0006 0.0002 0.0009 0.000 0.000 0.000 LATT -1 SYMM - X, - Y, 1/2 + Z SYMM 1/2 - X, 1/2 + Y, 1/2 + Z SYMM 1/2 + X, 1/2 - Y, Z SFAC C H O CL N UNIT 96 96 16 8 8 MERG 2 EQIV $1 x-1/2, -y+1/2, z HTAB O45 N1_$1 HTAB O45' N1'_$1 EQIV $2 x+1/2, -y+3/2, z HTAB C3 O45'_$2 HTAB C3' O45 FMAP 2 PLAN 20 ACTA BOND $H CONF L.S. 20 TEMP 20.00 WGHT 0.039300 0.552500 FVAR 0.87879 CL1 4 0.794463 -0.214963 0.773429 11.00000 0.02407 0.02281 = 0.01413 0.00341 -0.00258 0.00396 CL2 4 0.548485 -0.224014 0.226233 11.00000 0.02445 0.02193 = 0.01356 -0.00346 0.00313 0.00557 O41 3 0.631884 0.672003 0.610475 11.00000 0.01472 0.01497 = 0.01503 0.00121 0.00098 0.00276 O45 3 0.441146 0.700879 0.559686 11.00000 0.01940 0.03382 = 0.01494 -0.00719 0.00352 -0.01324 AFIX 83 H45 2 0.403799 0.606833 0.567271 11.00000 -1.50000 AFIX 0 N1 5 0.814671 0.132448 0.587579 11.00000 0.01301 0.01712 = 0.01515 0.00041 0.00105 0.00145 O41' 3 0.384665 0.666786 0.387599 11.00000 0.01448 0.01696 = 0.01322 -0.00356 -0.00023 0.00365 O45' 3 0.196131 0.690600 0.440560 11.00000 0.01828 0.02844 = 0.01504 0.00070 -0.00105 -0.00942 AFIX 83 H45' 2 0.158771 0.594822 0.433832 11.00000 -1.50000 AFIX 0 C8 1 0.763163 -0.012019 0.722098 11.00000 0.01640 0.01538 = 0.01225 0.00141 -0.00332 -0.00163 C7 1 0.702143 0.171164 0.731158 11.00000 0.01756 0.01768 = 0.01228 -0.00161 0.00094 -0.00105 AFIX 43 H7 2 0.678781 0.178844 0.763634 11.00000 -1.20000 AFIX 0 C6 1 0.677641 0.337308 0.691793 11.00000 0.01497 0.01596 = 0.01569 -0.00084 0.00222 0.00149 AFIX 43 H6 2 0.636733 0.456093 0.697386 11.00000 -1.20000 AFIX 0 C5 1 0.713965 0.330642 0.642399 11.00000 0.01135 0.01232 = 0.01332 -0.00072 -0.00020 -0.00230 C4 1 0.691276 0.504136 0.600365 11.00000 0.01177 0.01141 = 0.01621 0.00017 -0.00123 -0.00131 C42 1 0.604320 0.844104 0.568711 11.00000 0.01367 0.01445 = 0.01467 0.00325 -0.00064 -0.00025 AFIX 23 H42A 2 0.587485 0.732317 0.539670 11.00000 -1.20000 H42B 2 0.644790 0.965176 0.556758 11.00000 -1.20000 AFIX 0 C43 1 0.537767 1.010065 0.590073 11.00000 0.01380 0.01387 = 0.01850 -0.00014 -0.00018 -0.00003 AFIX 23 H43A 2 0.522163 1.143413 0.564154 11.00000 -1.20000 H43B 2 0.555020 1.110196 0.620496 11.00000 -1.20000 AFIX 0 C44 1 0.468656 0.836504 0.604928 11.00000 0.01337 0.02121 = 0.01128 -0.00078 0.00061 -0.00129 AFIX 23 H44A 2 0.483184 0.702545 0.631021 11.00000 -1.20000 H44B 2 0.428723 0.952259 0.619351 11.00000 -1.20000 AFIX 0 C10 1 0.775648 0.146424 0.634041 11.00000 0.01050 0.01448 = 0.01324 -0.00125 -0.00131 -0.00250 C2 1 0.791920 0.300420 0.550624 11.00000 0.01391 0.01928 = 0.01535 0.00059 0.00282 0.00089 AFIX 43 H2 2 0.818617 0.294241 0.519340 11.00000 -1.20000 AFIX 0 C3 1 0.730792 0.488977 0.554064 11.00000 0.01538 0.01479 = 0.01476 0.00243 -0.00024 -0.00111 AFIX 43 H3 2 0.717583 0.599518 0.525984 11.00000 -1.20000 AFIX 0 C9 1 0.798974 -0.028835 0.674764 11.00000 0.01204 0.01414 = 0.01651 -0.00204 -0.00105 0.00043 AFIX 43 H9 2 0.838310 -0.154656 0.669523 11.00000 -1.20000 AFIX 0 C8' 1 0.517347 -0.018177 0.277099 11.00000 0.01511 0.01383 = 0.01393 -0.00100 0.00367 -0.00003 C7' 1 0.455484 0.161509 0.267895 11.00000 0.01697 0.01807 = 0.01294 0.00011 -0.00232 -0.00002 AFIX 43 H7' 2 0.431763 0.165920 0.235517 11.00000 -1.20000 AFIX 0 C6' 1 0.430718 0.329211 0.307050 11.00000 0.01363 0.01475 = 0.01539 0.00143 -0.00127 0.00110 AFIX 43 H6' 2 0.389176 0.445175 0.301475 11.00000 -1.20000 AFIX 0 C5' 1 0.467907 0.327739 0.356146 11.00000 0.01222 0.01252 = 0.01224 -0.00005 0.00195 -0.00185 C4' 1 0.445290 0.503323 0.397775 11.00000 0.01188 0.01197 = 0.01481 0.00042 0.00102 -0.00178 C42' 1 0.357360 0.841607 0.429201 11.00000 0.01441 0.01427 = 0.01432 -0.00294 0.00086 -0.00126 AFIX 23 H42C 2 0.397701 0.964883 0.440529 11.00000 -1.20000 H42D 2 0.341152 0.731740 0.458666 11.00000 -1.20000 AFIX 0 C43' 1 0.290283 1.003102 0.407628 11.00000 0.01466 0.01401 = 0.01433 -0.00185 0.00136 0.00085 AFIX 23 H43C 2 0.306675 1.098426 0.376441 11.00000 -1.20000 H43D 2 0.275055 1.140320 0.432916 11.00000 -1.20000 AFIX 0 C44' 1 0.221322 0.825417 0.394610 11.00000 0.01437 0.01974 = 0.01386 -0.00043 -0.00056 -0.00011 AFIX 23 H44C 2 0.180349 0.938409 0.380753 11.00000 -1.20000 H44D 2 0.235240 0.690799 0.368486 11.00000 -1.20000 AFIX 0 C10' 1 0.530432 0.147012 0.364612 11.00000 0.01226 0.01298 = 0.01256 0.00070 0.00082 -0.00189 C9' 1 0.553924 -0.030923 0.324152 11.00000 0.01264 0.01532 = 0.01527 0.00077 0.00224 0.00169 AFIX 43 H9' 2 0.593693 -0.154914 0.329454 11.00000 -1.20000 AFIX 0 N1' 5 0.570120 0.139306 0.410915 11.00000 0.01423 0.01697 = 0.01347 0.00163 -0.00050 -0.00006 C2' 1 0.547222 0.309590 0.447570 11.00000 0.01622 0.01923 = 0.01275 0.00043 -0.00184 -0.00330 AFIX 43 H2' 2 0.574549 0.308020 0.478624 11.00000 -1.20000 AFIX 0 C3' 1 0.485164 0.493815 0.444062 11.00000 0.01505 0.01554 = 0.01280 -0.00137 0.00076 -0.00184 AFIX 43 H3' 2 0.471576 0.605030 0.471962 11.00000 -1.20000 AFIX 0 HKLF 4 1.0 1.00 0.00 0.00 0.00 1.00 0.00 0.00 0.00 1.00 REM mo_MMV0312_0ma_a.res in Pna2(1) REM wR2 = 0.0696, GooF = S = 1.040, Restrained GooF = 1.040 for all data REM R1 = 0.0266 for 5430 Fo > 4sig(Fo) and 0.0292 for all 5734 data REM 289 parameters refined using 1 restraints END WGHT 0.0398 0.5481 REM Highest difference peak 0.268, deepest hole -0.226, 1-sigma level 0.043 Q1 1 0.5403 0.0721 0.3418 11.00000 0.05 0.27 Q2 1 0.6885 0.2305 0.7083 11.00000 0.05 0.26 Q3 1 0.4525 0.3143 0.3320 11.00000 0.05 0.26 Q4 1 0.4431 0.2163 0.2913 11.00000 0.05 0.26 Q5 1 0.5018 0.2392 0.3599 11.00000 0.05 0.26 Q6 1 0.7500 0.2689 0.6399 11.00000 0.05 0.25 Q7 1 0.7878 0.0849 0.6575 11.00000 0.05 0.25 Q8 1 0.6971 0.3219 0.6681 11.00000 0.05 0.25 Q9 1 0.5045 0.9223 0.5939 11.00000 0.05 0.23 Q10 1 0.7586 0.3908 0.5532 11.00000 0.05 0.23 Q11 1 0.4716 0.5042 0.4201 11.00000 0.05 0.23 Q12 1 0.7039 0.4223 0.6235 11.00000 0.05 0.22 Q13 1 0.7839 -0.0198 0.6984 11.00000 0.05 0.22 Q14 1 0.4602 0.4241 0.3759 11.00000 0.05 0.22 Q15 1 0.3248 0.9240 0.4158 11.00000 0.05 0.22 Q16 1 0.5474 0.1617 0.3897 11.00000 0.05 0.21 Q17 1 0.5706 0.9192 0.5825 11.00000 0.05 0.21 Q18 1 0.7120 0.4908 0.5766 11.00000 0.05 0.21 Q19 1 0.2585 0.9172 0.4035 11.00000 0.05 0.21 Q20 1 0.5394 -0.0185 0.3005 11.00000 0.05 0.21 ; _shelx_res_checksum 56469 _shelx_hkl_file ; 0 -1 0 0.70 0.60 0 -1 0 0.20 0.50 0 1 0 -0.20 0.60 0 1 0 0.40 0.30 0 -3 0 0.70 1.40 0 3 0 -2.80 1.60 0 -3 0 -1.10 1.60 0 -4 0 806.82 18.20 0 4 0 814.72 18.20 0 -5 0 3.20 3.50 0 5 0 1.40 3.90 0 -6 0 5657.23 108.59 0 6 0 6117.79 112.89 0 -6 0 5502.75 110.39 0 -1 1 107.39 2.20 0 1 1 109.79 2.40 0 1 1 96.49 2.70 0 -1 1 110.29 2.30 0 1 1 106.69 2.80 0 -1 1 108.59 2.80 0 -1 -1 104.99 2.80 0 1 -1 105.59 2.80 0 -1 -1 103.79 2.60 0 2 1 0.40 0.70 0 -2 1 -0.10 0.70 0 2 1 0.10 1.10 0 -2 1 1.00 0.90 0 -2 1 -1.90 1.20 0 -2 -1 -2.30 1.20 0 2 -1 0.10 1.30 0 -2 -1 -0.10 1.10 0 -3 1 15.80 2.20 0 3 1 18.10 2.20 0 -3 1 25.30 2.30 0 -3 -1 17.80 2.30 0 -3 -1 16.50 1.90 0 3 -1 14.20 2.20 0 4 1 -5.80 2.90 0 -4 1 -2.10 2.40 0 -4 -1 -1.10 2.40 0 4 -1 -4.60 2.70 0 5 1 35.60 4.80 0 -5 1 39.50 4.60 0 -5 -1 30.60 4.70 0 5 -1 27.00 5.10 0 -6 1 18.20 5.80 0 6 1 -10.10 8.00 0 -6 1 -7.10 7.90 0 -6 -1 12.20 6.50 0 -6 -1 -3.80 8.20 0 1 2 2.10 0.80 0 -1 2 0.80 0.40 0 -1 2 1.60 0.90 0 1 -2 0.70 0.90 0 -1 -2 1.10 0.80 0 -2 2 1725.53 31.10 0 2 2 1666.93 31.30 0 2 2 1692.13 31.20 0 2 2 1736.53 32.20 0 -2 2 1710.63 32.20 0 -2 -2 1672.23 32.10 0 -2 -2 1740.63 31.90 0 2 -2 1731.63 32.30 0 3 2 -1.30 0.60 0 -3 2 3.90 1.90 0 -3 2 0.00 1.10 0 3 2 1.90 1.70 0 -3 -2 -0.60 1.70 0 -3 -2 0.90 1.50 0 3 -2 -0.10 1.80 0 4 2 623.64 15.20 0 -4 2 635.94 14.90 0 4 -2 624.34 15.40 0 -4 -2 625.14 14.90 0 -5 2 -2.00 3.50 0 5 2 1.80 4.40 0 -5 -2 -0.90 3.50 0 5 -2 4.10 4.10 0 -6 2 121.19 13.20 0 6 2 105.09 11.70 0 -6 2 147.89 10.20 0 -6 -2 125.39 10.50 0 -6 -2 135.89 12.80 0 -7 2 9.50 14.00 0 0 3 0.10 0.40 0 0 3 0.00 0.40 0 0 -3 0.70 0.50 0 2 3 -0.40 1.20 0 -2 3 0.80 1.30 0 2 3 0.30 0.80 0 2 3 -0.60 1.00 0 -2 3 0.40 0.70 0 2 -3 0.20 1.40 0 -2 -3 -2.70 1.30 0 -2 -3 0.90 1.20 0 -3 3 528.85 10.60 0 3 3 526.15 12.00 0 -3 3 521.05 12.00 0 3 3 534.95 10.20 0 3 3 535.35 10.40 0 3 -3 507.35 12.10 0 -3 -3 521.35 11.80 0 -3 -3 528.65 12.10 0 4 3 -6.60 2.90 0 -4 3 -2.80 1.60 0 -4 3 -3.30 2.40 0 4 -3 -6.50 3.10 0 -4 -3 -0.30 2.60 0 -5 3 398.86 12.20 0 5 3 391.16 12.50 0 -5 -3 389.36 12.20 0 -6 3 -15.80 7.20 0 -6 3 20.00 6.20 0 -6 -3 7.80 5.70 0 -6 -3 -3.40 8.30 0 -7 3 19.30 20.60 0 -1 4 -1.10 0.50 0 1 4 1.00 0.90 0 -1 -4 0.50 0.80 0 2 4 2432.66 45.10 0 -2 4 2387.26 43.90 0 2 4 2403.56 44.60 0 -2 4 2447.56 45.20 0 -2 -4 2440.06 45.10 0 -2 -4 2456.65 45.20 0 3 4 -0.60 1.30 0 -3 4 -1.30 1.00 0 -3 4 -0.90 2.00 0 3 4 -2.20 1.60 0 3 4 -0.30 1.10 0 3 -4 0.80 2.00 0 -3 -4 -5.10 1.70 0 -3 -4 0.90 1.80 0 -4 4 2055.19 38.60 0 -4 4 2059.19 40.40 0 -4 -4 2071.59 40.60 0 5 4 -0.90 4.50 0 -5 4 3.10 3.60 0 -5 -4 -4.40 4.00 0 -6 4 1193.48 29.40 0 -6 4 1222.08 27.70 0 6 4 1115.19 28.30 0 -6 -4 1151.08 30.60 0 -6 -4 1175.78 28.20 0 -2 5 -0.70 0.80 0 2 5 0.90 1.20 0 -2 5 3.20 1.40 0 2 5 2.90 1.30 0 -2 -5 1.40 1.40 0 -2 -5 -1.90 1.20 0 -3 5 2804.42 51.99 0 3 5 2847.81 52.49 0 -3 5 2848.81 53.69 0 3 5 2880.81 53.69 0 3 5 2916.91 52.19 0 -3 -5 2838.22 53.79 0 -3 -5 2869.51 53.59 0 -4 5 0.20 2.60 0 4 5 -1.80 2.80 0 4 5 0.20 0.90 0 -4 5 -2.20 1.60 0 -4 -5 1.00 2.70 0 -4 -5 3.30 3.10 0 -5 5 214.68 9.10 0 5 5 209.78 9.50 0 -5 -5 202.28 9.20 0 6 5 -12.30 7.30 0 -6 5 4.70 6.40 0 -6 5 -5.30 7.00 0 -6 -5 -3.40 7.80 0 -6 -5 -7.90 6.60 0 1 6 -0.30 1.10 0 -1 6 0.80 0.50 0 1 -6 -1.10 0.60 0 -2 6 1373.96 26.80 0 2 6 1370.16 26.70 0 -2 6 1373.06 25.50 0 2 6 1398.46 26.60 0 -2 -6 1423.66 27.00 0 -2 -6 1366.66 26.90 0 -3 6 -1.80 2.00 0 3 6 -0.90 1.50 0 3 6 -1.60 2.00 0 3 6 -1.50 1.40 0 -3 6 0.50 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33.50 3.20 1 -3 2 26.90 3.00 1 -3 2 33.90 2.00 1 -3 2 30.30 2.30 -1 3 -2 23.50 2.50 1 -3 -2 35.00 3.10 1 -3 -2 28.30 2.90 1 -4 2 30.50 3.20 -1 4 2 29.40 3.30 -1 4 -2 32.20 3.40 1 -4 -2 30.30 3.30 1 -4 -2 29.40 3.00 -1 5 2 483.35 13.80 1 -5 2 498.45 13.50 1 -5 -2 504.25 13.80 -1 5 -2 487.55 14.10 1 -6 2 72.99 9.20 1 -6 2 107.69 10.40 1 -6 -2 91.99 10.10 1 -6 -2 105.79 9.50 1 -7 2 39.10 12.40 -1 -7 3 63.49 13.50 -1 -6 3 4.20 5.80 1 6 3 -17.40 7.10 -1 -6 -3 10.20 6.60 -1 -5 3 713.23 17.90 1 5 3 701.13 18.20 -1 -5 -3 702.03 18.00 1 5 -3 698.03 19.00 -1 -4 3 72.99 5.70 -1 -4 3 74.29 3.90 1 4 3 63.49 5.60 -1 -4 -3 75.19 5.60 1 4 -3 72.69 5.90 1 3 3 621.14 12.30 1 3 3 595.24 11.90 -1 -3 3 607.34 12.30 -1 -3 3 618.04 13.70 1 3 3 604.54 13.70 -1 -3 -3 587.54 13.70 1 3 -3 594.14 13.90 -1 -2 3 567.64 11.30 1 2 3 585.64 11.80 1 2 3 573.84 11.50 1 2 3 577.24 12.30 -1 -2 3 583.34 12.40 -1 -2 -3 586.54 12.40 1 2 -3 578.84 12.50 -1 -2 -3 581.94 12.10 1 1 3 1644.54 30.80 -1 -1 3 1654.13 30.40 1 1 3 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482.15 9.50 1 4 4 474.75 12.70 -1 -4 -4 493.05 12.90 1 4 -4 479.75 13.00 1 3 4 2107.89 39.50 -1 -3 4 2009.50 37.90 1 3 4 2027.90 37.80 -1 -3 4 2059.89 39.50 1 3 4 2053.99 38.20 -1 -3 -4 2021.90 39.50 1 3 -4 2037.10 39.60 -1 -3 -4 2094.09 39.20 -1 -2 4 1563.74 29.30 1 2 4 1570.84 30.30 1 2 4 1615.04 29.70 1 2 4 1598.44 30.00 -1 -2 4 1563.24 30.40 1 2 -4 1616.64 30.60 -1 -2 -4 1640.44 30.40 -1 -2 -4 1564.14 30.40 1 1 4 2024.80 36.90 1 1 4 1986.40 36.90 -1 -1 4 1968.60 36.90 -1 -1 4 2018.70 36.40 -1 -1 4 1987.70 36.30 -1 -1 -4 1948.41 36.90 -1 -1 -4 2034.80 36.90 1 1 -4 2002.90 36.20 1 0 4 0.60 0.70 -1 0 4 -0.70 0.70 -1 0 4 1.00 0.60 1 0 -4 0.40 0.60 -1 0 -4 0.70 0.70 1 0 -4 0.00 0.70 -1 1 4 2031.00 37.10 -1 1 4 2026.60 37.10 1 -1 -4 1999.10 37.10 1 -1 -4 2028.90 37.20 1 -2 4 1564.84 28.60 1 -2 4 1595.34 30.00 -1 2 4 1567.14 29.40 -1 2 4 1592.44 29.90 1 -2 4 1553.54 28.60 1 -2 -4 1594.44 30.00 1 -2 -4 1634.94 30.00 -1 3 4 2049.49 38.50 1 -3 4 2011.40 38.50 -1 3 4 1957.90 36.60 -1 3 4 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27.10 -1 -3 6 1328.67 25.40 -1 -3 -6 1334.37 27.20 -1 -3 -6 1329.17 27.00 -1 -2 6 566.04 12.50 1 2 6 555.74 12.40 -1 -2 6 573.54 11.30 1 2 6 557.04 12.10 -1 -2 -6 558.04 12.50 -1 -2 -6 574.04 12.50 -1 -1 6 718.53 13.60 1 1 6 726.63 14.50 -1 -1 6 728.53 14.00 1 1 6 713.73 14.50 -1 -1 -6 718.33 14.70 1 1 -6 715.53 13.80 -1 -1 -6 729.63 14.60 1 0 6 -0.40 0.80 -1 0 6 -0.10 0.70 -1 0 6 -0.60 0.90 -1 0 -6 -1.00 0.80 1 0 -6 0.80 0.70 1 0 -6 0.50 0.90 1 -1 6 716.93 13.60 1 -1 6 705.43 13.10 -1 1 6 730.93 14.40 -1 1 6 739.23 14.40 1 -1 -6 725.33 14.50 1 -1 -6 717.63 14.80 1 -2 6 553.34 12.00 1 -2 6 565.54 10.70 -1 2 6 558.04 11.70 -1 2 6 565.54 12.00 1 -2 -6 565.14 12.30 1 -2 -6 569.24 12.20 -1 3 6 1335.67 25.30 1 -3 6 1313.67 24.60 -1 3 6 1344.87 25.10 1 -3 6 1322.77 26.50 -1 3 6 1348.17 26.40 1 -3 -6 1324.67 26.60 1 -3 -6 1330.47 26.60 1 -4 6 116.09 5.90 1 -4 6 117.79 3.90 -1 4 6 111.89 6.90 1 -4 -6 117.49 6.10 1 -4 -6 116.79 6.20 1 -5 6 60.39 7.10 -1 5 6 80.29 7.60 1 -5 -6 65.59 6.80 1 -5 -6 66.19 7.60 1 -6 6 130.09 11.10 1 -6 6 133.29 13.00 1 -6 -6 144.69 12.40 1 -6 -6 152.48 11.70 -1 -6 7 67.59 7.50 -1 -6 -7 64.09 9.70 -1 -6 -7 57.19 7.70 -1 -5 7 285.87 8.60 -1 -5 7 297.97 11.10 1 5 7 289.07 11.50 -1 -5 -7 295.37 11.50 1 4 7 125.79 6.40 -1 -4 7 125.29 6.40 1 4 7 130.89 5.00 -1 -4 7 130.79 4.70 1 4 7 127.69 4.70 -1 -4 -7 140.09 7.00 -1 -3 7 375.26 8.30 1 3 7 363.96 9.20 1 3 7 371.96 8.80 1 3 7 378.56 9.80 -1 -3 7 366.46 9.80 -1 -3 -7 384.86 10.10 -1 -3 -7 385.46 10.20 -1 -2 7 1962.00 36.40 -1 -2 7 1961.20 36.70 1 2 7 1972.90 37.50 -1 -2 7 1957.20 37.60 1 2 7 1927.41 37.30 -1 -2 -7 2032.30 37.90 -1 -2 -7 1999.50 37.70 1 1 7 614.44 12.90 -1 -1 7 615.84 11.80 -1 -1 7 620.74 12.30 1 1 7 612.94 12.90 1 1 -7 615.14 12.00 -1 -1 -7 639.54 13.00 1 1 -7 624.84 12.20 -1 0 7 -0.60 0.90 -1 0 7 1.70 1.00 1 0 7 -0.70 0.90 -1 0 -7 2.50 1.00 1 0 -7 0.70 1.00 1 0 -7 1.10 0.80 -1 1 7 627.44 12.90 1 -1 7 615.44 12.10 -1 1 7 613.54 12.80 1 -1 -7 633.44 13.30 1 -1 -7 630.24 13.00 -1 2 7 1990.20 37.50 -1 2 7 1967.80 37.40 1 -2 7 1969.00 36.20 1 -2 7 1972.60 37.60 1 -2 -7 2050.79 37.90 1 -2 -7 1979.20 37.70 -1 3 7 378.46 8.70 1 -3 7 371.06 7.80 1 -3 7 365.56 9.60 -1 3 7 370.26 9.50 1 -3 -7 365.96 9.80 1 -3 -7 388.66 9.80 -1 4 7 108.79 7.50 -1 4 7 126.79 3.60 1 -4 7 121.89 4.00 -1 4 7 128.49 3.90 1 -4 7 120.79 6.20 1 -4 -7 133.29 6.70 1 -4 -7 133.49 6.50 -1 5 7 290.67 10.70 1 -5 7 281.87 8.10 1 -5 7 297.57 10.40 1 -5 -7 301.57 11.10 1 -5 -7 277.37 14.30 1 -6 7 59.59 7.60 -1 6 7 55.69 7.70 1 -6 7 70.39 7.50 1 -6 -7 58.59 7.80 1 -6 -7 70.49 10.80 -1 -6 8 118.79 11.20 -1 -6 -8 102.59 11.60 -1 -6 -8 90.49 10.90 1 5 8 258.57 11.10 -1 -5 8 281.57 10.90 -1 -5 8 253.97 8.10 -1 -5 -8 246.78 11.00 1 4 8 350.56 9.00 1 4 8 362.86 11.00 -1 -4 8 378.66 11.10 1 4 8 364.46 8.80 -1 -4 8 360.06 8.60 -1 -4 -8 351.66 11.20 1 3 8 35.90 3.80 -1 -3 8 30.50 2.70 1 3 8 29.10 2.80 -1 -3 8 35.90 3.70 -1 -3 -8 28.00 3.20 -1 -3 -8 20.00 2.80 -1 -2 8 1808.32 33.80 -1 -2 8 1830.82 33.80 1 2 8 1844.12 35.00 1 2 8 1841.72 34.90 -1 -2 8 1820.82 35.10 -1 -2 -8 1785.92 35.10 -1 -2 -8 1785.62 34.90 -1 -1 8 57.49 2.50 1 1 8 52.79 3.00 -1 -1 8 58.79 2.00 1 1 8 54.79 3.20 -1 -1 -8 52.69 3.00 1 1 -8 55.79 2.10 1 1 -8 55.19 2.50 -1 0 8 -0.20 1.00 -1 0 8 -0.70 1.00 1 0 8 0.00 1.00 -1 0 -8 0.50 0.90 1 0 -8 -1.20 1.00 1 0 -8 0.50 0.90 -1 0 -8 2.40 1.10 1 -1 8 56.99 1.30 1 -1 8 56.39 2.40 -1 1 8 59.09 2.90 -1 1 8 55.49 2.90 1 -1 -8 54.89 3.00 1 -1 -8 56.99 3.20 -1 2 8 1794.82 34.80 -1 2 8 1855.21 35.00 1 -2 8 1837.02 33.70 1 -2 8 1826.32 35.10 1 -2 -8 1855.01 35.30 1 -3 8 28.90 2.20 -1 3 8 29.30 2.80 -1 3 8 33.00 2.90 1 -3 8 26.30 2.90 1 -3 -8 28.70 3.10 1 -3 -8 22.40 3.00 -1 4 8 364.26 8.20 -1 4 8 355.66 7.90 -1 4 8 373.56 10.60 1 -4 8 356.36 8.00 1 -4 8 364.46 10.70 1 -4 -8 308.67 12.10 1 -4 -8 344.87 10.50 1 -5 8 257.27 7.50 1 -5 8 261.77 9.90 -1 5 8 256.17 10.30 1 -5 -8 252.27 10.90 1 -5 -8 271.37 13.10 1 -5 -8 260.07 10.50 1 -6 8 108.99 11.20 -1 6 8 112.59 13.00 1 -6 8 128.69 12.00 1 -6 -8 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56.39 -2 6 1 435.86 15.90 2 -6 1 449.06 14.80 2 -6 1 465.75 17.90 2 -6 -1 444.86 14.90 2 -6 -1 442.26 18.30 2 -7 1 79.89 14.80 -2 -7 2 -1.30 11.10 -2 -7 -2 13.30 13.20 2 6 2 394.86 16.90 -2 -6 2 456.55 15.90 -2 -6 -2 457.65 16.30 -2 -5 2 238.58 10.30 2 5 2 212.08 10.80 2 5 -2 227.28 10.20 -2 -5 -2 216.18 9.50 2 4 2 106.19 2.80 2 4 2 104.19 6.50 -2 -4 2 112.59 6.30 -2 -4 -2 109.99 6.40 2 4 -2 105.59 6.70 2 3 2 4.70 1.50 -2 -3 2 11.70 2.40 2 3 2 9.70 2.40 -2 -3 2 9.30 1.60 2 3 2 9.00 1.40 2 3 -2 8.70 1.00 -2 -3 -2 8.60 2.10 2 3 -2 7.80 2.20 -2 -2 2 1587.74 30.60 2 2 2 1604.04 29.70 2 2 2 1582.34 30.00 2 2 2 1634.34 30.70 -2 -2 2 1597.94 29.70 2 2 -2 1640.34 30.70 2 2 -2 1594.34 29.40 2 2 -2 1570.54 29.50 -2 -2 -2 1579.74 30.60 2 1 2 2013.60 37.20 -2 -1 2 2014.60 37.30 2 1 2 2076.19 37.00 -2 -1 2 1964.30 36.70 2 1 2 2001.50 37.10 -2 -1 -2 2004.90 37.20 2 1 -2 2061.69 37.30 2 1 -2 2009.50 36.70 2 -1 -2 2056.29 37.50 2 -1 -2 2075.09 38.20 2 -2 2 1605.44 30.00 -2 2 2 1577.74 29.90 2 -2 -2 1619.54 29.80 2 -2 -2 1607.54 30.00 -2 2 -2 1629.84 30.10 2 -3 2 5.70 1.20 2 -3 2 7.90 1.80 2 -3 2 9.50 1.10 -2 3 2 9.50 1.90 -2 3 -2 9.40 2.00 2 -3 -2 8.50 1.70 2 -4 2 104.29 5.20 -2 4 2 104.89 5.40 -2 4 -2 100.99 5.80 2 -4 -2 110.69 5.10 2 -4 -2 106.29 5.30 2 -4 -2 111.29 7.10 -2 5 2 217.68 9.80 2 -5 2 258.57 9.40 2 -5 2 262.07 10.60 2 -5 -2 240.28 9.00 2 -5 -2 225.98 12.00 2 -6 2 461.05 14.70 -2 6 2 434.16 15.50 2 -6 2 450.95 17.50 2 -6 -2 453.95 14.90 2 -6 -2 432.26 17.40 2 6 3 9.80 8.60 -2 -6 3 43.00 6.90 -2 -6 -3 41.60 7.10 -2 -5 3 31.50 4.90 2 5 3 19.20 5.40 -2 -5 -3 30.80 5.00 2 5 -3 12.70 5.40 -2 -4 3 1042.50 20.90 -2 -4 3 1048.40 22.40 2 4 3 1030.20 19.40 2 4 3 1005.70 19.50 2 4 3 1030.90 22.50 2 4 -3 1026.10 22.70 -2 -4 -3 1032.50 22.60 2 3 3 1254.37 25.00 -2 -3 3 1207.08 24.80 -2 -3 3 1187.48 23.50 2 3 3 1207.88 23.70 2 3 3 1226.28 23.30 -2 -3 -3 1227.68 25.00 2 3 -3 1268.47 25.20 -2 -2 3 185.08 4.60 -2 -2 3 189.38 5.50 2 2 3 188.08 4.80 2 2 3 184.88 5.10 2 2 3 185.18 5.40 -2 -2 -3 189.18 5.50 2 2 -3 185.88 4.40 2 2 -3 183.98 5.60 2 2 -3 184.48 4.30 -2 2 3 186.58 4.00 2 -2 3 184.38 4.80 -2 2 3 185.28 4.00 -2 2 3 187.88 4.80 2 -2 -3 186.48 5.90 2 -2 -3 180.98 4.80 2 -2 -3 185.38 4.80 2 -3 3 1210.18 22.60 2 -3 3 1207.08 22.40 2 -3 3 1214.98 24.00 -2 3 3 1238.38 24.00 2 -3 -3 1227.68 24.10 2 -3 -3 1221.78 23.80 2 -4 3 1053.59 21.70 -2 4 3 1054.59 21.80 2 -4 -3 1026.70 21.80 2 -4 -3 1039.40 21.50 2 -4 -3 1034.30 23.70 2 -5 3 35.60 5.40 2 -5 3 32.00 4.30 2 -5 -3 26.10 5.60 2 -5 -3 34.50 4.30 2 -6 3 44.40 6.10 -2 6 3 31.90 7.00 2 -6 3 50.59 8.20 2 -6 -3 53.99 6.50 2 -6 -3 41.90 9.10 -2 -6 4 335.27 14.20 -2 -6 -4 308.67 14.50 2 5 4 514.75 15.70 -2 -5 4 536.85 15.20 -2 -5 -4 550.14 15.70 2 5 -4 543.25 16.30 2 4 4 261.17 6.30 2 4 4 265.27 6.60 2 4 4 262.47 9.20 -2 -4 4 278.27 8.90 -2 -4 4 257.87 7.30 -2 -4 -4 266.47 9.20 2 4 -4 274.57 9.60 2 3 4 850.01 17.60 2 3 4 875.41 18.70 2 3 4 876.41 17.20 -2 -3 4 862.41 17.20 -2 -3 4 894.41 18.80 2 3 -4 891.91 19.00 -2 -3 -4 865.21 18.80 2 2 4 282.37 6.90 -2 -2 4 279.17 7.30 2 2 4 273.97 6.50 2 2 4 278.77 7.20 -2 -2 4 277.67 6.20 2 2 -4 279.47 7.40 2 2 -4 276.17 5.80 -2 -2 -4 276.37 7.20 2 1 4 2311.77 42.40 -2 -1 4 2255.37 41.90 2 1 4 2314.67 42.40 -2 -1 4 2318.87 42.00 -2 -1 4 2309.77 42.50 2 1 -4 2300.17 41.80 -2 -1 -4 2262.37 42.40 -2 0 4 1918.91 35.00 2 0 4 1891.91 35.10 -2 0 4 1913.11 35.00 2 0 -4 1932.21 35.00 2 0 -4 1913.41 35.10 -2 1 4 2252.97 41.80 -2 1 4 2284.67 41.70 2 -1 -4 2298.27 42.50 2 -1 -4 2315.57 42.00 2 -2 4 282.77 6.60 -2 2 4 285.67 6.60 -2 2 4 281.77 6.10 2 -2 -4 279.37 7.80 2 -2 -4 275.47 6.70 2 -2 -4 278.07 6.80 -2 3 4 890.71 17.90 2 -3 4 860.31 16.30 2 -3 4 889.71 17.90 2 -3 4 854.81 16.10 2 -3 -4 869.01 18.00 2 -3 -4 869.51 17.90 2 -4 4 258.47 6.20 2 -4 4 261.87 8.20 -2 4 4 260.67 8.30 2 -4 -4 260.37 8.30 2 -4 -4 266.27 10.00 2 -4 -4 256.77 8.00 -2 5 4 522.85 14.60 2 -5 4 545.45 15.50 2 -5 4 566.14 14.50 2 -5 -4 535.55 14.30 2 -5 -4 539.05 14.30 2 -5 -4 546.65 16.90 2 -6 4 321.87 12.80 2 -6 4 328.07 14.90 -2 6 4 271.57 13.50 2 -6 -4 353.16 17.50 2 -6 -4 317.77 12.50 -2 -6 5 45.00 7.00 -2 -6 -5 31.30 7.20 2 5 5 15.90 5.10 -2 -5 5 17.90 4.40 -2 -5 -5 8.60 4.60 2 4 5 150.38 7.40 -2 -4 5 148.19 5.40 2 4 5 156.48 5.10 2 4 5 151.18 4.80 -2 -4 5 156.98 7.30 2 4 -5 152.78 7.80 -2 -4 -5 159.88 7.40 2 3 5 270.77 6.70 2 3 5 265.67 7.20 -2 -3 5 276.07 6.70 2 3 5 275.77 8.20 -2 -3 5 273.77 8.20 -2 -3 -5 270.47 8.00 2 3 -5 263.77 8.20 2 2 5 3869.91 70.49 2 2 5 3814.52 70.19 -2 -2 5 3861.81 70.59 -2 -2 5 3788.62 69.39 2 2 -5 3900.91 70.69 2 2 -5 3799.52 68.99 -2 -2 -5 3756.12 70.49 -2 -1 5 419.36 8.50 2 1 5 424.56 9.10 -2 -1 5 421.16 8.60 -2 -1 5 415.76 9.10 2 1 5 411.76 9.00 2 1 -5 426.66 8.60 2 1 -5 416.16 8.70 -2 -1 -5 409.96 9.10 -2 0 5 2330.77 42.20 2 0 5 2347.36 42.20 -2 0 5 2249.68 42.30 2 0 -5 2316.47 42.30 -2 1 5 410.86 8.60 -2 1 5 419.46 8.70 2 -1 -5 412.86 8.80 2 -1 -5 413.46 9.20 2 -2 5 3794.02 70.09 -2 2 5 3818.92 69.69 -2 2 5 3836.32 70.09 2 -2 -5 3981.60 70.39 2 -2 -5 3798.32 70.19 2 -2 -5 3830.02 71.39 2 -3 5 270.77 7.40 -2 3 5 269.77 5.70 2 -3 5 268.67 5.50 -2 3 5 272.27 7.40 -2 3 5 273.27 5.90 2 -3 -5 263.27 7.40 2 -3 -5 267.97 7.50 2 -3 -5 276.27 8.90 2 -4 5 154.28 6.30 -2 4 5 156.18 6.30 2 -4 5 153.48 4.30 2 -4 -5 154.68 8.20 2 -4 -5 148.19 6.30 2 -4 -5 149.79 6.60 2 -5 5 16.40 3.90 -2 5 5 18.80 4.60 2 -5 5 12.70 4.60 2 -5 -5 16.50 6.20 2 -5 -5 10.10 3.70 2 -5 -5 11.90 4.20 -2 6 5 15.70 8.10 2 -6 5 33.10 7.30 2 -6 5 39.00 6.30 2 -6 -5 30.60 6.00 2 -6 -5 23.80 8.20 -2 -6 6 191.18 12.60 -2 -6 -6 214.38 13.00 2 5 6 244.48 12.50 -2 -5 6 242.88 10.50 -2 -5 6 215.78 7.80 -2 -5 -6 230.88 10.50 -2 -4 6 12.00 2.30 -2 -4 6 12.70 3.00 2 4 6 13.30 2.10 2 4 6 11.60 2.30 2 4 6 14.40 3.10 -2 -4 -6 7.60 3.40 2 3 6 437.76 9.90 -2 -3 6 432.26 9.50 -2 -3 6 431.96 11.20 2 3 6 429.16 10.30 2 3 6 432.06 11.10 -2 -3 -6 446.06 11.30 2 2 6 6050.99 109.79 2 2 6 6058.69 109.99 -2 -2 -6 6024.50 110.09 -2 -2 -6 6022.80 109.89 -2 -1 6 22.20 1.90 2 1 6 24.80 2.20 2 1 6 22.20 2.10 -2 -1 6 25.10 1.60 2 1 -6 27.00 1.70 -2 -1 -6 25.70 2.20 2 1 -6 26.80 1.80 -2 -1 -6 26.40 2.20 -2 0 6 50.09 2.20 -2 0 6 50.39 2.30 2 0 6 53.29 2.20 2 0 -6 48.60 2.10 2 0 -6 46.70 2.30 -2 1 6 23.30 2.10 2 -1 -6 27.90 2.40 2 -1 -6 26.40 2.10 2 -2 -6 5918.11 108.39 -2 3 6 431.46 9.10 -2 3 6 434.26 9.00 2 -3 6 430.76 10.30 2 -3 6 422.86 8.40 -2 3 6 435.36 10.30 2 -3 -6 434.76 10.60 2 -3 -6 444.36 10.70 2 -3 -6 434.76 12.00 -2 4 6 10.40 2.80 2 -4 6 12.90 1.60 2 -4 6 17.00 3.00 2 -4 -6 10.80 2.80 2 -4 -6 18.80 3.20 2 -4 -6 6.40 3.80 2 -5 6 229.98 9.90 -2 5 6 241.38 9.80 2 -5 6 231.68 9.30 2 -5 -6 238.88 12.50 2 -5 -6 231.68 9.90 2 -5 -6 235.38 9.70 2 -6 6 198.98 11.30 2 -6 6 182.28 13.40 2 -6 -6 190.98 16.80 2 -6 -6 211.48 12.20 -2 -6 7 179.68 12.50 -2 -6 -7 188.68 14.00 2 5 7 313.77 7.00 2 5 7 329.67 7.10 -2 -5 7 320.97 9.50 -2 -5 7 330.57 11.90 -2 -5 -7 319.47 12.30 -2 -4 7 88.29 6.30 -2 -4 7 80.49 4.10 2 4 7 80.29 4.70 2 4 7 83.29 6.30 2 4 7 72.89 4.00 -2 -4 -7 80.49 6.50 2 3 7 1415.86 28.60 -2 -3 7 1412.86 28.70 2 3 7 1416.66 27.40 -2 -3 7 1401.36 27.00 2 3 7 1423.66 27.90 -2 -3 -7 1410.96 28.80 -2 -2 7 402.76 8.90 -2 -2 7 401.56 9.80 -2 -2 7 398.46 8.70 2 2 7 390.26 9.60 2 2 7 396.96 9.70 -2 -2 -7 395.66 9.70 -2 -2 -7 402.46 9.90 2 2 -7 389.76 8.00 2 1 7 651.43 13.60 -2 -1 7 655.83 12.60 2 1 7 642.44 13.50 -2 -1 7 649.24 13.00 -2 -1 -7 649.74 13.70 2 1 -7 655.43 12.80 2 1 -7 640.94 12.90 -2 -1 -7 644.24 13.50 -2 0 7 1404.16 26.50 -2 0 7 1409.56 26.30 2 0 7 1411.16 26.40 2 0 -7 1381.06 26.20 2 0 -7 1408.56 26.50 -2 1 7 628.14 13.00 2 -1 7 643.64 12.30 2 -1 -7 632.04 13.50 2 -1 -7 648.14 13.30 -2 2 7 398.06 9.10 2 -2 7 406.56 9.30 -2 2 7 395.26 9.00 2 -2 -7 391.06 9.40 2 -2 -7 400.16 10.40 -2 3 7 1370.06 26.60 2 -3 7 1384.96 25.70 2 -3 7 1429.76 27.80 -2 3 7 1395.86 27.50 2 -3 -7 1412.36 28.10 2 -3 -7 1410.46 27.90 2 -3 -7 1403.76 29.50 -2 4 7 70.29 5.20 2 -4 7 74.89 3.10 2 -4 7 74.29 5.60 2 -4 7 80.19 5.30 2 -4 -7 76.79 5.90 2 -4 -7 90.39 5.80 2 -4 -7 86.39 7.40 2 -5 7 320.47 11.50 2 -5 7 331.37 8.50 -2 5 7 328.57 10.90 2 -5 7 327.57 10.70 2 -5 -7 323.97 13.60 2 -5 -7 323.17 11.40 2 -5 -7 331.17 11.60 2 -6 7 171.38 11.00 2 -6 7 196.98 13.20 2 -6 -7 182.98 12.20 2 -6 -7 187.78 15.30 -2 -6 8 14.10 8.20 -2 -6 8 14.20 6.70 -2 -6 -8 2.90 6.90 -2 -5 8 7.90 4.60 -2 -5 8 5.50 3.20 2 5 8 4.90 2.30 2 5 8 4.00 2.20 -2 -5 -8 3.40 4.60 2 4 8 429.46 10.70 2 4 8 422.86 12.30 2 4 8 428.46 10.10 -2 -4 8 428.26 12.30 -2 -4 8 426.16 10.10 -2 -4 -8 430.76 12.60 2 3 8 158.78 6.00 -2 -3 8 163.48 6.60 2 3 8 156.48 5.40 2 3 8 155.28 6.50 -2 -3 8 154.28 4.90 -2 -3 8 167.58 6.00 -2 -3 -8 159.38 6.40 -2 -2 8 3168.58 58.69 -2 -2 8 3240.28 58.59 -2 -2 8 3229.08 59.89 2 2 8 3127.39 59.49 2 2 8 3265.27 59.79 2 2 -8 3216.08 57.99 -2 -2 -8 3173.58 59.89 -2 -2 -8 3191.08 59.69 -2 -1 8 4092.69 74.29 2 1 8 4046.60 74.79 2 1 8 4096.99 74.89 -2 -1 -8 4218.08 74.89 -2 -1 -8 3958.00 74.99 -2 1 8 4117.69 75.39 2 -1 -8 4137.39 75.49 2 -1 -8 4118.89 75.79 -2 2 8 3139.49 58.29 2 -2 8 3134.09 57.09 -2 2 8 3193.68 58.49 2 -2 8 3096.29 57.19 2 -2 -8 3218.38 59.79 2 -2 -8 3196.18 58.89 -2 3 8 160.68 5.70 2 -3 8 158.78 3.90 -2 3 8 164.08 5.10 2 -3 8 159.98 5.90 2 -3 -8 140.49 7.00 2 -3 -8 154.08 6.30 2 -3 -8 162.58 6.10 -2 4 8 432.86 9.00 -2 4 8 430.36 8.80 -2 4 8 409.06 12.40 2 -4 8 419.56 8.90 2 -4 8 425.26 11.40 2 -4 8 422.06 11.20 2 -4 -8 426.96 13.90 2 -4 -8 437.96 11.70 2 -5 8 0.80 3.90 2 -5 8 1.10 4.20 -2 5 8 3.40 4.10 2 -5 8 -0.50 2.40 2 -5 -8 1.60 5.50 2 -5 -8 3.70 4.90 2 -5 -8 6.90 4.00 2 -6 8 0.90 6.60 2 -6 8 9.30 6.00 2 -6 -8 17.90 8.50 2 -6 -8 2.60 6.60 -2 -6 9 38.20 9.30 -2 -6 9 36.20 7.50 -2 -6 -9 51.79 8.20 -2 -5 9 35.20 5.30 -2 -5 9 31.40 5.30 2 5 9 40.50 4.30 -2 -5 9 32.80 3.90 2 5 9 36.50 3.00 -2 -5 -9 31.80 5.60 -2 -4 9 116.69 6.80 2 4 9 123.19 5.20 2 4 9 111.19 5.80 -2 -4 9 114.19 6.70 -2 -4 9 113.09 4.90 2 4 9 113.79 6.60 -2 -4 -9 121.89 7.40 2 3 9 65.69 4.70 -2 -3 9 68.29 3.60 -2 -3 9 68.99 3.90 -2 -3 9 69.99 4.70 -2 -3 -9 66.09 5.30 -2 -3 -9 60.19 5.10 -2 -2 9 10.50 2.40 2 2 9 4.90 2.10 -2 -2 9 7.70 1.60 -2 -2 9 11.00 1.50 2 2 9 7.10 2.00 2 2 -9 6.50 1.20 -2 -2 -9 6.60 2.00 -2 -2 -9 6.80 2.10 -2 -1 9 2.40 0.90 2 1 9 2.00 1.50 2 1 9 2.80 1.50 -2 -1 9 2.60 1.40 2 1 -9 2.00 1.30 2 1 -9 -0.10 0.90 -2 -1 -9 1.40 1.70 -2 0 9 465.65 10.00 -2 0 9 459.05 10.20 2 0 9 464.35 10.30 -2 0 -9 469.05 10.10 2 0 -9 479.25 9.90 2 0 -9 469.95 10.30 -2 1 9 0.80 1.30 2 -1 9 2.90 1.10 2 -1 -9 2.10 1.70 2 -2 9 5.70 1.10 -2 2 9 8.60 1.90 2 -2 9 8.20 0.90 -2 2 9 9.90 1.90 2 -2 -9 5.00 2.20 2 -2 -9 4.50 2.30 -2 3 9 67.09 4.20 -2 3 9 64.49 3.90 2 -3 9 66.29 2.70 2 -3 9 68.39 4.40 2 -3 -9 70.59 5.70 2 -3 -9 61.19 4.90 2 -4 9 112.89 5.90 -2 4 9 111.49 4.10 -2 4 9 113.09 6.10 2 -4 9 106.39 3.70 -2 4 9 116.69 4.30 2 -4 9 111.39 6.20 2 -4 -9 106.29 6.40 2 -4 -9 89.29 9.60 2 -4 -9 113.99 6.90 -2 5 9 23.20 4.90 2 -5 9 37.30 4.80 2 -5 9 35.10 4.00 2 -5 9 39.80 4.90 2 -5 -9 29.70 7.20 2 -5 -9 36.40 4.90 2 -5 -9 45.00 5.90 2 -6 9 37.40 6.90 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110.79 7.50 10 3 -2 117.49 7.90 10 2 2 289.17 8.90 -10 -2 2 271.77 8.60 -10 -2 2 281.77 8.70 -10 -2 2 296.17 8.40 10 2 2 243.28 9.20 10 2 -2 287.17 9.10 -10 -2 -2 284.27 9.00 -10 -2 -2 289.77 8.80 10 2 -2 270.87 9.20 -10 -1 2 370.06 9.40 -10 -1 2 361.06 9.40 10 1 2 378.16 9.30 -10 -1 2 370.06 9.50 10 1 2 354.96 9.30 -10 -1 -2 344.47 9.40 10 1 -2 370.56 9.70 10 1 -2 358.86 9.30 -10 -1 -2 355.06 9.30 10 1 -2 357.36 10.10 10 0 2 99.29 4.20 10 0 2 92.29 4.60 -10 0 2 110.59 5.00 -10 0 2 102.99 4.10 10 0 2 92.79 4.00 -10 0 2 104.19 4.30 10 0 -2 89.39 4.50 10 0 -2 98.79 4.40 -10 0 -2 82.29 3.90 -10 0 -2 80.89 4.10 10 0 -2 113.59 4.50 -10 1 2 361.96 8.40 10 -1 2 366.66 9.10 10 -1 2 364.66 8.60 10 -1 2 361.66 7.60 -10 1 2 359.46 7.50 -10 1 2 365.06 9.80 10 -1 -2 358.86 8.90 -10 1 -2 344.37 9.00 -10 1 -2 355.36 7.70 10 -1 -2 353.66 9.20 10 -2 2 286.67 7.00 10 -2 2 284.77 7.90 -10 2 2 277.97 8.90 10 -2 -2 290.07 8.30 -10 2 -2 285.17 8.40 10 -2 -2 298.47 7.80 -10 3 2 109.09 7.60 10 -3 2 123.19 5.90 10 -3 2 117.49 4.50 10 -3 -2 118.59 5.10 10 -3 -2 117.09 6.60 10 -4 2 192.48 6.30 10 -4 2 198.18 8.10 10 -4 -2 196.58 10.00 10 -4 -2 194.98 7.30 10 -5 2 29.10 6.00 10 -5 2 33.30 4.10 10 -5 -2 20.60 5.20 10 -5 -2 27.10 6.20 10 -6 2 79.99 8.60 10 -6 -2 84.09 10.00 10 5 3 108.39 8.20 -10 -5 3 130.19 10.80 10 5 3 107.59 8.80 10 5 -3 101.59 8.10 -10 -5 -3 115.49 10.60 -10 -4 3 152.78 10.10 10 4 3 148.09 8.40 -10 -4 3 146.39 8.80 10 4 3 152.38 7.40 -10 -4 3 145.89 8.20 10 4 -3 165.38 7.10 -10 -4 -3 146.89 9.60 -10 -4 -3 146.19 10.50 10 3 3 1606.64 31.30 -10 -3 3 1568.84 32.50 10 3 3 1550.54 34.70 -10 -3 3 1590.34 31.70 -10 -3 3 1563.64 32.70 -10 -3 -3 1342.27 32.60 10 3 -3 1600.54 35.20 -10 -3 -3 1568.24 32.80 10 3 -3 1607.44 31.40 -10 -2 3 27.90 3.00 10 2 3 25.90 3.20 10 2 3 28.60 3.00 -10 -2 3 33.90 4.20 -10 -2 3 31.00 3.40 -10 -2 -3 27.90 3.20 10 2 -3 29.30 3.90 10 2 -3 25.40 3.60 -10 -2 -3 28.20 3.50 10 1 3 5121.99 93.09 -10 -1 3 5011.80 92.99 -10 -1 3 5085.59 93.09 -10 -1 3 4984.90 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4.90 -10 -5 4 17.40 6.90 10 5 -4 17.10 5.40 -10 -5 -4 29.00 6.40 10 5 -4 23.00 4.70 -10 -4 4 7.00 4.00 10 4 4 6.80 4.30 10 4 4 10.10 3.60 -10 -4 4 12.10 5.00 -10 -4 4 11.60 4.90 10 4 -4 7.00 3.50 -10 -4 -4 0.40 4.10 -10 -3 4 58.79 6.50 -10 -3 4 52.09 5.90 -10 -3 4 54.29 5.20 10 3 4 52.49 4.90 10 3 -4 54.79 5.30 -10 -3 -4 57.69 6.10 -10 -2 4 1009.40 21.10 -10 -2 4 977.10 21.50 -10 -2 4 1000.80 21.30 10 2 4 1010.50 21.10 10 2 4 978.40 21.60 10 2 -4 1014.00 21.90 -10 -2 -4 954.20 21.70 -10 -2 -4 1012.70 21.80 -10 -1 4 152.98 5.80 -10 -1 4 166.58 5.70 10 1 4 160.58 6.10 10 1 4 159.38 5.70 -10 -1 4 151.78 5.50 10 1 -4 153.48 6.30 10 1 -4 154.48 6.00 10 1 -4 150.48 5.80 -10 -1 -4 151.78 5.90 -10 -1 -4 154.18 5.90 10 0 4 77.89 4.10 10 0 4 76.49 3.70 -10 0 4 74.19 4.40 -10 0 4 72.99 3.90 10 0 4 82.49 4.70 -10 0 4 74.39 3.70 -10 0 -4 71.39 3.70 -10 0 -4 71.89 3.80 10 0 -4 72.59 4.30 10 0 -4 64.19 4.40 10 -1 4 156.88 4.30 -10 1 4 149.79 6.00 -10 1 4 151.08 4.80 10 -1 4 164.38 5.40 10 -1 4 151.38 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110.89 5.80 -10 -1 5 287.57 8.30 10 1 5 287.17 8.10 10 1 5 290.97 8.40 -10 -1 5 292.27 8.40 -10 -1 5 294.57 8.00 -10 -1 -5 286.87 8.40 10 1 -5 309.97 8.70 10 1 -5 285.87 8.70 -10 -1 -5 293.27 8.40 10 1 -5 296.57 8.40 -10 0 5 355.56 8.90 10 0 5 353.06 8.60 -10 0 5 352.76 9.30 10 0 5 360.16 9.00 -10 0 5 353.36 8.70 -10 0 -5 353.96 8.80 10 0 -5 352.46 9.20 10 0 -5 357.16 9.20 -10 0 -5 353.96 8.80 10 -1 5 285.67 7.60 -10 1 5 287.27 7.30 10 -1 5 291.17 7.40 10 -1 5 280.77 6.70 -10 1 5 288.47 6.70 -10 1 5 276.27 8.60 10 -1 -5 294.57 8.20 10 -1 -5 292.87 8.10 -10 1 -5 285.77 7.50 10 -2 5 107.79 4.50 -10 2 5 103.59 2.50 -10 2 5 103.29 6.30 -10 2 5 111.09 3.70 -10 2 5 107.79 2.50 10 -2 5 107.89 3.90 10 -2 5 103.89 2.60 10 -2 -5 105.49 5.50 -10 2 -5 101.89 4.80 10 -2 -5 105.89 5.00 -10 3 5 267.77 10.20 10 -3 5 263.77 7.90 10 -3 5 267.87 6.50 10 -3 -5 258.77 9.70 10 -3 -5 276.37 8.30 10 -4 5 63.19 5.30 10 -4 5 54.89 3.60 10 -4 -5 60.29 5.90 10 -4 -5 63.59 6.20 10 -5 5 24.40 5.00 10 -5 5 7.80 3.50 10 -5 -5 -0.80 6.20 10 -5 -5 8.20 5.50 10 -6 -5 33.60 10.20 10 5 6 6.30 5.80 -10 -5 6 -5.60 5.30 -10 -5 6 -8.90 6.30 10 5 6 3.20 5.10 10 5 -6 -3.90 4.10 -10 -5 -6 -8.50 5.80 -10 -4 6 887.81 20.80 -10 -4 6 847.62 22.10 10 4 6 862.91 21.00 -10 -4 6 840.32 21.30 10 4 6 894.71 20.10 -10 -4 -6 881.01 22.30 10 4 -6 909.31 19.80 -10 -3 6 340.47 10.40 -10 -3 6 328.87 10.50 10 3 6 338.17 9.90 10 3 6 331.07 10.90 10 3 -6 325.77 9.90 -10 -2 6 83.39 4.90 10 2 6 86.49 5.30 -10 -2 6 81.69 5.30 -10 -2 6 84.39 5.60 10 2 6 88.49 5.50 -10 -2 -6 85.49 5.90 10 2 -6 84.29 5.90 -10 -2 -6 87.39 5.50 10 2 -6 73.99 6.50 10 1 6 429.06 10.60 -10 -1 6 410.96 10.80 10 1 6 423.56 10.80 -10 -1 6 416.06 10.60 -10 -1 6 419.86 10.50 -10 -1 -6 426.66 10.90 10 1 -6 431.46 10.80 10 1 -6 415.66 11.10 -10 -1 -6 430.36 10.80 -10 0 6 1297.87 25.60 10 0 6 1297.37 25.80 10 0 6 1304.17 25.60 -10 0 6 1310.47 26.40 -10 0 6 1275.27 25.70 10 0 -6 1310.97 26.20 -10 0 -6 1295.77 25.80 10 0 -6 1302.67 26.20 -10 0 -6 1324.47 25.70 10 -1 6 436.86 9.90 -10 1 6 420.26 9.40 -10 1 6 420.66 9.90 -10 1 6 431.26 11.50 10 -1 6 443.66 10.30 10 -1 6 428.86 9.40 10 -1 -6 427.46 10.80 -10 1 -6 424.46 10.00 10 -1 -6 431.96 10.70 10 -2 6 89.09 2.80 10 -2 6 97.59 3.80 -10 2 6 87.29 2.90 -10 2 6 84.49 6.10 -10 2 6 91.89 2.90 10 -2 6 92.09 4.10 -10 2 6 94.19 3.80 10 -2 -6 95.89 5.10 10 -2 -6 96.19 5.40 -10 2 -6 87.99 4.40 10 -3 6 338.87 7.70 10 -3 6 340.07 8.90 10 -3 -6 335.97 10.90 10 -3 -6 340.47 9.80 10 -4 6 840.42 16.80 10 -4 6 876.71 18.90 10 -4 -6 863.01 21.50 10 -4 -6 885.21 19.90 10 -5 6 0.40 4.20 10 -5 -6 3.30 5.90 10 -5 -6 -3.20 6.40 -10 -5 7 129.69 11.20 10 5 7 103.89 10.60 -10 -5 7 134.59 10.00 10 5 -7 133.69 8.90 -10 -5 -7 130.59 11.70 -10 -4 7 317.57 11.80 -10 -4 7 327.27 12.50 10 4 7 311.87 12.20 10 4 7 337.87 11.00 -10 -4 7 331.87 10.90 -10 -4 -7 306.47 12.50 10 4 -7 352.86 10.70 10 3 7 867.81 18.70 10 3 7 844.52 19.70 -10 -3 7 863.11 19.30 -10 -3 7 697.33 21.10 -10 -3 -7 712.63 21.90 10 3 -7 853.81 18.50 -10 -2 7 170.98 6.50 -10 -2 7 143.79 6.10 10 2 7 157.88 7.20 -10 -2 7 166.48 7.20 10 2 7 160.98 6.30 -10 -2 -7 141.59 6.70 10 2 -7 144.79 6.40 -10 -2 -7 153.58 7.30 -10 -1 7 305.17 8.50 -10 -1 7 323.97 9.10 10 1 7 319.17 8.90 10 1 7 325.57 9.00 10 1 -7 322.27 9.00 -10 -1 -7 312.07 9.20 -10 -1 -7 311.77 8.90 10 1 -7 323.07 9.30 10 0 7 66.59 3.80 -10 0 7 68.09 4.20 -10 0 7 69.59 4.50 -10 0 7 72.09 4.20 10 0 7 65.49 3.90 -10 0 -7 62.09 4.00 -10 0 -7 67.39 4.00 10 0 -7 65.79 4.30 10 0 -7 66.79 4.50 -10 1 7 272.97 10.50 10 -1 7 313.77 8.20 -10 1 7 312.57 7.50 10 -1 7 310.67 7.40 -10 1 7 305.77 8.00 10 -1 -7 316.77 8.90 10 -1 -7 331.07 9.00 -10 1 -7 320.27 7.90 -10 2 7 157.08 4.40 10 -2 7 155.08 4.30 -10 2 7 137.39 7.30 -10 2 7 157.68 4.30 10 -2 7 168.28 5.30 -10 2 7 158.48 4.90 10 -2 -7 152.88 6.40 10 -2 -7 148.39 6.60 -10 2 -7 147.79 5.60 10 -3 7 814.32 15.60 10 -3 7 858.81 17.60 10 -3 7 855.71 16.60 10 -3 -7 846.92 20.20 10 -3 -7 844.22 18.90 10 -4 7 332.67 9.40 10 -4 7 317.77 7.30 10 -4 -7 320.07 12.00 10 -4 -7 333.47 11.30 10 -5 7 143.69 8.60 10 -5 -7 145.99 10.60 10 -5 -7 129.19 12.20 -10 -5 8 21.90 6.40 10 5 8 35.60 6.80 -10 -5 8 19.30 6.10 -10 -5 -8 10.30 7.50 10 4 8 924.31 27.80 10 4 8 972.10 23.10 10 4 8 964.90 21.60 -10 -4 8 918.71 22.60 -10 -4 8 939.81 21.90 -10 -4 8 954.60 23.50 -10 -4 -8 947.31 24.20 10 4 -8 942.11 20.90 -10 -3 8 378.56 11.10 -10 -3 8 364.66 12.30 10 3 8 369.86 11.20 10 3 8 352.16 13.80 -10 -3 -8 380.86 12.30 10 3 -8 376.56 10.90 -10 -2 8 1017.00 21.80 10 2 8 1022.90 21.90 10 2 8 1015.70 22.60 -10 -2 8 1021.70 22.60 -10 -2 8 1033.40 21.90 -10 -2 -8 1042.40 22.90 10 2 -8 1032.70 21.90 -10 -2 -8 1024.80 23.10 -10 -1 8 13.00 2.70 -10 -1 8 11.00 3.00 -10 -1 8 12.60 2.30 10 1 8 7.40 2.60 -10 -1 -8 8.70 2.60 10 1 -8 14.20 2.90 -10 -1 -8 17.90 2.70 10 1 -8 15.10 2.80 10 0 8 3451.75 63.49 -10 0 8 3386.86 63.49 -10 0 8 3412.16 63.69 -10 0 -8 3350.76 63.69 10 0 -8 3541.85 64.29 10 0 -8 3367.86 63.99 -10 0 -8 3392.56 63.19 10 -1 8 13.10 2.30 -10 1 8 15.80 3.10 10 -1 8 15.20 2.10 -10 1 8 12.60 2.30 -10 1 8 13.40 1.90 -10 1 -8 15.10 2.20 10 -1 -8 15.40 2.60 10 -1 -8 14.70 2.70 -10 2 8 1004.90 23.00 -10 2 8 1017.20 20.30 10 -2 8 1007.40 19.70 10 -2 8 1019.00 20.30 -10 2 8 1034.90 19.90 10 -2 -8 1019.40 21.70 10 -2 -8 1035.50 22.30 -10 2 -8 1012.20 20.70 -10 3 8 376.36 7.90 10 -3 8 370.66 7.80 10 -3 8 362.26 7.80 -10 3 8 359.86 7.70 10 -3 8 374.96 9.10 10 -3 -8 351.76 13.30 10 -3 -8 357.16 11.00 10 -4 8 925.51 19.70 10 -4 8 929.31 17.90 10 -4 -8 971.30 23.60 10 -4 -8 954.40 22.00 10 -5 8 15.50 4.50 10 -5 -8 27.10 6.60 10 -5 -8 20.60 6.70 -10 -5 9 75.79 7.20 -10 -5 9 63.79 7.80 10 5 9 78.49 8.20 -10 -5 -9 72.59 9.20 10 4 9 12.80 5.90 -10 -4 9 24.70 5.00 10 4 9 24.10 5.60 -10 -4 9 22.70 4.60 -10 -4 9 21.40 4.90 -10 -4 -9 23.40 5.20 10 4 -9 27.30 4.30 -10 -3 9 144.69 7.10 10 3 9 145.49 7.00 10 3 9 136.89 7.90 -10 -3 9 138.79 8.40 -10 -3 9 138.99 6.80 -10 -3 -9 135.09 8.00 10 3 -9 133.39 6.80 -10 -2 9 91.39 5.70 -10 -2 9 91.59 5.90 -10 -2 9 97.99 5.90 10 2 9 89.59 5.50 10 2 9 104.19 6.20 -10 -2 -9 92.19 6.60 10 2 -9 101.09 5.80 -10 -1 9 6.10 2.20 -10 -1 9 8.50 2.80 10 1 9 4.70 2.70 10 1 9 7.10 2.40 -10 -1 9 5.40 2.10 10 1 -9 2.00 2.40 10 1 -9 7.80 2.90 -10 -1 -9 3.90 2.30 -10 -1 -9 5.50 2.20 -10 0 9 181.08 6.30 10 0 9 186.38 6.00 -10 0 9 181.38 6.50 -10 0 9 166.68 6.90 -10 0 -9 180.78 5.90 10 0 -9 183.08 6.60 10 0 -9 178.78 6.90 -10 1 9 4.40 1.80 -10 1 9 8.10 2.90 10 -1 9 5.40 1.90 -10 1 9 7.70 2.20 10 -1 -9 6.50 2.40 10 -1 -9 3.60 2.30 -10 1 -9 9.80 2.00 10 -2 9 94.19 3.90 -10 2 9 83.79 7.40 10 -2 9 92.59 4.20 -10 2 9 91.29 4.40 -10 2 -9 86.19 4.30 10 -2 -9 87.69 5.90 -10 3 9 143.89 4.50 -10 3 9 143.59 4.50 10 -3 9 145.39 4.60 10 -3 9 138.19 4.60 10 -3 9 147.79 5.20 10 -3 -9 147.49 8.00 10 -3 -9 148.39 7.00 -10 4 9 23.30 2.20 10 -4 9 21.00 2.00 10 -4 9 21.10 2.20 10 -4 9 27.50 3.00 10 -4 9 23.10 3.10 10 -4 -9 26.20 4.80 10 -4 -9 26.20 5.40 10 -5 9 72.09 6.60 10 -5 -9 77.59 9.00 10 -5 -9 73.79 7.40 -10 -5 10 2.90 5.70 -10 -5 10 6.10 6.20 10 5 10 15.20 5.70 10 5 10 3.90 6.10 -10 -5 -10 17.30 7.90 -10 -4 10 467.15 13.20 -10 -4 10 436.66 14.10 -10 -4 10 432.26 15.40 10 4 10 422.76 15.00 10 4 10 462.65 15.10 -10 -4 -10 445.96 15.90 10 4 -10 440.86 13.60 10 3 10 1.70 4.20 -10 -3 10 1.80 3.20 10 3 10 2.90 3.50 -10 -3 10 4.00 3.30 -10 -3 10 3.50 3.10 -10 -3 -10 2.50 3.50 10 3 -10 1.20 3.00 -10 -2 10 671.13 16.40 -10 -2 10 663.83 15.80 -10 -2 10 680.33 15.70 10 2 10 689.03 16.00 10 2 10 653.53 16.30 -10 -2 -10 666.13 16.70 10 2 -10 670.23 16.00 -10 -1 10 121.29 5.80 -10 -1 10 123.59 6.00 10 1 10 108.29 6.60 -10 -1 10 120.89 5.70 10 1 -10 119.49 6.10 -10 -1 -10 117.29 5.70 10 1 -10 124.49 6.00 -10 -1 -10 115.59 6.10 10 0 10 3998.00 71.39 -10 0 10 3934.61 72.09 -10 0 10 3940.11 71.49 -10 0 10 3842.02 71.29 10 0 -10 3500.75 73.29 -10 0 -10 3804.72 70.69 10 0 -10 3799.42 71.59 10 -1 10 113.69 4.80 -10 1 10 121.39 6.50 -10 1 10 110.89 4.90 -10 1 10 115.79 5.20 10 -1 -10 105.69 7.20 10 -1 -10 111.69 5.60 -10 1 -10 111.89 4.30 10 -2 10 659.93 14.20 -10 2 10 667.33 17.30 -10 2 10 670.63 14.60 10 -2 10 674.63 14.20 10 -2 -10 672.23 16.20 -10 2 -10 675.93 14.30 10 -2 -10 688.53 16.70 10 -3 10 -0.80 2.00 -10 3 10 1.70 1.90 10 -3 10 0.30 1.90 10 -3 10 1.70 2.00 -10 3 10 -0.20 1.80 10 -3 -10 2.40 3.50 10 -3 -10 -5.10 3.50 10 -4 10 447.86 10.50 10 -4 10 433.76 9.70 10 -4 10 425.46 9.30 -10 4 10 439.46 9.70 10 -4 -10 453.25 14.90 10 -4 -10 451.45 14.50 10 -5 10 9.10 3.80 10 -5 -10 -3.50 7.20 10 -5 -10 -7.20 6.30 10 5 11 2.00 6.60 -10 -5 11 8.40 5.20 10 5 11 1.70 5.70 -10 -5 11 6.60 6.40 -10 -5 -11 8.60 7.90 -10 -4 11 25.60 4.80 10 4 11 22.60 5.60 -10 -4 11 28.90 5.80 -10 -4 11 29.70 5.70 -10 -4 -11 29.90 5.90 10 3 11 84.19 7.40 -10 -3 11 62.39 6.60 -10 -3 11 66.49 5.90 -10 -3 11 83.29 5.90 10 3 11 84.09 6.90 -10 -3 -11 74.29 7.20 10 3 -11 86.79 6.50 10 2 11 -0.70 3.10 -10 -2 11 3.90 2.90 -10 -2 11 -2.40 2.80 -10 -2 11 -1.60 2.50 10 2 11 -3.70 2.80 10 2 11 -2.20 2.60 -10 -2 -11 1.20 3.00 10 2 -11 -3.40 3.00 10 2 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2157.38 45.80 10 4 12 2191.78 45.60 10 4 12 2168.88 43.80 -10 -4 12 2176.48 43.90 -10 -4 12 2125.49 43.90 -10 -4 -12 2223.88 46.90 10 3 12 90.69 8.60 -10 -3 12 89.09 6.20 -10 -3 12 96.09 7.50 -10 -3 12 84.99 6.20 10 3 12 80.79 7.10 10 3 -12 83.19 6.50 -10 -3 -12 97.19 7.80 10 2 12 29.90 4.10 -10 -2 12 26.00 3.70 -10 -2 12 38.90 4.30 -10 -2 12 29.40 3.50 10 2 12 29.40 3.70 10 2 -12 22.70 3.80 10 2 -12 26.40 4.00 -10 -2 -12 26.30 4.10 10 1 12 42.90 4.00 -10 -1 12 39.70 4.40 -10 -1 12 49.40 5.20 -10 -1 12 47.20 4.50 10 1 -12 42.30 4.90 -10 -1 -12 48.40 5.10 -10 -1 -12 43.80 5.40 10 1 -12 44.60 4.90 10 0 12 1974.10 38.60 -10 0 12 1995.10 38.70 -10 0 12 1983.20 39.30 -10 0 12 1977.00 38.80 10 0 -12 1982.30 38.80 -10 0 -12 1916.51 37.60 10 0 -12 1990.10 39.30 10 -1 12 42.40 3.90 -10 1 12 43.40 4.50 -10 1 12 44.50 4.10 10 -1 -12 40.80 3.90 10 -1 -12 46.30 4.70 -10 1 -12 47.30 3.20 -10 2 12 31.50 3.20 10 -2 12 24.60 2.80 -10 2 12 28.50 4.70 10 -2 -12 26.10 3.70 -10 2 -12 28.50 3.30 10 -2 -12 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338.57 12.30 20 1 0 325.77 14.00 20 0 0 440.36 16.70 -20 0 0 451.25 13.10 -20 1 0 349.57 9.90 20 -1 0 359.96 14.20 20 -1 0 351.36 14.50 20 -2 0 141.49 11.40 20 -2 0 141.19 11.60 20 -3 0 175.68 13.20 20 -3 0 153.78 14.00 20 -4 0 518.45 20.10 -20 -3 1 86.39 9.10 -20 -3 -1 108.59 10.30 -20 -2 1 100.89 10.90 -20 -2 -1 105.59 10.90 -20 -1 1 37.40 5.80 20 1 1 28.50 6.70 -20 -1 -1 34.30 5.30 20 1 -1 27.90 6.90 -20 0 1 227.48 9.20 20 0 1 183.08 10.70 20 0 1 208.98 12.70 -20 0 -1 227.58 9.30 20 0 -1 230.18 14.10 -20 1 1 39.00 3.80 20 -1 1 35.10 6.30 20 -1 1 49.70 6.70 20 -1 -1 37.60 7.30 20 -1 -1 39.60 6.60 -20 1 -1 35.70 3.90 20 -2 1 141.29 11.30 20 -2 1 109.39 11.60 20 -2 -1 106.29 11.50 20 -2 -1 110.79 10.30 20 -3 1 95.49 9.00 20 -3 1 125.99 12.60 20 -3 -1 91.09 9.30 20 -4 1 349.77 17.60 20 -4 -1 411.86 21.40 -20 -3 2 92.39 10.00 -20 -3 -2 95.19 9.40 -20 -2 2 125.29 11.20 -20 -2 -2 120.59 11.20 -20 -1 2 92.09 9.10 20 1 2 94.99 8.10 -20 -1 -2 100.99 9.00 20 0 2 263.87 11.80 -20 0 2 288.67 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6.20 -20 1 4 8.00 3.30 20 -1 -4 7.90 5.80 -20 1 -4 0.80 5.60 20 -2 4 1291.47 30.40 20 -2 4 1299.57 30.20 20 -2 -4 1350.46 31.40 -20 2 -4 1339.37 35.10 20 -3 4 64.29 8.10 20 -3 4 56.19 8.90 20 -3 -4 52.19 7.80 -20 -3 5 67.29 8.60 -20 -3 -5 68.19 10.00 -20 -2 5 239.78 13.50 -20 -2 -5 245.38 14.00 20 1 5 162.78 11.30 -20 -1 5 158.48 9.70 -20 -1 -5 165.08 10.00 20 0 5 534.65 15.70 -20 0 5 550.84 14.70 20 0 -5 536.95 18.40 -20 0 -5 556.34 15.50 20 -1 5 147.49 10.90 20 -1 5 155.08 11.10 -20 1 5 148.39 6.60 20 -1 5 154.28 7.90 20 -1 -5 129.69 11.00 -20 1 -5 147.29 11.20 20 -2 5 226.18 12.60 20 -2 5 239.68 13.20 20 -2 -5 264.07 14.30 -20 2 -5 238.98 15.00 20 -3 5 69.59 8.10 20 -3 5 74.39 8.10 20 -3 -5 84.49 9.20 -20 -3 6 33.60 10.20 -20 -3 -6 13.60 9.20 -20 -2 6 476.55 18.00 -20 -2 6 478.45 17.20 -20 -2 -6 477.15 17.60 -20 -1 6 115.69 9.30 -20 -1 6 129.39 10.90 20 1 6 103.09 11.80 -20 -1 -6 117.39 9.70 20 1 -6 104.09 12.20 20 0 6 493.65 14.90 -20 0 6 498.15 14.00 20 0 -6 511.45 17.70 -20 0 -6 504.95 14.90 -20 1 6 119.49 6.50 20 -1 6 116.99 7.70 20 -1 6 107.49 9.80 -20 1 -6 119.39 10.80 20 -1 -6 109.49 10.50 20 -2 6 472.75 16.40 20 -2 6 506.25 16.80 20 -2 -6 491.85 16.90 -20 2 -6 488.85 18.30 20 -3 6 32.20 7.40 20 -3 -6 16.60 8.30 -20 -2 7 60.49 7.60 -20 -2 7 66.39 7.90 -20 -2 -7 69.79 8.50 -20 -1 7 359.36 13.60 -20 -1 7 366.16 14.60 20 1 7 376.16 15.00 -20 -1 -7 347.67 14.40 20 1 -7 362.06 16.50 20 0 7 20.10 5.50 -20 0 7 26.80 4.80 -20 0 7 28.90 5.80 20 0 -7 23.50 6.60 -20 0 -7 19.10 5.20 -20 0 -7 18.90 7.50 20 -1 7 362.76 11.50 20 -1 7 347.57 13.10 -20 1 7 358.36 10.30 -20 1 -7 359.16 15.00 20 -1 -7 351.96 14.50 20 -2 7 68.39 7.80 20 -2 7 62.89 7.40 20 -2 -7 53.89 7.40 -20 2 -7 70.29 8.40 20 -3 7 172.28 13.50 -20 -2 8 25.10 7.10 -20 -2 8 13.10 7.10 -20 -2 -8 26.30 6.70 -20 -1 8 219.98 11.20 20 1 8 227.58 12.90 -20 -1 8 225.28 11.50 20 1 -8 197.18 15.70 -20 -1 -8 223.48 12.20 -20 0 8 175.48 9.80 20 0 8 175.98 10.40 -20 0 8 170.18 8.90 -20 0 -8 172.38 12.60 20 0 -8 152.88 13.40 20 -1 8 207.38 9.10 -20 1 8 201.18 8.50 20 -1 8 207.38 14.10 20 -1 -8 207.88 12.40 -20 1 -8 206.08 12.90 20 -2 8 23.60 7.40 20 -2 8 7.10 6.70 20 -2 -8 19.90 7.60 -20 2 -8 19.40 7.50 20 -3 8 -2.30 7.60 -20 -2 9 112.89 10.90 -20 -2 -9 111.59 10.00 20 1 9 1330.87 31.40 -20 -1 9 1394.76 31.60 -20 -1 9 1386.86 30.80 20 1 -9 1326.17 33.90 -20 -1 -9 1379.96 31.60 -20 0 9 279.87 12.60 20 0 9 340.97 12.70 -20 0 9 337.37 13.40 -20 0 -9 327.87 19.50 20 0 -9 319.07 14.90 -20 1 9 1360.06 29.80 -20 1 9 1357.36 27.80 20 -1 -9 1367.86 32.10 -20 1 -9 1347.47 31.30 20 -2 9 115.29 11.60 -20 2 -9 120.79 12.20 20 -2 -9 105.89 9.20 -20 -2 10 542.45 18.80 -20 -2 -10 540.35 19.90 -20 -1 10 82.39 9.70 -20 -1 10 76.99 7.50 20 1 10 63.49 8.40 -20 -1 -10 71.89 8.30 20 1 -10 55.09 9.50 20 0 10 301.37 12.90 -20 0 10 318.97 11.70 -20 0 10 323.67 13.30 20 0 -10 308.07 16.10 -20 0 -10 297.17 12.90 -20 1 10 88.59 8.90 -20 1 10 72.89 7.10 -20 1 -10 83.29 8.40 20 -1 -10 70.39 8.80 20 -2 10 547.65 17.60 20 -2 -10 558.04 18.70 -20 -2 11 30.60 7.80 -20 -2 -11 28.40 8.50 -20 -1 11 588.24 17.70 -20 -1 11 591.54 18.00 20 1 11 547.55 19.10 20 1 -11 578.24 20.40 -20 -1 -11 611.74 18.80 20 0 11 237.18 12.30 -20 0 11 254.87 10.90 -20 0 11 244.88 12.70 -20 0 -11 254.77 15.30 20 0 -11 228.58 13.60 -20 1 11 602.34 16.80 -20 1 11 585.84 14.90 20 -1 -11 571.94 18.90 -20 1 -11 552.44 18.60 20 -2 11 15.80 7.20 -20 -2 12 109.19 13.20 -20 -2 -12 127.19 14.90 -20 -1 12 6.00 7.00 -20 -1 12 16.30 6.00 -20 -1 -12 18.10 6.80 20 1 -12 24.50 8.20 -20 0 12 188.88 10.40 20 0 12 190.98 12.10 -20 0 12 158.58 11.80 -20 0 -12 159.38 11.70 20 0 -12 178.48 13.20 -20 1 12 4.00 5.50 -20 1 12 3.00 5.00 20 -1 -12 19.90 7.20 -20 1 -12 11.90 6.80 -20 -2 13 208.58 15.00 -20 -2 -13 230.28 16.50 -20 -1 13 152.58 11.50 -20 -1 13 175.28 12.50 20 1 -13 110.89 10.80 20 0 13 1466.95 32.60 -20 0 13 1454.45 31.60 -20 0 13 1457.35 32.90 20 0 -13 1434.36 34.80 -20 1 13 148.29 10.70 -20 1 -13 142.89 13.10 20 -1 -13 168.08 14.90 -20 -2 14 563.64 20.50 -20 -2 -14 581.34 22.20 -20 -1 14 79.29 8.10 20 0 14 190.68 13.40 -20 0 14 176.38 11.10 -20 0 14 168.48 11.40 20 0 -14 148.49 15.60 -20 1 14 89.99 7.90 -20 -2 15 140.09 14.40 -20 -2 -15 117.19 11.90 -20 -1 15 1577.64 35.70 -20 0 15 99.79 10.70 -20 0 15 108.89 9.30 20 0 15 105.09 12.30 -20 1 15 1561.54 34.40 -20 -1 16 230.08 14.10 -20 0 16 89.89 10.00 -20 0 16 88.89 9.00 20 0 16 81.89 10.10 -20 1 16 272.37 14.10 -20 -1 17 474.85 18.20 -20 0 17 130.29 11.20 -20 1 17 458.65 16.80 -20 -1 18 76.69 9.60 -20 0 18 1154.48 27.90 -20 1 18 66.09 8.50 -20 -1 19 85.39 10.40 -20 0 19 504.95 18.70 -20 -1 20 57.09 11.80 -20 0 20 828.62 23.50 -20 0 21 138.79 17.20 -21 -2 0 925.61 24.90 21 1 0 31.50 7.50 -21 -1 0 32.70 6.20 21 0 0 9.50 7.20 -21 0 0 1.20 4.70 21 -1 0 24.10 7.90 21 -2 0 921.41 24.60 21 -3 0 660.83 20.70 -21 -2 1 234.68 13.60 -21 -2 -1 202.38 13.30 -21 -1 1 94.39 9.90 21 1 1 87.79 9.10 -21 -1 -1 97.39 9.40 21 1 -1 94.59 11.40 -21 0 1 0.20 4.20 21 0 -1 4.70 7.80 -21 0 -1 -2.20 4.00 21 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0 -8 3.20 7.40 21 -1 -8 11.00 7.90 -21 -2 9 73.29 8.90 -21 -2 -9 96.39 10.00 -21 -1 9 82.39 7.90 21 1 9 77.39 9.00 -21 -1 9 94.99 10.80 -21 -1 -9 83.49 8.80 -21 0 9 2.10 5.10 -21 0 9 0.60 6.20 21 0 9 -6.70 6.10 21 0 -9 1.80 7.30 21 -1 -9 80.19 8.90 -21 -2 10 78.69 9.40 -21 -2 -10 80.19 10.30 -21 -1 10 77.89 8.10 -21 -1 10 105.29 10.40 -21 -1 -10 100.39 11.50 -21 0 10 2.40 6.40 21 0 10 -1.20 6.30 -21 0 10 3.80 4.90 21 0 -10 1.40 7.70 -21 1 10 102.49 10.00 -21 -2 11 129.19 14.20 -21 -2 -11 131.19 15.80 -21 -1 11 9.40 8.40 -21 -1 11 22.90 6.50 -21 -1 -11 20.60 7.10 21 0 11 -0.60 7.20 -21 0 11 1.50 5.20 -21 0 11 -14.00 6.30 -21 1 11 21.10 6.30 -21 -2 12 54.39 9.00 -21 -2 -12 41.00 9.90 -21 -1 12 6.30 7.00 -21 0 12 11.30 5.70 -21 0 12 2.40 6.90 -21 1 12 6.70 6.20 -21 -2 13 2.50 9.90 -21 -2 -13 22.00 11.30 -21 -1 13 110.29 12.10 -21 0 13 17.90 7.40 -21 0 13 -2.80 5.80 -21 1 13 103.89 8.40 -21 -1 14 32.30 7.70 -21 0 14 9.50 6.40 -21 0 14 -4.60 7.20 -21 1 14 29.50 7.40 -21 -1 15 34.00 8.10 -21 0 15 0.90 6.60 -21 1 15 14.40 7.30 -21 -1 16 298.07 15.90 -21 0 16 2.70 7.20 -21 1 16 278.77 15.10 -21 -1 17 512.25 21.00 -21 1 17 504.35 18.30 -21 -1 18 32.60 9.20 -22 -2 0 -0.90 7.40 22 1 0 51.69 9.80 -22 -1 0 52.99 7.60 -22 0 0 20.40 5.50 22 -1 0 39.10 8.40 22 -2 0 -0.90 8.50 -22 -2 1 8.50 7.40 -22 -2 -1 -3.00 7.30 -22 -1 1 520.15 16.30 22 1 1 444.76 18.30 -22 -1 -1 515.85 16.70 -22 0 1 171.48 9.60 22 0 -1 161.38 14.70 -22 0 -1 168.58 9.80 22 -1 1 519.35 19.30 22 -1 -1 532.75 20.60 22 -2 1 8.30 8.70 22 -2 -1 13.50 8.80 22 -3 1 76.99 12.60 -22 -2 2 15.20 7.70 -22 -2 -2 14.90 7.90 -22 -1 2 68.79 7.70 22 1 2 53.59 9.80 -22 -1 -2 71.19 7.40 -22 0 2 501.05 15.40 -22 0 -2 499.45 15.70 22 0 -2 500.75 19.90 22 -1 2 58.59 8.80 22 -1 -2 49.60 8.60 22 -2 2 26.80 9.40 22 -2 -2 14.90 7.80 22 -3 2 27.30 10.10 -22 -2 3 103.39 9.70 -22 -2 -3 98.29 9.90 -22 -1 3 162.48 11.00 22 1 3 136.09 13.70 -22 -1 -3 151.88 12.50 -22 0 3 243.08 12.20 -22 0 -3 232.38 13.60 22 0 -3 252.17 17.60 22 -1 3 171.48 13.80 22 -1 -3 158.28 13.90 22 -2 3 110.29 11.00 22 -2 -3 138.59 15.50 22 -3 3 365.46 18.90 -22 -2 4 633.64 20.90 -22 -2 -4 608.44 21.40 22 1 4 14.00 9.00 -22 -1 4 20.10 6.70 -22 -1 -4 17.70 6.40 22 0 -4 69.69 10.50 22 -1 -4 13.10 9.10 22 -2 4 628.04 21.50 22 -3 4 139.29 15.90 -22 -2 5 26.80 8.20 -22 -2 -5 29.00 8.50 22 1 5 11.80 8.00 -22 -1 5 11.60 6.60 -22 -1 -5 19.10 7.00 22 0 -5 31.00 9.70 22 -1 -5 32.90 9.80 22 -2 5 8.30 8.90 22 -3 5 116.49 11.60 -22 -2 6 -2.50 7.60 -22 -2 -6 8.80 8.30 22 1 6 16.60 9.70 -22 -1 6 21.00 6.30 -22 -1 -6 29.30 6.80 -22 0 6 36.90 5.60 -22 0 -6 35.80 6.70 22 -2 6 14.00 9.10 -22 -2 7 -4.00 7.90 -22 -2 -7 -8.80 8.50 -22 -1 7 57.09 7.40 -22 -1 -7 49.50 8.20 -22 0 7 91.99 9.10 -22 -2 8 90.89 10.10 -22 -2 -8 109.79 11.10 -22 -1 8 30.10 6.80 -22 -1 -8 40.40 8.40 -22 0 8 914.91 22.10 -22 -2 9 80.59 9.90 -22 -2 -9 72.29 10.70 -22 -1 9 72.39 7.90 -22 -1 -9 83.99 9.00 -22 0 9 82.69 9.90 -22 0 9 123.89 12.70 -22 -2 10 171.28 17.70 -22 -2 -10 192.78 20.10 -22 -1 10 9.50 7.50 -22 -1 -10 11.90 7.70 -22 0 10 428.06 22.00 -22 0 10 482.45 17.60 -22 -1 11 8.10 6.90 -22 -1 -11 2.00 8.60 -22 0 11 56.09 8.60 -22 1 11 13.20 7.40 -22 -1 12 1.60 8.00 -22 0 12 50.89 8.60 -22 1 12 10.20 7.00 -22 -1 13 14.60 7.90 -22 1 13 7.50 9.50 -22 -1 14 95.19 12.30 -22 1 14 100.09 9.40 -22 -1 15 380.36 17.90 -22 1 15 341.77 16.40 -22 -1 16 30.50 9.40 -23 -2 0 11.30 8.70 -23 -1 0 15.00 6.50 -23 -2 1 58.99 9.50 -23 -2 -1 51.99 9.80 -23 -1 1 47.30 7.90 -23 -1 -1 56.59 8.00 23 -1 1 45.10 10.90 -23 -2 2 40.50 9.10 -23 -2 -2 53.79 9.70 -23 -1 2 15.00 7.10 -23 -1 -2 8.80 7.10 23 -1 2 3.50 9.90 23 -2 2 42.60 12.60 -23 -2 3 127.19 14.90 -23 -2 -3 106.29 11.10 -23 -1 3 43.40 7.00 -23 -1 -3 46.80 8.00 23 -2 3 105.49 11.80 -23 -2 4 25.60 9.00 -23 -2 -4 38.60 9.50 -23 -1 4 10.30 7.30 -23 -1 -4 9.70 7.60 23 -2 4 45.30 10.80 -23 -2 5 9.10 9.10 -23 -2 -5 -1.40 9.40 -23 -1 5 37.40 7.90 -23 -1 -5 62.09 8.20 23 -2 5 -1.10 10.70 -23 -1 6 17.20 7.70 -23 -1 -6 26.20 8.60 -23 -1 7 15.90 7.90 -23 -1 -7 26.00 8.90 -23 -1 8 46.00 8.60 -23 -1 -8 43.10 9.60 -23 -1 9 58.29 8.30 -23 -1 -9 55.99 9.20 -23 -1 10 22.60 7.90 -23 -1 -10 11.60 8.60 -23 -1 11 5.60 8.60 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 42395 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' '-x+1/2, y+1/2, z+1/2' 'x+1/2, -y+1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl 0.79446(3) -0.21496(11) 0.77343(2) 0.02034(12) Uani 1 1 d . . . . . Cl2 Cl 0.54849(3) -0.22401(10) 0.22623(2) 0.01998(12) Uani 1 1 d . . . . . O41 O 0.63188(7) 0.6720(3) 0.61048(6) 0.0149(3) Uani 1 1 d . . . . . O45 O 0.44115(9) 0.7009(4) 0.55969(7) 0.0227(4) Uani 1 1 d . . . . . H45 H 0.403799 0.606833 0.567271 0.034 Uiso 1 1 calc R U . . . N1 N 0.81467(9) 0.1324(4) 0.58758(7) 0.0151(3) Uani 1 1 d . . . . . O41' O 0.38467(7) 0.6668(3) 0.38760(5) 0.0149(3) Uani 1 1 d . . . . . O45' O 0.19613(8) 0.6906(4) 0.44056(7) 0.0206(3) Uani 1 1 d . . . . . H45' H 0.158771 0.594822 0.433832 0.031 Uiso 1 1 calc R U . . . C8 C 0.76316(10) -0.0120(4) 0.72210(7) 0.0147(3) Uani 1 1 d . . . . . C7 C 0.70214(10) 0.1712(4) 0.73116(8) 0.0158(3) Uani 1 1 d . . . . . H7 H 0.678781 0.178844 0.763634 0.019 Uiso 1 1 calc R U . . . C6 C 0.67764(11) 0.3373(4) 0.69179(8) 0.0155(4) Uani 1 1 d . . . . . H6 H 0.636733 0.456093 0.697386 0.019 Uiso 1 1 calc R U . . . C5 C 0.71396(10) 0.3306(4) 0.64240(7) 0.0123(3) Uani 1 1 d . . . . . C4 C 0.69128(10) 0.5041(4) 0.60037(7) 0.0131(3) Uani 1 1 d . . . . . C42 C 0.60432(10) 0.8441(4) 0.56871(7) 0.0143(4) Uani 1 1 d . . . . . H42A H 0.587485 0.732317 0.539670 0.017 Uiso 1 1 calc R U . . . H42B H 0.644790 0.965176 0.556758 0.017 Uiso 1 1 calc R U . . . C43 C 0.53777(10) 1.0101(4) 0.59007(8) 0.0154(4) Uani 1 1 d . . . . . H43A H 0.522163 1.143413 0.564154 0.018 Uiso 1 1 calc R U . . . H43B H 0.555020 1.110196 0.620496 0.018 Uiso 1 1 calc R U . . . C44 C 0.46866(11) 0.8365(5) 0.60493(8) 0.0153(4) Uani 1 1 d . . . . . H44A H 0.483184 0.702545 0.631021 0.018 Uiso 1 1 calc R U . . . H44B H 0.428723 0.952259 0.619351 0.018 Uiso 1 1 calc R U . . . C10 C 0.77565(10) 0.1464(4) 0.63404(8) 0.0127(3) Uani 1 1 d . . . . . C2 C 0.79192(11) 0.3004(5) 0.55062(10) 0.0162(4) Uani 1 1 d . . . . . H2 H 0.818617 0.294241 0.519340 0.019 Uiso 1 1 calc R U . . . C3 C 0.73079(10) 0.4890(4) 0.55406(8) 0.0150(4) Uani 1 1 d . . . . . H3 H 0.717583 0.599518 0.525984 0.018 Uiso 1 1 calc R U . . . C9 C 0.79897(10) -0.0288(4) 0.67476(8) 0.0142(4) Uani 1 1 d . . . . . H9 H 0.838310 -0.154656 0.669523 0.017 Uiso 1 1 calc R U . . . C8' C 0.51735(10) -0.0182(4) 0.27710(8) 0.0143(3) Uani 1 1 d . . . . . C7' C 0.45548(10) 0.1615(4) 0.26790(8) 0.0160(4) Uani 1 1 d . . . . . H7' H 0.431763 0.165920 0.235517 0.019 Uiso 1 1 calc R U . . . C6' C 0.43072(10) 0.3292(4) 0.30705(8) 0.0146(4) Uani 1 1 d . . . . . H6' H 0.389176 0.445175 0.301475 0.018 Uiso 1 1 calc R U . . . C5' C 0.46791(10) 0.3277(4) 0.35615(7) 0.0123(3) Uani 1 1 d . . . . . C4' C 0.44529(10) 0.5033(4) 0.39777(7) 0.0129(3) Uani 1 1 d . . . . . C42' C 0.35736(10) 0.8416(4) 0.42920(8) 0.0143(4) Uani 1 1 d . . . . . H42C H 0.397701 0.964883 0.440529 0.017 Uiso 1 1 calc R U . . . H42D H 0.341152 0.731740 0.458666 0.017 Uiso 1 1 calc R U . . . C43' C 0.29028(10) 1.0031(4) 0.40763(8) 0.0143(3) Uani 1 1 d . . . . . H43C H 0.306675 1.098426 0.376441 0.017 Uiso 1 1 calc R U . . . H43D H 0.275055 1.140320 0.432916 0.017 Uiso 1 1 calc R U . . . C44' C 0.22132(12) 0.8254(5) 0.39461(8) 0.0160(4) Uani 1 1 d . . . . . H44C H 0.180349 0.938409 0.380753 0.019 Uiso 1 1 calc R U . . . H44D H 0.235240 0.690799 0.368486 0.019 Uiso 1 1 calc R U . . . C10' C 0.53043(10) 0.1470(4) 0.36461(7) 0.0126(3) Uani 1 1 d . . . . . C9' C 0.55392(10) -0.0309(4) 0.32415(8) 0.0144(4) Uani 1 1 d . . . . . H9' H 0.593693 -0.154914 0.329454 0.017 Uiso 1 1 calc R U . . . N1' N 0.57012(9) 0.1393(3) 0.41092(7) 0.0149(3) Uani 1 1 d . . . . . C2' C 0.54722(11) 0.3096(5) 0.44757(9) 0.0161(4) Uani 1 1 d . . . . . H2' H 0.574549 0.308020 0.478624 0.019 Uiso 1 1 calc R U . . . C3' C 0.48516(10) 0.4938(4) 0.44406(7) 0.0145(3) Uani 1 1 d . . . . . H3' H 0.471576 0.605030 0.471962 0.017 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0241(2) 0.0228(2) 0.0141(3) 0.0034(2) -0.0026(2) 0.00396(18) Cl2 0.0245(2) 0.0219(2) 0.0136(3) -0.0035(2) 0.0031(2) 0.00557(18) O41 0.0147(6) 0.0150(6) 0.0150(7) 0.0012(6) 0.0010(5) 0.0028(5) O45 0.0194(7) 0.0338(8) 0.0149(8) -0.0072(7) 0.0035(6) -0.0132(7) N1 0.0130(7) 0.0171(8) 0.0152(8) 0.0004(6) 0.0010(6) 0.0014(6) O41' 0.0145(6) 0.0170(7) 0.0132(6) -0.0036(6) -0.0002(5) 0.0037(5) O45' 0.0183(7) 0.0284(7) 0.0150(8) 0.0007(7) -0.0011(6) -0.0094(6) C8 0.0164(8) 0.0154(8) 0.0123(9) 0.0014(7) -0.0033(6) -0.0016(6) C7 0.0176(8) 0.0177(9) 0.0123(9) -0.0016(8) 0.0009(7) -0.0010(7) C6 0.0150(8) 0.0160(9) 0.0157(9) -0.0008(7) 0.0022(7) 0.0015(7) C5 0.0113(7) 0.0123(9) 0.0133(9) -0.0007(7) -0.0002(6) -0.0023(7) C4 0.0118(7) 0.0114(8) 0.0162(8) 0.0002(7) -0.0012(7) -0.0013(6) C42 0.0137(8) 0.0144(9) 0.0147(9) 0.0033(7) -0.0006(7) -0.0003(7) C43 0.0138(8) 0.0139(8) 0.0185(9) -0.0001(7) -0.0002(7) 0.0000(7) C44 0.0134(8) 0.0212(10) 0.0113(9) -0.0008(8) 0.0006(7) -0.0013(8) C10 0.0105(8) 0.0145(9) 0.0132(8) -0.0013(7) -0.0013(6) -0.0025(7) C2 0.0139(9) 0.0193(9) 0.0154(11) 0.0006(9) 0.0028(7) 0.0009(7) C3 0.0154(8) 0.0148(8) 0.0148(9) 0.0024(7) -0.0002(7) -0.0011(7) C9 0.0120(8) 0.0141(8) 0.0165(9) -0.0020(7) -0.0011(6) 0.0004(6) C8' 0.0151(8) 0.0138(7) 0.0139(8) -0.0010(7) 0.0037(7) 0.0000(6) C7' 0.0170(8) 0.0181(9) 0.0129(9) 0.0001(8) -0.0023(7) 0.0000(7) C6' 0.0136(8) 0.0148(8) 0.0154(9) 0.0014(7) -0.0013(7) 0.0011(7) C5' 0.0122(8) 0.0125(8) 0.0122(8) 0.0000(7) 0.0019(6) -0.0018(7) C4' 0.0119(7) 0.0120(7) 0.0148(9) 0.0004(7) 0.0010(6) -0.0018(6) C42' 0.0144(8) 0.0143(9) 0.0143(9) -0.0029(7) 0.0009(7) -0.0013(7) C43' 0.0147(8) 0.0140(8) 0.0143(8) -0.0018(7) 0.0014(7) 0.0008(6) C44' 0.0144(8) 0.0197(9) 0.0139(9) -0.0004(8) -0.0006(7) -0.0001(8) C10' 0.0123(7) 0.0130(9) 0.0126(8) 0.0007(7) 0.0008(7) -0.0019(7) C9' 0.0126(8) 0.0153(8) 0.0153(9) 0.0008(7) 0.0022(6) 0.0017(6) N1' 0.0142(7) 0.0170(8) 0.0135(7) 0.0016(6) -0.0005(6) -0.0001(6) C2' 0.0162(9) 0.0192(9) 0.0127(10) 0.0004(9) -0.0018(7) -0.0033(8) C3' 0.0151(8) 0.0155(8) 0.0128(9) -0.0014(7) 0.0008(7) -0.0018(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C4 O41 C42 117.75(14) . . ? C44 O45 H45 109.5 . . ? C2 N1 C10 116.55(17) . . ? C4' O41' C42' 117.50(14) . . ? C44' O45' H45' 109.5 . . ? C9 C8 C7 121.94(17) . . ? C9 C8 Cl1 119.84(14) . . ? C7 C8 Cl1 118.20(15) . . ? C6 C7 C8 119.34(18) . . ? C6 C7 H7 120.3 . . ? C8 C7 H7 120.3 . . ? C7 C6 C5 120.68(17) . . ? C7 C6 H6 119.7 . . ? C5 C6 H6 119.7 . . ? C10 C5 C6 119.25(17) . . ? C10 C5 C4 118.07(16) . . ? C6 C5 C4 122.68(17) . . ? O41 C4 C3 125.78(17) . . ? O41 C4 C5 115.29(16) . . ? C3 C4 C5 118.93(16) . . ? O41 C42 C43 107.15(15) . . ? O41 C42 H42A 110.3 . . ? C43 C42 H42A 110.3 . . ? O41 C42 H42B 110.3 . . ? C43 C42 H42B 110.3 . . ? H42A C42 H42B 108.5 . . ? C42 C43 C44 113.59(16) . . ? C42 C43 H43A 108.8 . . ? C44 C43 H43A 108.8 . . ? C42 C43 H43B 108.8 . . ? C44 C43 H43B 108.8 . . ? H43A C43 H43B 107.7 . . ? O45 C44 C43 108.69(16) . . ? O45 C44 H44A 110.0 . . ? C43 C44 H44A 110.0 . . ? O45 C44 H44B 110.0 . . ? C43 C44 H44B 110.0 . . ? H44A C44 H44B 108.3 . . ? N1 C10 C9 118.14(16) . . ? N1 C10 C5 122.55(17) . . ? C9 C10 C5 119.32(17) . . ? N1 C2 C3 126.0(2) . . ? N1 C2 H2 117.0 . . ? C3 C2 H2 117.0 . . ? C4 C3 C2 117.85(18) . . ? C4 C3 H3 121.1 . . ? C2 C3 H3 121.1 . . ? C8 C9 C10 119.44(17) . . ? C8 C9 H9 120.3 . . ? C10 C9 H9 120.3 . . ? C9' C8' C7' 122.21(17) . . ? C9' C8' Cl2 119.61(14) . . ? C7' C8' Cl2 118.17(15) . . ? C6' C7' C8' 119.32(17) . . ? C6' C7' H7' 120.3 . . ? C8' C7' H7' 120.3 . . ? C7' C6' C5' 120.52(17) . . ? C7' C6' H6' 119.7 . . ? C5' C6' H6' 119.7 . . ? C10' C5' C6' 119.39(17) . . ? C10' C5' C4' 118.04(16) . . ? C6' C5' C4' 122.57(17) . . ? O41' C4' C3' 125.60(16) . . ? O41' C4' C5' 115.18(16) . . ? C3' C4' C5' 119.22(16) . . ? O41' C42' C43' 106.80(15) . . ? O41' C42' H42C 110.4 . . ? C43' C42' H42C 110.4 . . ? O41' C42' H42D 110.4 . . ? C43' C42' H42D 110.4 . . ? H42C C42' H42D 108.6 . . ? C42' C43' C44' 113.30(16) . . ? C42' C43' H43C 108.9 . . ? C44' C43' H43C 108.9 . . ? C42' C43' H43D 108.9 . . ? C44' C43' H43D 108.9 . . ? H43C C43' H43D 107.7 . . ? O45' C44' C43' 108.96(16) . . ? O45' C44' H44C 109.9 . . ? C43' C44' H44C 109.9 . . ? O45' C44' H44D 109.9 . . ? C43' C44' H44D 109.9 . . ? H44C C44' H44D 108.3 . . ? N1' C10' C9' 118.25(16) . . ? N1' C10' C5' 122.39(17) . . ? C9' C10' C5' 119.36(17) . . ? C8' C9' C10' 119.15(16) . . ? C8' C9' H9' 120.4 . . ? C10' C9' H9' 120.4 . . ? C2' N1' C10' 116.66(16) . . ? N1' C2' C3' 126.0(2) . . ? N1' C2' H2' 117.0 . . ? C3' C2' H2' 117.0 . . ? C4' C3' C2' 117.63(18) . . ? C4' C3' H3' 121.2 . . ? C2' C3' H3' 121.2 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl1 C8 1.738(2) . ? Cl2 C8' 1.736(2) . ? O41 C4 1.345(2) . ? O41 C42 1.445(2) . ? O45 C44 1.422(3) . ? O45 H45 0.8200 . ? N1 C2 1.316(3) . ? N1 C10 1.377(2) . ? O41' C4' 1.349(2) . ? O41' C42' 1.448(2) . ? O45' C44' 1.422(3) . ? O45' H45' 0.8200 . ? C8 C9 1.371(3) . ? C8 C7 1.409(3) . ? C7 C6 1.365(3) . ? C7 H7 0.9300 . ? C6 C5 1.420(3) . ? C6 H6 0.9300 . ? C5 C10 1.418(3) . ? C5 C4 1.428(3) . ? C4 C3 1.378(3) . ? C42 C43 1.518(2) . ? C42 H42A 0.9700 . ? C42 H42B 0.9700 . ? C43 C44 1.521(3) . ? C43 H43A 0.9700 . ? C43 H43B 0.9700 . ? C44 H44A 0.9700 . ? C44 H44B 0.9700 . ? C10 C9 1.411(3) . ? C2 C3 1.410(3) . ? C2 H2 0.9300 . ? C3 H3 0.9300 . ? C9 H9 0.9300 . ? C8' C9' 1.369(3) . ? C8' C7' 1.410(3) . ? C7' C6' 1.367(3) . ? C7' H7' 0.9300 . ? C6' C5' 1.419(3) . ? C6' H6' 0.9300 . ? C5' C10' 1.419(3) . ? C5' C4' 1.426(2) . ? C4' C3' 1.379(2) . ? C42' C43' 1.515(2) . ? C42' H42C 0.9700 . ? C42' H42D 0.9700 . ? C43' C44' 1.519(3) . ? C43' H43C 0.9700 . ? C43' H43D 0.9700 . ? C44' H44C 0.9700 . ? C44' H44D 0.9700 . ? C10' N1' 1.378(2) . ? C10' C9' 1.415(3) . ? C9' H9' 0.9300 . ? N1' C2' 1.318(3) . ? C2' C3' 1.409(3) . ? C2' H2' 0.9300 . ? C3' H3' 0.9300 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag O45 H45 N1 0.82 2.01 2.832(2) 177.9 4_455 yes O45' H45' N1' 0.82 2.01 2.828(2) 175.1 4_455 yes C3 H3 O45' 0.93 2.45 3.365(3) 167.2 4_565 yes C3' H3' O45 0.93 2.36 3.233(3) 155.3 . yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C9 C8 C7 C6 0.0(3) . . . . ? Cl1 C8 C7 C6 178.52(15) . . . . ? C8 C7 C6 C5 -1.2(3) . . . . ? C7 C6 C5 C10 0.8(3) . . . . ? C7 C6 C5 C4 -178.81(18) . . . . ? C42 O41 C4 C3 2.9(3) . . . . ? C42 O41 C4 C5 -177.46(15) . . . . ? C10 C5 C4 O41 179.25(16) . . . . ? C6 C5 C4 O41 -1.1(3) . . . . ? C10 C5 C4 C3 -1.1(3) . . . . ? C6 C5 C4 C3 178.49(17) . . . . ? C4 O41 C42 C43 179.75(15) . . . . ? O41 C42 C43 C44 -65.4(2) . . . . ? C42 C43 C44 O45 -61.5(2) . . . . ? C2 N1 C10 C9 -179.37(17) . . . . ? C2 N1 C10 C5 0.0(3) . . . . ? C6 C5 C10 N1 -178.60(17) . . . . ? C4 C5 C10 N1 1.0(3) . . . . ? C6 C5 C10 C9 0.8(3) . . . . ? C4 C5 C10 C9 -179.57(16) . . . . ? C10 N1 C2 C3 -1.1(3) . . . . ? O41 C4 C3 C2 179.81(18) . . . . ? C5 C4 C3 C2 0.2(3) . . . . ? N1 C2 C3 C4 1.0(3) . . . . ? C7 C8 C9 C10 1.6(3) . . . . ? Cl1 C8 C9 C10 -176.89(14) . . . . ? N1 C10 C9 C8 177.47(17) . . . . ? C5 C10 C9 C8 -2.0(3) . . . . ? C9' C8' C7' C6' -0.1(3) . . . . ? Cl2 C8' C7' C6' -178.88(15) . . . . ? C8' C7' C6' C5' 1.5(3) . . . . ? C7' C6' C5' C10' -1.0(3) . . . . ? C7' C6' C5' C4' 178.53(18) . . . . ? C42' O41' C4' C3' -2.0(3) . . . . ? C42' O41' C4' C5' 177.64(15) . . . . ? C10' C5' C4' O41' -178.89(16) . . . . ? C6' C5' C4' O41' 1.5(3) . . . . ? C10' C5' C4' C3' 0.8(3) . . . . ? C6' C5' C4' C3' -178.77(17) . . . . ? C4' O41' C42' C43' 179.55(15) . . . . ? O41' C42' C43' C44' 66.38(19) . . . . ? C42' C43' C44' O45' 60.0(2) . . . . ? C6' C5' C10' N1' 178.56(16) . . . . ? C4' C5' C10' N1' -1.0(3) . . . . ? C6' C5' C10' C9' -0.8(3) . . . . ? C4' C5' C10' C9' 179.62(16) . . . . ? C7' C8' C9' C10' -1.7(3) . . . . ? Cl2 C8' C9' C10' 177.03(13) . . . . ? N1' C10' C9' C8' -177.23(16) . . . . ? C5' C10' C9' C8' 2.2(3) . . . . ? C9' C10' N1' C2' 179.34(17) . . . . ? C5' C10' N1' C2' 0.0(3) . . . . ? C10' N1' C2' C3' 1.4(3) . . . . ? O41' C4' C3' C2' -179.97(18) . . . . ? C5' C4' C3' C2' 0.4(3) . . . . ? N1' C2' C3' C4' -1.6(3) . . . . ?