#------------------------------------------------------------------------------ #$Date: 2020-04-29 01:50:00 +0300 (Wed, 29 Apr 2020) $ #$Revision: 251254 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/04/7240420.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7240420 loop_ _publ_author_name 'Pan, Bochen' 'Wang, Zhanzhong' 'Shen, Yichun' 'Wei, Liangxiao' 'Wei, Hongyuan' 'Dang, Leping' _publ_section_title ; Solvatomorphism and Phase Transformation of CL-20: Probing Properties and Investigating Mechanisms ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D0CE00059K _journal_year 2020 _chemical_formula_moiety 'C6 H6 N12 O12, 2(C4 H9 N O)' _chemical_formula_sum 'C14 H24 N14 O14' _chemical_formula_weight 612.47 _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens geom _audit_creation_date 2019-07-19 _audit_creation_method ; Olex2 1.2 (compiled 2018.04.26 svn.r3504 for OlexSys, GUI svn.r5492) ; _audit_update_record ; 2019-07-20 deposited with the CCDC. 2020-04-27 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 103.25(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 13.344(3) _cell_length_b 8.2595(17) _cell_length_c 24.392(5) _cell_measurement_reflns_used 6850 _cell_measurement_temperature 113(2) _cell_measurement_theta_max 27.8824 _cell_measurement_theta_min 1.5678 _cell_volume 2616.8(10) _computing_cell_refinement crystalclear _computing_data_collection crystalclear _computing_data_reduction crystalclear _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _diffrn_ambient_temperature 113.15 _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'rigaku saturn' _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0503 _diffrn_reflns_av_unetI/netI 0.0736 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_limit_l_min -32 _diffrn_reflns_number 29338 _diffrn_reflns_point_group_measured_fraction_full 0.993 _diffrn_reflns_point_group_measured_fraction_max 0.992 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.826 _diffrn_reflns_theta_min 1.605 _exptl_absorpt_coefficient_mu 0.138 _exptl_absorpt_correction_T_max 1 _exptl_absorpt_correction_T_min 0.8339 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS (Sheldrick, 1996)' _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.555 _exptl_crystal_description prism _exptl_crystal_F_000 1272 _exptl_crystal_recrystallization_method 'Re-crystallisation from solvent' _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.18 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.299 _refine_diff_density_min -0.331 _refine_diff_density_rms 0.064 _refine_ls_abs_structure_details ; Flack x determined using 2251 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.1(8) _refine_ls_extinction_coef 0.029(2) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2017/1 (Sheldrick 2017)' _refine_ls_goodness_of_fit_ref 1.000 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 794 _refine_ls_number_reflns 12330 _refine_ls_number_restraints 50 _refine_ls_restrained_S_all 7.327 _refine_ls_R_factor_all 0.0785 _refine_ls_R_factor_gt 0.0591 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0801P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1434 _refine_ls_wR_factor_ref 0.1552 _reflns_Friedel_coverage 0.863 _reflns_Friedel_fraction_full 0.989 _reflns_Friedel_fraction_max 0.987 _reflns_number_gt 8012 _reflns_number_total 12330 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d0ce00059k2.cif _cod_data_source_block 1905620 _cod_depositor_comments ; The following automatic conversions were performed: data item '_exptl_absorpt_correction_type' value 'MULTI-SCAN' was changed to 'multi-scan' in accordance with the /home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 last updated on 2011-04-26. Automatic conversion script Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas ; _cod_database_code 7240420 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.984 _shelx_estimated_absorpt_t_min 0.973 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups, All C(H,H,H,H,H,H) groups 2. Restrained distances N27-C23 = N27-C24 = N28-C26 = N28-C27 = N28-C28 1.5 with sigma of 0.01 N25-C14 = N25-C15 = N25-C16 = N26_$1-C18_$1 = N26_$1-C19_$1 = N26_$1-C20_$1 1.5 with sigma of 0.01 C13-C14 = C17_$1-C18_$1 = C25_$3-C26_$5 1.54 with sigma of 0.01 O25-C14 = O26_$1-C18_$1 = O28_$5-C26_$5 1.22 with sigma of 0.01 C15-C14A = C14-C13 1.5 with sigma of 0.02 3. Uiso/Uaniso restraints and constraints Uanis(N28) \\sim Ueq, Uanis(C26) \\sim Ueq, Uanis(N27) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C21) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(C16) \\sim Ueq: with sigma of 0.003 and sigma for terminal atoms of 0.006 Uanis(C14A) = Uanis(C14) Uanis(N25A) = Uanis(N25) Uanis(C26A) = Uanis(C26) Uanis(N28) = Uanis(N28A) Uanis(N27A) = Uanis(N27) Uanis(C22) = Uanis(C22A) 4. Others Sof(H13D)=Sof(H13E)=Sof(H13F)=Sof(H16D)=Sof(H16E)=Sof(H16F)=Sof(N25A)=1-FVAR(1) Sof(N25)=Sof(H15A)=Sof(H15B)=Sof(H15C)=Sof(H16A)=Sof(H16B)=Sof(H16C)=FVAR(1) Sof(H15D)=Sof(H15E)=Sof(H15F)=Sof(C14A)=1-FVAR(2) Sof(H13A)=Sof(H13B)=Sof(H13C)=Sof(C14)=FVAR(2) Sof(H27D)=Sof(H27E)=Sof(H27F)=Sof(C26A)=1-FVAR(3) Sof(H25A)=Sof(H25B)=Sof(H25C)=Sof(C26)=FVAR(3) Sof(H25D)=Sof(H25E)=Sof(H25F)=Sof(H28D)=Sof(H28E)=Sof(H28F)=Sof(N28A)=1-FVAR(4) Sof(N28)=Sof(H27A)=Sof(H27B)=Sof(H27C)=Sof(H28A)=Sof(H28B)=Sof(H28C)=FVAR(4) Sof(H21D)=Sof(H21E)=Sof(H21F)=Sof(H23D)=Sof(H23E)=Sof(H23F)=Sof(N27A)=1-FVAR(5) Sof(N27)=Sof(H23A)=Sof(H23B)=Sof(H23C)=Sof(H24A)=Sof(H24B)=Sof(H24C)=FVAR(5) Sof(H24D)=Sof(H24E)=Sof(H24F)=Sof(C22A)=1-FVAR(6) Sof(H21A)=Sof(H21B)=Sof(H21C)=Sof(C22)=FVAR(6) 5.a Ternary CH refined with riding coordinates: C1(H1), C2(H2), C3(H3), C4(H4), C5(H5), C6(H6), C7(H7), C8(H8), C9(H9), C10(H10), C11(H11), C12(H12) 5.b Idealised Me refined as rotating group: C13(H13A,H13B,H13C), C13(H13D,H13E,H13F), C15(H15A,H15B,H15C), C15(H15D,H15E, H15F), C16(H16A,H16B,H16C), C16(H16D,H16E,H16F), C17(H17A,H17B,H17C), C19(H19A, H19B,H19C), C20(H20A,H20B,H20C), C21(H21A,H21B,H21C), C21(H21D,H21E,H21F), C23(H23A,H23B,H23C), C23(H23D,H23E,H23F), C24(H24A,H24B,H24C), C24(H24D,H24E, H24F), C25(H25A,H25B,H25C), C25(H25D,H25E,H25F), C27(H27A,H27B,H27C), C27(H27D, H27E,H27F), C28(H28A,H28B,H28C), C28(H28D,H28E,H28F) ; _shelx_res_file ; TITL shelxl in P2(1) New:P21 shelxl.res created by SHELXL-2017/1 at 18:36:03 on 19-Jul-2019 CELL 0.71073 13.344 8.2595 24.392 90 103.25 90 ZERR 4 0.003 0.0017 0.005 0 0.03 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H N O UNIT 56 96 56 56 EQIV $1 +X,1+Y,+Z EQIV $2 1-X,-0.5+Y,1-Z EQIV $3 1-X,1.5+Y,1-Z EQIV $4 1-X,-0.5+Y,2-Z EQIV $5 1-X,0.5+Y,1-Z DFIX 1.5 0.01 N27 C23 N27 C24 N28 C26 N28 C27 N28 C28 DFIX 1.5 0.01 N25 C14 N25 C15 N25 C16 N26_$1 C18_$1 N26_$1 C19_$1 N26_$1 = C20_$1 DFIX 1.54 0.01 C13 C14 C17_$1 C18_$1 C25_$3 C26_$5 DFIX 1.22 0.01 O25 C14 O26_$1 C18_$1 O28_$5 C26_$5 DFIX 1.5 C15 C14A C14 C13 ISOR 0.01 0.02 N28 C26 N27 ISOR 0.01 0.02 C21 ISOR 0.003 0.006 C16 EADP C14A C14 EADP N25A N25 EADP C26A C26 EADP N28 N28A EADP N27A N27 EADP C22 C22A L.S. 10 PLAN 10 SIZE 0.2 0.18 0.12 TEMP -160 HTAB C1 O25 HTAB C4 O25 HTAB C6 O6_$2 HTAB C7 O26 HTAB C10 O26 HTAB C11 O16_$4 HTAB C17 O4 HTAB C20 O10_$5 HTAB C20 O12_$2 BOND $H CONF HTAB fmap 2 acta OMIT 0 0 2 OMIT 1 0 0 OMIT -1 0 8 OMIT 1 0 13 OMIT -1 -4 1 OMIT -7 1 1 OMIT -7 3 1 OMIT 5 -3 11 OMIT -5 -1 7 OMIT 1 -2 0 OMIT -5 1 7 REM REM REM WGHT 0.080100 EXTI 0.029262 FVAR 0.65153 0.76130 0.74897 0.52394 0.59196 0.63020 0.64964 O1 4 1.011628 0.214785 0.573721 11.00000 0.05268 0.12700 = 0.08982 0.00405 -0.00441 0.04644 O2 4 1.009040 0.246637 0.485674 11.00000 0.05683 0.14995 = 0.09104 -0.03226 0.02322 0.03990 O3 4 0.841895 0.125888 0.642977 11.00000 0.08660 0.04103 = 0.03890 0.00408 -0.00895 0.01639 O4 4 0.679351 0.069994 0.611020 11.00000 0.07830 0.05842 = 0.05143 0.01845 0.03310 0.00677 O5 4 0.494595 0.461881 0.524574 11.00000 0.03371 0.07431 = 0.07204 -0.00306 0.01833 0.00466 O6 4 0.587083 0.671858 0.558976 11.00000 0.06065 0.04393 = 0.06502 -0.00569 0.01988 0.02048 O7 4 0.768108 0.854822 0.476351 11.00000 0.11809 0.02975 = 0.05393 0.00799 0.01953 -0.00478 O8 4 0.803066 0.835742 0.567881 11.00000 0.10168 0.03077 = 0.05161 -0.01535 0.02250 -0.00677 O9 4 0.839114 0.140893 0.390255 11.00000 0.07854 0.05636 = 0.06846 -0.02106 0.04353 0.00085 O10 4 0.676093 0.090344 0.380154 11.00000 0.07032 0.05412 = 0.04220 -0.01858 0.00803 -0.01860 O11 4 0.520566 0.409462 0.373213 11.00000 0.03862 0.08461 = 0.03661 0.01001 -0.00600 -0.00828 O12 4 0.589072 0.652727 0.383374 11.00000 0.06146 0.06168 = 0.05327 0.02681 0.00674 0.01468 O13 4 0.745162 0.626737 0.940901 11.00000 0.08367 0.03020 = 0.04690 0.00895 0.01402 0.00013 O14 4 0.793561 0.635004 1.032166 11.00000 0.12335 0.02984 = 0.04763 -0.01076 0.01248 -0.00844 O15 4 0.541982 0.471347 0.946539 11.00000 0.05716 0.03834 = 0.07321 0.00827 0.02118 0.02121 O16 4 0.472349 0.259868 0.977000 11.00000 0.03547 0.06839 = 0.08471 0.00712 0.02718 0.00642 O17 4 0.574714 -0.118830 0.885405 11.00000 0.05809 0.06092 = 0.05772 -0.02375 -0.00293 -0.01416 O18 4 0.716726 -0.084840 0.857364 11.00000 0.08800 0.03829 = 0.03655 -0.00737 0.01752 0.00947 O19 4 1.018432 0.022072 1.013713 11.00000 0.04538 0.13641 = 0.09067 0.02048 0.00849 0.05425 O20 4 0.944914 -0.000942 0.924668 11.00000 0.07239 0.10742 = 0.08305 -0.01360 0.03998 0.03978 O21 4 0.698207 0.427663 1.124676 11.00000 0.09456 0.04954 = 0.05891 -0.02536 0.03814 -0.00872 O22 4 0.633402 0.187497 1.131811 11.00000 0.07508 0.07887 = 0.04401 -0.01416 0.03571 -0.02542 O23 4 0.768157 -0.132270 1.119931 11.00000 0.09066 0.04416 = 0.03940 0.01672 0.01557 -0.01195 O24 4 0.922872 -0.095378 1.108147 11.00000 0.05721 0.05105 = 0.06069 0.01526 -0.01981 0.00477 N1 3 0.975389 0.266957 0.527252 11.00000 0.03471 0.08036 = 0.07843 -0.01369 0.00320 0.02106 N2 3 0.890125 0.373152 0.521552 11.00000 0.02008 0.03981 = 0.04998 -0.00563 0.00721 0.00417 N3 3 0.764114 0.220064 0.557727 11.00000 0.04435 0.02798 = 0.02944 0.00361 0.00372 0.00811 N4 3 0.761271 0.134821 0.609119 11.00000 0.07280 0.03086 = 0.03030 0.00327 0.01078 0.01481 N5 3 0.663962 0.436903 0.555847 11.00000 0.02881 0.03167 = 0.03464 0.00155 0.01149 0.00469 N6 3 0.575946 0.530183 0.545142 11.00000 0.04142 0.04608 = 0.04358 0.00336 0.01917 0.01208 N7 3 0.773704 0.612494 0.515421 11.00000 0.04295 0.01753 = 0.03612 -0.00031 0.01229 -0.00013 N8 3 0.780370 0.779796 0.520426 11.00000 0.06931 0.02215 = 0.05460 -0.00369 0.01990 0.00082 N9 3 0.756336 0.246103 0.451759 11.00000 0.03699 0.02926 = 0.03112 -0.00683 0.01102 0.00103 N10 3 0.756889 0.154003 0.402702 11.00000 0.06027 0.03868 = 0.03697 -0.00871 0.01591 -0.00078 N11 3 0.648807 0.466594 0.448711 11.00000 0.02873 0.03391 = 0.02926 0.00485 0.00326 0.00108 N12 3 0.582035 0.511557 0.396624 11.00000 0.03730 0.06168 = 0.03106 0.01041 0.00846 0.00934 N13 3 0.765934 0.397382 0.989295 11.00000 0.03779 0.01816 = 0.03055 -0.00014 0.00770 -0.00297 N14 3 0.767102 0.565657 0.987515 11.00000 0.06509 0.02362 = 0.04474 -0.00289 0.01203 -0.00447 N15 3 0.617118 0.232747 0.947576 11.00000 0.02657 0.02822 = 0.03204 -0.00129 0.00591 0.00512 N16 3 0.539208 0.327193 0.957481 11.00000 0.03184 0.04834 = 0.04959 -0.00445 0.00599 0.01386 N17 3 0.708978 0.010629 0.942497 11.00000 0.03366 0.02187 = 0.02732 -0.00484 0.00474 0.00167 N18 3 0.661253 -0.068648 0.890577 11.00000 0.06551 0.03008 = 0.02926 -0.00297 0.00378 0.01098 N19 3 0.869009 0.151343 0.979695 11.00000 0.02606 0.03582 = 0.03961 0.00307 0.01252 0.00931 N20 3 0.950266 0.048192 0.972414 11.00000 0.04872 0.07547 = 0.07150 -0.00126 0.02694 0.03109 N21 3 0.693145 0.249312 1.054847 11.00000 0.03797 0.02999 = 0.02879 -0.00578 0.01612 -0.00227 N22 3 0.674868 0.289912 1.108525 11.00000 0.05111 0.05438 = 0.03350 -0.01401 0.01959 -0.00633 N23 3 0.791795 0.024068 1.048407 11.00000 0.03319 0.02743 = 0.02930 0.00838 0.00258 -0.00038 N24 3 0.830556 -0.072683 1.096591 11.00000 0.06271 0.03233 = 0.03164 0.00266 -0.00964 -0.00290 C1 1 0.835025 0.361024 0.566122 11.00000 0.03255 0.03075 = 0.03110 -0.00274 -0.00024 0.00765 AFIX 13 H1 2 0.884488 0.354318 0.603659 11.00000 -1.20000 AFIX 0 C2 1 0.826743 0.384219 0.464491 11.00000 0.02533 0.03547 = 0.03663 -0.00413 0.01223 -0.00028 AFIX 13 H2 2 0.870416 0.393222 0.436343 11.00000 -1.20000 AFIX 0 C3 1 0.753863 0.536250 0.461499 11.00000 0.03088 0.02638 = 0.03377 0.00230 0.01044 -0.00144 AFIX 13 H3 2 0.763122 0.613639 0.431519 11.00000 -1.20000 AFIX 0 C4 1 0.765515 0.515004 0.562997 11.00000 0.03606 0.02349 = 0.02679 -0.00411 0.00692 0.00228 AFIX 13 H4 2 0.783505 0.578612 0.598795 11.00000 -1.20000 AFIX 0 C5 1 0.663045 0.280372 0.528249 11.00000 0.03329 0.03066 = 0.03542 -0.00007 0.00923 -0.00013 AFIX 13 H5 2 0.606577 0.209857 0.535537 11.00000 -1.20000 AFIX 0 C6 1 0.657679 0.295184 0.462333 11.00000 0.03099 0.03085 = 0.03323 -0.00021 0.00515 -0.00557 AFIX 13 H6 2 0.599283 0.231303 0.439331 11.00000 -1.20000 AFIX 0 C7 1 0.713578 0.306249 0.940883 11.00000 0.03160 0.02324 = 0.02817 -0.00130 0.00712 0.00331 AFIX 13 H7 2 0.702495 0.373031 0.905811 11.00000 -1.20000 AFIX 0 C8 1 0.789460 0.314321 1.042367 11.00000 0.03065 0.02739 = 0.02765 -0.00336 0.00597 -0.00440 AFIX 13 H8 2 0.826297 0.386992 1.073262 11.00000 -1.20000 AFIX 0 C9 1 0.854611 0.159788 1.037525 11.00000 0.02272 0.03241 = 0.03319 0.00627 0.00421 0.00076 AFIX 13 H9 2 0.922313 0.162612 1.065512 11.00000 -1.20000 AFIX 0 C10 1 0.776119 0.148794 0.935428 11.00000 0.04055 0.02570 = 0.03113 -0.00164 0.01371 0.00656 AFIX 13 H10 2 0.793365 0.144125 0.897666 11.00000 -1.20000 AFIX 0 C11 1 0.635633 0.071534 0.972951 11.00000 0.02527 0.02861 = 0.03181 -0.00018 0.00404 -0.00456 AFIX 13 H11 2 0.571258 0.005129 0.965103 11.00000 -1.20000 AFIX 0 C12 1 0.685606 0.080759 1.038521 11.00000 0.02986 0.03564 = 0.02819 -0.00306 0.00610 -0.00566 AFIX 13 H12 2 0.645022 0.017184 1.060823 11.00000 -1.20000 AFIX 0 O25 4 0.816952 0.499874 0.683199 11.00000 0.12529 0.07183 = 0.02965 0.00060 0.00194 0.03008 PART 1 N25 3 0.850557 0.508692 0.778297 21.00000 0.05001 0.06156 = 0.03660 -0.00442 0.00420 0.00969 PART 0 C13 1 0.771937 0.751607 0.726972 11.00000 0.08648 0.05946 = 0.07652 0.01596 0.03371 0.01792 PART 1 AFIX 137 H13A 2 0.723511 0.775407 0.691163 31.00000 -1.50000 H13B 2 0.829531 0.828131 0.732715 31.00000 -1.50000 H13C 2 0.736644 0.761927 0.757885 31.00000 -1.50000 AFIX 137 PART 0 PART 2 H13D 2 0.799434 0.856528 0.742150 -21.00000 -1.50000 H13E 2 0.698195 0.746557 0.726052 -21.00000 -1.50000 H13F 2 0.782274 0.738752 0.688709 -21.00000 -1.50000 AFIX 0 PART 0 PART 1 C14 1 0.812897 0.578135 0.725644 31.00000 0.06369 0.04902 = 0.04154 0.00224 0.00873 -0.00228 PART 0 C15 1 0.893785 0.347580 0.777241 11.00000 0.07084 0.05365 = 0.06594 0.00110 -0.00425 0.01524 PART 1 AFIX 137 H15A 2 0.880470 0.308631 0.738289 21.00000 -1.50000 H15B 2 0.861820 0.273898 0.799728 21.00000 -1.50000 H15C 2 0.968223 0.351539 0.792994 21.00000 -1.50000 AFIX 137 PART 0 PART 2 H15D 2 0.845722 0.310334 0.799501 -31.00000 -1.50000 H15E 2 0.957493 0.385194 0.802581 -31.00000 -1.50000 H15F 2 0.909405 0.258040 0.754185 -31.00000 -1.50000 AFIX 0 PART 0 C16 1 0.852253 0.600073 0.829197 11.00000 0.07193 0.08172 = 0.05772 -0.01508 0.01489 0.00745 PART 1 AFIX 137 H16A 2 0.870164 0.712995 0.823622 21.00000 -1.50000 H16B 2 0.903569 0.553398 0.860485 21.00000 -1.50000 H16C 2 0.784174 0.595641 0.837915 21.00000 -1.50000 AFIX 137 PART 0 PART 2 H16D 2 0.841894 0.704259 0.846314 -21.00000 -1.50000 H16E 2 0.924044 0.565935 0.842576 -21.00000 -1.50000 H16F 2 0.806669 0.518695 0.839780 -21.00000 -1.50000 AFIX 0 PART 0 O26 4 0.649568 0.269458 0.824180 11.00000 0.11388 0.05156 = 0.03335 -0.00170 -0.00247 0.02670 N26 3 0.574731 0.438182 0.754827 11.00000 0.05638 0.05546 = 0.04784 0.00162 -0.00416 0.00782 C17 1 0.640018 0.175170 0.730845 11.00000 0.08221 0.09001 = 0.05319 -0.03452 -0.01614 0.02480 AFIX 137 H17A 2 0.684545 0.223962 0.708517 11.00000 -1.50000 H17B 2 0.574150 0.144620 0.705945 11.00000 -1.50000 H17C 2 0.673506 0.078612 0.750117 11.00000 -1.50000 AFIX 0 C18 1 0.621358 0.295482 0.773794 11.00000 0.05758 0.06162 = 0.03621 -0.00957 -0.00214 0.00568 C19 1 0.549859 0.553119 0.795618 11.00000 0.08278 0.04844 = 0.08019 -0.00879 0.01369 0.01455 AFIX 137 H19A 2 0.550761 0.496872 0.831103 11.00000 -1.50000 H19B 2 0.481268 0.598811 0.780633 11.00000 -1.50000 H19C 2 0.600934 0.640444 0.802363 11.00000 -1.50000 AFIX 0 C20 1 0.537946 0.472221 0.695106 11.00000 0.10386 0.07923 = 0.04668 0.01128 -0.02115 0.00252 AFIX 137 H20A 2 0.546770 0.587677 0.688232 11.00000 -1.50000 H20B 2 0.464868 0.443778 0.683273 11.00000 -1.50000 H20C 2 0.577409 0.408148 0.673560 11.00000 -1.50000 AFIX 0 O27 4 0.746024 0.460131 0.344512 11.00000 0.06918 0.06189 = 0.03751 -0.00012 0.01768 -0.00794 PART 1 N27 3 0.713866 0.636291 0.276011 61.00000 0.08815 0.04653 = 0.04052 -0.00261 0.02746 -0.01425 PART 0 C21 1 0.620569 0.383307 0.257080 11.00000 0.14271 0.08747 = 0.06420 -0.03526 0.04586 -0.05333 PART 1 AFIX 137 H21A 2 0.652534 0.330230 0.229442 71.00000 -1.50000 H21B 2 0.564009 0.452587 0.237468 71.00000 -1.50000 H21C 2 0.593706 0.300967 0.278855 71.00000 -1.50000 AFIX 137 PART 0 PART 2 H21D 2 0.547362 0.376142 0.257317 -61.00000 -1.50000 H21E 2 0.661395 0.327365 0.290177 -61.00000 -1.50000 H21F 2 0.632287 0.332403 0.222798 -61.00000 -1.50000 AFIX 0 PART 0 C23 1 0.649491 0.690066 0.218873 11.00000 0.14793 0.05882 = 0.06845 0.02248 0.05300 0.02964 PART 1 AFIX 137 H23A 2 0.601354 0.774895 0.224329 61.00000 -1.50000 H23B 2 0.610812 0.597399 0.199692 61.00000 -1.50000 H23C 2 0.694966 0.732436 0.195905 61.00000 -1.50000 AFIX 137 PART 0 PART 2 H23D 2 0.696623 0.664894 0.194590 -61.00000 -1.50000 H23E 2 0.669761 0.792774 0.238390 -61.00000 -1.50000 H23F 2 0.579140 0.699163 0.195863 -61.00000 -1.50000 AFIX 0 PART 0 C24 1 0.785354 0.748098 0.312817 11.00000 0.12334 0.05896 = 0.07080 0.00265 0.02309 -0.04364 PART 1 AFIX 137 H24A 2 0.840193 0.779780 0.294269 61.00000 -1.50000 H24B 2 0.815595 0.694085 0.348552 61.00000 -1.50000 H24C 2 0.747764 0.844705 0.320080 61.00000 -1.50000 AFIX 137 PART 0 PART 2 H24D 2 0.736789 0.835889 0.298872 -71.00000 -1.50000 H24E 2 0.839446 0.746790 0.291593 -71.00000 -1.50000 H24F 2 0.816431 0.765363 0.352854 -71.00000 -1.50000 AFIX 0 PART 0 O28 4 0.883984 0.228270 0.158143 11.00000 0.07612 0.06381 = 0.03138 -0.00216 0.00014 -0.01988 PART 1 N28 3 0.926614 0.258401 0.253467 51.00000 0.06296 0.05619 = 0.04209 -0.01051 0.01199 -0.01583 PART 0 C25 1 0.956774 0.491194 0.198858 11.00000 0.13062 0.04900 = 0.10373 0.00485 0.03152 -0.03504 PART 1 AFIX 137 H25A 2 1.029235 0.491988 0.219137 41.00000 -1.50000 H25B 2 0.917244 0.563514 0.217805 41.00000 -1.50000 H25C 2 0.951144 0.528351 0.160113 41.00000 -1.50000 AFIX 137 PART 0 PART 2 H25D 2 0.936897 0.595182 0.212561 -51.00000 -1.50000 H25E 2 0.914989 0.470772 0.160888 -51.00000 -1.50000 H25F 2 1.029724 0.494404 0.197807 -51.00000 -1.50000 AFIX 0 PART 0 PART 1 C26 1 0.916714 0.329389 0.198150 41.00000 0.05539 0.05558 = 0.03466 0.00047 -0.00026 -0.00963 PART 0 C27 1 0.881834 0.094296 0.252135 11.00000 0.11768 0.05996 = 0.08872 0.01959 0.05193 -0.00717 PART 1 AFIX 137 H27A 2 0.812896 0.101347 0.259643 51.00000 -1.50000 H27B 2 0.925818 0.026772 0.280949 51.00000 -1.50000 H27C 2 0.877111 0.046005 0.214930 51.00000 -1.50000 AFIX 137 PART 0 PART 2 H27D 2 0.836636 0.138099 0.275015 -41.00000 -1.50000 H27E 2 0.947384 0.061113 0.276772 -41.00000 -1.50000 H27F 2 0.848816 0.000401 0.230843 -41.00000 -1.50000 AFIX 0 PART 0 C28 1 0.969726 0.356530 0.303106 11.00000 0.07290 0.08761 = 0.05155 -0.02937 0.01892 -0.02041 PART 1 AFIX 137 H28A 2 0.995225 0.459050 0.291313 51.00000 -1.50000 H28B 2 1.026653 0.297841 0.327574 51.00000 -1.50000 H28C 2 0.916218 0.378519 0.323726 51.00000 -1.50000 AFIX 137 PART 0 PART 2 H28D 2 1.028327 0.283615 0.316005 -51.00000 -1.50000 H28E 2 0.911271 0.319355 0.317840 -51.00000 -1.50000 H28F 2 0.988876 0.466403 0.316732 -51.00000 -1.50000 AFIX 0 N25A 3 0.827027 0.618108 0.763803 -21.00000 0.05001 0.06156 = 0.03660 -0.00442 0.00420 0.00969 C14A 1 0.843610 0.490687 0.737852 -31.00000 0.06369 0.04902 = 0.04154 0.00224 0.00873 -0.00228 C26A 1 0.902565 0.230597 0.209211 -41.00000 0.05539 0.05558 = 0.03466 0.00047 -0.00026 -0.00963 N28A 3 0.939300 0.356870 0.238049 -51.00000 0.06296 0.05619 = 0.04209 -0.01051 0.01199 -0.01583 PART 0 PART 1 C22 1 0.703912 0.490425 0.298340 71.00000 0.07092 0.04278 = 0.03185 -0.00648 0.02258 -0.00905 PART 0 PART 2 N27A 3 0.653708 0.566158 0.258601 -61.00000 0.08815 0.04653 = 0.04052 -0.00261 0.02746 -0.01425 C22A 1 0.725516 0.578506 0.304857 -71.00000 0.07092 0.04278 = 0.03185 -0.00648 0.02258 -0.00905 HKLF 4 REM shelxl in P2(1) New:P21 REM R1 = 0.0591 for 8012 Fo > 4sig(Fo) and 0.0785 for all 12330 data REM 794 parameters refined using 50 restraints END WGHT 0.0801 0.0000 REM Instructions for potential hydrogen bonds HTAB C1 O25 HTAB C4 O25 HTAB C6 O6_$2 HTAB C7 O26 HTAB C11 O16_$4 HTAB C12 O15_$4 EQIV $6 -x+2, y+1/2, -z+2 HTAB C15 O24_$6 HTAB C16 O24_$6 HTAB C16 O18_$1 HTAB C16 O24_$6 HTAB C20 O10_$5 EQIV $7 x, y, z-1 HTAB C21 O22_$7 HTAB C21 O27 HTAB C21 O22_$7 EQIV $8 x, y+1, z-1 HTAB C23 O23_$8 HTAB C23 O21_$7 EQIV $9 -x+2, y+1/2, -z+1 HTAB C24 O1_$9 HTAB C28 O27 HTAB C28 O9 HTAB C28 O3_$9 REM Highest difference peak 0.299, deepest hole -0.331, 1-sigma level 0.064 Q1 1 0.9303 0.3016 0.2095 11.00000 0.05 0.30 Q2 1 0.9055 0.1538 0.6357 11.00000 0.05 0.28 Q3 1 0.4779 0.5781 0.6183 11.00000 0.05 0.27 Q4 1 0.8224 0.5789 0.7410 11.00000 0.05 0.27 Q5 1 1.0341 0.1609 1.0483 11.00000 0.05 0.25 Q6 1 0.9361 0.1654 0.6158 11.00000 0.05 0.24 Q7 1 0.4785 -0.1141 0.8849 11.00000 0.05 0.24 Q8 1 0.8824 0.5876 0.5905 11.00000 0.05 0.23 Q9 1 0.5967 0.3484 0.7319 11.00000 0.05 0.23 Q10 1 1.0008 0.1680 0.6357 11.00000 0.05 0.22 ; _shelx_res_checksum 94088 _shelx_hkl_file ; 0 0 -2 0.86 0.96 0 0 2 -0.15 0.21 0 0 -3 6.67 3.27 0 0 3 1.90 8.62 0 0 -3 5.70 4.18 0 0 3 4.73 2.42 0 0 3 5.70 0.49 0 0 -3 6.42 3.96 0 0 -5 41.00 2.15 0 0 5 48.51 27.74 0 0 -5 32.65 17.00 0 0 5 37.93 7.05 0 0 -5 43.08 5.26 0 0 -6 1364.35 24.47 0 0 6 1319.09 23.54 0 0 -6 1361.62 23.92 0 0 6 1272.11 22.26 0 0 -7 101.51 4.24 0 0 7 79.38 11.88 0 0 -7 86.76 2.95 0 0 7 85.15 2.62 0 0 7 89.25 2.84 0 0 -7 82.47 2.59 0 0 -8 6.47 7.30 0 0 -8 5.94 3.63 0 0 8 6.90 4.33 0 0 8 9.40 4.09 0 0 -8 9.27 3.81 0 0 -9 13.66 7.91 0 0 -9 7.74 5.94 0 0 9 10.10 1.36 0 0 9 21.80 4.20 0 0 -9 9.68 4.77 0 0 -10 1787.54 43.62 0 0 -10 1903.19 46.27 0 0 -10 1882.07 44.90 0 0 -11 218.38 31.89 0 0 -11 237.58 14.44 0 0 -12 4748.72 112.96 0 0 12 4846.36 24.94 0 0 -13 55.90 6.73 0 0 -13 64.75 23.49 0 0 13 52.76 5.63 0 0 -13 52.77 6.26 0 0 -14 1932.98 59.48 0 0 -14 1852.16 54.98 0 0 14 1913.17 56.15 0 0 -15 -1.87 4.33 0 0 -15 1.51 1.46 0 0 15 1.77 2.00 0 0 -16 179.71 14.61 0 0 -16 164.12 12.63 0 0 16 167.66 12.76 0 0 -17 -0.25 5.28 0 0 -17 12.55 4.63 0 0 17 10.21 3.00 0 0 -18 547.15 34.24 0 0 -18 585.98 35.22 0 0 18 591.48 34.41 0 0 -19 132.29 14.66 0 0 -19 137.11 13.60 0 0 -20 8.29 5.79 0 0 -20 7.17 5.94 0 0 -21 0.99 3.92 0 0 -21 7.96 4.55 0 0 21 11.76 3.75 0 0 -22 141.54 8.84 0 0 -22 145.36 15.69 0 0 22 151.48 8.24 0 0 -23 166.10 15.79 0 0 -23 160.72 9.19 0 0 23 197.29 16.94 0 0 -24 235.98 14.00 0 0 -24 253.49 13.38 0 0 24 266.62 12.37 0 0 -25 -0.50 3.18 0 0 -25 1.06 3.27 0 0 -26 6.62 7.12 0 0 -26 9.70 6.34 0 0 -27 10.82 9.35 0 0 -27 11.27 8.03 0 0 -28 14.61 11.54 0 0 -28 6.91 6.61 0 0 -29 5.03 8.17 0 0 -29 2.06 4.33 0 0 -30 2.47 6.49 0 0 -30 6.11 5.74 0 0 -31 4.13 4.82 0 -1 0 -0.65 1.01 0 1 0 0.31 1.10 0 -1 0 0.59 1.03 0 1 0 1.09 1.57 0 1 0 2.28 1.69 0 -1 0 0.66 0.94 0 -1 1 116.02 3.25 0 1 -1 127.24 3.35 0 -1 -1 118.15 3.03 0 1 1 120.41 3.36 0 -1 1 128.62 3.48 0 1 -1 111.12 3.22 0 -1 -1 106.09 3.51 0 1 1 118.12 3.37 0 -1 -1 108.01 2.79 0 1 1 118.95 3.07 0 1 -1 112.48 2.48 0 -1 2 518.44 17.40 0 1 -2 484.60 16.57 0 -1 -2 529.12 17.67 0 1 2 499.42 16.79 0 1 -2 513.92 17.38 0 -1 -2 507.66 17.30 0 1 2 524.14 17.77 0 1 -2 600.04 20.14 0 1 -2 522.31 17.12 0 1 2 555.38 18.50 0 -1 -2 595.22 19.81 0 1 -3 226.82 19.05 0 -1 3 228.18 19.15 0 -1 -3 241.73 8.70 0 1 3 222.15 18.55 0 1 3 241.11 8.88 0 -1 -3 216.31 18.28 0 1 -3 246.69 8.80 0 -1 3 218.21 18.28 0 -1 3 218.67 18.10 0 1 -3 235.20 7.89 0 1 3 223.56 18.75 0 -1 -3 225.12 19.01 0 -1 4 729.71 24.43 0 1 -4 733.65 24.70 0 -1 -4 691.12 23.08 0 1 4 768.18 25.40 0 -1 -4 681.69 23.22 0 1 4 726.32 24.29 0 1 -4 710.00 23.63 0 -1 4 725.58 24.03 0 -1 4 764.87 24.66 0 1 4 826.88 27.41 0 -1 -4 733.19 24.43 0 -1 5 2704.85 46.64 0 1 -5 2649.78 45.89 0 -1 -5 2625.02 45.04 0 1 5 2860.14 48.68 0 -1 -5 2688.95 46.83 0 1 5 2605.99 44.98 0 1 -5 2712.85 46.19 0 -1 5 2739.29 46.68 0 1 5 2678.00 46.11 0 -1 -5 2704.50 46.58 0 -1 6 1983.22 35.35 0 1 -6 1829.02 32.89 0 -1 -6 1851.09 33.19 0 1 6 1819.97 31.87 0 -1 -6 1852.16 34.09 0 1 6 1996.44 35.28 0 1 -6 1797.99 31.12 0 -1 6 2054.40 36.10 0 1 6 1886.36 33.31 0 -1 -6 1888.71 33.28 0 -1 7 1637.18 30.09 0 -1 -7 1712.61 31.25 0 1 7 1590.40 28.21 0 -1 -7 1613.34 30.01 0 1 -7 1730.67 30.38 0 -1 7 1573.31 26.75 0 1 -7 1736.27 29.17 0 1 7 1661.87 29.98 0 -1 -7 1620.54 29.18 0 -1 -8 130.85 5.36 0 1 8 129.95 4.24 0 -1 -8 136.65 11.61 0 1 8 131.32 5.95 0 1 -8 126.12 6.11 0 -1 8 134.24 4.26 0 -1 8 133.64 3.30 0 1 8 145.49 4.93 0 1 -8 143.28 3.14 0 -1 -8 128.31 4.19 0 -1 -9 76.57 4.46 0 1 -9 88.87 3.99 0 -1 -9 93.25 4.99 0 1 -9 84.90 3.46 0 -1 9 85.66 6.88 0 -1 9 87.25 2.52 0 1 9 89.98 5.38 0 1 -9 95.02 2.47 0 -1 -9 90.02 4.74 0 -1 -10 146.86 11.12 0 1 -10 166.09 12.47 0 -1 -10 160.25 11.98 0 1 -10 159.37 13.02 0 -1 10 158.18 11.50 0 1 10 168.95 12.63 0 1 -10 166.18 11.77 0 -1 -11 255.28 15.84 0 1 -11 245.77 15.76 0 -1 -11 231.40 14.48 0 1 -11 237.04 15.54 0 -1 11 242.03 14.35 0 1 11 294.25 17.81 0 1 -11 269.42 15.94 0 -1 -12 407.90 18.87 0 1 -12 424.27 21.35 0 -1 -12 396.83 8.25 0 1 -12 417.27 19.12 0 -1 12 427.91 18.67 0 1 12 425.69 19.27 0 1 -12 442.71 19.53 0 -1 -13 428.40 23.97 0 1 -13 449.83 25.04 0 -1 -13 440.88 24.27 0 1 -13 449.43 24.23 0 1 13 448.30 26.75 0 1 -13 468.25 25.07 0 -1 -14 110.62 17.94 0 1 -14 103.78 12.32 0 -1 -14 103.90 10.34 0 1 -14 115.83 11.95 0 -1 14 109.35 10.46 0 1 14 112.34 11.75 0 1 -14 124.74 11.53 0 -1 -15 145.48 6.58 0 1 -15 160.55 12.99 0 -1 -15 149.83 12.01 0 1 -15 174.05 12.78 0 -1 15 157.41 11.64 0 1 15 181.40 13.90 0 1 -15 182.86 13.22 0 -1 -16 243.16 18.33 0 1 -16 243.04 18.42 0 -1 -16 241.66 17.91 0 1 -16 246.52 17.73 0 -1 16 246.92 18.09 0 1 16 249.01 19.11 0 1 -16 249.86 17.48 0 -1 -17 23.19 17.04 0 1 -17 19.07 11.82 0 -1 -17 24.06 14.42 0 1 -17 24.56 3.20 0 -1 17 25.00 2.52 0 1 17 30.33 13.21 0 -1 -18 253.03 18.02 0 1 -18 228.76 16.09 0 -1 -18 228.88 15.68 0 1 -18 258.17 16.24 0 -1 18 246.96 17.36 0 1 18 259.03 16.55 0 1 -18 260.13 16.06 0 -1 -19 289.00 18.55 0 1 -19 259.02 14.78 0 -1 -19 282.74 16.02 0 1 -19 272.12 14.80 0 -1 19 279.52 15.16 0 1 19 283.88 16.26 0 -1 -20 -0.47 6.03 0 1 -20 -2.89 4.83 0 -1 -20 0.35 3.85 0 1 -20 1.12 1.35 0 -1 20 0.89 1.03 0 1 20 1.19 2.39 0 -1 -21 24.29 14.71 0 1 -21 22.60 12.69 0 -1 -21 25.64 13.85 0 1 -21 19.17 7.28 0 -1 21 24.33 4.34 0 1 21 18.60 10.99 0 -1 -22 3.79 5.69 0 1 -22 4.66 5.61 0 -1 -22 1.90 4.23 0 1 -22 -1.33 2.90 0 -1 22 3.03 2.18 0 1 22 2.57 2.24 0 -1 -23 145.68 12.25 0 1 -23 161.11 14.11 0 -1 -23 145.81 11.17 0 1 -23 151.88 9.98 0 1 23 161.07 11.02 0 -1 -24 68.19 8.88 0 1 -24 50.37 28.76 0 -1 -24 64.06 7.96 0 1 -24 60.19 6.27 0 1 24 78.30 6.91 0 -1 -25 144.22 12.77 0 1 -25 177.69 12.69 0 -1 -25 157.92 13.38 0 1 -25 163.37 9.69 0 -1 -26 76.19 27.94 0 1 -26 81.92 8.14 0 -1 -26 80.18 7.03 0 1 -26 93.16 11.82 0 -1 -27 54.77 30.42 0 1 -27 59.08 8.33 0 -1 -27 50.07 6.83 0 1 -27 51.55 6.87 0 -1 -28 12.05 7.75 0 1 -28 13.31 10.77 0 -1 -28 14.28 9.45 0 1 -28 12.87 7.91 0 -1 -29 16.12 7.19 0 1 -29 7.54 6.81 0 -1 -29 5.53 4.14 0 1 -29 5.25 4.73 0 1 -30 36.81 23.09 0 -1 -30 31.20 17.74 0 -1 -30 40.46 14.75 0 -1 -31 33.44 21.85 0 1 -31 25.21 17.79 0 -2 0 117.94 4.25 0 2 0 130.62 4.99 0 -2 0 142.78 6.04 0 2 0 134.35 4.97 0 2 0 136.59 4.08 0 -2 0 136.47 4.09 0 -2 1 806.06 27.61 0 2 -1 701.45 24.51 0 -2 -1 816.96 27.66 0 2 1 753.88 25.76 0 -2 1 657.95 23.12 0 2 -1 736.96 25.65 0 -2 -1 729.44 25.67 0 2 1 741.48 26.49 0 2 -1 724.73 24.29 0 2 1 770.78 26.14 0 -2 1 723.92 24.17 0 -2 -1 782.95 26.31 0 -2 2 94.99 10.62 0 2 -2 89.65 4.69 0 -2 -2 86.91 4.01 0 2 2 86.51 3.65 0 -2 2 91.96 8.20 0 2 -2 92.87 4.60 0 -2 -2 78.40 4.32 0 2 2 92.39 4.65 0 2 -2 89.50 3.40 0 2 2 85.29 4.26 0 2 -2 86.42 3.19 0 -2 -2 74.93 3.04 0 -2 3 8788.70 721.00 0 2 -3 8316.39 682.33 0 -2 -3 7982.69 654.84 0 -2 3 7671.87 629.62 0 2 -3 8037.83 659.49 0 -2 -3 7744.42 635.61 0 2 3 8173.86 670.70 0 2 3 8521.96 699.01 0 2 -4 545.53 19.79 0 -2 -4 514.26 19.27 0 2 4 529.01 18.75 0 2 -4 489.24 17.72 0 -2 -4 473.96 17.97 0 2 4 495.12 18.18 0 2 -4 534.25 20.58 0 2 -4 482.28 16.47 0 -2 -4 488.28 17.54 0 2 -4 481.15 16.44 0 -2 5 8423.75 691.16 0 2 -5 6438.14 109.57 0 -2 -5 7251.40 595.18 0 2 5 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0 -5 -26 6.03 4.36 0 5 26 1.30 4.57 0 -5 -27 39.30 41.51 0 5 -27 49.28 21.10 0 -5 -27 20.24 29.23 0 5 27 44.94 33.05 0 -6 0 114.79 13.13 0 -6 0 94.55 13.10 0 6 0 114.40 10.31 0 -6 1 55.51 5.88 0 -6 -1 65.02 5.82 0 -6 -1 63.76 10.06 0 -6 1 58.79 26.63 0 6 -1 71.93 6.61 0 6 1 69.16 6.75 0 -6 2 8.84 9.79 0 -6 -2 13.01 6.12 0 -6 2 11.13 7.71 0 -6 -2 15.52 10.11 0 6 2 8.85 8.40 0 6 -2 10.22 10.84 0 -6 3 232.63 16.57 0 -6 -3 211.28 15.59 0 -6 3 214.70 16.17 0 -6 -3 215.24 17.04 0 6 3 228.08 16.85 0 6 -3 241.31 18.82 0 -6 4 25.74 4.64 0 -6 -4 25.27 4.27 0 -6 4 29.10 11.88 0 -6 -4 26.02 10.49 0 6 4 20.23 10.52 0 6 -4 23.03 12.61 0 -6 5 141.32 16.81 0 -6 -5 135.86 10.91 0 -6 5 134.43 12.28 0 -6 -5 141.95 26.16 0 6 5 137.46 12.05 0 6 -5 156.24 11.13 0 -6 6 137.84 11.08 0 -6 -6 143.64 14.00 0 -6 -6 127.44 14.93 0 6 -6 129.86 12.20 0 6 6 132.56 11.98 0 6 -6 132.56 10.71 0 -6 7 408.55 24.23 0 -6 -7 450.33 28.57 0 6 -7 425.35 28.11 0 6 7 417.28 22.20 0 6 -7 437.68 20.80 0 -6 8 537.26 28.90 0 -6 -8 483.59 29.02 0 6 -8 492.35 29.49 0 6 -8 507.24 23.64 0 6 8 496.06 26.69 0 -6 9 246.24 16.40 0 -6 -9 278.25 19.47 0 6 -9 262.72 18.17 0 6 -9 275.24 13.85 0 6 9 243.37 14.68 0 -6 10 4.87 5.99 0 -6 -10 10.12 6.40 0 -6 -10 4.81 7.80 0 6 -10 10.96 5.66 0 6 -10 6.56 3.75 0 6 10 3.56 4.06 0 -6 11 179.05 24.20 0 -6 -11 189.24 16.14 0 -6 -11 210.81 18.98 0 6 -11 206.19 15.08 0 6 11 185.59 13.29 0 6 -11 190.58 10.74 0 -6 12 21.83 10.85 0 -6 -12 23.63 12.43 0 -6 -12 28.93 12.96 0 6 -12 21.81 5.02 0 6 -12 21.35 4.38 0 6 12 18.00 10.55 0 -6 13 8.44 7.13 0 -6 -13 10.55 6.24 0 -6 -13 9.61 4.65 0 6 -13 13.50 8.11 0 6 13 10.68 7.71 0 -6 14 90.24 9.02 0 -6 -14 90.51 10.33 0 -6 -14 79.21 25.64 0 6 -14 89.18 10.45 0 6 14 71.28 7.35 0 -6 15 10.76 9.32 0 -6 -15 14.89 7.88 0 -6 -15 7.85 8.57 0 6 -15 5.72 5.93 0 6 15 13.69 8.26 0 -6 16 2.70 4.08 0 -6 -16 1.02 3.32 0 6 -16 1.22 4.37 0 6 16 3.86 5.47 0 -6 17 37.63 19.78 0 -6 -17 25.38 18.56 0 -6 -17 29.45 12.12 0 6 -17 30.21 15.11 0 6 17 27.91 16.68 0 -6 18 3.74 5.18 0 -6 -18 1.74 4.68 0 -6 -18 9.13 6.52 0 6 -18 4.94 3.90 0 6 18 3.60 7.72 0 -6 -19 6.59 5.73 0 6 -19 9.32 4.80 0 -6 -19 -2.20 6.05 0 6 -19 7.50 5.58 0 6 19 3.49 4.10 0 -6 -20 3.60 5.95 0 6 -20 1.84 4.33 0 -6 -20 2.72 5.14 0 6 -20 3.42 3.62 0 6 20 4.58 4.65 0 -6 -21 3.51 5.41 0 6 -21 -1.01 5.61 0 -6 -21 6.38 9.60 0 6 -21 4.71 3.22 0 6 21 3.06 3.41 0 -6 -22 12.32 8.43 0 6 -22 1.52 3.51 0 -6 -22 3.80 7.21 0 6 -22 5.09 3.09 0 6 22 4.15 5.98 0 -6 -23 22.24 17.32 0 6 -23 18.74 13.52 0 -6 -23 24.18 15.19 0 6 -23 25.13 12.20 0 6 23 22.99 13.83 0 -6 -24 22.79 19.80 0 6 -24 23.59 12.78 0 -6 -24 25.53 18.80 0 6 24 12.34 19.20 0 -6 -25 0.68 4.13 0 6 -25 3.08 5.20 0 -6 -25 0.92 4.38 0 6 25 4.46 6.53 0 -7 0 1.86 5.25 0 -7 0 9.06 11.61 0 7 0 1.27 2.15 0 -7 1 9.87 7.20 0 -7 -1 14.06 4.01 0 -7 1 10.28 16.37 0 -7 -1 14.27 8.41 0 7 -1 10.32 5.01 0 7 1 11.20 4.88 0 -7 2 26.08 17.16 0 -7 -2 20.10 4.35 0 -7 2 21.98 19.27 0 -7 -2 35.43 15.77 0 7 2 11.64 7.35 0 7 -2 26.74 15.15 0 -7 3 110.15 9.44 0 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0 -7 12 283.17 20.44 0 -7 -12 254.14 18.93 0 -7 -12 260.08 19.94 0 7 -12 250.02 28.91 0 7 12 241.11 15.48 0 -7 13 2.39 6.15 0 -7 -13 11.75 6.84 0 -7 -13 8.62 8.74 0 7 -13 4.19 6.28 0 7 13 2.17 5.27 0 -7 14 94.86 13.04 0 -7 -14 108.65 11.27 0 -7 -14 96.42 13.54 0 7 -14 92.27 13.12 0 7 14 84.18 9.35 0 -7 15 7.69 11.56 0 -7 -15 18.52 12.76 0 -7 -15 7.87 6.22 0 7 -15 6.72 5.41 0 7 15 9.72 11.17 0 -7 16 43.36 18.08 0 -7 -16 36.31 22.70 0 -7 -16 36.70 23.67 0 7 -16 31.18 17.33 0 7 16 33.84 19.85 0 -7 17 5.09 5.65 0 -7 -17 2.76 3.75 0 -7 -17 6.74 6.03 0 7 -17 4.77 3.79 0 7 17 -2.31 6.11 0 -7 18 31.19 18.79 0 -7 -18 22.55 11.84 0 -7 -18 15.63 13.97 0 7 -18 21.92 10.27 0 7 18 22.66 13.94 0 -7 -19 1.37 4.42 0 -7 -19 4.72 4.50 0 7 -19 4.30 3.57 0 7 19 2.61 2.59 0 -7 -20 29.52 27.63 0 7 -20 30.55 19.08 0 -7 -20 29.94 21.86 0 7 -20 25.50 7.60 0 7 20 26.38 23.36 0 -7 -21 4.86 9.26 0 7 -21 3.21 5.55 0 -7 -21 2.09 4.99 0 7 -21 3.84 3.02 0 7 21 6.37 7.04 0 -7 -22 16.45 17.57 0 7 -22 12.80 6.48 0 -7 -22 16.52 13.27 0 7 -22 14.02 9.14 0 7 22 13.18 12.87 0 -7 -23 2.80 7.19 0 7 -23 3.23 4.21 0 -7 -23 4.76 7.14 0 7 23 6.32 6.11 0 -8 0 216.96 25.66 0 -8 0 252.52 23.47 0 8 0 223.48 17.80 0 -8 1 91.48 9.63 0 -8 1 77.79 10.80 0 -8 -1 99.92 11.01 0 8 -1 71.79 9.32 0 8 1 72.83 8.79 0 -8 2 83.27 9.83 0 -8 2 73.45 35.65 0 -8 -2 91.18 10.33 0 8 -2 81.03 7.45 0 8 2 89.06 8.37 0 -8 3 6.60 6.28 0 -8 -3 4.63 5.69 0 -8 3 9.70 7.28 0 8 3 4.55 5.91 0 8 -3 1.60 6.25 0 -8 4 22.27 14.72 0 -8 -4 19.40 6.74 0 -8 4 16.60 10.29 0 -8 -4 21.17 15.28 0 8 -4 15.80 4.91 0 8 4 15.17 11.31 0 -8 5 22.97 9.98 0 -8 -5 25.80 15.44 0 -8 -5 19.17 13.77 0 8 5 27.89 10.61 0 8 -5 25.12 12.73 0 -8 6 5.31 7.86 0 -8 -6 7.48 6.56 0 -8 -6 6.83 6.15 0 8 -6 10.11 8.87 0 8 6 5.58 3.68 0 8 -6 4.34 3.72 0 -8 7 30.46 17.09 0 -8 -7 24.31 13.39 0 -8 -7 38.63 11.63 0 8 -7 23.63 13.77 0 8 -7 30.64 6.52 0 8 7 26.95 12.74 0 -8 8 94.69 14.57 0 -8 -8 80.16 9.18 0 -8 -8 80.13 36.24 0 8 -8 72.45 25.66 0 8 -8 71.47 11.35 0 8 8 73.47 8.07 0 -8 9 86.58 20.89 0 -8 -9 85.91 11.79 0 8 -9 80.83 9.57 0 8 -9 81.95 5.89 0 8 9 81.63 8.50 0 -8 10 4.36 6.53 0 -8 -10 11.63 8.70 0 -8 -10 5.02 7.94 0 8 -10 6.94 4.12 0 8 10 10.03 10.87 0 -8 11 4.77 3.74 0 -8 -11 2.47 5.81 0 -8 -11 1.76 4.78 0 8 -11 3.17 4.43 0 8 11 2.69 3.42 0 -8 12 5.88 7.11 0 -8 -12 7.89 6.76 0 8 -12 7.63 7.39 0 8 12 11.38 5.38 0 -8 13 16.29 13.26 0 -8 -13 21.61 7.13 0 -8 -13 16.51 10.90 0 8 -13 15.86 7.39 0 8 13 10.68 8.34 0 -8 14 31.59 15.06 0 -8 -14 28.26 26.87 0 -8 -14 40.03 19.70 0 8 -14 32.00 13.36 0 8 14 31.89 13.29 0 -8 15 82.36 9.75 0 -8 -15 70.83 15.10 0 -8 -15 68.94 12.90 0 8 -15 80.77 10.36 0 8 15 64.99 29.50 0 -8 16 20.90 11.13 0 -8 -16 30.33 8.67 0 -8 -16 16.14 13.45 0 8 -16 15.05 10.09 0 8 16 16.67 9.99 0 -8 17 44.63 30.31 0 -8 -17 53.14 7.79 0 -8 -17 52.69 25.66 0 8 -17 35.51 18.55 0 8 17 34.57 23.32 0 -8 18 2.21 2.71 0 -8 -18 3.07 8.20 0 8 -18 6.76 5.49 0 8 18 2.63 3.56 0 -8 19 6.86 3.76 0 -8 -19 13.23 10.30 0 8 -19 3.28 5.86 0 8 19 6.53 5.30 0 8 -20 4.62 4.90 0 -8 -20 2.13 7.06 0 8 -20 3.52 2.67 0 8 20 -4.17 5.95 0 8 -21 2.57 3.26 0 -8 -21 4.20 3.77 0 8 -21 5.18 5.77 0 8 21 6.02 4.41 0 -9 0 0.09 2.81 0 -9 0 3.91 5.37 0 9 0 -0.01 4.39 0 -9 1 2.69 4.22 0 -9 -1 3.71 4.22 0 9 1 8.99 4.60 0 9 -1 4.72 3.87 0 -9 2 8.71 7.20 0 -9 -2 7.35 4.65 0 -9 2 6.73 6.01 0 -9 -2 3.18 4.77 0 9 2 3.51 5.15 0 9 -2 2.62 3.12 0 -9 3 26.79 6.92 0 -9 3 13.99 8.62 0 -9 -3 19.13 12.70 0 9 3 31.18 12.68 0 9 -3 19.53 10.32 0 -9 4 1.31 3.20 0 -9 -4 5.77 5.95 0 9 -4 -1.37 4.00 0 9 4 -0.38 6.17 0 -9 5 31.84 18.06 0 -9 -5 33.34 23.15 0 9 -5 27.28 17.50 0 9 -5 23.53 10.54 0 9 5 31.97 15.57 0 -9 6 2.32 4.72 0 -9 -6 1.68 4.27 0 9 -6 4.44 6.78 0 9 -6 2.25 3.06 0 9 6 -1.56 5.54 0 -9 7 8.77 8.35 0 -9 -7 10.66 6.30 0 -9 -7 10.14 9.49 0 9 -7 5.32 4.98 0 9 -7 3.13 2.83 0 9 7 4.20 3.66 0 -9 8 12.82 6.43 0 -9 -8 9.43 6.26 0 -9 -8 6.80 11.61 0 9 -8 11.46 9.68 0 9 8 6.40 4.40 0 -9 9 63.69 6.66 0 -9 -9 61.98 7.73 0 -9 -9 63.80 25.80 0 9 -9 43.79 26.80 0 9 9 54.81 32.72 0 -9 10 1.32 3.96 0 -9 -10 0.56 4.13 0 9 -10 1.41 2.26 0 9 10 -0.86 6.86 0 -9 11 44.77 26.91 0 -9 -11 51.19 12.44 0 9 -11 47.93 18.27 0 9 11 43.53 26.32 0 -9 12 4.11 4.35 0 -9 -12 8.38 9.35 0 9 -12 4.10 7.88 0 9 12 10.19 11.09 0 -9 13 23.53 15.02 0 -9 -13 22.09 17.27 0 9 -13 22.11 13.58 0 9 13 28.25 11.73 0 -9 14 18.06 6.02 0 -9 -14 11.30 6.94 0 9 -14 5.15 5.82 0 9 14 13.13 8.16 0 -9 15 21.37 11.03 0 -9 -15 16.90 11.14 0 9 -15 14.83 11.18 0 9 15 15.43 16.07 0 -9 16 2.36 6.30 0 -9 -16 -4.22 7.01 0 9 -16 1.25 3.65 0 9 16 -1.31 5.36 0 -9 17 29.33 20.79 0 -9 -17 36.59 16.61 0 9 -17 18.49 15.12 0 9 17 24.08 15.26 0 -10 0 49.21 8.38 0 -10 0 41.46 37.00 0 10 0 33.01 16.23 0 -10 1 24.69 11.30 0 -10 -1 15.18 11.42 0 -10 1 10.81 12.97 0 -10 -1 17.20 14.75 0 10 1 15.39 11.84 0 10 -1 9.28 8.02 0 -10 2 20.20 17.57 0 -10 2 9.36 12.07 0 -10 -2 2.87 10.92 0 10 2 13.90 9.79 0 10 -2 13.87 8.92 0 -10 3 11.34 5.08 0 -10 -3 11.61 9.79 0 10 -3 6.29 4.30 0 10 3 1.61 5.30 0 -10 4 27.57 17.31 0 -10 -4 25.00 19.00 0 10 -4 27.07 26.16 0 10 -4 20.46 16.41 0 10 4 26.23 14.66 0 -10 5 4.83 5.91 0 -10 -5 6.10 7.50 0 10 -5 3.64 6.00 0 10 -5 7.58 4.50 0 10 5 3.62 2.86 0 -10 6 55.92 9.06 0 -10 -6 46.85 25.14 0 10 -6 28.90 23.97 0 10 6 36.45 18.22 0 -10 7 8.47 10.59 0 -10 -7 17.95 22.97 0 10 -7 8.28 7.76 0 10 7 8.18 9.96 0 -10 8 54.87 7.91 0 -10 -8 36.24 27.70 0 10 -8 35.05 25.70 0 10 8 45.60 24.54 0 -10 9 -0.21 4.44 0 -10 -9 5.97 10.12 0 10 -9 15.03 7.57 0 10 9 -0.50 5.35 0 -10 10 37.76 29.22 0 -10 -10 40.99 30.63 0 10 -10 25.84 20.47 0 10 10 31.68 24.34 0 -10 11 9.36 7.82 0 -10 -11 11.09 15.28 0 10 -11 8.87 3.69 0 10 11 8.82 6.44 0 -10 12 2.65 5.90 0 -10 -12 4.27 10.31 0 10 -12 1.81 4.66 0 10 12 5.99 7.06 1 0 -31 4.50 5.71 1 0 -31 -0.11 3.83 1 0 -30 4.06 3.80 1 0 -30 7.35 8.26 1 0 -29 26.33 17.32 1 0 -29 27.35 12.90 1 0 -28 5.02 9.89 1 0 -28 8.66 5.64 1 0 -27 182.98 15.53 1 0 -27 166.86 13.27 1 0 -26 21.64 9.12 1 0 -26 20.37 7.24 1 0 -25 2.56 3.30 1 0 -25 4.50 4.77 1 0 -24 27.59 13.14 1 0 -24 25.27 18.84 1 0 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125.33 20.04 -5 6 2 123.31 8.54 5 -6 -2 127.96 12.52 5 6 -2 148.97 14.81 5 6 -2 134.99 11.41 -5 6 2 132.13 12.14 -5 -6 1 32.51 23.93 -5 6 1 40.98 7.53 5 -6 -1 60.13 8.02 5 6 -1 41.20 15.27 -5 -6 0 260.80 19.32 -5 6 0 228.17 10.86 5 -6 0 263.60 15.87 5 -6 0 250.20 17.56 5 6 0 269.09 15.79 -5 -6 -1 46.24 32.18 -5 6 -1 26.06 2.91 -5 -6 -1 37.27 19.24 5 -6 1 41.03 14.25 5 -6 1 28.08 12.21 5 6 1 30.41 13.35 -5 -6 -2 67.12 11.43 -5 6 -2 65.58 6.82 5 -6 2 67.32 8.68 5 -6 2 64.51 6.32 5 6 2 57.02 6.07 -5 -6 -3 256.73 21.85 -5 6 -3 228.36 15.60 -5 -6 -3 230.00 23.43 5 -6 3 222.16 17.14 5 -6 3 245.80 17.94 5 6 3 238.86 18.76 -5 6 -4 290.76 18.71 -5 -6 -4 311.55 23.72 5 -6 4 291.33 20.25 5 -6 4 306.93 21.95 5 6 4 279.51 20.20 -5 -6 -5 3.72 12.09 -5 6 -5 16.00 10.35 5 -6 5 20.37 10.52 -5 -6 -5 30.59 16.01 5 -6 5 6.39 5.17 5 6 5 16.68 15.70 -5 -6 -6 77.03 12.37 -5 6 -6 67.72 5.21 5 -6 6 62.37 9.59 -5 -6 -6 61.08 36.75 5 -6 6 68.97 6.34 5 6 6 73.66 26.60 -5 -6 -7 70.10 10.17 -5 6 -7 78.15 5.60 -5 -6 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9.42 10.34 5 6 17 4.22 6.98 -5 -6 -18 9.60 8.10 -5 6 -18 6.72 7.69 -5 -6 -18 15.99 8.78 5 6 18 6.08 5.56 -5 -6 -19 3.10 4.34 -5 6 -19 3.09 3.67 -5 -6 -19 0.83 6.31 5 6 19 3.97 7.04 -5 -6 -20 1.72 4.24 -5 6 -20 3.21 3.86 -5 -6 -20 2.11 5.84 5 6 20 2.38 5.58 -5 -6 -21 1.60 5.57 -5 6 -21 9.24 9.73 -5 -6 -21 7.60 7.09 5 6 21 5.41 5.20 -5 -6 -22 12.28 16.07 -5 6 -22 6.14 5.85 -5 -6 -22 5.97 6.49 5 6 22 5.03 5.70 -5 -7 24 5.87 3.72 5 -7 -24 5.85 8.04 5 7 -24 4.80 6.90 -5 7 24 4.17 6.71 -5 -7 23 32.13 14.25 5 -7 -23 49.79 20.64 5 7 -23 35.24 18.23 -5 7 23 27.68 20.52 -5 -7 22 7.86 7.61 5 -7 -22 8.88 11.38 5 7 -22 4.71 3.50 -5 7 22 4.41 6.34 -5 -7 21 9.26 6.44 5 -7 -21 11.44 13.12 5 7 -21 10.12 5.63 -5 7 21 10.76 7.52 -5 -7 20 6.39 7.04 5 -7 -20 16.19 17.09 5 7 -20 4.52 2.67 -5 7 20 7.68 7.67 -5 -7 19 31.01 19.54 5 -7 -19 11.00 12.68 5 7 -19 30.38 10.71 -5 7 19 29.06 16.39 -5 -7 18 14.45 11.30 5 -7 -18 15.63 14.94 5 7 -18 23.36 14.67 -5 7 18 16.32 14.90 -5 -7 17 38.95 19.50 5 -7 -17 32.94 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15.49 5 7 -5 41.13 5.01 -5 7 5 25.97 18.29 5 -7 -4 9.73 6.33 5 7 -4 14.21 9.33 5 7 -4 5.55 3.81 -5 7 4 2.80 3.92 5 -7 -3 262.81 23.04 5 7 -3 268.56 23.89 5 7 -3 302.22 23.73 -5 7 3 266.10 21.82 -5 -7 2 5.52 7.53 5 -7 -2 11.42 15.38 5 7 -2 7.19 11.77 5 7 -2 10.19 5.27 -5 7 2 7.92 8.91 -5 -7 1 209.92 20.81 5 -7 -1 229.22 24.52 5 7 -1 185.32 17.50 5 7 -1 193.32 17.50 -5 7 1 182.33 18.08 -5 -7 0 42.55 33.25 -5 7 0 41.60 3.28 -5 -7 0 50.27 23.22 5 -7 0 54.67 10.86 5 7 0 44.48 19.99 -5 7 0 43.68 13.22 -5 -7 -1 56.01 35.98 -5 7 -1 67.15 3.81 -5 -7 -1 85.20 11.94 5 -7 1 62.71 11.16 5 7 1 54.28 6.44 -5 7 -1 77.63 9.51 -5 -7 -2 32.79 26.74 -5 7 -2 17.86 10.77 -5 -7 -2 29.73 14.38 5 -7 2 29.10 15.57 5 7 2 33.41 10.53 -5 7 -2 25.24 10.13 -5 7 -3 12.90 8.15 -5 -7 -3 22.50 12.57 5 -7 3 32.81 22.64 5 7 3 12.44 4.86 -5 7 -3 13.52 9.11 -5 7 -4 92.04 7.03 5 -7 4 103.95 18.51 -5 -7 -4 96.15 12.19 5 7 4 115.14 12.28 -5 7 -4 98.78 7.67 -5 7 -5 172.11 11.34 -5 -7 -5 206.15 40.59 5 -7 5 190.35 24.88 5 7 5 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18.32 5.98 -7 -5 3 7.80 6.51 7 -5 -3 0.38 5.08 7 5 -3 5.63 6.71 7 -5 -3 4.40 7.71 7 5 -3 3.79 3.59 -7 -5 2 15.27 7.59 -7 5 2 9.36 3.02 7 -5 -2 12.01 5.65 7 5 -2 13.54 8.86 7 -5 -2 11.11 7.59 7 5 -2 14.03 5.41 -7 -5 1 7.58 6.11 -7 5 1 1.98 2.45 7 -5 -1 4.34 3.36 7 5 -1 6.58 7.43 7 -5 -1 3.25 6.78 7 5 -1 5.50 4.03 -7 -5 0 175.55 17.06 -7 5 0 194.42 13.45 7 -5 0 185.40 15.46 7 5 0 191.94 18.60 7 -5 0 225.71 17.10 7 5 0 199.33 17.98 -7 -5 -1 151.44 16.31 -7 5 -1 115.91 7.98 7 -5 1 148.39 13.33 7 5 1 147.14 15.95 7 -5 1 138.17 14.77 7 5 1 119.86 11.70 -7 5 -2 115.43 4.50 7 -5 2 114.49 7.86 7 5 2 111.12 9.69 7 -5 2 111.03 8.80 7 5 2 101.30 9.56 -7 5 -3 53.24 6.44 7 -5 3 51.54 15.67 7 -5 3 56.27 7.82 7 5 3 46.26 19.09 -7 5 -4 56.49 5.00 -7 -5 -4 61.67 10.37 7 -5 4 51.99 10.12 7 -5 4 53.26 6.00 7 5 4 46.33 19.32 -7 5 -5 67.05 5.30 7 -5 5 72.10 6.56 -7 -5 -5 60.88 8.69 7 -5 5 73.19 23.52 7 5 5 66.61 29.03 -7 5 -6 5.29 4.39 -7 -5 -6 8.03 5.19 7 -5 6 4.24 7.20 7 5 6 7.37 7.43 -7 -5 -7 51.18 14.15 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85.25 9.03 7 6 -5 110.63 39.39 7 -6 -5 118.26 13.03 7 6 -5 94.29 7.59 -7 -6 4 265.51 22.70 7 -6 -4 232.45 18.78 7 6 -4 289.57 21.99 7 -6 -4 236.87 19.49 7 6 -4 242.75 24.14 -7 -6 3 510.74 34.27 7 -6 -3 512.92 39.48 7 6 -3 511.18 32.50 7 -6 -3 524.49 34.34 7 6 -3 474.58 28.55 -7 -6 2 295.42 29.11 7 -6 -2 286.25 21.58 7 -6 -2 290.30 20.79 7 6 -2 283.24 19.13 -7 -6 1 92.36 14.45 7 -6 -1 92.11 10.49 7 -6 -1 91.31 9.36 7 6 -1 97.01 9.12 -7 -6 0 65.25 27.38 7 -6 0 49.12 18.23 7 6 0 51.02 20.34 7 -6 0 52.59 26.94 7 6 0 68.13 23.29 -7 -6 -1 129.29 31.48 7 -6 1 106.38 11.40 7 6 1 138.73 12.94 7 6 1 119.01 9.03 7 -6 2 36.46 13.92 7 6 2 29.81 13.67 7 -6 2 25.19 14.40 7 6 2 35.22 15.04 7 -6 3 144.47 9.43 7 -6 3 156.23 10.83 7 6 3 125.23 8.67 -7 6 -4 14.70 8.08 -7 -6 -4 14.95 8.23 7 -6 4 25.97 14.40 7 -6 4 11.02 11.08 7 6 4 20.35 8.92 -7 -6 -5 20.16 10.41 -7 6 -5 9.12 3.58 7 -6 5 10.39 9.91 -7 -6 -5 5.83 5.63 7 -6 5 10.18 9.82 7 6 5 11.65 4.66 -7 6 -6 50.07 5.08 -7 -6 -6 54.73 27.90 7 -6 6 40.21 21.68 7 -6 6 39.55 19.93 7 6 6 44.90 17.59 -7 -6 -7 34.15 11.33 -7 6 -7 14.45 7.50 -7 -6 -7 24.93 17.75 -7 6 -7 17.89 8.52 7 -6 7 30.58 13.77 7 6 7 19.87 12.57 -7 -6 -8 82.81 17.03 -7 6 -8 57.44 15.60 -7 -6 -8 57.52 20.14 7 -6 8 60.77 7.32 7 6 8 67.35 7.91 -7 -6 -9 1.96 7.47 -7 6 -9 3.78 3.56 -7 -6 -9 12.55 9.65 7 -6 9 9.17 6.35 7 6 9 2.52 1.75 -7 -6 -10 11.18 9.09 -7 6 -10 6.48 4.18 -7 -6 -10 10.83 8.98 7 -6 10 2.36 3.18 7 6 10 9.64 6.41 -7 -6 -11 11.54 16.65 -7 6 -11 16.03 12.59 -7 -6 -11 22.39 14.43 7 -6 11 33.05 11.40 7 6 11 18.32 12.57 -7 6 -12 2.34 3.43 -7 -6 -12 3.76 3.13 7 -6 12 2.97 3.68 7 6 12 1.71 3.86 -7 -6 -13 2.69 6.85 -7 6 -13 1.61 2.40 -7 -6 -13 4.17 3.62 7 -6 13 8.20 5.13 7 6 13 4.77 3.87 -7 -6 -14 16.31 16.98 -7 6 -14 3.87 4.05 -7 -6 -14 13.36 7.13 7 -6 14 11.49 6.11 7 6 14 4.39 4.00 -7 -6 -15 3.80 5.60 -7 6 -15 3.92 4.23 -7 -6 -15 3.52 7.21 7 6 15 6.57 4.90 -7 -6 -16 20.23 17.24 -7 6 -16 27.74 20.54 -7 -6 -16 30.94 23.41 7 6 16 26.92 11.76 -7 -6 -17 6.59 7.75 -7 6 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43.70 29.50 -7 -7 13 51.94 32.92 7 -7 -13 35.53 28.47 7 7 -13 59.60 19.77 -7 7 13 32.67 18.77 -7 -7 12 2.41 8.45 7 -7 -12 3.58 10.51 7 7 -12 1.73 3.80 -7 7 12 3.67 3.25 -7 -7 11 40.73 13.55 7 -7 -11 33.56 16.77 7 7 -11 30.68 18.55 7 7 -11 41.83 10.37 -7 7 11 31.71 17.06 7 -7 -10 95.51 11.63 7 7 -10 63.67 32.33 7 7 -10 90.17 7.31 -7 7 10 82.87 10.88 7 -7 -9 16.81 14.57 7 7 -9 23.14 14.69 7 7 -9 20.13 12.83 -7 7 9 24.71 17.79 7 -7 -8 157.51 15.89 7 7 -8 175.84 15.41 7 7 -8 156.12 17.56 -7 7 8 159.95 13.07 -7 -7 7 5.97 7.34 7 -7 -7 16.81 8.40 7 7 -7 17.86 7.83 7 7 -7 18.19 9.28 -7 7 7 15.38 8.24 7 -7 -6 11.23 16.61 7 7 -6 22.34 7.92 7 7 -6 20.41 7.97 -7 7 6 18.46 11.81 7 -7 -5 10.11 10.47 7 7 -5 14.97 8.75 7 7 -5 18.18 8.58 -7 7 5 11.92 9.31 -7 -7 4 22.87 11.27 7 -7 -4 30.59 20.44 7 7 -4 19.29 8.98 7 7 -4 15.31 4.27 -7 7 4 16.74 7.13 7 -7 -3 165.99 14.76 7 7 -3 157.60 16.38 7 7 -3 156.05 15.89 -7 7 3 151.66 13.56 -7 -7 2 17.59 10.12 7 -7 -2 9.78 4.21 7 7 -2 5.87 3.59 -7 -7 1 40.96 14.36 7 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265.94 21.68 8 -4 -4 238.80 18.42 8 4 -4 213.50 17.62 8 -4 -4 252.66 18.95 8 4 -4 226.68 8.72 -8 4 3 100.53 7.37 -8 -4 3 144.09 16.06 8 -4 -3 136.89 25.24 8 4 -3 117.37 12.11 8 -4 -3 128.46 9.70 8 4 -3 125.71 13.70 -8 4 2 8.06 3.12 -8 -4 2 36.26 9.48 -8 4 2 7.44 4.26 8 -4 -2 24.16 8.95 8 4 -2 39.29 20.06 8 -4 -2 34.30 9.51 -8 4 1 166.23 10.26 -8 -4 1 214.25 19.35 -8 4 1 169.96 11.00 8 -4 -1 168.75 14.98 8 4 -1 201.29 16.04 -8 -4 0 179.69 17.91 -8 4 0 213.98 11.42 8 -4 0 188.84 19.90 8 -4 0 171.77 36.13 8 4 0 193.60 15.86 -8 4 -1 71.66 8.28 8 -4 1 83.87 6.98 8 4 1 64.52 7.90 -8 -4 -2 168.17 24.49 -8 4 -2 192.32 14.82 8 -4 2 140.34 12.50 8 4 2 207.21 17.18 8 -4 2 178.44 19.51 8 4 2 170.97 14.55 -8 4 -3 260.34 20.99 8 -4 3 281.37 15.42 8 -4 3 275.85 21.74 8 4 3 258.83 16.06 -8 -4 -4 135.54 23.05 -8 4 -4 132.71 10.92 8 -4 4 118.76 10.18 8 -4 4 152.88 14.73 8 4 4 119.89 11.87 -8 -4 -5 452.03 32.10 -8 4 -5 452.79 28.89 8 -4 5 396.75 23.49 8 4 5 430.62 28.00 -8 -4 -6 18.09 6.63 -8 4 -6 13.41 10.54 8 -4 6 9.11 8.18 8 4 6 3.94 5.76 -8 -4 -7 5.55 5.82 -8 4 -7 4.92 5.77 8 -4 7 4.25 6.73 8 4 7 8.43 5.96 -8 -4 -8 41.19 23.70 -8 4 -8 18.77 15.81 -8 -4 -8 25.32 20.98 8 -4 8 41.36 8.09 8 4 8 41.77 8.07 -8 4 -9 97.35 6.69 -8 -4 -9 105.02 8.54 8 -4 9 105.85 12.35 8 4 9 98.96 15.08 -8 -4 -10 35.26 19.45 -8 4 -10 36.02 21.21 -8 -4 -10 51.46 7.30 8 -4 10 48.01 8.20 8 4 10 40.26 15.35 -8 -4 -11 4.10 6.74 -8 4 -11 6.58 7.68 -8 -4 -11 8.92 7.50 8 -4 11 7.82 6.82 8 4 11 9.57 8.12 -8 -4 -12 33.72 37.86 -8 4 -12 54.31 24.65 -8 -4 -12 50.00 12.21 8 -4 12 65.39 6.66 8 4 12 60.09 9.50 -8 -4 -13 38.71 39.41 -8 4 -13 46.14 8.79 -8 -4 -13 42.86 8.54 8 -4 13 47.15 6.06 8 4 13 36.31 19.12 -8 -4 -14 -2.29 8.94 -8 4 -14 -0.63 4.33 -8 -4 -14 5.46 3.40 8 -4 14 0.73 2.51 8 4 14 2.30 4.10 -8 -4 -15 41.98 29.88 -8 4 -15 51.09 20.94 -8 -4 -15 47.66 11.01 8 -4 15 51.59 25.02 8 4 15 41.38 26.51 -8 -4 -16 21.84 17.03 -8 4 -16 23.65 11.74 8 -4 16 23.68 12.32 8 4 16 15.19 10.03 -8 -4 -17 27.80 16.70 -8 4 -17 41.63 23.25 8 -4 17 47.05 7.05 8 4 17 44.67 20.78 -8 -4 -18 2.81 10.71 -8 4 -18 5.98 4.21 8 4 18 12.08 7.37 -8 -4 -19 5.33 5.62 -8 4 -19 5.94 5.42 8 4 19 1.27 3.73 -8 -4 -20 13.81 12.47 -8 4 -20 18.88 6.47 8 4 20 15.57 9.44 -8 -4 -21 19.10 18.93 -8 4 -21 7.67 9.43 8 4 21 9.71 9.23 -8 -5 27 20.84 13.73 8 -5 -27 14.28 12.78 8 5 -27 14.26 4.88 -8 5 27 14.65 10.91 -8 -5 26 7.34 8.03 8 -5 -26 1.40 8.72 8 5 -26 8.02 7.45 -8 5 26 5.72 8.35 -8 -5 25 25.03 16.06 8 -5 -25 36.31 30.07 8 5 -25 31.47 12.08 -8 5 25 30.88 20.35 -8 -5 24 27.80 15.42 8 -5 -24 9.40 9.73 8 5 -24 14.78 11.13 -8 5 24 13.28 7.27 -8 -5 23 2.96 5.65 8 -5 -23 14.92 14.97 8 5 -23 7.87 8.25 -8 5 23 10.04 6.82 -8 -5 22 7.08 8.65 8 -5 -22 5.24 5.64 8 5 -22 17.82 9.42 -8 5 22 11.87 12.44 -8 -5 21 51.92 25.75 8 -5 -21 33.23 15.99 8 5 -21 42.17 18.54 -8 5 21 29.20 20.28 -8 -5 20 77.57 14.79 8 -5 -20 83.83 11.80 8 5 -20 100.48 12.64 -8 5 20 81.44 9.20 -8 -5 19 57.94 27.59 8 -5 -19 49.12 29.38 8 5 -19 62.25 20.78 -8 5 19 50.07 34.25 -8 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-8 -5 7 167.21 17.00 8 -5 -7 174.94 16.74 8 5 -7 151.28 14.06 8 -5 -7 177.13 18.15 8 5 -7 162.74 11.23 8 5 -6 63.70 25.37 8 -5 -5 61.77 25.45 8 5 -5 61.30 28.75 8 -5 -5 67.74 9.31 -8 -5 4 12.59 6.32 8 -5 -4 18.00 8.60 8 5 -4 23.71 12.95 8 -5 -4 15.85 8.53 8 5 -4 19.22 12.01 -8 -5 3 21.78 7.52 8 -5 -3 14.92 6.57 8 5 -3 10.86 6.69 8 -5 -3 18.62 11.85 8 5 -3 8.79 3.49 8 -5 -2 121.16 8.53 8 5 -2 114.60 14.33 8 -5 -2 131.99 14.51 8 5 -2 132.98 9.35 -8 5 1 207.86 12.34 8 -5 -1 241.49 17.42 8 -5 -1 210.88 17.61 8 5 -1 209.05 14.22 8 -5 0 27.55 10.57 8 5 0 25.33 9.48 8 -5 0 11.25 5.68 8 5 0 24.79 17.20 -8 5 -1 18.64 5.94 8 -5 1 17.62 8.88 8 -5 1 18.92 11.13 8 5 1 17.56 7.35 -8 5 -2 5.61 2.99 8 -5 2 6.14 5.28 8 5 2 7.87 5.99 8 -5 2 6.01 10.02 8 5 2 6.63 7.42 -8 5 -3 16.55 10.34 8 -5 3 14.93 10.38 8 5 3 17.85 14.07 8 -5 3 13.74 4.17 8 5 3 16.11 15.86 -8 5 -4 76.98 8.19 8 -5 4 67.63 7.18 8 5 4 70.16 9.62 8 -5 4 74.06 7.38 8 5 4 70.34 15.35 -8 -5 -5 15.05 10.54 -8 5 -5 9.37 4.89 8 -5 5 9.10 5.04 8 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8 -6 -16 19.20 8.14 8 6 -16 34.80 12.94 -8 6 16 22.89 19.35 -8 -6 15 51.64 21.19 8 -6 -15 44.33 24.58 8 6 -15 47.56 17.57 -8 6 15 34.07 17.43 -8 -6 14 52.58 21.40 8 -6 -14 45.51 19.29 8 6 -14 41.74 15.18 -8 6 14 37.18 21.77 -8 -6 13 24.97 9.77 8 -6 -13 8.98 7.16 8 6 -13 11.65 5.22 -8 6 13 12.86 7.30 -8 -6 12 27.81 14.17 8 -6 -12 28.58 17.21 8 6 -12 25.19 10.89 8 6 -12 33.32 5.65 -8 6 12 23.91 22.91 -8 -6 11 35.45 12.80 8 -6 -11 32.99 10.92 8 6 -11 30.28 17.31 8 6 -11 26.66 10.15 -8 6 11 16.43 28.73 -8 -6 10 62.47 15.79 8 -6 -10 36.83 26.63 8 6 -10 52.02 25.21 8 6 -10 43.89 6.67 -8 6 10 40.16 26.76 -8 -6 9 9.05 9.05 8 -6 -9 5.24 6.72 8 6 -9 3.00 6.40 8 -6 -9 3.01 5.06 8 6 -9 6.84 5.09 -8 -6 8 18.33 22.58 8 -6 -8 13.56 4.92 8 6 -8 13.72 7.50 8 -6 -8 18.66 8.98 8 6 -8 12.68 7.79 -8 -6 7 14.75 9.53 8 -6 -7 19.94 9.04 8 6 -7 17.43 7.74 8 -6 -7 12.28 10.44 -8 -6 6 70.13 30.86 8 -6 -6 65.48 12.14 8 6 -6 78.27 9.32 8 -6 -6 90.90 10.63 8 6 -6 70.93 7.84 -8 -6 5 70.76 12.63 8 -6 -5 46.45 29.82 8 6 -5 52.63 24.01 8 -6 -5 53.06 22.19 8 6 -5 44.14 21.08 -8 -6 4 31.26 9.68 8 -6 -4 36.89 13.46 8 6 -4 34.10 16.08 8 -6 -4 39.75 12.99 8 6 -4 30.32 14.48 -8 -6 3 18.82 8.89 8 -6 -3 10.30 6.53 8 6 -3 14.08 11.24 8 -6 -3 6.35 4.66 8 6 -3 13.24 7.78 -8 -6 2 57.21 24.70 8 -6 -2 36.63 7.85 8 6 -2 44.03 22.00 8 -6 -2 45.88 22.30 8 6 -2 42.59 26.58 -8 -6 1 17.16 8.15 8 -6 -1 7.52 8.57 8 6 -1 18.82 12.65 8 -6 -1 12.71 12.63 8 6 -1 11.88 16.83 8 -6 0 4.69 3.91 8 6 0 5.75 5.33 8 -6 0 4.23 5.23 8 6 0 2.00 2.67 8 -6 1 7.42 4.72 8 6 1 8.16 6.91 8 -6 1 3.26 6.47 8 6 1 13.22 7.29 8 -6 2 50.96 20.69 8 6 2 44.62 17.61 8 -6 2 34.20 26.51 8 6 2 45.62 6.41 8 -6 3 55.78 23.13 8 6 3 61.82 28.28 8 -6 3 46.43 21.56 8 6 3 58.01 8.46 -8 6 -4 2.96 3.22 8 -6 4 5.92 4.56 8 -6 4 6.15 5.90 8 6 4 -1.11 5.22 -8 6 -5 48.26 5.92 8 -6 5 47.43 6.08 8 6 5 41.46 27.40 8 -6 5 53.44 8.29 8 6 5 46.16 18.55 -8 6 -6 4.42 3.15 8 -6 6 -0.11 5.56 8 6 6 3.75 3.48 -8 6 -7 50.14 6.45 -8 -6 -7 57.06 8.86 8 -6 7 50.93 7.73 8 6 7 47.45 18.86 -8 6 -8 128.50 11.59 -8 -6 -8 137.02 10.80 8 -6 8 119.17 8.91 8 6 8 127.78 9.99 -8 -6 -9 38.23 11.89 -8 6 -9 24.57 14.09 -8 -6 -9 22.37 16.59 8 -6 9 26.81 16.31 8 6 9 23.66 11.51 -8 -6 -10 8.79 7.74 -8 6 -10 0.94 1.97 -8 -6 -10 3.02 3.01 8 -6 10 2.16 5.24 8 6 10 -3.60 5.21 -8 -6 -11 3.68 7.65 -8 6 -11 -0.54 3.37 -8 -6 -11 2.92 1.69 8 -6 11 2.33 4.57 8 6 11 -0.63 5.99 -8 -6 -12 32.05 21.74 -8 6 -12 22.05 16.50 -8 -6 -12 17.99 17.39 8 -6 12 32.75 21.46 8 6 12 22.07 11.20 -8 -6 -13 1.90 5.13 -8 6 -13 3.67 3.64 -8 -6 -13 2.86 6.18 8 -6 13 2.99 4.32 8 6 13 0.56 5.04 -8 -6 -14 7.08 17.82 -8 6 -14 10.74 6.22 -8 -6 -14 5.81 6.48 8 6 14 10.94 9.89 -8 -6 -15 4.42 14.23 -8 6 -15 3.12 5.53 -8 -6 -15 5.28 4.28 8 6 15 0.96 5.35 -8 -6 -16 23.07 33.54 -8 6 -16 20.73 15.47 -8 -6 -16 13.23 20.49 8 6 16 25.53 18.13 -8 -6 -17 6.22 6.36 -8 6 -17 2.78 3.88 8 6 17 -3.82 6.49 -8 -6 -18 -0.27 8.98 -8 6 -18 5.52 6.98 8 6 18 6.28 7.13 -8 -7 22 21.59 16.55 8 -7 -22 38.20 11.85 8 7 -22 31.39 13.05 -8 7 22 22.89 13.63 -8 -7 21 7.65 13.80 8 -7 -21 9.42 7.46 8 7 -21 11.40 13.69 -8 7 21 4.48 7.67 -8 -7 20 68.50 14.29 8 -7 -20 45.43 14.73 8 7 -20 36.88 20.31 -8 7 20 47.39 35.07 -8 -7 19 11.59 8.43 8 -7 -19 0.83 8.61 8 7 -19 7.30 5.83 -8 7 19 6.18 6.58 8 -7 -18 8.63 11.21 8 7 -18 6.58 4.71 -8 7 18 7.77 6.65 -8 -7 17 15.97 11.57 8 -7 -17 16.46 12.90 8 7 -17 2.35 5.21 -8 7 17 5.10 4.76 -8 -7 16 15.75 9.34 8 -7 -16 12.96 13.91 8 7 -16 21.94 9.07 -8 7 16 21.45 10.43 -8 -7 15 20.58 14.80 8 -7 -15 7.11 9.38 8 7 -15 5.29 3.74 -8 7 15 11.85 10.35 -8 -7 14 21.82 13.97 8 -7 -14 11.52 15.17 8 7 -14 16.30 10.06 -8 7 14 11.53 11.22 -8 -7 13 16.18 11.00 8 -7 -13 21.25 13.07 8 7 -13 22.93 13.61 -8 7 13 18.62 12.39 -8 -7 12 12.93 7.94 8 -7 -12 9.10 8.75 8 7 -12 8.10 6.14 -8 7 12 12.83 9.28 8 -7 -11 14.79 11.90 8 7 -11 30.54 12.54 8 7 -11 13.53 8.45 -8 7 11 16.69 12.80 8 -7 -10 48.57 25.10 8 7 -10 73.17 13.30 8 7 -10 54.61 8.47 -8 7 10 47.03 28.42 -8 -7 9 10.35 8.25 8 -7 -9 9.58 7.66 8 7 -9 6.75 12.75 8 7 -9 2.87 3.02 -8 7 9 7.14 6.61 -8 -7 8 70.34 14.86 8 -7 -8 90.79 9.42 8 7 -8 88.95 10.32 8 7 -8 74.28 6.21 -8 7 8 72.74 9.66 8 -7 -7 4.21 6.60 8 7 -7 11.67 7.85 8 7 -7 3.09 8.58 -8 7 7 0.40 4.27 8 -7 -6 45.21 18.80 8 7 -6 50.41 22.18 8 7 -6 56.64 6.27 -8 7 6 60.98 11.94 -8 -7 5 44.87 11.30 8 -7 -5 29.40 16.49 8 7 -5 29.72 13.30 8 7 -5 33.76 12.18 8 -7 -4 16.11 11.03 8 7 -4 11.35 8.61 8 -7 -4 11.91 4.68 8 7 -4 8.83 7.22 8 -7 -3 31.89 21.68 8 7 -3 29.88 21.00 8 -7 -3 34.92 15.02 8 7 -3 36.51 22.54 -8 -7 2 3.89 10.43 8 -7 -2 18.06 9.89 8 -7 -2 13.19 9.09 8 7 -2 11.13 6.54 -8 -7 1 15.02 17.07 8 -7 -1 23.83 12.56 8 7 -1 34.78 8.39 8 -7 -1 35.26 19.18 8 7 -1 26.01 13.51 -8 -7 0 48.62 12.30 8 -7 0 54.61 10.18 8 7 0 46.49 20.53 8 -7 0 72.90 10.30 8 7 0 51.84 12.06 -8 -7 -1 13.99 13.01 8 -7 1 1.88 4.09 8 -7 1 3.88 3.72 8 7 1 7.90 6.94 8 -7 2 38.47 21.79 8 7 2 40.40 29.77 8 -7 2 51.67 19.45 8 7 2 42.85 18.70 8 -7 3 17.76 14.18 8 7 3 27.19 10.94 8 -7 3 16.05 3.90 8 7 3 24.63 9.16 -8 -7 -4 20.21 8.64 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13.14 7.83 9 5 -12 16.38 27.28 9 -5 -12 8.96 10.33 9 -5 -11 319.96 30.50 9 5 -11 277.90 40.73 9 -5 -11 316.82 26.19 9 5 -11 329.09 25.46 -9 -5 10 88.03 20.84 9 -5 -10 24.00 27.94 9 -5 -10 23.69 38.17 -9 -5 9 208.54 20.72 9 -5 -9 251.04 27.94 9 5 -9 271.75 21.00 -9 -5 8 176.29 17.61 9 -5 -8 166.35 12.89 9 -5 -8 168.36 15.19 9 5 -8 155.42 9.26 -9 -5 7 17.58 13.21 9 -5 -7 5.46 7.38 9 -5 -7 14.25 7.61 9 5 -7 10.11 7.42 -9 -5 6 128.27 15.71 9 -5 -6 129.42 11.09 9 5 -6 114.81 9.88 9 -5 -6 116.59 12.72 9 5 -6 129.06 9.00 -9 -5 5 16.18 36.68 9 -5 -5 28.94 14.83 9 5 -5 14.42 9.15 9 -5 -5 26.57 12.10 9 5 -5 14.46 4.23 -9 -5 4 6.03 6.88 9 -5 -4 6.76 7.46 9 5 -4 3.17 6.80 9 -5 -4 0.90 6.09 9 5 -4 2.88 4.57 -9 -5 3 16.88 8.66 9 -5 -3 12.04 13.78 9 -5 -3 14.10 12.27 9 5 -3 11.15 6.26 -9 -5 2 70.55 32.07 9 -5 -2 80.71 18.14 9 5 -2 94.47 13.38 9 -5 -2 75.87 34.37 9 5 -2 75.38 12.34 9 -5 -1 0.81 7.94 9 5 -1 7.63 7.24 9 -5 -1 10.11 6.90 9 5 -1 4.27 5.44 9 -5 0 132.67 8.48 9 -5 0 141.71 11.74 9 5 0 118.76 9.34 -9 5 -1 64.37 4.20 9 -5 1 69.19 8.29 9 -5 1 95.12 18.86 9 5 1 68.87 10.43 -9 -5 -2 195.56 22.60 -9 5 -2 142.92 8.84 9 -5 2 157.80 9.01 9 -5 2 164.36 26.88 9 5 2 183.69 18.28 -9 5 -3 231.60 17.91 9 -5 3 196.91 16.06 9 -5 3 187.28 18.15 9 5 3 183.23 19.56 -9 5 -4 127.65 8.90 9 -5 4 146.30 6.83 9 5 4 255.59 25.51 9 -5 4 178.29 18.81 9 5 4 130.55 10.12 -9 -5 -5 159.49 22.58 -9 5 -5 140.23 9.82 9 5 5 167.02 17.41 9 -5 5 153.33 13.51 9 5 5 144.09 27.79 -9 5 -6 14.97 9.99 9 5 6 13.44 9.04 9 -5 6 8.09 5.52 9 5 6 16.39 13.39 -9 -5 -7 66.25 14.86 -9 5 -7 70.04 7.11 9 5 7 77.94 15.84 9 -5 7 75.99 9.00 9 5 7 81.79 11.02 -9 -5 -8 13.73 9.59 -9 5 -8 13.69 7.81 9 5 8 15.37 11.88 9 -5 8 11.96 9.98 9 5 8 14.04 14.66 -9 -5 -9 38.25 35.54 -9 5 -9 45.42 8.55 9 5 9 27.41 15.61 9 -5 9 38.05 24.54 9 5 9 51.18 20.55 -9 -5 -10 14.73 13.68 -9 5 -10 16.65 10.09 9 -5 10 22.39 9.12 9 5 10 20.90 16.88 -9 -5 -11 23.00 13.68 -9 5 -11 25.80 20.23 9 -5 11 35.74 20.94 9 5 11 21.13 13.25 -9 -5 -12 7.74 8.98 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6.86 9 -6 -18 8.45 12.96 9 6 -18 13.43 6.74 -9 6 18 25.81 11.56 -9 -6 17 2.45 7.48 9 -6 -17 5.11 8.38 9 6 -17 3.23 4.01 -9 6 17 5.87 6.74 -9 -6 16 2.03 8.95 9 -6 -16 8.80 10.31 9 6 -16 4.63 4.97 -9 6 16 8.76 8.78 -9 -6 15 30.91 14.37 9 -6 -15 24.02 17.24 9 6 -15 27.68 9.75 -9 6 15 24.40 15.19 -9 -6 14 78.87 14.85 9 -6 -14 72.46 24.95 9 6 -14 58.67 22.89 -9 6 14 64.74 35.29 -9 -6 13 10.67 7.35 9 -6 -13 7.14 10.27 9 6 -13 7.15 6.58 -9 6 13 3.27 11.70 -9 -6 12 61.71 12.08 9 -6 -12 48.80 23.78 9 6 -12 25.62 17.46 9 6 -12 33.18 4.08 -9 6 12 44.48 27.52 -9 -6 11 37.67 13.99 9 -6 -11 28.81 13.29 9 6 -11 35.68 11.54 9 -6 -11 19.32 10.11 9 6 -11 24.33 10.78 -9 -6 10 69.56 42.26 9 -6 -10 120.45 14.23 9 6 -10 105.72 13.80 9 -6 -10 92.10 46.98 9 6 -10 81.35 7.00 -9 -6 9 25.14 11.82 9 -6 -9 9.00 6.54 9 6 -9 8.79 5.13 9 -6 -9 13.59 8.31 9 6 -9 2.68 7.46 -9 -6 8 22.48 12.78 9 -6 -8 24.70 13.86 9 6 -8 17.79 10.43 9 -6 -8 10.10 15.65 9 6 -8 13.67 7.43 9 -6 -7 14.03 10.13 9 6 -7 19.37 8.70 9 -6 -7 20.38 8.44 9 6 -7 19.72 10.67 -9 -6 6 9.11 9.26 9 -6 -6 6.68 6.76 9 6 -6 9.08 11.69 9 -6 -6 13.72 11.38 9 6 -6 10.66 6.06 -9 -6 5 47.54 21.27 9 -6 -5 32.83 21.70 9 6 -5 40.51 20.65 9 -6 -5 39.16 23.97 9 6 -5 43.41 11.58 -9 -6 4 12.03 12.28 9 -6 -4 12.24 5.44 9 6 -4 9.99 11.01 9 -6 -4 10.78 10.52 9 6 -4 12.04 5.98 -9 -6 3 44.10 13.80 9 -6 -3 23.99 13.88 9 6 -3 21.53 10.98 9 -6 -3 21.39 7.11 9 6 -3 18.74 8.35 -9 -6 2 70.12 12.62 9 -6 -2 61.12 6.90 9 6 -2 66.77 9.76 9 -6 -2 59.98 28.11 9 6 -2 79.54 18.51 9 -6 -1 16.51 5.25 9 6 -1 17.21 14.93 9 -6 -1 17.51 7.11 9 6 -1 16.90 6.12 9 -6 0 6.91 7.70 9 -6 0 20.29 10.13 9 6 0 4.83 5.28 9 -6 1 49.91 7.56 9 6 1 40.42 25.91 9 -6 1 50.06 27.90 9 6 1 51.24 13.27 9 -6 2 58.10 15.95 9 6 2 58.43 28.74 9 -6 2 56.33 9.49 9 6 2 72.27 23.62 9 -6 3 63.40 6.82 9 -6 3 65.06 10.20 9 6 3 57.92 21.27 -9 -6 -4 1.96 13.56 9 6 4 4.12 2.98 9 -6 4 3.92 4.65 9 6 4 -0.51 5.24 -9 -6 -5 15.87 17.90 9 6 5 4.69 4.66 9 -6 5 8.84 7.72 9 6 5 12.62 6.97 9 6 6 8.16 8.36 9 -6 6 12.67 9.05 9 6 6 10.77 9.07 -9 -6 -7 17.72 24.78 9 6 7 9.53 13.42 9 -6 7 18.48 6.97 9 6 7 14.93 9.32 -9 -6 -8 9.08 14.43 -9 6 -8 11.44 8.95 9 6 8 3.37 9.39 9 -6 8 8.64 9.59 9 6 8 10.30 8.89 -9 -6 -9 14.44 12.06 -9 6 -9 7.50 4.90 9 -6 9 12.19 5.02 9 6 9 1.76 4.42 -9 -6 -10 3.61 7.95 -9 6 -10 0.86 2.29 9 -6 10 1.13 2.96 9 6 10 4.32 4.43 -9 -6 -11 8.97 11.00 -9 6 -11 4.76 6.04 -9 -6 -11 6.72 7.71 9 -6 11 9.98 8.62 9 6 11 6.00 7.63 -9 -6 -12 -1.35 7.93 -9 6 -12 2.85 2.45 -9 -6 -12 3.29 4.72 9 -6 12 4.02 4.26 9 6 12 4.09 7.49 -9 -6 -13 6.36 6.88 -9 6 -13 4.32 5.08 -9 -6 -13 4.07 3.02 9 -6 13 1.55 5.72 9 6 13 5.62 4.04 -9 -6 -14 10.48 10.50 -9 6 -14 6.53 5.53 -9 -6 -14 10.47 7.19 9 6 14 8.53 7.79 -9 -6 -15 26.65 11.82 -9 6 -15 9.95 6.91 9 6 15 15.05 10.06 -9 -6 -16 38.22 21.92 -9 6 -16 18.95 14.95 9 6 16 35.13 15.38 -9 -7 21 5.48 7.56 9 -7 -21 4.90 6.26 9 7 -21 1.69 3.77 -9 7 21 3.55 6.12 9 -7 -20 2.54 8.71 9 7 -20 6.38 3.54 -9 7 20 -3.66 8.53 -9 -7 19 10.59 9.64 9 -7 -19 40.51 15.55 9 7 -19 14.45 8.29 -9 7 19 10.16 14.60 -9 -7 18 23.55 12.59 9 -7 -18 10.26 16.86 9 7 -18 12.39 9.90 -9 7 18 5.57 5.20 -9 -7 17 15.04 17.11 9 -7 -17 14.62 15.25 9 7 -17 7.21 10.92 -9 7 17 17.35 11.04 -9 -7 16 98.39 45.10 9 -7 -16 80.37 34.65 9 7 -16 102.68 10.75 -9 7 16 86.64 14.18 -9 -7 15 17.97 15.37 9 -7 -15 6.44 5.60 9 7 -15 22.16 14.64 -9 7 15 4.23 7.52 -9 -7 14 49.13 31.77 9 -7 -14 44.94 27.36 9 7 -14 57.72 26.49 -9 7 14 39.67 34.36 -9 -7 13 14.89 13.08 9 -7 -13 10.92 24.79 9 7 -13 23.20 14.32 -9 7 13 14.00 10.60 -9 -7 12 4.58 5.64 9 -7 -12 1.24 6.73 9 7 -12 5.15 9.45 -9 7 12 1.02 4.46 -9 -7 11 18.21 12.23 9 -7 -11 5.61 6.18 9 7 -11 7.49 5.74 -9 7 11 3.31 7.32 -9 -7 10 10.19 8.58 9 -7 -10 12.22 6.65 9 7 -10 8.54 6.53 9 7 -10 10.82 3.64 -9 7 10 6.48 6.90 -9 -7 9 9.50 12.92 9 -7 -9 8.96 4.88 9 7 -9 7.82 8.80 9 7 -9 6.89 3.88 -9 7 9 10.49 7.99 -9 -7 8 10.26 12.15 9 -7 -8 7.19 6.28 9 7 -8 11.29 10.06 9 7 -8 10.32 7.91 -9 7 8 8.14 7.66 9 -7 -7 20.01 12.62 9 7 -7 22.09 8.79 9 -7 -7 10.77 6.11 9 7 -7 7.91 6.81 -9 -7 6 34.81 13.92 9 -7 -6 23.95 12.82 9 7 -6 16.40 7.53 9 -7 -6 15.64 10.67 9 7 -6 13.92 9.18 -9 -7 5 86.99 14.53 9 -7 -5 72.35 26.86 9 7 -5 51.58 24.24 9 -7 -5 55.05 30.12 9 7 -5 70.08 9.54 -9 -7 4 3.61 8.74 9 -7 -4 5.52 4.20 9 7 -4 5.83 3.57 9 -7 -4 4.39 3.33 9 7 -4 5.33 4.06 9 -7 -3 33.62 14.10 9 7 -3 33.71 17.30 9 -7 -3 39.03 22.56 9 7 -3 27.69 31.04 9 -7 -2 36.82 7.27 9 7 -2 9.78 10.25 9 -7 -2 8.23 14.25 9 7 -2 20.86 10.39 -9 -7 1 14.26 19.05 9 -7 -1 6.37 3.76 9 7 -1 6.69 5.77 9 -7 -1 23.74 8.12 9 7 -1 6.41 4.01 9 -7 0 7.12 5.72 9 7 0 8.43 9.62 9 -7 0 8.84 5.91 9 7 0 11.20 7.70 9 -7 1 33.29 16.04 9 7 1 31.92 18.71 9 -7 1 36.28 16.94 9 7 1 35.39 19.38 9 -7 2 2.67 2.63 9 7 2 2.40 5.51 9 -7 2 -1.47 4.45 9 7 2 4.17 4.58 9 7 3 -1.12 5.95 9 -7 3 3.87 4.42 9 7 3 -1.30 5.56 -9 -7 -4 8.14 9.39 9 7 4 7.51 11.88 9 -7 4 14.35 8.40 9 7 4 10.14 10.07 -9 -7 -5 21.91 13.36 9 7 5 19.41 8.84 9 -7 5 17.80 9.68 9 7 5 16.64 8.05 -9 -7 -6 63.84 39.38 9 7 6 40.47 18.07 9 -7 6 32.84 28.02 9 7 6 36.52 10.15 9 7 7 11.12 6.11 9 -7 7 4.44 5.17 9 7 7 4.74 6.04 -9 -7 -8 81.32 43.81 9 7 8 60.62 32.25 9 -7 8 100.68 11.08 9 7 8 73.06 14.04 -9 -7 -9 41.92 17.07 9 7 9 6.41 15.67 9 -7 9 8.41 9.31 9 7 9 5.10 4.04 -9 -7 -10 14.96 10.98 9 -7 10 24.05 19.08 9 7 10 28.68 12.13 -9 -7 -11 9.35 10.77 9 -7 11 10.29 12.75 9 7 11 3.55 10.51 -9 -7 -12 3.49 9.98 -9 -7 -12 21.02 13.28 9 7 12 2.64 10.89 -9 -7 -13 0.00 13.67 -9 -7 -13 7.78 5.28 9 7 13 5.07 8.64 -9 -8 17 42.40 38.15 9 -8 -17 35.99 25.08 9 8 -17 41.13 26.81 -9 8 17 37.94 29.16 9 8 -16 -0.22 6.85 -9 8 16 5.65 5.11 -9 -8 15 18.69 19.73 9 -8 -15 20.72 8.87 9 8 -15 25.08 13.88 -9 8 15 12.14 11.55 -9 -8 14 4.49 8.08 9 -8 -14 5.15 7.12 9 8 -14 -3.16 7.67 -9 8 14 8.03 9.82 -9 -8 13 10.71 11.19 9 -8 -13 5.34 7.70 9 8 -13 4.04 7.32 -9 8 13 7.51 7.31 -9 -8 12 19.28 17.61 9 -8 -12 20.77 15.32 9 8 -12 18.30 16.61 -9 8 12 22.27 14.60 9 -8 -11 28.90 18.85 9 8 -11 24.87 8.12 -9 8 11 38.53 22.42 -9 -8 10 15.21 11.70 9 -8 -10 8.72 9.58 9 8 -10 9.46 6.33 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9.90 6.43 9 -8 4 9.41 5.40 9 8 4 10.23 8.28 -9 -8 -5 10.78 11.46 9 8 5 3.05 9.29 9 -8 5 8.60 9.30 9 8 5 8.74 6.59 -9 -8 -6 21.41 10.18 9 8 6 6.33 6.88 9 -8 6 17.07 11.62 9 8 6 8.50 7.37 9 8 7 20.00 10.89 9 -8 7 7.25 5.69 9 8 7 15.53 8.37 -9 -8 -8 12.76 9.19 9 8 8 3.08 6.92 9 -8 8 5.97 3.98 9 8 8 6.32 7.69 -9 -8 -9 6.61 7.31 9 8 9 1.43 6.83 9 -8 9 5.39 3.69 9 8 9 6.15 4.18 -9 -9 10 14.00 21.85 9 -9 -10 14.61 16.24 9 9 -10 11.14 11.58 -9 9 10 12.58 9.15 -9 -9 9 5.53 8.51 9 -9 -9 9.83 8.36 9 9 -9 6.10 10.28 -9 9 9 7.41 8.71 -9 -9 8 8.06 8.61 9 -9 -8 -1.06 7.96 -9 9 8 4.08 4.08 9 -9 -7 3.98 6.17 9 9 -7 9.59 9.11 -9 9 7 13.88 7.97 9 -9 -6 19.88 11.68 9 9 -6 8.55 4.64 9 9 -6 6.34 4.88 -9 9 6 3.93 7.76 9 -9 -5 5.87 10.35 9 9 -5 4.45 4.02 -9 9 5 7.22 6.63 9 -9 -4 75.51 11.43 9 9 -4 55.88 35.96 9 9 -4 50.69 31.32 -9 9 4 42.13 32.10 9 -9 -3 8.65 14.13 9 9 -3 16.65 8.51 9 9 -3 16.11 10.49 -9 9 3 19.67 12.81 9 -9 -2 3.21 4.41 9 9 -2 2.49 6.65 9 9 -2 4.62 3.07 -9 9 2 5.65 5.32 -9 -9 1 10.38 15.55 9 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480.07 30.30 -10 0 15 114.96 11.01 10 0 -15 93.77 10.68 10 0 -15 110.98 10.60 -10 0 14 256.82 26.77 10 0 -14 234.00 15.39 10 0 -14 227.24 15.82 -10 0 13 135.47 12.81 10 0 -13 122.73 9.72 10 0 -13 112.94 23.74 -10 0 12 157.76 16.49 10 0 -12 146.80 11.93 10 0 -12 164.83 14.05 -10 0 11 2.88 3.44 10 0 -11 3.65 2.91 10 0 -11 4.43 5.81 -10 0 10 1.92 2.09 10 0 -10 3.19 2.81 10 0 -10 2.44 5.81 -10 0 9 7.53 5.47 10 0 -9 5.35 3.44 -10 0 8 128.26 7.89 10 0 -8 144.24 20.85 -10 0 7 20.76 6.83 10 0 -7 19.19 12.35 10 0 -7 26.51 9.95 -10 0 6 251.03 18.97 10 0 -6 266.64 16.90 10 0 -6 267.93 18.63 -10 0 5 3.93 4.79 10 0 -5 5.88 4.65 10 0 -5 9.87 6.69 -10 0 4 333.22 23.33 10 0 -4 303.85 18.37 10 0 -4 305.55 21.28 -10 0 3 1.36 5.08 10 0 -3 -0.09 2.23 10 0 -3 1.29 5.00 -10 0 2 58.49 9.34 10 0 -2 78.07 8.21 10 0 -2 109.24 17.44 -10 0 1 11.19 11.92 10 0 -1 4.51 4.01 -10 0 0 173.51 14.76 10 0 0 154.10 11.89 10 0 0 178.14 14.99 -10 0 -1 3.09 2.83 10 0 1 -0.44 1.70 10 0 1 4.81 5.22 -10 0 -2 12.57 5.66 10 0 2 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123.78 13.08 10 -4 -17 115.95 29.63 -10 -4 16 16.05 7.34 10 -4 -16 29.73 22.77 10 -4 -16 30.30 13.38 10 4 -16 23.62 15.55 -10 -4 15 68.47 31.90 10 -4 -15 69.42 32.69 10 4 -15 74.00 28.65 10 -4 -15 56.60 28.51 10 4 -15 65.05 10.33 -10 -4 14 11.28 8.99 10 -4 -14 3.53 6.22 10 4 -14 2.03 5.17 10 -4 -14 5.88 5.79 10 4 -14 1.61 2.90 -10 -4 13 5.69 6.83 10 -4 -13 5.42 4.56 10 4 -13 4.41 3.99 10 -4 -13 12.62 10.08 10 4 -13 2.96 4.37 -10 -4 12 143.82 15.11 10 -4 -12 120.50 9.19 10 -4 -12 132.51 13.98 10 4 -12 142.55 16.93 -10 -4 11 148.70 17.65 10 -4 -11 132.17 21.09 10 4 -11 147.96 24.12 10 -4 -11 147.70 28.28 10 4 -11 170.26 14.98 -10 -4 10 159.06 35.33 10 -4 -10 140.29 15.54 10 4 -10 133.62 16.39 10 -4 -10 162.00 17.17 10 4 -10 137.59 17.28 -10 -4 9 29.91 10.29 10 -4 -9 40.92 7.61 10 4 -9 41.79 19.26 10 -4 -9 29.38 30.26 10 4 -9 57.16 7.98 -10 -4 8 10.79 10.47 10 -4 -8 18.54 7.68 10 4 -8 14.89 5.28 10 -4 -8 10.64 9.65 10 4 -8 9.64 6.19 -10 -4 7 4.93 9.31 10 -4 -7 -0.13 5.62 10 4 -7 5.65 3.89 10 -4 -7 5.28 6.04 10 4 -7 5.63 4.05 -10 -4 6 60.58 22.22 10 -4 -6 52.22 7.58 10 4 -6 51.57 20.99 10 -4 -6 64.82 8.77 10 4 -6 42.23 5.84 -10 -4 5 37.88 14.81 10 -4 -5 20.40 10.54 10 4 -5 14.73 12.47 10 -4 -5 28.82 11.13 10 4 -5 23.47 9.70 -10 -4 4 98.53 19.33 10 -4 -4 111.17 8.45 10 4 -4 115.90 13.90 10 -4 -4 126.41 14.45 10 4 -4 103.05 9.41 -10 -4 3 12.32 8.88 10 -4 -3 14.51 8.37 10 4 -3 11.76 7.96 10 -4 -3 12.64 8.00 10 4 -3 19.88 6.57 10 -4 -2 13.44 8.78 10 4 -2 16.29 9.96 10 -4 -2 5.05 8.85 10 4 -2 14.87 17.14 -10 -4 1 15.93 12.30 -10 4 1 22.51 8.01 10 -4 -1 24.89 12.25 10 4 -1 17.35 8.26 10 -4 -1 22.16 13.51 10 4 -1 26.13 10.32 -10 -4 0 23.13 10.37 -10 4 0 15.44 9.31 10 -4 0 12.39 7.38 10 4 0 14.33 9.20 10 -4 0 15.03 7.61 10 4 0 10.04 5.87 -10 4 -1 156.00 8.04 10 -4 1 152.53 13.34 10 -4 1 176.99 15.59 10 4 1 169.21 26.16 -10 -4 -2 133.20 19.32 -10 4 -2 92.57 6.84 10 4 2 110.06 10.09 10 -4 2 80.53 28.13 10 4 2 103.94 15.08 -10 4 -3 318.85 23.88 10 -4 3 329.00 26.75 10 4 3 292.49 24.96 -10 -4 -4 21.92 17.01 10 -4 4 9.86 28.00 10 4 4 16.34 16.90 -10 -4 -5 26.07 9.61 -10 4 -5 11.47 9.81 10 4 5 11.82 8.40 10 -4 5 10.47 10.06 10 4 5 13.44 10.81 -10 -4 -6 33.99 17.25 -10 4 -6 27.38 15.49 10 4 6 31.80 13.62 10 -4 6 24.89 18.11 10 4 6 29.92 7.49 -10 -4 -7 20.18 17.97 -10 4 -7 21.08 17.17 10 4 7 18.45 14.01 10 -4 7 11.23 5.96 10 4 7 17.61 15.82 -10 4 -8 7.57 3.82 10 4 8 5.68 4.29 10 -4 8 15.88 7.88 10 4 8 6.83 10.08 -10 4 -9 105.06 16.73 10 4 9 109.75 10.15 10 -4 9 117.48 15.25 10 4 9 123.55 11.56 -10 4 -10 3.52 4.89 10 4 10 5.45 4.94 10 -4 10 2.29 6.16 10 4 10 7.75 6.91 -10 4 -11 22.09 14.48 10 4 11 14.17 9.11 10 -4 11 23.52 13.41 10 4 11 19.81 13.81 -10 -4 -12 24.69 18.13 -10 4 -12 10.51 7.19 10 -4 12 9.12 9.64 10 4 12 11.68 11.30 -10 -4 -13 25.43 19.07 -10 4 -13 27.96 15.40 10 -4 13 28.73 14.03 10 4 13 18.43 13.39 -10 -4 -14 18.00 15.42 -10 4 -14 10.20 7.45 10 -4 14 9.88 6.81 10 4 14 9.50 6.74 -10 -4 -15 29.41 23.50 -10 4 -15 31.97 20.78 10 -4 15 22.77 22.47 10 4 15 32.27 15.30 -10 -4 -16 1.12 7.06 -10 4 -16 4.60 4.25 10 -4 16 2.33 2.33 10 4 16 -0.14 7.76 -10 -4 -17 6.74 10.16 -10 4 -17 1.29 3.08 10 -4 17 4.77 10.98 10 4 17 5.57 9.89 -10 -4 -18 22.78 17.65 -10 4 -18 13.27 12.77 10 4 18 8.64 8.72 -10 -5 25 16.86 13.09 10 -5 -25 19.95 15.68 10 5 -25 22.65 15.37 -10 5 25 30.69 21.63 -10 -5 24 16.97 16.27 10 -5 -24 26.88 19.44 10 5 -24 13.08 9.02 -10 5 24 13.49 8.07 -10 -5 23 3.11 2.99 10 -5 -23 3.49 4.40 10 5 -23 0.21 5.01 -10 5 23 5.00 9.74 -10 -5 22 10.17 8.58 10 5 -22 2.35 4.82 -10 5 22 1.83 3.12 -10 -5 21 -1.40 6.18 10 -5 -21 0.74 10.81 10 5 -21 4.66 7.68 -10 5 21 -0.40 6.02 -10 -5 20 10.47 10.58 10 -5 -20 27.44 17.44 10 5 -20 21.71 10.90 -10 5 20 19.19 8.01 -10 -5 19 8.36 6.96 10 -5 -19 9.40 8.92 10 5 -19 11.31 7.65 -10 5 19 14.40 8.86 -10 -5 18 18.17 8.92 10 -5 -18 13.09 8.55 10 5 -18 4.53 5.81 -10 5 18 5.79 5.54 -10 -5 17 9.26 9.08 10 -5 -17 6.90 7.07 10 5 -17 10.79 7.52 -10 5 17 8.33 4.48 -10 -5 16 33.45 20.10 10 -5 -16 34.43 27.57 10 5 -16 38.11 15.62 -10 -5 15 2.91 5.79 10 -5 -15 9.20 17.42 10 5 -15 9.84 11.67 10 -5 -15 14.76 8.41 -10 -5 14 147.30 16.79 10 -5 -14 141.73 16.70 10 5 -14 114.87 13.56 10 -5 -14 125.33 32.50 10 5 -14 114.72 14.98 -10 -5 13 12.98 8.53 10 -5 -13 7.81 9.50 10 5 -13 9.13 6.46 10 -5 -13 18.21 11.57 10 5 -13 12.05 9.81 -10 -5 12 186.76 22.00 10 -5 -12 173.08 16.22 10 5 -12 180.98 12.57 10 -5 -12 205.78 27.00 10 5 -12 177.20 21.57 10 -5 -11 77.35 8.55 10 5 -11 85.68 8.60 10 -5 -11 66.33 43.86 10 5 -11 80.50 8.64 -10 -5 10 44.93 12.56 10 -5 -10 33.72 14.32 10 -5 -10 44.68 31.92 10 5 -10 36.28 14.59 -10 -5 9 79.98 18.12 10 -5 -9 59.41 9.81 10 5 -9 55.69 16.87 10 -5 -9 73.89 22.19 10 5 -9 51.31 5.57 -10 -5 8 71.43 13.69 10 -5 -8 70.63 22.10 10 5 -8 77.01 10.48 10 -5 -8 67.91 12.24 10 5 -8 70.94 11.72 -10 -5 7 0.74 8.60 10 -5 -7 -1.55 5.22 10 5 -7 3.33 3.79 10 -5 -7 8.21 7.59 10 5 -7 1.67 5.37 -10 -5 6 6.85 9.34 10 -5 -6 13.05 7.50 10 5 -6 8.22 6.12 10 -5 -6 17.03 7.78 10 5 -6 9.54 5.08 -10 -5 5 15.83 10.98 10 -5 -5 11.35 7.02 10 5 -5 12.10 10.43 10 -5 -5 11.78 7.21 10 5 -5 14.93 10.43 -10 -5 4 1.29 6.86 10 -5 -4 -0.78 3.95 10 5 -4 5.66 5.61 10 -5 -4 0.79 5.95 10 5 -4 1.52 2.60 -10 -5 3 32.93 14.15 10 -5 -3 38.32 17.74 10 5 -3 23.01 11.06 10 -5 -3 30.34 20.98 10 5 -3 34.68 18.30 10 -5 -2 16.69 9.82 10 5 -2 19.43 11.33 10 -5 -2 18.10 7.06 10 5 -2 15.44 10.43 -10 -5 1 23.90 12.58 10 -5 -1 11.25 6.74 10 5 -1 6.82 4.73 10 -5 -1 8.00 7.80 10 5 -1 3.19 5.84 10 -5 0 11.94 14.37 10 -5 0 18.13 12.85 10 5 0 19.64 18.45 10 -5 1 67.86 10.72 10 5 1 60.03 15.21 10 -5 1 82.82 15.32 10 5 1 59.07 7.47 10 -5 2 26.60 17.24 10 5 2 38.96 8.74 10 -5 2 41.40 8.90 10 5 2 28.13 18.53 10 5 3 92.75 10.87 10 -5 3 87.97 11.57 10 5 3 77.70 16.40 10 5 4 117.59 23.97 10 -5 4 142.19 13.56 10 5 4 129.87 11.45 -10 5 -5 40.11 5.14 10 5 5 27.52 16.24 10 -5 5 36.14 20.98 10 5 5 25.90 12.86 -10 5 -6 90.21 7.05 10 5 6 111.68 13.17 10 -5 6 102.17 10.61 10 5 6 96.33 10.01 -10 -5 -7 7.62 9.41 -10 5 -7 6.84 5.16 10 5 7 5.91 2.65 10 -5 7 10.03 7.00 10 5 7 15.20 11.86 -10 -5 -8 9.45 9.36 -10 5 -8 7.20 7.48 10 5 8 13.08 7.15 10 -5 8 18.63 12.27 10 5 8 9.49 12.21 -10 -5 -9 5.63 8.72 -10 5 -9 2.94 3.67 10 5 9 2.91 4.73 10 -5 9 5.36 4.28 10 5 9 3.57 5.31 -10 -5 -10 11.31 15.17 -10 5 -10 5.79 5.47 10 5 10 4.94 7.67 10 -5 10 8.21 4.09 10 5 10 9.57 9.16 -10 -5 -11 3.97 7.55 -10 5 -11 3.91 2.35 10 5 11 3.95 5.55 10 -5 11 6.77 7.67 10 5 11 -2.67 6.06 -10 -5 -12 24.83 19.60 -10 5 -12 16.11 8.81 10 5 12 10.14 6.23 10 -5 12 9.71 13.86 10 5 12 22.82 8.75 -10 -5 -13 0.99 6.69 -10 5 -13 1.71 4.09 10 -5 13 3.23 4.15 10 5 13 9.60 7.32 -10 -5 -14 4.68 5.33 -10 5 -14 9.47 4.69 10 -5 14 2.99 3.61 10 5 14 1.86 3.62 -10 -5 -15 7.09 10.15 -10 5 -15 12.43 9.39 10 -5 15 4.27 5.34 10 5 15 9.50 9.03 -10 -5 -16 38.57 20.75 -10 5 -16 17.02 17.99 10 5 16 37.58 26.83 -10 5 -17 3.91 5.96 10 5 17 5.21 4.33 -10 -6 23 4.42 6.04 10 -6 -23 7.43 7.35 10 6 -23 16.33 7.34 -10 6 23 4.12 5.36 -10 -6 22 22.87 12.03 10 -6 -22 5.09 7.53 10 6 -22 9.73 7.88 -10 6 22 5.27 6.00 -10 -6 21 2.51 7.89 10 -6 -21 10.82 13.06 10 6 -21 7.61 5.03 -10 6 21 12.80 8.12 -10 -6 20 81.71 15.14 10 -6 -20 76.96 15.90 10 6 -20 56.98 22.50 -10 6 20 43.85 29.12 -10 -6 19 27.04 12.53 10 -6 -19 10.98 13.15 10 6 -19 14.14 10.86 -10 6 19 14.51 14.00 -10 -6 18 41.91 21.06 10 -6 -18 34.96 28.96 10 6 -18 50.90 16.98 -10 6 18 41.69 26.47 -10 -6 17 5.30 7.46 10 -6 -17 4.86 7.23 10 6 -17 5.65 9.68 -10 6 17 2.14 7.13 -10 -6 16 12.30 7.24 10 -6 -16 20.05 13.59 10 6 -16 19.84 8.84 -10 6 16 15.78 10.03 -10 -6 15 8.29 16.62 10 -6 -15 10.89 10.24 10 6 -15 14.79 8.55 -10 6 15 9.59 6.85 -10 -6 14 7.97 9.35 10 -6 -14 5.89 9.20 10 6 -14 4.09 5.36 -10 6 14 4.63 10.46 10 -6 -13 36.55 23.27 10 6 -13 37.21 13.58 -10 -6 12 14.65 15.38 10 -6 -12 13.00 13.23 10 6 -12 9.36 10.47 10 -6 -12 19.08 14.37 10 6 -12 7.91 13.43 -10 -6 11 7.30 7.74 10 -6 -11 2.45 3.21 10 6 -11 3.63 2.88 10 -6 -11 7.55 7.76 10 6 -11 6.51 6.44 -10 -6 10 8.89 7.18 10 -6 -10 10.13 5.42 10 6 -10 3.65 8.99 10 -6 -10 6.15 5.17 10 6 -10 9.76 5.21 -10 -6 9 8.92 4.68 10 -6 -9 21.08 6.48 10 6 -9 17.66 8.83 10 -6 -9 16.54 10.17 10 6 -9 18.37 9.57 -10 -6 8 19.49 10.70 10 -6 -8 9.09 6.89 10 6 -8 15.92 11.72 10 6 -8 14.81 5.81 -10 -6 7 55.11 11.94 10 -6 -7 54.89 8.41 10 6 -7 33.86 15.90 10 -6 -7 65.81 37.29 10 6 -7 60.12 7.96 10 -6 -6 11.62 5.58 10 6 -6 11.05 10.92 10 -6 -6 12.50 13.95 10 6 -6 7.42 3.23 -10 -6 5 5.83 8.49 10 -6 -5 0.32 3.24 10 6 -5 0.62 7.20 10 -6 -5 4.99 5.46 10 6 -5 1.50 4.80 -10 -6 4 9.85 10.27 10 -6 -4 15.03 5.18 10 6 -4 11.97 7.78 10 -6 -4 10.37 9.85 10 6 -4 8.56 7.02 -10 -6 3 3.22 7.96 10 -6 -3 4.69 3.15 10 6 -3 4.70 6.08 10 -6 -3 5.03 6.55 10 6 -3 1.71 2.67 10 -6 -2 18.20 14.46 10 6 -2 31.34 12.75 10 -6 -2 23.21 11.49 10 6 -2 21.49 10.03 10 -6 -1 6.97 10.25 10 6 -1 5.91 8.19 10 -6 -1 11.35 10.71 10 6 -1 8.26 11.97 10 -6 0 14.28 7.99 10 6 0 17.14 13.05 10 -6 0 21.04 11.51 10 6 0 10.67 11.89 10 -6 1 9.62 6.53 10 6 1 7.91 5.08 10 -6 1 19.35 10.44 10 6 1 11.01 9.39 10 6 2 1.47 3.94 10 -6 2 -4.10 6.48 10 6 2 0.68 3.93 -10 -6 -3 18.77 13.59 10 6 3 6.99 5.65 10 -6 3 10.58 8.22 10 6 3 3.68 4.70 10 6 4 30.66 17.66 10 -6 4 35.37 24.82 10 6 4 31.26 15.05 10 6 5 6.69 5.62 10 -6 5 8.15 7.33 10 6 5 11.92 8.55 -10 -6 -6 12.81 9.19 10 6 6 7.54 6.11 10 -6 6 1.10 2.55 10 6 6 5.05 4.19 10 6 7 1.91 5.83 10 -6 7 4.44 4.37 10 6 7 4.55 6.06 -10 -6 -8 15.32 11.91 10 6 8 5.85 3.27 10 -6 8 5.24 6.94 10 6 8 3.65 4.35 -10 -6 -9 15.78 20.09 10 6 9 24.82 12.28 10 -6 9 28.49 17.60 10 6 9 26.04 13.73 -10 -6 -10 14.39 14.85 10 6 10 21.68 13.92 10 -6 10 12.11 14.64 10 6 10 10.13 9.19 10 6 11 55.18 26.03 10 -6 11 79.97 20.17 10 6 11 49.25 20.80 10 6 12 8.78 6.83 10 -6 12 2.89 4.74 10 6 12 2.96 8.27 -10 -6 -13 24.46 19.96 10 -6 13 27.01 27.81 10 6 13 26.23 18.76 -10 -6 -14 13.28 6.93 10 6 14 4.38 5.69 -10 -7 20 5.75 6.63 -10 7 20 -1.90 7.46 -10 -7 19 5.60 7.53 10 -7 -19 3.27 10.15 10 7 -19 4.68 6.82 -10 7 19 2.54 7.06 -10 -7 18 11.83 14.53 10 -7 -18 21.27 7.42 10 7 -18 26.24 14.24 -10 7 18 14.33 8.83 -10 -7 17 61.74 35.40 10 -7 -17 69.92 25.72 10 7 -17 39.72 24.55 -10 7 17 37.18 17.44 -10 -7 16 10.38 17.42 10 -7 -16 6.16 6.83 10 7 -16 8.61 9.80 -10 7 16 6.93 6.98 -10 -7 15 48.15 18.01 10 -7 -15 22.75 12.43 10 7 -15 25.49 19.05 -10 7 15 23.55 12.82 10 -7 -14 1.43 3.21 10 7 -14 6.08 4.88 -10 7 14 2.54 4.84 -10 -7 13 23.81 9.06 10 -7 -13 7.62 10.05 10 7 -13 4.39 6.17 -10 7 13 11.80 12.19 -10 -7 12 15.29 14.44 10 -7 -12 12.24 14.54 10 7 -12 8.96 6.71 -10 7 12 10.04 8.14 -10 -7 11 2.85 5.37 10 -7 -11 8.59 6.19 10 7 -11 7.26 5.58 -10 7 11 7.46 6.72 10 -7 -10 10.91 9.02 10 7 -10 6.42 8.48 10 7 -10 4.84 5.62 -10 7 10 5.49 4.13 10 -7 -9 27.07 21.99 10 7 -9 19.05 8.36 10 -7 -9 23.22 9.10 10 7 -9 32.52 11.96 10 -7 -8 8.53 8.54 10 7 -8 10.90 10.70 10 -7 -8 9.72 6.25 10 7 -8 6.89 5.40 10 -7 -7 1.44 3.11 10 7 -7 6.46 6.55 10 -7 -7 4.00 10.13 10 7 -7 5.64 6.46 -10 -7 6 9.55 8.62 10 -7 -6 4.61 4.75 10 7 -6 3.00 5.43 10 -7 -6 5.18 9.59 10 7 -6 5.97 3.69 -10 -7 5 41.10 21.86 10 -7 -5 47.20 27.81 10 7 -5 48.81 18.74 10 -7 -5 41.31 32.13 10 7 -5 39.22 16.78 -10 -7 4 3.70 10.31 10 -7 -4 1.42 5.27 10 7 -4 2.32 4.30 10 -7 -4 5.48 5.95 10 7 -4 2.44 4.80 -10 -7 3 20.22 8.85 10 -7 -3 23.00 15.73 10 7 -3 24.10 20.02 10 -7 -3 20.22 14.54 10 7 -3 24.99 18.24 -10 -7 2 10.23 8.81 10 -7 -2 19.11 9.22 10 7 -2 9.49 6.80 10 -7 -2 16.43 13.66 10 7 -2 12.09 10.77 -10 -7 1 23.96 21.99 10 -7 -1 27.44 12.58 10 7 -1 31.81 12.15 10 -7 -1 40.71 13.94 10 7 -1 23.20 9.01 10 7 0 15.32 14.62 10 -7 0 20.87 12.08 10 7 0 18.34 11.68 10 7 1 43.19 21.01 10 -7 1 34.61 30.58 10 7 1 40.98 31.95 10 7 2 28.35 18.11 10 -7 2 18.99 10.92 10 7 2 14.49 9.13 10 7 3 7.93 5.88 10 -7 3 19.24 9.60 10 7 3 7.97 5.81 10 7 4 17.03 13.10 10 -7 4 19.23 12.18 10 7 4 12.64 15.44 10 7 5 28.04 15.43 10 -7 5 34.74 18.03 10 7 5 28.18 16.09 10 7 6 6.97 7.67 10 -7 6 1.81 5.44 10 7 6 3.55 4.92 -10 -7 -7 36.92 14.96 10 7 7 25.18 20.47 10 -7 7 46.87 12.64 10 7 7 35.32 24.28 10 7 8 11.35 11.38 10 -7 8 14.73 8.09 10 7 8 7.62 5.46 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15.35 11 -5 -15 36.41 22.81 11 5 -15 28.28 16.97 11 -5 -15 42.44 22.79 -11 -5 14 24.07 9.38 11 -5 -14 20.89 14.54 11 5 -14 19.37 10.14 11 -5 -14 29.03 26.66 11 5 -14 25.13 16.91 -11 -5 13 7.91 8.02 11 -5 -13 10.62 6.44 11 5 -13 8.69 6.39 11 -5 -13 15.41 10.68 -11 -5 12 84.76 13.06 11 -5 -12 77.18 36.51 11 5 -12 74.45 29.65 11 -5 -12 98.36 11.68 11 5 -12 71.28 14.01 -11 -5 11 69.59 10.81 11 -5 -11 76.05 8.44 11 5 -11 80.87 10.31 11 -5 -11 70.94 33.51 11 5 -11 76.21 20.27 -11 -5 10 12.49 10.52 11 -5 -10 4.45 5.33 11 5 -10 10.68 7.22 11 -5 -10 12.83 7.05 11 5 -10 8.10 5.62 -11 -5 9 83.34 13.49 11 -5 -9 93.60 11.68 11 5 -9 93.27 12.38 11 -5 -9 101.60 16.61 11 5 -9 90.91 10.51 -11 -5 8 47.94 38.58 11 -5 -8 52.11 7.08 11 5 -8 65.66 26.65 11 -5 -8 60.90 33.51 11 5 -8 55.47 19.14 -11 -5 7 11.27 8.55 11 -5 -7 8.98 7.79 11 5 -7 12.16 7.26 11 -5 -7 14.68 9.01 11 5 -7 8.75 10.01 -11 -5 6 87.63 18.52 11 -5 -6 65.19 10.22 11 5 -6 48.54 32.07 11 -5 -6 60.06 39.94 11 5 -6 66.94 9.61 -11 -5 5 31.07 26.75 11 -5 -5 17.09 9.47 11 5 -5 34.16 17.99 11 -5 -5 32.88 11.06 11 5 -5 34.26 12.41 -11 -5 4 119.07 15.27 11 -5 -4 149.21 12.02 11 5 -4 135.13 11.04 11 -5 -4 140.40 13.74 11 5 -4 127.92 11.83 -11 -5 3 14.23 19.30 11 -5 -3 10.25 8.11 11 5 -3 9.37 6.83 11 -5 -3 16.63 9.00 11 5 -3 23.09 9.78 11 -5 -2 53.17 6.10 11 5 -2 66.13 9.59 11 -5 -2 76.27 9.03 11 5 -2 60.88 28.13 -11 -5 1 29.53 12.08 11 -5 -1 13.39 8.76 11 5 -1 19.67 11.27 11 -5 -1 15.27 9.99 11 5 -1 18.10 6.43 -11 -5 0 64.10 13.31 11 5 0 41.30 5.93 11 -5 0 60.04 10.86 11 5 0 47.29 10.68 -11 -5 -1 64.45 12.40 11 5 1 30.45 18.32 11 -5 1 52.09 27.16 11 5 1 34.00 13.21 -11 -5 -2 16.21 11.89 11 5 2 15.18 11.66 11 -5 2 19.34 11.18 11 5 2 19.34 10.64 11 5 3 84.07 9.31 11 -5 3 96.27 17.19 11 5 3 82.71 11.62 -11 -5 -4 74.36 12.85 11 5 4 48.41 5.77 11 -5 4 49.01 33.62 11 5 4 51.48 28.57 -11 -5 -5 31.84 18.40 11 5 5 16.58 13.34 11 -5 5 17.26 10.63 11 5 5 19.07 8.08 -11 -5 -6 16.66 8.48 11 5 6 21.93 10.38 11 -5 6 13.65 12.57 11 5 6 27.57 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3.57 3.35 13 -6 -3 12.19 11.40 13 6 -3 5.11 4.06 -13 -6 2 11.45 8.63 13 6 -2 14.15 11.74 13 -6 -2 20.05 20.99 13 6 -2 22.74 9.26 13 6 -1 10.01 11.66 13 -6 -1 11.54 9.87 13 6 -1 1.83 6.21 13 6 0 2.63 6.71 13 -6 0 5.26 6.93 13 6 0 9.58 10.19 13 6 1 13.41 9.33 13 -6 1 12.53 8.46 13 6 1 22.07 7.16 13 6 2 5.04 5.08 13 -6 2 6.12 8.62 13 6 2 5.93 6.98 -13 -6 -3 6.31 10.03 13 6 3 4.25 3.71 13 -6 3 9.03 6.89 13 6 3 4.20 3.71 13 6 4 1.98 4.85 13 -6 4 5.88 5.52 13 6 4 0.96 3.44 -13 -6 -5 12.52 10.08 13 6 5 0.79 2.85 13 -6 5 5.88 11.38 13 6 5 6.51 6.78 -13 -6 -6 5.23 9.48 13 -6 6 12.91 7.72 13 6 6 10.16 6.27 -13 -7 11 7.79 13.61 13 -7 -11 8.89 13.06 -13 -7 10 45.28 12.82 13 -7 -10 43.39 36.51 13 7 -10 55.11 31.09 13 -7 -10 40.61 31.54 -13 -7 9 2.20 7.01 13 -7 -9 5.04 7.91 13 7 -9 3.97 6.16 13 -7 -9 4.07 3.59 13 7 -9 1.97 2.92 -13 -7 8 49.70 12.33 13 7 -8 22.28 12.10 13 -7 -8 25.85 14.66 13 7 -8 9.44 7.65 13 7 -7 8.08 8.00 13 -7 -7 13.06 10.78 13 7 -7 4.38 4.65 13 7 -6 4.48 9.75 13 -7 -6 8.44 5.13 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15 5 -2 5.67 5.91 15 -5 -2 13.36 8.06 15 5 -2 7.18 10.98 15 5 -1 20.68 11.70 15 -5 -1 8.57 27.09 15 5 -1 15.56 10.22 15 -5 0 12.16 10.63 15 5 0 13.37 9.89 16 0 -19 10.09 11.59 16 0 -19 16.37 11.91 16 0 -18 3.51 4.78 16 0 -18 3.80 3.72 16 0 -17 7.35 5.67 16 0 -17 10.22 7.86 16 0 -16 -2.59 5.05 16 0 -16 2.25 5.35 16 0 -15 2.71 3.71 16 0 -15 4.91 4.73 16 0 -14 2.85 4.68 16 0 -14 4.33 5.39 16 0 -13 3.67 4.53 16 0 -13 4.32 7.94 16 0 -12 5.28 5.00 16 0 -12 9.94 4.65 16 0 -11 7.52 7.90 16 0 -11 4.93 9.17 16 0 -10 4.90 7.52 16 0 -10 6.89 7.30 16 0 -9 4.70 3.78 16 0 -9 10.59 8.28 16 0 -8 1.00 2.29 16 0 -8 0.91 2.92 16 0 -7 0.31 3.72 -16 0 6 6.88 5.75 16 0 -6 10.11 7.63 -16 0 5 16.50 6.59 16 0 -5 13.89 13.30 -16 0 4 9.86 8.18 16 0 -4 18.24 12.46 -16 0 3 3.95 6.15 16 0 -3 3.84 8.51 -16 0 2 17.17 6.81 16 0 -2 9.77 10.06 -16 0 1 7.03 4.67 16 0 -1 4.45 7.54 -16 0 0 7.44 11.94 16 0 0 6.05 10.96 -16 0 -1 9.49 8.84 16 0 1 3.27 6.29 -16 0 -2 6.18 8.77 16 0 2 0.76 6.32 -16 0 -3 3.32 4.96 16 0 3 3.54 6.85 -16 0 -4 8.99 5.80 16 0 4 11.41 7.18 -16 0 -5 4.70 11.22 16 0 5 9.24 13.14 16 -1 -18 0.87 5.08 16 1 -18 2.07 3.22 16 1 -18 -0.73 4.67 16 -1 -18 5.30 3.28 16 -1 -17 1.93 4.19 16 1 -17 2.35 4.08 16 -1 -17 5.48 5.64 16 1 -17 0.43 4.47 16 -1 -16 7.74 5.57 16 1 -16 9.31 7.27 16 -1 -16 6.15 3.94 16 1 -16 5.27 4.31 16 -1 -15 1.82 5.25 16 1 -15 9.47 9.00 16 -1 -15 5.91 3.71 16 1 -15 6.14 9.51 16 -1 -14 31.33 26.10 16 1 -14 40.67 27.70 16 -1 -14 50.04 24.62 16 1 -14 29.29 36.79 -16 -1 13 44.58 10.46 16 -1 -13 21.03 16.67 16 1 -13 15.65 15.51 16 1 -13 19.37 19.96 16 -1 -13 24.79 13.05 -16 -1 12 19.39 17.12 16 -1 -12 19.45 18.18 16 1 -12 19.43 14.01 16 -1 -12 18.61 13.51 16 1 -12 10.03 11.40 -16 -1 11 27.32 7.61 16 -1 -11 12.69 10.15 16 1 -11 8.16 4.82 16 -1 -11 23.70 17.83 16 1 -11 11.87 13.21 -16 -1 10 13.62 6.20 16 -1 -10 2.82 4.52 16 1 -10 6.31 3.90 16 -1 -10 11.69 8.52 16 1 -10 4.74 6.67 -16 -1 9 12.56 5.88 16 -1 -9 5.39 7.25 16 1 -9 2.54 3.71 16 -1 -9 4.72 6.75 16 1 -9 5.08 5.32 -16 -1 8 -0.15 3.86 16 1 -8 2.86 5.21 16 -1 -8 9.03 10.52 16 1 -8 4.64 6.17 -16 -1 7 1.59 5.93 16 1 -7 0.76 3.69 16 -1 -7 7.77 5.98 16 1 -7 2.85 6.83 -16 -1 6 2.79 4.23 16 -1 -6 6.81 4.45 16 -1 -5 10.85 8.09 16 1 -5 2.90 3.94 -16 -1 4 13.46 9.50 16 -1 -4 2.87 8.38 16 1 -4 9.94 11.01 -16 -1 3 22.92 17.20 16 -1 -3 17.37 17.26 16 1 -3 20.52 9.86 -16 -1 2 10.58 8.97 16 -1 -2 5.35 6.03 16 1 -2 1.73 5.52 -16 -1 1 53.73 11.89 16 -1 -1 31.89 36.75 16 1 -1 58.17 11.28 -16 -1 0 3.67 5.78 16 -1 0 10.70 8.25 16 1 0 12.81 7.15 -16 -1 -1 31.58 25.60 16 -1 1 37.34 25.89 16 1 1 32.03 30.30 -16 -1 -2 8.55 7.52 -16 1 -2 6.69 6.09 16 -1 2 4.51 6.32 16 1 2 8.38 8.50 -16 1 -3 6.52 4.34 -16 -1 -3 0.74 2.80 16 -1 3 5.02 6.47 16 1 3 0.85 5.09 -16 1 -4 3.01 3.18 -16 -1 -4 4.01 6.14 16 -1 4 -2.93 6.91 16 1 4 2.66 8.20 -16 -1 -5 7.04 5.33 -16 1 -5 2.96 4.11 16 -1 5 7.30 12.07 16 1 5 5.38 6.71 -16 -2 17 6.48 4.78 16 -2 -17 -4.40 5.76 16 2 -17 -2.44 5.78 16 -2 -17 7.50 5.99 16 2 -17 5.71 6.94 -16 -2 16 16.98 16.61 16 -2 -16 20.02 20.76 16 2 -16 12.85 15.51 16 -2 -16 24.59 12.35 16 2 -16 9.15 7.78 -16 -2 15 4.91 6.87 16 -2 -15 2.17 4.90 16 2 -15 1.27 4.91 16 -2 -15 1.13 4.42 16 2 -15 -0.04 3.72 -16 -2 14 38.84 7.99 16 -2 -14 15.36 17.79 16 2 -14 10.53 7.85 16 -2 -14 16.51 12.56 16 2 -14 17.16 14.38 -16 -2 13 10.63 7.32 16 -2 -13 0.08 4.91 16 2 -13 3.09 2.95 16 -2 -13 5.40 5.99 16 2 -13 3.25 3.24 16 -2 -12 13.35 13.62 16 2 -12 18.67 12.72 16 -2 -12 16.24 11.19 16 2 -12 21.98 11.42 -16 -2 11 5.14 11.86 16 -2 -11 5.85 6.14 16 2 -11 6.91 6.02 16 -2 -11 4.72 6.85 16 2 -11 3.59 3.93 -16 -2 10 13.24 8.04 16 -2 -10 1.89 3.08 16 2 -10 -4.07 4.15 16 -2 -10 6.75 5.51 16 2 -10 1.51 3.55 -16 -2 9 13.33 18.25 16 2 -9 18.84 12.12 16 -2 -9 15.20 14.28 16 2 -9 20.21 10.82 16 2 -8 3.18 2.21 16 -2 -8 9.89 11.48 16 2 -8 6.63 9.83 -16 -2 7 17.62 17.33 16 2 -7 16.61 8.49 16 -2 -7 24.54 16.17 16 2 -7 19.40 14.52 -16 -2 6 6.05 6.18 16 2 -6 3.16 3.52 16 -2 -6 3.56 8.35 16 2 -6 1.73 5.94 -16 -2 5 7.44 13.68 16 -2 -5 9.59 9.63 16 2 -5 14.20 9.28 -16 -2 4 -0.61 5.49 16 -2 -4 1.59 8.82 16 2 -4 -0.76 5.48 -16 -2 3 3.74 7.41 16 -2 -3 2.52 6.95 16 2 -3 1.48 5.72 -16 -2 2 25.01 9.02 16 -2 -2 28.66 20.36 16 2 -2 36.02 18.80 -16 -2 1 9.00 8.33 16 -2 -1 7.27 6.38 16 2 -1 6.85 5.16 -16 -2 0 13.48 14.37 16 -2 0 16.69 12.35 16 2 0 22.64 13.52 -16 -2 -1 15.94 9.82 16 -2 1 4.25 5.56 16 2 1 7.64 6.62 -16 -2 -2 24.84 19.19 16 -2 2 19.24 11.72 16 2 2 17.38 12.67 -16 -2 -3 21.34 9.85 16 -2 3 11.94 14.20 16 2 3 4.79 8.28 -16 -2 -4 32.55 25.54 16 -2 4 11.24 17.08 16 2 4 37.24 18.53 -16 -3 15 1.34 5.90 16 -3 -15 3.04 4.17 16 3 -15 5.86 5.17 16 -3 -15 4.68 6.05 16 3 -15 6.84 7.79 -16 -3 14 7.85 7.04 16 -3 -14 3.13 4.92 16 3 -14 -1.05 4.70 16 -3 -14 6.16 5.89 16 3 -14 0.02 5.03 -16 -3 13 29.97 8.68 16 -3 -13 11.36 10.10 16 3 -13 9.55 8.26 16 -3 -13 11.24 14.14 16 3 -13 6.69 5.32 16 -3 -12 0.28 2.91 16 3 -12 2.08 5.58 16 -3 -12 -0.77 6.60 16 3 -12 9.03 7.36 16 3 -11 16.74 12.57 16 -3 -11 23.98 8.21 16 3 -11 15.04 12.34 16 3 -10 3.42 5.74 16 -3 -10 4.52 6.75 16 3 -10 3.78 6.08 16 3 -9 5.67 4.27 16 -3 -9 9.69 6.75 16 3 -9 7.71 10.03 16 3 -8 5.27 5.75 16 -3 -8 7.92 7.17 16 3 -8 4.81 3.34 -16 -3 7 15.86 9.57 16 3 -7 6.52 6.39 16 -3 -7 9.55 9.70 16 3 -7 6.28 3.72 -16 -3 6 2.69 5.87 16 3 -6 4.63 5.01 16 -3 -6 -1.15 7.68 16 3 -6 2.77 7.51 16 3 -5 3.01 4.72 16 -3 -5 9.53 9.21 16 3 -5 7.01 12.17 16 -3 -4 17.21 15.45 16 3 -4 21.04 18.63 16 -3 -3 7.71 7.07 16 3 -3 15.02 12.06 16 -3 -2 5.17 5.74 16 3 -2 12.36 8.02 -16 -3 1 17.84 9.49 16 -3 -1 8.73 11.73 16 3 -1 7.93 12.00 -16 -3 0 7.83 8.63 16 -3 0 4.61 4.09 16 3 0 5.94 6.99 -16 -3 -1 10.77 9.13 16 -3 1 2.38 4.66 16 3 1 7.38 6.99 -16 -3 -2 3.28 7.35 16 -3 2 3.55 5.59 16 3 2 3.09 6.82 16 4 -11 8.24 5.33 16 -4 -11 7.61 3.88 16 4 -11 12.51 9.06 -16 -4 10 14.11 9.10 16 4 -10 2.64 3.12 16 -4 -10 5.41 6.86 16 4 -10 10.66 6.79 -16 -4 9 9.75 6.54 16 4 -9 0.12 2.78 16 -4 -9 1.94 5.78 16 4 -9 5.14 5.09 16 4 -8 5.65 5.28 16 -4 -8 5.07 6.04 16 4 -8 11.53 9.48 16 4 -7 2.15 3.88 16 -4 -7 8.85 8.36 16 4 -7 7.56 5.32 -16 -4 6 5.17 9.09 16 4 -6 3.47 3.71 16 -4 -6 8.59 8.93 16 4 -6 7.22 3.97 -16 -4 5 -0.97 6.19 16 4 -5 2.75 2.95 16 -4 -5 4.80 6.48 16 4 -5 4.07 4.94 16 -4 -4 7.26 11.02 16 4 -4 3.44 8.89 -16 -4 3 12.46 9.85 16 -4 -3 10.72 16.22 16 4 -3 6.36 10.47 -16 -4 2 11.36 10.35 16 -4 -2 5.81 5.64 16 4 -2 13.33 10.61 17 0 -14 38.36 26.86 17 0 -14 81.90 10.96 17 0 -13 58.66 18.63 17 0 -13 69.75 9.35 17 0 -12 17.62 7.36 17 0 -12 13.86 10.55 17 0 -11 75.21 8.30 17 0 -11 35.56 33.57 17 0 -10 2.74 4.84 17 0 -9 7.12 6.16 17 0 -8 3.85 3.47 17 0 -7 5.01 6.11 17 0 -6 6.46 5.34 17 0 -5 6.18 8.98 17 0 -4 0.62 2.81 17 0 -3 52.33 28.56 17 0 -2 17.44 11.18 17 0 -1 62.00 31.92 17 0 0 23.87 27.69 17 -1 -13 6.51 8.92 17 1 -13 4.10 4.12 17 1 -13 16.00 11.12 17 -1 -13 10.08 10.21 17 -1 -12 5.54 7.15 17 1 -12 2.87 2.07 17 -1 -12 9.79 8.47 17 1 -12 8.97 6.73 17 1 -11 8.36 13.54 17 -1 -11 12.85 14.90 17 1 -11 23.90 10.84 17 1 -10 6.46 7.00 17 -1 -10 15.76 6.96 17 1 -10 8.33 7.09 17 -1 -9 4.31 6.92 17 1 -9 7.13 6.46 -17 -1 8 13.45 8.36 17 -1 -8 1.72 5.52 17 1 -8 8.04 7.09 -17 -1 7 4.87 7.86 17 -1 -7 5.20 5.95 17 1 -7 -0.13 5.56 -17 -1 6 7.88 13.65 17 -1 -6 10.28 8.57 17 1 -6 9.57 7.08 -17 -1 5 7.61 12.12 17 1 -5 13.87 9.10 17 -1 -5 6.72 5.08 17 -1 -4 18.85 17.79 17 1 -4 38.49 23.29 -17 -1 3 3.89 6.63 17 -1 -3 26.88 21.57 17 1 -3 13.02 12.91 -17 -1 2 29.80 25.13 17 -1 -2 20.38 20.81 17 1 -2 37.11 20.62 -17 -1 1 8.34 7.28 17 -1 -1 10.66 8.90 17 1 -1 3.84 3.77 -17 -2 11 4.05 6.28 17 2 -11 4.57 4.86 17 -2 -11 10.17 12.43 17 2 -11 5.51 5.80 -17 -2 10 10.16 7.07 17 2 -10 3.47 3.73 17 -2 -10 3.83 5.13 17 2 -10 2.38 4.38 -17 -2 9 5.36 6.21 17 2 -9 1.89 2.40 17 -2 -9 0.74 6.26 17 2 -9 3.93 3.33 -17 -2 8 1.65 4.33 17 -2 -8 5.30 9.45 17 2 -8 2.31 5.06 -17 -2 7 5.67 8.88 17 -2 -7 3.07 5.26 17 2 -7 7.17 9.33 -17 -2 6 3.36 3.35 17 -2 -6 3.00 3.07 17 2 -6 2.37 5.39 -17 -2 5 1.99 7.91 17 -2 -5 0.00 4.03 17 2 -5 1.95 4.17 -17 -2 4 6.56 5.40 17 -2 -4 1.06 9.44 17 2 -4 4.42 7.48 -17 -2 3 2.04 4.39 17 -2 -3 -2.02 7.85 17 2 -3 -0.10 6.23 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 94088 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 1.0116(3) 0.2148(8) 0.5737(2) 0.0932(18) Uani 1 1 d . . . . . O2 O 1.0090(4) 0.2466(8) 0.4857(2) 0.098(2) Uani 1 1 d . . . . . O3 O 0.8419(3) 0.1259(5) 0.64298(15) 0.0593(11) Uani 1 1 d . . . . . O4 O 0.6794(3) 0.0700(5) 0.61102(15) 0.0598(11) Uani 1 1 d . . . . . O5 O 0.4946(3) 0.4619(6) 0.52457(16) 0.0590(10) Uani 1 1 d . . . . . O6 O 0.5871(3) 0.6719(5) 0.55898(16) 0.0557(10) Uani 1 1 d . . . . . O7 O 0.7681(4) 0.8548(5) 0.47635(16) 0.0673(12) Uani 1 1 d . . . . . O8 O 0.8031(4) 0.8357(4) 0.56788(16) 0.0606(11) Uani 1 1 d . . . . . O9 O 0.8391(3) 0.1409(5) 0.39026(17) 0.0635(11) Uani 1 1 d . . . . . O10 O 0.6761(3) 0.0903(5) 0.38015(15) 0.0563(10) Uani 1 1 d . . . . . O11 O 0.5206(3) 0.4095(6) 0.37321(14) 0.0556(10) Uani 1 1 d . . . . . O12 O 0.5891(3) 0.6527(5) 0.38337(15) 0.0598(10) Uani 1 1 d . . . . . O13 O 0.7452(3) 0.6267(4) 0.94090(15) 0.0537(9) Uani 1 1 d . . . . . O14 O 0.7936(4) 0.6350(4) 1.03217(16) 0.0681(12) Uani 1 1 d . . . . . O15 O 0.5420(3) 0.4713(5) 0.94654(16) 0.0552(10) Uani 1 1 d . . . . . O16 O 0.4723(3) 0.2599(6) 0.97700(17) 0.0607(11) Uani 1 1 d . . . . . O17 O 0.5747(3) -0.1188(5) 0.88540(16) 0.0615(11) Uani 1 1 d . . . . . O18 O 0.7167(3) -0.0848(4) 0.85736(14) 0.0538(9) Uani 1 1 d . . . . . O19 O 1.0184(3) 0.0221(8) 1.0137(2) 0.0920(18) Uani 1 1 d . . . . . O20 O 0.9449(3) -0.0009(7) 0.9247(2) 0.0840(15) Uani 1 1 d . . . . . O21 O 0.6982(3) 0.4277(5) 1.12468(16) 0.0644(11) Uani 1 1 d . . . . . O22 O 0.6334(3) 0.1875(6) 1.13181(15) 0.0624(11) Uani 1 1 d . . . . . O23 O 0.7682(3) -0.1323(5) 1.11993(14) 0.0580(10) Uani 1 1 d . . . . . O24 O 0.9229(3) -0.0954(5) 1.10815(16) 0.0617(11) Uani 1 1 d . . . . . N1 N 0.9754(4) 0.2670(7) 0.5273(2) 0.0661(15) Uani 1 1 d . . . . . N2 N 0.8901(3) 0.3732(5) 0.52155(16) 0.0368(9) Uani 1 1 d . . . . . N3 N 0.7641(3) 0.2201(4) 0.55773(15) 0.0347(8) Uani 1 1 d . . . . . N4 N 0.7613(4) 0.1348(5) 0.60912(16) 0.0448(10) Uani 1 1 d . . . . . N5 N 0.6640(3) 0.4369(4) 0.55585(15) 0.0310(8) Uani 1 1 d . . . . . N6 N 0.5759(3) 0.5302(6) 0.54514(17) 0.0422(9) Uani 1 1 d . . . . . N7 N 0.7737(3) 0.6125(4) 0.51542(14) 0.0317(8) Uani 1 1 d . . . . . N8 N 0.7804(4) 0.7798(5) 0.52043(18) 0.0478(10) Uani 1 1 d . . . . . N9 N 0.7563(3) 0.2461(4) 0.45176(14) 0.0319(8) Uani 1 1 d . . . . . N10 N 0.7569(3) 0.1540(5) 0.40270(16) 0.0445(10) Uani 1 1 d . . . . . N11 N 0.6488(3) 0.4666(5) 0.44871(14) 0.0312(8) Uani 1 1 d . . . . . N12 N 0.5820(3) 0.5116(6) 0.39662(15) 0.0432(10) Uani 1 1 d . . . . . N13 N 0.7659(3) 0.3974(4) 0.98930(14) 0.0289(7) Uani 1 1 d . . . . . N14 N 0.7671(3) 0.5657(5) 0.98752(18) 0.0446(10) Uani 1 1 d . . . . . N15 N 0.6171(3) 0.2327(4) 0.94758(14) 0.0291(7) Uani 1 1 d . . . . . N16 N 0.5392(3) 0.3272(5) 0.95748(17) 0.0438(10) Uani 1 1 d . . . . . N17 N 0.7090(3) 0.0106(4) 0.94250(13) 0.0280(7) Uani 1 1 d . . . . . N18 N 0.6613(4) -0.0686(5) 0.89058(15) 0.0428(10) Uani 1 1 d . . . . . N19 N 0.8690(2) 0.1513(5) 0.97969(15) 0.0330(8) Uani 1 1 d . . . . . N20 N 0.9503(4) 0.0482(7) 0.9724(2) 0.0631(14) Uani 1 1 d . . . . . N21 N 0.6931(3) 0.2493(4) 1.05485(14) 0.0309(8) Uani 1 1 d . . . . . N22 N 0.6749(3) 0.2899(6) 1.10853(16) 0.0447(10) Uani 1 1 d . . . . . N23 N 0.7918(3) 0.0241(4) 1.04841(14) 0.0307(8) Uani 1 1 d . . . . . N24 N 0.8306(4) -0.0727(5) 1.09659(16) 0.0455(10) Uani 1 1 d . . . . . C1 C 0.8350(3) 0.3610(5) 0.56612(17) 0.0327(9) Uani 1 1 d . . . . . H1 H 0.884488 0.354318 0.603659 0.039 Uiso 1 1 calc R . . . . C2 C 0.8267(3) 0.3842(6) 0.46449(17) 0.0316(9) Uani 1 1 d . . . . . H2 H 0.870416 0.393222 0.436343 0.038 Uiso 1 1 calc R . . . . C3 C 0.7539(3) 0.5362(5) 0.46150(17) 0.0299(9) Uani 1 1 d . . . . . H3 H 0.763122 0.613639 0.431519 0.036 Uiso 1 1 calc R . . . . C4 C 0.7655(3) 0.5150(5) 0.56300(16) 0.0288(9) Uani 1 1 d . . . . . H4 H 0.783505 0.578612 0.598795 0.035 Uiso 1 1 calc R . . . . C5 C 0.6630(3) 0.2804(6) 0.52825(17) 0.0329(9) Uani 1 1 d . . . . . H5 H 0.606577 0.209857 0.535537 0.039 Uiso 1 1 calc R . . . . C6 C 0.6577(3) 0.2952(5) 0.46233(17) 0.0320(9) Uani 1 1 d . . . . . H6 H 0.599283 0.231303 0.439331 0.038 Uiso 1 1 calc R . . . . C7 C 0.7136(3) 0.3062(5) 0.94088(17) 0.0276(9) Uani 1 1 d . . . . . H7 H 0.702495 0.373031 0.905811 0.033 Uiso 1 1 calc R . . . . C8 C 0.7895(3) 0.3143(5) 1.04237(17) 0.0287(9) Uani 1 1 d . . . . . H8 H 0.826297 0.386992 1.073262 0.034 Uiso 1 1 calc R . . . . C9 C 0.8546(3) 0.1598(5) 1.03753(16) 0.0298(9) Uani 1 1 d . . . . . H9 H 0.922313 0.162612 1.065512 0.036 Uiso 1 1 calc R . . . . C10 C 0.7761(3) 0.1488(5) 0.93543(17) 0.0316(9) Uani 1 1 d . . . . . H10 H 0.793365 0.144125 0.897666 0.038 Uiso 1 1 calc R . . . . C11 C 0.6356(3) 0.0715(5) 0.97295(17) 0.0290(9) Uani 1 1 d . . . . . H11 H 0.571258 0.005129 0.965103 0.035 Uiso 1 1 calc R . . . . C12 C 0.6856(3) 0.0808(6) 1.03852(17) 0.0313(9) Uani 1 1 d . . . . . H12 H 0.645022 0.017184 1.060823 0.038 Uiso 1 1 calc R . . . . O25 O 0.8170(4) 0.4999(6) 0.68320(15) 0.0781(14) Uani 1 1 d D . . . . N25 N 0.8506(5) 0.5087(8) 0.7783(2) 0.0503(15) Uani 0.761(9) 1 d D . P A 1 C13 C 0.7719(5) 0.7516(8) 0.7270(3) 0.0717(18) Uani 1 1 d D . . . . H13A H 0.723511 0.775407 0.691163 0.108 Uiso 0.749(11) 1 calc GR . P A 1 H13B H 0.829531 0.828131 0.732715 0.108 Uiso 0.749(11) 1 calc GR . P A 1 H13C H 0.736644 0.761927 0.757885 0.108 Uiso 0.749(11) 1 calc GR . P A 1 H13D H 0.799434 0.856528 0.742150 0.108 Uiso 0.239(9) 1 calc GR . P A 2 H13E H 0.698195 0.746557 0.726052 0.108 Uiso 0.239(9) 1 calc GR . P A 2 H13F H 0.782274 0.738752 0.688709 0.108 Uiso 0.239(9) 1 calc GR . P A 2 C14 C 0.8129(6) 0.5781(9) 0.7256(3) 0.0520(19) Uani 0.749(11) 1 d D . P A 1 C15 C 0.8938(5) 0.3476(7) 0.7772(3) 0.0667(17) Uani 1 1 d D . . . . H15A H 0.880470 0.308631 0.738289 0.100 Uiso 0.761(9) 1 calc GR . P A 1 H15B H 0.861820 0.273898 0.799728 0.100 Uiso 0.761(9) 1 calc GR . P A 1 H15C H 0.968223 0.351539 0.792994 0.100 Uiso 0.761(9) 1 calc GR . P A 1 H15D H 0.845722 0.310334 0.799501 0.100 Uiso 0.251(11) 1 calc GR . P A 2 H15E H 0.957493 0.385194 0.802581 0.100 Uiso 0.251(11) 1 calc GR . P A 2 H15F H 0.909405 0.258040 0.754185 0.100 Uiso 0.251(11) 1 calc GR . P A 2 C16 C 0.8523(5) 0.6001(9) 0.8292(2) 0.0704(17) Uani 1 1 d D U . . . H16A H 0.870164 0.712995 0.823622 0.106 Uiso 0.761(9) 1 calc GR . P A 1 H16B H 0.903569 0.553398 0.860485 0.106 Uiso 0.761(9) 1 calc GR . P A 1 H16C H 0.784174 0.595641 0.837915 0.106 Uiso 0.761(9) 1 calc GR . P A 1 H16D H 0.841894 0.704259 0.846314 0.106 Uiso 0.239(9) 1 calc GR . P A 2 H16E H 0.924044 0.565935 0.842576 0.106 Uiso 0.239(9) 1 calc GR . P A 2 H16F H 0.806669 0.518695 0.839780 0.106 Uiso 0.239(9) 1 calc GR . P A 2 O26 O 0.6496(4) 0.2695(5) 0.82418(14) 0.0694(13) Uani 1 1 d D . . . . N26 N 0.5747(4) 0.4382(6) 0.75483(17) 0.0558(12) Uani 1 1 d D . . . . C17 C 0.6400(5) 0.1752(10) 0.7308(2) 0.080(2) Uani 1 1 d D . . . . H17A H 0.684545 0.223962 0.708517 0.120 Uiso 1 1 calc GR . . . . H17B H 0.574150 0.144620 0.705945 0.120 Uiso 1 1 calc GR . . . . H17C H 0.673506 0.078612 0.750117 0.120 Uiso 1 1 calc GR . . . . C18 C 0.6214(4) 0.2955(7) 0.77379(19) 0.0539(14) Uani 1 1 d D . . . . C19 C 0.5499(5) 0.5531(8) 0.7956(3) 0.0713(18) Uani 1 1 d D . . . . H19A H 0.550761 0.496872 0.831103 0.107 Uiso 1 1 calc GR . . . . H19B H 0.481268 0.598811 0.780633 0.107 Uiso 1 1 calc GR . . . . H19C H 0.600934 0.640444 0.802363 0.107 Uiso 1 1 calc GR . . . . C20 C 0.5379(6) 0.4722(10) 0.6951(2) 0.083(2) Uani 1 1 d D . . . . H20A H 0.546770 0.587677 0.688232 0.124 Uiso 1 1 calc GR . . . . H20B H 0.464868 0.443778 0.683273 0.124 Uiso 1 1 calc GR . . . . H20C H 0.577409 0.408148 0.673560 0.124 Uiso 1 1 calc GR . . . . O27 O 0.7460(3) 0.4601(5) 0.34451(14) 0.0553(10) Uani 1 1 d . . . . . N27 N 0.7139(6) 0.6363(10) 0.2760(3) 0.0564(18) Uani 0.630(8) 1 d D U P B 1 C21 C 0.6206(7) 0.3833(10) 0.2571(3) 0.095(3) Uani 1 1 d . U . . . H21A H 0.652534 0.330230 0.229442 0.142 Uiso 0.650(12) 1 calc GR . P B 1 H21B H 0.564009 0.452587 0.237468 0.142 Uiso 0.650(12) 1 calc GR . P B 1 H21C H 0.593706 0.300967 0.278855 0.142 Uiso 0.650(12) 1 calc GR . P B 1 H21D H 0.547362 0.376142 0.257317 0.142 Uiso 0.370(8) 1 calc GR . P B 2 H21E H 0.661395 0.327365 0.290177 0.142 Uiso 0.370(8) 1 calc GR . P B 2 H21F H 0.632287 0.332403 0.222798 0.142 Uiso 0.370(8) 1 calc GR . P B 2 C23 C 0.6495(7) 0.6901(9) 0.2189(3) 0.087(2) Uani 1 1 d D . . . . H23A H 0.601354 0.774895 0.224329 0.131 Uiso 0.630(8) 1 calc GR . P B 1 H23B H 0.610812 0.597399 0.199692 0.131 Uiso 0.630(8) 1 calc GR . P B 1 H23C H 0.694966 0.732436 0.195905 0.131 Uiso 0.630(8) 1 calc GR . P B 1 H23D H 0.696623 0.664894 0.194590 0.131 Uiso 0.370(8) 1 calc GR . P B 2 H23E H 0.669761 0.792774 0.238390 0.131 Uiso 0.370(8) 1 calc GR . P B 2 H23F H 0.579140 0.699163 0.195863 0.131 Uiso 0.370(8) 1 calc GR . P B 2 C24 C 0.7854(6) 0.7481(9) 0.3128(3) 0.084(2) Uani 1 1 d D . . . . H24A H 0.840193 0.779780 0.294269 0.126 Uiso 0.630(8) 1 calc GR . P B 1 H24B H 0.815595 0.694085 0.348552 0.126 Uiso 0.630(8) 1 calc GR . P B 1 H24C H 0.747764 0.844705 0.320080 0.126 Uiso 0.630(8) 1 calc GR . P B 1 H24D H 0.736789 0.835889 0.298872 0.126 Uiso 0.350(12) 1 calc GR . P B 2 H24E H 0.839446 0.746790 0.291593 0.126 Uiso 0.350(12) 1 calc GR . P B 2 H24F H 0.816431 0.765363 0.352854 0.126 Uiso 0.350(12) 1 calc GR . P B 2 O28 O 0.8840(3) 0.2283(5) 0.15814(14) 0.0591(10) Uani 1 1 d D . . . . N28 N 0.9266(6) 0.2584(10) 0.2535(3) 0.0538(17) Uani 0.592(8) 1 d D U P C 1 C25 C 0.9568(7) 0.4912(9) 0.1989(3) 0.094(3) Uani 1 1 d D . . . . H25A H 1.029235 0.491988 0.219137 0.141 Uiso 0.524(10) 1 calc GR . P C 1 H25B H 0.917244 0.563514 0.217805 0.141 Uiso 0.524(10) 1 calc GR . P C 1 H25C H 0.951144 0.528351 0.160113 0.141 Uiso 0.524(10) 1 calc GR . P C 1 H25D H 0.936897 0.595182 0.212561 0.141 Uiso 0.408(8) 1 calc GR . P C 2 H25E H 0.914989 0.470772 0.160888 0.141 Uiso 0.408(8) 1 calc GR . P C 2 H25F H 1.029724 0.494404 0.197807 0.141 Uiso 0.408(8) 1 calc GR . P C 2 C26 C 0.9167(9) 0.3294(13) 0.1981(3) 0.050(2) Uani 0.524(10) 1 d D U P C 1 C27 C 0.8818(6) 0.0943(8) 0.2521(3) 0.084(2) Uani 1 1 d D . . . . H27A H 0.812896 0.101347 0.259643 0.126 Uiso 0.592(8) 1 calc GR . P C 1 H27B H 0.925818 0.026772 0.280949 0.126 Uiso 0.592(8) 1 calc GR . P C 1 H27C H 0.877111 0.046005 0.214930 0.126 Uiso 0.592(8) 1 calc GR . P C 1 H27D H 0.836636 0.138099 0.275015 0.126 Uiso 0.476(10) 1 calc GR . P C 2 H27E H 0.947384 0.061113 0.276772 0.126 Uiso 0.476(10) 1 calc GR . P C 2 H27F H 0.848816 0.000401 0.230843 0.126 Uiso 0.476(10) 1 calc GR . P C 2 C28 C 0.9697(5) 0.3565(9) 0.3031(2) 0.0699(18) Uani 1 1 d D . . . . H28A H 0.995225 0.459050 0.291313 0.105 Uiso 0.592(8) 1 calc GR . P C 1 H28B H 1.026653 0.297841 0.327574 0.105 Uiso 0.592(8) 1 calc GR . P C 1 H28C H 0.916218 0.378519 0.323726 0.105 Uiso 0.592(8) 1 calc GR . P C 1 H28D H 1.028327 0.283615 0.316005 0.105 Uiso 0.408(8) 1 calc GR . P C 2 H28E H 0.911271 0.319355 0.317840 0.105 Uiso 0.408(8) 1 calc GR . P C 2 H28F H 0.988876 0.466403 0.316732 0.105 Uiso 0.408(8) 1 calc GR . P C 2 N25A N 0.8270(15) 0.618(3) 0.7638(8) 0.0503(15) Uani 0.239(9) 1 d . . P A 2 C14A C 0.8436(19) 0.491(3) 0.7379(9) 0.0520(19) Uani 0.251(11) 1 d D . P A 2 C26A C 0.9026(10) 0.2306(16) 0.2092(5) 0.050(2) Uani 0.476(10) 1 d . . P C 2 N28A N 0.9393(9) 0.3569(17) 0.2380(5) 0.0538(17) Uani 0.408(8) 1 d . . P C 2 C22 C 0.7039(7) 0.4904(12) 0.2983(3) 0.0468(19) Uani 0.650(12) 1 d . . P B 1 N27A N 0.6537(12) 0.5662(16) 0.2586(5) 0.0564(18) Uani 0.370(8) 1 d . . P B 2 C22A C 0.7255(15) 0.579(2) 0.3049(7) 0.0468(19) Uani 0.350(12) 1 d . . P B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.053(3) 0.127(5) 0.090(3) 0.004(3) -0.004(2) 0.046(3) O2 0.057(3) 0.150(5) 0.091(4) -0.032(4) 0.023(2) 0.040(3) O3 0.087(3) 0.041(2) 0.0389(18) 0.0041(16) -0.0090(19) 0.016(2) O4 0.078(3) 0.058(3) 0.051(2) 0.0184(19) 0.033(2) 0.007(2) O5 0.0337(18) 0.074(3) 0.072(3) -0.003(2) 0.0183(17) 0.0047(19) O6 0.061(2) 0.044(2) 0.065(2) -0.0057(19) 0.0199(18) 0.0205(19) O7 0.118(4) 0.0297(19) 0.054(2) 0.0080(17) 0.020(2) -0.005(2) O8 0.102(3) 0.0308(19) 0.052(2) -0.0154(16) 0.023(2) -0.007(2) O9 0.079(3) 0.056(3) 0.068(2) -0.021(2) 0.044(2) 0.001(2) O10 0.070(2) 0.054(2) 0.0422(19) -0.0186(17) 0.0080(18) -0.019(2) O11 0.0386(18) 0.085(3) 0.0366(18) 0.0100(19) -0.0060(15) -0.008(2) O12 0.061(2) 0.062(3) 0.053(2) 0.027(2) 0.0067(18) 0.015(2) O13 0.084(3) 0.0302(18) 0.047(2) 0.0089(15) 0.0140(18) 0.0001(18) O14 0.123(4) 0.0298(19) 0.048(2) -0.0108(17) 0.012(2) -0.008(2) O15 0.057(2) 0.038(2) 0.073(2) 0.0083(19) 0.0212(19) 0.0212(18) O16 0.0355(19) 0.068(3) 0.085(3) 0.007(2) 0.0272(19) 0.0064(19) O17 0.058(2) 0.061(3) 0.058(2) -0.024(2) -0.0029(19) -0.014(2) O18 0.088(3) 0.0383(19) 0.0366(17) -0.0074(15) 0.0175(18) 0.0095(19) O19 0.045(2) 0.136(5) 0.091(3) 0.020(3) 0.008(2) 0.054(3) O20 0.072(3) 0.107(4) 0.083(3) -0.014(3) 0.040(2) 0.040(3) O21 0.095(3) 0.050(2) 0.059(2) -0.0254(19) 0.038(2) -0.009(2) O22 0.075(3) 0.079(3) 0.0440(19) -0.014(2) 0.0357(19) -0.025(2) O23 0.091(3) 0.044(2) 0.0394(18) 0.0167(16) 0.0156(19) -0.012(2) O24 0.057(2) 0.051(2) 0.061(2) 0.0153(19) -0.0198(19) 0.0048(19) N1 0.035(2) 0.080(4) 0.078(4) -0.014(3) 0.003(2) 0.021(3) N2 0.0201(16) 0.040(2) 0.050(2) -0.0056(18) 0.0072(15) 0.0042(16) N3 0.044(2) 0.0280(18) 0.0294(18) 0.0036(14) 0.0037(16) 0.0081(16) N4 0.073(3) 0.031(2) 0.0303(19) 0.0033(17) 0.011(2) 0.015(2) N5 0.0288(17) 0.0317(19) 0.0346(18) 0.0015(15) 0.0115(14) 0.0047(15) N6 0.041(2) 0.046(2) 0.044(2) 0.0034(19) 0.0192(18) 0.0121(19) N7 0.043(2) 0.0175(16) 0.0361(19) -0.0003(14) 0.0123(16) -0.0001(15) N8 0.069(3) 0.0222(19) 0.055(3) -0.0037(19) 0.020(2) 0.0008(19) N9 0.037(2) 0.0293(19) 0.0311(18) -0.0068(15) 0.0110(15) 0.0010(16) N10 0.060(3) 0.039(2) 0.037(2) -0.0087(18) 0.0159(19) -0.001(2) N11 0.0287(17) 0.0339(19) 0.0293(17) 0.0049(15) 0.0033(14) 0.0011(15) N12 0.037(2) 0.062(3) 0.0311(19) 0.010(2) 0.0085(16) 0.009(2) N13 0.0378(19) 0.0182(16) 0.0305(17) -0.0001(13) 0.0077(14) -0.0030(14) N14 0.065(3) 0.0236(19) 0.045(2) -0.0029(17) 0.012(2) -0.0045(19) N15 0.0266(17) 0.0282(18) 0.0320(17) -0.0013(14) 0.0059(14) 0.0051(14) N16 0.032(2) 0.048(3) 0.050(2) -0.0044(19) 0.0060(18) 0.0139(18) N17 0.0337(18) 0.0219(17) 0.0273(16) -0.0048(14) 0.0047(14) 0.0017(14) N18 0.066(3) 0.030(2) 0.0293(19) -0.0030(16) 0.0038(19) 0.011(2) N19 0.0261(17) 0.036(2) 0.0396(19) 0.0031(16) 0.0125(15) 0.0093(15) N20 0.049(3) 0.075(4) 0.072(3) -0.001(3) 0.027(3) 0.031(3) N21 0.0380(19) 0.0300(19) 0.0288(17) -0.0058(14) 0.0161(15) -0.0023(15) N22 0.051(2) 0.054(3) 0.034(2) -0.0140(19) 0.0196(19) -0.006(2) N23 0.0332(18) 0.0274(18) 0.0293(17) 0.0084(15) 0.0026(14) -0.0004(15) N24 0.063(3) 0.032(2) 0.0316(19) 0.0027(16) -0.0096(19) -0.003(2) C1 0.033(2) 0.031(2) 0.031(2) -0.0027(18) -0.0002(17) 0.0076(18) C2 0.025(2) 0.035(2) 0.037(2) -0.0041(19) 0.0122(17) -0.0003(18) C3 0.031(2) 0.026(2) 0.034(2) 0.0023(17) 0.0104(17) -0.0014(17) C4 0.036(2) 0.0235(19) 0.0268(19) -0.0041(16) 0.0069(17) 0.0023(17) C5 0.033(2) 0.031(2) 0.035(2) -0.0001(18) 0.0092(18) -0.0001(18) C6 0.031(2) 0.031(2) 0.033(2) -0.0002(18) 0.0051(17) -0.0056(18) C7 0.032(2) 0.023(2) 0.0282(19) -0.0013(16) 0.0071(17) 0.0033(16) C8 0.031(2) 0.027(2) 0.0277(19) -0.0034(16) 0.0060(17) -0.0044(17) C9 0.0227(19) 0.032(2) 0.033(2) 0.0063(18) 0.0042(16) 0.0008(17) C10 0.041(2) 0.026(2) 0.031(2) -0.0016(17) 0.0137(18) 0.0066(19) C11 0.0253(19) 0.029(2) 0.032(2) -0.0002(16) 0.0040(16) -0.0046(17) C12 0.030(2) 0.036(2) 0.028(2) -0.0031(17) 0.0061(16) -0.0057(18) O25 0.125(4) 0.072(3) 0.0297(18) 0.001(2) 0.002(2) 0.030(3) N25 0.050(3) 0.062(4) 0.037(3) -0.004(3) 0.004(2) 0.010(3) C13 0.086(5) 0.059(4) 0.077(4) 0.016(3) 0.034(4) 0.018(4) C14 0.064(5) 0.049(5) 0.042(4) 0.002(4) 0.009(3) -0.002(4) C15 0.071(4) 0.054(4) 0.066(4) 0.001(3) -0.004(3) 0.015(3) C16 0.072(3) 0.082(3) 0.058(3) -0.015(3) 0.015(2) 0.007(3) O26 0.114(4) 0.052(2) 0.0334(19) -0.0017(17) -0.002(2) 0.027(2) N26 0.056(3) 0.055(3) 0.048(2) 0.002(2) -0.004(2) 0.008(2) C17 0.082(4) 0.090(5) 0.053(3) -0.035(4) -0.016(3) 0.025(4) C18 0.058(3) 0.062(4) 0.036(3) -0.010(2) -0.002(2) 0.006(3) C19 0.083(5) 0.048(4) 0.080(4) -0.009(3) 0.014(4) 0.015(3) C20 0.104(5) 0.079(5) 0.047(3) 0.011(3) -0.021(3) 0.003(4) O27 0.069(2) 0.062(2) 0.0375(19) -0.0001(17) 0.0177(17) -0.008(2) N27 0.088(5) 0.047(4) 0.041(4) -0.003(3) 0.027(4) -0.014(3) C21 0.143(6) 0.087(5) 0.064(4) -0.035(4) 0.046(4) -0.053(5) C23 0.148(7) 0.059(4) 0.068(4) 0.022(3) 0.053(4) 0.030(5) C24 0.123(6) 0.059(4) 0.071(4) 0.003(3) 0.023(4) -0.044(4) O28 0.076(3) 0.064(2) 0.0314(17) -0.0022(16) 0.0001(17) -0.020(2) N28 0.063(4) 0.056(5) 0.042(4) -0.011(3) 0.012(3) -0.016(4) C25 0.131(7) 0.049(4) 0.104(6) 0.005(4) 0.032(5) -0.035(4) C26 0.055(4) 0.056(5) 0.035(4) 0.000(4) 0.000(3) -0.010(4) C27 0.118(6) 0.060(4) 0.089(5) 0.020(4) 0.052(5) -0.007(4) C28 0.073(4) 0.088(5) 0.052(3) -0.029(3) 0.019(3) -0.020(4) N25A 0.050(3) 0.062(4) 0.037(3) -0.004(3) 0.004(2) 0.010(3) C14A 0.064(5) 0.049(5) 0.042(4) 0.002(4) 0.009(3) -0.002(4) C26A 0.055(4) 0.056(5) 0.035(4) 0.000(4) 0.000(3) -0.010(4) N28A 0.063(4) 0.056(5) 0.042(4) -0.011(3) 0.012(3) -0.016(4) C22 0.071(5) 0.043(5) 0.032(3) -0.006(4) 0.023(3) -0.009(5) N27A 0.088(5) 0.047(4) 0.041(4) -0.003(3) 0.027(4) -0.014(3) C22A 0.071(5) 0.043(5) 0.032(3) -0.006(4) 0.023(3) -0.009(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 N1 O2 126.3(5) . . ? O1 N1 N2 117.0(5) . . ? O2 N1 N2 116.5(5) . . ? N1 N2 C1 114.7(4) . . ? N1 N2 C2 114.2(4) . . ? C1 N2 C2 116.0(3) . . ? N4 N3 C1 113.9(3) . . ? N4 N3 C5 112.8(4) . . ? C5 N3 C1 106.7(3) . . ? O3 N4 O4 127.8(4) . . ? O3 N4 N3 115.4(5) . . ? O4 N4 N3 116.5(4) . . ? N6 N5 C4 119.9(4) . . ? N6 N5 C5 119.5(4) . . ? C5 N5 C4 110.7(3) . . ? O5 N6 N5 117.2(4) . . ? O6 N6 O5 126.7(4) . . ? O6 N6 N5 116.1(4) . . ? N8 N7 C3 121.0(4) . . ? N8 N7 C4 120.1(3) . . ? C3 N7 C4 117.7(3) . . ? O7 N8 N7 115.8(4) . . ? O8 N8 O7 126.8(4) . . ? O8 N8 N7 117.3(4) . . ? N10 N9 C2 118.0(3) . . ? N10 N9 C6 118.6(3) . . ? C6 N9 C2 107.9(3) . . ? O9 N10 O10 127.7(4) . . ? O9 N10 N9 116.1(4) . . ? O10 N10 N9 116.0(4) . . ? N12 N11 C3 117.1(3) . . ? N12 N11 C6 117.4(4) . . ? C6 N11 C3 107.9(3) . . ? O11 N12 N11 116.9(4) . . ? O12 N12 O11 128.3(4) . . ? O12 N12 N11 114.6(4) . . ? N14 N13 C7 120.3(3) . . ? N14 N13 C8 120.3(3) . . ? C8 N13 C7 117.1(3) . . ? O13 N14 N13 116.2(4) . . ? O14 N14 O13 127.1(4) . . ? O14 N14 N13 116.6(4) . . ? N16 N15 C7 120.5(4) . . ? N16 N15 C11 120.4(4) . . ? C11 N15 C7 110.9(3) . . ? O15 N16 O16 125.7(4) . . ? O15 N16 N15 117.1(4) . . ? O16 N16 N15 117.2(4) . . ? N18 N17 C10 113.9(3) . . ? N18 N17 C11 113.3(3) . . ? C11 N17 C10 106.8(3) . . ? O17 N18 O18 127.1(4) . . ? O17 N18 N17 118.0(4) . . ? O18 N18 N17 114.8(4) . . ? N20 N19 C9 114.8(4) . . ? N20 N19 C10 116.5(4) . . ? C10 N19 C9 116.1(3) . . ? O19 N20 O20 127.1(5) . . ? O19 N20 N19 116.8(5) . . ? O20 N20 N19 116.1(4) . . ? N22 N21 C8 116.2(3) . . ? N22 N21 C12 117.6(3) . . ? C12 N21 C8 107.5(3) . . ? O21 N22 N21 115.5(4) . . ? O22 N22 O21 127.3(4) . . ? O22 N22 N21 117.1(4) . . ? N24 N23 C9 117.9(3) . . ? N24 N23 C12 118.3(4) . . ? C12 N23 C9 107.4(3) . . ? O23 N24 N23 117.2(4) . . ? O24 N24 O23 126.6(4) . . ? O24 N24 N23 116.0(4) . . ? N2 C1 N3 111.6(3) . . ? N2 C1 H1 110.4 . . ? N2 C1 C4 107.7(3) . . ? N3 C1 H1 110.4 . . ? N3 C1 C4 106.2(3) . . ? C4 C1 H1 110.4 . . ? N2 C2 N9 110.9(4) . . ? N2 C2 H2 111.0 . . ? N2 C2 C3 108.1(3) . . ? N9 C2 H2 111.0 . . ? N9 C2 C3 104.5(3) . . ? C3 C2 H2 111.0 . . ? N7 C3 N11 109.4(3) . . ? N7 C3 C2 109.0(3) . . ? N7 C3 H3 111.3 . . ? N11 C3 C2 104.1(3) . . ? N11 C3 H3 111.3 . . ? C2 C3 H3 111.3 . . ? N5 C4 C1 99.7(3) . . ? N5 C4 H4 111.3 . . ? N7 C4 N5 112.8(3) . . ? N7 C4 C1 109.9(3) . . ? N7 C4 H4 111.3 . . ? C1 C4 H4 111.3 . . ? N3 C5 H5 111.2 . . ? N3 C5 C6 110.1(3) . . ? N5 C5 N3 99.6(3) . . ? N5 C5 H5 111.2 . . ? N5 C5 C6 113.0(4) . . ? C6 C5 H5 111.2 . . ? N9 C6 C5 108.9(3) . . ? N9 C6 H6 111.9 . . ? N11 C6 N9 105.1(3) . . ? N11 C6 C5 106.7(3) . . ? N11 C6 H6 111.9 . . ? C5 C6 H6 111.9 . . ? N13 C7 N15 113.5(3) . . ? N13 C7 H7 111.2 . . ? N13 C7 C10 109.6(3) . . ? N15 C7 H7 111.2 . . ? N15 C7 C10 99.4(3) . . ? C10 C7 H7 111.2 . . ? N13 C8 N21 109.7(3) . . ? N13 C8 H8 111.2 . . ? N13 C8 C9 109.4(3) . . ? N21 C8 H8 111.2 . . ? N21 C8 C9 104.0(3) . . ? C9 C8 H8 111.2 . . ? N19 C9 C8 108.0(3) . . ? N19 C9 H9 111.1 . . ? N23 C9 N19 110.2(3) . . ? N23 C9 C8 105.1(3) . . ? N23 C9 H9 111.1 . . ? C8 C9 H9 111.1 . . ? N17 C10 C7 106.3(3) . . ? N17 C10 H10 110.5 . . ? N19 C10 N17 111.2(3) . . ? N19 C10 C7 107.9(3) . . ? N19 C10 H10 110.5 . . ? C7 C10 H10 110.5 . . ? N15 C11 H11 111.3 . . ? N15 C11 C12 111.9(3) . . ? N17 C11 N15 99.6(3) . . ? N17 C11 H11 111.3 . . ? N17 C11 C12 110.9(3) . . ? C12 C11 H11 111.3 . . ? N21 C12 N23 105.1(3) . . ? N21 C12 C11 108.1(3) . . ? N21 C12 H12 111.6 . . ? N23 C12 C11 108.6(3) . . ? N23 C12 H12 111.6 . . ? C11 C12 H12 111.6 . . ? C14 N25 C15 115.0(5) . . ? C14 N25 C16 120.5(6) . . ? C16 N25 C15 124.3(6) . . ? H13A C13 H13B 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? H13D C13 H13E 109.5 . . ? H13D C13 H13F 109.5 . . ? H13E C13 H13F 109.5 . . ? C14 C13 H13A 109.5 . . ? C14 C13 H13B 109.5 . . ? C14 C13 H13C 109.5 . . ? N25A C13 H13D 109.5 . . ? N25A C13 H13E 109.5 . . ? N25A C13 H13F 109.5 . . ? O25 C14 N25 118.9(6) . . ? O25 C14 C13 126.2(6) . . ? N25 C14 C13 114.8(6) . . ? N25 C15 H15A 109.5 . . ? N25 C15 H15B 109.5 . . ? N25 C15 H15C 109.5 . . ? H15A C15 H15B 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? H15D C15 H15E 109.5 . . ? H15D C15 H15F 109.5 . . ? H15E C15 H15F 109.5 . . ? C14A C15 H15D 109.5 . . ? C14A C15 H15E 109.5 . . ? C14A C15 H15F 109.5 . . ? N25 C16 H16A 109.5 . . ? N25 C16 H16B 109.5 . . ? N25 C16 H16C 109.5 . . ? H16A C16 H16B 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? H16D C16 H16E 109.5 . . ? H16D C16 H16F 109.5 . . ? H16E C16 H16F 109.5 . . ? N25A C16 H16D 109.5 . . ? N25A C16 H16E 109.5 . . ? N25A C16 H16F 109.5 . . ? C18 N26 C19 119.1(4) . . ? C18 N26 C20 122.0(5) . . ? C20 N26 C19 118.5(5) . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C18 C17 H17A 109.5 . . ? C18 C17 H17B 109.5 . . ? C18 C17 H17C 109.5 . . ? O26 C18 N26 120.4(5) . . ? O26 C18 C17 121.5(5) . . ? N26 C18 C17 118.0(5) . . ? N26 C19 H19A 109.5 . . ? N26 C19 H19B 109.5 . . ? N26 C19 H19C 109.5 . . ? H19A C19 H19B 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? N26 C20 H20A 109.5 . . ? N26 C20 H20B 109.5 . . ? N26 C20 H20C 109.5 . . ? H20A C20 H20B 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C24 N27 C23 121.6(7) . . ? C22 N27 C23 123.0(7) . . ? C22 N27 C24 115.2(7) . . ? H21A C21 H21B 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? H21D C21 H21E 109.5 . . ? H21D C21 H21F 109.5 . . ? H21E C21 H21F 109.5 . . ? C22 C21 H21A 109.5 . . ? C22 C21 H21B 109.5 . . ? C22 C21 H21C 109.5 . . ? N27A C21 H21D 109.5 . . ? N27A C21 H21E 109.5 . . ? N27A C21 H21F 109.5 . . ? N27 C23 H23A 109.5 . . ? N27 C23 H23B 109.5 . . ? N27 C23 H23C 109.5 . . ? H23A C23 H23B 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? H23D C23 H23E 109.5 . . ? H23D C23 H23F 109.5 . . ? H23E C23 H23F 109.5 . . ? N27A C23 H23D 109.5 . . ? N27A C23 H23E 109.5 . . ? N27A C23 H23F 109.5 . . ? N27 C24 H24A 109.5 . . ? N27 C24 H24B 109.5 . . ? N27 C24 H24C 109.5 . . ? H24A C24 H24B 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? H24D C24 H24E 109.5 . . ? H24D C24 H24F 109.5 . . ? H24E C24 H24F 109.5 . . ? C22A C24 H24D 109.5 . . ? C22A C24 H24E 109.5 . . ? C22A C24 H24F 109.5 . . ? C26 N28 C27 113.6(7) . . ? C26 N28 C28 118.8(7) . . ? C28 N28 C27 127.4(7) . . ? H25A C25 H25B 109.5 . . ? H25A C25 H25C 109.5 . . ? H25B C25 H25C 109.5 . . ? H25D C25 H25E 109.5 . . ? H25D C25 H25F 109.5 . . ? H25E C25 H25F 109.5 . . ? C26 C25 H25A 109.5 . . ? C26 C25 H25B 109.5 . . ? C26 C25 H25C 109.5 . . ? N28A C25 H25D 109.5 . . ? N28A C25 H25E 109.5 . . ? N28A C25 H25F 109.5 . . ? O28 C26 N28 112.8(8) . . ? O28 C26 C25 132.5(8) . . ? C25 C26 N28 114.2(7) . . ? N28 C27 H27A 109.5 . . ? N28 C27 H27B 109.5 . . ? N28 C27 H27C 109.5 . . ? H27A C27 H27B 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? H27D C27 H27E 109.5 . . ? H27D C27 H27F 109.5 . . ? H27E C27 H27F 109.5 . . ? C26A C27 H27D 109.5 . . ? C26A C27 H27E 109.5 . . ? C26A C27 H27F 109.5 . . ? N28 C28 H28A 109.5 . . ? N28 C28 H28B 109.5 . . ? N28 C28 H28C 109.5 . . ? H28A C28 H28B 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? H28D C28 H28E 109.5 . . ? H28D C28 H28F 109.5 . . ? H28E C28 H28F 109.5 . . ? N28A C28 H28D 109.5 . . ? N28A C28 H28E 109.5 . . ? N28A C28 H28F 109.5 . . ? C13 N25A C16 130.0(15) . . ? C14A N25A C13 115.2(17) . . ? C14A N25A C16 114.1(18) . . ? O25 C14A C15 130.4(19) . . ? N25A C14A O25 115.0(19) . . ? N25A C14A C15 114.6(18) . . ? O28 C26A C27 129.3(10) . . ? O28 C26A N28A 122.4(12) . . ? N28A C26A C27 108.2(9) . . ? C25 N28A C28 127.3(9) . . ? C26A N28A C25 110.0(10) . . ? C26A N28A C28 122.4(11) . . ? O27 C22 N27 121.0(9) . . ? O27 C22 C21 127.3(8) . . ? N27 C22 C21 111.3(7) . . ? C23 N27A C21 136.0(11) . . ? C22A N27A C21 104.0(13) . . ? C22A N27A C23 116.5(14) . . ? O27 C22A C24 122.0(14) . . ? N27A C22A O27 123.2(16) . . ? N27A C22A C24 114.8(15) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 N1 1.205(7) . ? O2 N1 1.211(6) . ? O3 N4 1.199(6) . ? O4 N4 1.228(6) . ? O5 N6 1.224(6) . ? O6 N6 1.217(6) . ? O7 N8 1.219(5) . ? O8 N8 1.218(5) . ? O9 N10 1.209(5) . ? O10 N10 1.212(5) . ? O11 N12 1.223(6) . ? O12 N12 1.219(6) . ? O13 N14 1.217(5) . ? O14 N14 1.209(5) . ? O15 N16 1.223(6) . ? O16 N16 1.236(6) . ? O17 N18 1.206(6) . ? O18 N18 1.224(5) . ? O19 N20 1.212(6) . ? O20 N20 1.220(6) . ? O21 N22 1.221(6) . ? O22 N22 1.220(6) . ? O23 N24 1.215(6) . ? O24 N24 1.214(6) . ? N1 N2 1.418(6) . ? N2 C1 1.449(6) . ? N2 C2 1.456(6) . ? N3 N4 1.446(5) . ? N3 C1 1.485(6) . ? N3 C5 1.463(6) . ? N5 N6 1.379(5) . ? N5 C4 1.475(6) . ? N5 C5 1.456(6) . ? N7 N8 1.388(5) . ? N7 C3 1.427(5) . ? N7 C4 1.437(5) . ? N9 N10 1.419(5) . ? N9 C2 1.465(6) . ? N9 C6 1.456(6) . ? N11 N12 1.424(5) . ? N11 C3 1.481(5) . ? N11 C6 1.453(6) . ? N13 N14 1.391(5) . ? N13 C7 1.439(5) . ? N13 C8 1.435(5) . ? N15 N16 1.365(5) . ? N15 C7 1.466(5) . ? N15 C11 1.465(6) . ? N17 N18 1.438(5) . ? N17 C10 1.485(6) . ? N17 C11 1.448(5) . ? N19 N20 1.422(5) . ? N19 C9 1.468(5) . ? N19 C10 1.445(6) . ? N21 N22 1.426(5) . ? N21 C8 1.487(5) . ? N21 C12 1.445(6) . ? N23 N24 1.417(5) . ? N23 C9 1.460(6) . ? N23 C12 1.459(5) . ? C1 H1 1.0000 . ? C1 C4 1.566(6) . ? C2 H2 1.0000 . ? C2 C3 1.580(6) . ? C3 H3 1.0000 . ? C4 H4 1.0000 . ? C5 H5 1.0000 . ? C5 C6 1.598(6) . ? C6 H6 1.0000 . ? C7 H7 1.0000 . ? C7 C10 1.567(6) . ? C8 H8 1.0000 . ? C8 C9 1.564(6) . ? C9 H9 1.0000 . ? C10 H10 1.0000 . ? C11 H11 1.0000 . ? C11 C12 1.587(6) . ? C12 H12 1.0000 . ? O25 C14 1.232(7) . ? O25 C14A 1.30(2) . ? N25 C14 1.391(8) . ? N25 C15 1.453(7) . ? N25 C16 1.449(7) . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C13 H13D 0.9800 . ? C13 H13E 0.9800 . ? C13 H13F 0.9800 . ? C13 C14 1.536(8) . ? C13 N25A 1.50(2) . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C15 H15D 0.9800 . ? C15 H15E 0.9800 . ? C15 H15F 0.9800 . ? C15 C14A 1.57(2) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C16 H16D 0.9800 . ? C16 H16E 0.9800 . ? C16 H16F 0.9800 . ? C16 N25A 1.56(2) . ? O26 C18 1.219(5) . ? N26 C18 1.363(7) . ? N26 C19 1.467(7) . ? N26 C20 1.454(6) . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C17 C18 1.506(7) . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? O27 C22 1.165(9) . ? O27 C22A 1.358(19) . ? N27 C23 1.526(9) . ? N27 C24 1.475(8) . ? N27 C22 1.341(13) . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C21 H21C 0.9800 . ? C21 H21D 0.9800 . ? C21 H21E 0.9800 . ? C21 H21F 0.9800 . ? C21 C22 1.587(12) . ? C21 N27A 1.572(15) . ? C23 H23A 0.9800 . ? C23 H23B 0.9800 . ? C23 H23C 0.9800 . ? C23 H23D 0.9800 . ? C23 H23E 0.9800 . ? C23 H23F 0.9800 . ? C23 N27A 1.402(14) . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? C24 H24D 0.9800 . ? C24 H24E 0.9800 . ? C24 H24F 0.9800 . ? C24 C22A 1.60(2) . ? O28 C26 1.283(9) . ? O28 C26A 1.213(12) . ? N28 C26 1.449(10) . ? N28 C27 1.479(9) . ? N28 C28 1.461(8) . ? C25 H25A 0.9800 . ? C25 H25B 0.9800 . ? C25 H25C 0.9800 . ? C25 H25D 0.9800 . ? C25 H25E 0.9800 . ? C25 H25F 0.9800 . ? C25 C26 1.438(12) . ? C25 N28A 1.517(15) . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C27 H27C 0.9800 . ? C27 H27D 0.9800 . ? C27 H27E 0.9800 . ? C27 H27F 0.9800 . ? C27 C26A 1.604(14) . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C28 H28D 0.9800 . ? C28 H28E 0.9800 . ? C28 H28F 0.9800 . ? C28 N28A 1.545(13) . ? N25A C14A 1.27(3) . ? C26A N28A 1.290(17) . ? N27A C22A 1.31(2) . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag C1 H1 O25 1.00 2.61 3.138(6) 112.8 . yes C4 H4 O25 1.00 2.11 2.857(5) 130.2 . yes C6 H6 O6 1.00 2.54 3.346(5) 137.0 2_646 yes C7 H7 O26 1.00 2.13 2.795(5) 122.0 . yes C10 H10 O26 1.00 2.53 3.018(5) 109.9 . yes C11 H11 O16 1.00 2.61 3.317(6) 127.6 2_647 yes C17 H17A O4 0.98 2.68 3.206(7) 113.7 . yes C20 H20B O10 0.98 2.46 3.174(8) 129.2 2_656 yes C20 H20B O12 0.98 2.90 3.466(8) 117.8 2_646 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 N1 N2 C1 -21.0(7) . . . . ? O1 N1 N2 C2 -158.3(5) . . . . ? O2 N1 N2 C1 164.0(5) . . . . ? O2 N1 N2 C2 26.7(7) . . . . ? N1 N2 C1 N3 -79.5(5) . . . . ? N1 N2 C1 C4 164.3(4) . . . . ? N1 N2 C2 N9 80.1(5) . . . . ? N1 N2 C2 C3 -165.8(4) . . . . ? N2 C1 C4 N5 122.2(3) . . . . ? N2 C1 C4 N7 3.5(5) . . . . ? N2 C2 C3 N7 -0.1(4) . . . . ? N2 C2 C3 N11 -116.8(3) . . . . ? N3 C1 C4 N5 2.6(4) . . . . ? N3 C1 C4 N7 -116.1(4) . . . . ? N3 C5 C6 N9 -0.9(5) . . . . ? N3 C5 C6 N11 -113.8(4) . . . . ? N4 N3 C1 N2 140.3(4) . . . . ? N4 N3 C1 C4 -102.6(4) . . . . ? N4 N3 C5 N5 87.9(4) . . . . ? N4 N3 C5 C6 -153.2(3) . . . . ? N5 C5 C6 N9 109.5(4) . . . . ? N5 C5 C6 N11 -3.4(5) . . . . ? N6 N5 C4 N7 -56.6(5) . . . . ? N6 N5 C4 C1 -173.2(3) . . . . ? N6 N5 C5 N3 -172.5(3) . . . . ? N6 N5 C5 C6 70.7(5) . . . . ? N8 N7 C3 N11 -109.7(4) . . . . ? N8 N7 C3 C2 137.0(4) . . . . ? N8 N7 C4 N5 111.3(4) . . . . ? N8 N7 C4 C1 -138.4(4) . . . . ? N9 C2 C3 N7 118.1(3) . . . . ? N9 C2 C3 N11 1.5(4) . . . . ? N10 N9 C2 N2 -126.5(4) . . . . ? N10 N9 C2 C3 117.2(4) . . . . ? N10 N9 C6 N11 -105.1(4) . . . . ? N10 N9 C6 C5 140.9(4) . . . . ? N12 N11 C3 N7 126.7(4) . . . . ? N12 N11 C3 C2 -116.9(4) . . . . ? N12 N11 C6 N9 103.6(4) . . . . ? N12 N11 C6 C5 -140.9(3) . . . . ? N13 C7 C10 N17 116.6(3) . . . . ? N13 C7 C10 N19 -2.7(4) . . . . ? N13 C8 C9 N19 -0.5(4) . . . . ? N13 C8 C9 N23 -118.1(3) . . . . ? N14 N13 C7 N15 -107.1(4) . . . . ? N14 N13 C7 C10 142.7(4) . . . . ? N14 N13 C8 N21 105.2(4) . . . . ? N14 N13 C8 C9 -141.3(4) . . . . ? N15 C7 C10 N17 -2.7(4) . . . . ? N15 C7 C10 N19 -122.0(3) . . . . ? N15 C11 C12 N21 3.1(5) . . . . ? N15 C11 C12 N23 -110.3(4) . . . . ? N16 N15 C7 N13 59.6(5) . . . . ? N16 N15 C7 C10 175.9(3) . . . . ? N16 N15 C11 N17 169.7(3) . . . . ? N16 N15 C11 C12 -73.0(5) . . . . ? N17 C11 C12 N21 113.4(4) . . . . ? N17 C11 C12 N23 -0.1(5) . . . . ? N18 N17 C10 N19 -139.6(3) . . . . ? N18 N17 C10 C7 103.3(4) . . . . ? N18 N17 C11 N15 -88.6(4) . . . . ? N18 N17 C11 C12 153.4(3) . . . . ? N20 N19 C9 N23 -83.5(5) . . . . ? N20 N19 C9 C8 162.2(4) . . . . ? N20 N19 C10 N17 82.5(4) . . . . ? N20 N19 C10 C7 -161.4(4) . . . . ? N21 C8 C9 N19 116.7(3) . . . . ? N21 C8 C9 N23 -0.9(4) . . . . ? N22 N21 C8 N13 -127.9(4) . . . . ? N22 N21 C8 C9 115.1(4) . . . . ? N22 N21 C12 N23 -101.3(4) . . . . ? N22 N21 C12 C11 142.9(4) . . . . ? N24 N23 C9 N19 127.5(4) . . . . ? N24 N23 C9 C8 -116.4(4) . . . . ? N24 N23 C12 N21 103.8(4) . . . . ? N24 N23 C12 C11 -140.8(4) . . . . ? C1 N2 C2 N9 -56.6(5) . . . . ? C1 N2 C2 C3 57.5(5) . . . . ? C1 N3 N4 O3 -36.5(5) . . . . ? C1 N3 N4 O4 149.0(4) . . . . ? C1 N3 C5 N5 -37.9(4) . . . . ? C1 N3 C5 C6 81.0(4) . . . . ? C2 N2 C1 N3 57.0(5) . . . . ? C2 N2 C1 C4 -59.2(5) . . . . ? C2 N9 N10 O9 33.9(6) . . . . ? C2 N9 N10 O10 -150.2(4) . . . . ? C2 N9 C6 N11 32.4(4) . . . . ? C2 N9 C6 C5 -81.6(4) . . . . ? C3 N7 N8 O7 0.1(7) . . . . ? C3 N7 N8 O8 -176.1(4) . . . . ? C3 N7 C4 N5 -56.3(5) . . . . ? C3 N7 C4 C1 54.0(5) . . . . ? C3 N11 N12 O11 146.4(4) . . . . ? C3 N11 N12 O12 -38.8(5) . . . . ? C3 N11 C6 N9 -31.3(4) . . . . ? C3 N11 C6 C5 84.2(4) . . . . ? C4 N5 N6 O5 160.5(4) . . . . ? C4 N5 N6 O6 -21.9(6) . . . . ? C4 N5 C5 N3 41.9(4) . . . . ? C4 N5 C5 C6 -74.9(4) . . . . ? C4 N7 N8 O7 -167.0(4) . . . . ? C4 N7 N8 O8 16.8(7) . . . . ? C4 N7 C3 N11 57.8(5) . . . . ? C4 N7 C3 C2 -55.5(5) . . . . ? C5 N3 N4 O3 -158.3(4) . . . . ? C5 N3 N4 O4 27.1(5) . . . . ? C5 N3 C1 N2 -94.6(4) . . . . ? C5 N3 C1 C4 22.5(4) . . . . ? C5 N5 N6 O5 18.1(6) . . . . ? C5 N5 N6 O6 -164.2(4) . . . . ? C5 N5 C4 N7 88.8(4) . . . . ? C5 N5 C4 C1 -27.8(4) . . . . ? C6 N9 N10 O9 167.2(4) . . . . ? C6 N9 N10 O10 -16.9(6) . . . . ? C6 N9 C2 N2 95.7(4) . . . . ? C6 N9 C2 C3 -20.5(4) . . . . ? C6 N11 N12 O11 15.7(6) . . . . ? C6 N11 N12 O12 -169.5(4) . . . . ? C6 N11 C3 N7 -98.3(4) . . . . ? C6 N11 C3 C2 18.2(4) . . . . ? C7 N13 N14 O13 -17.3(6) . . . . ? C7 N13 N14 O14 165.5(4) . . . . ? C7 N13 C8 N21 -57.2(4) . . . . ? C7 N13 C8 C9 56.3(4) . . . . ? C7 N15 N16 O15 18.0(6) . . . . ? C7 N15 N16 O16 -161.7(4) . . . . ? C7 N15 C11 N17 -41.8(4) . . . . ? C7 N15 C11 C12 75.5(4) . . . . ? C8 N13 N14 O13 -179.2(4) . . . . ? C8 N13 N14 O14 3.5(7) . . . . ? C8 N13 C7 N15 55.4(5) . . . . ? C8 N13 C7 C10 -54.8(4) . . . . ? C8 N21 N22 O21 39.1(6) . . . . ? C8 N21 N22 O22 -144.5(4) . . . . ? C8 N21 C12 N23 32.1(4) . . . . ? C8 N21 C12 C11 -83.7(4) . . . . ? C9 N19 N20 O19 -23.8(7) . . . . ? C9 N19 N20 O20 158.1(5) . . . . ? C9 N19 C10 N17 -57.6(5) . . . . ? C9 N19 C10 C7 58.6(5) . . . . ? C9 N23 N24 O23 147.9(4) . . . . ? C9 N23 N24 O24 -36.5(6) . . . . ? C9 N23 C12 N21 -32.8(4) . . . . ? C9 N23 C12 C11 82.6(4) . . . . ? C10 N17 N18 O17 -143.7(4) . . . . ? C10 N17 N18 O18 40.0(5) . . . . ? C10 N17 C11 N15 37.6(4) . . . . ? C10 N17 C11 C12 -80.5(4) . . . . ? C10 N19 N20 O19 -164.3(5) . . . . ? C10 N19 N20 O20 17.6(7) . . . . ? C10 N19 C9 N23 57.2(5) . . . . ? C10 N19 C9 C8 -57.1(5) . . . . ? C11 N15 N16 O15 163.5(4) . . . . ? C11 N15 N16 O16 -16.1(6) . . . . ? C11 N15 C7 N13 -88.9(4) . . . . ? C11 N15 C7 C10 27.4(4) . . . . ? C11 N17 N18 O17 -21.4(5) . . . . ? C11 N17 N18 O18 162.4(4) . . . . ? C11 N17 C10 N19 94.6(4) . . . . ? C11 N17 C10 C7 -22.5(4) . . . . ? C12 N21 N22 O21 168.5(4) . . . . ? C12 N21 N22 O22 -15.1(6) . . . . ? C12 N21 C8 N13 97.9(4) . . . . ? C12 N21 C8 C9 -19.0(4) . . . . ? C12 N23 N24 O23 15.8(6) . . . . ? C12 N23 N24 O24 -168.6(4) . . . . ? C12 N23 C9 N19 -95.7(4) . . . . ? C12 N23 C9 C8 20.4(4) . . . . ? C13 N25A C14A O25 5(3) . . . . ? C13 N25A C14A C15 -175.6(14) . . . . ? C15 N25 C14 O25 1.2(10) . . . . ? C15 N25 C14 C13 -177.2(6) . . . . ? C16 N25 C14 O25 176.6(7) . . . . ? C16 N25 C14 C13 -1.8(10) . . . . ? C16 N25A C14A O25 175.8(15) . . . . ? C16 N25A C14A C15 -5(3) . . . . ? C19 N26 C18 O26 -5.9(9) . . . . ? C19 N26 C18 C17 176.2(6) . . . . ? C20 N26 C18 O26 -178.6(6) . . . . ? C20 N26 C18 C17 3.6(9) . . . . ? C21 N27A C22A O27 -10.8(19) . . . . ? C21 N27A C22A C24 171.6(10) . . . . ? C23 N27 C22 O27 -171.5(7) . . . . ? C23 N27 C22 C21 1.8(11) . . . . ? C23 N27A C22A O27 -173.0(12) . . . . ? C23 N27A C22A C24 9.5(19) . . . . ? C24 N27 C22 O27 3.3(12) . . . . ? C24 N27 C22 C21 176.5(7) . . . . ? O28 C26A N28A C25 -1.6(18) . . . . ? O28 C26A N28A C28 -175.9(10) . . . . ? C27 N28 C26 O28 -9.1(12) . . . . ? C27 N28 C26 C25 178.0(9) . . . . ? C27 C26A N28A C25 -178.1(9) . . . . ? C27 C26A N28A C28 7.6(16) . . . . ? C28 N28 C26 O28 175.9(8) . . . . ? C28 N28 C26 C25 3.0(13) . . . . ?