#------------------------------------------------------------------------------ #$Date: 2020-04-29 01:50:00 +0300 (Wed, 29 Apr 2020) $ #$Revision: 251254 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/04/7240422.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7240422 loop_ _publ_author_name 'Pan, Bochen' 'Wang, Zhanzhong' 'Shen, Yichun' 'Wei, Liangxiao' 'Wei, Hongyuan' 'Dang, Leping' _publ_section_title ; Solvatomorphism and Phase Transformation of CL-20: Probing Properties and Investigating Mechanisms ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D0CE00059K _journal_year 2020 _chemical_formula_moiety 'C6 H6 N12 O12, C6 H10 O4' _chemical_formula_sum 'C12 H16 N12 O16' _chemical_formula_weight 584.37 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _audit_creation_date 2019-07-20 _audit_creation_method ; Olex2 1.2 (compiled 2017.08.10 svn.r3458 for OlexSys, GUI svn.r5381) ; _audit_update_record ; 2019-07-20 deposited with the CCDC. 2020-04-27 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 96.91(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 7.9666(16) _cell_length_b 18.078(4) _cell_length_c 15.915(3) _cell_measurement_reflns_used 6132 _cell_measurement_temperature 113(2) _cell_measurement_theta_max 27.8346 _cell_measurement_theta_min 2.5755 _cell_volume 2275.4(8) _computing_cell_refinement crystalclear _computing_data_collection crystalclear _computing_data_reduction crystalclear _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXS (Sheldrick, 2008)' _diffrn_ambient_temperature 113.15 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'rigaku saturn' _diffrn_measurement_method '\w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0526 _diffrn_reflns_av_unetI/netI 0.0427 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 26987 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.865 _diffrn_reflns_theta_min 2.575 _exptl_absorpt_coefficient_mu 0.159 _exptl_absorpt_correction_T_max 1.0000 _exptl_absorpt_correction_T_min 0.8051 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS (Sheldrick, 1996)' _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.706 _exptl_crystal_description prism _exptl_crystal_F_000 1200 _exptl_crystal_recrystallization_method 'Re-crystallisation from solvent' _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.18 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.271 _refine_diff_density_min -0.240 _refine_diff_density_rms 0.053 _refine_ls_extinction_coef 0.0164(12) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2017/1 (Sheldrick 2017)' _refine_ls_goodness_of_fit_ref 1.027 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 364 _refine_ls_number_reflns 5400 _refine_ls_number_restraints 7 _refine_ls_restrained_S_all 1.028 _refine_ls_R_factor_all 0.0624 _refine_ls_R_factor_gt 0.0443 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0575P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1010 _refine_ls_wR_factor_ref 0.1111 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3957 _reflns_number_total 5400 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d0ce00059k2.cif _cod_data_source_block 1905619 _cod_database_code 7240422 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.981 _shelx_estimated_absorpt_t_min 0.969 _olex2_refinement_description ; 1. Others Fixed Uiso: H1(0.028) H2(0.027) H3(0.026) H4(0.027) H5(0.03) H6(0.03) H7A(0.088) H7B(0.088) H7C(0.088) H8A(0.049) H8B(0.049) H11A(0.052) H11B(0.052) H12A(0.087) H12B(0.087) H12C(0.087) Fixed X: H1(0.40902) H2(0.268094) H3(0.057363) H4(-0.088721) H5(0.496448) H6(0.290594) H7A(-0.004146) H7B(-0.124043) H7C(-0.072758) H8A(-0.347054) H8B(- 0.226736) H11A(-0.275525) H11B(-0.141794) H12A(-0.349752) H12B(-0.483722) H12C(-0.412624) Fixed Y: H1(0.753006) H2(0.65083) H3(0.77986) H4(0.679939) H5(0.586349) H6(0.603202) H7A(0.644406) H7B(0.6493) H7C(0.570323) H8A(0.597282) H8B(0.596984) H11A(0.949189) H11B(0.956647) H12A(0.923012) H12B(0.912372) H12C(0.993071) Fixed Z: H1(0.17004) H2(0.211044) H3(-0.034337) H4(0.00894) H5(0.021576) H6(- 0.095218) H7A(-0.290555) H7B(-0.378592) H7C(-0.337901) H8A(-0.312379) H8B(- 0.224215) H11A(-0.181244) H11B(-0.098174) H12A(-0.013472) H12B(-0.095931) H12C(-0.070196) ; _shelx_res_file ; TITL shelxl in P2(1)/c 1905619.res created by SHELXL-2017/1 at 13:34:44 on 20-Jul-2019 CELL 0.71073 7.9666 18.0781 15.9149 90 96.914 90 ZERR 4 0.0016 0.0036 0.0032 0 0.03 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N O UNIT 48 64 48 64 DELU 0.001 0.001 O12 N12 SIMU 0.01 0.02 2 O12 N12 L.S. 4 PLAN 20 SIZE 0.12 0.18 0.2 TEMP -160 CONF HTAB BOND $H fmap 2 acta OMIT 0 1 1 REM REM REM WGHT 0.057500 EXTI 0.016437 FVAR 0.54769 O1 4 0.338059 0.875527 0.137547 11.00000 0.05676 0.02626 = 0.04086 -0.00307 -0.00924 -0.01108 O2 4 0.165746 0.887885 0.021781 11.00000 0.06723 0.02478 = 0.05281 0.00905 -0.01787 0.00190 O3 4 0.007425 0.600553 0.226749 11.00000 0.05599 0.05370 = 0.02174 -0.00061 0.00958 -0.02452 O4 4 -0.187342 0.625325 0.123731 11.00000 0.02046 0.06913 = 0.07505 0.02659 0.01207 -0.00059 O5 4 0.591216 0.796788 0.044862 11.00000 0.05493 0.05082 = 0.04279 0.00811 0.00395 -0.02848 O6 4 0.621033 0.701562 -0.037071 11.00000 0.03040 0.06596 = 0.04144 0.01474 0.01662 0.00913 O7 4 0.514802 0.501340 0.125602 11.00000 0.03457 0.03256 = 0.06093 0.00960 0.00195 0.01202 O8 4 0.374731 0.533143 0.229554 11.00000 0.05859 0.03140 = 0.02998 0.01092 -0.00427 -0.00805 O9 4 0.203789 0.802248 -0.153337 11.00000 0.04562 0.04156 = 0.03809 0.01901 0.00702 0.00521 O10 4 0.286473 0.695114 -0.195908 11.00000 0.05861 0.05916 = 0.02323 0.00028 0.01428 0.00517 O11 4 0.047734 0.536751 -0.130628 11.00000 0.06814 0.04184 = 0.04598 -0.02321 -0.01124 0.00928 O12 4 -0.155007 0.565022 -0.056357 11.00000 0.03841 0.03481 = 0.06475 -0.00047 -0.00819 -0.01407 O13 4 -0.102956 0.708380 -0.151324 11.00000 0.02705 0.03569 = 0.03197 0.00149 -0.00330 0.00203 O14 4 -0.304758 0.699456 -0.262328 11.00000 0.03103 0.02967 = 0.03355 -0.00266 -0.00579 0.00183 O15 4 -0.419572 0.832249 -0.229739 11.00000 0.04388 0.04343 = 0.04496 -0.00804 -0.01244 0.01477 O16 4 -0.197610 0.849945 -0.130697 11.00000 0.03331 0.03141 = 0.04079 -0.00574 -0.00036 -0.00236 N1 3 0.248335 0.851630 0.076332 11.00000 0.04074 0.02223 = 0.03376 0.00152 0.00020 -0.00379 N2 3 0.230968 0.774469 0.070168 11.00000 0.02772 0.01861 = 0.02480 0.00027 -0.00141 -0.00133 N3 3 0.074760 0.666600 0.116525 11.00000 0.02171 0.02697 = 0.02343 0.00106 0.00634 -0.00234 N4 3 -0.043487 0.626769 0.158581 11.00000 0.03139 0.02945 = 0.03300 -0.00250 0.01496 -0.00300 N5 3 0.565759 0.732825 0.022410 11.00000 0.02185 0.04760 = 0.03153 0.01364 0.00055 -0.00343 N6 3 0.469896 0.690342 0.069853 11.00000 0.01938 0.03043 = 0.02487 0.00620 0.00311 -0.00146 N7 3 0.324511 0.593021 0.106417 11.00000 0.02428 0.02372 = 0.02258 0.00307 0.00019 0.00421 N8 3 0.414665 0.539270 0.158682 11.00000 0.03089 0.02322 = 0.03478 0.00684 -0.00717 -0.00451 N9 3 0.243185 0.737611 -0.143218 11.00000 0.02974 0.04430 = 0.02327 0.00795 0.00333 -0.00032 N10 3 0.249518 0.710684 -0.060064 11.00000 0.02502 0.03021 = 0.01742 0.00449 0.00363 0.00545 N11 3 0.101031 0.611123 -0.019019 11.00000 0.02444 0.02583 = 0.02290 -0.00438 -0.00264 0.00030 N12 3 -0.010747 0.568806 -0.073666 11.00000 0.04172 0.02130 = 0.03873 -0.00241 -0.01074 -0.00107 C1 1 0.349174 0.726396 0.120065 11.00000 0.02492 0.02476 = 0.02074 0.00233 0.00026 -0.00244 AFIX 13 H1 2 0.409020 0.753006 0.170040 11.00000 -1.20000 AFIX 0 C2 1 0.252182 0.656558 0.148091 11.00000 0.02516 0.02202 = 0.01944 -0.00031 0.00241 -0.00275 AFIX 13 H2 2 0.268094 0.650830 0.211044 11.00000 -1.20000 AFIX 0 C3 1 0.135560 0.742746 -0.003917 11.00000 0.01936 0.02379 = 0.02254 0.00198 0.00048 0.00208 AFIX 13 H3 2 0.057363 0.779860 -0.034337 11.00000 -1.20000 AFIX 0 C4 1 0.035695 0.673936 0.025333 11.00000 0.01903 0.02417 = 0.02469 -0.00106 0.00136 0.00061 AFIX 13 H4 2 -0.088721 0.679939 0.008940 11.00000 -1.20000 AFIX 0 C5 1 0.403751 0.619948 0.035215 11.00000 0.02161 0.02897 = 0.02411 0.00198 0.00322 0.00473 AFIX 13 H5 2 0.496448 0.586349 0.021576 11.00000 -1.20000 AFIX 0 C6 1 0.263955 0.631311 -0.044351 11.00000 0.02744 0.02817 = 0.02017 -0.00058 0.00396 0.00676 AFIX 13 H6 2 0.290594 0.603202 -0.095218 11.00000 -1.20000 AFIX 0 C7 1 -0.100193 0.621716 -0.325487 11.00000 0.05109 0.06329 = 0.05902 -0.01854 -0.00327 0.02015 AFIX 137 H7A 2 -0.004146 0.644406 -0.290555 11.00000 -1.50000 H7B 2 -0.124043 0.649300 -0.378592 11.00000 -1.50000 H7C 2 -0.072758 0.570323 -0.337901 11.00000 -1.50000 AFIX 0 C8 1 -0.252561 0.623428 -0.278711 11.00000 0.04276 0.02728 = 0.04774 -0.00515 -0.01153 0.00243 AFIX 23 H8A 2 -0.347054 0.597282 -0.312379 11.00000 -1.20000 H8B 2 -0.226736 0.596984 -0.224215 11.00000 -1.20000 AFIX 0 C9 1 -0.220474 0.733343 -0.197004 11.00000 0.02294 0.03171 = 0.02324 0.00269 0.00338 -0.00141 C10 1 -0.293448 0.811362 -0.187919 11.00000 0.02675 0.03147 = 0.02487 -0.00057 0.00372 -0.00053 C11 1 -0.242351 0.928971 -0.123834 11.00000 0.05077 0.02919 = 0.04918 -0.00521 0.00654 -0.00336 AFIX 23 H11A 2 -0.275525 0.949189 -0.181244 11.00000 -1.20000 H11B 2 -0.141794 0.956647 -0.098174 11.00000 -1.20000 AFIX 0 C12 1 -0.384426 0.940342 -0.071306 11.00000 0.09227 0.03441 = 0.05242 -0.00137 0.02986 0.00487 AFIX 137 H12A 2 -0.349752 0.923012 -0.013472 11.00000 -1.50000 H12B 2 -0.483722 0.912372 -0.095931 11.00000 -1.50000 H12C 2 -0.412624 0.993071 -0.070196 11.00000 -1.50000 AFIX 0 HKLF 4 REM shelxl in P2(1)/c REM R1 = 0.0443 for 3957 Fo > 4sig(Fo) and 0.0624 for all 5400 data REM 364 parameters refined using 7 restraints END WGHT 0.0575 0.0000 REM Instructions for potential hydrogen bonds EQIV $1 x, -y+3/2, z+1/2 HTAB C1 O10_$1 EQIV $2 x+1, -y+3/2, z+1/2 HTAB C1 O14_$2 HTAB C1 O15_$2 HTAB C2 O9_$1 HTAB C2 O15_$2 EQIV $3 x-1, y, z HTAB C4 O6_$3 EQIV $4 -x+1, -y+1, -z HTAB C6 O7_$4 EQIV $5 x-1, -y+3/2, z-1/2 HTAB C7 O5_$5 HTAB C8 O1_$5 EQIV $6 -x, -y+1, -z HTAB C8 O8_$6 HTAB C12 O5_$3 REM Highest difference peak 0.271, deepest hole -0.240, 1-sigma level 0.053 Q1 1 0.0934 0.7071 0.0199 11.00000 0.05 0.27 Q2 1 0.2540 0.6710 -0.0570 11.00000 0.05 0.24 Q3 1 -0.1150 0.9397 -0.0713 11.00000 0.05 0.24 Q4 1 -0.2506 0.7722 -0.1954 11.00000 0.05 0.24 Q5 1 0.1720 0.6181 -0.0193 11.00000 0.05 0.22 Q6 1 0.2331 0.7638 0.0388 11.00000 0.05 0.22 Q7 1 0.0512 0.6640 0.0759 11.00000 0.05 0.21 Q8 1 0.3863 0.8651 0.0942 11.00000 0.05 0.21 Q9 1 -0.1888 0.9560 -0.0439 11.00000 0.05 0.21 Q10 1 0.2941 0.7522 0.0959 11.00000 0.05 0.21 Q11 1 0.2964 0.6920 0.1372 11.00000 0.05 0.20 Q12 1 0.0597 0.6033 -0.0478 11.00000 0.05 0.20 Q13 1 0.2565 0.7966 0.0676 11.00000 0.05 0.20 Q14 1 0.3883 0.7476 0.1433 11.00000 0.05 0.20 Q15 1 0.0626 0.6395 0.0069 11.00000 0.05 0.19 Q16 1 -0.1661 0.6051 -0.3000 11.00000 0.05 0.19 Q17 1 -0.2771 0.6090 -0.2032 11.00000 0.05 0.19 Q18 1 -0.1365 0.6473 0.1645 11.00000 0.05 0.19 Q19 1 0.1362 0.6572 0.1241 11.00000 0.05 0.19 Q20 1 -0.1066 0.6352 -0.3453 11.00000 0.05 0.18 ; _shelx_res_checksum 43741 _shelx_hkl_file ; 0 0 -1 0.09 0.43 0 0 -1 -0.32 0.40 0 0 -2 1347.43 19.18 0 0 2 1410.15 20.05 0 0 2 1258.48 19.02 0 0 -2 1327.70 19.76 0 0 3 0.83 1.83 0 0 -3 0.37 1.42 0 0 3 0.43 1.49 0 0 -3 -0.34 1.30 0 0 4 1421.26 21.85 0 0 4 1383.01 22.67 0 0 -4 1501.08 24.09 0 0 5 0.73 2.55 0 0 -5 0.12 1.58 0 0 5 -0.67 2.79 0 0 -5 0.95 2.09 0 0 6 193.83 7.89 0 0 6 214.37 9.75 0 0 7 0.36 1.36 0 0 7 1.23 2.47 0 0 8 743.68 18.74 0 0 8 794.94 20.29 0 0 9 1.05 1.08 0 0 9 0.88 2.07 0 0 10 1931.65 63.95 0 0 10 1803.32 63.32 0 0 11 2.31 2.75 0 0 11 0.32 3.63 0 0 12 540.09 17.53 0 0 12 556.17 20.15 0 0 13 -0.58 3.16 0 0 13 -0.20 4.82 0 0 14 232.65 12.17 0 0 14 189.38 11.34 0 0 15 1.50 2.56 0 0 15 -3.33 6.05 0 0 16 13.83 9.84 0 0 16 8.86 6.46 0 0 17 1.85 3.26 0 0 17 -1.10 4.92 0 0 18 15.79 10.70 0 0 18 11.48 14.04 0 0 19 2.29 2.79 0 0 19 1.89 4.26 0 0 20 49.83 6.45 0 0 20 34.59 28.43 0 1 1 -0.07 0.34 0 -1 1 -0.20 0.32 0 1 -2 247.34 7.47 0 -1 2 238.65 7.30 0 -1 -2 225.96 6.78 0 1 2 261.32 8.20 0 -1 -2 232.78 7.39 0 -1 2 265.36 8.42 0 1 -2 233.12 7.43 0 1 2 254.38 8.15 0 -1 -2 256.47 8.27 0 1 -2 255.03 8.30 0 -1 2 247.35 9.10 0 1 -3 122.92 3.97 0 1 3 121.15 3.72 0 -1 3 121.78 4.12 0 -1 -3 119.44 3.72 0 1 3 118.66 4.61 0 -1 -3 120.15 4.63 0 -1 3 109.12 4.27 0 1 -3 122.12 4.83 0 1 3 117.96 4.90 0 -1 -3 112.74 4.62 0 -1 3 120.98 5.19 0 1 -3 107.22 4.52 0 1 -4 1721.11 23.40 0 1 4 1602.33 24.18 0 -1 -4 1656.32 25.44 0 -1 4 1589.48 24.50 0 1 -4 1781.39 27.29 0 1 4 1735.07 27.07 0 -1 -4 1752.27 27.33 0 -1 4 1568.15 25.28 0 1 -4 1732.05 27.14 0 1 -5 62.62 3.10 0 1 5 80.10 44.88 0 -1 -5 64.07 4.15 0 -1 5 62.44 4.17 0 1 -5 68.76 4.63 0 1 5 51.39 4.10 0 -1 5 51.09 4.15 0 1 -6 90.79 1.83 0 1 6 74.93 5.90 0 -1 6 87.28 8.92 0 1 -6 107.29 5.73 0 1 6 69.08 5.08 0 -1 6 68.05 5.67 0 1 -7 32.79 1.92 0 1 7 33.20 3.32 0 -1 7 40.32 3.98 0 1 7 43.18 4.55 0 -1 7 35.29 4.22 0 1 -8 236.91 8.99 0 -1 8 265.01 10.00 0 1 8 225.90 10.76 0 -1 8 251.54 11.86 0 1 8 260.72 17.65 0 -1 8 224.95 11.92 0 1 9 27.05 3.18 0 -1 9 28.95 3.45 0 1 9 32.53 5.31 0 -1 9 28.66 4.85 0 1 10 262.23 11.21 0 -1 10 274.77 12.02 0 1 10 247.62 13.08 0 -1 10 264.22 13.30 0 1 11 289.12 19.53 0 -1 11 283.26 12.36 0 1 11 295.75 19.87 0 -1 11 274.97 19.26 0 1 12 0.89 3.51 0 -1 12 2.23 1.55 0 -1 12 -1.26 4.47 0 1 12 3.27 4.56 0 1 13 3.14 2.24 0 -1 13 1.90 2.82 0 1 13 3.44 3.00 0 -1 13 -0.62 4.51 0 1 14 246.37 12.50 0 -1 14 231.71 11.45 0 1 14 248.05 13.77 0 -1 14 237.47 13.95 0 1 15 37.19 5.15 0 -1 15 46.21 17.08 0 1 15 46.67 22.99 0 -1 15 65.54 29.14 0 1 16 65.68 6.57 0 -1 16 81.85 10.81 0 1 16 77.05 8.09 0 -1 16 67.73 8.75 0 1 17 -0.61 4.09 0 -1 17 5.19 4.04 0 1 17 3.77 3.76 0 -1 17 0.87 5.64 0 1 18 69.02 18.16 0 -1 18 56.14 28.27 0 1 18 80.14 21.52 0 -1 18 58.08 26.85 0 -1 19 11.76 10.60 0 1 19 13.09 7.10 0 -1 19 6.54 6.91 0 1 19 13.59 10.70 0 1 20 21.59 11.03 0 -1 20 19.75 17.84 0 -1 20 14.44 16.60 0 1 20 15.08 11.41 0 2 1 878.89 13.27 0 -2 1 924.43 14.92 0 -2 -1 867.85 10.27 0 2 1 913.25 13.29 0 -2 -1 942.31 13.66 0 -2 1 929.14 13.41 0 2 -1 930.15 13.40 0 -2 1 934.58 14.47 0 2 -1 927.45 13.94 0 -2 -1 960.27 13.96 0 2 2 429.98 12.81 0 2 -2 407.23 12.36 0 -2 2 401.75 12.36 0 -2 -2 467.40 14.09 0 2 2 423.59 13.16 0 -2 -2 393.98 12.04 0 -2 2 440.45 13.36 0 2 -2 390.30 11.89 0 2 -2 467.04 14.41 0 -2 -2 405.63 12.46 0 2 2 394.36 12.00 0 2 -3 59.81 3.23 0 2 3 57.28 3.11 0 -2 3 57.29 3.30 0 -2 -3 60.44 3.18 0 2 3 58.65 3.57 0 -2 -3 57.27 3.39 0 -2 3 55.38 3.30 0 2 -3 60.26 3.55 0 -2 -3 53.24 3.25 0 -2 3 61.48 4.15 0 2 -3 53.72 3.71 0 -2 -3 51.92 3.18 0 2 -4 790.37 6.77 0 2 4 772.03 22.28 0 -2 -4 766.57 22.44 0 2 4 771.61 23.66 0 -2 -4 703.45 21.79 0 2 -4 712.44 21.74 0 2 4 773.92 23.95 0 2 -4 714.35 22.35 0 2 -5 2988.52 40.77 0 -2 5 2910.10 40.62 0 -2 -5 2775.22 37.45 0 2 5 2798.52 40.87 0 -2 5 2873.08 41.68 0 2 -5 2967.31 43.05 0 2 5 3044.01 45.12 0 -2 5 2676.19 41.40 0 2 -6 813.56 7.37 0 -2 6 910.23 15.06 0 -2 -6 816.92 4.87 0 2 6 801.42 15.65 0 2 -6 908.12 16.60 0 2 6 843.33 12.74 0 -2 6 857.20 13.98 0 2 -7 2385.38 39.81 0 2 7 2227.89 40.81 0 -2 7 2250.83 41.24 0 2 7 2258.86 44.07 0 -2 7 2471.44 47.22 0 2 -8 296.58 11.54 0 2 8 273.43 12.36 0 -2 8 279.61 12.91 0 2 8 311.37 14.91 0 -2 8 278.18 16.76 0 2 -9 180.26 8.03 0 2 9 178.40 9.58 0 -2 9 222.66 11.94 0 2 9 198.30 12.06 0 -2 9 173.69 11.14 0 2 -10 100.73 6.97 0 -2 10 107.90 7.45 0 2 10 101.04 8.83 0 -2 10 104.35 10.41 0 2 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5 -6 309.95 13.19 0 -5 -6 286.92 14.09 0 5 6 250.31 13.79 0 -5 6 261.85 11.86 0 -5 6 261.47 12.90 0 -5 -6 265.21 12.01 0 5 7 865.13 17.04 0 5 -7 813.30 16.90 0 -5 -7 776.90 16.19 0 5 7 842.06 19.65 0 -5 7 914.24 22.52 0 -5 7 763.91 19.52 0 -5 -7 792.33 18.57 0 5 8 144.36 3.63 0 5 -8 163.51 5.48 0 -5 -8 145.29 4.46 0 5 8 161.98 6.60 0 -5 8 177.83 10.21 0 -5 8 178.53 11.90 0 -5 -8 147.88 7.31 0 5 9 2.27 0.89 0 5 -9 2.67 1.39 0 -5 -9 3.46 1.98 0 5 9 -1.55 2.93 0 -5 9 6.60 4.20 0 -5 9 4.56 3.42 0 -5 -9 9.70 4.61 0 5 10 58.32 2.27 0 5 -10 67.92 4.29 0 -5 -10 56.05 2.34 0 5 10 68.23 12.47 0 -5 10 69.04 5.78 0 -5 10 55.05 6.23 0 -5 -10 50.30 5.14 0 5 11 0.71 0.82 0 5 -11 0.39 1.11 0 5 11 1.83 2.17 0 -5 11 0.00 1.86 0 -5 11 1.92 2.85 0 -5 -11 1.89 1.98 0 5 -12 65.13 3.44 0 5 12 66.79 8.43 0 -5 12 55.66 11.74 0 -5 12 57.79 7.35 0 -5 -12 51.42 22.61 0 5 -13 62.56 6.86 0 5 13 76.06 6.58 0 -5 13 83.73 6.85 0 -5 13 70.71 8.08 0 -5 -13 53.24 18.37 0 5 14 44.02 6.14 0 -5 14 32.91 5.73 0 -5 14 43.28 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28.98 0 -7 2 1824.79 30.22 0 7 3 -1.08 3.52 0 7 -3 0.29 2.07 0 -7 3 -0.07 0.99 0 7 3 0.30 1.34 0 -7 3 1.28 1.90 0 -7 3 -0.30 2.98 0 -7 -3 0.66 2.09 0 7 -4 203.70 10.08 0 7 4 245.54 11.29 0 7 4 205.18 9.95 0 -7 4 223.72 11.24 0 7 -4 197.92 5.16 0 -7 4 225.46 11.36 0 -7 -4 217.62 10.86 0 7 -5 25.73 10.83 0 7 5 28.76 3.33 0 7 5 31.09 11.19 0 -7 5 24.57 2.77 0 -7 5 31.21 4.00 0 -7 -5 22.96 10.53 0 7 6 2.70 3.00 0 7 -6 2.66 2.24 0 7 6 1.44 2.97 0 -7 6 4.77 4.36 0 -7 6 2.07 2.93 0 -7 -6 2.71 3.27 0 7 -7 197.69 10.50 0 7 7 210.28 10.21 0 7 7 220.74 12.16 0 -7 7 194.79 11.63 0 -7 7 214.49 12.52 0 -7 -7 196.53 10.75 0 7 8 1.34 2.38 0 7 -8 4.26 3.00 0 7 8 1.71 2.17 0 -7 8 3.14 2.43 0 -7 8 2.58 3.46 0 -7 -8 10.70 8.55 0 7 9 0.49 1.15 0 7 -9 -0.85 2.67 0 -7 -9 0.59 2.13 0 7 9 7.83 4.44 0 -7 9 1.57 2.46 0 -7 9 7.47 4.32 0 -7 -9 -3.60 4.66 0 7 10 72.39 5.80 0 7 -10 69.00 3.97 0 -7 -10 55.50 3.39 0 7 10 75.06 15.15 0 -7 10 74.66 5.38 0 -7 10 73.62 7.16 0 -7 -10 49.33 5.44 0 7 11 20.60 3.31 0 7 -11 16.41 2.37 0 7 11 20.46 8.78 0 -7 11 22.18 10.23 0 -7 11 21.19 8.68 0 -7 -11 23.81 11.78 0 7 12 6.77 3.55 0 7 -12 9.87 3.13 0 7 12 5.90 4.08 0 -7 12 6.48 4.07 0 -7 12 8.72 7.04 0 -7 -12 7.04 3.33 0 7 -13 33.79 8.45 0 7 13 38.91 17.01 0 -7 13 34.18 18.44 0 -7 13 40.29 28.91 0 -7 -13 60.73 7.70 0 7 14 30.59 17.56 0 -7 14 39.93 8.94 0 -7 14 36.71 22.87 0 -7 -14 25.99 16.12 0 7 15 98.80 9.02 0 -7 15 96.30 7.03 0 -7 15 98.12 22.87 0 -7 -15 96.38 8.50 0 7 16 11.96 9.08 0 -7 16 11.64 5.23 0 -7 16 11.45 6.59 0 -7 -16 11.88 9.27 0 7 17 2.74 3.64 0 -7 17 1.32 4.66 0 -7 17 4.58 5.12 0 -7 -17 -0.48 5.05 0 7 18 3.28 3.33 0 -7 18 -0.87 3.56 0 -7 18 -2.50 6.40 0 -7 -18 3.04 5.60 0 7 19 2.54 4.73 0 -7 19 4.55 7.02 0 -7 -19 3.43 7.71 0 8 0 -0.30 9.87 0 8 0 3.23 2.44 0 -8 0 3.20 4.33 0 8 -1 2231.15 41.98 0 8 1 2184.44 40.27 0 -8 -1 1936.21 36.67 0 8 2 45.05 24.77 0 8 -2 48.63 23.57 0 8 2 37.83 3.75 0 -8 2 55.77 4.16 0 -8 2 53.91 25.72 0 -8 -2 61.79 5.53 0 8 3 2.47 2.06 0 8 -3 9.37 3.51 0 8 3 2.88 2.41 0 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3 171.34 10.55 0 -9 -3 144.30 9.11 0 9 4 452.52 10.10 0 9 -4 431.12 19.84 0 9 4 436.50 22.03 0 -9 4 475.49 17.43 0 -9 4 460.35 18.38 0 -9 -4 454.19 17.44 0 9 -5 -0.35 3.72 0 9 5 1.19 2.29 0 9 5 2.29 3.01 0 -9 5 3.34 2.75 0 -9 5 2.65 2.45 0 -9 -5 2.90 2.85 0 9 6 57.15 4.19 0 9 -6 48.50 4.69 0 9 6 65.43 5.18 0 -9 6 49.51 3.93 0 -9 6 73.43 19.02 0 -9 -6 46.37 8.09 0 9 7 50.96 7.93 0 9 -7 43.77 17.61 0 9 7 52.80 4.93 0 -9 7 51.21 4.95 0 -9 7 49.47 5.47 0 -9 -7 42.83 5.44 0 9 -8 202.39 9.52 0 9 8 203.78 7.99 0 9 8 207.60 9.20 0 -9 8 195.71 12.71 0 -9 8 209.50 11.88 0 -9 -8 170.90 10.43 0 9 9 336.97 13.29 0 9 -9 296.18 10.93 0 9 9 345.21 12.99 0 -9 9 323.28 12.09 0 -9 9 322.17 14.44 0 -9 -9 307.92 12.10 0 9 10 168.75 9.12 0 9 -10 158.44 9.40 0 9 10 156.24 10.37 0 -9 10 190.17 9.01 0 -9 10 175.16 12.93 0 -9 -10 150.99 10.69 0 9 11 18.05 10.24 0 9 -11 14.00 4.75 0 9 11 19.26 11.65 0 -9 11 11.38 8.27 0 -9 11 20.83 8.91 0 -9 -11 7.37 6.39 0 9 -12 63.33 4.89 0 9 12 49.78 4.06 0 9 12 60.86 6.77 0 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286.14 15.80 0 10 -4 530.91 19.78 0 10 4 535.62 19.52 0 10 4 560.32 20.22 0 -10 4 574.00 20.98 0 -10 4 547.75 21.03 0 -10 -4 528.22 19.87 0 10 -5 -1.07 4.15 0 10 5 0.44 2.51 0 10 5 -0.33 2.89 0 -10 5 2.90 4.28 0 -10 5 2.82 3.27 0 -10 -5 5.12 5.53 0 10 6 5.00 3.41 0 10 -6 3.73 2.74 0 10 6 2.61 3.53 0 -10 6 2.82 3.84 0 -10 6 8.02 3.67 0 -10 -6 5.64 2.67 0 10 -7 6.59 7.18 0 10 7 6.59 4.87 0 10 7 5.04 6.04 0 -10 7 6.35 3.52 0 -10 7 4.66 4.75 0 -10 -7 3.78 3.92 0 10 -8 48.14 4.51 0 10 8 52.13 4.35 0 10 8 52.86 21.77 0 -10 8 56.77 5.01 0 -10 8 53.94 21.20 0 -10 -8 51.00 5.88 0 10 9 40.16 5.86 0 10 -9 41.32 15.57 0 10 9 41.47 4.36 0 -10 9 42.97 4.16 0 -10 9 33.19 23.56 0 -10 -9 44.81 21.65 0 10 -10 7.22 4.94 0 10 10 4.44 3.35 0 10 10 0.63 2.44 0 -10 10 4.55 3.40 0 -10 10 3.22 3.91 0 -10 -10 15.15 8.19 0 10 11 41.64 3.56 0 10 -11 47.25 17.27 0 10 11 44.34 5.47 0 -10 11 59.26 5.54 0 -10 11 53.60 26.87 0 -10 -11 41.19 19.87 0 10 12 18.35 10.72 0 10 -12 19.44 10.34 0 10 12 18.24 10.54 0 -10 12 19.57 13.39 0 -10 12 23.84 14.70 0 -10 -12 20.65 11.59 0 10 -13 26.56 13.88 0 10 13 12.52 11.10 0 -10 13 29.56 5.22 0 -10 13 30.16 8.94 0 -10 -13 27.87 16.11 0 10 -14 152.99 9.85 0 10 14 157.14 12.19 0 -10 14 169.18 12.07 0 -10 14 154.36 13.45 0 -10 -14 133.95 11.02 0 10 15 -2.03 4.77 0 -10 15 2.38 3.98 0 -10 15 -1.32 6.15 0 -10 -15 4.97 2.47 0 10 16 7.95 8.74 0 -10 16 7.89 4.64 0 -10 16 12.89 6.60 0 -10 -16 12.94 7.17 0 10 17 41.02 28.04 0 -10 17 62.88 9.18 0 -10 -17 36.46 20.61 0 10 18 2.91 3.22 0 -10 18 2.90 5.49 0 -10 -18 6.14 10.01 0 11 0 -1.20 5.89 0 11 0 -1.91 2.89 0 -11 0 -2.14 5.99 0 11 1 4.91 2.70 0 11 -1 1.75 5.35 0 11 1 2.86 2.19 0 -11 1 3.58 4.12 0 -11 1 5.27 4.64 0 -11 -1 4.48 5.35 0 11 2 276.90 15.55 0 11 -2 278.15 17.11 0 11 2 272.69 13.52 0 -11 2 250.99 12.97 0 -11 2 277.18 20.47 0 -11 -2 244.00 18.45 0 11 3 91.38 8.22 0 11 -3 102.36 9.30 0 11 3 90.11 7.70 0 -11 3 110.46 9.66 0 -11 3 103.41 11.81 0 -11 -3 108.12 10.03 0 11 -4 11.53 6.79 0 11 4 12.76 9.30 0 11 4 12.69 4.88 0 -11 4 13.24 6.72 0 -11 4 11.66 9.28 0 -11 -4 17.70 7.45 0 11 -5 457.62 17.71 0 11 5 475.34 17.62 0 11 5 469.44 16.96 0 -11 5 446.41 18.76 0 -11 5 438.88 18.14 0 -11 -5 427.89 17.34 0 11 6 93.67 7.02 0 11 -6 97.48 18.44 0 11 6 100.34 8.09 0 -11 6 87.69 6.44 0 -11 6 109.89 9.20 0 -11 -6 89.47 7.89 0 11 -7 323.51 14.06 0 11 7 323.35 11.66 0 11 7 363.74 13.67 0 -11 7 341.25 12.90 0 -11 7 328.61 14.44 0 -11 -7 327.62 14.76 0 11 8 234.32 10.14 0 11 -8 224.59 10.54 0 11 8 213.62 10.78 0 -11 8 225.88 10.71 0 -11 8 246.72 33.10 0 -11 -8 193.79 10.96 0 11 9 57.39 4.77 0 11 -9 54.01 5.98 0 11 9 66.68 16.93 0 -11 9 55.48 8.27 0 -11 9 69.26 7.69 0 -11 -9 45.95 21.09 0 11 -10 93.04 11.43 0 11 10 111.82 8.06 0 11 10 126.44 10.50 0 -11 10 116.09 9.15 0 -11 10 91.57 10.08 0 -11 -10 130.17 11.30 0 11 11 77.71 5.04 0 11 -11 71.98 6.59 0 11 11 65.36 6.48 0 -11 11 76.16 6.57 0 -11 11 75.15 20.49 0 -11 -11 76.05 22.51 0 11 12 201.31 13.56 0 11 -12 206.69 22.38 0 11 12 178.40 14.01 0 -11 12 225.39 16.94 0 -11 12 210.47 18.08 0 -11 -12 159.08 10.27 0 11 -13 2.14 2.83 0 11 13 2.82 2.81 0 -11 13 5.56 3.68 0 -11 13 5.60 6.13 0 -11 -13 1.28 3.31 0 11 -14 6.50 5.38 0 11 14 4.37 3.81 0 -11 14 11.79 4.04 0 -11 14 9.83 7.89 0 -11 -14 14.03 8.55 0 11 15 12.86 6.27 0 -11 15 8.19 5.98 0 -11 15 5.67 9.15 0 -11 -15 10.06 10.11 0 11 16 23.24 16.08 0 -11 16 22.37 19.65 0 -11 -16 9.40 10.94 0 11 17 1.77 5.22 0 -11 17 3.10 5.36 0 -11 -17 2.63 6.42 0 11 18 46.90 6.77 0 -11 18 29.58 27.73 0 -11 -18 26.45 19.10 0 12 0 1571.16 49.67 0 12 0 1492.39 47.40 0 -12 0 1456.89 56.12 0 12 1 82.14 8.21 0 12 -1 80.88 8.42 0 12 1 89.47 8.20 0 -12 1 82.47 7.73 0 -12 1 85.82 8.51 0 -12 -1 74.00 6.81 0 12 2 9.35 5.71 0 12 -2 20.49 7.36 0 12 2 17.05 7.15 0 -12 2 14.25 10.79 0 -12 2 11.39 8.67 0 -12 -2 14.67 5.28 0 12 -3 45.09 5.08 0 12 3 48.38 4.71 0 12 3 47.79 4.08 0 -12 3 50.32 4.86 0 -12 3 48.06 5.35 0 -12 -3 59.55 16.66 0 12 4 27.02 4.42 0 12 -4 22.72 10.94 0 12 4 21.72 9.02 0 -12 4 19.30 12.83 0 -12 4 24.56 9.40 0 -12 -4 35.95 16.90 0 12 -5 210.36 10.09 0 12 5 194.81 16.47 0 12 5 169.59 16.92 0 -12 5 203.15 10.86 0 -12 5 186.10 10.12 0 -12 -5 210.77 10.54 0 12 6 211.83 10.29 0 12 -6 198.88 12.25 0 12 6 190.32 8.26 0 -12 6 188.28 8.08 0 -12 6 181.62 12.55 0 -12 -6 199.86 11.22 0 12 7 8.90 7.16 0 12 -7 5.01 2.30 0 12 7 3.18 4.43 0 -12 7 5.74 5.74 0 -12 7 2.68 3.01 0 -12 -7 4.08 4.75 0 12 8 156.79 9.71 0 12 -8 164.83 10.94 0 12 8 150.39 15.22 0 -12 8 148.97 8.25 0 -12 8 145.35 10.13 0 -12 -8 141.32 9.62 0 12 -9 445.64 18.17 0 12 9 457.59 17.20 0 12 9 416.92 18.00 0 -12 9 361.06 16.90 0 -12 9 434.37 20.86 0 -12 -9 402.38 18.63 0 12 10 585.53 35.70 0 12 -10 579.27 38.18 0 12 10 579.48 36.93 0 -12 10 555.87 37.15 0 -12 10 594.08 39.43 0 -12 -10 615.18 39.90 0 12 -11 292.38 20.96 0 12 11 307.46 19.82 0 12 11 297.74 21.00 0 -12 11 279.89 19.72 0 -12 11 295.55 22.86 0 -12 -11 242.54 18.30 0 12 12 0.74 2.78 0 12 -12 -1.93 3.80 0 12 12 -0.83 6.85 0 -12 12 0.08 4.29 0 -12 12 -0.58 6.60 0 -12 -12 4.37 3.54 0 12 -13 26.24 14.69 0 12 13 26.73 16.07 0 -12 13 28.24 12.59 0 -12 13 32.99 15.62 0 -12 -13 25.90 15.80 0 12 -14 0.34 1.96 0 12 14 0.79 2.74 0 -12 14 1.13 1.65 0 -12 14 5.77 7.44 0 -12 -14 1.62 2.16 0 12 15 20.64 12.32 0 -12 15 27.35 16.04 0 -12 -15 21.53 12.90 0 12 16 32.36 16.70 0 -12 16 38.11 28.64 0 -12 -16 30.49 17.89 0 12 17 3.94 3.41 0 -12 17 0.41 7.07 0 -12 -17 5.50 7.53 0 13 0 -3.04 4.20 0 13 0 1.20 2.18 0 -13 0 1.61 3.54 0 13 -1 1.05 2.31 0 13 1 -0.69 4.38 0 13 1 -1.93 3.19 0 -13 1 1.60 1.88 0 -13 1 -1.99 4.75 0 -13 -1 -0.80 4.72 0 13 2 155.41 10.84 0 13 -2 178.99 12.21 0 13 2 164.31 10.03 0 -13 2 172.73 10.42 0 -13 2 168.87 10.82 0 -13 -2 184.32 29.62 0 13 3 22.89 12.05 0 13 -3 16.90 10.48 0 13 3 19.99 10.08 0 -13 3 17.17 11.03 0 -13 3 16.35 8.06 0 -13 -3 19.80 11.94 0 13 -4 278.50 12.61 0 13 4 274.55 12.26 0 13 4 284.00 11.15 0 -13 4 267.96 11.55 0 -13 4 281.04 13.81 0 -13 -4 275.88 14.36 0 13 -5 46.09 5.76 0 13 5 47.98 4.98 0 13 5 49.70 17.94 0 -13 5 41.03 4.42 0 -13 5 46.55 6.20 0 -13 -5 53.02 18.89 0 13 -6 52.32 19.47 0 13 6 49.65 5.29 0 13 6 52.45 8.09 0 -13 6 49.25 5.08 0 -13 6 48.69 27.53 0 -13 -6 45.55 6.75 0 13 7 138.40 7.95 0 13 -7 140.52 30.93 0 13 7 153.82 25.00 0 -13 7 128.03 7.89 0 -13 7 134.89 19.46 0 -13 -7 141.36 10.25 0 13 8 15.67 10.19 0 13 -8 17.92 11.97 0 13 8 19.55 9.28 0 -13 8 10.51 6.08 0 -13 8 23.86 8.67 0 -13 -8 12.72 5.05 0 13 9 24.00 13.60 0 13 -9 30.13 15.47 0 13 9 20.61 10.21 0 -13 9 26.62 12.64 0 -13 9 21.41 12.80 0 -13 -9 44.79 20.70 0 13 -10 -1.73 7.80 0 13 10 -0.24 3.43 0 13 10 2.06 2.23 0 -13 10 1.90 3.38 0 -13 10 2.39 6.78 0 -13 -10 2.11 3.52 0 13 11 2.43 3.02 0 13 -11 4.16 3.68 0 13 11 4.43 5.24 0 -13 11 4.22 3.70 0 -13 11 3.35 5.48 0 -13 -11 7.61 7.06 0 13 12 1.21 1.95 0 13 -12 0.26 1.76 0 13 12 3.27 5.81 0 -13 12 0.29 4.57 0 -13 12 3.32 5.20 0 -13 -12 -1.19 5.54 0 13 -13 13.65 11.39 0 13 13 27.19 10.49 0 -13 13 11.23 11.56 0 -13 13 20.23 13.72 0 -13 -13 13.63 8.07 0 13 -14 4.25 3.40 0 13 14 4.33 3.05 0 -13 14 4.69 6.69 0 -13 -14 4.62 3.78 0 13 15 12.21 5.60 0 -13 15 4.92 7.01 0 -13 -15 8.47 8.08 0 13 16 6.48 7.25 0 -13 16 7.51 7.61 0 -13 -16 4.38 6.38 0 13 17 4.87 6.11 0 -13 17 2.17 5.60 0 -13 -17 0.22 4.83 0 14 0 -0.66 3.58 0 -14 0 2.57 3.33 0 14 1 402.89 17.39 0 14 -1 351.70 15.31 0 14 1 325.07 15.50 0 -14 1 335.31 13.97 0 -14 -1 329.15 15.25 0 -14 1 346.55 15.60 0 14 -2 139.88 18.20 0 14 2 129.29 10.12 0 14 2 121.02 8.27 0 -14 2 130.67 9.40 0 -14 2 117.86 10.49 0 -14 -2 136.87 16.30 0 14 3 3.59 4.26 0 14 -3 5.30 5.28 0 14 3 4.52 2.97 0 -14 3 1.33 1.98 0 -14 3 3.34 3.00 0 -14 -3 6.66 4.98 0 14 -4 566.17 21.30 0 14 4 569.34 23.84 0 14 4 547.99 20.26 0 -14 4 573.66 27.66 0 -14 4 553.37 23.06 0 -14 -4 533.20 20.59 0 14 5 146.23 10.54 0 14 -5 119.52 8.20 0 14 5 141.86 15.42 0 -14 5 101.27 6.54 0 -14 5 139.77 8.98 0 -14 -5 112.53 9.11 0 14 -6 193.34 12.93 0 14 6 207.92 17.74 0 14 6 207.95 12.92 0 -14 6 165.51 11.88 0 -14 6 183.55 13.41 0 -14 -6 179.62 13.86 0 14 7 47.33 8.16 0 14 -7 36.21 16.51 0 14 7 31.23 16.35 0 -14 7 46.28 5.39 0 -14 7 39.24 13.61 0 -14 -7 50.10 30.88 0 14 8 204.26 19.22 0 14 -8 190.00 14.50 0 14 8 199.75 17.09 0 -14 8 170.94 10.96 0 -14 8 185.15 12.94 0 -14 -8 171.64 11.66 0 14 9 409.47 26.21 0 14 -9 407.68 26.82 0 14 9 381.53 25.35 0 -14 9 339.07 30.95 0 -14 9 381.22 27.32 0 -14 -9 333.78 23.66 0 14 -10 124.39 26.94 0 14 10 134.06 9.85 0 14 10 109.53 10.43 0 -14 10 123.31 13.25 0 -14 10 153.23 54.49 0 -14 -10 127.65 42.94 0 14 -11 172.52 19.82 0 14 11 174.28 18.45 0 14 11 176.10 17.71 0 -14 11 166.36 11.40 0 -14 11 156.21 13.49 0 -14 -11 153.90 13.00 0 14 12 2.40 4.01 0 14 -12 1.65 2.64 0 14 12 -0.64 5.19 0 -14 12 1.18 4.61 0 -14 12 2.95 5.33 0 -14 -12 1.67 2.72 0 14 -13 3.83 2.58 0 14 13 3.76 4.14 0 -14 13 1.65 3.12 0 -14 13 3.15 9.08 0 -14 -13 8.09 7.01 0 14 -14 21.62 13.42 0 14 14 20.59 11.86 0 -14 14 34.10 22.61 0 -14 -14 31.62 14.57 0 14 15 11.15 6.48 0 -14 15 12.75 11.73 0 -14 -15 10.49 10.27 0 14 16 29.12 13.50 0 -14 16 37.04 25.96 0 -14 -16 30.19 15.40 0 15 0 2.80 3.23 0 -15 0 2.78 2.92 0 -15 0 2.26 4.32 0 15 1 55.19 20.36 0 15 -1 56.46 18.81 0 15 1 60.06 5.82 0 -15 1 57.41 5.95 0 -15 1 58.70 23.64 0 -15 -1 66.03 10.72 0 15 2 20.30 12.52 0 15 -2 17.99 7.06 0 15 2 26.33 10.44 0 -15 2 20.11 13.77 0 -15 2 18.47 8.91 0 -15 -2 24.86 10.80 0 15 -3 300.59 18.95 0 15 3 312.11 18.40 0 15 3 296.47 16.86 0 -15 3 269.49 15.18 0 -15 3 328.08 19.94 0 -15 -3 256.04 16.99 0 15 4 -4.14 4.58 0 15 -4 2.88 3.75 0 15 4 2.46 4.51 0 -15 4 1.36 1.80 0 -15 4 -0.01 9.41 0 -15 -4 4.44 5.39 0 15 -5 41.54 20.77 0 15 5 44.77 19.61 0 15 5 35.80 15.20 0 -15 5 41.78 19.35 0 -15 5 21.61 17.11 0 -15 -5 51.89 28.15 0 15 6 2.79 3.69 0 15 -6 2.55 5.44 0 15 6 1.34 2.85 0 -15 6 -1.82 4.86 0 -15 6 2.01 1.98 0 -15 -6 1.75 8.81 0 15 7 221.04 16.09 0 15 -7 256.89 18.86 0 15 7 245.21 19.63 0 -15 7 244.32 17.87 0 -15 7 249.26 19.60 0 -15 -7 226.80 18.21 0 15 8 69.03 6.73 0 15 -8 101.33 34.23 0 15 8 98.08 21.59 0 -15 8 89.60 7.91 0 -15 8 101.66 10.95 0 -15 -8 62.62 36.80 0 15 9 408.38 23.58 0 15 -9 403.93 25.77 0 15 9 380.51 23.30 0 -15 9 394.30 23.82 0 -15 9 391.10 25.78 0 -15 -9 413.22 34.49 0 15 -10 22.78 9.89 0 15 10 30.23 16.58 0 15 10 24.20 11.42 0 -15 10 23.64 15.62 0 -15 10 31.56 18.55 0 -15 -10 29.92 12.31 0 15 -11 20.04 9.41 0 15 11 10.36 6.19 0 15 11 17.62 8.69 0 -15 11 20.69 14.18 0 -15 11 15.15 6.81 0 -15 -11 6.53 6.62 0 15 12 2.83 3.00 0 15 -12 2.58 3.70 0 15 12 2.09 2.67 0 -15 12 1.70 3.73 0 -15 12 3.55 5.16 0 -15 -12 7.24 6.58 0 15 -13 3.53 3.53 0 15 13 3.41 2.47 0 -15 13 2.94 5.38 0 -15 -13 4.35 4.87 0 15 -14 -0.58 3.06 0 15 14 1.23 4.14 0 -15 14 2.51 3.21 0 -15 -14 4.85 5.01 0 15 15 15.11 11.01 0 -15 15 10.31 19.10 0 -15 -15 13.14 5.23 0 15 16 22.27 15.48 0 -15 16 23.71 25.60 0 -15 -16 19.63 8.02 0 16 0 137.49 14.97 0 -16 0 124.63 10.01 0 -16 0 126.04 11.61 0 16 1 76.28 6.86 0 16 -1 75.06 7.22 0 16 1 79.09 14.42 0 -16 1 67.56 6.02 0 -16 1 74.14 7.83 0 -16 -1 68.45 7.92 0 16 -2 86.65 8.55 0 16 2 86.14 8.66 0 16 2 80.13 6.48 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226.88 10.27 -1 11 7 234.07 10.12 -1 -11 7 194.99 10.10 -1 -11 7 245.26 12.32 1 -11 -7 207.94 11.07 1 11 -6 29.73 9.51 -1 11 6 29.95 14.92 -1 11 6 22.74 12.21 -1 -11 6 28.60 14.70 -1 -11 6 18.20 8.81 1 -11 -6 27.22 14.65 1 11 -5 453.69 17.23 -1 11 5 395.74 15.62 -1 11 5 434.06 21.73 -1 -11 5 438.44 17.92 -1 -11 5 441.37 20.72 1 -11 -5 431.41 17.11 1 11 -4 -1.70 7.63 -1 11 4 1.94 2.03 -1 11 4 2.87 2.48 -1 -11 4 2.40 4.16 -1 -11 4 1.57 1.50 1 -11 -4 2.68 3.76 1 11 -3 2044.40 61.84 -1 11 3 1976.45 60.80 -1 11 3 2014.03 59.52 -1 -11 3 1857.77 56.86 -1 -11 3 1903.58 58.05 1 -11 -3 1820.38 56.38 1 11 -2 608.27 33.01 -1 11 2 659.28 25.81 -1 11 2 585.01 22.90 -1 -11 2 611.94 38.81 -1 -11 2 581.77 32.84 1 -11 -2 623.93 24.98 1 11 -1 6.20 5.70 -1 11 1 9.36 10.00 -1 11 1 4.10 3.43 -1 -11 1 6.39 4.82 -1 -11 1 6.63 6.14 1 -11 -1 7.10 6.33 1 11 0 282.33 17.34 -1 11 0 293.25 16.77 -1 11 0 265.98 12.66 -1 -11 0 296.43 15.16 -1 -11 0 259.33 13.98 1 -11 0 270.42 14.92 1 11 1 58.73 5.76 -1 11 -1 50.81 6.49 -1 11 -1 60.49 3.60 1 11 1 65.69 7.47 1 -11 1 46.80 5.43 -1 -11 -1 65.68 20.24 1 11 2 4.62 5.80 -1 11 -2 4.48 5.13 1 11 2 5.99 3.89 1 -11 2 6.96 4.04 1 -11 2 2.45 5.12 -1 -11 -2 5.84 3.56 1 11 3 534.71 19.08 -1 11 -3 517.55 19.41 1 11 3 548.76 20.17 1 -11 3 570.39 19.08 1 -11 3 570.09 21.76 -1 -11 -3 601.53 21.85 1 11 4 -0.01 3.46 -1 11 -4 -0.70 3.96 1 11 4 -0.83 3.53 1 -11 4 0.17 1.43 1 -11 4 1.09 4.28 -1 -11 -4 1.41 1.90 1 11 5 310.97 12.05 -1 11 -5 300.24 12.88 1 11 5 299.62 11.75 1 -11 5 283.28 13.70 1 -11 5 284.63 17.11 -1 -11 -5 274.70 11.48 1 11 6 38.83 4.19 -1 11 -6 35.41 4.97 1 11 6 42.24 7.98 1 -11 6 42.91 3.78 1 -11 6 47.53 19.09 -1 -11 -6 40.14 15.76 1 11 7 -0.29 3.08 -1 11 -7 -0.90 3.82 1 11 7 -0.71 3.51 1 -11 7 -0.08 2.07 1 -11 7 -2.75 5.56 -1 -11 -7 5.09 3.50 1 11 8 50.13 4.25 -1 11 -8 48.65 5.18 1 11 8 51.72 5.74 1 -11 8 43.24 10.93 1 -11 8 65.74 18.46 -1 -11 -8 48.07 22.88 1 11 9 10.20 4.20 -1 11 -9 10.85 4.04 1 11 9 10.01 4.43 1 -11 9 10.40 6.86 1 -11 9 11.82 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15 0.16 4.28 -1 -12 15 1.80 2.15 -1 -12 15 2.50 3.08 1 -12 -15 1.82 5.80 1 12 -14 55.44 5.45 -1 12 14 70.84 7.67 -1 -12 14 52.95 7.46 -1 -12 14 63.14 8.05 1 -12 -14 31.49 25.61 1 12 -13 -1.23 3.47 -1 12 13 2.15 3.18 -1 -12 13 0.96 2.51 -1 -12 13 2.87 7.33 1 -12 -13 -0.39 6.79 1 12 -12 12.49 4.96 -1 12 12 11.53 7.12 -1 12 12 10.28 7.89 -1 -12 12 13.01 7.37 -1 -12 12 15.29 8.65 1 -12 -12 13.35 10.53 1 12 -11 238.38 21.24 -1 12 11 246.37 16.80 -1 12 11 261.40 18.69 -1 -12 11 213.28 16.90 -1 -12 11 242.91 18.98 1 -12 -11 206.83 17.02 1 12 -10 9.16 3.66 -1 12 10 8.31 3.87 -1 12 10 5.44 8.81 -1 -12 10 8.05 4.17 -1 -12 10 7.05 5.54 1 -12 -10 7.69 5.57 1 12 -9 3.16 2.83 -1 12 9 2.18 2.94 -1 12 9 2.81 2.77 -1 -12 9 1.31 2.72 -1 -12 9 4.13 4.90 1 -12 -9 2.49 3.29 1 12 -8 168.44 10.80 -1 12 8 187.89 15.92 -1 12 8 179.71 12.84 -1 -12 8 160.66 11.25 -1 -12 8 194.10 13.48 1 -12 -8 148.54 9.86 1 12 -7 1016.91 31.94 -1 12 7 1021.43 47.06 -1 12 7 1034.69 34.42 -1 -12 7 1023.15 33.46 -1 -12 7 1060.13 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11 -5 1.96 2.94 -4 11 5 6.94 8.78 -4 11 5 2.51 3.79 -4 -11 5 3.27 3.80 -4 -11 5 4.45 2.57 4 -11 -5 4.11 4.21 4 11 -4 16.88 7.28 -4 11 4 4.67 6.59 -4 11 4 10.58 7.58 -4 -11 4 17.24 10.24 -4 -11 4 12.77 4.41 4 -11 -4 16.62 11.36 4 11 -3 -2.52 5.22 -4 11 3 5.73 6.71 -4 11 3 1.49 2.23 -4 -11 3 1.38 4.00 -4 -11 3 2.09 1.48 4 -11 -3 -1.90 4.74 4 11 -2 102.61 9.49 -4 11 2 88.55 9.54 -4 11 2 105.99 6.50 -4 -11 2 98.49 8.88 -4 -11 2 110.54 7.35 4 -11 -2 96.23 7.97 4 11 -1 158.12 11.83 -4 11 1 159.99 12.98 -4 11 1 166.85 8.98 -4 -11 1 169.33 14.94 -4 -11 1 165.46 9.36 4 -11 -1 156.73 10.52 4 11 0 430.82 25.30 -4 11 0 448.54 23.66 -4 11 0 478.07 14.52 -4 -11 0 426.86 18.11 4 -11 0 474.37 18.60 -4 -11 0 457.68 16.03 4 11 1 6.61 5.62 -4 11 -1 -0.64 5.91 -4 11 -1 1.68 0.94 -4 -11 -1 -1.13 6.16 4 -11 1 1.74 3.29 -4 -11 -1 -0.13 2.09 4 11 2 5.21 2.23 -4 11 -2 7.11 8.10 -4 11 -2 6.97 2.87 -4 -11 -2 6.47 10.90 4 -11 2 3.68 3.16 -4 -11 -2 10.78 4.99 4 11 3 20.46 12.52 -4 11 -3 29.10 6.65 4 -11 3 25.97 1.43 -4 -11 -3 24.38 13.41 4 -11 3 29.08 12.74 -4 -11 -3 30.81 4.28 4 11 4 78.77 6.86 -4 11 -4 91.66 8.91 -4 -11 -4 75.81 8.10 4 -11 4 87.84 8.00 -4 -11 -4 102.66 9.69 4 11 5 4.61 3.68 -4 11 -5 9.25 6.67 -4 -11 -5 6.79 3.79 4 -11 5 2.62 2.21 -4 -11 -5 13.76 5.20 4 11 6 108.35 11.91 -4 11 -6 75.69 8.43 4 11 6 82.05 6.48 4 -11 6 98.90 9.91 -4 -11 -6 107.13 13.67 4 11 7 2.31 5.37 -4 11 -7 8.81 5.44 4 11 7 7.35 3.89 4 -11 7 5.48 6.27 -4 -11 -7 3.88 3.56 4 11 8 20.36 12.39 -4 11 -8 15.36 13.96 4 11 8 17.58 11.84 4 -11 8 25.03 9.28 -4 -11 -8 17.48 8.00 4 11 9 7.36 6.49 -4 11 -9 5.99 5.88 4 11 9 6.27 6.06 4 -11 9 7.28 8.97 -4 -11 -9 8.61 7.02 4 11 10 107.82 12.72 -4 11 -10 97.93 16.75 4 11 10 107.12 10.65 4 -11 10 91.71 9.70 -4 -11 -10 101.69 8.68 4 11 11 4.10 4.10 -4 11 -11 4.83 3.97 4 11 11 7.55 7.86 4 -11 11 3.23 3.33 -4 -11 -11 3.33 2.43 -4 11 -12 7.33 4.91 4 11 12 7.95 6.01 4 -11 12 4.28 3.22 -4 -11 -12 5.93 7.60 -4 11 -13 12.04 9.01 4 11 13 14.53 12.01 4 -11 13 16.42 14.86 -4 -11 -13 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180.31 14.06 -4 -12 9 155.98 19.09 -4 -12 9 160.10 10.04 4 -12 -9 147.57 10.01 4 12 -8 81.04 21.67 -4 12 8 64.84 7.86 -4 12 8 58.91 5.81 -4 -12 8 63.89 16.90 -4 -12 8 63.29 5.60 4 -12 -8 77.74 17.27 4 12 -7 7.57 5.44 -4 12 7 4.54 5.01 -4 12 7 4.58 4.64 -4 -12 7 -1.50 6.13 -4 -12 7 4.77 2.22 4 -12 -7 2.20 2.12 4 12 -6 150.06 13.33 -4 12 6 123.17 15.94 -4 12 6 156.01 11.62 -4 -12 6 142.32 33.74 -4 -12 6 155.59 18.11 4 -12 -6 142.04 14.31 4 12 -5 113.31 10.90 -4 12 5 127.34 12.25 -4 12 5 116.50 8.54 -4 -12 5 118.05 12.77 -4 -12 5 113.55 8.61 4 -12 -5 116.19 10.61 4 12 -4 25.41 13.93 -4 12 4 23.70 9.86 -4 12 4 34.67 4.99 -4 -12 4 31.18 11.92 -4 -12 4 27.52 3.76 4 -12 -4 25.47 13.52 4 12 -3 517.89 28.47 -4 12 3 451.40 26.29 -4 12 3 531.48 24.84 -4 -12 3 441.70 24.55 -4 -12 3 447.15 21.97 4 -12 -3 515.87 27.06 4 12 -2 106.31 9.68 -4 12 2 82.68 9.18 -4 12 2 95.28 4.95 -4 -12 2 75.49 9.37 -4 -12 2 95.65 5.75 4 -12 -2 89.64 7.39 4 12 -1 47.03 19.78 -4 12 1 35.07 6.95 -4 12 1 35.95 9.09 -4 -12 1 32.87 14.96 -4 -12 1 35.06 4.15 4 -12 -1 35.84 19.07 4 12 0 262.13 16.92 -4 12 0 287.34 19.97 -4 12 0 275.33 13.22 -4 -12 0 223.24 15.72 4 -12 0 285.52 16.69 -4 -12 0 288.69 15.32 4 12 1 110.70 9.36 -4 12 -1 107.42 10.11 -4 12 -1 104.64 3.94 -4 -12 -1 91.96 8.04 4 -12 1 113.49 12.37 -4 -12 -1 123.76 6.78 4 12 2 21.73 10.57 -4 12 -2 26.33 8.14 -4 12 -2 22.11 2.27 -4 -12 -2 18.89 11.54 4 -12 2 20.35 12.38 -4 -12 -2 19.31 11.23 4 12 3 14.75 12.99 4 -12 3 12.12 2.95 -4 -12 -3 7.21 6.62 4 -12 3 15.23 4.53 -4 -12 -3 11.70 6.60 4 12 4 139.71 12.35 -4 12 -4 147.97 14.11 -4 -12 -4 139.26 11.90 4 -12 4 135.94 11.60 -4 -12 -4 145.99 12.78 4 12 5 192.81 15.83 -4 12 -5 177.47 16.32 -4 -12 -5 169.45 10.43 4 -12 5 190.41 16.66 -4 -12 -5 157.38 7.66 4 12 6 26.53 12.53 -4 12 -6 28.28 15.08 4 -12 6 33.81 28.28 -4 -12 -6 25.12 14.58 4 12 7 193.58 16.55 -4 12 -7 163.88 15.05 4 12 7 168.48 13.41 4 -12 7 162.70 13.80 -4 -12 -7 174.35 12.99 4 12 8 15.94 8.93 -4 12 -8 13.62 7.22 4 -12 8 14.34 9.99 -4 -12 -8 19.96 11.90 4 12 9 2.26 1.45 -4 12 -9 1.62 2.06 4 12 9 1.47 1.61 4 -12 9 6.54 5.74 -4 -12 -9 3.09 2.09 4 12 10 128.45 18.50 -4 12 -10 75.74 7.57 4 12 10 95.11 8.30 4 -12 10 94.69 10.62 -4 -12 -10 87.94 15.12 4 12 11 3.00 4.03 -4 12 -11 7.82 6.84 4 12 11 6.27 5.32 4 -12 11 3.91 3.55 -4 -12 -11 5.10 7.01 -4 12 -12 52.94 11.05 4 12 12 72.60 7.62 4 -12 12 76.42 9.82 -4 -12 -12 78.23 12.24 -4 12 -13 2.17 5.49 4 12 13 0.57 2.11 4 -12 13 5.79 8.07 -4 -12 -13 4.76 3.87 4 12 14 26.08 14.19 4 -12 14 17.98 17.84 -4 -12 -14 16.87 14.47 4 12 15 1.63 4.25 4 -12 15 1.26 8.43 -4 -12 -15 -0.38 3.45 -4 13 16 2.76 4.04 -4 -13 16 3.60 11.10 -4 -13 16 4.12 4.61 4 -13 -16 1.87 4.17 4 13 -15 17.46 16.24 -4 13 15 11.44 9.03 -4 -13 15 8.75 7.00 -4 -13 15 15.47 11.88 4 -13 -15 13.22 8.34 4 13 -14 5.00 2.70 -4 13 14 5.30 4.54 -4 -13 14 7.55 10.70 -4 -13 14 3.71 8.92 4 -13 -14 5.09 5.24 4 13 -13 6.02 4.81 -4 13 13 1.27 2.92 -4 13 13 3.95 3.68 -4 -13 13 0.62 1.88 -4 -13 13 -0.70 3.35 4 -13 -13 1.89 5.37 4 13 -12 7.72 8.71 -4 13 12 9.60 8.47 -4 13 12 5.78 6.98 -4 -13 12 3.62 6.15 -4 -13 12 8.24 9.16 4 -13 -12 13.42 8.82 4 13 -11 36.78 8.91 -4 13 11 25.33 18.61 -4 13 11 24.40 13.08 -4 -13 11 30.31 20.74 -4 -13 11 23.40 13.83 4 -13 -11 29.26 16.03 4 13 -10 6.31 5.06 -4 13 10 12.97 10.03 -4 13 10 10.46 5.37 -4 -13 10 8.89 9.66 -4 -13 10 11.45 6.11 4 -13 -10 8.74 7.67 4 13 -9 50.41 10.65 -4 13 9 56.91 13.50 -4 13 9 60.16 7.74 -4 -13 9 44.96 32.18 -4 -13 9 47.72 5.48 4 -13 -9 52.74 30.97 4 13 -8 1.26 3.45 -4 13 8 1.92 3.41 -4 13 8 -0.27 2.13 -4 -13 8 3.40 4.73 -4 -13 8 -0.22 1.94 4 -13 -8 -5.90 6.46 4 13 -7 88.49 10.30 -4 13 7 74.24 8.48 -4 13 7 91.06 20.10 -4 -13 7 95.54 10.50 -4 -13 7 92.76 9.82 4 -13 -7 89.65 8.16 4 13 -6 63.59 28.74 -4 13 6 46.85 24.56 -4 13 6 70.16 5.62 -4 -13 6 55.04 22.94 -4 -13 6 60.93 10.50 4 -13 -6 39.40 18.72 4 13 -5 1.48 5.16 -4 13 5 -0.13 6.01 -4 13 5 1.75 3.38 -4 -13 5 2.00 2.59 -4 -13 5 -0.15 2.29 4 -13 -5 -3.14 5.48 4 13 -4 27.82 10.55 -4 13 4 23.51 13.35 -4 13 4 17.09 7.15 -4 -13 4 25.08 14.06 -4 -13 4 18.36 9.48 4 -13 -4 22.58 17.50 4 13 -3 104.45 15.61 -4 13 3 96.44 20.33 -4 13 3 100.00 7.38 -4 -13 3 85.77 10.13 -4 -13 3 100.59 8.15 4 -13 -3 94.94 9.95 4 13 -2 14.17 8.48 -4 13 2 28.05 9.91 -4 13 2 19.23 10.78 -4 -13 2 22.24 12.26 -4 -13 2 24.40 13.15 4 -13 -2 16.25 11.69 4 13 -1 232.91 15.15 -4 13 1 222.19 15.05 -4 13 1 237.54 9.60 -4 -13 1 198.40 12.37 -4 -13 1 213.85 10.74 4 -13 -1 210.04 12.58 4 13 0 97.07 11.18 -4 13 0 126.87 11.84 -4 13 0 99.67 8.22 -4 -13 0 109.21 10.88 4 -13 0 107.22 9.72 -4 -13 0 138.31 21.02 4 13 1 384.88 19.81 -4 13 -1 328.60 18.81 -4 13 -1 340.98 12.94 -4 -13 -1 323.82 16.15 4 -13 1 361.42 17.10 -4 -13 -1 345.59 14.97 4 13 2 53.03 24.42 -4 13 -2 40.01 22.04 -4 -13 -2 36.10 23.03 4 -13 2 43.04 7.70 4 -13 2 38.57 16.56 -4 -13 -2 51.25 5.43 4 13 3 500.91 37.53 -4 13 -3 495.61 34.20 -4 -13 -3 452.11 29.97 4 -13 3 504.36 35.03 -4 -13 -3 539.10 46.89 4 13 4 9.88 7.55 -4 13 -4 9.12 9.51 -4 -13 -4 6.84 7.39 4 -13 4 12.46 6.22 -4 -13 -4 10.74 6.91 4 13 5 371.73 25.64 -4 13 -5 410.84 28.95 -4 -13 -5 393.41 27.07 4 -13 5 407.33 32.08 -4 -13 -5 391.54 25.23 4 13 6 2.54 5.00 -4 13 -6 3.64 5.88 -4 -13 -6 5.84 7.19 4 -13 6 1.68 3.52 -4 -13 -6 0.95 3.97 4 13 7 3.35 3.74 -4 13 -7 3.47 2.58 4 13 7 4.10 3.37 4 -13 7 2.18 2.61 -4 -13 -7 2.13 3.80 4 13 8 82.73 7.81 -4 13 -8 41.70 25.55 4 13 8 53.88 26.89 4 -13 8 63.48 14.34 -4 -13 -8 69.53 9.40 4 13 9 53.29 17.94 -4 13 -9 34.09 14.11 4 13 9 44.22 19.97 4 -13 9 35.86 34.13 -4 -13 -9 33.59 14.74 4 13 10 17.93 10.03 -4 13 -10 12.11 10.51 4 13 10 11.97 6.10 4 -13 10 20.01 13.64 -4 -13 -10 18.52 6.84 4 13 11 51.16 6.56 -4 13 -11 60.96 9.10 4 13 11 51.26 8.00 4 -13 11 59.03 34.89 -4 -13 -11 43.00 21.17 -4 13 -12 9.24 7.70 4 13 12 4.05 5.76 4 -13 12 12.60 9.87 -4 -13 -12 10.30 7.60 -4 13 -13 35.13 10.42 4 13 13 27.63 12.13 4 -13 13 38.45 29.54 -4 -13 -13 24.18 11.03 4 13 14 25.24 12.03 4 -13 14 19.52 20.81 -4 -13 -14 17.02 14.76 4 14 -15 5.61 6.76 -4 14 15 5.41 5.25 -4 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7.19 -4 14 6 6.33 5.20 -4 14 6 6.95 4.94 -4 -14 6 12.24 7.10 -4 -14 6 8.93 3.13 4 -14 -6 6.44 6.85 4 14 -5 156.29 11.91 -4 14 5 151.16 11.96 -4 14 5 161.68 11.57 -4 -14 5 145.27 10.51 -4 -14 5 177.13 13.37 4 -14 -5 161.45 15.39 4 14 -4 19.58 12.96 -4 14 4 14.52 9.52 -4 14 4 8.35 5.99 -4 -14 4 19.52 9.53 -4 -14 4 14.42 7.93 4 -14 -4 15.36 6.86 4 14 -3 151.53 22.58 -4 14 3 126.07 24.07 -4 14 3 155.07 6.88 -4 -14 3 118.22 10.71 -4 -14 3 152.06 8.38 4 -14 -3 140.81 9.84 4 14 -2 46.34 25.08 -4 14 2 40.22 20.52 -4 14 2 49.34 6.73 -4 -14 2 42.51 23.31 -4 -14 2 47.37 5.07 4 -14 -2 40.01 22.53 4 14 -1 311.20 23.90 -4 14 1 315.83 25.23 -4 14 1 284.98 18.01 -4 -14 1 256.04 20.50 -4 -14 1 279.78 18.98 4 -14 -1 262.96 19.45 4 14 0 210.43 17.45 -4 14 0 166.27 12.10 -4 14 0 172.21 7.35 -4 -14 0 168.86 23.80 4 -14 0 178.38 13.42 -4 -14 0 196.74 14.58 4 14 1 3.20 3.69 -4 14 -1 0.63 4.78 -4 14 -1 0.77 1.34 -4 -14 -1 -0.35 6.88 4 -14 1 -2.51 5.54 -4 -14 -1 1.76 1.84 4 14 2 28.27 16.02 -4 14 -2 34.25 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4.51 8 8 -7 3.23 3.01 -8 8 7 7.05 10.30 -8 8 7 5.14 2.92 -8 -8 7 7.75 5.12 8 8 -6 4.47 7.09 -8 8 6 4.20 6.14 -8 8 6 1.02 3.11 -8 -8 6 -1.16 5.59 8 8 -5 4.16 6.93 -8 8 5 13.47 9.37 -8 8 5 6.25 4.18 -8 -8 5 6.65 6.49 8 8 -4 50.81 29.19 -8 8 4 72.61 10.07 -8 8 4 71.50 6.36 -8 -8 4 81.94 15.40 8 8 -3 0.98 5.96 -8 8 3 0.75 5.07 -8 -8 3 2.46 7.00 8 8 -2 50.02 36.52 -8 8 2 57.14 41.03 -8 -8 2 48.53 28.11 8 8 -1 9.59 10.73 -8 8 1 5.50 5.56 -8 -8 1 8.63 8.41 8 8 0 47.85 26.13 -8 8 0 39.33 24.24 -8 -8 0 31.46 17.77 8 8 1 2.21 5.56 -8 8 -1 8.22 5.01 -8 -8 -1 7.39 11.81 8 8 2 5.75 7.75 -8 8 -2 1.31 7.18 -8 -8 -2 5.89 10.60 8 8 3 31.25 18.52 -8 8 -3 26.40 10.49 -8 -8 -3 34.98 18.98 8 8 4 5.31 7.11 -8 8 -4 4.72 5.99 -8 -8 -4 9.14 6.04 8 8 5 2.72 2.81 -8 8 -5 1.68 6.55 -8 -8 -5 0.56 2.63 8 8 6 5.08 5.20 -8 8 -6 5.23 5.55 -8 -8 -6 1.88 4.12 8 8 7 80.67 10.40 -8 8 -7 56.07 30.93 -8 -8 -7 62.31 7.06 8 8 8 5.33 7.32 -8 8 -8 3.86 4.59 -8 -8 -8 6.39 3.83 -8 8 -9 7.19 12.89 -8 -8 -9 5.82 9.22 -8 -8 -9 6.89 8.49 8 9 -12 2.58 8.22 -8 9 12 4.57 4.81 -8 9 12 4.63 2.86 -8 -9 12 1.26 6.72 8 9 -11 7.84 3.43 -8 9 11 13.06 8.29 -8 9 11 4.93 3.79 -8 -9 11 5.93 6.78 8 9 -10 4.50 3.63 -8 9 10 7.50 10.14 -8 9 10 7.26 5.80 -8 -9 10 4.01 5.95 8 9 -9 2.04 2.75 -8 9 9 2.23 6.44 -8 9 9 1.57 2.56 -8 -9 9 3.19 3.97 8 9 -8 -0.24 3.34 -8 9 8 -0.87 5.74 -8 9 8 1.16 2.39 -8 -9 8 1.60 5.01 8 9 -7 5.32 4.24 -8 9 7 1.15 3.51 -8 9 7 3.01 4.77 -8 -9 7 1.29 6.74 8 9 -6 1.30 3.35 -8 9 6 4.78 2.60 -8 9 6 4.48 4.23 -8 -9 6 4.09 6.44 8 9 -5 9.08 9.88 -8 9 5 24.71 20.02 -8 9 5 9.93 6.64 -8 -9 5 24.26 14.64 8 9 -4 14.73 12.39 -8 9 4 15.91 17.17 -8 -9 4 17.91 13.65 8 9 -3 2.17 5.17 -8 9 3 5.47 9.71 -8 -9 3 2.47 5.39 8 9 -2 8.89 8.68 -8 9 2 7.06 5.14 -8 -9 2 6.63 13.04 8 9 -1 3.72 6.23 -8 9 1 6.53 8.86 -8 -9 1 7.16 7.75 8 9 0 116.44 12.75 -8 9 0 114.56 11.96 -8 -9 0 120.93 10.52 8 9 1 22.05 15.45 -8 9 -1 13.41 5.39 -8 -9 -1 19.00 16.37 8 9 2 70.01 9.81 -8 9 -2 60.15 39.44 -8 -9 -2 54.32 32.00 8 9 3 3.65 8.14 -8 9 -3 2.45 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3.87 5.95 -9 -4 -4 2.18 4.36 -9 -4 -4 3.56 3.23 -9 4 -5 2.32 3.46 -9 -4 -5 3.77 4.81 -9 4 -6 1.61 5.37 -9 -4 -6 6.68 4.70 -9 4 -7 7.89 9.03 -9 -4 -7 15.50 13.97 -9 5 11 8.68 14.26 -9 -5 11 11.02 14.18 -9 5 11 9.22 11.62 -9 -5 11 7.27 8.12 -9 5 10 3.96 5.06 -9 -5 10 5.07 7.86 -9 5 10 0.84 2.67 -9 -5 10 -1.39 6.17 9 5 -9 42.79 29.36 -9 5 9 32.25 29.73 -9 5 9 58.80 8.17 -9 -5 9 70.35 10.00 9 5 -8 2.02 3.73 -9 5 8 3.31 2.50 -9 5 8 3.96 3.88 -9 -5 8 -0.76 5.58 9 5 -7 49.51 33.08 -9 5 7 54.43 41.40 -9 5 7 78.32 7.65 -9 -5 7 68.89 15.72 9 5 -6 11.59 6.26 -9 5 6 14.02 8.43 -9 5 6 12.35 12.69 -9 -5 6 6.66 3.56 9 5 -5 10.44 7.20 -9 5 5 11.21 14.00 -9 5 5 5.79 5.64 -9 -5 5 7.61 5.00 9 5 -4 -0.95 4.77 -9 5 4 2.69 4.39 -9 5 4 -1.93 2.80 -9 -5 4 6.35 5.91 9 5 -3 7.39 10.89 -9 5 3 4.26 7.34 -9 -5 3 7.29 8.07 9 5 -2 3.35 5.04 -9 5 2 1.72 6.81 -9 -5 2 3.91 6.03 9 5 -1 15.04 16.69 -9 5 1 14.58 11.64 -9 -5 1 14.04 5.49 9 5 0 11.94 13.65 -9 5 0 11.65 14.95 -9 -5 0 8.66 8.03 -9 5 -1 0.96 7.05 -9 -5 -1 -0.82 5.26 -9 -5 -1 0.47 3.95 -9 5 -2 6.45 10.36 -9 -5 -2 8.10 5.00 -9 -5 -2 10.94 9.95 -9 5 -3 13.28 11.42 -9 -5 -3 14.56 7.65 -9 -5 -3 11.43 9.58 -9 5 -4 96.88 15.94 -9 -5 -4 103.45 10.99 -9 -5 -4 84.93 8.24 -9 5 -5 4.30 2.82 -9 -5 -5 3.59 4.30 -9 5 -6 3.15 6.01 -9 -5 -6 -4.11 4.69 -9 5 -7 1.81 4.92 -9 -5 -7 2.19 2.62 9 6 -11 1.76 4.26 -9 6 11 4.48 5.66 -9 6 11 1.25 2.32 -9 -6 11 6.21 8.06 9 6 -10 81.74 9.88 -9 6 10 34.50 34.05 -9 6 10 42.11 29.94 -9 -6 10 68.31 10.75 9 6 -9 50.62 39.01 -9 6 9 35.88 33.20 -9 6 9 43.44 20.37 -9 -6 9 40.47 23.66 9 6 -8 0.07 5.27 -9 6 8 3.38 6.41 -9 6 8 5.17 3.95 -9 -6 8 -0.70 6.22 9 6 -7 8.34 8.31 -9 6 7 3.01 5.17 -9 6 7 -0.34 3.42 -9 -6 7 7.16 6.50 9 6 -6 9.23 7.77 -9 6 6 4.00 5.78 -9 6 6 1.74 4.06 -9 -6 6 5.74 5.80 9 6 -5 0.56 3.78 -9 6 5 3.53 9.33 -9 6 5 1.00 2.48 -9 -6 5 1.96 2.61 9 6 -4 7.90 6.01 -9 6 4 4.26 4.64 -9 -6 4 10.96 8.18 9 6 -3 5.42 5.64 -9 6 3 3.91 6.12 -9 -6 3 37.72 8.02 9 6 -2 3.38 3.39 -9 6 2 6.72 6.65 -9 -6 2 2.82 7.00 9 6 -1 21.96 12.36 -9 6 1 15.75 10.79 -9 -6 1 10.37 15.03 9 6 0 139.52 13.36 -9 6 0 121.34 16.46 -9 -6 0 144.16 10.86 9 6 1 13.52 10.75 -9 6 -1 12.51 13.06 -9 -6 -1 18.80 12.26 9 6 2 1.02 4.58 -9 6 -2 9.70 29.84 -9 -6 -2 2.69 4.24 -9 6 -3 10.47 7.35 -9 -6 -3 12.11 8.78 -9 6 -4 3.64 5.47 -9 -6 -4 2.83 4.24 -9 -6 -4 1.02 2.66 -9 6 -5 5.58 7.90 -9 -6 -5 5.67 4.76 -9 -6 -5 6.45 6.02 -9 6 -6 8.29 7.05 -9 -6 -6 10.82 6.35 -9 6 -7 20.72 18.19 -9 -6 -7 18.69 14.52 9 7 -10 1.84 3.18 -9 7 10 6.89 8.14 -9 7 10 1.59 1.82 -9 -7 10 5.22 2.92 9 7 -9 2.28 4.52 -9 7 9 8.39 7.37 -9 7 9 7.96 7.76 -9 -7 9 4.85 6.67 9 7 -8 57.40 29.88 -9 7 8 42.54 33.21 -9 7 8 67.17 7.26 -9 -7 8 60.29 9.12 9 7 -7 51.19 28.96 -9 7 7 34.58 31.63 -9 7 7 38.68 5.39 -9 -7 7 26.50 20.44 9 7 -6 52.11 31.64 -9 7 6 38.09 37.96 -9 7 6 52.78 15.67 -9 -7 6 50.51 32.09 9 7 -5 4.14 6.81 -9 7 5 5.01 9.55 -9 -7 5 6.96 3.82 9 7 -4 42.93 21.67 -9 7 4 45.53 39.29 -9 -7 4 39.16 27.25 9 7 -3 5.62 8.14 -9 7 3 17.50 17.12 -9 -7 3 11.67 8.70 9 7 -2 5.94 5.70 -9 7 2 1.70 5.32 -9 -7 2 2.69 4.07 9 7 -1 2.59 3.47 -9 7 1 7.36 7.85 -9 -7 1 6.08 5.71 9 7 0 7.14 7.30 -9 7 0 6.49 6.94 -9 -7 0 1.73 4.51 9 7 1 125.88 14.66 -9 7 -1 116.13 13.17 -9 -7 -1 78.79 8.67 9 7 2 4.97 4.58 -9 7 -2 14.51 7.29 -9 -7 -2 4.82 3.59 9 7 3 68.45 21.84 -9 7 -3 61.65 40.67 -9 -7 -3 61.11 7.80 9 7 4 31.14 24.58 -9 7 -4 12.57 16.11 -9 -7 -4 18.64 11.73 -9 7 -5 8.17 6.34 -9 -7 -5 11.75 8.00 -9 -7 -5 9.34 8.94 -9 7 -6 2.16 6.45 -9 -7 -6 3.92 6.14 9 8 -10 5.48 8.29 -9 8 10 2.08 8.92 -9 8 10 -0.61 3.72 -9 -8 10 1.49 6.19 9 8 -9 5.69 4.70 -9 8 9 1.53 5.05 -9 8 9 6.46 4.76 -9 -8 9 0.61 4.38 9 8 -8 24.66 12.38 -9 8 8 26.55 21.12 -9 8 8 16.26 19.46 -9 -8 8 23.76 11.55 9 8 -7 14.45 10.45 -9 8 7 16.58 14.43 -9 8 7 9.58 12.66 -9 -8 7 10.13 6.35 9 8 -6 11.68 14.32 -9 8 6 13.93 12.30 -9 -8 6 12.74 11.98 9 8 -5 24.19 16.45 -9 8 5 24.11 19.55 -9 -8 5 20.54 21.89 9 8 -4 0.93 3.60 -9 8 4 3.64 4.11 -9 -8 4 4.11 3.08 9 8 -3 28.02 23.18 -9 8 3 25.24 22.02 -9 -8 3 40.86 23.56 9 8 -2 10.33 8.60 -9 8 2 4.12 7.46 -9 -8 2 5.60 5.99 9 8 -1 5.81 4.06 -9 8 1 9.06 11.05 -9 -8 1 3.50 5.10 9 8 0 12.32 11.54 -9 8 0 11.88 11.32 -9 -8 0 5.45 5.79 9 8 1 17.48 12.44 -9 8 -1 15.48 11.24 -9 -8 -1 13.78 10.48 9 8 2 14.39 12.03 -9 8 -2 20.19 14.00 -9 -8 -2 10.04 10.90 9 8 3 16.76 9.50 -9 8 -3 12.82 6.56 -9 -8 -3 20.33 18.05 9 8 4 30.98 33.72 -9 8 -4 28.46 27.44 -9 -8 -4 27.65 20.50 9 8 5 4.42 7.36 -9 8 -5 4.63 4.47 -9 -8 -5 2.80 2.43 9 9 -9 14.63 12.50 -9 9 9 13.51 10.14 -9 9 9 12.42 10.44 -9 -9 9 4.15 9.34 9 9 -8 18.13 20.23 -9 9 8 5.75 8.00 -9 9 8 16.64 17.05 -9 -9 8 21.44 14.79 9 9 -7 7.96 12.20 -9 9 7 9.53 10.04 -9 -9 7 4.70 3.54 9 9 -6 31.34 13.35 -9 9 6 20.72 16.41 -9 -9 6 23.55 15.95 9 9 -5 -1.69 6.82 -9 9 5 5.13 4.92 -9 -9 5 1.76 4.82 9 9 -4 51.45 34.62 -9 9 4 33.08 23.47 -9 -9 4 42.72 29.18 9 9 -3 3.10 6.18 -9 9 3 3.22 4.44 -9 -9 3 1.46 2.30 9 9 -2 19.46 21.18 -9 9 2 15.61 19.73 -9 -9 2 11.78 10.36 9 9 -1 5.04 3.98 -9 9 1 6.69 9.75 -9 -9 1 -0.03 4.79 9 9 0 3.51 5.51 -9 9 0 4.03 6.95 -9 -9 0 3.98 5.03 9 9 1 70.75 21.28 -9 9 -1 53.80 33.60 -9 -9 -1 59.16 8.02 9 9 2 1.94 2.33 -9 9 -2 2.33 7.10 -9 -9 -2 1.96 3.43 9 9 3 3.65 6.32 -9 9 -3 6.25 7.26 -9 -9 -3 4.96 3.03 9 9 4 9.38 8.54 -9 9 -4 6.23 5.41 -9 -9 -4 5.61 3.95 -9 -9 -5 33.64 28.18 9 10 -8 3.25 7.72 -9 -10 8 4.29 7.47 9 10 -7 4.01 3.61 -9 10 7 1.98 6.13 -9 -10 7 4.60 5.71 9 10 -6 4.22 5.75 -9 10 6 3.92 6.46 -9 -10 6 2.16 4.14 9 10 -5 29.34 16.81 -9 10 5 14.50 16.81 -9 -10 5 15.85 9.99 9 10 -4 3.00 13.75 -9 10 4 13.10 11.69 -9 -10 4 5.19 6.83 9 10 -3 11.59 14.45 -9 10 3 8.78 5.97 -9 -10 3 6.80 4.69 9 10 -2 -1.37 5.22 -9 10 2 1.14 6.81 -9 -10 2 1.66 3.54 9 10 -1 16.30 11.28 -9 10 1 24.86 22.48 -9 -10 1 21.05 19.42 9 10 0 0.90 4.95 -9 10 0 -0.95 7.27 -9 -10 0 0.43 2.43 9 10 1 5.78 7.61 -9 10 -1 7.78 8.20 -9 -10 -1 3.02 3.25 9 10 2 8.64 4.83 -9 10 -2 -2.22 6.44 -9 -10 -2 1.34 2.63 9 10 3 8.35 7.08 -9 10 -3 5.06 7.16 -9 -10 -3 2.65 3.55 9 11 -6 46.90 39.25 -9 11 6 37.27 38.92 -9 -11 6 84.07 13.47 9 11 -5 -1.46 6.26 -9 11 5 5.61 6.19 -9 -11 5 4.20 3.74 9 11 -4 1.63 4.54 -9 11 4 4.80 11.00 -9 -11 4 -0.85 5.46 9 11 -3 3.56 7.91 -9 11 3 4.30 5.53 -9 -11 3 -0.29 5.68 -9 11 2 5.36 7.70 -9 -11 2 4.54 3.84 9 11 -1 1.91 6.32 -9 11 1 5.22 10.62 -9 -11 1 1.02 4.29 9 11 0 0.94 4.23 -9 11 0 2.86 6.52 -9 -11 0 2.14 1.96 9 11 1 4.09 4.42 -9 11 -1 4.61 7.54 -9 -11 -1 3.09 5.68 9 11 2 1.81 7.52 -9 11 -2 7.35 5.52 -9 -11 -2 0.42 3.06 9 12 -3 2.12 6.82 -9 12 3 3.99 5.36 -9 -12 3 5.15 7.16 9 12 -2 -2.28 5.55 -9 12 2 2.70 9.68 -9 -12 2 3.17 4.70 9 12 -1 9.10 10.88 -9 12 1 11.99 12.82 -9 -12 1 8.47 8.57 -10 0 8 6.14 9.93 -10 0 8 4.14 3.94 -10 0 7 1.93 5.21 -10 0 7 2.32 3.03 -10 0 6 5.64 5.37 -10 0 6 -1.05 5.15 -10 0 5 -0.07 3.38 -10 0 5 2.42 4.10 -10 0 4 4.38 4.68 -10 0 4 1.22 2.17 -10 0 3 4.49 7.56 -10 0 3 2.82 2.92 -10 0 2 22.50 17.19 -10 0 1 4.76 9.31 -10 0 0 -2.73 6.13 -10 0 -1 3.55 5.13 -10 0 -2 63.96 27.90 -10 0 -3 5.88 7.54 -10 -1 8 17.26 12.58 -10 1 8 34.21 29.59 -10 1 8 16.70 22.50 -10 -1 8 33.03 7.86 -10 -1 7 1.70 5.65 -10 1 7 3.59 4.12 -10 1 7 1.60 5.98 -10 -1 7 1.27 2.68 -10 -1 6 2.15 3.49 -10 1 6 3.54 7.19 -10 1 6 0.68 2.88 -10 -1 6 -0.62 4.55 -10 -1 5 6.07 5.56 -10 1 5 2.72 3.82 -10 1 5 2.62 3.91 -10 -1 5 4.46 9.00 -10 -1 4 21.38 11.00 -10 1 4 14.05 16.05 -10 -1 4 9.92 11.96 -10 1 4 24.81 5.37 -10 -1 3 13.75 15.33 -10 1 3 8.18 13.51 -10 -1 3 15.86 18.39 -10 -1 2 98.67 33.27 -10 1 2 99.46 26.04 -10 -1 2 113.49 10.61 -10 -1 1 8.87 9.24 -10 1 1 5.03 8.39 -10 -1 0 2.58 5.04 -10 1 0 3.76 9.39 -10 -1 -1 1.34 3.97 -10 1 -1 5.38 5.10 -10 -1 -2 2.81 4.60 -10 1 -2 8.11 5.26 -10 1 -3 2.83 7.87 -10 -1 -3 -2.13 5.89 -10 2 8 34.65 23.00 -10 -2 8 23.96 19.17 -10 2 8 39.08 8.03 -10 -2 8 26.67 26.58 -10 2 7 15.49 11.40 -10 -2 7 10.99 11.16 -10 2 7 14.08 11.04 -10 -2 7 12.12 7.66 -10 2 6 7.44 10.56 -10 -2 6 7.43 14.85 -10 2 6 9.75 6.81 -10 -2 6 8.60 10.40 -10 2 5 10.16 10.12 -10 -2 5 1.15 5.64 -10 2 5 3.58 4.45 -10 -2 5 3.59 9.58 -10 2 4 6.51 12.29 -10 -2 4 9.33 8.29 -10 -2 4 3.25 5.64 -10 2 3 2.43 4.98 -10 -2 3 -6.35 8.06 -10 -2 3 0.80 2.77 -10 2 2 134.82 14.27 -10 -2 2 136.25 13.59 -10 -2 2 140.41 10.80 -10 2 1 4.24 5.21 -10 -2 1 -2.21 6.64 -10 -2 1 1.73 4.62 -10 -2 0 14.28 14.40 -10 2 -1 4.90 7.31 -10 -2 -1 5.48 8.23 -10 2 -2 8.14 8.05 -10 -2 -2 2.58 3.10 -10 2 -3 5.60 9.27 -10 -2 -3 5.18 8.50 -10 3 8 8.01 9.71 -10 -3 8 3.17 5.31 -10 3 7 2.93 3.75 -10 -3 7 0.10 8.88 -10 3 7 1.45 2.82 -10 -3 7 0.52 4.75 -10 3 6 4.76 5.80 -10 -3 6 5.85 8.49 -10 3 6 4.38 4.00 -10 -3 6 0.09 4.21 -10 3 5 0.70 2.96 -10 -3 5 -0.04 3.09 -10 -3 5 0.10 3.18 -10 3 4 5.69 8.28 -10 -3 4 5.02 6.72 -10 -3 4 1.92 3.97 -10 3 3 7.81 8.78 -10 -3 3 3.64 9.01 -10 -3 3 2.07 7.33 -10 3 2 29.53 21.88 -10 -3 2 20.32 21.50 -10 -3 2 23.17 23.07 -10 3 1 24.46 15.20 -10 -3 1 23.80 19.20 -10 -3 1 11.88 14.09 -10 3 0 11.08 6.54 -10 -3 0 4.46 3.36 -10 3 -1 2.66 6.81 -10 -3 -1 3.67 5.52 -10 3 -2 2.87 6.77 -10 -3 -2 2.11 5.46 -10 3 -3 37.08 33.50 -10 -3 -3 59.68 14.41 -10 4 7 5.74 6.13 -10 -4 7 4.88 7.03 -10 4 7 2.26 4.22 -10 -4 7 1.92 5.44 -10 4 6 -1.07 7.19 -10 -4 6 6.46 4.45 -10 -4 6 5.60 4.76 -10 4 5 21.63 8.79 -10 -4 5 21.33 22.14 -10 4 4 23.44 24.67 -10 -4 4 25.30 25.97 -10 -4 4 15.55 12.46 -10 4 3 19.14 13.15 -10 -4 3 15.59 16.37 -10 -4 3 20.49 20.95 -10 4 2 14.57 21.07 -10 -4 2 35.14 19.05 -10 -4 2 20.78 22.72 -10 4 1 2.10 2.47 -10 -4 1 3.03 4.68 -10 -4 1 3.08 2.86 -10 4 0 9.58 7.02 -10 -4 0 6.42 10.34 -10 -4 0 3.76 7.45 -10 4 -1 33.57 27.71 -10 -4 -1 24.52 18.38 -10 4 -2 18.11 11.79 -10 -4 -2 18.10 12.24 -10 5 6 1.97 8.23 -10 -5 6 2.98 3.79 -10 -5 6 3.06 3.93 -10 5 5 35.19 26.65 -10 -5 5 36.11 21.91 -10 -5 5 41.34 9.87 -10 5 4 6.25 7.25 -10 -5 4 2.29 4.90 -10 -5 4 0.31 2.27 -10 5 3 77.71 10.86 -10 -5 3 65.76 11.18 -10 -5 3 74.31 25.53 -10 5 2 4.12 10.72 -10 -5 2 9.84 8.47 -10 -5 2 12.37 10.50 -10 5 1 51.16 32.82 -10 -5 1 41.75 36.75 -10 -5 1 51.93 7.98 -10 5 0 10.19 6.81 -10 -5 0 5.18 8.33 -10 -5 0 6.51 4.06 -10 5 -1 29.56 20.90 -10 -5 -1 14.80 23.33 -10 -5 -1 18.44 19.30 -10 -5 -2 25.33 25.14 -10 6 5 38.04 21.62 -10 -6 5 25.27 27.73 -10 6 4 1.92 4.93 -10 -6 4 6.45 9.49 -10 -6 4 9.10 5.98 -10 6 3 4.56 7.49 -10 -6 3 0.12 7.77 -10 -6 3 4.76 5.37 -10 6 2 19.82 24.01 -10 -6 2 19.51 16.88 -10 -6 2 13.50 11.98 -10 6 1 3.78 8.27 -10 -6 1 4.98 6.15 -10 -6 1 5.98 4.82 -10 -6 0 6.01 7.81 -10 -6 0 6.59 9.42 -10 -7 3 49.70 32.15 10 7 -2 3.87 5.02 -10 -7 2 7.84 8.03 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 89149 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.33806(17) 0.87553(7) 0.13755(8) 0.0425(3) Uani 1 1 d . . . . . O2 O 0.16575(18) 0.88788(7) 0.02178(9) 0.0503(4) Uani 1 1 d . . . . . O3 O 0.00742(16) 0.60055(8) 0.22675(7) 0.0434(3) Uani 1 1 d . . . . . O4 O -0.18734(15) 0.62532(9) 0.12373(9) 0.0544(4) Uani 1 1 d . . . . . O5 O 0.59122(17) 0.79679(8) 0.04486(8) 0.0497(4) Uani 1 1 d . . . . . O6 O 0.62103(16) 0.70156(8) -0.03707(8) 0.0449(3) Uani 1 1 d . . . . . O7 O 0.51480(15) 0.50134(7) 0.12560(8) 0.0430(3) Uani 1 1 d . . . . . O8 O 0.37473(16) 0.53314(7) 0.22955(8) 0.0408(3) Uani 1 1 d . . . . . O9 O 0.20379(16) 0.80225(7) -0.15334(8) 0.0416(3) Uani 1 1 d . . . . . O10 O 0.28647(17) 0.69511(8) -0.19591(7) 0.0462(4) Uani 1 1 d . . . . . O11 O 0.04773(19) 0.53675(8) -0.13063(8) 0.0535(4) Uani 1 1 d . . . . . O12 O -0.15501(17) 0.56502(7) -0.05636(9) 0.0472(3) Uani 1 1 d . U . . . O13 O -0.10296(14) 0.70838(6) -0.15132(7) 0.0321(3) Uani 1 1 d . . . . . O14 O -0.30476(14) 0.69946(6) -0.26233(7) 0.0322(3) Uani 1 1 d . . . . . O15 O -0.41957(16) 0.83225(7) -0.22974(8) 0.0455(4) Uani 1 1 d . . . . . O16 O -0.19761(15) 0.84995(7) -0.13070(7) 0.0356(3) Uani 1 1 d . . . . . N1 N 0.24833(18) 0.85163(7) 0.07633(9) 0.0326(3) Uani 1 1 d . . . . . N2 N 0.23097(16) 0.77447(7) 0.07017(8) 0.0241(3) Uani 1 1 d . . . . . N3 N 0.07476(16) 0.66660(7) 0.11653(8) 0.0237(3) Uani 1 1 d . . . . . N4 N -0.04349(18) 0.62677(8) 0.15858(9) 0.0304(3) Uani 1 1 d . . . . . N5 N 0.56576(17) 0.73283(9) 0.02241(9) 0.0339(3) Uani 1 1 d . . . . . N6 N 0.46990(16) 0.69034(7) 0.06985(8) 0.0249(3) Uani 1 1 d . . . . . N7 N 0.32451(16) 0.59302(7) 0.10642(8) 0.0237(3) Uani 1 1 d . . . . . N8 N 0.41466(17) 0.53927(7) 0.15868(9) 0.0305(3) Uani 1 1 d . . . . . N9 N 0.24319(17) 0.73761(9) -0.14322(8) 0.0324(3) Uani 1 1 d . . . . . N10 N 0.24952(16) 0.71068(7) -0.06006(7) 0.0241(3) Uani 1 1 d . . . . . N11 N 0.10103(16) 0.61112(7) -0.01902(8) 0.0248(3) Uani 1 1 d . . . . . N12 N -0.0107(2) 0.56881(8) -0.07367(9) 0.0352(3) Uani 1 1 d . U . . . C1 C 0.34917(19) 0.72640(8) 0.12006(9) 0.0237(3) Uani 1 1 d . . . . . H1 H 0.409020 0.753006 0.170040 0.028 Uiso 1 1 calc R . . . . C2 C 0.25218(19) 0.65656(8) 0.14809(9) 0.0222(3) Uani 1 1 d . . . . . H2 H 0.268094 0.650830 0.211044 0.027 Uiso 1 1 calc R . . . . C3 C 0.13556(18) 0.74275(8) -0.00392(9) 0.0221(3) Uani 1 1 d . . . . . H3 H 0.057363 0.779860 -0.034337 0.026 Uiso 1 1 calc R . . . . C4 C 0.03569(19) 0.67394(8) 0.02533(9) 0.0227(3) Uani 1 1 d . . . . . H4 H -0.088721 0.679939 0.008940 0.027 Uiso 1 1 calc R . . . . C5 C 0.40375(19) 0.61995(9) 0.03522(9) 0.0249(3) Uani 1 1 d . . . . . H5 H 0.496448 0.586349 0.021576 0.030 Uiso 1 1 calc R . . . . C6 C 0.26396(19) 0.63131(9) -0.04435(9) 0.0252(3) Uani 1 1 d . . . . . H6 H 0.290594 0.603202 -0.095218 0.030 Uiso 1 1 calc R . . . . C7 C -0.1002(3) 0.62172(14) -0.32549(14) 0.0586(6) Uani 1 1 d . . . . . H7A H -0.004146 0.644406 -0.290555 0.088 Uiso 1 1 calc GR . . . . H7B H -0.124043 0.649300 -0.378592 0.088 Uiso 1 1 calc GR . . . . H7C H -0.072758 0.570323 -0.337901 0.088 Uiso 1 1 calc GR . . . . C8 C -0.2526(2) 0.62343(10) -0.27871(12) 0.0406(5) Uani 1 1 d . . . . . H8A H -0.347054 0.597282 -0.312379 0.049 Uiso 1 1 calc R . . . . H8B H -0.226736 0.596984 -0.224215 0.049 Uiso 1 1 calc R . . . . C9 C -0.22047(19) 0.73334(9) -0.19700(10) 0.0259(3) Uani 1 1 d . . . . . C10 C -0.2934(2) 0.81136(9) -0.18792(10) 0.0276(4) Uani 1 1 d . . . . . C11 C -0.2424(2) 0.92897(10) -0.12383(12) 0.0430(5) Uani 1 1 d . . . . . H11A H -0.275525 0.949189 -0.181244 0.052 Uiso 1 1 calc R . . . . H11B H -0.141794 0.956647 -0.098174 0.052 Uiso 1 1 calc R . . . . C12 C -0.3844(3) 0.94034(12) -0.07131(14) 0.0580(6) Uani 1 1 d . . . . . H12A H -0.349752 0.923012 -0.013472 0.087 Uiso 1 1 calc GR . . . . H12B H -0.483722 0.912372 -0.095931 0.087 Uiso 1 1 calc GR . . . . H12C H -0.412624 0.993071 -0.070196 0.087 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0568(8) 0.0263(6) 0.0409(7) -0.0031(5) -0.0092(6) -0.0111(6) O2 0.0672(9) 0.0248(7) 0.0528(8) 0.0090(6) -0.0179(7) 0.0019(6) O3 0.0560(8) 0.0537(8) 0.0217(6) -0.0006(6) 0.0096(6) -0.0245(7) O4 0.0205(7) 0.0691(10) 0.0751(10) 0.0266(8) 0.0121(7) -0.0006(6) O5 0.0549(9) 0.0508(9) 0.0428(8) 0.0081(6) 0.0040(6) -0.0285(7) O6 0.0304(7) 0.0660(9) 0.0414(8) 0.0147(7) 0.0166(6) 0.0091(6) O7 0.0346(7) 0.0326(7) 0.0609(9) 0.0096(6) 0.0020(6) 0.0120(6) O8 0.0586(8) 0.0314(7) 0.0300(7) 0.0109(5) -0.0043(6) -0.0080(6) O9 0.0456(8) 0.0416(8) 0.0381(7) 0.0190(6) 0.0070(6) 0.0052(6) O10 0.0586(9) 0.0592(9) 0.0232(6) 0.0003(6) 0.0143(6) 0.0052(7) O11 0.0681(10) 0.0418(8) 0.0460(8) -0.0232(7) -0.0112(7) 0.0093(7) O12 0.0384(7) 0.0348(7) 0.0648(9) -0.0005(6) -0.0082(6) -0.0141(6) O13 0.0271(6) 0.0357(7) 0.0320(6) 0.0015(5) -0.0033(5) 0.0020(5) O14 0.0310(6) 0.0297(6) 0.0336(6) -0.0027(5) -0.0058(5) 0.0018(5) O15 0.0439(8) 0.0434(8) 0.0450(8) -0.0080(6) -0.0124(6) 0.0148(6) O16 0.0333(7) 0.0314(7) 0.0408(7) -0.0057(5) -0.0004(5) -0.0024(5) N1 0.0407(9) 0.0222(7) 0.0338(8) 0.0015(6) 0.0002(6) -0.0038(6) N2 0.0277(7) 0.0186(6) 0.0248(7) 0.0003(5) -0.0014(5) -0.0013(5) N3 0.0217(7) 0.0270(7) 0.0234(7) 0.0011(5) 0.0063(5) -0.0023(5) N4 0.0314(8) 0.0295(7) 0.0330(8) -0.0025(6) 0.0150(6) -0.0030(6) N5 0.0218(7) 0.0476(9) 0.0315(8) 0.0136(7) 0.0005(6) -0.0034(7) N6 0.0194(7) 0.0304(7) 0.0249(7) 0.0062(5) 0.0031(5) -0.0015(5) N7 0.0243(7) 0.0237(7) 0.0226(7) 0.0031(5) 0.0002(5) 0.0042(5) N8 0.0309(8) 0.0232(7) 0.0348(8) 0.0068(6) -0.0072(6) -0.0045(6) N9 0.0297(8) 0.0443(9) 0.0233(7) 0.0079(6) 0.0033(6) -0.0003(6) N10 0.0250(7) 0.0302(7) 0.0174(6) 0.0045(5) 0.0036(5) 0.0055(5) N11 0.0244(7) 0.0258(7) 0.0229(7) -0.0044(5) -0.0026(5) 0.0003(5) N12 0.0417(7) 0.0213(7) 0.0387(8) -0.0024(6) -0.0107(7) -0.0011(6) C1 0.0249(8) 0.0248(8) 0.0207(7) 0.0023(6) 0.0003(6) -0.0024(6) C2 0.0252(8) 0.0220(7) 0.0194(7) -0.0003(6) 0.0024(6) -0.0027(6) C3 0.0194(7) 0.0238(8) 0.0225(8) 0.0020(6) 0.0005(6) 0.0021(6) C4 0.0190(8) 0.0242(7) 0.0247(8) -0.0011(6) 0.0014(6) 0.0006(6) C5 0.0216(8) 0.0290(8) 0.0241(8) 0.0020(6) 0.0032(6) 0.0047(6) C6 0.0274(8) 0.0282(8) 0.0202(8) -0.0006(6) 0.0040(6) 0.0068(7) C7 0.0511(13) 0.0633(15) 0.0590(14) -0.0185(11) -0.0033(11) 0.0201(11) C8 0.0428(11) 0.0273(9) 0.0477(11) -0.0051(8) -0.0115(9) 0.0024(8) C9 0.0229(8) 0.0317(9) 0.0232(8) 0.0027(6) 0.0034(6) -0.0014(7) C10 0.0268(9) 0.0315(9) 0.0249(8) -0.0006(7) 0.0037(7) -0.0005(7) C11 0.0508(12) 0.0292(9) 0.0492(11) -0.0052(8) 0.0065(9) -0.0034(8) C12 0.0923(17) 0.0344(11) 0.0524(13) -0.0014(9) 0.0299(12) 0.0049(11) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C9 O14 C8 116.53(12) . . ? C10 O16 C11 115.98(14) . . ? O1 N1 N2 116.89(13) . . ? O2 N1 O1 126.57(14) . . ? O2 N1 N2 116.44(13) . . ? N1 N2 C1 120.42(12) . . ? N1 N2 C3 119.33(12) . . ? C3 N2 C1 117.00(12) . . ? N4 N3 C2 116.60(12) . . ? N4 N3 C4 116.34(12) . . ? C2 N3 C4 116.04(12) . . ? O3 N4 O4 126.81(14) . . ? O3 N4 N3 116.95(13) . . ? O4 N4 N3 116.16(13) . . ? O5 N5 O6 126.82(15) . . ? O5 N5 N6 116.96(15) . . ? O6 N5 N6 116.19(15) . . ? N5 N6 C1 119.57(13) . . ? N5 N6 C5 118.67(13) . . ? C5 N6 C1 111.14(12) . . ? N8 N7 C2 117.84(12) . . ? N8 N7 C5 116.90(12) . . ? C5 N7 C2 108.70(12) . . ? O7 N8 N7 116.37(13) . . ? O8 N8 O7 127.50(14) . . ? O8 N8 N7 115.92(14) . . ? O9 N9 O10 127.26(14) . . ? O9 N9 N10 115.92(14) . . ? O10 N9 N10 116.68(14) . . ? N9 N10 C3 118.81(12) . . ? N9 N10 C6 119.69(12) . . ? C6 N10 C3 109.02(11) . . ? N12 N11 C4 119.20(13) . . ? N12 N11 C6 119.31(13) . . ? C6 N11 C4 108.68(12) . . ? O11 N12 O12 126.88(15) . . ? O11 N12 N11 116.94(15) . . ? O12 N12 N11 116.06(14) . . ? N2 C1 N6 113.08(12) . . ? N2 C1 H1 111.4 . . ? N2 C1 C2 109.17(12) . . ? N6 C1 H1 111.4 . . ? N6 C1 C2 100.00(12) . . ? C2 C1 H1 111.4 . . ? N3 C2 N7 110.95(12) . . ? N3 C2 C1 107.00(11) . . ? N3 C2 H2 111.1 . . ? N7 C2 C1 105.39(12) . . ? N7 C2 H2 111.1 . . ? C1 C2 H2 111.1 . . ? N2 C3 N10 110.55(12) . . ? N2 C3 H3 111.4 . . ? N2 C3 C4 107.89(11) . . ? N10 C3 H3 111.4 . . ? N10 C3 C4 103.84(12) . . ? C4 C3 H3 111.4 . . ? N3 C4 N11 111.38(12) . . ? N3 C4 C3 108.17(12) . . ? N3 C4 H4 110.9 . . ? N11 C4 C3 104.36(12) . . ? N11 C4 H4 110.9 . . ? C3 C4 H4 110.9 . . ? N6 C5 H5 111.7 . . ? N6 C5 C6 111.91(12) . . ? N7 C5 N6 99.75(11) . . ? N7 C5 H5 111.7 . . ? N7 C5 C6 109.65(12) . . ? C6 C5 H5 111.7 . . ? N10 C6 C5 107.20(12) . . ? N10 C6 H6 112.4 . . ? N11 C6 N10 103.90(12) . . ? N11 C6 C5 108.01(12) . . ? N11 C6 H6 112.4 . . ? C5 C6 H6 112.4 . . ? H7A C7 H7B 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C8 C7 H7A 109.5 . . ? C8 C7 H7B 109.5 . . ? C8 C7 H7C 109.5 . . ? O14 C8 C7 111.79(16) . . ? O14 C8 H8A 109.3 . . ? O14 C8 H8B 109.3 . . ? C7 C8 H8A 109.3 . . ? C7 C8 H8B 109.3 . . ? H8A C8 H8B 107.9 . . ? O13 C9 O14 126.02(15) . . ? O13 C9 C10 124.25(14) . . ? O14 C9 C10 109.73(13) . . ? O15 C10 O16 126.56(16) . . ? O15 C10 C9 122.54(15) . . ? O16 C10 C9 110.89(13) . . ? O16 C11 H11A 109.2 . . ? O16 C11 H11B 109.2 . . ? O16 C11 C12 112.22(15) . . ? H11A C11 H11B 107.9 . . ? C12 C11 H11A 109.2 . . ? C12 C11 H11B 109.2 . . ? C11 C12 H12A 109.5 . . ? C11 C12 H12B 109.5 . . ? C11 C12 H12C 109.5 . . ? H12A C12 H12B 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 N1 1.2162(17) . ? O2 N1 1.2160(18) . ? O3 N4 1.2084(18) . ? O4 N4 1.2119(18) . ? O5 N5 1.220(2) . ? O6 N5 1.2287(19) . ? O7 N8 1.2185(18) . ? O8 N8 1.2133(17) . ? O9 N9 1.2156(19) . ? O10 N9 1.2174(19) . ? O11 N12 1.2151(19) . ? O12 N12 1.216(2) . ? O13 C9 1.2020(18) . ? O14 C8 1.468(2) . ? O14 C9 1.3187(19) . ? O15 C10 1.1975(19) . ? O16 C10 1.3158(19) . ? O16 C11 1.480(2) . ? N1 N2 1.4040(18) . ? N2 C1 1.4466(19) . ? N2 C3 1.4426(19) . ? N3 N4 1.4162(18) . ? N3 C2 1.453(2) . ? N3 C4 1.453(2) . ? N5 N6 1.3719(18) . ? N6 C1 1.474(2) . ? N6 C5 1.460(2) . ? N7 N8 1.4171(17) . ? N7 C2 1.4776(19) . ? N7 C5 1.4463(19) . ? N9 N10 1.4053(18) . ? N10 C3 1.4676(19) . ? N10 C6 1.459(2) . ? N11 N12 1.3958(18) . ? N11 C4 1.4653(19) . ? N11 C6 1.451(2) . ? C1 H1 1.0000 . ? C1 C2 1.573(2) . ? C2 H2 1.0000 . ? C3 H3 1.0000 . ? C3 C4 1.577(2) . ? C4 H4 1.0000 . ? C5 H5 1.0000 . ? C5 C6 1.596(2) . ? C6 H6 1.0000 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C7 C8 1.499(3) . ? C8 H8A 0.9900 . ? C8 H8B 0.9900 . ? C9 C10 1.539(2) . ? C11 H11A 0.9900 . ? C11 H11B 0.9900 . ? C11 C12 1.500(3) . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 N1 N2 C1 -16.8(2) . . . . ? O1 N1 N2 C3 -175.79(14) . . . . ? O2 N1 N2 C1 166.50(15) . . . . ? O2 N1 N2 C3 7.5(2) . . . . ? O5 N5 N6 C1 24.5(2) . . . . ? O5 N5 N6 C5 166.07(14) . . . . ? O6 N5 N6 C1 -157.46(13) . . . . ? O6 N5 N6 C5 -15.92(19) . . . . ? O9 N9 N10 C3 30.6(2) . . . . ? O9 N9 N10 C6 168.47(13) . . . . ? O10 N9 N10 C3 -153.32(14) . . . . ? O10 N9 N10 C6 -15.4(2) . . . . ? O13 C9 C10 O15 -173.32(17) . . . . ? O13 C9 C10 O16 7.8(2) . . . . ? O14 C9 C10 O15 7.5(2) . . . . ? O14 C9 C10 O16 -171.38(13) . . . . ? N1 N2 C1 N6 -105.60(15) . . . . ? N1 N2 C1 C2 144.03(13) . . . . ? N1 N2 C3 N10 104.18(15) . . . . ? N1 N2 C3 C4 -142.89(13) . . . . ? N2 C1 C2 N3 -2.33(16) . . . . ? N2 C1 C2 N7 115.83(13) . . . . ? N2 C3 C4 N3 -0.02(16) . . . . ? N2 C3 C4 N11 -118.71(12) . . . . ? N4 N3 C2 N7 88.24(15) . . . . ? N4 N3 C2 C1 -157.30(12) . . . . ? N4 N3 C4 N11 -87.73(15) . . . . ? N4 N3 C4 C3 158.14(12) . . . . ? N5 N6 C1 N2 54.62(17) . . . . ? N5 N6 C1 C2 170.58(12) . . . . ? N5 N6 C5 N7 176.19(12) . . . . ? N5 N6 C5 C6 -67.90(16) . . . . ? N6 C1 C2 N3 -121.20(12) . . . . ? N6 C1 C2 N7 -3.04(13) . . . . ? N6 C5 C6 N10 2.01(16) . . . . ? N6 C5 C6 N11 -109.41(14) . . . . ? N7 C5 C6 N10 111.73(13) . . . . ? N7 C5 C6 N11 0.31(16) . . . . ? N8 N7 C2 N3 -129.45(13) . . . . ? N8 N7 C2 C1 115.09(13) . . . . ? N8 N7 C5 N6 -100.83(14) . . . . ? N8 N7 C5 C6 141.57(12) . . . . ? N9 N10 C3 N2 -120.67(14) . . . . ? N9 N10 C3 C4 123.84(13) . . . . ? N9 N10 C6 N11 -110.68(14) . . . . ? N9 N10 C6 C5 135.11(13) . . . . ? N10 C3 C4 N3 117.33(12) . . . . ? N10 C3 C4 N11 -1.36(14) . . . . ? N12 N11 C4 N3 122.63(14) . . . . ? N12 N11 C4 C3 -120.89(14) . . . . ? N12 N11 C6 N10 109.57(14) . . . . ? N12 N11 C6 C5 -136.80(13) . . . . ? C1 N2 C3 N10 -55.56(16) . . . . ? C1 N2 C3 C4 57.37(16) . . . . ? C1 N6 C5 N7 -39.26(14) . . . . ? C1 N6 C5 C6 76.64(15) . . . . ? C2 N3 N4 O3 15.08(19) . . . . ? C2 N3 N4 O4 -167.95(14) . . . . ? C2 N3 C4 N11 55.20(16) . . . . ? C2 N3 C4 C3 -58.93(15) . . . . ? C2 N7 N8 O7 -158.07(13) . . . . ? C2 N7 N8 O8 26.68(18) . . . . ? C2 N7 C5 N6 35.62(14) . . . . ? C2 N7 C5 C6 -81.99(14) . . . . ? C3 N2 C1 N6 53.91(17) . . . . ? C3 N2 C1 C2 -56.46(17) . . . . ? C3 N10 C6 N11 30.89(15) . . . . ? C3 N10 C6 C5 -83.33(14) . . . . ? C4 N3 N4 O3 157.81(14) . . . . ? C4 N3 N4 O4 -25.22(19) . . . . ? C4 N3 C2 N7 -54.60(16) . . . . ? C4 N3 C2 C1 59.86(15) . . . . ? C4 N11 N12 O11 153.81(14) . . . . ? C4 N11 N12 O12 -29.8(2) . . . . ? C4 N11 C6 N10 -31.75(15) . . . . ? C4 N11 C6 C5 81.89(14) . . . . ? C5 N6 C1 N2 -89.56(15) . . . . ? C5 N6 C1 C2 26.39(14) . . . . ? C5 N7 N8 O7 -25.64(18) . . . . ? C5 N7 N8 O8 159.11(13) . . . . ? C5 N7 C2 N3 94.58(13) . . . . ? C5 N7 C2 C1 -20.89(14) . . . . ? C6 N10 C3 N2 97.38(14) . . . . ? C6 N10 C3 C4 -18.11(14) . . . . ? C6 N11 N12 O11 16.5(2) . . . . ? C6 N11 N12 O12 -167.11(14) . . . . ? C6 N11 C4 N3 -96.01(14) . . . . ? C6 N11 C4 C3 20.47(14) . . . . ? C8 O14 C9 O13 2.0(2) . . . . ? C8 O14 C9 C10 -178.83(14) . . . . ? C9 O14 C8 C7 -80.96(19) . . . . ? C10 O16 C11 C12 81.6(2) . . . . ? C11 O16 C10 O15 -6.3(3) . . . . ? C11 O16 C10 C9 172.51(13) . . . . ?