#------------------------------------------------------------------------------ #$Date: 2020-05-07 00:20:09 +0300 (Thu, 07 May 2020) $ #$Revision: 251830 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/04/7240474.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7240474 loop_ _publ_author_name 'Campillo-Alvarado, Gonzalo' 'Keene, Elizabeth' 'Swenson, Dale C.' 'MacGillivray, Len R.' _publ_section_title ; Repurposing of the anti-HIV drug Emtricitabine as a hydrogen-bonded cleft for bipyridines via cocrystallization ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D0CE00474J _journal_year 2020 _chemical_absolute_configuration unk _chemical_formula_moiety '2(C8 H10 F N3 O3 S), 2(C10 H8 N2), H2 O' _chemical_formula_sum 'C36 H38 F2 N10 O7 S2' _chemical_formula_weight 824.895 _chemical_name_systematic '[4-amino-5-fluoro-1-((2R,5S)-2-(hydroxymethyl)-1,3-oxathiolan-5-yl)pyrimidin-2(1H)-one]-[4,4'-bipyridine]' _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _symmetry_Int_Tables_number 4 _atom_sites_solution_primary dual _audit_creation_date 2020-01-28 _audit_creation_method ; Olex2 1.3 (compiled Nov 21 2019 18:26:39 for OlexSys, GUI svn.r6003) ; _audit_update_record ; 2020-02-03 deposited with the CCDC. 2020-05-06 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90.087(4) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 7.4668(10) _cell_length_b 9.6700(14) _cell_length_c 26.187(4) _cell_measurement_reflns_used 9905 _cell_measurement_temperature 150.15 _cell_measurement_theta_max 25.04 _cell_measurement_theta_min 2.245 _cell_volume 1890.8(5) _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine 1.3 (Bourhis et al., 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _diffrn_ambient_temperature 150.15 _diffrn_measured_fraction_theta_full 0.9992 _diffrn_measured_fraction_theta_max 0.9933 _diffrn_measurement_device_type 'Bruker D-8 Venture Duo-Photon 3' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0550 _diffrn_reflns_av_unetI/netI 0.0423 _diffrn_reflns_Laue_measured_fraction_full 0.9992 _diffrn_reflns_Laue_measured_fraction_max 0.9933 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 32 _diffrn_reflns_limit_l_min -32 _diffrn_reflns_number 48450 _diffrn_reflns_point_group_measured_fraction_full 0.9977 _diffrn_reflns_point_group_measured_fraction_max 0.9901 _diffrn_reflns_theta_full 25.2417 _diffrn_reflns_theta_max 26.49 _diffrn_reflns_theta_min 2.25 _exptl_absorpt_coefficient_mu 0.215 _exptl_absorpt_correction_T_max 1.0000 _exptl_absorpt_correction_T_min 0.7869 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0949 before and 0.0706 after correction. The Ratio of minimum to maximum transmission is 0.7869. The \l/2 correction factor is Not present. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.449 _exptl_crystal_description irregular _exptl_crystal_F_000 860.930 _exptl_crystal_size_max 0.115 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.06 _refine_diff_density_max 0.4154 _refine_diff_density_min -0.3906 _refine_diff_density_rms 0.0777 _refine_ls_abs_structure_details 'Flack, H. D. (1983). Acta Cryst. A39, 876-881.' _refine_ls_abs_structure_Flack 0.3(4) _refine_ls_d_res_high 0.7968 _refine_ls_d_res_low 9.0713 _refine_ls_goodness_of_fit_ref 1.0385 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_constraints 70 _refine_ls_number_parameters 508 _refine_ls_number_reflns 7767 _refine_ls_number_restraints 49 _refine_ls_restrained_S_all 1.0351 _refine_ls_R_factor_all 0.0633 _refine_ls_R_factor_gt 0.0559 _refine_ls_shift/su_max 0.0003 _refine_ls_shift/su_mean 0.0000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0265P)^2^+3.6194P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1267 _refine_ls_wR_factor_ref 0.1307 _reflns_Friedel_coverage 0.986 _reflns_limit_h_max 9 _reflns_limit_h_min -9 _reflns_limit_k_max 12 _reflns_limit_k_min -12 _reflns_limit_l_max 32 _reflns_limit_l_min -32 _reflns_number_gt 7060 _reflns_number_total 7767 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL mcg19121d_a.res in P2(1) REM Old TITL Mcg19_121d in P2(1) sample #19180 EMT-Bpv REM SHELXT solution in P2(1): R1 0.311, Rweak 0.272, Alpha 0.058 REM 9.383 for 6 systematic absences, Orientation as input REM Flack x = 0.391 ( 0.031 ) from 2703 Parsons' quotients REM Formula found by SHELXT: C40 N7 O6 F4 S2 CELL 0.71073 7.4668 9.67 26.187 90 90.087 90 ZERR 2 0.001 0.0014 0.004 0 0.004 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H F N O S UNIT 72 76 4 20 14 4 DELU H8 C29 C28 C27 N10 C31 C30 SIMU C29 C28 C27 N10 C31 C30 L.S. 15 PLAN 10 SIZE 0.06 0.1 0.115 TEMP -123 CONF BOND list 4 MORE -1 BOND $H HTAB fmap 2 ACTA BASF 0.5 TWIN 1 0 0 0 -1 0 -0.010651 0 -1 2 WGHT 0.026539 3.619429 FVAR 0.553676 REM REM REM S1 6 0.14468 0.48180 0.03187 11.00000 0.04120 0.03728 0.03785 = 0.00085 0.00636 0.00251 S2 6 0.61978 0.57708 0.50297 11.00000 0.04772 0.04519 0.03631 = 0.00082 -0.00569 -0.00228 F2 3 1.36589 0.67000 0.63169 11.00000 0.02374 0.06261 0.05035 = 0.00940 0.00804 -0.00260 F1 3 0.88618 0.33743 -0.09412 11.00000 0.02576 0.05435 0.04155 = 0.00535 0.00024 0.00378 O6 5 0.71119 0.55877 0.69950 11.00000 0.02100 0.05222 0.03444 = 0.00359 0.00256 -0.00803 O3 5 0.23424 0.47697 -0.16226 11.00000 0.02221 0.03835 0.04302 = 0.00711 -0.00203 0.00452 O2 5 0.25755 0.29496 -0.03348 11.00000 0.03470 0.02810 0.03605 = 0.00098 0.00687 -0.00115 O5 5 0.73095 0.74654 0.57531 11.00000 0.04060 0.03644 0.02933 = 0.00006 -0.00014 0.00463 C15 1 1.19961 0.63197 0.64691 11.00000 0.02238 0.01270 0.05456 = 0.00297 0.00422 0.00559 C6 1 0.69419 0.42724 -0.15956 11.00000 0.03939 0.02675 0.03561 = -0.00402 0.00319 -0.01322 N1 4 0.41711 0.41443 -0.09492 11.00000 0.01775 0.03649 0.03547 = 0.00191 0.00686 0.00726 C12 1 0.74076 0.61209 0.59552 11.00000 0.02349 0.05032 0.02453 = 0.00073 -0.00452 -0.00510 AFIX 13 H12 2 0.62673 0.59008 0.61377 11.00000 -1.20000 AFIX 0 N2 4 0.53086 0.45733 -0.17794 11.00000 0.02532 0.01744 0.03867 = 0.00290 0.00113 0.00004 C5 1 0.38634 0.44975 -0.14631 11.00000 0.03104 0.03153 0.03447 = -0.00152 0.01163 -0.00360 C24 1 0.37693 0.59608 0.39447 11.00000 0.04310 0.06897 0.03312 = 0.00055 -0.00191 0.00842 AFIX 43 H24 2 0.34212 0.55301 0.42551 11.00000 -1.20000 AFIX 0 C22 1 0.40443 0.58576 0.30398 11.00000 0.03289 0.02841 0.04249 = -0.00303 0.00111 0.01120 C16 1 1.06067 0.64393 0.61450 11.00000 0.03342 0.05111 0.02536 = 0.00369 0.00682 -0.01426 AFIX 43 H16 2 1.07841 0.67462 0.58042 11.00000 -1.20000 AFIX 0 N3 4 0.83395 0.44363 -0.19092 11.00000 0.03741 0.05535 0.03425 = 0.00380 0.01217 0.00309 AFIX 93 H3a 2 0.81685 0.47317 -0.22234 11.00000 -1.20000 H3b 2 0.94294 0.42487 -0.18013 11.00000 -1.20000 AFIX 0 O4 5 0.97192 0.75252 0.49021 11.00000 0.04742 0.03059 0.06206 = -0.00507 0.00713 -0.00848 AFIX 147 H4a 2 0.96571 0.69124 0.46754 11.00000 -1.50000 AFIX 0 N4 4 0.89019 0.61030 0.63202 11.00000 0.01643 0.05464 0.03150 = -0.00294 -0.00059 0.01117 N5 4 1.01082 0.56049 0.71447 11.00000 0.02791 0.02041 0.03786 = -0.00336 -0.00257 -0.00578 C21 1 0.33245 0.51143 0.16350 11.00000 0.06973 0.05932 0.02605 = 0.00492 -0.00041 -0.00117 AFIX 43 H21 2 0.30987 0.56314 0.13332 11.00000 -1.20000 AFIX 0 AFIX 66 C29 1 0.87921 0.53224 0.23102 11.00000 0.03002 0.01868 0.06468 = 0.01035 -0.00248 -0.00488 C28 1 0.88719 0.39271 0.21847 11.00000 0.04960 0.05114 0.04052 = 0.01095 0.00544 0.00183 AFIX 43 H28 2 0.90864 0.32579 0.24433 11.00000 -1.20000 AFIX 0 AFIX 65 C27 1 0.86378 0.35110 0.16810 11.00000 0.04800 0.03489 0.05221 = 0.00499 0.00110 -0.00010 AFIX 43 H27 2 0.86923 0.25573 0.15952 11.00000 -1.20000 AFIX 0 AFIX 65 N10 4 0.83240 0.44901 0.13027 11.00000 0.05570 0.04942 0.04560 = 0.00398 -0.00740 -0.00550 C31 1 0.82442 0.58855 0.14282 11.00000 0.04129 0.05306 0.05091 = 0.01470 -0.00144 -0.02387 AFIX 43 H31 2 0.80298 0.65547 0.11696 11.00000 -1.20000 AFIX 0 AFIX 65 C30 1 0.84783 0.63016 0.19319 11.00000 0.04179 0.04355 0.04412 = 0.01617 -0.00071 0.00509 AFIX 43 H30 2 0.84238 0.72552 0.20177 11.00000 -1.20000 AFIX 0 C20 1 0.35300 0.57877 0.20869 11.00000 0.05048 0.01652 0.05298 = 0.00705 0.00147 0.00284 AFIX 43 H20 2 0.34628 0.67688 0.20873 11.00000 -1.20000 AFIX 0 C13 1 0.86701 0.57484 0.68312 11.00000 0.01269 0.01937 0.04443 = -0.00132 -0.00093 -0.00171 N9 4 0.93739 0.65368 0.38872 11.00000 0.06440 0.04936 0.04228 = 0.00440 0.00890 -0.00033 C35 1 0.96936 0.70341 0.29911 11.00000 0.02794 0.03027 0.05300 = 0.00593 0.00453 -0.00476 AFIX 43 H35 2 1.00053 0.76807 0.27330 11.00000 -1.20000 AFIX 0 C18 1 0.39101 0.37087 0.25135 11.00000 0.04767 0.02831 0.04812 = 0.00142 -0.00466 0.01038 AFIX 43 H18 2 0.40934 0.31805 0.28150 11.00000 -1.20000 AFIX 0 N7 4 0.34348 0.37382 0.16082 11.00000 0.04431 0.04544 0.03837 = -0.00553 0.00412 -0.00226 O1 5 0.35812 0.21738 0.07166 11.00000 0.03977 0.04017 0.04435 = -0.00717 -0.00200 -0.00548 AFIX 147 H1 2 0.34163 0.25127 0.10081 11.00000 -1.50000 AFIX 0 AFIX 6 O7 5 0.66776 0.36311 0.03724 11.00000 0.05145 0.05048 0.05313 = -0.00391 0.00420 -0.02559 H7a 2 0.68742 0.40898 0.06527 11.00000 -1.50000 H7b 2 0.58907 0.30088 0.04570 11.00000 -1.50000 AFIX 0 N8 4 0.44667 0.72441 0.39797 11.00000 0.06410 0.03816 0.04248 = -0.00475 -0.00230 0.00769 C14 1 1.17339 0.58742 0.69809 11.00000 0.01520 0.03695 0.03431 = -0.00370 -0.00184 0.00081 C10 1 0.66915 0.75313 0.52356 11.00000 0.03681 0.04140 0.03791 = 0.00095 0.00490 0.00913 AFIX 13 H10 2 0.55469 0.80681 0.52309 11.00000 -1.20000 AFIX 0 C33 1 0.84179 0.49256 0.32545 11.00000 0.02602 0.04807 0.04670 = 0.00553 0.00362 0.00187 AFIX 43 H33 2 0.78180 0.40811 0.31828 11.00000 -1.20000 AFIX 0 C4 1 0.26779 0.42564 -0.05776 11.00000 0.02244 0.01756 0.04299 = 0.00461 0.00758 0.00521 AFIX 13 H4 2 0.15289 0.44743 -0.07570 11.00000 -1.20000 AFIX 0 N6 4 1.31697 0.56603 0.72858 11.00000 0.01665 0.03609 0.04589 = 0.00012 -0.00118 -0.00060 AFIX 93 H6a 2 1.42574 0.57969 0.71671 11.00000 -1.20000 H6b 2 1.30167 0.53845 0.76030 11.00000 -1.20000 AFIX 0 C7 1 0.71963 0.37868 -0.10977 11.00000 0.01574 0.01884 0.04411 = 0.00113 0.00266 0.00305 C32 1 0.86495 0.53193 0.37571 11.00000 0.04579 0.04822 0.04704 = 0.00660 0.01557 0.00220 AFIX 43 H32 2 0.82820 0.47050 0.40199 11.00000 -1.20000 AFIX 0 C3 1 0.30469 0.53040 -0.01628 11.00000 0.03882 0.01810 0.05364 = -0.00046 0.00551 0.00298 AFIX 23 H3c 2 0.28357 0.62591 -0.02850 11.00000 -1.20000 H3d 2 0.42900 0.52266 -0.00339 11.00000 -1.20000 AFIX 0 C23 1 0.35094 0.52044 0.34972 11.00000 0.01749 0.03471 0.05675 = 0.00010 0.00157 0.00247 AFIX 43 H23 2 0.30026 0.43033 0.34999 11.00000 -1.20000 AFIX 0 C25 1 0.49089 0.78136 0.35374 11.00000 0.06357 0.03592 0.04401 = 0.00025 0.00274 0.01848 AFIX 43 H25 2 0.53934 0.87219 0.35435 11.00000 -1.20000 AFIX 0 C8 1 0.58214 0.37562 -0.07736 11.00000 0.02658 0.04523 0.03398 = 0.00748 -0.00009 0.00660 AFIX 43 H8 2 0.59844 0.34719 -0.04294 11.00000 -1.20000 AFIX 0 C2 1 0.13796 0.30003 0.00797 11.00000 0.04090 0.03632 0.02926 = 0.00583 0.00987 -0.00549 AFIX 13 H2 2 0.01431 0.27848 -0.00441 11.00000 -1.20000 AFIX 0 C11 1 0.76625 0.51227 0.55230 11.00000 0.03296 0.03726 0.03377 = -0.00142 0.00245 -0.00403 AFIX 23 H11a 2 0.73170 0.41742 0.56255 11.00000 -1.20000 H11b 2 0.89235 0.51157 0.54068 11.00000 -1.20000 AFIX 0 C19 1 0.38304 0.51238 0.25444 11.00000 0.03042 0.03830 0.03849 = -0.00350 0.00239 -0.00018 C26 1 0.47147 0.71788 0.30676 11.00000 0.04081 0.02934 0.05012 = 0.00019 0.00551 -0.01356 AFIX 43 H26 2 0.50440 0.76550 0.27646 11.00000 -1.20000 AFIX 0 C36 1 0.98908 0.73730 0.35116 11.00000 0.04842 0.03418 0.05454 = 0.00272 0.00952 0.01102 AFIX 43 H36 2 1.04160 0.82367 0.35982 11.00000 -1.20000 AFIX 0 C17 1 0.37261 0.30376 0.20467 11.00000 0.05437 0.04777 0.03925 = -0.00998 -0.00355 -0.00893 AFIX 43 H17 2 0.38077 0.20576 0.20359 11.00000 -1.20000 AFIX 0 C34 1 0.90187 0.57050 0.28598 11.00000 0.03429 0.02875 0.04719 = 0.00861 0.01232 0.01834 C9 1 0.80453 0.83036 0.49146 11.00000 0.04072 0.03805 0.04519 = -0.00666 0.00427 -0.00347 AFIX 23 H9a 2 0.82591 0.92321 0.50618 11.00000 -1.20000 H9b 2 0.75788 0.84220 0.45633 11.00000 -1.20000 AFIX 0 C1 1 0.19157 0.19573 0.04764 11.00000 0.03959 0.03730 0.04968 = 0.00567 0.00731 -0.00862 AFIX 23 H1a 2 0.19357 0.10334 0.03137 11.00000 -1.20000 H1b 2 0.09780 0.19384 0.07432 11.00000 -1.20000 AFIX 0 HKLF 4 END Q1 1 0.166667 0.46875 0 11 0.05 0.42 Q2 1 0.125 0.5 0.066667 11 0.05 0.36 Q3 1 0.875 0.53125 0.188889 11 0.05 0.34 Q4 1 0.333333 0.5 0.388889 11 0.05 0.33 Q5 1 0.958333 0.75 0.455556 11 0.05 0.3 Q6 1 0.375 0.78125 0.244444 11 0.05 0.3 Q7 1 0.166667 0.59375 0.044444 11 0.05 0.28 Q8 1 0.791667 0.625 0.111111 11 0.05 0.28 Q9 1 1 0.5625 0.744444 11 0.05 0.28 Q10 1 0.541667 0.46875 -0.211111 11 0.05 0.28 REM The information below was added by Olex2. REM REM R1 = 0.0559 for 7060 Fo > 4sig(Fo) and 0.0633 for all 7767 data REM 508 parameters refined using 49 restraints REM Highest difference peak 0.4154, deepest hole -0.3906 REM Mean Shift 0.0000, Max Shift 0.0003. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0633 REM R1_gt = 0.0559 REM wR_ref = 0.1307 REM GOOF = 1.0385 REM Shift_max = 0.0003 REM Shift_mean = 0.0000 REM Reflections_all = 7767 REM Reflections_gt = 7060 REM Parameters = 508 REM Hole = -0.3906 REM Peak = 0.4154 REM Flack = 0.3(4) ; _cod_data_source_file d0ce00474j2.cif _cod_data_source_block FTC-bipy _cod_original_sg_symbol_Hall ' P 2yb' _cod_database_code 7240474 _olex2_refinement_description ; 1. Twinned data refinement Scales: 0.5000(16) 0.5000(16) 2. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All N(H,H) groups At 1.5 times of: All O(H) groups, All O(H,H) groups 3. Rigid bond restraints H8, C29, C28, C27, N10, C31, C30 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01 4. Uiso/Uaniso restraints and constraints C29 \\sim C28 \\sim C27 \\sim N10 \\sim C31 \\sim C30: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A 5.a Free rotating group: O7(H7a,H7b) 5.b Ternary CH refined with riding coordinates: C12(H12), C10(H10), C4(H4), C2(H2) 5.c Secondary CH2 refined with riding coordinates: C3(H3c,H3d), C11(H11a,H11b), C9(H9a,H9b), C1(H1a,H1b) 5.d Aromatic/amide H refined with riding coordinates: C24(H24), C16(H16), C21(H21), C28(H28), C27(H27), C31(H31), C30(H30), C20(H20), C35(H35), C18(H18), C33(H33), C32(H32), C23(H23), C25(H25), C8(H8), C26(H26), C36(H36), C17(H17) 5.e Fitted hexagon refined as free rotating group: C29(C28,C27,N10,C31,C30) 5.f X=CH2 refined with riding coordinates: N3(H3a,H3b), N6(H6a,H6b) 5.g Idealised tetrahedral OH refined as rotating group: O4(H4a), O1(H1) ; _iucr_refine_fcf_details ; data_FTC-bipy_CCDC1 _computing_structure_refinement 'olex2.refine 1.3 (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,y+1/2,-z _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_H-M_alt 'P 1 21 1' _space_group_name_Hall ' P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _symmetry_space_group_name_Hall ' P 2yb' _symmetry_Int_Tables_number 4 _cell_length_a 7.4668(10) _cell_length_b 9.6700(14) _cell_length_c 26.187(4) _cell_angle_alpha 90 _cell_angle_beta 90.087(4) _cell_angle_gamma 90 _cell_volume 1890.8(5) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -9 -3 -3 26.855 -0.167 14.580 129.042 o -9 -3 -2 4.828 3.657 12.165 218.360 o -9 -3 -1 23.832 17.415 9.720 206.685 o -9 -3 0 15.085 14.448 9.615 244.628 o -9 -2 -6 32.796 28.767 9.424 176.172 o -9 -2 -5 60.228 47.580 12.634 98.263 o -9 -2 -4 18.753 29.819 14.360 124.472 o -9 -2 -3 14.476 0.001 11.216 222.783 o -9 -2 -2 27.798 32.662 12.650 134.107 o -9 -2 -1 32.203 27.628 11.933 140.987 o -9 -2 0 15.466 26.052 10.240 206.043 o -9 -1 -8 8.974 12.594 10.576 240.785 o -9 -1 -7 16.130 13.409 12.252 174.427 o -9 -1 -6 5.574 9.869 10.242 274.961 o -9 -1 -5 22.681 16.567 14.169 129.905 o -9 -1 -4 16.214 8.160 13.327 158.015 o -9 -1 -3 14.635 25.030 12.938 153.665 o -9 -1 -2 25.591 43.928 13.513 120.191 o -9 -1 -1 66.517 88.300 18.018 60.156 o -9 -1 0 44.204 70.017 26.912 39.051 o -9 0 1 13.555 10.026 12.596 175.984 o -9 0 2 11.497 11.166 10.810 226.488 o -9 0 3 9.735 6.340 9.158 311.365 o -9 0 4 3.782 6.333 10.425 285.513 o -9 0 5 19.247 33.489 13.159 137.562 o -9 0 6 3.368 8.450 11.085 253.661 o -9 0 7 8.306 -6.380 15.658 135.066 o -9 0 8 0.089 5.898 14.107 173.602 o -9 1 1 66.517 88.300 18.018 60.156 o -9 1 2 25.591 43.928 13.513 120.191 o -9 1 3 14.635 25.030 12.938 153.665 o -9 1 4 16.214 8.160 13.327 158.015 o -9 1 5 22.681 16.567 14.169 129.905 o -9 1 6 5.574 9.869 10.242 274.961 o -9 1 7 16.130 13.409 12.252 174.427 o -9 1 8 8.974 12.594 10.576 240.785 o -9 2 1 32.203 27.628 11.933 140.987 o -9 2 2 27.798 32.662 12.650 134.107 o -9 2 3 14.476 0.001 11.216 222.783 o -9 2 4 18.753 29.819 14.360 124.472 o -9 2 5 60.228 47.580 12.634 98.263 o -9 2 6 32.796 28.767 9.424 176.172 o -9 3 1 23.832 17.415 9.720 206.685 o -9 3 2 4.828 3.657 12.165 218.360 o -9 3 3 26.855 -0.167 14.580 129.042 o -8 -6 -4 5.112 12.121 9.839 289.371 o -8 -6 -3 26.563 77.840 11.267 125.125 o -8 -6 -2 140.686 129.467 13.834 51.157 o -8 -6 -1 117.022 114.042 10.936 65.248 o -8 -6 0 2.460 51.310 9.729 220.131 o -8 -5 -10 42.406 39.240 15.327 92.856 o -8 -5 -9 54.653 23.211 18.920 68.996 o -8 -5 -8 9.711 7.531 9.996 270.381 o -8 -5 -7 9.685 8.071 7.966 370.726 o -8 -5 -6 20.580 19.784 8.307 250.829 o -8 -5 -5 41.825 32.420 9.459 155.374 o -8 -5 -4 26.285 37.022 8.770 192.983 o -8 -5 -3 68.297 51.364 10.361 106.342 o -8 -5 -2 98.731 102.651 9.911 76.651 o -8 -5 -1 80.184 95.526 10.097 86.154 o -8 -5 0 53.108 67.019 9.124 121.601 o -8 -4 -13 3.242 43.462 15.604 117.868 o -8 -4 -12 72.615 49.338 11.932 94.251 o -8 -4 -11 8.520 41.181 11.995 167.102 o -8 -4 -10 114.067 107.996 12.634 62.411 o -8 -4 -9 53.494 45.332 13.760 95.545 o -8 -4 -8 73.270 73.280 11.333 90.137 o -8 -4 -7 34.581 33.593 11.668 137.285 o -8 -4 -6 97.447 62.716 12.539 75.700 o -8 -4 -5 13.756 22.995 6.995 325.472 o -8 -4 -4 80.325 62.164 8.435 104.184 o -8 -4 -3 27.515 43.655 9.778 166.288 o -8 -4 -2 52.209 41.420 14.353 93.382 o -8 -4 -1 62.986 82.202 9.715 102.665 o -8 -4 0 130.527 124.082 11.433 59.020 o -8 -3 -14 22.465 8.581 16.005 111.622 o -8 -3 -13 37.296 42.541 13.183 113.296 o -8 -3 -12 58.195 43.504 10.680 115.942 o -8 -3 -11 31.410 22.693 9.139 191.308 o -8 -3 -10 20.605 24.790 9.293 215.369 o -8 -3 -9 41.276 25.576 11.017 141.738 o -8 -3 -8 13.433 7.419 9.845 258.867 o -8 -3 -7 137.858 180.402 19.490 37.851 o -8 -3 -6 55.589 71.902 12.260 95.830 o -8 -3 -5 42.788 42.207 11.313 126.396 o -8 -3 -4 70.336 44.647 10.291 107.845 o -8 -3 -3 34.819 22.067 7.355 216.587 o -8 -3 -2 31.242 40.244 6.379 216.518 o -8 -3 -1 32.981 27.806 7.380 212.875 o -8 -3 0 20.104 28.163 6.175 296.090 o -8 -2 -16 43.444 31.056 13.550 109.553 o -8 -2 -15 15.195 -2.041 15.903 123.676 o -8 -2 -14 37.884 35.200 12.756 120.388 o -8 -2 -13 27.784 6.901 10.356 195.847 o -8 -2 -12 50.263 65.591 11.292 108.528 o -8 -2 -11 163.556 125.608 13.941 47.349 o -8 -2 -10 46.423 38.567 9.329 145.079 o -8 -2 -9 61.990 71.437 10.490 102.707 o -8 -2 -8 59.552 72.355 12.011 94.743 o -8 -2 -7 108.358 106.279 10.902 69.332 o -8 -2 -6 37.591 53.166 8.113 161.402 o -8 -2 -5 77.458 78.377 9.688 94.379 o -8 -2 -4 77.076 93.988 9.260 91.867 o -8 -2 -3 41.653 74.345 10.148 121.379 o -8 -2 -2 33.074 74.793 8.528 146.620 o -8 -2 -1 181.088 166.937 9.416 47.832 o -8 -2 0 34.218 85.082 10.302 122.183 o -8 -1 -16 18.538 22.089 12.472 157.670 o -8 -1 -15 53.863 40.114 13.055 102.203 o -8 -1 -14 23.366 -5.142 16.310 111.055 o -8 -1 -13 36.403 2.512 14.174 122.588 o -8 -1 -12 96.939 96.197 41.754 17.059 o -8 -1 -11 34.205 27.836 12.029 136.969 o -8 -1 -10 22.912 25.710 12.618 145.667 o -8 -1 -9 30.038 19.538 10.236 177.935 o -8 -1 -8 0.822 6.524 15.658 140.470 o -8 -1 -7 21.503 16.311 8.266 255.576 o -8 -1 -6 132.589 156.584 27.770 27.686 o -8 -1 -5 90.842 118.774 22.606 40.682 o -8 -1 -4 192.543 189.909 17.948 34.389 o -8 -1 -3 155.734 185.106 13.932 44.090 o -8 -1 -2 77.699 134.715 13.555 66.297 o -8 -1 -1 101.014 107.345 9.323 76.603 o -8 -1 0 72.637 98.086 9.495 92.233 o -8 0 1 30.394 103.738 18.594 65.567 o -8 0 2 11.801 11.164 6.462 427.527 o -8 0 3 15.064 29.796 7.459 279.412 o -8 0 4 6.161 32.371 8.993 265.458 o -8 0 5 112.589 73.848 9.375 78.620 o -8 0 6 10.074 17.100 9.037 282.713 o -8 0 7 87.052 59.846 9.313 95.973 o -8 0 8 117.846 102.215 42.569 16.073 o -8 0 9 9.340 6.248 8.250 364.847 o -8 0 10 55.652 39.830 12.339 106.499 o -8 0 11 24.451 1.882 13.831 141.725 o -8 0 12 22.662 26.514 13.400 134.357 o -8 0 13 21.202 3.588 17.615 97.894 o -8 0 14 9.603 28.123 11.253 194.794 o -8 0 15 88.217 53.324 13.454 77.485 o -8 0 16 8.055 27.022 16.963 105.390 o -8 0 17 15.848 30.733 14.048 131.241 o -8 1 1 101.014 107.345 9.323 76.603 o -8 1 2 77.699 134.715 13.555 66.297 o -8 1 3 155.734 185.106 13.932 44.090 o -8 1 4 192.543 189.909 17.948 34.389 o -8 1 5 90.842 118.774 22.606 40.682 o -8 1 6 132.589 156.584 27.770 27.686 o -8 1 7 21.503 16.311 8.266 255.576 o -8 1 8 0.822 6.524 15.658 140.470 o -8 1 9 30.038 19.538 10.236 177.935 o -8 1 10 22.912 25.710 12.618 145.667 o -8 1 11 34.205 27.836 12.029 136.969 o -8 1 12 96.939 96.197 41.754 17.059 o -8 1 13 36.403 2.512 14.174 122.588 o -8 1 14 23.366 -5.142 16.310 111.055 o -8 1 15 53.863 40.114 13.055 102.203 o -8 1 16 18.538 22.089 12.472 157.670 o -8 2 1 181.088 166.937 9.416 47.832 o -8 2 2 33.074 74.793 8.528 146.620 o -8 2 3 41.653 74.345 10.148 121.379 o -8 2 4 77.076 93.988 9.260 91.867 o -8 2 5 77.458 78.377 9.688 94.379 o -8 2 6 37.591 53.166 8.113 161.402 o -8 2 7 108.358 106.279 10.902 69.332 o -8 2 8 59.552 72.355 12.011 94.743 o -8 2 9 61.990 71.437 10.490 102.707 o -8 2 10 46.423 38.567 9.329 145.079 o -8 2 11 163.556 125.608 13.941 47.349 o -8 2 12 50.263 65.591 11.292 108.528 o -8 2 13 27.784 6.901 10.356 195.847 o -8 2 14 37.884 35.200 12.756 120.388 o -8 2 15 15.195 -2.041 15.903 123.676 o -8 2 16 43.444 31.056 13.550 109.553 o -8 3 1 32.981 27.806 7.380 212.875 o -8 3 2 31.242 40.244 6.379 216.518 o -8 3 3 34.819 22.067 7.355 216.587 o -8 3 4 70.336 44.647 10.291 107.845 o -8 3 5 42.788 42.207 11.313 126.396 o -8 3 6 55.589 71.902 12.260 95.830 o -8 3 7 137.858 180.402 19.490 37.851 o -8 3 8 13.433 7.419 9.845 258.867 o -8 3 9 41.276 25.576 11.017 141.738 o -8 3 10 20.605 24.790 9.293 215.369 o -8 3 11 31.410 22.693 9.139 191.308 o -8 3 12 58.195 43.504 10.680 115.942 o -8 3 13 37.296 42.541 13.183 113.296 o -8 3 14 22.465 8.581 16.005 111.622 o -8 4 1 62.986 82.202 9.715 102.665 o -8 4 2 52.209 41.420 14.353 93.382 o -8 4 3 27.515 43.655 9.778 166.288 o -8 4 4 80.325 62.164 8.435 104.184 o -8 4 5 13.756 22.995 6.995 325.472 o -8 4 6 97.447 62.716 12.539 75.700 o -8 4 7 34.581 33.593 11.668 137.285 o -8 4 8 73.270 73.280 11.333 90.137 o -8 4 9 53.494 45.332 13.760 95.545 o -8 4 10 114.067 107.996 12.634 62.411 o -8 4 11 8.520 41.181 11.995 167.102 o -8 4 12 72.615 49.338 11.932 94.251 o -8 4 13 3.242 43.462 15.604 117.868 o -8 5 1 80.184 95.526 10.097 86.154 o -8 5 2 98.731 102.651 9.911 76.651 o -8 5 3 68.297 51.364 10.361 106.342 o -8 5 4 26.285 37.022 8.770 192.983 o -8 5 5 41.825 32.420 9.459 155.374 o -8 5 6 20.580 19.784 8.307 250.829 o -8 5 7 9.685 8.071 7.966 370.726 o -8 5 8 9.711 7.531 9.996 270.381 o -8 5 9 54.653 23.211 18.920 68.996 o -8 5 10 42.406 39.240 15.327 92.856 o -8 6 1 117.022 114.042 10.936 65.248 o -8 6 2 140.686 129.467 13.834 51.157 o -8 6 3 26.563 77.840 11.267 125.125 o -8 6 4 5.112 12.121 9.839 289.371 o -7 -8 -2 30.086 63.283 21.203 59.734 o -7 -8 -1 50.787 54.812 16.537 77.195 o -7 -8 0 1.421 22.616 12.656 187.610 o -7 -7 -10 32.584 23.401 8.288 203.348 o -7 -7 -9 43.677 22.520 10.005 153.343 o -7 -7 -8 55.908 64.381 9.444 117.767 o -7 -7 -7 159.779 111.060 11.758 53.285 o -7 -7 -6 56.781 88.373 9.243 107.818 o -7 -7 -5 58.306 85.730 10.567 99.788 o -7 -7 -4 177.158 175.400 16.508 38.373 o -7 -7 -3 95.655 119.198 11.783 68.758 o -7 -7 -2 69.265 119.108 11.666 79.235 o -7 -7 -1 213.037 143.430 15.011 38.199 o -7 -7 0 38.425 71.393 10.600 122.295 o -7 -6 -14 19.794 20.333 9.244 226.694 o -7 -6 -13 74.588 37.422 9.133 115.087 o -7 -6 -12 38.172 22.797 8.645 183.596 o -7 -6 -11 43.377 30.082 8.175 171.516 o -7 -6 -10 29.233 26.895 8.446 204.833 o -7 -6 -9 7.425 10.117 9.214 311.341 o -7 -6 -8 81.753 69.325 7.572 104.598 o -7 -6 -7 55.309 41.020 7.742 146.403 o -7 -6 -6 32.059 47.658 8.041 178.678 o -7 -6 -5 78.049 74.719 10.090 93.181 o -7 -6 -4 176.655 163.838 14.724 41.575 o -7 -6 -3 22.019 81.393 7.903 166.608 o -7 -6 -2 239.348 224.254 11.617 35.062 o -7 -6 -1 96.847 133.871 9.971 71.216 o -7 -6 0 98.512 105.786 8.701 79.923 o -7 -5 -17 21.116 -1.957 20.225 77.856 o -7 -5 -16 4.779 7.362 12.737 196.114 o -7 -5 -15 36.256 23.776 12.550 130.559 o -7 -5 -14 85.678 68.208 13.616 74.799 o -7 -5 -13 36.913 41.002 9.591 154.709 o -7 -5 -12 71.044 43.094 9.605 112.526 o -7 -5 -11 46.326 26.711 7.913 172.447 o -7 -5 -10 45.199 62.591 13.513 97.080 o -7 -5 -9 54.569 62.015 10.379 113.185 o -7 -5 -8 73.202 65.928 15.539 71.479 o -7 -5 -7 71.313 66.875 8.588 108.572 o -7 -5 -6 45.343 42.088 6.882 171.459 o -7 -5 -5 32.139 47.397 7.493 186.728 o -7 -5 -4 158.487 190.022 11.436 46.977 o -7 -5 -3 202.373 224.591 14.596 35.705 o -7 -5 -2 75.365 118.136 9.969 83.421 o -7 -5 -1 320.588 361.837 16.393 23.000 o -7 -5 0 496.477 544.696 22.103 14.167 o -7 -4 -18 42.261 9.937 13.409 121.652 o -7 -4 -17 72.959 37.901 16.238 73.397 o -7 -4 -16 37.634 27.891 12.641 125.662 o -7 -4 -15 33.341 19.374 10.560 165.910 o -7 -4 -14 7.877 30.974 11.565 188.255 o -7 -4 -13 244.006 196.353 19.252 29.054 o -7 -4 -12 73.602 73.781 10.779 92.657 o -7 -4 -11 108.659 115.727 11.493 66.024 o -7 -4 -10 79.709 56.177 10.017 98.391 o -7 -4 -9 32.640 26.670 7.908 205.717 o -7 -4 -8 104.384 111.462 8.807 75.907 o -7 -4 -7 111.123 71.458 11.741 71.796 o -7 -4 -6 89.638 106.915 11.621 73.597 o -7 -4 -5 161.819 150.357 9.334 52.949 o -7 -4 -4 59.258 103.825 8.523 103.908 o -7 -4 -3 365.850 358.190 15.467 21.749 o -7 -4 -2 152.195 244.544 11.299 44.035 o -7 -4 -1 330.165 282.286 18.539 23.105 o -7 -4 0 47.194 97.407 7.458 123.571 o -7 -3 -20 22.318 9.400 9.652 225.887 o -7 -3 -19 16.412 12.837 9.522 245.496 o -7 -3 -18 66.849 42.437 16.368 74.192 o -7 -3 -17 65.365 28.500 11.226 111.907 o -7 -3 -16 31.742 9.505 11.112 169.020 o -7 -3 -15 33.055 22.952 9.148 186.821 o -7 -3 -14 39.360 18.858 8.400 189.506 o -7 -3 -13 106.867 93.683 10.477 73.399 o -7 -3 -12 158.771 110.943 14.172 48.928 o -7 -3 -11 70.369 65.415 10.096 101.204 o -7 -3 -10 155.127 150.862 29.092 25.240 o -7 -3 -9 192.412 183.718 11.180 42.840 o -7 -3 -8 129.685 175.901 16.893 43.403 o -7 -3 -7 78.730 90.556 10.688 85.646 o -7 -3 -6 110.539 138.570 8.374 69.675 o -7 -3 -5 185.330 195.521 12.637 41.278 o -7 -3 -4 255.349 273.892 18.015 27.153 o -7 -3 -3 235.619 272.703 15.629 30.227 o -7 -3 -2 236.802 211.285 9.578 37.521 o -7 -3 -1 97.695 173.237 11.704 60.475 o -7 -3 0 607.661 537.850 21.151 12.780 o -7 -2 -21 19.760 19.504 14.866 122.486 o -7 -2 -20 91.108 58.183 19.951 51.724 o -7 -2 -19 7.145 -8.711 9.480 334.376 o -7 -2 -18 83.853 74.970 13.258 75.711 o -7 -2 -17 46.638 30.519 11.360 128.127 o -7 -2 -16 40.810 24.436 11.754 134.181 o -7 -2 -15 36.408 30.691 11.056 144.476 o -7 -2 -14 52.601 38.269 11.378 117.775 o -7 -2 -13 15.865 35.677 9.640 205.166 o -7 -2 -12 208.478 182.814 13.164 38.726 o -7 -2 -11 92.303 77.612 15.820 62.627 o -7 -2 -10 48.688 52.440 8.802 137.791 o -7 -2 -9 59.082 47.586 9.763 120.436 o -7 -2 -8 207.802 229.276 21.332 28.305 o -7 -2 -7 253.922 237.903 20.629 26.171 o -7 -2 -6 65.588 60.142 8.607 116.402 o -7 -2 -5 155.105 155.822 9.829 53.004 o -7 -2 -4 264.859 293.951 13.419 29.198 o -7 -2 -3 254.756 311.726 17.835 26.308 o -7 -2 -2 375.239 346.421 18.303 20.441 o -7 -2 -1 360.402 461.871 18.156 19.198 o -7 -2 0 351.984 472.306 22.635 17.562 o -7 -1 -21 97.174 47.258 12.477 79.301 o -7 -1 -20 18.824 15.360 9.146 242.334 o -7 -1 -19 30.136 15.239 9.368 199.796 o -7 -1 -18 82.471 66.296 23.161 43.709 o -7 -1 -17 7.241 11.549 9.741 283.555 o -7 -1 -16 22.893 2.773 9.456 241.747 o -7 -1 -15 67.070 61.538 10.287 103.864 o -7 -1 -14 117.400 82.963 11.029 69.842 o -7 -1 -13 36.966 14.410 9.106 188.437 o -7 -1 -12 9.347 3.333 10.138 276.858 o -7 -1 -11 13.066 37.808 12.602 151.616 o -7 -1 -10 231.945 225.732 33.761 17.831 o -7 -1 -9 282.118 261.818 15.467 27.786 o -7 -1 -8 180.255 165.622 26.036 26.848 o -7 -1 -7 157.254 183.549 19.530 35.761 o -7 -1 -6 247.576 253.653 13.919 31.396 o -7 -1 -5 166.755 172.462 12.867 45.003 o -7 -1 -4 195.729 227.692 21.366 29.042 o -7 -1 -3 253.909 181.399 21.298 27.092 o -7 -1 -2 99.174 177.103 18.571 44.288 o -7 -1 -1 350.570 320.685 19.534 21.121 o -7 -1 0 99.741 123.739 6.807 80.598 o -7 0 1 502.476 518.422 70.154 5.161 o -7 0 2 396.365 444.967 42.294 10.530 o -7 0 3 232.401 242.751 16.102 31.094 o -7 0 4 214.812 222.959 17.226 32.060 o -7 0 5 103.488 143.440 12.546 60.740 o -7 0 6 194.132 203.885 18.212 33.369 o -7 0 7 518.164 545.913 41.916 9.276 o -7 0 8 163.354 130.237 12.322 49.791 o -7 0 9 119.647 124.995 24.243 34.524 o -7 0 10 170.078 115.354 15.020 45.267 o -7 0 11 83.563 78.928 12.709 77.355 o -7 0 12 19.341 7.199 11.154 199.097 o -7 0 13 8.656 3.989 7.916 405.260 o -7 0 14 145.072 105.728 13.908 52.428 o -7 0 15 30.226 49.641 10.270 149.737 o -7 0 16 73.228 41.434 9.353 113.035 o -7 0 17 164.437 149.969 15.675 42.577 o -7 0 18 89.975 76.971 13.653 71.426 o -7 0 19 12.834 12.794 9.211 272.690 o -7 0 20 44.973 48.380 12.816 107.696 o -7 0 21 39.740 41.769 12.066 122.257 o -7 1 1 350.570 320.685 19.534 21.121 o -7 1 2 99.174 177.103 18.571 44.288 o -7 1 3 253.909 181.399 21.298 27.092 o -7 1 4 195.729 227.692 21.366 29.042 o -7 1 5 166.755 172.462 12.867 45.003 o -7 1 6 247.576 253.653 13.919 31.396 o -7 1 7 157.254 183.549 19.530 35.761 o -7 1 8 180.255 165.622 26.036 26.848 o -7 1 9 282.118 261.818 15.467 27.786 o -7 1 10 231.945 225.732 33.761 17.831 o -7 1 11 13.066 37.808 12.602 151.616 o -7 1 12 9.347 3.333 10.138 276.858 o -7 1 13 36.966 14.410 9.106 188.437 o -7 1 14 117.400 82.963 11.029 69.842 o -7 1 15 67.070 61.538 10.287 103.864 o -7 1 16 22.893 2.773 9.456 241.747 o -7 1 17 7.241 11.549 9.741 283.555 o -7 1 18 82.471 66.296 23.161 43.709 o -7 1 19 30.136 15.239 9.368 199.796 o -7 1 20 18.824 15.360 9.146 242.334 o -7 1 21 97.174 47.258 12.477 79.301 o -7 2 1 360.402 461.871 18.156 19.198 o -7 2 2 375.239 346.421 18.303 20.441 o -7 2 3 254.756 311.726 17.835 26.308 o -7 2 4 264.859 293.951 13.419 29.198 o -7 2 5 155.105 155.822 9.829 53.004 o -7 2 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62.679 16.696 80.018 o 8 2 7 109.596 113.883 13.860 59.446 o 8 2 8 59.378 72.385 17.286 67.304 o 8 2 9 62.882 73.658 13.479 84.215 o 8 2 10 45.463 16.636 17.289 83.392 o 8 2 11 162.060 125.429 17.491 41.457 o 8 2 12 49.057 15.005 18.594 74.138 o 8 2 13 28.046 19.567 12.147 149.717 o 8 2 14 38.399 46.689 10.726 135.068 o 8 2 15 15.270 14.491 12.122 177.838 o 8 2 16 42.756 27.401 21.203 61.049 o 8 3 0 20.104 28.163 6.175 296.090 o 8 3 1 33.049 34.843 9.922 162.079 o 8 3 2 30.448 39.651 9.087 175.019 o 8 3 3 34.491 50.438 14.426 101.399 o 8 3 4 71.103 77.088 14.018 77.066 o 8 3 5 42.681 66.611 10.242 123.502 o 8 3 6 56.450 76.375 10.364 105.805 o 8 3 7 139.455 107.478 27.208 29.409 o 8 3 8 13.407 13.531 11.416 199.981 o 8 3 9 40.780 28.430 13.575 112.682 o 8 3 10 21.367 12.532 10.114 211.704 o 8 3 11 31.464 20.509 8.508 206.357 o 8 3 12 57.989 54.515 18.833 63.667 o 8 3 13 37.742 12.102 11.321 152.805 o 8 3 14 22.852 25.444 21.529 65.163 o 8 4 0 130.527 124.082 11.433 59.020 o 8 4 1 63.743 93.529 8.425 104.914 o 8 4 2 53.489 61.132 12.137 101.671 o 8 4 3 28.602 42.252 14.190 111.212 o 8 4 4 79.127 44.429 11.078 96.700 o 8 4 5 12.321 22.391 9.520 242.778 o 8 4 6 98.076 75.181 10.009 82.675 o 8 4 7 35.435 42.891 9.597 155.512 o 8 4 8 74.585 90.357 12.559 79.397 o 8 4 9 53.844 57.774 14.976 84.081 o 8 4 10 113.591 128.755 19.820 43.047 o 8 4 11 8.736 30.237 10.861 203.884 o 8 4 12 72.285 83.405 10.695 91.039 o 8 4 13 3.481 18.594 23.487 61.499 o 8 5 0 53.108 67.019 9.124 121.601 o 8 5 1 80.967 91.833 11.614 80.306 o 8 5 2 98.765 108.899 9.305 77.269 o 8 5 3 67.112 69.108 10.183 101.700 o 8 5 4 26.464 52.866 9.146 168.851 o 8 5 5 42.703 34.547 9.331 153.812 o 8 5 6 20.482 18.147 9.958 209.802 o 8 5 7 9.878 10.015 9.436 286.531 o 8 5 8 9.928 3.554 11.988 208.269 o 8 5 9 54.059 33.890 12.576 108.205 o 8 5 10 42.418 46.354 18.845 69.592 o 8 6 0 2.460 51.310 9.729 220.131 o 8 6 1 117.244 120.524 12.638 59.915 o 8 6 2 142.028 126.169 15.414 48.041 o 8 6 3 26.605 37.141 15.708 100.516 o 8 6 4 5.230 20.585 14.117 151.271 o 9 -3 -3 26.388 13.189 12.902 145.398 o 9 -3 -2 4.476 1.043 9.909 324.919 o 9 -3 -1 22.695 19.573 9.973 201.064 o 9 -2 -7 26.672 21.054 16.588 98.048 o 9 -2 -6 33.017 23.959 12.062 140.641 o 9 -2 -5 60.601 51.353 11.677 103.280 o 9 -2 -4 18.627 23.678 9.997 206.182 o 9 -2 -3 14.549 19.366 12.555 165.640 o 9 -2 -2 27.953 32.124 11.442 150.683 o 9 -2 -1 32.578 33.915 11.233 145.346 o 9 -1 -8 8.633 18.568 10.666 228.034 o 9 -1 -7 15.623 23.317 9.700 223.681 o 9 -1 -6 5.780 -0.299 11.223 256.051 o 9 -1 -5 22.911 8.571 13.864 138.820 o 9 -1 -4 16.451 14.259 10.305 219.405 o 9 -1 -3 14.714 18.502 9.881 230.156 o 9 -1 -2 25.582 37.065 9.711 177.908 o 9 -1 -1 66.180 43.287 11.738 101.738 o 9 0 0 40.009 71.765 16.608 77.753 o 9 0 1 13.555 10.026 12.596 175.984 o 9 0 2 11.497 11.166 10.810 226.488 o 9 0 3 9.735 6.340 9.158 311.365 o 9 0 4 3.782 6.333 10.425 285.513 o 9 0 5 19.247 33.489 13.159 137.562 o 9 0 6 3.368 8.450 11.085 253.661 o 9 0 7 8.306 -6.380 15.658 135.066 o 9 0 8 0.089 5.898 14.107 173.602 o 9 1 0 44.204 70.017 26.912 39.051 o 9 1 1 66.180 43.287 11.738 101.738 o 9 1 2 25.582 37.065 9.711 177.908 o 9 1 3 14.714 18.502 9.881 230.156 o 9 1 4 16.451 14.259 10.305 219.405 o 9 1 5 22.911 8.571 13.864 138.820 o 9 1 6 5.780 -0.299 11.223 256.051 o 9 1 7 15.623 23.317 9.700 223.681 o 9 1 8 8.633 18.568 10.666 228.034 o 9 2 0 15.466 26.052 10.240 206.043 o 9 2 1 32.578 33.915 11.233 145.346 o 9 2 2 27.953 32.124 11.442 150.683 o 9 2 3 14.549 19.366 12.555 165.640 o 9 2 4 18.627 23.678 9.997 206.182 o 9 2 5 60.601 51.353 11.677 103.280 o 9 2 6 33.017 23.959 12.062 140.641 o 9 2 7 26.672 21.054 16.588 98.048 o 9 3 0 15.085 14.448 9.615 244.628 o 9 3 1 22.695 19.573 9.973 201.064 o 9 3 2 4.476 1.043 9.909 324.919 o 9 3 3 26.388 13.189 12.902 145.398 o ; _olex2_date_sample_data_collection 2020-01-08 _olex2_date_sample_submission 2020-01-07 _olex2_submission_original_sample_id FTC-bipy _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,y+1/2,-z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp S1 S 0.1447(2) 0.48180(15) 0.03187(6) 0.0388(3) Uani 1.000000 . . S2 S 0.6198(2) 0.57708(17) 0.50297(6) 0.0431(4) Uani 1.000000 . . F2 F 1.3659(5) 0.6700(4) 0.63169(13) 0.0456(9) Uani 1.000000 . . F1 F 0.8862(5) 0.3374(4) -0.09412(13) 0.0406(8) Uani 1.000000 . . O6 O 0.7112(5) 0.5588(5) 0.69950(14) 0.0359(9) Uani 1.000000 . . O3 O 0.2342(5) 0.4770(4) -0.16226(15) 0.0345(9) Uani 1.000000 . . O2 O 0.2576(5) 0.2950(4) -0.03348(15) 0.0329(9) Uani 1.000000 . . O5 O 0.7310(6) 0.7465(4) 0.57531(14) 0.0355(9) Uani 1.000000 . . C15 C 1.1996(7) 0.6320(5) 0.6469(2) 0.0299(12) Uani 1.000000 . . C6 C 0.6942(9) 0.4272(6) -0.1596(2) 0.0339(13) Uani 1.000000 . . N1 N 0.4171(6) 0.4144(5) -0.09492(18) 0.0299(11) Uani 1.000000 . . C12 C 0.7408(8) 0.6121(6) 0.59552(19) 0.0328(14) Uani 1.000000 . . H12 H 0.6267(8) 0.5901(6) 0.61377(19) 0.0393(16) Uiso 1.000000 R . N2 N 0.5309(6) 0.4573(4) -0.17794(18) 0.0271(10) Uani 1.000000 . . C5 C 0.3863(8) 0.4497(6) -0.1463(2) 0.0323(12) Uani 1.000000 . . C24 C 0.3769(10) 0.5961(8) 0.3945(2) 0.0484(16) Uani 1.000000 . . H24 H 0.3421(10) 0.5530(8) 0.4255(2) 0.058(2) Uiso 1.000000 R . C22 C 0.4044(8) 0.5858(6) 0.3040(2) 0.0346(12) Uani 1.000000 . . C16 C 1.0607(8) 0.6439(7) 0.6145(2) 0.0366(14) Uani 1.000000 . . H16 H 1.0784(8) 0.6746(7) 0.5804(2) 0.0439(16) Uiso 1.000000 R . N3 N 0.8339(7) 0.4436(5) -0.19092(18) 0.0423(13) Uani 1.000000 . . H3a H 0.8169(7) 0.4732(5) -0.22234(18) 0.0508(15) Uiso 1.000000 R . H3b H 0.9429(7) 0.4249(5) -0.18013(18) 0.0508(15) Uiso 1.000000 R . O4 O 0.9719(6) 0.7525(5) 0.49021(18) 0.0467(12) Uani 1.000000 . . H4a H 0.966(4) 0.691(6) 0.468(2) 0.0700(17) Uiso 1.000000 GR . N4 N 0.8902(6) 0.6103(5) 0.63202(17) 0.0342(12) Uani 1.000000 . . N5 N 1.0108(6) 0.5605(5) 0.71447(17) 0.0287(10) Uani 1.000000 . . C21 C 0.3324(11) 0.5114(7) 0.1635(2) 0.0517(18) Uani 1.000000 . . H21 H 0.3099(11) 0.5631(7) 0.1333(2) 0.062(2) Uiso 1.000000 R . C29 C 0.8792(6) 0.5322(3) 0.23102(10) 0.0378(14) Uani 1.000000 . U C28 C 0.8872(6) 0.3927(3) 0.21847(12) 0.0471(16) Uani 1.000000 G U H28 H 0.9086(6) 0.3258(3) 0.24433(12) 0.0565(19) Uiso 1.000000 R . C27 C 0.8638(7) 0.3511(3) 0.16810(14) 0.0450(15) Uani 1.000000 G U H27 H 0.8692(7) 0.2557(3) 0.15952(14) 0.0540(18) Uiso 1.000000 R . N10 N 0.8324(6) 0.4490(4) 0.13027(11) 0.0502(14) Uani 1.000000 G U C31 C 0.8244(6) 0.5885(3) 0.14282(12) 0.0484(15) Uani 1.000000 G U H31 H 0.8030(6) 0.6555(3) 0.11696(12) 0.0581(18) Uiso 1.000000 R . C30 C 0.8478(6) 0.6302(3) 0.19319(13) 0.0432(14) Uani 1.000000 G U H30 H 0.8424(6) 0.7255(3) 0.20177(13) 0.0518(17) Uiso 1.000000 R . C20 C 0.3530(9) 0.5788(6) 0.2087(2) 0.0400(13) Uani 1.000000 . . H20 H 0.3463(9) 0.6769(6) 0.2087(2) 0.0480(16) Uiso 1.000000 R . C13 C 0.8670(6) 0.5748(5) 0.68312(19) 0.0255(10) Uani 1.000000 . . N9 N 0.9374(9) 0.6537(7) 0.3887(2) 0.0520(15) Uani 1.000000 . . C35 C 0.9694(8) 0.7034(6) 0.2991(2) 0.0371(14) Uani 1.000000 . . H35 H 1.0005(8) 0.7681(6) 0.2733(2) 0.0445(16) Uiso 1.000000 R . C18 C 0.3910(9) 0.3709(6) 0.2514(2) 0.0414(14) Uani 1.000000 . . H18 H 0.4093(9) 0.3180(6) 0.2815(2) 0.0496(17) Uiso 1.000000 R . N7 N 0.3435(8) 0.3738(6) 0.16082(19) 0.0427(12) Uani 1.000000 . . O1 O 0.3581(6) 0.2174(4) 0.07166(15) 0.0414(10) Uani 1.000000 . . H1 H 0.3416(7) 0.251(7) 0.1008(11) 0.0621(15) Uiso 1.000000 GR . O7 O 0.6678(7) 0.3631(5) 0.03724(18) 0.0517(12) Uani 1.000000 . . H7a H 0.687(11) 0.409(7) 0.0653(15) 0.0775(18) Uiso 1.000000 G . H7b H 0.589(9) 0.301(6) 0.046(2) 0.0775(18) Uiso 1.000000 G . N8 N 0.4467(9) 0.7244(6) 0.3980(2) 0.0482(14) Uani 1.000000 . . C14 C 1.1734(7) 0.5874(6) 0.6981(2) 0.0288(11) Uani 1.000000 . . C10 C 0.6691(9) 0.7531(6) 0.5236(2) 0.0387(14) Uani 1.000000 . . H10 H 0.5547(9) 0.8068(6) 0.5231(2) 0.0464(16) Uiso 1.000000 R . C33 C 0.8418(8) 0.4926(7) 0.3254(2) 0.0403(14) Uani 1.000000 . . H33 H 0.7818(8) 0.4081(7) 0.3183(2) 0.0483(16) Uiso 1.000000 R . C4 C 0.2678(7) 0.4256(5) -0.0578(2) 0.0277(12) Uani 1.000000 . . H4 H 0.1529(7) 0.4474(5) -0.0757(2) 0.0332(14) Uiso 1.000000 R . N6 N 1.3170(6) 0.5660(5) 0.72858(17) 0.0329(10) Uani 1.000000 . . H6a H 1.4257(6) 0.5797(5) 0.71671(17) 0.0395(12) Uiso 1.000000 R . H6b H 1.3017(6) 0.5385(5) 0.76030(17) 0.0395(12) Uiso 1.000000 R . C7 C 0.7196(7) 0.3787(5) -0.1098(2) 0.0262(11) Uani 1.000000 . . C32 C 0.8649(10) 0.5319(7) 0.3757(2) 0.0470(16) Uani 1.000000 . . H32 H 0.8282(10) 0.4705(7) 0.4020(2) 0.0564(19) Uiso 1.000000 R . C3 C 0.3047(8) 0.5304(5) -0.0163(2) 0.0368(14) Uani 1.000000 . . H3c H 0.2836(8) 0.6259(5) -0.0285(2) 0.0442(16) Uiso 1.000000 R . H3d H 0.4290(8) 0.5227(5) -0.0034(2) 0.0442(16) Uiso 1.000000 R . C23 C 0.3509(7) 0.5204(6) 0.3497(2) 0.0363(13) Uani 1.000000 . . H23 H 0.3003(7) 0.4303(6) 0.3500(2) 0.0436(15) Uiso 1.000000 R . C25 C 0.4909(10) 0.7814(7) 0.3537(2) 0.0478(17) Uani 1.000000 . . H25 H 0.5393(10) 0.8722(7) 0.3544(2) 0.057(2) Uiso 1.000000 R . C8 C 0.5821(8) 0.3756(7) -0.0774(2) 0.0353(13) Uani 1.000000 . . H8 H 0.5984(8) 0.3472(7) -0.0429(2) 0.0423(16) Uiso 1.000000 R U C2 C 0.1380(9) 0.3000(6) 0.0080(2) 0.0355(13) Uani 1.000000 . . H2 H 0.0143(9) 0.2785(6) -0.0044(2) 0.0426(15) Uiso 1.000000 R . C11 C 0.7663(8) 0.5123(6) 0.5523(2) 0.0347(13) Uani 1.000000 . . H11a H 0.7317(8) 0.4174(6) 0.5626(2) 0.0416(16) Uiso 1.000000 R . H11b H 0.8924(8) 0.5116(6) 0.5407(2) 0.0416(16) Uiso 1.000000 R . C19 C 0.3830(8) 0.5124(6) 0.2544(2) 0.0357(13) Uani 1.000000 . . C26 C 0.4715(9) 0.7179(6) 0.3068(3) 0.0401(14) Uani 1.000000 . . H26 H 0.5044(9) 0.7655(6) 0.2765(3) 0.0481(17) Uiso 1.000000 R . C36 C 0.9891(9) 0.7373(7) 0.3512(3) 0.0457(16) Uani 1.000000 . . H36 H 1.0416(9) 0.8237(7) 0.3598(3) 0.0548(19) Uiso 1.000000 R . C17 C 0.3726(10) 0.3038(7) 0.2047(2) 0.0471(16) Uani 1.000000 . . H17 H 0.3808(10) 0.2058(7) 0.2036(2) 0.0566(19) Uiso 1.000000 R . C34 C 0.9019(8) 0.5705(7) 0.2860(2) 0.0367(13) Uani 1.000000 . . C9 C 0.8045(9) 0.8304(6) 0.4915(2) 0.0413(15) Uani 1.000000 . . H9a H 0.8259(9) 0.9232(6) 0.5062(2) 0.0496(18) Uiso 1.000000 R . H9b H 0.7579(9) 0.8422(6) 0.4563(2) 0.0496(18) Uiso 1.000000 R . C1 C 0.1916(9) 0.1957(6) 0.0476(2) 0.0422(15) Uani 1.000000 . . H1a H 0.1936(9) 0.1033(6) 0.0314(2) 0.0506(18) Uiso 1.000000 R . H1b H 0.0978(9) 0.1938(6) 0.0743(2) 0.0506(18) Uiso 1.000000 R . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 S1 0.0412(8) 0.0373(8) 0.0379(7) 0.0025(7) 0.0064(7) 0.0009(6) S2 0.0477(9) 0.0452(8) 0.0363(7) -0.0023(8) -0.0057(7) 0.0008(7) F2 0.0237(18) 0.063(2) 0.050(2) -0.0026(19) 0.0080(17) 0.0094(17) F1 0.0258(18) 0.054(2) 0.0416(17) 0.0038(16) 0.0002(15) 0.0054(15) O6 0.0210(19) 0.052(3) 0.034(2) -0.0080(18) 0.0026(15) 0.004(2) O3 0.022(2) 0.038(2) 0.043(2) 0.0045(18) -0.0020(16) 0.0071(19) O2 0.035(2) 0.028(2) 0.036(2) -0.0011(16) 0.0069(19) 0.0010(16) O5 0.041(2) 0.036(2) 0.0293(19) 0.0046(19) -0.0001(18) 0.0001(17) C15 0.022(3) 0.013(2) 0.055(3) 0.006(2) 0.004(3) 0.003(2) C6 0.039(3) 0.027(3) 0.036(3) -0.013(2) 0.003(3) -0.004(2) N1 0.018(2) 0.036(3) 0.035(2) 0.0073(18) 0.0069(19) 0.0019(19) C12 0.023(3) 0.050(4) 0.025(3) -0.005(3) -0.005(2) 0.001(2) N2 0.025(2) 0.017(2) 0.039(2) 0.0000(18) 0.0011(19) 0.0029(18) C5 0.031(3) 0.032(3) 0.034(3) -0.004(3) 0.012(2) -0.002(2) C24 0.043(4) 0.069(5) 0.033(3) 0.008(4) -0.002(3) 0.001(3) C22 0.033(3) 0.028(3) 0.042(3) 0.011(2) 0.001(2) -0.003(3) C16 0.033(3) 0.051(4) 0.025(3) -0.014(3) 0.007(3) 0.004(3) N3 0.037(3) 0.055(3) 0.034(2) 0.003(3) 0.012(2) 0.004(2) O4 0.047(3) 0.031(2) 0.062(3) -0.008(2) 0.007(2) -0.005(2) N4 0.016(2) 0.055(3) 0.031(2) 0.011(2) -0.0006(19) -0.003(2) N5 0.028(2) 0.020(2) 0.038(2) -0.006(2) -0.0026(19) -0.0034(19) C21 0.070(5) 0.059(5) 0.026(3) -0.001(4) -0.000(3) 0.005(3) C29 0.030(3) 0.019(3) 0.065(4) -0.005(2) -0.002(3) 0.010(2) C28 0.050(4) 0.051(4) 0.041(3) 0.002(3) 0.005(3) 0.011(3) C27 0.048(4) 0.035(3) 0.052(3) -0.000(3) 0.001(3) 0.005(3) N10 0.056(4) 0.049(3) 0.046(3) -0.006(3) -0.007(3) 0.004(2) C31 0.041(4) 0.053(3) 0.051(3) -0.024(3) -0.001(3) 0.015(3) C30 0.042(4) 0.044(3) 0.044(3) 0.005(3) -0.001(3) 0.016(2) C20 0.050(4) 0.017(2) 0.053(3) 0.003(3) 0.001(3) 0.007(3) C13 0.013(2) 0.019(2) 0.044(3) -0.002(2) -0.001(2) -0.001(2) N9 0.064(4) 0.049(4) 0.042(3) -0.000(3) 0.009(3) 0.004(3) C35 0.028(3) 0.030(3) 0.053(4) -0.005(2) 0.005(3) 0.006(3) C18 0.048(4) 0.028(3) 0.048(3) 0.010(3) -0.005(3) 0.001(2) N7 0.044(3) 0.045(3) 0.038(3) -0.002(3) 0.004(2) -0.006(2) O1 0.040(2) 0.040(2) 0.044(2) -0.005(2) -0.002(2) -0.0072(19) O7 0.051(3) 0.050(3) 0.053(3) -0.026(2) 0.004(2) -0.004(2) N8 0.064(4) 0.038(3) 0.042(3) 0.008(3) -0.002(3) -0.005(2) C14 0.015(2) 0.037(3) 0.034(3) 0.001(2) -0.002(2) -0.004(2) C10 0.037(3) 0.041(3) 0.038(3) 0.009(3) 0.005(3) 0.001(3) C33 0.026(3) 0.048(4) 0.047(3) 0.002(3) 0.004(3) 0.006(3) C4 0.022(3) 0.018(2) 0.043(3) 0.005(2) 0.008(2) 0.005(2) N6 0.017(2) 0.036(3) 0.046(3) -0.001(2) -0.0012(18) 0.000(2) C7 0.016(2) 0.019(2) 0.044(3) 0.003(2) 0.003(2) 0.001(2) C32 0.046(4) 0.048(4) 0.047(4) 0.002(3) 0.016(3) 0.007(3) C3 0.039(3) 0.018(2) 0.054(3) 0.003(2) 0.006(3) -0.000(2) C23 0.017(3) 0.035(3) 0.057(3) 0.002(2) 0.002(3) 0.000(3) C25 0.064(5) 0.036(3) 0.044(3) 0.018(3) 0.003(3) 0.000(3) C8 0.027(3) 0.045(4) 0.034(3) 0.007(3) -0.000(2) 0.007(2) C2 0.041(3) 0.036(3) 0.029(3) -0.005(3) 0.010(3) 0.006(2) C11 0.033(3) 0.037(3) 0.034(3) -0.004(2) 0.002(2) -0.001(2) C19 0.030(3) 0.038(3) 0.038(3) -0.000(3) 0.002(3) -0.004(2) C26 0.041(3) 0.029(3) 0.050(3) -0.014(3) 0.006(3) 0.000(3) C36 0.048(4) 0.034(3) 0.055(4) 0.011(3) 0.010(3) 0.003(3) C17 0.054(4) 0.048(4) 0.039(3) -0.009(3) -0.004(3) -0.010(3) C34 0.034(3) 0.029(3) 0.047(3) 0.018(3) 0.012(3) 0.009(3) C9 0.041(4) 0.038(3) 0.045(3) -0.003(3) 0.004(3) -0.007(3) C1 0.040(4) 0.037(3) 0.050(3) -0.009(3) 0.007(3) 0.006(3) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source C 0.00347 0.00161 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.215599998832 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' F 0.01794 0.01033 3.53920 2.64120 1.51700 1.02430 10.28250 4.29440 0.26150 26.14760 0.277599990368 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.0030380000826 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' O 0.01158 0.00611 3.04850 2.28680 1.54630 0.86700 13.27710 5.70110 0.32390 32.90890 0.250800013542 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' N 0.00653 0.00323 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750 0.58260 -11.5290002823 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' S 0.12424 0.12443 6.90530 5.20340 1.43790 1.58630 1.46790 22.21510 0.25360 56.17200 0.866900026798 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u _diffrn_refln_scale_group_code -1 0 0 3.5 0.9 -2 1 0 0 3.5 0.9 1 1 0 0 3.3 1 -2 -1 0 0 3.3 1 1 -1 0 0 6.7 0.8 -2 1 0 0 6.7 0.8 1 -2 0 0 1881.91 133.59 -2 2 0 0 1881.91 133.59 1 2 0 0 1874.61 133.59 -2 -2 0 0 1874.61 133.59 1 -2 0 0 2050.09 133.39 -2 2 0 0 2050.09 133.39 1 2 0 0 1952.1 133.39 -2 -2 0 0 1952.1 133.39 1 3 0 0 140.69 10.9 -2 -3 0 0 140.69 10.9 1 3 0 0 149.69 10.6 -2 -3 0 0 149.69 10.6 1 -3 0 0 160.58 10.6 -2 3 0 0 160.58 10.6 1 -3 0 0 141.79 11 -2 3 0 0 141.79 11 1 -4 0 0 2050.59 133.89 -2 4 0 0 2050.59 133.89 1 -4 0 0 1790.52 134.29 -2 4 0 0 1790.52 134.29 1 -4 0 0 1880.71 133.89 -2 4 0 0 1880.71 133.89 1 4 0 0 2055.09 133.99 -2 -4 0 0 2055.09 133.99 1 -5 0 0 16.6 2.5 -2 5 0 0 16.6 2.5 1 -5 0 0 13.1 3.3 -2 5 0 0 13.1 3.3 1 5 0 0 11.2 2.5 -2 -5 0 0 11.2 2.5 1 -5 0 0 14 2.3 -2 5 0 0 14 2.3 1 -5 0 0 13.5 3.1 -2 5 0 0 13.5 3.1 1 -6 0 0 106.69 9.2 -2 6 0 0 106.69 9.2 1 -6 0 0 100.89 8.1 -2 6 0 0 100.89 8.1 1 -6 0 0 91.99 8.1 -2 6 0 0 91.99 8.1 1 -6 0 0 106.59 9.4 -2 6 0 0 106.59 9.4 1 -7 0 0 69.69 7.2 -2 7 0 0 69.69 7.2 1 -7 0 0 44.5 5.8 -2 7 0 0 44.5 5.8 1 -7 0 0 57.09 5.9 -2 7 0 0 57.09 5.9 1 -8 0 0 173.58 14.4 -2 8 0 0 173.58 14.4 1 -8 0 0 126.79 13.4 -2 8 0 0 126.79 13.4 1 -9 0 0 22 7.2 -2 9 0 0 22 7.2 1 0 1 0 -0.5 0.6 -2 0 -1 0 -0.5 0.6 1 0 1 0 0.2 0.5 -2 0 -1 0 0.2 0.5 1 0 -1 0 1.3 0.6 -2 0 1 0 1.3 0.6 1 0 -1 0 0.1 0.6 -2 0 1 0 0.1 0.6 1 0 -1 0 -0.1 0.6 -2 0 1 0 -0.1 0.6 1 0 -1 0 0 0.4 -2 0 1 0 0 0.4 1 -1 1 0 1106.59 76.19 -2 1 -1 0 1106.59 76.19 1 1 1 0 1026.3 76.19 -2 -1 -1 0 1026.3 76.19 1 -1 1 0 1148.09 76.19 -2 1 -1 0 1148.09 76.19 1 1 1 0 1073.29 76.19 -2 -1 -1 0 1073.29 76.19 1 -1 -1 0 1079.79 76.19 -2 1 1 0 1079.79 76.19 1 1 -1 0 1099.59 76.29 -2 -1 1 0 1099.59 76.29 1 -1 -1 0 1096.09 76.19 -2 1 1 0 1096.09 76.19 1 -1 -1 0 1100.19 76.19 -2 1 1 0 1100.19 76.19 1 1 -1 0 1180.78 76.19 -2 -1 1 0 1180.78 76.19 1 1 -1 0 1162.18 76.19 -2 -1 1 0 1162.18 76.19 1 -2 1 0 3659.13 273.17 -2 2 -1 0 3659.13 273.17 1 -2 1 0 4034.1 273.17 -2 2 -1 0 4034.1 273.17 1 -2 1 0 3924.61 273.37 -2 2 -1 0 3924.61 273.37 1 2 -1 0 4315.67 273.17 -2 -2 1 0 4315.67 273.17 1 -2 -1 0 3940.41 273.17 -2 2 1 0 3940.41 273.17 1 2 -1 0 3952.6 273.37 -2 -2 1 0 3952.6 273.37 1 -2 -1 0 4263.67 273.17 -2 2 1 0 4263.67 273.17 1 -2 -1 0 4108.89 273.17 -2 2 1 0 4108.89 273.17 1 -2 -1 0 3742.53 273.27 -2 2 1 0 3742.53 273.27 1 -2 -1 0 3798.22 273.17 -2 2 1 0 3798.22 273.17 1 -3 1 0 140.29 10.5 -2 3 -1 0 140.29 10.5 1 -3 1 0 142.89 10 -2 3 -1 0 142.89 10 1 -3 1 0 133.99 10 -2 3 -1 0 133.99 10 1 -3 -1 0 146.09 10.1 -2 3 1 0 146.09 10.1 1 3 -1 0 143.99 10.1 -2 -3 1 0 143.99 10.1 1 -3 -1 0 138.49 10.3 -2 3 1 0 138.49 10.3 1 -3 -1 0 146.39 10.2 -2 3 1 0 146.39 10.2 1 -3 -1 0 133.29 10.1 -2 3 1 0 133.29 10.1 1 -3 -1 0 141.69 10 -2 3 1 0 141.69 10 1 3 -1 0 138.39 10.5 -2 -3 1 0 138.39 10.5 1 -4 1 0 76.79 6.1 -2 4 -1 0 76.79 6.1 1 -4 1 0 75.09 7.5 -2 4 -1 0 75.09 7.5 1 -4 1 0 73.09 6 -2 4 -1 0 73.09 6 1 4 -1 0 65.19 6 -2 -4 1 0 65.19 6 1 -4 -1 0 87.59 6 -2 4 1 0 87.59 6 1 -4 -1 0 92.19 6.2 -2 4 1 0 92.19 6.2 1 -4 -1 0 83.89 6.3 -2 4 1 0 83.89 6.3 1 4 -1 0 66.39 6.7 -2 -4 1 0 66.39 6.7 1 -5 1 0 9.8 2.2 -2 5 -1 0 9.8 2.2 1 -5 1 0 10.1 2.2 -2 5 -1 0 10.1 2.2 1 -5 1 0 8.5 3.2 -2 5 -1 0 8.5 3.2 1 -5 -1 0 8.8 2.3 -2 5 1 0 8.8 2.3 1 -5 -1 0 7.4 2.6 -2 5 1 0 7.4 2.6 1 -5 -1 0 8 2 -2 5 1 0 8 2 1 5 -1 0 7.1 2.3 -2 -5 1 0 7.1 2.3 1 -5 -1 0 11.2 3.1 -2 5 1 0 11.2 3.1 1 -5 -1 0 14.3 3 -2 5 1 0 14.3 3 1 -6 1 0 210.48 17.3 -2 6 -1 0 210.48 17.3 1 -6 1 0 257.27 18.1 -2 6 -1 0 257.27 18.1 1 -6 1 0 272.47 18.5 -2 6 -1 0 272.47 18.5 1 -6 1 0 254.17 17.3 -2 6 -1 0 254.17 17.3 1 -6 -1 0 221.48 18.1 -2 6 1 0 221.48 18.1 1 -6 -1 0 225.48 17.2 -2 6 1 0 225.48 17.2 1 -6 -1 0 226.98 18.5 -2 6 1 0 226.98 18.5 1 -6 -1 0 240.68 17.7 -2 6 1 0 240.68 17.7 1 6 -1 0 244.78 17.4 -2 -6 1 0 244.78 17.4 1 -7 1 0 35.6 4.8 -2 7 -1 0 35.6 4.8 1 -7 1 0 37.3 4.7 -2 7 -1 0 37.3 4.7 1 -7 1 0 47.1 6.3 -2 7 -1 0 47.1 6.3 1 -7 -1 0 31.3 4.6 -2 7 1 0 31.3 4.6 1 -7 -1 0 44.4 6.3 -2 7 1 0 44.4 6.3 1 7 -1 0 32.5 4.9 -2 -7 1 0 32.5 4.9 1 -7 -1 0 47.7 7 -2 7 1 0 47.7 7 1 -7 -1 0 34.2 4.7 -2 7 1 0 34.2 4.7 1 -8 1 0 29.1 6.7 -2 8 -1 0 29.1 6.7 1 -8 -1 0 26.1 7.3 -2 8 1 0 26.1 7.3 1 -8 -1 0 33.2 5.8 -2 8 1 0 33.2 5.8 1 -8 -1 0 29.7 4.6 -2 8 1 0 29.7 4.6 1 -9 -1 0 29.5 7.1 -2 9 1 0 29.5 7.1 1 -9 -1 0 13 5.4 -2 9 1 0 13 5.4 1 0 2 0 2435.86 169.68 -2 0 -2 0 2435.86 169.68 1 0 2 0 2531.25 169.68 -2 0 -2 0 2531.25 169.68 1 0 2 0 2503.75 169.58 -2 0 -2 0 2503.75 169.58 1 0 -2 0 2526.55 169.68 -2 0 2 0 2526.55 169.68 1 0 -2 0 2465.15 169.68 -2 0 2 0 2465.15 169.68 1 0 -2 0 2506.05 169.68 -2 0 2 0 2506.05 169.68 1 0 -2 0 2306.47 169.68 -2 0 2 0 2306.47 169.68 1 -1 2 0 265.87 19.4 -2 1 -2 0 265.87 19.4 1 1 2 0 264.27 19.3 -2 -1 -2 0 264.27 19.3 1 -1 2 0 290.27 19.3 -2 1 -2 0 290.27 19.3 1 -1 2 0 271.97 19.3 -2 1 -2 0 271.97 19.3 1 1 -2 0 279.07 19.2 -2 -1 2 0 279.07 19.2 1 1 -2 0 286.77 19.3 -2 -1 2 0 286.77 19.3 1 1 -2 0 266.07 19.3 -2 -1 2 0 266.07 19.3 1 -1 -2 0 273.17 19.3 -2 1 2 0 273.17 19.3 1 -1 -2 0 271.37 19.3 -2 1 2 0 271.37 19.3 1 1 -2 0 295.17 19.3 -2 -1 2 0 295.17 19.3 1 -2 2 0 1549.64 102.69 -2 2 -2 0 1549.64 102.69 1 2 2 0 1406.26 102.79 -2 -2 -2 0 1406.26 102.79 1 -2 2 0 1464.45 102.89 -2 2 -2 0 1464.45 102.89 1 -2 2 0 1503.75 102.69 -2 2 -2 0 1503.75 102.69 1 2 -2 0 1477.35 102.89 -2 -2 2 0 1477.35 102.89 1 2 -2 0 1570.74 102.79 -2 -2 2 0 1570.74 102.79 1 -2 -2 0 1460.35 102.79 -2 2 2 0 1460.35 102.79 1 2 -2 0 1586.24 102.69 -2 -2 2 0 1586.24 102.69 1 -2 -2 0 1439.86 102.79 -2 2 2 0 1439.86 102.79 1 -2 -2 0 1461.35 102.79 -2 2 2 0 1461.35 102.79 1 -3 2 0 474.55 32.9 -2 3 -2 0 474.55 32.9 1 -3 2 0 474.65 32.9 -2 3 -2 0 474.65 32.9 1 -3 2 0 478.55 33.3 -2 3 -2 0 478.55 33.3 1 -3 -2 0 437.56 33 -2 3 2 0 437.56 33 1 -3 -2 0 480.75 33 -2 3 2 0 480.75 33 1 3 -2 0 507.25 33.4 -2 -3 2 0 507.25 33.4 1 3 -2 0 486.65 32.9 -2 -3 2 0 486.65 32.9 1 -3 -2 0 464.55 33 -2 3 2 0 464.55 33 1 -3 -2 0 483.25 33 -2 3 2 0 483.25 33 1 -3 -2 0 443.26 32.9 -2 3 2 0 443.26 32.9 1 3 -2 0 485.15 32.9 -2 -3 2 0 485.15 32.9 1 -4 2 0 645.24 44 -2 4 -2 0 645.24 44 1 -4 2 0 605.24 44 -2 4 -2 0 605.24 44 1 -4 2 0 686.33 44.5 -2 4 -2 0 686.33 44.5 1 4 -2 0 602.94 43.9 -2 -4 2 0 602.94 43.9 1 -4 -2 0 635.94 44.1 -2 4 2 0 635.94 44.1 1 -4 -2 0 668.23 44.1 -2 4 2 0 668.23 44.1 1 -4 -2 0 627.14 44.2 -2 4 2 0 627.14 44.2 1 4 -2 0 631.14 44 -2 -4 2 0 631.14 44 1 -4 -2 0 599.24 44.2 -2 4 2 0 599.24 44.2 1 -4 -2 0 640.34 44.1 -2 4 2 0 640.34 44.1 1 -5 2 0 68.79 5.5 -2 5 -2 0 68.79 5.5 1 -5 2 0 60.29 5.6 -2 5 -2 0 60.29 5.6 1 -5 2 0 75.69 6.7 -2 5 -2 0 75.69 6.7 1 5 -2 0 57.29 5.3 -2 -5 2 0 57.29 5.3 1 -5 -2 0 66.79 5.6 -2 5 2 0 66.79 5.6 1 -5 -2 0 62.09 6.5 -2 5 2 0 62.09 6.5 1 -5 -2 0 61.89 5.9 -2 5 2 0 61.89 5.9 1 -5 -2 0 58.39 5.5 -2 5 2 0 58.39 5.5 1 -6 2 0 45.2 6.1 -2 6 -2 0 45.2 6.1 1 -6 2 0 43.7 5.6 -2 6 -2 0 43.7 5.6 1 -6 2 0 41.2 4.7 -2 6 -2 0 41.2 4.7 1 -6 -2 0 50.99 5.7 -2 6 2 0 50.99 5.7 1 -6 -2 0 44.4 6 -2 6 2 0 44.4 6 1 6 -2 0 30.3 4.4 -2 -6 2 0 30.3 4.4 1 -6 -2 0 38.7 5.1 -2 6 2 0 38.7 5.1 1 -7 2 0 166.68 13.7 -2 7 -2 0 166.68 13.7 1 -7 2 0 175.58 12.9 -2 7 -2 0 175.58 12.9 1 -7 2 0 118.39 11.1 -2 7 -2 0 118.39 11.1 1 -7 2 0 120.59 11.6 -2 7 -2 0 120.59 11.6 1 -7 -2 0 160.68 13 -2 7 2 0 160.68 13 1 -7 -2 0 141.79 12.4 -2 7 2 0 141.79 12.4 1 -7 -2 0 123.99 11.1 -2 7 2 0 123.99 11.1 1 -7 -2 0 148.69 12.5 -2 7 2 0 148.69 12.5 1 -8 2 0 18.7 6.8 -2 8 -2 0 18.7 6.8 1 -8 2 0 26.5 6.8 -2 8 -2 0 26.5 6.8 1 -8 -2 0 37.4 5.7 -2 8 2 0 37.4 5.7 1 -8 -2 0 24.1 6.4 -2 8 2 0 24.1 6.4 1 -8 -2 0 15.6 4.3 -2 8 2 0 15.6 4.3 1 -9 2 0 6.6 7.2 -2 9 -2 0 6.6 7.2 1 -9 2 0 13.8 7.4 -2 9 -2 0 13.8 7.4 1 -9 -2 0 3.9 4.9 -2 9 2 0 3.9 4.9 1 -9 -2 0 9.6 6.7 -2 9 2 0 9.6 6.7 1 0 3 0 0.5 1.1 -2 0 -3 0 0.5 1.1 1 0 3 0 -0.3 1.2 -2 0 -3 0 -0.3 1.2 1 0 3 0 -0.2 1.6 -2 0 -3 0 -0.2 1.6 1 0 -3 0 1.2 1.2 -2 0 3 0 1.2 1.2 1 0 -3 0 2.6 1.6 -2 0 3 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12.6 1 -3 3 0 185.38 12.9 -2 3 -3 0 185.38 12.9 1 -3 -3 0 165.88 12.5 -2 3 3 0 165.88 12.5 1 -3 -3 0 164.78 12.4 -2 3 3 0 164.78 12.4 1 3 -3 0 182.08 12.4 -2 -3 3 0 182.08 12.4 1 3 -3 0 167.18 12.8 -2 -3 3 0 167.18 12.8 1 3 -3 0 178.98 12.5 -2 -3 3 0 178.98 12.5 1 -3 -3 0 164.78 12.5 -2 3 3 0 164.78 12.5 1 -3 -3 0 168.98 12.3 -2 3 3 0 168.98 12.3 1 -4 3 0 276.27 21.3 -2 4 -3 0 276.27 21.3 1 -4 3 0 322.47 21.8 -2 4 -3 0 322.47 21.8 1 -4 3 0 313.37 21.2 -2 4 -3 0 313.37 21.2 1 -4 -3 0 302.87 21.4 -2 4 3 0 302.87 21.4 1 4 -3 0 311.57 21.3 -2 -4 3 0 311.57 21.3 1 -4 -3 0 292.87 21.3 -2 4 3 0 292.87 21.3 1 -4 -3 0 317.07 21.5 -2 4 3 0 317.07 21.5 1 4 -3 0 292.37 21.2 -2 -4 3 0 292.37 21.2 1 -4 -3 0 311.77 21.4 -2 4 3 0 311.77 21.4 1 -4 -3 0 270.17 21.4 -2 4 3 0 270.17 21.4 1 -5 3 0 30.3 3.8 -2 5 -3 0 30.3 3.8 1 -5 3 0 33.7 5 -2 5 -3 0 33.7 5 1 -5 3 0 26.8 3.9 -2 5 -3 0 26.8 3.9 1 -5 -3 0 43.3 4.9 -2 5 3 0 43.3 4.9 1 5 -3 0 30.7 3.7 -2 -5 3 0 30.7 3.7 1 -5 -3 0 46.9 4.8 -2 5 3 0 46.9 4.8 1 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5.6 7 1 -9 -3 0 6.2 4.5 -2 9 3 0 6.2 4.5 1 -9 -3 0 2.7 6.2 -2 9 3 0 2.7 6.2 1 0 4 0 566.14 39 -2 0 -4 0 566.14 39 1 0 4 0 579.44 38.9 -2 0 -4 0 579.44 38.9 1 0 4 0 557.44 39.1 -2 0 -4 0 557.44 39.1 1 0 -4 0 600.54 39.1 -2 0 4 0 600.54 39.1 1 0 -4 0 552.24 39.1 -2 0 4 0 552.24 39.1 1 0 -4 0 517.05 38.9 -2 0 4 0 517.05 38.9 1 0 -4 0 565.64 39.1 -2 0 4 0 565.64 39.1 1 -1 4 0 31.9 3.5 -2 1 -4 0 31.9 3.5 1 -1 4 0 27.9 3.5 -2 1 -4 0 27.9 3.5 1 1 -4 0 31.1 3.5 -2 -1 4 0 31.1 3.5 1 1 -4 0 40 3.5 -2 -1 4 0 40 3.5 1 -1 -4 0 41.1 3.7 -2 1 4 0 41.1 3.7 1 -2 4 0 96.19 7.7 -2 2 -4 0 96.19 7.7 1 -2 4 0 95.49 7.9 -2 2 -4 0 95.49 7.9 1 -2 4 0 93.39 7.6 -2 2 -4 0 93.39 7.6 1 2 -4 0 100.99 7.7 -2 -2 4 0 100.99 7.7 1 2 -4 0 112.09 7.5 -2 -2 4 0 112.09 7.5 1 2 -4 0 79.79 7.8 -2 -2 4 0 79.79 7.8 1 -2 -4 0 109.09 7.8 -2 2 4 0 109.09 7.8 1 2 -4 0 99.09 7.6 -2 -2 4 0 99.09 7.6 1 -2 -4 0 118.79 7.8 -2 2 4 0 118.79 7.8 1 -3 4 0 130.69 10.3 -2 3 -4 0 130.69 10.3 1 -3 4 0 106.89 9 -2 3 -4 0 106.89 9 1 3 4 0 98.69 9.2 -2 -3 -4 0 98.69 9.2 1 -3 4 0 135.79 9 -2 3 -4 0 135.79 9 1 3 -4 0 111.59 9.4 -2 -3 4 0 111.59 9.4 1 3 -4 0 114.29 8.9 -2 -3 4 0 114.29 8.9 1 -3 -4 0 125.59 9.2 -2 3 4 0 125.59 9.2 1 3 -4 0 131.09 9.2 -2 -3 4 0 131.09 9.2 1 -4 4 0 392.96 27.6 -2 4 -4 0 392.96 27.6 1 -4 4 0 396.86 27 -2 4 -4 0 396.86 27 1 4 -4 0 384.16 27.1 -2 -4 4 0 384.16 27.1 1 -4 -4 0 387.96 27.2 -2 4 4 0 387.96 27.2 1 -4 -4 0 403.36 27.2 -2 4 4 0 403.36 27.2 1 4 -4 0 325.87 27.2 -2 -4 4 0 325.87 27.2 1 -4 -4 0 374.86 26.9 -2 4 4 0 374.86 26.9 1 -4 -4 0 379.16 26.9 -2 4 4 0 379.16 26.9 1 -4 -4 0 394.96 27.2 -2 4 4 0 394.96 27.2 1 -5 4 0 35.8 4.7 -2 5 -4 0 35.8 4.7 1 -5 4 0 33.2 5.9 -2 5 -4 0 33.2 5.9 1 -5 4 0 31.8 4.2 -2 5 -4 0 31.8 4.2 1 -5 -4 0 42.4 4.6 -2 5 4 0 42.4 4.6 1 5 -4 0 35.6 4.3 -2 -5 4 0 35.6 4.3 1 -5 -4 0 42 4.7 -2 5 4 0 42 4.7 1 5 -4 0 36.1 4.3 -2 -5 4 0 36.1 4.3 1 -5 -4 0 40.7 4.7 -2 5 4 0 40.7 4.7 1 -5 -4 0 38.4 4.5 -2 5 4 0 38.4 4.5 1 -5 -4 0 43.2 5 -2 5 4 0 43.2 5 1 -6 4 0 111.69 10.7 -2 6 -4 0 111.69 10.7 1 -6 -4 0 109.89 9.1 -2 6 4 0 109.89 9.1 1 6 -4 0 83.19 8.4 -2 -6 4 0 83.19 8.4 1 -6 -4 0 92.69 9 -2 6 4 0 92.69 9 1 -6 -4 0 106.39 9.1 -2 6 4 0 106.39 9.1 1 6 -4 0 96.59 8.3 -2 -6 4 0 96.59 8.3 1 -6 -4 0 105.59 8.4 -2 6 4 0 105.59 8.4 1 -6 -4 0 94.49 9.9 -2 6 4 0 94.49 9.9 1 -7 4 0 28.5 6.9 -2 7 -4 0 28.5 6.9 1 -7 4 0 24.6 4.7 -2 7 -4 0 24.6 4.7 1 -7 4 0 23.7 6.2 -2 7 -4 0 23.7 6.2 1 -7 -4 0 30.4 4.8 -2 7 4 0 30.4 4.8 1 -7 -4 0 38.2 6.1 -2 7 4 0 38.2 6.1 1 -7 -4 0 31.2 5.9 -2 7 4 0 31.2 5.9 1 -8 4 0 37.4 5.9 -2 8 -4 0 37.4 5.9 1 -8 -4 0 43.8 6.6 -2 8 4 0 43.8 6.6 1 -8 -4 0 32.8 5.8 -2 8 4 0 32.8 5.8 1 0 5 0 84.79 6.6 -2 0 -5 0 84.79 6.6 1 0 -5 0 85.09 6.6 -2 0 5 0 85.09 6.6 1 0 -5 0 75.69 6.5 -2 0 5 0 75.69 6.5 1 0 -5 0 70.09 6.6 -2 0 5 0 70.09 6.6 1 -1 5 0 802.22 54.59 -2 1 -5 0 802.22 54.59 1 -1 5 0 798.32 54.79 -2 1 -5 0 798.32 54.79 1 -1 5 0 790.12 54.69 -2 1 -5 0 790.12 54.69 1 1 5 0 734.23 54.69 -2 -1 -5 0 734.23 54.69 1 -1 -5 0 819.02 55.09 -2 1 5 0 819.02 55.09 1 1 -5 0 821.62 54.69 -2 -1 5 0 821.62 54.69 1 -1 -5 0 766.32 54.69 -2 1 5 0 766.32 54.69 1 1 -5 0 752.62 54.59 -2 -1 5 0 752.62 54.59 1 1 -5 0 787.72 54.69 -2 -1 5 0 787.72 54.69 1 1 -5 0 801.22 54.69 -2 -1 5 0 801.22 54.69 1 2 5 0 84.99 7.2 -2 -2 -5 0 84.99 7.2 1 -2 5 0 72.89 6.8 -2 2 -5 0 72.89 6.8 1 -2 5 0 81.39 6.8 -2 2 -5 0 81.39 6.8 1 -2 5 0 87.19 7 -2 2 -5 0 87.19 7 1 2 -5 0 75.69 6.5 -2 -2 5 0 75.69 6.5 1 -2 -5 0 74.19 6.9 -2 2 5 0 74.19 6.9 1 2 -5 0 90.09 6.8 -2 -2 5 0 90.09 6.8 1 -2 -5 0 91.99 6.9 -2 2 5 0 91.99 6.9 1 2 -5 0 79.79 6.8 -2 -2 5 0 79.79 6.8 1 -3 5 0 33.1 4.3 -2 3 -5 0 33.1 4.3 1 -3 5 0 40.6 4.9 -2 3 -5 0 40.6 4.9 1 -3 5 0 33.8 4.3 -2 3 -5 0 33.8 4.3 1 -3 -5 0 45.1 4.6 -2 3 5 0 45.1 4.6 1 3 -5 0 36.8 3.9 -2 -3 5 0 36.8 3.9 1 -3 -5 0 40.3 4.9 -2 3 5 0 40.3 4.9 1 3 -5 0 36.6 4.1 -2 -3 5 0 36.6 4.1 1 -4 5 0 57.79 6.9 -2 4 -5 0 57.79 6.9 1 -4 5 0 80.29 7.3 -2 4 -5 0 80.29 7.3 1 4 -5 0 63.49 6.4 -2 -4 5 0 63.49 6.4 1 4 -5 0 74.89 6.8 -2 -4 5 0 74.89 6.8 1 -4 -5 0 75.19 6.8 -2 4 5 0 75.19 6.8 1 -4 -5 0 80.49 6.9 -2 4 5 0 80.49 6.9 1 -4 -5 0 73.39 6.5 -2 4 5 0 73.39 6.5 1 -5 5 0 40.5 5.9 -2 5 -5 0 40.5 5.9 1 -5 5 0 36.4 4.7 -2 5 -5 0 36.4 4.7 1 -5 -5 0 33.5 4.1 -2 5 5 0 33.5 4.1 1 5 -5 0 39.7 4.6 -2 -5 5 0 39.7 4.6 1 -5 -5 0 33.7 5.5 -2 5 5 0 33.7 5.5 1 -5 -5 0 27 4.8 -2 5 5 0 27 4.8 1 -5 -5 0 33.7 5.2 -2 5 5 0 33.7 5.2 1 -6 5 0 64.39 7.1 -2 6 -5 0 64.39 7.1 1 -6 5 0 89.89 9.4 -2 6 -5 0 89.89 9.4 1 -6 -5 0 65.69 7.5 -2 6 5 0 65.69 7.5 1 -6 -5 0 70.79 7.5 -2 6 5 0 70.79 7.5 1 6 -5 0 60.49 7 -2 -6 5 0 60.49 7 1 -6 -5 0 72.59 8.1 -2 6 5 0 72.59 8.1 1 -7 5 0 169.48 13.6 -2 7 -5 0 169.48 13.6 1 -7 5 0 195.48 15.9 -2 7 -5 0 195.48 15.9 1 -7 5 0 193.18 15.2 -2 7 -5 0 193.18 15.2 1 -7 -5 0 160.58 14.1 -2 7 5 0 160.58 14.1 1 -7 -5 0 159.78 14.7 -2 7 5 0 159.78 14.7 1 -7 -5 0 143.29 13.3 -2 7 5 0 143.29 13.3 1 -7 -5 0 145.29 13.8 -2 7 5 0 145.29 13.8 1 -8 5 0 20 8.2 -2 8 -5 0 20 8.2 1 -8 5 0 12 7 -2 8 -5 0 12 7 1 -8 -5 0 27.1 6.3 -2 8 5 0 27.1 6.3 1 -8 -5 0 22.6 5.4 -2 8 5 0 22.6 5.4 1 -8 -5 0 16.5 5.5 -2 8 5 0 16.5 5.5 1 0 6 0 379.46 26 -2 0 -6 0 379.46 26 1 0 6 0 386.06 26.1 -2 0 -6 0 386.06 26.1 1 0 -6 0 371.26 26.4 -2 0 6 0 371.26 26.4 1 0 -6 0 388.06 26.5 -2 0 6 0 388.06 26.5 1 0 -6 0 334.97 26 -2 0 6 0 334.97 26 1 -1 6 0 237.18 17.5 -2 1 -6 0 237.18 17.5 1 -1 6 0 260.87 17.8 -2 1 -6 0 260.87 17.8 1 1 -6 0 252.57 17.9 -2 -1 6 0 252.57 17.9 1 -1 -6 0 257.27 18 -2 1 6 0 257.27 18 1 1 -6 0 228.88 17.7 -2 -1 6 0 228.88 17.7 1 -1 -6 0 240.38 18 -2 1 6 0 240.38 18 1 -2 6 0 42.6 5.1 -2 2 -6 0 42.6 5.1 1 2 -6 0 52.09 5.3 -2 -2 6 0 52.09 5.3 1 -2 -6 0 51.99 5.6 -2 2 6 0 51.99 5.6 1 -2 -6 0 59.59 6 -2 2 6 0 59.59 6 1 2 -6 0 56.09 5.3 -2 -2 6 0 56.09 5.3 1 2 -6 0 55.49 5.5 -2 -2 6 0 55.49 5.5 1 -3 6 0 652.73 44.4 -2 3 -6 0 652.73 44.4 1 -3 6 0 643.14 44.7 -2 3 -6 0 643.14 44.7 1 -3 -6 0 596.54 44.4 -2 3 6 0 596.54 44.4 1 3 -6 0 632.14 44.2 -2 -3 6 0 632.14 44.2 1 3 -6 0 672.83 44.6 -2 -3 6 0 672.83 44.6 1 -3 -6 0 587.54 44.4 -2 3 6 0 587.54 44.4 1 -4 6 0 42.4 5.6 -2 4 -6 0 42.4 5.6 1 -4 6 0 48.2 6.5 -2 4 -6 0 48.2 6.5 1 -4 -6 0 53.99 6.1 -2 4 6 0 53.99 6.1 1 4 -6 0 49.2 6 -2 -4 6 0 49.2 6 1 -5 6 0 14.9 4.2 -2 5 -6 0 14.9 4.2 1 -5 -6 0 3.4 4 -2 5 6 0 3.4 4 1 5 -6 0 4.9 3.8 -2 -5 6 0 4.9 3.8 1 -5 -6 0 6.1 4.7 -2 5 6 0 6.1 4.7 1 -5 -6 0 10.6 4.9 -2 5 6 0 10.6 4.9 1 -5 -6 0 7 3.8 -2 5 6 0 7 3.8 1 -6 6 0 11.1 4.3 -2 6 -6 0 11.1 4.3 1 -6 6 0 16.4 6 -2 6 -6 0 16.4 6 1 -6 -6 0 11.7 5 -2 6 6 0 11.7 5 1 6 -6 0 21.1 4.9 -2 -6 6 0 21.1 4.9 1 -6 -6 0 15.9 5.4 -2 6 6 0 15.9 5.4 1 -6 -6 0 13.5 5.8 -2 6 6 0 13.5 5.8 1 -7 6 0 32 7.5 -2 7 -6 0 32 7.5 1 -7 6 0 30.4 7 -2 7 -6 0 30.4 7 1 -7 -6 0 40.4 7.2 -2 7 6 0 40.4 7.2 1 -7 -6 0 34.4 7.2 -2 7 6 0 34.4 7.2 1 -7 -6 0 21.5 5.6 -2 7 6 0 21.5 5.6 1 7 -6 0 33.8 5.6 -2 -7 6 0 33.8 5.6 1 -8 6 0 10.4 8.5 -2 8 -6 0 10.4 8.5 1 -8 6 0 13.6 8.6 -2 8 -6 0 13.6 8.6 1 -8 -6 0 23.1 6.7 -2 8 6 0 23.1 6.7 1 -8 -6 0 15.7 5.5 -2 8 6 0 15.7 5.5 1 -8 -6 0 13.5 5.8 -2 8 6 0 13.5 5.8 1 0 7 0 50.59 4.6 -2 0 -7 0 50.59 4.6 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7.7 -2 3 11 1 13.8 7.7 1 -3 -11 1 19 8.1 -2 3 11 1 19 8.1 1 3 -11 -1 9.8 7.1 -2 -3 11 -1 9.8 7.1 1 0 -12 1 58.99 10.4 -2 0 12 1 58.99 10.4 1 -1 -12 1 17.7 8 -2 1 12 1 17.7 8 1 -9 0 -2 8.2 6.8 -2 9 0 -2 8.2 6.8 1 -8 0 -2 4.3 4.9 -2 8 0 -2 4.3 4.9 1 -8 0 -2 1.2 4.8 -2 8 0 -2 1.2 4.8 1 -8 0 -2 0.4 4.9 -2 8 0 -2 0.4 4.9 1 -7 0 -2 168.68 14.6 -2 7 0 -2 168.68 14.6 1 -6 0 -2 67.39 6.9 -2 6 0 -2 67.39 6.9 1 -6 0 -2 47.8 5.7 -2 6 0 -2 47.8 5.7 1 -6 0 -2 72.59 6.7 -2 6 0 -2 72.59 6.7 1 -5 0 -2 153.98 11.5 -2 5 0 -2 153.98 11.5 1 -5 0 -2 148.99 11.4 -2 5 0 -2 148.99 11.4 1 -5 0 -2 137.19 10.8 -2 5 0 -2 137.19 10.8 1 -4 0 -2 198.08 14.8 -2 4 0 -2 198.08 14.8 1 -4 0 -2 203.78 15.2 -2 4 0 -2 203.78 15.2 1 -4 0 -2 219.38 15.1 -2 4 0 -2 219.38 15.1 1 4 0 2 211.38 15.3 -2 -4 0 2 211.38 15.3 1 -3 0 -2 439.26 30.9 -2 3 0 -2 439.26 30.9 1 -3 0 -2 425.56 31.1 -2 3 0 -2 425.56 31.1 1 -3 0 -2 455.75 31.1 -2 3 0 -2 455.75 31.1 1 3 0 2 457.45 31.1 -2 -3 0 2 457.45 31.1 1 -1 0 -2 52.29 3.9 -2 1 0 -2 52.29 3.9 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-2 22.6 3.2 1 -5 1 -2 29 4 -2 5 -1 -2 29 4 1 -5 -1 -2 23.7 3 -2 5 1 -2 23.7 3 1 -5 -1 -2 27.1 3.2 -2 5 1 -2 27.1 3.2 1 -5 -1 -2 30.6 3.9 -2 5 1 -2 30.6 3.9 1 -5 -1 -2 24.6 3.7 -2 5 1 -2 24.6 3.7 1 -4 1 -2 84.59 7.9 -2 4 -1 -2 84.59 7.9 1 -4 -1 -2 81.49 6.5 -2 4 1 -2 81.49 6.5 1 4 -1 2 72.09 7.1 -2 -4 1 2 72.09 7.1 1 -4 -1 -2 98.09 7.1 -2 4 1 -2 98.09 7.1 1 -4 -1 -2 96.99 7.2 -2 4 1 -2 96.99 7.2 1 3 1 2 95.19 7.3 -2 -3 -1 2 95.19 7.3 1 -3 1 -2 96.59 7.4 -2 3 -1 -2 96.59 7.4 1 -3 1 -2 99.29 7.4 -2 3 -1 -2 99.29 7.4 1 -3 1 -2 88.29 7 -2 3 -1 -2 88.29 7 1 -3 -1 -2 106.39 7.2 -2 3 1 -2 106.39 7.2 1 -3 -1 -2 90.49 6.9 -2 3 1 -2 90.49 6.9 1 3 -1 2 86.29 7.4 -2 -3 1 2 86.29 7.4 1 -3 -1 -2 92.59 7.2 -2 3 1 -2 92.59 7.2 1 -2 1 -2 5617.44 388.26 -2 2 -1 -2 5617.44 388.26 1 2 1 2 5499.15 388.16 -2 -2 -1 2 5499.15 388.16 1 2 1 2 5657.93 388.16 -2 -2 -1 2 5657.93 388.16 1 -2 1 -2 5559.44 388.26 -2 2 -1 -2 5559.44 388.26 1 -2 1 -2 5866.31 388.16 -2 2 -1 -2 5866.31 388.16 1 -2 -1 -2 5834.12 388.16 -2 2 1 -2 5834.12 388.16 1 2 -1 2 5937.21 388.16 -2 -2 1 2 5937.21 388.16 1 -2 -1 -2 5219.08 388.16 -2 2 1 -2 5219.08 388.16 1 2 -1 2 5635.64 388.26 -2 -2 1 2 5635.64 388.26 1 -1 1 -2 1951.9 136.89 -2 1 -1 -2 1951.9 136.89 1 -1 1 -2 2115.69 136.89 -2 1 -1 -2 2115.69 136.89 1 1 1 2 2086.29 136.79 -2 -1 -1 2 2086.29 136.79 1 -1 1 -2 1957.5 136.89 -2 1 -1 -2 1957.5 136.89 1 -1 -1 -2 2059.79 136.79 -2 1 1 -2 2059.79 136.79 1 -1 -1 -2 1777.22 136.69 -2 1 1 -2 1777.22 136.69 1 1 -1 2 1926.41 136.69 -2 -1 1 2 1926.41 136.69 1 1 -1 2 2019.4 136.99 -2 -1 1 2 2019.4 136.99 1 -1 -1 -2 2009.8 136.99 -2 1 1 -2 2009.8 136.99 1 0 1 -2 85.39 6.3 -2 0 -1 -2 85.39 6.3 1 0 1 2 81.39 6.3 -2 0 -1 2 81.39 6.3 1 0 1 -2 89.09 6.3 -2 0 -1 -2 89.09 6.3 1 0 1 -2 93.09 6.2 -2 0 -1 -2 93.09 6.2 1 0 1 -2 101.89 6.4 -2 0 -1 -2 101.89 6.4 1 0 1 2 86.29 6.3 -2 0 -1 2 86.29 6.3 1 0 1 2 91.69 6.3 -2 0 -1 2 91.69 6.3 1 0 -1 2 96.59 6.4 -2 0 1 2 96.59 6.4 1 0 -1 -2 96.49 6.3 -2 0 1 -2 96.49 6.3 1 0 -1 2 84.39 6.3 -2 0 1 2 84.39 6.3 1 0 -1 -2 79.59 6.3 -2 0 1 -2 79.59 6.3 1 0 -1 2 92.89 6.2 -2 0 1 2 92.89 6.2 1 0 -1 -2 84.49 6.3 -2 0 1 -2 84.49 6.3 1 0 -1 2 83.69 6.3 -2 0 1 2 83.69 6.3 1 1 1 -2 1815.52 130.99 -2 -1 -1 -2 1815.52 130.99 1 -1 1 2 1976.6 131.29 -2 1 -1 2 1976.6 131.29 1 -1 1 2 1808.12 130.99 -2 1 -1 2 1808.12 130.99 1 1 1 -2 1887.71 131.09 -2 -1 -1 -2 1887.71 131.09 1 -1 -1 2 1770.42 130.99 -2 1 1 2 1770.42 130.99 1 -1 -1 2 2002.4 131.19 -2 1 1 2 2002.4 131.19 1 -1 -1 2 1923.81 131.19 -2 1 1 2 1923.81 131.19 1 1 -1 -2 2084.39 131.09 -2 -1 1 -2 2084.39 131.09 1 1 -1 -2 1885.91 130.99 -2 -1 1 -2 1885.91 130.99 1 2 1 -2 6033.3 399.86 -2 -2 -1 -2 6033.3 399.86 1 -2 1 2 5589.94 399.96 -2 2 -1 2 5589.94 399.96 1 2 1 -2 5629.84 399.76 -2 -2 -1 -2 5629.84 399.76 1 -2 1 2 6190.28 399.86 -2 2 -1 2 6190.28 399.86 1 2 1 -2 5711.63 399.76 -2 -2 -1 -2 5711.63 399.76 1 2 -1 -2 6130.09 399.86 -2 -2 1 -2 6130.09 399.86 1 -2 -1 2 5823.92 399.86 -2 2 1 2 5823.92 399.86 1 -2 -1 2 5144.69 399.76 -2 2 1 2 5144.69 399.76 1 -2 -1 2 6104.69 399.86 -2 2 1 2 6104.69 399.86 1 3 1 -2 99.49 7.1 -2 -3 -1 -2 99.49 7.1 1 -3 1 2 99.19 7.7 -2 3 -1 2 99.19 7.7 1 -3 1 2 104.79 7.2 -2 3 -1 2 104.79 7.2 1 3 1 -2 89.29 7.3 -2 -3 -1 -2 89.29 7.3 1 -3 -1 2 94.19 7 -2 3 1 2 94.19 7 1 -3 -1 2 87.59 7.5 -2 3 1 2 87.59 7.5 1 -3 -1 2 97.29 7 -2 3 1 2 97.29 7 1 -3 -1 2 101.79 7.3 -2 3 1 2 101.79 7.3 1 3 -1 -2 89.29 7.1 -2 -3 1 -2 89.29 7.1 1 -4 1 2 81.59 6.5 -2 4 -1 2 81.59 6.5 1 4 1 -2 74.89 6.5 -2 -4 -1 -2 74.89 6.5 1 -4 -1 2 89.49 6.3 -2 4 1 2 89.49 6.3 1 -4 -1 2 95.19 7.1 -2 4 1 2 95.19 7.1 1 4 -1 -2 66.79 6.4 -2 -4 1 -2 66.79 6.4 1 -4 -1 2 74.09 6.3 -2 4 1 2 74.09 6.3 1 -4 -1 2 94.99 6.6 -2 4 1 2 94.99 6.6 1 -5 1 2 36.4 4.9 -2 5 -1 2 36.4 4.9 1 -5 1 2 29.8 3.9 -2 5 -1 2 29.8 3.9 1 5 1 -2 35.4 4.4 -2 -5 -1 -2 35.4 4.4 1 -5 -1 2 34.1 3.8 -2 5 1 2 34.1 3.8 1 -5 -1 2 35.8 4.7 -2 5 1 2 35.8 4.7 1 -5 -1 2 36.2 4.3 -2 5 1 2 36.2 4.3 1 -5 -1 2 38.4 3.9 -2 5 1 2 38.4 3.9 1 5 -1 -2 26.5 3.6 -2 -5 1 -2 26.5 3.6 1 -6 1 2 590.54 42.6 -2 6 -1 2 590.54 42.6 1 -6 -1 2 566.04 40.9 -2 6 1 2 566.04 40.9 1 -6 -1 2 665.33 41.3 -2 6 1 2 665.33 41.3 1 -6 -1 2 547.45 41.9 -2 6 1 2 547.45 41.9 1 6 -1 -2 624.64 40.9 -2 -6 1 -2 624.64 40.9 1 -6 -1 2 508.05 40.5 -2 6 1 2 508.05 40.5 1 -7 1 2 50.39 5.3 -2 7 -1 2 50.39 5.3 1 -7 1 2 41.7 6.1 -2 7 -1 2 41.7 6.1 1 -7 1 2 32.7 6.4 -2 7 -1 2 32.7 6.4 1 -7 -1 2 30.3 5.5 -2 7 1 2 30.3 5.5 1 -7 -1 2 40.2 6.5 -2 7 1 2 40.2 6.5 1 -7 -1 2 39.1 7.9 -2 7 1 2 39.1 7.9 1 -7 -1 2 42.9 5 -2 7 1 2 42.9 5 1 -8 1 2 29.4 5.3 -2 8 -1 2 29.4 5.3 1 -8 1 2 50.99 8.2 -2 8 -1 2 50.99 8.2 1 -8 1 2 47.6 7.3 -2 8 -1 2 47.6 7.3 1 -8 -1 2 54.59 7.9 -2 8 1 2 54.59 7.9 1 -8 -1 2 46.1 7.3 -2 8 1 2 46.1 7.3 1 -8 -1 2 26.6 5.4 -2 8 1 2 26.6 5.4 1 -9 1 2 22.9 8.4 -2 9 -1 2 22.9 8.4 1 -9 1 2 3.5 5 -2 9 -1 2 3.5 5 1 -9 1 2 21.7 7.9 -2 9 -1 2 21.7 7.9 1 -9 -1 2 15.2 6.3 -2 9 1 2 15.2 6.3 1 -9 -1 2 11.8 5 -2 9 1 2 11.8 5 1 -9 -1 2 10.2 6.2 -2 9 1 2 10.2 6.2 1 -9 2 -2 16.2 7.7 -2 9 -2 -2 16.2 7.7 1 -9 -2 -2 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181.28 14.7 1 -6 -3 -4 201.28 14.4 -2 6 3 -4 201.28 14.4 1 -6 -3 -4 196.98 14.7 -2 6 3 -4 196.98 14.7 1 -6 -3 -4 163.08 14 -2 6 3 -4 163.08 14 1 -6 -3 -4 158.48 13.6 -2 6 3 -4 158.48 13.6 1 -5 3 -4 139.89 10.3 -2 5 -3 -4 139.89 10.3 1 -5 3 -4 122.59 9.8 -2 5 -3 -4 122.59 9.8 1 -5 -3 -4 111.99 9.1 -2 5 3 -4 111.99 9.1 1 -5 -3 -4 104.69 9.1 -2 5 3 -4 104.69 9.1 1 -5 -3 -4 116.69 9.7 -2 5 3 -4 116.69 9.7 1 5 -3 4 104.59 9.2 -2 -5 3 4 104.59 9.2 1 -5 -3 -4 125.59 9.2 -2 5 3 -4 125.59 9.2 1 -5 -3 -4 117.79 9.9 -2 5 3 -4 117.79 9.9 1 -4 3 -4 285.17 19.6 -2 4 -3 -4 285.17 19.6 1 -4 3 -4 262.07 19 -2 4 -3 -4 262.07 19 1 -4 3 -4 293.97 19.3 -2 4 -3 -4 293.97 19.3 1 -4 -3 -4 281.77 19.5 -2 4 3 -4 281.77 19.5 1 -4 -3 -4 234.38 18.8 -2 4 3 -4 234.38 18.8 1 4 -3 4 264.17 19 -2 -4 3 4 264.17 19 1 -4 -3 -4 244.68 19 -2 4 3 -4 244.68 19 1 3 3 4 414.26 30.6 -2 -3 -3 4 414.26 30.6 1 -3 3 -4 456.05 31.1 -2 3 -3 -4 456.05 31.1 1 -3 3 -4 426.66 30.8 -2 3 -3 -4 426.66 30.8 1 -3 3 -4 441.56 30.7 -2 3 -3 -4 441.56 30.7 1 3 -3 4 416.66 30.9 -2 -3 3 4 416.66 30.9 1 3 -3 4 472.75 30.4 -2 -3 3 4 472.75 30.4 1 -3 -3 -4 440.36 30.8 -2 3 3 -4 440.36 30.8 1 -3 -3 -4 434.56 30.5 -2 3 3 -4 434.56 30.5 1 3 -3 4 431.66 30.6 -2 -3 3 4 431.66 30.6 1 -2 3 -4 261.37 19 -2 2 -3 -4 261.37 19 1 -2 3 -4 273.27 18.8 -2 2 -3 -4 273.27 18.8 1 -2 3 -4 267.67 19.2 -2 2 -3 -4 267.67 19.2 1 -2 3 -4 260.77 19 -2 2 -3 -4 260.77 19 1 2 3 4 274.47 18.9 -2 -2 -3 4 274.47 18.9 1 -2 -3 -4 284.17 18.9 -2 2 3 -4 284.17 18.9 1 2 -3 4 263.47 19 -2 -2 3 4 263.47 19 1 2 -3 4 271.47 18.8 -2 -2 3 4 271.47 18.8 1 2 -3 4 289.47 18.8 -2 -2 3 4 289.47 18.8 1 -2 -3 -4 271.77 19.1 -2 2 3 -4 271.77 19.1 1 2 -3 4 255.27 19.1 -2 -2 3 4 255.27 19.1 1 -2 -3 -4 249.28 18.9 -2 2 3 -4 249.28 18.9 1 -1 3 -4 120.79 9 -2 1 -3 -4 120.79 9 1 -1 3 -4 119.29 9.1 -2 1 -3 -4 119.29 9.1 1 -1 3 -4 127.79 9 -2 1 -3 -4 127.79 9 1 -1 3 -4 125.99 9.3 -2 1 -3 -4 125.99 9.3 1 1 3 4 116.39 9.2 -2 -1 -3 4 116.39 9.2 1 1 3 4 130.29 9 -2 -1 -3 4 130.29 9 1 1 -3 4 124.79 9.2 -2 -1 3 4 124.79 9.2 1 -1 -3 -4 129.59 9 -2 1 3 -4 129.59 9 1 1 -3 4 125.09 9.2 -2 -1 3 4 125.09 9.2 1 -1 -3 -4 121.69 9.1 -2 1 3 -4 121.69 9.1 1 1 -3 4 124.09 9 -2 -1 3 4 124.09 9 1 -1 -3 -4 120.89 9.2 -2 1 3 -4 120.89 9.2 1 0 3 -4 3495.75 231.78 -2 0 -3 -4 3495.75 231.78 1 0 3 -4 3322.77 231.78 -2 0 -3 -4 3322.77 231.78 1 0 3 -4 3337.67 231.78 -2 0 -3 -4 3337.67 231.78 1 0 3 4 3374.76 231.68 -2 0 -3 4 3374.76 231.68 1 0 3 4 3463.65 231.78 -2 0 -3 4 3463.65 231.78 1 0 3 4 3201.68 231.68 -2 0 -3 4 3201.68 231.68 1 0 -3 4 3249.18 231.68 -2 0 3 4 3249.18 231.68 1 0 -3 4 3374.46 231.68 -2 0 3 4 3374.46 231.68 1 0 -3 -4 3354.86 231.68 -2 0 3 -4 3354.86 231.68 1 0 -3 -4 3292.77 231.68 -2 0 3 -4 3292.77 231.68 1 0 -3 -4 3669.93 231.68 -2 0 3 -4 3669.93 231.68 1 0 -3 4 3284.37 231.78 -2 0 3 4 3284.37 231.78 1 -1 3 4 121.99 8.8 -2 1 -3 4 121.99 8.8 1 1 3 -4 114.19 8.8 -2 -1 -3 -4 114.19 8.8 1 -1 3 4 115.39 8.7 -2 1 -3 4 115.39 8.7 1 1 3 -4 114.29 8.9 -2 -1 -3 -4 114.29 8.9 1 -1 3 4 130.39 8.9 -2 1 -3 4 130.39 8.9 1 1 3 -4 119.89 8.9 -2 -1 -3 -4 119.89 8.9 1 -1 3 4 117.69 8.9 -2 1 -3 4 117.69 8.9 1 -1 -3 4 114.09 8.8 -2 1 3 4 114.09 8.8 1 1 -3 -4 129.39 8.8 -2 -1 3 -4 129.39 8.8 1 -1 -3 4 124.29 8.9 -2 1 3 4 124.29 8.9 1 -1 -3 4 119.09 8.8 -2 1 3 4 119.09 8.8 1 1 -3 -4 122.49 8.9 -2 -1 3 -4 122.49 8.9 1 1 -3 -4 118.39 8.9 -2 -1 3 -4 118.39 8.9 1 -2 3 4 281.97 19.1 -2 2 -3 4 281.97 19.1 1 -2 3 4 265.97 19.3 -2 2 -3 4 265.97 19.3 1 -2 3 4 248.98 18.9 -2 2 -3 4 248.98 18.9 1 2 3 -4 263.17 19.2 -2 -2 -3 -4 263.17 19.2 1 -2 3 4 263.77 19.2 -2 2 -3 4 263.77 19.2 1 2 3 -4 271.07 19.1 -2 -2 -3 -4 271.07 19.1 1 2 -3 -4 293.47 19 -2 -2 3 -4 293.47 19 1 2 -3 -4 266.17 18.9 -2 -2 3 -4 266.17 18.9 1 -2 -3 4 252.97 19 -2 2 3 4 252.97 19 1 -2 -3 4 281.87 19.1 -2 2 3 4 281.87 19.1 1 -2 -3 4 274.37 19.2 -2 2 3 4 274.37 19.2 1 2 -3 -4 278.27 19.1 -2 -2 3 -4 278.27 19.1 1 -2 -3 4 277.07 19.2 -2 2 3 4 277.07 19.2 1 -3 3 4 453.15 30.2 -2 3 -3 4 453.15 30.2 1 -3 3 4 407.66 30.3 -2 3 -3 4 407.66 30.3 1 -3 3 4 442.46 30.5 -2 3 -3 4 442.46 30.5 1 -3 3 4 426.66 30 -2 3 -3 4 426.66 30 1 3 3 -4 423.76 30.1 -2 -3 -3 -4 423.76 30.1 1 -3 -3 4 415.76 30.2 -2 3 3 4 415.76 30.2 1 -3 -3 4 431.76 30.2 -2 3 3 4 431.76 30.2 1 -3 -3 4 405.26 30.2 -2 3 3 4 405.26 30.2 1 3 -3 -4 495.95 30 -2 -3 3 -4 495.95 30 1 3 -3 -4 429.96 30.1 -2 -3 3 -4 429.96 30.1 1 -3 -3 4 404.16 30 -2 3 3 4 404.16 30 1 -4 3 4 291.07 19.5 -2 4 -3 4 291.07 19.5 1 -4 3 4 270.37 18.9 -2 4 -3 4 270.37 18.9 1 -4 3 4 278.97 18.6 -2 4 -3 4 278.97 18.6 1 4 3 -4 256.57 19.1 -2 -4 -3 -4 256.57 19.1 1 4 -3 -4 241.58 18.9 -2 -4 3 -4 241.58 18.9 1 -4 -3 4 258.67 18.9 -2 4 3 4 258.67 18.9 1 -4 -3 4 265.77 18.8 -2 4 3 4 265.77 18.8 1 -4 -3 4 268.97 19 -2 4 3 4 268.97 19 1 4 -3 -4 267.87 18.6 -2 -4 3 -4 267.87 18.6 1 -4 -3 4 240.58 18.7 -2 4 3 4 240.58 18.7 1 -5 3 4 120.99 8.8 -2 5 -3 4 120.99 8.8 1 -5 3 4 131.19 10.2 -2 5 -3 4 131.19 10.2 1 -5 -3 4 113.29 8.5 -2 5 3 4 113.29 8.5 1 -5 -3 4 106.49 8.6 -2 5 3 4 106.49 8.6 1 -5 -3 4 104.99 8.7 -2 5 3 4 104.99 8.7 1 -5 -3 4 89.79 9 -2 5 3 4 89.79 9 1 -5 -3 4 107.69 9 -2 5 3 4 107.69 9 1 5 -3 -4 101.59 8.8 -2 -5 3 -4 101.59 8.8 1 -6 3 4 179.28 13.4 -2 6 -3 4 179.28 13.4 1 -6 3 4 169.68 13.5 -2 6 -3 4 169.68 13.5 1 -6 -3 4 182.48 13.6 -2 6 3 4 182.48 13.6 1 -6 -3 4 160.08 14.2 -2 6 3 4 160.08 14.2 1 -6 -3 4 187.68 13.9 -2 6 3 4 187.68 13.9 1 -6 -3 4 189.48 13.7 -2 6 3 4 189.48 13.7 1 -6 -3 4 158.18 13.8 -2 6 3 4 158.18 13.8 1 -7 3 4 73.49 8 -2 7 -3 4 73.49 8 1 -7 3 4 104.99 10.8 -2 7 -3 4 104.99 10.8 1 -7 -3 4 60.79 8.1 -2 7 3 4 60.79 8.1 1 -7 -3 4 88.69 9.6 -2 7 3 4 88.69 9.6 1 -7 -3 4 66.29 8.2 -2 7 3 4 66.29 8.2 1 -7 -3 4 83.69 8.6 -2 7 3 4 83.69 8.6 1 -8 3 4 15.4 5.4 -2 8 -3 4 15.4 5.4 1 -8 -3 4 14.9 7 -2 8 3 4 14.9 7 1 -8 -4 -4 20.8 6.3 -2 8 4 -4 20.8 6.3 1 -8 -4 -4 28.5 5.7 -2 8 4 -4 28.5 5.7 1 -8 -4 -4 16.1 4.4 -2 8 4 -4 16.1 4.4 1 -8 -4 -4 15.5 5.5 -2 8 4 -4 15.5 5.5 1 -7 4 -4 26.3 6.4 -2 7 -4 -4 26.3 6.4 1 -7 4 -4 26.4 6.9 -2 7 -4 -4 26.4 6.9 1 -7 -4 -4 40.3 6.6 -2 7 4 -4 40.3 6.6 1 -7 -4 -4 25 4.5 -2 7 4 -4 25 4.5 1 -7 -4 -4 36.9 5.4 -2 7 4 -4 36.9 5.4 1 -6 4 -4 104.79 9.3 -2 6 -4 -4 104.79 9.3 1 -6 4 -4 84.39 8.3 -2 6 -4 -4 84.39 8.3 1 -6 -4 -4 74.89 7.9 -2 6 4 -4 74.89 7.9 1 -6 -4 -4 77.49 8.2 -2 6 4 -4 77.49 8.2 1 -6 -4 -4 74.19 7.5 -2 6 4 -4 74.19 7.5 1 6 -4 4 71.79 7.5 -2 -6 4 4 71.79 7.5 1 -5 4 -4 135.19 10.4 -2 5 -4 -4 135.19 10.4 1 -5 4 -4 122.89 10.7 -2 5 -4 -4 122.89 10.7 1 -5 -4 -4 116.39 10 -2 5 4 -4 116.39 10 1 -5 -4 -4 115.79 10.1 -2 5 4 -4 115.79 10.1 1 5 -4 4 116.49 10.1 -2 -5 4 4 116.49 10.1 1 -5 -4 -4 143.39 10.7 -2 5 4 -4 143.39 10.7 1 -5 -4 -4 126.09 10.1 -2 5 4 -4 126.09 10.1 1 -5 -4 -4 126.39 9.7 -2 5 4 -4 126.39 9.7 1 -4 4 -4 43.1 5.4 -2 4 -4 -4 43.1 5.4 1 4 4 4 53.09 5 -2 -4 -4 4 53.09 5 1 -4 4 -4 49.7 5.7 -2 4 -4 -4 49.7 5.7 1 -4 -4 -4 54.39 4.6 -2 4 4 -4 54.39 4.6 1 -4 -4 -4 52.19 5.4 -2 4 4 -4 52.19 5.4 1 -4 -4 -4 50.69 5.9 -2 4 4 -4 50.69 5.9 1 4 -4 4 47.4 5.2 -2 -4 4 4 47.4 5.2 1 -4 -4 -4 59.99 4.9 -2 4 4 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0 -4 4 2165.18 153.68 -2 0 4 4 2165.18 153.68 1 -1 4 4 464.45 33.6 -2 1 -4 4 464.45 33.6 1 1 4 -4 473.75 33.7 -2 -1 -4 -4 473.75 33.7 1 1 4 -4 513.95 33.6 -2 -1 -4 -4 513.95 33.6 1 -1 4 4 450.75 33.6 -2 1 -4 4 450.75 33.6 1 -1 4 4 499.75 33.7 -2 1 -4 4 499.75 33.7 1 -1 4 4 452.15 33.6 -2 1 -4 4 452.15 33.6 1 -1 -4 4 468.95 33.7 -2 1 4 4 468.95 33.7 1 1 -4 -4 506.95 33.7 -2 -1 4 -4 506.95 33.7 1 -1 -4 4 478.85 33.6 -2 1 4 4 478.85 33.6 1 -1 -4 4 489.65 33.6 -2 1 4 4 489.65 33.6 1 1 -4 -4 503.35 33.7 -2 -1 4 -4 503.35 33.7 1 1 -4 -4 486.75 33.7 -2 -1 4 -4 486.75 33.7 1 -2 4 4 117.99 8.8 -2 2 -4 4 117.99 8.8 1 -2 4 4 113.39 8.6 -2 2 -4 4 113.39 8.6 1 2 4 -4 98.29 8.6 -2 -2 -4 -4 98.29 8.6 1 -2 4 4 113.89 8.6 -2 2 -4 4 113.89 8.6 1 2 4 -4 109.59 8.5 -2 -2 -4 -4 109.59 8.5 1 -2 4 4 110.49 8.4 -2 2 -4 4 110.49 8.4 1 2 -4 -4 106.89 8.5 -2 -2 4 -4 106.89 8.5 1 2 -4 -4 114.69 8.4 -2 -2 4 -4 114.69 8.4 1 -2 -4 4 119.29 8.4 -2 2 4 4 119.29 8.4 1 -2 -4 4 119.39 8.6 -2 2 4 4 119.39 8.6 1 -2 -4 4 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2 -2 -8 67.49 5.4 1 2 2 8 58.89 5.5 -2 -2 -2 8 58.89 5.5 1 -2 2 -8 62.09 5.3 -2 2 -2 -8 62.09 5.3 1 -2 2 -8 62.39 5.1 -2 2 -2 -8 62.39 5.1 1 -2 2 -8 66.79 5.7 -2 2 -2 -8 66.79 5.7 1 2 -2 8 66.89 5.5 -2 -2 2 8 66.89 5.5 1 -2 -2 -8 66.49 5.4 -2 2 2 -8 66.49 5.4 1 -2 -2 -8 62.89 5.3 -2 2 2 -8 62.89 5.3 1 -2 -2 -8 64.69 5.1 -2 2 2 -8 64.69 5.1 1 2 -2 8 67.59 5.1 -2 -2 2 8 67.59 5.1 1 -2 -2 -8 57.89 5 -2 2 2 -8 57.89 5 1 2 -2 8 65.09 5.4 -2 -2 2 8 65.09 5.4 1 1 2 8 318.87 21.3 -2 -1 -2 8 318.87 21.3 1 1 2 8 286.57 21.3 -2 -1 -2 8 286.57 21.3 1 -1 2 -8 307.67 21.4 -2 1 -2 -8 307.67 21.4 1 -1 2 -8 297.27 21.4 -2 1 -2 -8 297.27 21.4 1 -1 2 -8 313.17 21.3 -2 1 -2 -8 313.17 21.3 1 1 2 8 295.47 21.4 -2 -1 -2 8 295.47 21.4 1 -1 2 -8 309.87 21.6 -2 1 -2 -8 309.87 21.6 1 -1 -2 -8 282.67 21.3 -2 1 2 -8 282.67 21.3 1 1 -2 8 302.57 21.4 -2 -1 2 8 302.57 21.4 1 1 -2 8 327.07 21.4 -2 -1 2 8 327.07 21.4 1 -1 -2 -8 298.47 21.4 -2 1 2 -8 298.47 21.4 1 1 -2 8 307.27 21.2 -2 -1 2 8 307.27 21.2 1 1 -2 8 308.47 21.6 -2 -1 2 8 308.47 21.6 1 -1 -2 -8 293.17 21.4 -2 1 2 -8 293.17 21.4 1 -1 -2 -8 292.77 21.3 -2 1 2 -8 292.77 21.3 1 1 -2 8 330.17 21.4 -2 -1 2 8 330.17 21.4 1 0 2 -8 269.07 17.6 -2 0 -2 -8 269.07 17.6 1 0 2 -8 241.98 17.7 -2 0 -2 -8 241.98 17.7 1 0 2 -8 241.48 17.7 -2 0 -2 -8 241.48 17.7 1 0 2 8 239.58 17.7 -2 0 -2 8 239.58 17.7 1 0 2 -8 250.07 17.7 -2 0 -2 -8 250.07 17.7 1 0 2 8 255.77 17.7 -2 0 -2 8 255.77 17.7 1 0 2 8 246.78 17.6 -2 0 -2 8 246.78 17.6 1 0 2 8 247.28 17.7 -2 0 -2 8 247.28 17.7 1 0 2 -8 259.67 17.9 -2 0 -2 -8 259.67 17.9 1 0 -2 8 246.08 17.7 -2 0 2 8 246.08 17.7 1 0 -2 -8 255.67 17.7 -2 0 2 -8 255.67 17.7 1 0 -2 -8 243.48 17.6 -2 0 2 -8 243.48 17.6 1 0 -2 8 241.38 17.8 -2 0 2 8 241.38 17.8 1 0 -2 8 274.97 17.6 -2 0 2 8 274.97 17.6 1 0 -2 8 243.38 17.7 -2 0 2 8 243.38 17.7 1 0 -2 8 247.28 17.7 -2 0 2 8 247.28 17.7 1 0 -2 -8 262.97 17.8 -2 0 2 -8 262.97 17.8 1 0 -2 -8 241.78 17.7 -2 0 2 -8 241.78 17.7 1 1 2 -8 307.27 21.8 -2 -1 -2 -8 307.27 21.8 1 1 2 -8 303.67 21.9 -2 -1 -2 -8 303.67 21.9 1 1 2 -8 332.37 22 -2 -1 -2 -8 332.37 22 1 -1 2 8 308.27 21.8 -2 1 -2 8 308.27 21.8 1 1 2 -8 315.17 21.7 -2 -1 -2 -8 315.17 21.7 1 -1 2 8 317.17 21.9 -2 1 -2 8 317.17 21.9 1 1 2 -8 306.87 21.8 -2 -1 -2 -8 306.87 21.8 1 -1 2 8 303.37 21.8 -2 1 -2 8 303.37 21.8 1 1 -2 -8 325.07 22 -2 -1 2 -8 325.07 22 1 -1 -2 8 309.17 21.7 -2 1 2 8 309.17 21.7 1 -1 -2 8 313.07 21.9 -2 1 2 8 313.07 21.9 1 1 -2 -8 332.87 21.7 -2 -1 2 -8 332.87 21.7 1 -1 -2 8 311.87 21.9 -2 1 2 8 311.87 21.9 1 -1 -2 8 290.77 21.7 -2 1 2 8 290.77 21.7 1 1 -2 -8 298.77 21.8 -2 -1 2 -8 298.77 21.8 1 -1 -2 8 304.17 21.8 -2 1 2 8 304.17 21.8 1 1 -2 -8 305.97 21.8 -2 -1 2 -8 305.97 21.8 1 -2 2 8 50.99 5.7 -2 2 -2 8 50.99 5.7 1 -2 2 8 60.29 5.2 -2 2 -2 8 60.29 5.2 1 2 2 -8 56.59 5.7 -2 -2 -2 -8 56.59 5.7 1 2 2 -8 69.69 5.1 -2 -2 -2 -8 69.69 5.1 1 2 2 -8 68.89 5 -2 -2 -2 -8 68.89 5 1 -2 2 8 69.59 5.5 -2 2 -2 8 69.59 5.5 1 2 2 -8 59.59 5.3 -2 -2 -2 -8 59.59 5.3 1 -2 -2 8 62.29 5.5 -2 2 2 8 62.29 5.5 1 2 -2 -8 71.49 5.6 -2 -2 2 -8 71.49 5.6 1 2 -2 -8 65.19 5.2 -2 -2 2 -8 65.19 5.2 1 -2 -2 8 59.59 5.3 -2 2 2 8 59.59 5.3 1 -2 -2 8 62.79 5.5 -2 2 2 8 62.79 5.5 1 -2 -2 8 66.89 5 -2 2 2 8 66.89 5 1 -2 -2 8 62.69 5 -2 2 2 8 62.69 5 1 2 -2 -8 63.79 5.5 -2 -2 2 -8 63.79 5.5 1 -3 2 8 381.86 25.5 -2 3 -2 8 381.86 25.5 1 3 2 -8 397.96 25.5 -2 -3 -2 -8 397.96 25.5 1 -3 2 8 369.46 25.8 -2 3 -2 8 369.46 25.8 1 -3 2 8 361.76 25.8 -2 3 -2 8 361.76 25.8 1 3 2 -8 358.56 25.9 -2 -3 -2 -8 358.56 25.9 1 -3 -2 8 375.46 25.7 -2 3 2 8 375.46 25.7 1 3 -2 -8 352.26 25.7 -2 -3 2 -8 352.26 25.7 1 -3 -2 8 351.66 25.4 -2 3 2 8 351.66 25.4 1 -3 -2 8 379.96 26.1 -2 3 2 8 379.96 26.1 1 -3 -2 8 356.86 25.9 -2 3 2 8 356.86 25.9 1 3 -2 -8 370.36 25.5 -2 -3 2 -8 370.36 25.5 1 -3 -2 8 328.97 25.5 -2 3 2 8 328.97 25.5 1 4 2 -8 238.98 17.4 -2 -4 -2 -8 238.98 17.4 1 -4 2 8 271.67 18 -2 4 -2 8 271.67 18 1 -4 2 8 253.17 17.4 -2 4 -2 8 253.17 17.4 1 -4 -2 8 216.68 17 -2 4 2 8 216.68 17 1 -4 -2 8 231.58 17.3 -2 4 2 8 231.58 17.3 1 -4 -2 8 228.08 17.4 -2 4 2 8 228.08 17.4 1 -5 2 8 85.09 7.1 -2 5 -2 8 85.09 7.1 1 -5 2 8 78.69 8.1 -2 5 -2 8 78.69 8.1 1 5 2 -8 84.79 7.3 -2 -5 -2 -8 84.79 7.3 1 -5 -2 8 63.19 6.9 -2 5 2 8 63.19 6.9 1 -5 -2 8 73.19 7.2 -2 5 2 8 73.19 7.2 1 -6 2 8 59.29 10.2 -2 6 -2 8 59.29 10.2 1 -6 2 8 87.59 7.9 -2 6 -2 8 87.59 7.9 1 -6 -2 8 83.89 9.3 -2 6 2 8 83.89 9.3 1 -6 -2 8 80.69 7.6 -2 6 2 8 80.69 7.6 1 -6 -2 8 73.59 7.9 -2 6 2 8 73.59 7.9 1 -7 2 8 77.09 9.7 -2 7 -2 8 77.09 9.7 1 -7 2 8 50.99 6.3 -2 7 -2 8 50.99 6.3 1 -7 -2 8 50.79 6.6 -2 7 2 8 50.79 6.6 1 -7 -2 8 35.8 6.1 -2 7 2 8 35.8 6.1 1 -8 2 8 9.8 5.1 -2 8 -2 8 9.8 5.1 1 -8 2 8 14.1 7.1 -2 8 -2 8 14.1 7.1 1 -8 -2 8 4.9 5.5 -2 8 2 8 4.9 5.5 1 -8 -2 8 19.9 6.7 -2 8 2 8 19.9 6.7 1 -8 -2 8 11.3 5.3 -2 8 2 8 11.3 5.3 1 -8 3 -8 12.2 6.5 -2 8 -3 -8 12.2 6.5 1 -8 -3 -8 1.8 5.7 -2 8 3 -8 1.8 5.7 1 -8 -3 -8 4.1 4.8 -2 8 3 -8 4.1 4.8 1 -7 3 -8 49.2 8.1 -2 7 -3 -8 49.2 8.1 1 -7 -3 -8 61.29 7.4 -2 7 3 -8 61.29 7.4 1 -7 -3 -8 63.59 7.5 -2 7 3 -8 63.59 7.5 1 -6 3 -8 87.29 8.6 -2 6 -3 -8 87.29 8.6 1 -6 -3 -8 62.09 6.7 -2 6 3 -8 62.09 6.7 1 -6 -3 -8 58.39 7.1 -2 6 3 -8 58.39 7.1 1 -6 -3 -8 77.79 8 -2 6 3 -8 77.79 8 1 -6 -3 -8 79.69 8.6 -2 6 3 -8 79.69 8.6 1 5 3 8 55.49 7 -2 -5 -3 8 55.49 7 1 -5 3 -8 85.19 7.5 -2 5 -3 -8 85.19 7.5 1 -5 3 -8 92.79 7.6 -2 5 -3 -8 92.79 7.6 1 -5 -3 -8 71.39 7.8 -2 5 3 -8 71.39 7.8 1 -5 -3 -8 70.29 7 -2 5 3 -8 70.29 7 1 -5 -3 -8 72.79 6.1 -2 5 3 -8 72.79 6.1 1 -5 -3 -8 72.29 6.5 -2 5 3 -8 72.29 6.5 1 -4 3 -8 111.89 8.6 -2 4 -3 -8 111.89 8.6 1 4 3 8 93.99 8.2 -2 -4 -3 8 93.99 8.2 1 -4 3 -8 117.49 8.9 -2 4 -3 -8 117.49 8.9 1 4 -3 8 114.49 8.4 -2 -4 3 8 114.49 8.4 1 -4 -3 -8 85.99 8 -2 4 3 -8 85.99 8 1 -4 -3 -8 108.79 8.8 -2 4 3 -8 108.79 8.8 1 -4 -3 -8 95.69 7.9 -2 4 3 -8 95.69 7.9 1 -4 -3 -8 103.09 8.4 -2 4 3 -8 103.09 8.4 1 -3 3 -8 455.85 32.1 -2 3 -3 -8 455.85 32.1 1 3 3 8 408.46 32 -2 -3 -3 8 408.46 32 1 -3 3 -8 494.05 32.3 -2 3 -3 -8 494.05 32.3 1 -3 3 -8 475.25 31.7 -2 3 -3 -8 475.25 31.7 1 -3 -3 -8 492.15 32.3 -2 3 3 -8 492.15 32.3 1 3 -3 8 446.96 32 -2 -3 3 8 446.96 32 1 3 -3 8 482.75 31.7 -2 -3 3 8 482.75 31.7 1 -3 -3 -8 407.46 31.9 -2 3 3 -8 407.46 31.9 1 -3 -3 -8 437.36 31.8 -2 3 3 -8 437.36 31.8 1 -3 -3 -8 452.35 32 -2 3 3 -8 452.35 32 1 -2 3 -8 230.08 15.2 -2 2 -3 -8 230.08 15.2 1 -2 3 -8 234.28 15.4 -2 2 -3 -8 234.28 15.4 1 2 3 8 197.28 15.3 -2 -2 -3 8 197.28 15.3 1 -2 3 -8 205.48 15.3 -2 2 -3 -8 205.48 15.3 1 -2 3 -8 216.08 15.6 -2 2 -3 -8 216.08 15.6 1 -2 -3 -8 220.98 15.6 -2 2 3 -8 220.98 15.6 1 2 -3 8 208.98 15.6 -2 -2 3 8 208.98 15.6 1 2 -3 8 216.48 15.5 -2 -2 3 8 216.48 15.5 1 -2 -3 -8 195.98 15.3 -2 2 3 -8 195.98 15.3 1 2 -3 8 225.78 15.4 -2 -2 3 8 225.78 15.4 1 -2 -3 -8 212.08 15.3 -2 2 3 -8 212.08 15.3 1 -2 -3 -8 195.28 15.1 -2 2 3 -8 195.28 15.1 1 2 -3 8 214.18 15.2 -2 -2 3 8 214.18 15.2 1 1 3 8 433.66 32.2 -2 -1 -3 8 433.66 32.2 1 -1 3 -8 453.85 32.2 -2 1 -3 -8 453.85 32.2 1 -1 3 -8 437.16 32.2 -2 1 -3 -8 437.16 32.2 1 1 3 8 492.85 32.3 -2 -1 -3 8 492.85 32.3 1 -1 3 -8 486.85 32.4 -2 1 -3 -8 486.85 32.4 1 -1 3 -8 484.55 32.5 -2 1 -3 -8 484.55 32.5 1 1 -3 8 443.46 32.4 -2 -1 3 8 443.46 32.4 1 -1 -3 -8 431.26 32.1 -2 1 3 -8 431.26 32.1 1 1 -3 8 466.75 32.2 -2 -1 3 8 466.75 32.2 1 -1 -3 -8 466.65 32.4 -2 1 3 -8 466.65 32.4 1 -1 -3 -8 483.45 32.3 -2 1 3 -8 483.45 32.3 1 -1 -3 -8 479.25 32.4 -2 1 3 -8 479.25 32.4 1 1 -3 8 475.05 32.2 -2 -1 3 8 475.05 32.2 1 1 -3 8 443.06 32.3 -2 -1 3 8 443.06 32.3 1 1 -3 8 453.35 32.2 -2 -1 3 8 453.35 32.2 1 0 3 -8 829.42 58.79 -2 0 -3 -8 829.42 58.79 1 0 3 8 823.02 58.79 -2 0 -3 8 823.02 58.79 1 0 3 8 888.91 58.79 -2 0 -3 8 888.91 58.79 1 0 3 -8 854.01 58.79 -2 0 -3 -8 854.01 58.79 1 0 3 -8 869.81 58.89 -2 0 -3 -8 869.81 58.89 1 0 3 -8 840.72 58.59 -2 0 -3 -8 840.72 58.59 1 0 3 8 821.02 58.59 -2 0 -3 8 821.02 58.59 1 0 -3 -8 825.22 58.79 -2 0 3 -8 825.22 58.79 1 0 -3 -8 858.21 58.79 -2 0 3 -8 858.21 58.79 1 0 -3 8 847.02 58.79 -2 0 3 8 847.02 58.79 1 0 -3 8 838.82 58.69 -2 0 3 8 838.82 58.69 1 0 -3 8 811.92 58.89 -2 0 3 8 811.92 58.89 1 0 -3 8 861.31 58.79 -2 0 3 8 861.31 58.79 1 0 -3 8 871.81 58.79 -2 0 3 8 871.81 58.79 1 0 -3 -8 841.02 58.79 -2 0 3 -8 841.02 58.79 1 0 -3 -8 905.41 58.89 -2 0 3 -8 905.41 58.89 1 1 3 -8 439.26 31.5 -2 -1 -3 -8 439.26 31.5 1 1 3 -8 485.45 31.7 -2 -1 -3 -8 485.45 31.7 1 1 3 -8 446.76 31.3 -2 -1 -3 -8 446.76 31.3 1 -1 3 8 436.86 31.2 -2 1 -3 8 436.86 31.2 1 -1 3 8 429.46 31.3 -2 1 -3 8 429.46 31.3 1 -1 3 8 471.05 31.4 -2 1 -3 8 471.05 31.4 1 1 -3 -8 447.76 31.3 -2 -1 3 -8 447.76 31.3 1 1 -3 -8 481.85 31.3 -2 -1 3 -8 481.85 31.3 1 -1 -3 8 408.26 31.4 -2 1 3 8 408.26 31.4 1 1 -3 -8 459.45 31.4 -2 -1 3 -8 459.45 31.4 1 -1 -3 8 440.76 31.4 -2 1 3 8 440.76 31.4 1 -1 -3 8 418.46 31.3 -2 1 3 8 418.46 31.3 1 -1 -3 8 434.76 31.4 -2 1 3 8 434.76 31.4 1 1 -3 -8 488.15 31.6 -2 -1 3 -8 488.15 31.6 1 2 3 -8 201.98 15.8 -2 -2 -3 -8 201.98 15.8 1 -2 3 8 216.98 15.5 -2 2 -3 8 216.98 15.5 1 2 3 -8 226.48 15.7 -2 -2 -3 -8 226.48 15.7 1 -2 3 8 223.68 15.8 -2 2 -3 8 223.68 15.8 1 -2 3 8 231.38 15.8 -2 2 -3 8 231.38 15.8 1 2 -3 -8 215.28 15.6 -2 -2 3 -8 215.28 15.6 1 2 -3 -8 221.18 15.8 -2 -2 3 -8 221.18 15.8 1 -2 -3 8 199.48 15.6 -2 2 3 8 199.48 15.6 1 2 -3 -8 232.58 15.6 -2 -2 3 -8 232.58 15.6 1 -2 -3 8 213.58 15.8 -2 2 3 8 213.58 15.8 1 -2 -3 8 224.08 15.9 -2 2 3 8 224.08 15.9 1 2 -3 -8 245.98 16 -2 -2 3 -8 245.98 16 1 -2 -3 8 204.78 15.8 -2 2 3 8 204.78 15.8 1 -3 3 8 500.85 33.6 -2 3 -3 8 500.85 33.6 1 -3 3 8 497.45 34 -2 3 -3 8 497.45 34 1 3 3 -8 521.65 33.8 -2 -3 -3 -8 521.65 33.8 1 3 3 -8 501.15 33.4 -2 -3 -3 -8 501.15 33.4 1 -3 -3 8 458.05 33.6 -2 3 3 8 458.05 33.6 1 -3 -3 8 478.95 33.7 -2 3 3 8 478.95 33.7 1 -3 -3 8 443.46 33.3 -2 3 3 8 443.46 33.3 1 3 -3 -8 432.56 33.2 -2 -3 3 -8 432.56 33.2 1 -4 3 8 120.99 9.5 -2 4 -3 8 120.99 9.5 1 4 3 -8 105.09 8.3 -2 -4 -3 -8 105.09 8.3 1 -4 3 8 111.39 8.7 -2 4 -3 8 111.39 8.7 1 -4 -3 8 108.59 8.6 -2 4 3 8 108.59 8.6 1 -4 -3 8 97.59 8.1 -2 4 3 8 97.59 8.1 1 -4 -3 8 109.79 8.1 -2 4 3 8 109.79 8.1 1 -4 -3 8 101.69 8.8 -2 4 3 8 101.69 8.8 1 -5 3 8 89.79 8.8 -2 5 -3 8 89.79 8.8 1 -5 3 8 83.79 7.5 -2 5 -3 8 83.79 7.5 1 -5 -3 8 69.29 7.2 -2 5 3 8 69.29 7.2 1 -5 -3 8 71.69 7.6 -2 5 3 8 71.69 7.6 1 -5 -3 8 90.09 6.9 -2 5 3 8 90.09 6.9 1 -5 -3 8 87.49 7.8 -2 5 3 8 87.49 7.8 1 -6 3 8 92.79 10.3 -2 6 -3 8 92.79 10.3 1 -6 3 8 79.49 8.3 -2 6 -3 8 79.49 8.3 1 -6 -3 8 90.79 8.3 -2 6 3 8 90.79 8.3 1 -6 -3 8 92.49 8.6 -2 6 3 8 92.49 8.6 1 -6 -3 8 82.09 9.3 -2 6 3 8 82.09 9.3 1 -7 3 8 43.2 5.8 -2 7 -3 8 43.2 5.8 1 -7 3 8 45.8 8.3 -2 7 -3 8 45.8 8.3 1 -7 -3 8 41.3 8.3 -2 7 3 8 41.3 8.3 1 -7 -3 8 24.6 5.8 -2 7 3 8 24.6 5.8 1 -7 -3 8 31.4 5.9 -2 7 3 8 31.4 5.9 1 -8 3 8 0.7 5.3 -2 8 -3 8 0.7 5.3 1 -8 -3 8 -0.4 5.7 -2 8 3 8 -0.4 5.7 1 -8 -3 8 1.9 5.1 -2 8 3 8 1.9 5.1 1 -8 4 -8 40 8 -2 8 -4 -8 40 8 1 -8 4 -8 31.9 7.5 -2 8 -4 -8 31.9 7.5 1 -8 -4 -8 26.1 7.3 -2 8 4 -8 26.1 7.3 1 -8 -4 -8 25.5 7.1 -2 8 4 -8 25.5 7.1 1 -7 4 -8 43.4 7.5 -2 7 -4 -8 43.4 7.5 1 -7 4 -8 44.4 7.1 -2 7 -4 -8 44.4 7.1 1 -7 -4 -8 38.5 6.3 -2 7 4 -8 38.5 6.3 1 -7 -4 -8 36.7 6.4 -2 7 4 -8 36.7 6.4 1 -7 -4 -8 27.6 4.5 -2 7 4 -8 27.6 4.5 1 -7 -4 -8 36.9 6.6 -2 7 4 -8 36.9 6.6 1 -6 4 -8 155.68 12.3 -2 6 -4 -8 155.68 12.3 1 -6 -4 -8 123.49 10.2 -2 6 4 -8 123.49 10.2 1 -6 -4 -8 118.79 11.7 -2 6 4 -8 118.79 11.7 1 -6 -4 -8 113.79 11.4 -2 6 4 -8 113.79 11.4 1 -5 4 -8 54.89 6.2 -2 5 -4 -8 54.89 6.2 1 -5 4 -8 51.49 7.2 -2 5 -4 -8 51.49 7.2 1 -5 -4 -8 57.89 6.2 -2 5 4 -8 57.89 6.2 1 -5 -4 -8 49.6 6.6 -2 5 4 -8 49.6 6.6 1 -5 -4 -8 61.09 5.9 -2 5 4 -8 61.09 5.9 1 5 -4 8 36.2 5.6 -2 -5 4 8 36.2 5.6 1 -5 -4 -8 55.19 5.4 -2 5 4 -8 55.19 5.4 1 -4 4 -8 8.5 3.1 -2 4 -4 -8 8.5 3.1 1 -4 4 -8 7.4 3.3 -2 4 -4 -8 7.4 3.3 1 -4 -4 -8 3.2 2.5 -2 4 4 -8 3.2 2.5 1 -4 -4 -8 5.9 3.6 -2 4 4 -8 5.9 3.6 1 -4 -4 -8 11.5 2.9 -2 4 4 -8 11.5 2.9 1 4 -4 8 10.1 3.1 -2 -4 4 8 10.1 3.1 1 -3 4 -8 223.28 15.4 -2 3 -4 -8 223.28 15.4 1 3 4 8 199.98 15.6 -2 -3 -4 8 199.98 15.6 1 -3 4 -8 221.98 15.8 -2 3 -4 -8 221.98 15.8 1 -3 4 -8 220.78 16.1 -2 3 -4 -8 220.78 16.1 1 3 -4 8 198.68 15.3 -2 -3 4 8 198.68 15.3 1 -3 -4 -8 203.28 15.5 -2 3 4 -8 203.28 15.5 1 -3 -4 -8 211.28 16 -2 3 4 -8 211.28 16 1 -3 -4 -8 213.08 15.6 -2 3 4 -8 213.08 15.6 1 3 -4 8 221.88 15.8 -2 -3 4 8 221.88 15.8 1 3 -4 8 228.48 15.4 -2 -3 4 8 228.48 15.4 1 2 4 8 310.07 22 -2 -2 -4 8 310.07 22 1 -2 4 -8 303.47 22 -2 2 -4 -8 303.47 22 1 -2 4 -8 309.77 21.9 -2 2 -4 -8 309.77 21.9 1 -2 4 -8 305.67 22.3 -2 2 -4 -8 305.67 22.3 1 2 -4 8 294.07 21.9 -2 -2 4 8 294.07 21.9 1 2 -4 8 317.57 22.6 -2 -2 4 8 317.57 22.6 1 -2 -4 -8 337.37 22 -2 2 4 -8 337.37 22 1 2 -4 8 307.87 22.1 -2 -2 4 8 307.87 22.1 1 -2 -4 -8 294.77 21.9 -2 2 4 -8 294.77 21.9 1 -2 -4 -8 318.07 22.3 -2 2 4 -8 318.07 22.3 1 -1 4 -8 295.67 21.8 -2 1 -4 -8 295.67 21.8 1 1 4 8 317.87 21.5 -2 -1 -4 8 317.87 21.5 1 1 4 8 310.97 21.6 -2 -1 -4 8 310.97 21.6 1 -1 4 -8 282.47 21.6 -2 1 -4 -8 282.47 21.6 1 -1 4 -8 285.77 21.4 -2 1 -4 -8 285.77 21.4 1 1 -4 8 291.87 21.8 -2 -1 4 8 291.87 21.8 1 -1 -4 -8 274.27 21.5 -2 1 4 -8 274.27 21.5 1 -1 -4 -8 351.06 21.6 -2 1 4 -8 351.06 21.6 1 -1 -4 -8 326.97 21.8 -2 1 4 -8 326.97 21.8 1 1 -4 8 305.57 21.5 -2 -1 4 8 305.57 21.5 1 0 4 -8 370.16 27.5 -2 0 -4 -8 370.16 27.5 1 0 4 8 410.36 27.5 -2 0 -4 8 410.36 27.5 1 0 4 -8 386.26 27.2 -2 0 -4 -8 386.26 27.2 1 0 4 -8 413.06 27.6 -2 0 -4 -8 413.06 27.6 1 0 4 8 420.26 27.6 -2 0 -4 8 420.26 27.6 1 0 4 -8 397.36 27.6 -2 0 -4 -8 397.36 27.6 1 0 -4 8 369.36 27.6 -2 0 4 8 369.36 27.6 1 0 -4 -8 422.26 27.5 -2 0 4 -8 422.26 27.5 1 0 -4 8 377.46 27.5 -2 0 4 8 377.46 27.5 1 0 -4 -8 375.46 27.5 -2 0 4 -8 375.46 27.5 1 0 -4 8 408.66 27.5 -2 0 4 8 408.66 27.5 1 0 -4 -8 398.86 27.6 -2 0 4 -8 398.86 27.6 1 0 -4 8 352.46 27.2 -2 0 4 8 352.46 27.2 1 0 -4 8 374.06 27.5 -2 0 4 8 374.06 27.5 1 0 -4 -8 392.06 27.5 -2 0 4 -8 392.06 27.5 1 1 4 -8 272.17 20.8 -2 -1 -4 -8 272.17 20.8 1 -1 4 8 267.27 20.5 -2 1 -4 8 267.27 20.5 1 1 4 -8 288.27 20.7 -2 -1 -4 -8 288.27 20.7 1 -1 4 8 287.87 20.6 -2 1 -4 8 287.87 20.6 1 1 4 -8 280.27 20.7 -2 -1 -4 -8 280.27 20.7 1 -1 4 8 326.37 20.8 -2 1 -4 8 326.37 20.8 1 -1 4 8 297.67 21.2 -2 1 -4 8 297.67 21.2 1 -1 -4 8 271.37 20.6 -2 1 4 8 271.37 20.6 1 1 -4 -8 303.77 20.7 -2 -1 4 -8 303.77 20.7 1 1 -4 -8 298.87 20.8 -2 -1 4 -8 298.87 20.8 1 1 -4 -8 325.27 20.8 -2 -1 4 -8 325.27 20.8 1 1 -4 -8 281.07 20.6 -2 -1 4 -8 281.07 20.6 1 -1 -4 8 312.27 21 -2 1 4 8 312.27 21 1 -1 -4 8 265.87 20.7 -2 1 4 8 265.87 20.7 1 -1 -4 8 285.97 20.7 -2 1 4 8 285.97 20.7 1 -2 4 8 294.97 21.1 -2 2 -4 8 294.97 21.1 1 -2 4 8 304.27 21.3 -2 2 -4 8 304.27 21.3 1 2 4 -8 281.37 21.3 -2 -2 -4 -8 281.37 21.3 1 -2 4 8 303.17 21.5 -2 2 -4 8 303.17 21.5 1 -2 4 8 295.67 21.3 -2 2 -4 8 295.67 21.3 1 -2 -4 8 267.37 21.1 -2 2 4 8 267.37 21.1 1 2 -4 -8 317.17 21.4 -2 -2 4 -8 317.17 21.4 1 -2 -4 8 291.77 21.5 -2 2 4 8 291.77 21.5 1 -2 -4 8 312.57 21.3 -2 2 4 8 312.57 21.3 1 -2 -4 8 300.07 21.3 -2 2 4 8 300.07 21.3 1 2 -4 -8 290.87 21.1 -2 -2 4 -8 290.87 21.1 1 2 -4 -8 317.17 21 -2 -2 4 -8 317.17 21 1 -3 4 8 216.38 15.3 -2 3 -4 8 216.38 15.3 1 3 4 -8 177.28 14.9 -2 -3 -4 -8 177.28 14.9 1 -3 4 8 201.08 14.4 -2 3 -4 8 201.08 14.4 1 -3 4 8 211.28 14.8 -2 3 -4 8 211.28 14.8 1 -3 -4 8 187.18 14.8 -2 3 4 8 187.18 14.8 1 -3 -4 8 192.38 14.7 -2 3 4 8 192.38 14.7 1 -3 -4 8 205.08 14.9 -2 3 4 8 205.08 14.9 1 3 -4 -8 203.58 14.4 -2 -3 4 -8 203.58 14.4 1 -3 -4 8 203.78 14.5 -2 3 4 8 203.78 14.5 1 -4 4 8 8.3 2.6 -2 4 -4 8 8.3 2.6 1 4 4 -8 7.2 2.8 -2 -4 -4 -8 7.2 2.8 1 -4 4 8 12 3.3 -2 4 -4 8 12 3.3 1 -4 4 8 13.5 4.2 -2 4 -4 8 13.5 4.2 1 -4 -4 8 4.4 3.1 -2 4 4 8 4.4 3.1 1 -4 -4 8 13.1 2.6 -2 4 4 8 13.1 2.6 1 -4 -4 8 8.2 3.2 -2 4 4 8 8.2 3.2 1 5 4 -8 29.6 5.1 -2 -5 -4 -8 29.6 5.1 1 -5 4 8 47.5 6.8 -2 5 -4 8 47.5 6.8 1 -5 4 8 42.3 4.6 -2 5 -4 8 42.3 4.6 1 -5 4 8 37.7 5.4 -2 5 -4 8 37.7 5.4 1 -5 -4 8 53.79 5.7 -2 5 4 8 53.79 5.7 1 -5 -4 8 57.49 5.6 -2 5 4 8 57.49 5.6 1 -5 -4 8 53.59 6 -2 5 4 8 53.59 6 1 -5 -4 8 49 4.9 -2 5 4 8 49 4.9 1 -6 4 8 155.48 12.7 -2 6 -4 8 155.48 12.7 1 -6 4 8 121.09 10.7 -2 6 -4 8 121.09 10.7 1 -6 -4 8 107.19 10.2 -2 6 4 8 107.19 10.2 1 -6 -4 8 119.09 11.4 -2 6 4 8 119.09 11.4 1 -6 -4 8 117.49 11.3 -2 6 4 8 117.49 11.3 1 -7 4 8 34.5 8.1 -2 7 -4 8 34.5 8.1 1 -7 -4 8 17.4 5.4 -2 7 4 8 17.4 5.4 1 -7 -4 8 20 5.2 -2 7 4 8 20 5.2 1 -7 -4 8 12 6.1 -2 7 4 8 12 6.1 1 -8 4 8 23.4 8.3 -2 8 -4 8 23.4 8.3 1 -8 4 8 15.4 5.8 -2 8 -4 8 15.4 5.8 1 -8 -4 8 15.7 8 -2 8 4 8 15.7 8 1 -8 -4 8 22.6 6.7 -2 8 4 8 22.6 6.7 1 -8 -4 8 22.8 6.1 -2 8 4 8 22.8 6.1 1 -8 5 -8 2.2 6.5 -2 8 -5 -8 2.2 6.5 1 -8 5 -8 -0.5 7.6 -2 8 -5 -8 -0.5 7.6 1 -8 -5 -8 1 4.4 -2 8 5 -8 1 4.4 1 -8 -5 -8 2.2 5.6 -2 8 5 -8 2.2 5.6 1 -7 5 -8 32.9 7 -2 7 -5 -8 32.9 7 1 -7 5 -8 28.8 6.6 -2 7 -5 -8 28.8 6.6 1 -7 -5 -8 13.2 4.4 -2 7 5 -8 13.2 4.4 1 -7 -5 -8 31.2 7.5 -2 7 5 -8 31.2 7.5 1 -6 5 -8 103.39 9.9 -2 6 -5 -8 103.39 9.9 1 -6 5 -8 106.99 9.8 -2 6 -5 -8 106.99 9.8 1 -6 -5 -8 80.19 8.7 -2 6 5 -8 80.19 8.7 1 -6 -5 -8 80.59 8.2 -2 6 5 -8 80.59 8.2 1 6 -5 8 78.79 9 -2 -6 5 8 78.79 9 1 -6 -5 -8 81.89 9.7 -2 6 5 -8 81.89 9.7 1 -6 -5 -8 65.49 9 -2 6 5 -8 65.49 9 1 -5 5 -8 73.29 8.5 -2 5 -5 -8 73.29 8.5 1 -5 5 -8 73.39 8 -2 5 -5 -8 73.39 8 1 5 -5 8 70.29 7.5 -2 -5 5 8 70.29 7.5 1 -5 -5 -8 66.19 8.1 -2 5 5 -8 66.19 8.1 1 -5 -5 -8 67.99 7.1 -2 5 5 -8 67.99 7.1 1 -4 5 -8 60.89 6.4 -2 4 -5 -8 60.89 6.4 1 -4 -5 -8 70.59 7.9 -2 4 5 -8 70.59 7.9 1 4 -5 8 56.89 6.6 -2 -4 5 8 56.89 6.6 1 3 5 8 144.49 10.2 -2 -3 -5 8 144.49 10.2 1 -3 5 -8 120.09 10.3 -2 3 -5 -8 120.09 10.3 1 -3 5 -8 135.89 10.8 -2 3 -5 -8 135.89 10.8 1 -3 -5 -8 153.08 10.2 -2 3 5 -8 153.08 10.2 1 3 -5 8 108.99 9.9 -2 -3 5 8 108.99 9.9 1 3 -5 8 114.39 9.9 -2 -3 5 8 114.39 9.9 1 -3 -5 -8 137.19 10.8 -2 3 5 -8 137.19 10.8 1 3 -5 8 136.39 10.5 -2 -3 5 8 136.39 10.5 1 -2 5 -8 62.69 6.1 -2 2 -5 -8 62.69 6.1 1 -2 5 -8 60.09 5.6 -2 2 -5 -8 60.09 5.6 1 -2 5 -8 59.09 5.5 -2 2 -5 -8 59.09 5.5 1 2 -5 8 61.59 5.9 -2 -2 5 8 61.59 5.9 1 2 -5 8 65.39 5.8 -2 -2 5 8 65.39 5.8 1 2 -5 8 54.19 5.7 -2 -2 5 8 54.19 5.7 1 -2 -5 -8 67.59 6.4 -2 2 5 -8 67.59 6.4 1 1 5 8 338.77 23.9 -2 -1 -5 8 338.77 23.9 1 -1 5 -8 320.37 23.1 -2 1 -5 -8 320.37 23.1 1 1 5 8 330.17 23.1 -2 -1 -5 8 330.17 23.1 1 -1 5 -8 314.67 22.8 -2 1 -5 -8 314.67 22.8 1 -1 -5 -8 331.17 22.9 -2 1 5 -8 331.17 22.9 1 1 -5 8 305.77 23.2 -2 -1 5 8 305.77 23.2 1 -1 -5 -8 316.87 23.2 -2 1 5 -8 316.87 23.2 1 1 -5 8 331.77 23.1 -2 -1 5 8 331.77 23.1 1 0 5 8 22.5 3.2 -2 0 -5 8 22.5 3.2 1 0 5 8 24.2 3.6 -2 0 -5 8 24.2 3.6 1 0 5 8 21.1 4 -2 0 -5 8 21.1 4 1 0 5 -8 34.9 4 -2 0 -5 -8 34.9 4 1 0 -5 -8 27.6 3.6 -2 0 5 -8 27.6 3.6 1 0 -5 -8 32.2 4 -2 0 5 -8 32.2 4 1 0 -5 8 31.7 3.9 -2 0 5 8 31.7 3.9 1 0 -5 8 29.6 3.9 -2 0 5 8 29.6 3.9 1 -1 5 8 336.97 23.4 -2 1 -5 8 336.97 23.4 1 -1 5 8 333.37 23.4 -2 1 -5 8 333.37 23.4 1 1 5 -8 353.46 23.4 -2 -1 -5 -8 353.46 23.4 1 -1 5 8 312.67 23.3 -2 1 -5 8 312.67 23.3 1 -1 5 8 312.87 23.3 -2 1 -5 8 312.87 23.3 1 1 -5 -8 336.77 23.4 -2 -1 5 -8 336.77 23.4 1 -1 -5 8 334.57 23.4 -2 1 5 8 334.57 23.4 1 -1 -5 8 304.47 23.5 -2 1 5 8 304.47 23.5 1 1 -5 -8 314.47 23.4 -2 -1 5 -8 314.47 23.4 1 -1 -5 8 327.97 23.3 -2 1 5 8 327.97 23.3 1 -1 -5 8 338.07 23.5 -2 1 5 8 338.07 23.5 1 2 5 -8 62.19 5.8 -2 -2 -5 -8 62.19 5.8 1 -2 5 8 61.89 5.5 -2 2 -5 8 61.89 5.5 1 -2 5 8 62.59 5.9 -2 2 -5 8 62.59 5.9 1 -2 -5 8 65.59 6.1 -2 2 5 8 65.59 6.1 1 2 -5 -8 59.89 5.8 -2 -2 5 -8 59.89 5.8 1 -2 -5 8 55.39 5.7 -2 2 5 8 55.39 5.7 1 2 -5 -8 58.19 5.7 -2 -2 5 -8 58.19 5.7 1 -2 -5 8 68.09 6 -2 2 5 8 68.09 6 1 -2 -5 8 65.19 5.7 -2 2 5 8 65.19 5.7 1 -3 5 8 122.59 10.2 -2 3 -5 8 122.59 10.2 1 -3 5 8 153.28 10.8 -2 3 -5 8 153.28 10.8 1 -3 -5 8 132.89 9.9 -2 3 5 8 132.89 9.9 1 3 -5 -8 111.49 9.9 -2 -3 5 -8 111.49 9.9 1 -3 -5 8 139.69 10.2 -2 3 5 8 139.69 10.2 1 -3 -5 8 116.39 10.3 -2 3 5 8 116.39 10.3 1 -3 -5 8 112.69 10 -2 3 5 8 112.69 10 1 3 -5 -8 133.89 10 -2 -3 5 -8 133.89 10 1 -4 5 8 58.39 7.5 -2 4 -5 8 58.39 7.5 1 -4 5 8 54.19 6 -2 4 -5 8 54.19 6 1 -5 5 8 71.19 6.5 -2 5 -5 8 71.19 6.5 1 -5 5 8 59.09 7.5 -2 5 -5 8 59.09 7.5 1 -5 5 8 67.99 8.8 -2 5 -5 8 67.99 8.8 1 -5 -5 8 56.89 7.3 -2 5 5 8 56.89 7.3 1 -5 -5 8 77.29 8 -2 5 5 8 77.29 8 1 -5 -5 8 69.99 7.6 -2 5 5 8 69.99 7.6 1 -6 5 8 101.29 11.4 -2 6 -5 8 101.29 11.4 1 -6 5 8 90.29 9.3 -2 6 -5 8 90.29 9.3 1 -6 -5 8 78.39 9.7 -2 6 5 8 78.39 9.7 1 -6 -5 8 108.29 8.8 -2 6 5 8 108.29 8.8 1 -6 -5 8 75.19 9.3 -2 6 5 8 75.19 9.3 1 -7 5 8 18 5.5 -2 7 -5 8 18 5.5 1 -7 -5 8 9.2 5.4 -2 7 5 8 9.2 5.4 1 -7 -5 8 14.7 6.6 -2 7 5 8 14.7 6.6 1 -8 5 8 4.4 6.6 -2 8 -5 8 4.4 6.6 1 -8 -5 8 1.3 5.5 -2 8 5 8 1.3 5.5 1 -7 -6 -8 19.2 6.5 -2 7 6 -8 19.2 6.5 1 -7 -6 -8 29 6.9 -2 7 6 -8 29 6.9 1 7 -6 8 27.9 6 -2 -7 6 8 27.9 6 1 -7 -6 -8 14.8 4.8 -2 7 6 -8 14.8 4.8 1 -7 -6 -8 14.8 5 -2 7 6 -8 14.8 5 1 -6 6 -8 14.7 6 -2 6 -6 -8 14.7 6 1 -6 6 -8 11.3 5.3 -2 6 -6 -8 11.3 5.3 1 -6 -6 -8 20.5 6.2 -2 6 6 -8 20.5 6.2 1 6 -6 8 5.6 4.7 -2 -6 6 8 5.6 4.7 1 -6 -6 -8 9.3 4.2 -2 6 6 -8 9.3 4.2 1 -6 -6 -8 15.7 6 -2 6 6 -8 15.7 6 1 -5 6 -8 169.98 13.4 -2 5 -6 -8 169.98 13.4 1 -5 -6 -8 123.79 11.6 -2 5 6 -8 123.79 11.6 1 -5 -6 -8 135.99 13.1 -2 5 6 -8 135.99 13.1 1 -5 -6 -8 147.49 13.2 -2 5 6 -8 147.49 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59.29 8.5 1 -6 -3 -9 62.79 7.6 -2 6 3 -9 62.79 7.6 1 -6 -3 -9 79.69 8.3 -2 6 3 -9 79.69 8.3 1 -6 -3 -9 76.99 8.6 -2 6 3 -9 76.99 8.6 1 -6 -3 -9 68.09 6.1 -2 6 3 -9 68.09 6.1 1 -5 3 -9 23.1 4.5 -2 5 -3 -9 23.1 4.5 1 -5 3 -9 29.7 4.8 -2 5 -3 -9 29.7 4.8 1 -5 -3 -9 27.2 4.8 -2 5 3 -9 27.2 4.8 1 -5 -3 -9 20.6 3 -2 5 3 -9 20.6 3 1 -5 -3 -9 27.1 4 -2 5 3 -9 27.1 4 1 -4 3 -9 76.69 7 -2 4 -3 -9 76.69 7 1 4 3 9 69.09 6.4 -2 -4 -3 9 69.09 6.4 1 -4 3 -9 66.89 6.6 -2 4 -3 -9 66.89 6.6 1 -4 -3 -9 66.29 5.9 -2 4 3 -9 66.29 5.9 1 -4 -3 -9 77.69 6.6 -2 4 3 -9 77.69 6.6 1 -4 -3 -9 69.59 6 -2 4 3 -9 69.59 6 1 4 -3 9 64.39 6.5 -2 -4 3 9 64.39 6.5 1 -4 -3 -9 78.19 7.2 -2 4 3 -9 78.19 7.2 1 3 3 9 198.38 13.7 -2 -3 -3 9 198.38 13.7 1 -3 3 -9 182.48 13.6 -2 3 -3 -9 182.48 13.6 1 3 3 9 205.38 13.4 -2 -3 -3 9 205.38 13.4 1 -3 3 -9 163.18 13.2 -2 3 -3 -9 163.18 13.2 1 -3 3 -9 196.68 14 -2 3 -3 -9 196.68 14 1 3 -3 9 170.78 13.6 -2 -3 3 9 170.78 13.6 1 3 -3 9 165.18 13.2 -2 -3 3 9 165.18 13.2 1 -3 -3 -9 157.78 13.7 -2 3 3 -9 157.78 13.7 1 -3 -3 -9 162.78 13.3 -2 3 3 -9 162.78 13.3 1 -3 -3 -9 211.48 13.7 -2 3 3 -9 211.48 13.7 1 -3 -3 -9 192.28 14 -2 3 3 -9 192.28 14 1 -3 -3 -9 204.68 13.3 -2 3 3 -9 204.68 13.3 1 2 3 9 119.09 8.2 -2 -2 -3 9 119.09 8.2 1 -2 3 -9 92.99 8.2 -2 2 -3 -9 92.99 8.2 1 -2 3 -9 102.09 8 -2 2 -3 -9 102.09 8 1 2 3 9 138.19 10.2 -2 -2 -3 9 138.19 10.2 1 -2 3 -9 110.79 8.3 -2 2 -3 -9 110.79 8.3 1 -2 3 -9 104.49 9.2 -2 2 -3 -9 104.49 9.2 1 -2 -3 -9 94.49 8 -2 2 3 -9 94.49 8 1 2 -3 9 96.29 8.6 -2 -2 3 9 96.29 8.6 1 -2 -3 -9 93.29 8.3 -2 2 3 -9 93.29 8.3 1 -2 -3 -9 120.89 8.3 -2 2 3 -9 120.89 8.3 1 2 -3 9 107.69 8.6 -2 -2 3 9 107.69 8.6 1 2 -3 9 112.39 8.1 -2 -2 3 9 112.39 8.1 1 2 -3 9 112.69 7.9 -2 -2 3 9 112.69 7.9 1 1 3 9 390.06 26.5 -2 -1 -3 9 390.06 26.5 1 -1 3 -9 381.56 26.7 -2 1 -3 -9 381.56 26.7 1 -1 3 -9 386.46 26.6 -2 1 -3 -9 386.46 26.6 1 -1 3 -9 379.16 26.5 -2 1 -3 -9 379.16 26.5 1 1 3 9 351.76 26.5 -2 -1 -3 9 351.76 26.5 1 -1 3 -9 369.76 26.5 -2 1 -3 -9 369.76 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4.2 1 -6 6 -9 101.59 11.3 -2 6 -6 -9 101.59 11.3 1 -6 -6 -9 87.69 10.1 -2 6 6 -9 87.69 10.1 1 -6 -6 -9 113.09 11.6 -2 6 6 -9 113.09 11.6 1 -6 -6 -9 94.99 11.7 -2 6 6 -9 94.99 11.7 1 6 -6 9 128.99 11.1 -2 -6 6 9 128.99 11.1 1 -5 6 -9 58.99 8.3 -2 5 -6 -9 58.99 8.3 1 -5 6 -9 77.29 7.9 -2 5 -6 -9 77.29 7.9 1 5 -6 9 76.29 8.8 -2 -5 6 9 76.29 8.8 1 -5 -6 -9 78.69 7.7 -2 5 6 -9 78.69 7.7 1 -5 -6 -9 73.49 9.2 -2 5 6 -9 73.49 9.2 1 -4 6 -9 49.2 6.1 -2 4 -6 -9 49.2 6.1 1 -4 6 -9 53.59 7.4 -2 4 -6 -9 53.59 7.4 1 -4 6 -9 43.6 6.7 -2 4 -6 -9 43.6 6.7 1 4 -6 9 49.99 5.7 -2 -4 6 9 49.99 5.7 1 4 -6 9 54.79 6.6 -2 -4 6 9 54.79 6.6 1 4 -6 9 55.29 5.8 -2 -4 6 9 55.29 5.8 1 -4 -6 -9 54.89 6 -2 4 6 -9 54.89 6 1 3 6 9 39.1 5.4 -2 -3 -6 9 39.1 5.4 1 -3 6 -9 62.09 5.7 -2 3 -6 -9 62.09 5.7 1 -3 6 -9 50.79 7.2 -2 3 -6 -9 50.79 7.2 1 -3 -6 -9 38.5 5.3 -2 3 6 -9 38.5 5.3 1 3 -6 9 39.8 5.1 -2 -3 6 9 39.8 5.1 1 3 -6 9 53.79 6 -2 -3 6 9 53.79 6 1 3 -6 9 45.9 5.3 -2 -3 6 9 45.9 5.3 1 -3 -6 -9 55.49 6.6 -2 3 6 -9 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1 -3 10 189.18 14.2 -2 -1 3 10 189.18 14.2 1 -1 -3 -10 179.98 14.3 -2 1 3 -10 179.98 14.3 1 -1 -3 -10 207.98 14.4 -2 1 3 -10 207.98 14.4 1 0 3 10 221.78 15.3 -2 0 -3 10 221.78 15.3 1 0 3 -10 210.28 15.3 -2 0 -3 -10 210.28 15.3 1 0 3 10 197.98 15.1 -2 0 -3 10 197.98 15.1 1 0 3 -10 217.98 15.1 -2 0 -3 -10 217.98 15.1 1 0 3 -10 218.28 15.5 -2 0 -3 -10 218.28 15.5 1 0 -3 -10 205.58 15.3 -2 0 3 -10 205.58 15.3 1 0 -3 10 202.58 15.7 -2 0 3 10 202.58 15.7 1 0 -3 10 213.38 15.3 -2 0 3 10 213.38 15.3 1 0 -3 -10 233.38 15.4 -2 0 3 -10 233.38 15.4 1 0 -3 10 202.58 15.3 -2 0 3 10 202.58 15.3 1 0 -3 10 204.78 15.1 -2 0 3 10 204.78 15.1 1 0 -3 -10 221.48 15.4 -2 0 3 -10 221.48 15.4 1 0 -3 10 216.58 15.3 -2 0 3 10 216.58 15.3 1 -1 3 10 176.18 13.7 -2 1 -3 10 176.18 13.7 1 1 3 -10 193.58 13.5 -2 -1 -3 -10 193.58 13.5 1 1 3 -10 188.98 13.8 -2 -1 -3 -10 188.98 13.8 1 1 3 -10 185.08 13.7 -2 -1 -3 -10 185.08 13.7 1 1 3 -10 185.48 14 -2 -1 -3 -10 185.48 14 1 -1 3 10 195.68 13.8 -2 1 -3 10 195.68 13.8 1 1 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258.37 17.2 -2 -2 3 -10 258.37 17.2 1 2 -3 -10 230.28 16.8 -2 -2 3 -10 230.28 16.8 1 3 3 -10 325.97 21.2 -2 -3 -3 -10 325.97 21.2 1 -3 3 10 313.17 21.4 -2 3 -3 10 313.17 21.4 1 -3 -3 10 305.77 21.3 -2 3 3 10 305.77 21.3 1 -3 -3 10 291.47 21.1 -2 3 3 10 291.47 21.1 1 -3 -3 10 272.97 20.9 -2 3 3 10 272.97 20.9 1 3 -3 -10 274.67 21 -2 -3 3 -10 274.67 21 1 -3 -3 10 310.37 21.5 -2 3 3 10 310.37 21.5 1 -4 3 10 87.79 8.3 -2 4 -3 10 87.79 8.3 1 -4 3 10 87.49 7.3 -2 4 -3 10 87.49 7.3 1 4 3 -10 79.79 6.7 -2 -4 -3 -10 79.79 6.7 1 -4 -3 10 87.69 6.6 -2 4 3 10 87.69 6.6 1 -4 -3 10 81.99 7.1 -2 4 3 10 81.99 7.1 1 -4 -3 10 69.99 6.5 -2 4 3 10 69.99 6.5 1 -4 -3 10 80.19 7.4 -2 4 3 10 80.19 7.4 1 -5 3 10 45.5 5.6 -2 5 -3 10 45.5 5.6 1 -5 3 10 53.89 7.2 -2 5 -3 10 53.89 7.2 1 -5 -3 10 46 5.8 -2 5 3 10 46 5.8 1 -5 -3 10 44.9 4.9 -2 5 3 10 44.9 4.9 1 -5 -3 10 33.3 4.5 -2 5 3 10 33.3 4.5 1 -5 -3 10 37.7 5.3 -2 5 3 10 37.7 5.3 1 -6 3 10 1 5.6 -2 6 -3 10 1 5.6 1 -6 3 10 11 4.2 -2 6 -3 10 11 4.2 1 -6 -3 10 13.5 3.9 -2 6 3 10 13.5 3.9 1 -6 -3 10 8.4 3.2 -2 6 3 10 8.4 3.2 1 -6 -3 10 8.7 4.3 -2 6 3 10 8.7 4.3 1 -7 3 10 35.7 5.8 -2 7 -3 10 35.7 5.8 1 -7 -3 10 26.8 6 -2 7 3 10 26.8 6 1 -7 -3 10 25.9 6.1 -2 7 3 10 25.9 6.1 1 -7 -3 10 34.5 5.8 -2 7 3 10 34.5 5.8 1 -8 3 10 10.9 8.7 -2 8 -3 10 10.9 8.7 1 -8 3 10 1.4 5.1 -2 8 -3 10 1.4 5.1 1 -8 -3 10 0.1 5.9 -2 8 3 10 0.1 5.9 1 -8 -3 10 2.2 7.9 -2 8 3 10 2.2 7.9 1 -8 -3 10 6.3 5.3 -2 8 3 10 6.3 5.3 1 -8 4 -10 58.89 9.1 -2 8 -4 -10 58.89 9.1 1 -8 4 -10 44.8 8.2 -2 8 -4 -10 44.8 8.2 1 -8 -4 -10 26.7 7.6 -2 8 4 -10 26.7 7.6 1 -8 -4 -10 35.7 7.6 -2 8 4 -10 35.7 7.6 1 -7 4 -10 26.4 6.9 -2 7 -4 -10 26.4 6.9 1 -7 4 -10 30 6.8 -2 7 -4 -10 30 6.8 1 -7 -4 -10 21.4 6.9 -2 7 4 -10 21.4 6.9 1 -7 -4 -10 18.4 5.8 -2 7 4 -10 18.4 5.8 1 -6 4 -10 26.6 5.6 -2 6 -4 -10 26.6 5.6 1 -6 -4 -10 13.4 4 -2 6 4 -10 13.4 4 1 -6 -4 -10 24.7 5.9 -2 6 4 -10 24.7 5.9 1 -6 -4 -10 17.3 4.9 -2 6 4 -10 17.3 4.9 1 -5 4 -10 39.5 5.9 -2 5 -4 -10 39.5 5.9 1 -5 -4 -10 34.9 4.9 -2 5 4 -10 34.9 4.9 1 5 -4 10 34.5 5.3 -2 -5 4 10 34.5 5.3 1 -5 -4 -10 45.1 5.3 -2 5 4 -10 45.1 5.3 1 -5 -4 -10 33.8 5.8 -2 5 4 -10 33.8 5.8 1 -5 -4 -10 58.99 6.4 -2 5 4 -10 58.99 6.4 1 -4 4 -10 177.58 13.4 -2 4 -4 -10 177.58 13.4 1 -4 4 -10 163.58 12.3 -2 4 -4 -10 163.58 12.3 1 -4 4 -10 175.68 13 -2 4 -4 -10 175.68 13 1 -4 -4 -10 160.98 12.7 -2 4 4 -10 160.98 12.7 1 4 -4 10 174.28 12.9 -2 -4 4 10 174.28 12.9 1 -4 -4 -10 142.49 12.5 -2 4 4 -10 142.49 12.5 1 -4 -4 -10 165.08 13.4 -2 4 4 -10 165.08 13.4 1 -3 4 -10 87.69 7.5 -2 3 -4 -10 87.69 7.5 1 -3 4 -10 104.99 8.1 -2 3 -4 -10 104.99 8.1 1 3 4 10 92.39 8.1 -2 -3 -4 10 92.39 8.1 1 3 -4 10 85.09 7.6 -2 -3 4 10 85.09 7.6 1 3 -4 10 72.79 6.8 -2 -3 4 10 72.79 6.8 1 -3 -4 -10 84.89 7.3 -2 3 4 -10 84.89 7.3 1 -3 -4 -10 96.49 7.5 -2 3 4 -10 96.49 7.5 1 -3 -4 -10 100.69 8.2 -2 3 4 -10 100.69 8.2 1 3 -4 10 79.19 7 -2 -3 4 10 79.19 7 1 2 4 10 247.38 16.7 -2 -2 -4 10 247.38 16.7 1 -2 4 -10 219.78 16.5 -2 2 -4 -10 219.78 16.5 1 2 4 10 210.88 16.6 -2 -2 -4 10 210.88 16.6 1 -2 4 -10 234.88 16.9 -2 2 -4 -10 234.88 16.9 1 -2 4 -10 224.18 16.6 -2 2 -4 -10 224.18 16.6 1 -2 -4 -10 229.98 16.6 -2 2 4 -10 229.98 16.6 1 -2 -4 -10 236.38 16.9 -2 2 4 -10 236.38 16.9 1 2 -4 10 243.18 16.4 -2 -2 4 10 243.18 16.4 1 2 -4 10 238.28 16.5 -2 -2 4 10 238.28 16.5 1 2 -4 10 231.28 16.7 -2 -2 4 10 231.28 16.7 1 -2 -4 -10 202.88 16.5 -2 2 4 -10 202.88 16.5 1 -1 4 -10 17.4 3.3 -2 1 -4 -10 17.4 3.3 1 -1 4 -10 17.4 2.8 -2 1 -4 -10 17.4 2.8 1 -1 4 -10 14.9 2.4 -2 1 -4 -10 14.9 2.4 1 1 4 10 9.9 2.5 -2 -1 -4 10 9.9 2.5 1 1 4 10 9.3 2.9 -2 -1 -4 10 9.3 2.9 1 1 -4 10 13.2 2.4 -2 -1 4 10 13.2 2.4 1 1 -4 10 16.8 2.8 -2 -1 4 10 16.8 2.8 1 -1 -4 -10 13.2 2.6 -2 1 4 -10 13.2 2.6 1 1 -4 10 23.9 3.1 -2 -1 4 10 23.9 3.1 1 -1 -4 -10 16.7 2.8 -2 1 4 -10 16.7 2.8 1 1 -4 10 13.4 2.5 -2 -1 4 10 13.4 2.5 1 -1 -4 -10 11 3.1 -2 1 4 -10 11 3.1 1 1 -4 10 10 3 -2 -1 4 10 10 3 1 0 4 -10 754.72 55.69 -2 0 -4 -10 754.72 55.69 1 0 4 10 856.61 56.19 -2 0 -4 10 856.61 56.19 1 0 4 10 771.52 55.49 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8.4 2.5 -2 0 3 14 8.4 2.5 1 0 -3 -14 9.4 2.9 -2 0 3 -14 9.4 2.9 1 0 -3 14 11.8 2.8 -2 0 3 14 11.8 2.8 1 0 -3 14 13.6 2.8 -2 0 3 14 13.6 2.8 1 0 -3 -14 13.5 3.4 -2 0 3 -14 13.5 3.4 1 -1 3 14 91.99 7.3 -2 1 -3 14 91.99 7.3 1 -1 3 14 78.19 7.1 -2 1 -3 14 78.19 7.1 1 1 3 -14 85.29 7.2 -2 -1 -3 -14 85.29 7.2 1 1 3 -14 93.99 7.7 -2 -1 -3 -14 93.99 7.7 1 -1 3 14 89.39 7.3 -2 1 -3 14 89.39 7.3 1 1 3 -14 81.59 6.9 -2 -1 -3 -14 81.59 6.9 1 1 -3 -14 89.49 7.5 -2 -1 3 -14 89.49 7.5 1 -1 -3 14 87.29 7.3 -2 1 3 14 87.29 7.3 1 1 -3 -14 93.19 7.3 -2 -1 3 -14 93.19 7.3 1 -1 -3 14 76.79 6.9 -2 1 3 14 76.79 6.9 1 -1 -3 14 99.19 7.4 -2 1 3 14 99.19 7.4 1 -1 -3 14 93.09 7.2 -2 1 3 14 93.09 7.2 1 -2 3 14 231.08 16.4 -2 2 -3 14 231.08 16.4 1 2 3 -14 224.68 16.7 -2 -2 -3 -14 224.68 16.7 1 2 3 -14 235.88 16.1 -2 -2 -3 -14 235.88 16.1 1 2 3 -14 207.58 16.4 -2 -2 -3 -14 207.58 16.4 1 -2 3 14 229.08 16.3 -2 2 -3 14 229.08 16.3 1 -2 -3 14 200.38 15.9 -2 2 3 14 200.38 15.9 1 -2 -3 14 220.78 16.1 -2 2 3 14 220.78 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3.8 1 1 4 14 38.7 4.2 -2 -1 -4 14 38.7 4.2 1 -1 4 -14 33.6 4 -2 1 -4 -14 33.6 4 1 -1 4 -14 38.5 4.7 -2 1 -4 -14 38.5 4.7 1 1 -4 14 32.9 3.9 -2 -1 4 14 32.9 3.9 1 1 -4 14 32.5 4.1 -2 -1 4 14 32.5 4.1 1 -1 -4 -14 33.9 4.7 -2 1 4 -14 33.9 4.7 1 1 -4 14 34.7 4.3 -2 -1 4 14 34.7 4.3 1 1 -4 14 35.5 4.6 -2 -1 4 14 35.5 4.6 1 -1 -4 -14 38.1 4.4 -2 1 4 -14 38.1 4.4 1 0 4 14 173.48 12.2 -2 0 -4 14 173.48 12.2 1 0 4 -14 169.88 11.8 -2 0 -4 -14 169.88 11.8 1 0 4 -14 157.18 12.4 -2 0 -4 -14 157.18 12.4 1 0 4 14 138.89 11.8 -2 0 -4 14 138.89 11.8 1 0 -4 14 147.29 11.9 -2 0 4 14 147.29 11.9 1 0 -4 14 176.48 12.2 -2 0 4 14 176.48 12.2 1 0 -4 14 160.58 12.3 -2 0 4 14 160.58 12.3 1 0 -4 -14 169.98 12.4 -2 0 4 -14 169.98 12.4 1 0 -4 14 166.48 12.2 -2 0 4 14 166.48 12.2 1 0 -4 -14 159.48 12.2 -2 0 4 -14 159.48 12.2 1 1 4 -14 33 4.5 -2 -1 -4 -14 33 4.5 1 1 4 -14 32.3 3.6 -2 -1 -4 -14 32.3 3.6 1 -1 4 14 39.8 4.3 -2 1 -4 14 39.8 4.3 1 -1 4 14 25.2 4 -2 1 -4 14 25.2 4 1 -1 -4 14 35.3 4.3 -2 1 4 14 35.3 4.3 1 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21 5.6 1 -5 -5 -14 21.4 5 -2 5 5 -14 21.4 5 1 5 -5 14 18.7 4.2 -2 -5 5 14 18.7 4.2 1 5 -5 14 23 5.4 -2 -5 5 14 23 5.4 1 -5 -5 -14 21.9 6.1 -2 5 5 -14 21.9 6.1 1 -4 5 -14 49 6.9 -2 4 -5 -14 49 6.9 1 -4 5 -14 63.99 7.9 -2 4 -5 -14 63.99 7.9 1 4 -5 14 42.3 5.6 -2 -4 5 14 42.3 5.6 1 4 -5 14 53.69 6.6 -2 -4 5 14 53.69 6.6 1 -4 -5 -14 47.8 7.1 -2 4 5 -14 47.8 7.1 1 -4 -5 -14 55.39 6.8 -2 4 5 -14 55.39 6.8 1 -3 5 -14 180.08 13.5 -2 3 -5 -14 180.08 13.5 1 -3 5 -14 157.58 12.4 -2 3 -5 -14 157.58 12.4 1 3 -5 14 170.08 12.2 -2 -3 5 14 170.08 12.2 1 -3 -5 -14 145.39 13.2 -2 3 5 -14 145.39 13.2 1 -3 -5 -14 151.28 12.5 -2 3 5 -14 151.28 12.5 1 3 -5 14 148.19 12.6 -2 -3 5 14 148.19 12.6 1 3 -5 14 154.48 12.2 -2 -3 5 14 154.48 12.2 1 2 5 14 114.19 9.4 -2 -2 -5 14 114.19 9.4 1 -2 5 -14 112.39 9.1 -2 2 -5 -14 112.39 9.1 1 -2 5 -14 110.09 9.8 -2 2 -5 -14 110.09 9.8 1 2 -5 14 119.29 9.7 -2 -2 5 14 119.29 9.7 1 -2 -5 -14 104.69 10 -2 2 5 -14 104.69 10 1 -2 -5 -14 106.89 9.3 -2 2 5 -14 106.89 9.3 1 2 -5 14 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-2 0 31 19.5 6.4 1 1 0 31 73.39 9.4 -2 -1 0 31 73.39 9.4 1 -1 0 -31 82.19 9.5 -2 1 0 -31 82.19 9.5 1 -1 0 -31 96.39 10.1 -2 1 0 -31 96.39 10.1 1 1 0 31 77.49 8.5 -2 -1 0 31 77.49 8.5 1 0 0 31 25.9 6.2 -2 0 0 31 25.9 6.2 1 0 0 31 21.9 5.3 -2 0 0 31 21.9 5.3 1 -1 0 31 100.09 10.3 -2 1 0 31 100.09 10.3 1 -1 0 31 87.69 9.7 -2 1 0 31 87.69 9.7 1 -2 0 31 13.1 6.3 -2 2 0 31 13.1 6.3 1 -2 0 31 23.1 7.3 -2 2 0 31 23.1 7.3 1 -3 0 31 14 7.4 -2 3 0 31 14 7.4 1 -3 0 31 22.3 6.8 -2 3 0 31 22.3 6.8 1 -3 1 -31 3.4 5.5 -2 3 -1 -31 3.4 5.5 1 -3 -1 -31 -2.3 6.8 -2 3 1 -31 -2.3 6.8 1 2 1 31 4.2 4.4 -2 -2 -1 31 4.2 4.4 1 -2 1 -31 13.1 6.1 -2 2 -1 -31 13.1 6.1 1 2 1 31 2.2 5.8 -2 -2 -1 31 2.2 5.8 1 -2 1 -31 18.1 5.5 -2 2 -1 -31 18.1 5.5 1 2 -1 31 3.6 4.8 -2 -2 1 31 3.6 4.8 1 2 -1 31 14.3 6.2 -2 -2 1 31 14.3 6.2 1 -2 -1 -31 3.4 4.9 -2 2 1 -31 3.4 4.9 1 -2 -1 -31 12.4 6 -2 2 1 -31 12.4 6 1 -1 1 -31 11.5 6.8 -2 1 -1 -31 11.5 6.8 1 1 1 31 18.5 5 -2 -1 -1 31 18.5 5 1 1 1 31 19.7 6.1 -2 -1 -1 31 19.7 6.1 1 1 -1 31 15.9 4.9 -2 -1 1 31 15.9 4.9 1 -1 -1 -31 14.4 6 -2 1 1 -31 14.4 6 1 1 -1 31 12.6 6.1 -2 -1 1 31 12.6 6.1 1 -1 -1 -31 8.6 4.9 -2 1 1 -31 8.6 4.9 1 0 1 -31 2.1 4.4 -2 0 -1 -31 2.1 4.4 1 0 1 -31 -5.3 5.2 -2 0 -1 -31 -5.3 5.2 1 0 1 31 1.6 5.3 -2 0 -1 31 1.6 5.3 1 0 1 31 0.7 4.4 -2 0 -1 31 0.7 4.4 1 0 -1 -31 -0.2 4.3 -2 0 1 -31 -0.2 4.3 1 0 -1 31 -0.3 4.6 -2 0 1 31 -0.3 4.6 1 0 -1 31 -3.7 5.4 -2 0 1 31 -3.7 5.4 1 -1 1 31 19.8 5.5 -2 1 -1 31 19.8 5.5 1 -1 1 31 20.1 6 -2 1 -1 31 20.1 6 1 1 1 -31 11.1 5.1 -2 -1 -1 -31 11.1 5.1 1 -1 -1 31 17.5 6 -2 1 1 31 17.5 6 1 -1 -1 31 14.6 6.2 -2 1 1 31 14.6 6.2 1 1 -1 -31 10.2 5.4 -2 -1 1 -31 10.2 5.4 1 2 1 -31 5.3 5.3 -2 -2 -1 -31 5.3 5.3 1 -2 1 31 7.7 6.1 -2 2 -1 31 7.7 6.1 1 -2 1 31 12.7 5.7 -2 2 -1 31 12.7 5.7 1 2 -1 -31 11 5.6 -2 -2 1 -31 11 5.6 1 -2 -1 31 14.5 6.7 -2 2 1 31 14.5 6.7 1 -2 -1 31 15.6 7 -2 2 1 31 15.6 7 1 2 2 31 16.7 5.2 -2 -2 -2 31 16.7 5.2 1 -2 2 -31 22.9 6.6 -2 2 -2 -31 22.9 6.6 1 2 2 31 23.4 6.5 -2 -2 -2 31 23.4 6.5 1 -2 2 -31 19.3 6.1 -2 2 -2 -31 19.3 6.1 1 2 -2 31 20.8 5.1 -2 -2 2 31 20.8 5.1 1 2 -2 31 20.8 6.6 -2 -2 2 31 20.8 6.6 1 -2 -2 -31 15.4 5.6 -2 2 2 -31 15.4 5.6 1 -2 -2 -31 19.5 6.3 -2 2 2 -31 19.5 6.3 1 -1 2 -31 26.4 6.4 -2 1 -2 -31 26.4 6.4 1 1 2 31 16.4 5.1 -2 -1 -2 31 16.4 5.1 1 1 2 31 30.4 6.6 -2 -1 -2 31 30.4 6.6 1 1 -2 31 12.5 6.7 -2 -1 2 31 12.5 6.7 1 -1 -2 -31 9.2 5.1 -2 1 2 -31 9.2 5.1 1 1 -2 31 22.7 5.8 -2 -1 2 31 22.7 5.8 1 0 2 31 65.69 8.5 -2 0 -2 31 65.69 8.5 1 0 2 -31 72.79 8.2 -2 0 -2 -31 72.79 8.2 1 0 2 31 65.79 7.7 -2 0 -2 31 65.79 7.7 1 0 2 -31 53.09 8.2 -2 0 -2 -31 53.09 8.2 1 0 -2 -31 50.69 7.6 -2 0 2 -31 50.69 7.6 1 0 -2 31 64.59 9 -2 0 2 31 64.59 9 1 0 -2 31 74.39 8.6 -2 0 2 31 74.39 8.6 1 1 2 -31 8.3 4.9 -2 -1 -2 -31 8.3 4.9 1 -1 2 31 21.3 5.8 -2 1 -2 31 21.3 5.8 1 -1 2 31 24 6.4 -2 1 -2 31 24 6.4 1 -1 -2 31 20.9 7.5 -2 1 2 31 20.9 7.5 1 -1 -2 31 17.3 6.2 -2 1 2 31 17.3 6.2 1 1 -2 -31 14.5 5.4 -2 -1 2 -31 14.5 5.4 1 -2 2 31 29.3 6.3 -2 2 -2 31 29.3 6.3 1 -2 2 31 23.6 6.8 -2 2 -2 31 23.6 6.8 1 2 2 -31 17.7 5.6 -2 -2 -2 -31 17.7 5.6 1 2 -2 -31 40.7 8.3 -2 -2 2 -31 40.7 8.3 1 -2 -2 31 15.5 6.5 -2 2 2 31 15.5 6.5 1 -2 -2 31 22.2 7 -2 2 2 31 22.2 7 1 2 -2 -31 13.2 5.9 -2 -2 2 -31 13.2 5.9 1 -2 3 -31 3.4 6.2 -2 2 -3 -31 3.4 6.2 1 -1 3 -31 -1.5 4.3 -2 1 -3 -31 -1.5 4.3 1 -1 3 -31 5.3 5.6 -2 1 -3 -31 5.3 5.6 1 1 3 31 7.5 5.9 -2 -1 -3 31 7.5 5.9 1 1 3 31 1.6 4.8 -2 -1 -3 31 1.6 4.8 1 1 -3 31 -1.1 4.4 -2 -1 3 31 -1.1 4.4 1 -1 -3 -31 7.4 5.2 -2 1 3 -31 7.4 5.2 1 1 -3 31 -2.3 6.5 -2 -1 3 31 -2.3 6.5 1 0 3 31 2.8 5.7 -2 0 -3 31 2.8 5.7 1 0 3 -31 -1.9 5.1 -2 0 -3 -31 -1.9 5.1 1 0 3 31 4.2 4.9 -2 0 -3 31 4.2 4.9 1 0 3 -31 3.7 4.6 -2 0 -3 -31 3.7 4.6 1 0 -3 -31 -5.7 4.6 -2 0 3 -31 -5.7 4.6 1 0 -3 31 5.7 5.3 -2 0 3 31 5.7 5.3 1 0 -3 -31 11.3 6.5 -2 0 3 -31 11.3 6.5 1 0 -3 31 1.2 7.1 -2 0 3 31 1.2 7.1 1 -1 3 31 -2.9 5.6 -2 1 -3 31 -2.9 5.6 1 -1 3 31 -0.2 5.5 -2 1 -3 31 -0.2 5.5 1 1 3 -31 8.4 5.6 -2 -1 -3 -31 8.4 5.6 1 1 3 -31 0.5 4.5 -2 -1 -3 -31 0.5 4.5 1 -1 -3 31 6.7 7 -2 1 3 31 6.7 7 1 -1 -3 31 3.3 5.3 -2 1 3 31 3.3 5.3 1 1 -3 -31 -2.4 4.8 -2 -1 3 -31 -2.4 4.8 1 1 -3 -31 5.9 6.1 -2 -1 3 -31 5.9 6.1 1 -2 0 -32 1.1 5.1 -2 2 0 -32 1.1 5.1 1 -1 0 -32 -6 4.1 -2 1 0 -32 -6 4.1 1 1 0 32 6.9 5.7 -2 -1 0 32 6.9 5.7 1 -1 0 -32 3 5.4 -2 1 0 -32 3 5.4 1 1 0 32 0.5 4.3 -2 -1 0 32 0.5 4.3 1 0 0 -32 9.6 5.1 -2 0 0 -32 9.6 5.1 1 0 0 32 18 5.2 -2 0 0 32 18 5.2 1 0 0 32 14.9 6.1 -2 0 0 32 14.9 6.1 1 -1 0 32 -2.7 5.8 -2 1 0 32 -2.7 5.8 1 -1 0 32 5.5 5.2 -2 1 0 32 5.5 5.2 1 1 0 -32 2.6 4.8 -2 -1 0 -32 2.6 4.8 1 1 1 32 9.7 4.8 -2 -1 -1 32 9.7 4.8 1 -1 1 -32 6.3 5.7 -2 1 -1 -32 6.3 5.7 1 1 1 32 6.5 5.9 -2 -1 -1 32 6.5 5.9 1 -1 1 -32 7 5 -2 1 -1 -32 7 5 1 1 -1 32 5.4 5.1 -2 -1 1 32 5.4 5.1 1 1 -1 32 1.7 5.8 -2 -1 1 32 1.7 5.8 1 -1 -1 -32 7 4.9 -2 1 1 -32 7 4.9 1 0 1 32 32.7 6.1 -2 0 -1 32 32.7 6.1 1 0 1 -32 35.1 6.5 -2 0 -1 -32 35.1 6.5 1 0 1 32 48.8 7.6 -2 0 -1 32 48.8 7.6 1 0 1 -32 31.9 7.2 -2 0 -1 -32 31.9 7.2 1 0 -1 32 44.8 7.7 -2 0 1 32 44.8 7.7 1 0 -1 32 38.8 6.6 -2 0 1 32 38.8 6.6 1 0 -1 -32 30.1 6.2 -2 0 1 -32 30.1 6.2 1 1 1 -32 6.3 5.9 -2 -1 -1 -32 6.3 5.9 1 -1 1 32 8.1 5.9 -2 1 -1 32 8.1 5.9 1 -1 -1 32 -1.3 5.2 -2 1 1 32 -1.3 5.2 1 1 -1 -32 8.5 5.1 -2 -1 1 -32 8.5 5.1 1 -1 -1 32 4.7 6.2 -2 1 1 32 4.7 6.2 1 -1 2 -32 12.2 5.4 -2 1 -2 -32 12.2 5.4 1 -1 2 -32 21.7 6.5 -2 1 -2 -32 21.7 6.5 1 1 2 32 18 5.3 -2 -1 -2 32 18 5.3 1 1 -2 32 14 5.2 -2 -1 2 32 14 5.2 1 1 -2 32 12.5 7.5 -2 -1 2 32 12.5 7.5 1 0 2 32 37 6.4 -2 0 -2 32 37 6.4 1 0 2 32 37.5 8 -2 0 -2 32 37.5 8 1 0 2 -32 35.3 7.2 -2 0 -2 -32 35.3 7.2 1 0 -2 32 39.2 6.9 -2 0 2 32 39.2 6.9 1 0 -2 32 51.59 8.2 -2 0 2 32 51.59 8.2 1 0 -2 -32 38.7 6.9 -2 0 2 -32 38.7 6.9 1 -1 2 32 13 6.6 -2 1 -2 32 13 6.6 1 -1 2 32 12.7 5.8 -2 1 -2 32 12.7 5.8 1 1 2 -32 20.7 6.9 -2 -1 -2 -32 20.7 6.9 1 1 -2 -32 10.7 5.7 -2 -1 2 -32 10.7 5.7 1 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 S1 C3 91.6(2) . . ? C11 S2 C10 89.5(3) . . ? C2 O2 C4 110.5(4) . . ? C10 O5 C12 114.5(4) . . ? C16 C15 F2 119.8(5) . . ? C14 C15 F2 119.1(5) . . ? C14 C15 C16 120.9(5) . . ? N3 C6 N2 117.6(5) . . ? C7 C6 N2 122.0(5) . . ? C7 C6 N3 120.5(6) . . ? C4 N1 C5 119.2(4) . . ? C8 N1 C5 122.3(5) . . ? C8 N1 C4 118.5(5) . . ? N4 C12 O5 107.2(5) . . ? C11 C12 O5 108.5(4) . . ? C11 C12 N4 112.7(5) . . ? C5 N2 C6 119.3(5) . . ? N1 C5 O3 121.5(5) . . ? N2 C5 O3 120.7(5) . . ? N2 C5 N1 117.8(5) . . ? C23 C24 N8 126.4(6) . . ? C19 C22 C23 119.8(5) . . ? C26 C22 C23 118.3(6) . . ? C26 C22 C19 121.9(6) . . ? N4 C16 C15 118.5(5) . . ? C16 N4 C12 118.5(4) . . ? C13 N4 C12 122.2(4) . . ? C13 N4 C16 119.3(4) . . ? C14 N5 C13 120.8(5) . . ? N7 C21 C20 121.1(6) . . ? C30 C29 C28 120.0 . . ? C34 C29 C28 117.6 . . ? C34 C29 C30 122.4 . . ? C27 C28 C29 120.0 . . ? N10 C27 C28 120.0 . . ? C31 N10 C27 120.0 . . ? C30 C31 N10 120.0 . . ? C31 C30 C29 120.0 . . ? C19 C20 C21 123.5(6) . . ? N4 C13 O6 118.5(4) . . ? N5 C13 O6 121.0(5) . . ? N5 C13 N4 120.5(4) . . ? C36 N9 C32 117.6(6) . . ? C34 C35 C36 118.7(6) . . ? C17 C18 C19 120.9(6) . . ? C17 N7 C21 117.7(6) . . ? C25 N8 C24 114.8(6) . . ? N5 C14 C15 119.8(5) . . ? N6 C14 C15 119.5(5) . . ? N6 C14 N5 120.6(5) . . ? O5 C10 S2 107.6(4) . . ? C9 C10 S2 115.6(4) . . ? C9 C10 O5 109.4(5) . . ? C34 C33 C32 122.1(7) . . ? N1 C4 O2 105.7(4) . . ? C3 C4 O2 106.6(4) . . ? C3 C4 N1 112.6(5) . . ? C6 C7 F1 119.9(5) . . ? C8 C7 F1 120.2(5) . . ? C8 C7 C6 119.8(5) . . ? C33 C32 N9 122.3(6) . . ? C4 C3 S1 102.0(4) . . ? C22 C23 C24 116.0(6) . . ? C26 C25 N8 124.6(7) . . ? C7 C8 N1 118.3(5) . . ? O2 C2 S1 105.9(4) . . ? C1 C2 S1 113.2(4) . . ? C1 C2 O2 110.0(5) . . ? C12 C11 S2 103.8(4) . . ? C20 C19 C22 123.6(5) . . ? C18 C19 C22 121.5(5) . . ? C18 C19 C20 114.9(6) . . ? C25 C26 C22 119.9(6) . . ? C35 C36 N9 122.9(7) . . ? N7 C17 C18 121.9(6) . . ? C35 C34 C29 119.7(5) . . ? C33 C34 C29 124.0(6) . . ? C33 C34 C35 115.8(6) . . ? C10 C9 O4 109.3(5) . . ? C2 C1 O1 116.3(5) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S1 C3 1.801(6) . ? S1 C2 1.866(6) . ? S2 C10 1.823(7) . ? S2 C11 1.804(6) . ? F2 C15 1.355(6) . ? F1 C7 1.368(6) . ? O6 C13 1.250(6) . ? O3 C5 1.238(7) . ? O2 C4 1.417(6) . ? O2 C2 1.407(7) . ? O5 C12 1.406(7) . ? O5 C10 1.432(7) . ? C15 C16 1.344(8) . ? C15 C14 1.422(8) . ? C6 N2 1.342(8) . ? C6 N3 1.338(8) . ? C6 C7 1.399(8) . ? N1 C5 1.407(7) . ? N1 C4 1.485(6) . ? N1 C8 1.367(7) . ? C12 N4 1.468(7) . ? C12 C11 1.500(7) . ? N2 C5 1.363(7) . ? C24 N8 1.349(9) . ? C24 C23 1.395(9) . ? C22 C23 1.412(8) . ? C22 C19 1.487(8) . ? C22 C26 1.374(8) . ? C16 N4 1.392(7) . ? O4 C9 1.459(8) . ? N4 C13 1.392(7) . ? N5 C13 1.358(6) . ? N5 C14 1.314(7) . ? C21 C20 1.359(8) . ? C21 N7 1.335(9) . ? C29 C28 1.3900 . ? C29 C30 1.3900 . ? C29 C34 1.495(6) . ? C28 C27 1.3900 . ? C27 N10 1.3900 . ? N10 C31 1.3900 . ? C31 C30 1.3900 . ? C20 C19 1.377(8) . ? N9 C32 1.339(9) . ? N9 C36 1.331(8) . ? C35 C36 1.409(9) . ? C35 C34 1.422(9) . ? C18 C19 1.372(8) . ? C18 C17 1.391(8) . ? N7 C17 1.351(8) . ? O1 C1 1.408(7) . ? N8 C25 1.325(8) . ? C14 N6 1.352(6) . ? C10 C9 1.513(8) . ? C33 C32 1.381(9) . ? C33 C34 1.356(8) . ? C4 C3 1.510(8) . ? C7 C8 1.333(7) . ? C25 C26 1.382(9) . ? C2 C1 1.502(8) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag S1 C3 C4 O2 -46.7(4) . . . . ? S1 C3 C4 N1 -162.1(3) . . . . ? S1 C2 O2 C4 -29.1(5) . . . . ? S1 C2 C1 O1 -53.7(4) . . . . ? S2 C10 O5 C12 1.3(5) . . . . ? S2 C10 C9 O4 -57.4(4) . . . . ? S2 C11 C12 O5 -40.7(4) . . . . ? S2 C11 C12 N4 -159.2(3) . . . . ? F2 C15 C16 N4 -177.0(5) . . . . ? F2 C15 C14 N5 174.8(5) . . . . ? F2 C15 C14 N6 -8.8(6) . . . . ? F1 C7 C6 N2 174.1(5) . . . . ? F1 C7 C6 N3 -5.1(6) . . . . ? F1 C7 C8 N1 -178.4(5) . . . . ? O6 C13 N4 C12 -7.9(7) . . . . ? O6 C13 N4 C16 172.8(6) . . . . ? O6 C13 N5 C14 -174.9(5) . . . . ? O3 C5 N1 C4 -7.1(7) . . . . ? O3 C5 N1 C8 175.8(5) . . . . ? O3 C5 N2 C6 180.0(5) . . . . ? O2 C4 N1 C5 127.0(4) . . . . ? O2 C4 N1 C8 -55.8(5) . . . . ? O2 C2 C1 O1 64.5(5) . . . . ? O5 C12 N4 C16 -58.9(5) . . . . ? O5 C12 N4 C13 121.8(4) . . . . ? O5 C10 C9 O4 64.3(5) . . . . ? C15 C16 N4 C12 -174.9(6) . . . . ? C15 C16 N4 C13 4.4(7) . . . . ? C15 C14 N5 C13 -0.1(7) . . . . ? C6 N2 C5 N1 2.0(6) . . . . ? C6 C7 C8 N1 3.1(6) . . . . ? C12 N4 C13 N5 173.2(5) . . . . ? C24 N8 C25 C26 -0.7(8) . . . . ? C24 C23 C22 C19 179.5(5) . . . . ? C24 C23 C22 C26 -2.0(7) . . . . ? C22 C19 C20 C21 -179.6(7) . . . . ? C22 C19 C18 C17 -179.3(7) . . . . ? C22 C26 C25 N8 -0.9(8) . . . . ? C16 N4 C13 N5 -6.1(6) . . . . ? N4 C13 N5 C14 3.9(7) . . . . ? C21 C20 C19 C18 -0.0(8) . . . . ? C21 N7 C17 C18 -0.1(8) . . . . ? C29 C28 C27 N10 0.0(3) . . . . ? C29 C30 C31 N10 -0.0(4) . . . . ? C29 C34 C35 C36 179.8(5) . . . . ? C29 C34 C33 C32 -179.8(6) . . . . ? C28 C27 N10 C31 -0.0(4) . . . . ? C27 N10 C31 C30 0.0(3) . . . . ? C20 C19 C18 C17 1.1(7) . . . . ? N9 C32 C33 C34 4.6(8) . . . . ? N9 C36 C35 C34 -4.1(8) . . . . ? C35 C34 C33 C32 -7.8(7) . . . . ? loop_ _restr_U_rigid_atom_site_label_1 _restr_U_rigid_atom_site_label_2 _restr_U_rigid_target_weight_param _restr_U_rigid_U_parallel _restr_U_rigid_diff C29 C28 0.0100 0.0409 -0.0288 C29 C27 0.0100 0.0491 0.0020 C29 C31 0.0100 0.0510 0.0107 C29 C30 0.0100 0.0298 0.0061 C28 C27 0.0100 0.0513 -0.0047 C28 N10 0.0100 0.0403 -0.0042 C28 C30 0.0100 0.0392 0.0107 C27 N10 0.0100 0.0414 -0.0038 C27 C31 0.0100 0.0422 -0.0166 N10 C31 0.0100 0.0567 -0.0100 N10 C30 0.0100 0.0555 -0.0095 C31 C30 0.0100 0.0550 0.0038 loop_ _restr_U_similar_atom_site_label_1 _restr_U_similar_atom_site_label_2 _restr_U_similar_weight_param C29 C28 0.0400 C29 C30 0.0400 C28 C27 0.0400 C27 N10 0.0400 N10 C31 0.0400 C31 C30 0.0400 loop_ _twin_individual_id _twin_individual_mass_fraction_refined 1 0.5000(16) 2 0.5000(16)