#------------------------------------------------------------------------------ #$Date: 2020-05-07 02:26:53 +0300 (Thu, 07 May 2020) $ #$Revision: 251842 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/04/7240476.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7240476 loop_ _publ_author_name 'Mihaly, Joseph J.' 'Phillips, Alexis' 'Stewart, David J.' 'Marsh, Zachary M.' 'McCleese, Christopher' 'Haley, Joy E.' 'Zeller, Matthias' 'Grusenmeyer, Tod' 'Gray, Thomas' _publ_section_title ; Synthesis and Photophysics of Gold(I) Alkynyls Bearing a Benzothiazole-2,7-Fluorenyl Moiety: A Comparative Study Analyzing Influence of Ancillary Ligand, Bridging Moiety, and Number of Metal Centers on Photophysical Properties ; _journal_name_full 'Physical Chemistry Chemical Physics' _journal_paper_doi 10.1039/D0CP01539C _journal_year 2020 _chemical_formula_sum 'C42 H53 Au N P S' _chemical_formula_weight 831.85 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_block_doi 10.5517/ccdc.csd.cc22cdsn _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2019-05-21 deposited with the CCDC. 2020-04-30 downloaded from the CCDC. ; _cell_angle_alpha 104.775(2) _cell_angle_beta 104.891(2) _cell_angle_gamma 111.277(2) _cell_formula_units_Z 2 _cell_length_a 12.5710(8) _cell_length_b 12.7256(8) _cell_length_c 13.7715(9) _cell_measurement_reflns_used 9760 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 33.2676 _cell_measurement_theta_min 2.5688 _cell_volume 1829.6(2) _computing_cell_refinement 'SAINT V8.38A (Bruker, 2016)' _computing_data_collection 'Apex3 v2018.1-0 (Bruker, 2018)' _computing_data_reduction 'SAINT V8.38A (Bruker, 2016)' _computing_structure_refinement ; SHELXL-2018/3 (Sheldrick, 2015, 2018), SHELXLE Rev946 (H\"ubschle et al., 2011) ; _computing_structure_solution 'SHELXS-97 (Sheldrick, 2008)' _diffrn_ambient_temperature 150(2) _diffrn_detector_area_resol_mean 10.4167 _diffrn_measured_fraction_theta_full 0.995 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device_type 'Bruker AXS D8 Quest CMOS diffractometer' _diffrn_measurement_method 'omega and phi scans' _diffrn_radiation_monochromator 'Triumph curved graphite crystal' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0308 _diffrn_reflns_av_unetI/netI 0.0208 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_h_min -19 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 90033 _diffrn_reflns_point_group_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 33.295 _diffrn_reflns_theta_min 2.569 _diffrn_source 'fine focus sealed tube X-ray source' _diffrn_source_current '30 mA' _diffrn_source_voltage '50 kV' _exptl_absorpt_coefficient_mu 4.152 _exptl_absorpt_correction_T_max 0.7465 _exptl_absorpt_correction_T_min 0.5579 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D. (2015). J. Appl. Cryst. 48 3-10. ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.510 _exptl_crystal_description fragment _exptl_crystal_F_000 844 _exptl_crystal_size_max 0.510 _exptl_crystal_size_mid 0.460 _exptl_crystal_size_min 0.360 _refine_diff_density_max 4.223 _refine_diff_density_min -1.174 _refine_diff_density_rms 0.101 _refine_ls_extinction_coef 0.00333(14) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.136 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 418 _refine_ls_number_reflns 14030 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.136 _refine_ls_R_factor_all 0.0268 _refine_ls_R_factor_gt 0.0215 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0118P)^2^+1.9569P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0446 _refine_ls_wR_factor_ref 0.0463 _reflns_Friedel_coverage 0.000 _reflns_number_gt 12735 _reflns_number_total 14030 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d0cp01539c2.cif _cod_data_source_block JJM_1_200_0m _cod_database_code 7240476 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.226 _shelx_estimated_absorpt_t_max 0.316 _shelx_res_file ; TITL JJM_1_200_0m in P1 New:P-1 JJM_1_200_0m.res created by SHELXL-2018/3 at 11:01:17 on 28-Feb-2019 CELL 0.71073 12.5710 12.7256 13.7715 104.775 104.891 111.277 ZERR 2 0.0008 0.0008 0.0009 0.002 0.002 0.002 LATT 1 SFAC C H Au N P S UNIT 84 106 2 2 2 2 LIST 6 ! automatically inserted. Change 6 to 4 for CHECKCIF!! TEMP -123.170 SIZE 0.51 0.46 0.36 OMIT -1 1 1 L.S. 5 FMAP 2 PLAN -20 ACTA BOND $H CONF WGHT 0.011800 1.956900 EXTI 0.003326 FVAR 0.11530 C1 1 0.511129 -0.009894 0.265155 11.00000 0.01552 0.01170 = 0.01303 0.00401 0.00606 0.00538 C2 1 0.563277 0.105734 0.346226 11.00000 0.01782 0.01472 = 0.01391 0.00337 0.00655 0.00697 AFIX 43 H2 2 0.544200 0.114895 0.409348 11.00000 -1.20000 AFIX 0 C3 1 0.644017 0.209738 0.336488 11.00000 0.01559 0.01352 = 0.01631 0.00535 0.00655 0.00775 C4 1 0.670630 0.191788 0.242595 11.00000 0.02447 0.01317 = 0.01985 0.00534 0.01105 0.00465 AFIX 43 H4 2 0.723874 0.260919 0.233995 11.00000 -1.20000 AFIX 0 C5 1 0.621879 0.076220 0.161275 11.00000 0.02883 0.01543 = 0.01770 0.00520 0.01430 0.00704 AFIX 43 H5 2 0.642495 0.066531 0.098954 11.00000 -1.20000 AFIX 0 C6 1 0.542441 -0.024515 0.173399 11.00000 0.02153 0.01177 = 0.01502 0.00409 0.00891 0.00663 C7 1 0.482135 -0.155084 0.105233 11.00000 0.02109 0.01245 = 0.01445 0.00417 0.00841 0.00614 C8 1 0.485463 -0.216879 0.007693 11.00000 0.03075 0.01518 = 0.01700 0.00523 0.01390 0.00777 AFIX 43 H8 2 0.530013 -0.173201 -0.027218 11.00000 -1.20000 AFIX 0 C9 1 0.422198 -0.343812 -0.037444 11.00000 0.03029 0.01462 = 0.01636 0.00359 0.01193 0.00838 AFIX 43 H9 2 0.423162 -0.387030 -0.104294 11.00000 -1.20000 AFIX 0 C10 1 0.357236 -0.409120 0.013479 11.00000 0.01961 0.01173 = 0.01470 0.00250 0.00529 0.00603 C11 1 0.353252 -0.346319 0.110925 11.00000 0.01847 0.01403 = 0.01506 0.00440 0.00673 0.00502 AFIX 43 H11 2 0.308618 -0.390020 0.145774 11.00000 -1.20000 AFIX 0 C12 1 0.414964 -0.220074 0.155836 11.00000 0.01763 0.01312 = 0.01273 0.00307 0.00607 0.00592 C13 1 0.420186 -0.132770 0.257907 11.00000 0.01917 0.01168 = 0.01433 0.00386 0.00826 0.00518 C14 1 0.288208 -0.143291 0.233155 11.00000 0.01904 0.02205 = 0.02537 0.00481 0.01062 0.00666 AFIX 23 H14A 2 0.266141 -0.120661 0.169916 11.00000 -1.20000 H14B 2 0.229302 -0.230094 0.211033 11.00000 -1.20000 AFIX 0 C15 1 0.269097 -0.066321 0.325010 11.00000 0.02968 0.03091 = 0.03650 0.00925 0.02102 0.01422 AFIX 137 H15A 2 0.328542 0.019851 0.349881 11.00000 -1.50000 H15B 2 0.281821 -0.093360 0.385698 11.00000 -1.50000 H15C 2 0.184612 -0.075848 0.298649 11.00000 -1.50000 AFIX 0 C16 1 0.463119 -0.160050 0.359391 11.00000 0.03305 0.01744 = 0.01634 0.00714 0.01214 0.01103 AFIX 23 H16A 2 0.472168 -0.095411 0.423557 11.00000 -1.20000 H16B 2 0.397862 -0.238650 0.350635 11.00000 -1.20000 AFIX 0 C17 1 0.584430 -0.167421 0.381934 11.00000 0.04155 0.03492 = 0.02222 0.01090 0.00823 0.02390 AFIX 137 H17A 2 0.575143 -0.234544 0.320921 11.00000 -1.50000 H17B 2 0.606588 -0.182256 0.448971 11.00000 -1.50000 H17C 2 0.649844 -0.090220 0.390459 11.00000 -1.50000 AFIX 0 C18 1 0.295222 -0.543005 -0.032752 11.00000 0.01953 0.01384 = 0.01393 0.00240 0.00408 0.00665 C19 1 0.172966 -0.733653 -0.062249 11.00000 0.02930 0.01437 = 0.01846 0.00183 0.00806 0.00140 C20 1 0.082793 -0.830820 -0.053630 11.00000 0.05970 0.01945 = 0.03468 0.00197 0.02841 -0.00403 AFIX 43 H20 2 0.039658 -0.815977 -0.008560 11.00000 -1.20000 AFIX 0 C21 1 0.057492 -0.949305 -0.112124 11.00000 0.07628 0.01536 = 0.03622 0.00131 0.02565 -0.00821 AFIX 43 H21 2 -0.003599 -1.016014 -0.106864 11.00000 -1.20000 AFIX 0 C22 1 0.120070 -0.972023 -0.178314 11.00000 0.06662 0.01272 = 0.02733 0.00219 0.01292 0.00517 AFIX 43 H22 2 0.101769 -1.053980 -0.216741 11.00000 -1.20000 AFIX 0 C23 1 0.208230 -0.877779 -0.189223 11.00000 0.04560 0.01512 = 0.02618 0.00359 0.01191 0.01171 AFIX 43 H23 2 0.250875 -0.893407 -0.234542 11.00000 -1.20000 AFIX 0 C24 1 0.232606 -0.758755 -0.131429 11.00000 0.02703 0.01322 = 0.01875 0.00378 0.00529 0.00623 C25 1 0.710552 0.611203 0.639147 11.00000 0.01656 0.01446 = 0.01830 0.00558 0.00767 0.00638 AFIX 13 H25 2 0.643555 0.593255 0.570298 11.00000 -1.20000 AFIX 0 C26 1 0.645779 0.526929 0.690235 11.00000 0.02511 0.01982 = 0.03200 0.01338 0.01791 0.01079 AFIX 23 H26A 2 0.614781 0.440620 0.642460 11.00000 -1.20000 H26B 2 0.706027 0.543420 0.761583 11.00000 -1.20000 AFIX 0 C27 1 0.537553 0.547059 0.706007 11.00000 0.02597 0.03340 = 0.03926 0.01868 0.02182 0.01440 AFIX 23 H27A 2 0.473292 0.522191 0.633931 11.00000 -1.20000 H27B 2 0.500250 0.495067 0.742697 11.00000 -1.20000 AFIX 0 C28 1 0.579491 0.680248 0.773792 11.00000 0.03167 0.04033 = 0.03018 0.01822 0.02058 0.02477 AFIX 23 H28A 2 0.506609 0.691368 0.778011 11.00000 -1.20000 H28B 2 0.636022 0.702341 0.848773 11.00000 -1.20000 AFIX 0 C29 1 0.645596 0.764277 0.724439 11.00000 0.03477 0.02801 = 0.03718 0.01433 0.02250 0.02215 AFIX 23 H29A 2 0.675910 0.850371 0.772368 11.00000 -1.20000 H29B 2 0.586240 0.748166 0.652775 11.00000 -1.20000 AFIX 0 C30 1 0.754928 0.745645 0.709777 11.00000 0.02636 0.01733 = 0.03121 0.00622 0.01518 0.01086 AFIX 23 H30A 2 0.818110 0.768704 0.781894 11.00000 -1.20000 H30B 2 0.793463 0.798893 0.674517 11.00000 -1.20000 AFIX 0 C31 1 0.943710 0.577885 0.709455 11.00000 0.01802 0.01690 = 0.01607 0.00709 0.00504 0.00699 AFIX 13 H31 2 1.012336 0.580745 0.684478 11.00000 -1.20000 AFIX 0 C32 1 1.001574 0.693101 0.813380 11.00000 0.03508 0.01841 = 0.01669 0.00422 -0.00185 0.00701 AFIX 23 H32A 2 1.036072 0.766191 0.796280 11.00000 -1.20000 H32B 2 0.936387 0.696886 0.839859 11.00000 -1.20000 AFIX 0 C33 1 1.104127 0.695286 0.903136 11.00000 0.02640 0.03324 = 0.01793 0.00870 -0.00096 0.00539 AFIX 23 H33A 2 1.173997 0.701267 0.880412 11.00000 -1.20000 H33B 2 1.135067 0.767956 0.970319 11.00000 -1.20000 AFIX 0 C34 1 1.055889 0.580280 0.926130 11.00000 0.02321 0.04307 = 0.02193 0.01996 0.00873 0.01629 AFIX 23 H34A 2 1.123665 0.582265 0.983571 11.00000 -1.20000 H34B 2 0.989342 0.576860 0.953032 11.00000 -1.20000 AFIX 0 C35 1 1.005834 0.467423 0.823817 11.00000 0.02787 0.03272 = 0.03133 0.02019 0.00815 0.01722 AFIX 23 H35A 2 0.974926 0.393341 0.840313 11.00000 -1.20000 H35B 2 1.073300 0.469161 0.798727 11.00000 -1.20000 AFIX 0 C36 1 0.900774 0.461753 0.733542 11.00000 0.02418 0.01977 = 0.02786 0.01293 0.00349 0.00817 AFIX 23 H36A 2 0.830206 0.452317 0.756026 11.00000 -1.20000 H36B 2 0.872052 0.389615 0.666575 11.00000 -1.20000 AFIX 0 C37 1 0.903852 0.696656 0.556987 11.00000 0.01532 0.01410 = 0.01630 0.00563 0.00561 0.00500 AFIX 13 H37 2 0.942138 0.774727 0.622133 11.00000 -1.20000 AFIX 0 C38 1 1.007563 0.685085 0.523800 11.00000 0.02145 0.03194 = 0.03658 0.02115 0.01751 0.01605 AFIX 23 H38A 2 0.972209 0.608150 0.459488 11.00000 -1.20000 H38B 2 1.067542 0.681757 0.584149 11.00000 -1.20000 AFIX 0 C39 1 1.074564 0.793988 0.496478 11.00000 0.02474 0.03517 = 0.04297 0.02466 0.02107 0.01352 AFIX 23 H39A 2 1.116265 0.870044 0.562767 11.00000 -1.20000 H39B 2 1.138867 0.783023 0.472313 11.00000 -1.20000 AFIX 0 C40 1 0.984897 0.806075 0.407389 11.00000 0.03718 0.03665 = 0.03946 0.02698 0.02663 0.02150 AFIX 23 H40A 2 1.029699 0.880392 0.395377 11.00000 -1.20000 H40B 2 0.950741 0.734488 0.338509 11.00000 -1.20000 AFIX 0 C41 1 0.879654 0.814104 0.438055 11.00000 0.03473 0.03388 = 0.04026 0.02748 0.02240 0.02211 AFIX 23 H41A 2 0.819887 0.816484 0.376840 11.00000 -1.20000 H41B 2 0.912972 0.890838 0.502046 11.00000 -1.20000 AFIX 0 C42 1 0.812816 0.705427 0.464809 11.00000 0.02012 0.02873 = 0.02629 0.01802 0.01005 0.01287 AFIX 23 H42A 2 0.773424 0.629089 0.399092 11.00000 -1.20000 H42B 2 0.746839 0.714879 0.487031 11.00000 -1.20000 AFIX 0 AU1 3 0.725096 0.380752 0.456736 11.00000 0.01480 0.01151 = 0.01481 0.00262 0.00446 0.00514 N1 4 0.210907 -0.610604 -0.006315 11.00000 0.02773 0.01267 = 0.02115 0.00060 0.01125 0.00208 P1 5 0.822473 0.570710 0.594726 11.00000 0.01408 0.01128 = 0.01339 0.00376 0.00466 0.00496 S1 6 0.336460 -0.622958 -0.127925 11.00000 0.02994 0.01334 = 0.03070 0.00415 0.01766 0.00825 HKLF 4 REM JJM_1_200_0m in P1 New:P-1 REM wR2 = 0.0463, GooF = S = 1.136, Restrained GooF = 1.136 for all data REM R1 = 0.0215 for 12735 Fo > 4sig(Fo) and 0.0268 for all 14030 data REM 418 parameters refined using 0 restraints END WGHT 0.0114 1.9620 REM Highest difference peak 4.223, deepest hole -1.174, 1-sigma level 0.101 Q1 1 0.8238 0.8568 0.6304 11.00000 0.05 4.22 Q2 1 0.7255 0.6654 0.4879 11.00000 0.05 1.21 Q3 1 0.8842 0.6125 0.9564 11.00000 0.05 1.00 Q4 1 0.2175 -0.1340 0.2165 11.00000 0.05 0.83 Q5 1 0.7231 0.4953 0.3720 11.00000 0.05 0.63 Q6 1 0.5270 -0.0166 0.2192 11.00000 0.05 0.61 Q7 1 0.7975 0.9069 0.5951 11.00000 0.05 0.61 Q8 1 0.5998 0.1557 0.3395 11.00000 0.05 0.59 Q9 1 0.6005 0.3448 0.5351 11.00000 0.05 0.59 Q10 1 0.7219 0.2630 0.5423 11.00000 0.05 0.57 Q11 1 0.3435 -0.3759 0.0502 11.00000 0.05 0.57 Q12 1 0.1652 -0.6869 -0.0461 11.00000 0.05 0.56 Q13 1 0.3172 -0.4810 -0.0096 11.00000 0.05 0.56 Q14 1 0.3783 -0.3803 -0.0153 11.00000 0.05 0.56 Q15 1 0.4481 -0.1887 0.1252 11.00000 0.05 0.56 Q16 1 0.3947 -0.2808 0.1397 11.00000 0.05 0.52 Q17 1 0.8764 0.6563 0.5698 11.00000 0.05 0.52 Q18 1 0.4768 -0.1800 0.0503 11.00000 0.05 0.52 Q19 1 0.9221 0.8151 0.6020 11.00000 0.05 0.52 Q20 1 0.6298 0.1259 0.1971 11.00000 0.05 0.51 ; _shelx_res_checksum 45769 _shelx_hkl_file ; -2 0 0 105.28 2.76 -2 0 0 102.57 2.75 -2 0 0 107.04 2.75 -2 0 0 103.34 2.76 -2 0 0 103.85 2.73 -2 0 0 101.16 2.72 -2 0 0 111.40 2.81 -2 0 0 105.46 2.75 2 0 0 98.82 2.73 2 0 0 102.42 2.75 2 0 0 104.26 2.75 2 0 0 101.20 2.74 2 0 0 98.98 2.72 -3 0 0 108.94 2.78 -3 0 0 100.46 2.75 -3 0 0 101.30 2.80 -3 0 0 103.51 2.76 -3 0 0 106.17 2.79 -3 0 0 102.63 2.79 -3 0 0 111.55 2.88 -3 0 0 107.48 2.78 3 0 0 100.67 2.74 3 0 0 105.01 2.78 3 0 0 104.48 2.78 3 0 0 101.42 2.78 3 0 0 100.57 2.76 -4 0 0 121.53 3.12 -4 0 0 115.04 3.08 -4 0 0 113.91 3.07 -4 0 0 113.79 3.14 -4 0 0 113.43 3.12 -4 0 0 122.17 3.11 -4 0 0 115.97 3.24 -4 0 0 120.37 3.14 4 0 0 115.69 3.12 4 0 0 111.17 3.09 4 0 0 113.60 3.11 4 0 0 119.01 3.12 -5 0 0 77.56 2.03 -5 0 0 76.44 2.12 -5 0 0 80.39 2.06 -5 0 0 81.50 2.13 -5 0 0 72.13 2.36 -5 0 0 78.87 2.10 -5 0 0 80.95 2.11 5 0 0 66.52 2.14 5 0 0 76.41 2.11 5 0 0 78.36 2.11 5 0 0 74.44 2.06 -6 0 0 23.42 0.73 -6 0 0 21.24 0.80 -6 0 0 23.29 0.66 -6 0 0 22.31 0.75 -6 0 0 22.24 0.60 -6 0 0 22.55 0.77 6 0 0 20.65 0.66 6 0 0 20.45 0.73 6 0 0 21.12 0.74 6 0 0 21.65 0.77 -7 0 0 71.86 1.85 -7 0 0 70.07 1.97 -7 0 0 69.95 1.94 -7 0 0 68.42 1.99 -7 0 0 69.26 1.96 -7 0 0 67.27 2.19 -7 0 0 69.52 1.92 7 0 0 67.34 1.94 7 0 0 65.25 1.93 7 0 0 67.29 1.95 7 0 0 62.96 1.86 -8 0 0 2.58 0.37 -8 0 0 3.36 0.39 -8 0 0 3.83 0.32 -8 0 0 3.10 0.33 -8 0 0 3.02 0.44 -8 0 0 3.07 0.43 -8 0 0 3.50 0.36 8 0 0 4.66 0.60 8 0 0 3.12 0.34 8 0 0 3.02 0.38 8 0 0 2.60 0.33 8 0 0 2.48 0.36 -9 0 0 65.39 1.74 -9 0 0 65.12 1.91 -9 0 0 62.61 1.96 -9 0 0 62.39 2.13 -9 0 0 63.95 1.86 -9 0 0 62.47 1.92 9 0 0 64.83 2.16 9 0 0 60.98 1.88 9 0 0 62.28 1.90 9 0 0 61.85 1.76 9 0 0 60.35 1.86 -10 0 0 -0.53 0.45 -10 0 0 0.64 0.52 -10 0 0 0.04 0.34 -10 0 0 0.72 0.48 10 0 0 0.49 0.45 10 0 0 0.02 0.43 10 0 0 0.43 0.45 10 0 0 0.18 0.23 -11 0 0 102.21 3.03 -11 0 0 102.27 3.29 -11 0 0 104.23 2.97 11 0 0 104.36 2.77 11 0 0 93.39 3.27 11 0 0 99.44 2.94 11 0 0 102.84 2.95 -12 0 0 -0.14 0.54 -12 0 0 0.78 0.66 12 0 0 0.68 0.56 12 0 0 0.54 0.26 12 0 0 -0.09 0.52 -13 0 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1.39 -6 2 0 49.59 1.50 -6 2 0 50.00 1.65 -6 2 0 50.28 1.38 -6 2 0 48.40 1.50 -6 2 0 52.81 1.45 -6 2 0 52.59 1.46 5 -2 0 34.98 1.08 5 -2 0 36.88 1.23 5 -2 0 39.28 1.08 5 -2 0 37.53 1.06 5 -2 0 34.87 1.01 5 -2 0 37.83 1.02 -5 2 0 35.45 1.01 -5 2 0 33.62 1.09 -5 2 0 36.54 1.05 -5 2 0 36.87 1.05 -5 2 0 34.02 1.08 -5 2 0 36.10 1.23 -5 2 0 37.02 1.01 4 -2 0 157.36 4.28 4 -2 0 162.68 4.31 4 -2 0 168.43 4.32 4 -2 0 162.89 4.32 4 -2 0 175.33 4.47 4 -2 0 154.76 4.28 4 -2 0 159.45 4.29 -4 2 0 154.43 4.28 -4 2 0 171.33 4.31 -4 2 0 149.49 4.31 -4 2 0 160.29 4.28 -4 2 0 152.19 4.31 -4 2 0 168.47 4.46 -4 2 0 159.14 4.29 -4 2 0 167.47 4.30 3 -2 0 116.97 3.09 3 -2 0 113.32 3.07 3 -2 0 121.01 3.20 3 -2 0 117.84 3.08 3 -2 0 116.65 3.07 3 -2 0 117.33 3.09 3 -2 0 114.51 3.07 -3 2 0 112.02 3.06 -3 2 0 120.97 3.09 -3 2 0 119.27 3.20 -3 2 0 111.04 3.07 -3 2 0 108.92 3.09 -3 2 0 117.44 3.07 -3 2 0 109.77 3.08 2 -2 0 2.68 0.16 2 -2 0 2.93 0.17 2 -2 0 2.57 0.18 2 -2 0 2.59 0.15 2 -2 0 2.76 0.17 2 -2 0 2.60 0.23 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2.66 -4 -2 0 61.31 1.63 -4 -2 0 59.90 1.61 -4 -2 0 60.45 1.66 -4 -2 0 60.88 1.73 -4 -2 0 58.89 1.66 -4 -2 0 59.43 1.70 -4 -2 0 61.73 1.66 4 2 0 60.18 1.75 4 2 0 56.01 1.66 4 2 0 59.71 1.64 4 2 0 58.46 1.67 -5 -2 0 132.25 3.60 -5 -2 0 134.96 3.50 -5 -2 0 133.39 3.55 -5 -2 0 132.61 3.51 -5 -2 0 131.58 3.47 -5 -2 0 127.68 3.45 -5 -2 0 126.64 3.44 -5 -2 0 125.63 3.51 -5 -2 0 128.07 3.54 5 2 0 126.28 3.48 5 2 0 130.46 3.51 5 2 0 129.43 3.64 5 2 0 130.02 3.52 -6 -2 0 79.24 2.19 -6 -2 0 79.01 2.12 -6 -2 0 76.52 2.09 -6 -2 0 78.16 2.09 -6 -2 0 77.82 2.23 -6 -2 0 80.57 2.17 -6 -2 0 77.80 2.30 -6 -2 0 75.86 2.23 -6 -2 0 77.28 2.18 6 2 0 76.23 2.13 6 2 0 79.78 2.34 6 2 0 76.02 2.19 6 2 0 78.93 2.20 -7 -2 0 82.48 2.37 -7 -2 0 81.42 2.19 -7 -2 0 84.23 2.32 -7 -2 0 80.56 2.39 -7 -2 0 83.72 2.19 -7 -2 0 83.06 2.46 -7 -2 0 83.33 2.33 -7 -2 0 82.05 2.24 -7 -2 0 85.66 2.31 7 2 0 78.70 2.32 7 2 0 79.24 2.25 7 2 0 81.36 2.50 7 2 0 80.37 2.33 -8 -2 0 96.20 2.88 -8 -2 0 98.82 2.70 -8 -2 0 97.03 2.80 -8 -2 0 98.56 2.72 8 2 0 94.37 2.92 8 2 0 96.06 2.73 8 2 0 93.62 2.71 8 2 0 93.33 2.63 -9 -2 0 22.69 0.75 -9 -2 0 21.51 1.11 -9 -2 0 22.32 1.06 -9 -2 0 23.24 0.98 9 2 0 21.43 0.99 9 2 0 21.90 1.02 9 2 0 18.47 0.91 9 2 0 21.14 1.12 -10 -2 0 38.94 1.53 -10 -2 0 35.70 1.55 -10 -2 0 38.77 1.13 -10 -2 0 37.43 1.38 10 2 0 36.13 1.34 10 2 0 37.14 1.60 10 2 0 36.99 1.37 -11 -2 0 -0.12 0.27 -11 -2 0 0.16 0.51 -11 -2 0 -0.29 0.65 11 2 0 0.28 0.55 11 2 0 0.40 0.52 -12 -2 0 49.73 1.96 -12 -2 0 50.06 1.80 12 2 0 52.03 1.89 12 2 0 51.09 1.85 -13 -2 0 7.82 1.08 -13 -2 0 8.24 0.77 13 2 0 9.74 0.83 -14 -2 0 12.81 1.17 -14 -2 0 9.89 1.05 14 2 0 12.74 1.36 -15 -2 0 8.17 1.13 -15 -2 0 8.09 0.88 17 -3 0 0.02 0.81 17 -3 0 0.84 0.83 -17 3 0 0.63 0.97 -17 3 0 1.28 0.86 -17 3 0 -0.55 0.86 16 -3 0 22.78 1.40 16 -3 0 26.16 1.55 -16 3 0 20.01 1.48 -16 3 0 21.29 1.68 15 -3 0 -0.08 0.68 15 -3 0 0.41 0.68 -15 3 0 -0.20 0.90 -15 3 0 0.54 0.74 14 -3 0 28.30 1.40 14 -3 0 27.32 1.40 -14 3 0 27.29 1.42 -14 3 0 28.79 1.57 13 -3 0 0.67 0.55 13 -3 0 1.63 0.58 -13 3 0 1.00 0.67 -13 3 0 1.28 0.63 12 -3 0 45.43 1.61 12 -3 0 46.85 1.65 12 -3 0 42.52 2.00 -12 3 0 46.20 1.74 -12 3 0 47.59 2.02 -12 3 0 46.48 1.65 11 -3 0 18.92 0.91 11 -3 0 18.28 1.28 11 -3 0 20.21 0.94 -11 3 0 18.35 0.95 -11 3 0 18.40 1.02 -11 3 0 15.69 1.21 -11 3 0 18.82 1.02 10 -3 0 41.10 1.70 10 -3 0 41.99 1.36 10 -3 0 42.26 1.15 10 -3 0 40.65 1.37 10 -3 0 38.76 1.23 10 -3 0 41.25 1.38 -10 3 0 38.19 1.68 -10 3 0 42.51 1.35 -10 3 0 39.75 1.34 -10 3 0 40.51 1.36 -10 3 0 41.79 1.49 -10 3 0 43.64 1.44 9 -3 0 63.56 1.88 9 -3 0 62.65 1.85 9 -3 0 64.11 2.20 9 -3 0 64.76 1.74 9 -3 0 60.64 1.78 9 -3 0 62.42 1.88 -9 3 0 62.06 1.73 -9 3 0 62.94 1.85 -9 3 0 64.61 1.94 -9 3 0 65.56 1.87 -9 3 0 64.23 2.19 -9 3 0 61.33 1.92 -9 3 0 65.18 1.86 8 -3 0 44.20 1.37 8 -3 0 42.80 1.22 8 -3 0 42.35 1.61 8 -3 0 44.52 1.36 8 -3 0 43.38 1.34 8 -3 0 41.95 1.25 8 -3 0 42.02 1.31 -8 3 0 41.65 1.21 -8 3 0 44.23 1.32 -8 3 0 44.47 1.32 -8 3 0 43.72 1.40 -8 3 0 43.49 1.60 -8 3 0 42.63 1.38 -8 3 0 44.31 1.31 7 -3 0 239.36 6.45 7 -3 0 241.90 6.43 7 -3 0 251.65 6.47 7 -3 0 240.20 6.47 7 -3 0 235.31 6.40 7 -3 0 246.77 6.72 7 -3 0 242.54 6.40 -7 3 0 244.30 6.71 -7 3 0 240.65 6.43 -7 3 0 253.78 6.45 -7 3 0 229.03 6.39 -7 3 0 233.25 6.48 -7 3 0 233.75 6.47 -7 3 0 246.75 6.44 6 -3 0 20.15 0.65 6 -3 0 21.13 0.73 6 -3 0 18.50 0.72 6 -3 0 19.25 0.63 6 -3 0 21.02 0.73 6 -3 0 20.29 0.91 -6 3 0 17.20 0.75 -6 3 0 22.05 0.70 -6 3 0 21.07 0.66 -6 3 0 20.20 0.63 -6 3 0 17.49 0.79 -6 3 0 21.23 0.68 -6 3 0 20.60 0.90 5 -3 0 226.54 5.79 5 -3 0 214.12 5.76 5 -3 0 211.82 5.75 5 -3 0 219.50 5.78 5 -3 0 231.63 5.98 5 -3 0 216.35 5.75 -5 3 0 226.65 5.77 -5 3 0 225.96 5.97 -5 3 0 206.91 5.79 -5 3 0 217.83 5.82 -5 3 0 215.49 5.74 -5 3 0 203.05 5.75 -5 3 0 204.81 5.78 4 -3 0 2.70 0.29 4 -3 0 3.04 0.23 4 -3 0 2.69 0.24 4 -3 0 2.52 0.22 4 -3 0 3.14 0.26 4 -3 0 2.36 0.27 4 -3 0 2.63 0.37 -4 3 0 2.75 0.26 -4 3 0 3.05 0.23 -4 3 0 2.50 0.27 -4 3 0 2.59 0.29 -4 3 0 2.80 0.18 -4 3 0 2.72 0.36 -4 3 0 3.15 0.25 3 -3 0 236.32 6.20 3 -3 0 253.25 6.34 3 -3 0 230.66 6.19 3 -3 0 238.22 6.21 3 -3 0 234.05 6.21 3 -3 0 238.02 6.20 -3 3 0 229.07 6.19 -3 3 0 222.52 6.20 -3 3 0 224.60 6.21 -3 3 0 225.45 6.16 -3 3 0 242.16 6.21 -3 3 0 247.87 6.33 -3 3 0 225.24 6.20 2 -3 0 37.28 1.04 2 -3 0 36.18 1.02 2 -3 0 39.26 1.05 2 -3 0 38.12 1.02 2 -3 0 38.75 1.05 2 -3 0 38.08 1.12 -2 3 0 36.77 1.12 -2 3 0 38.10 1.04 -2 3 0 36.25 1.05 -2 3 0 37.09 1.05 -2 3 0 36.89 1.02 -2 3 0 38.05 1.02 1 -3 0 101.42 2.79 1 -3 0 103.98 2.79 1 -3 0 111.38 2.85 1 -3 0 110.34 2.82 1 -3 0 101.35 2.79 1 -3 0 109.46 2.81 -1 3 0 109.12 2.85 -1 3 0 105.48 2.82 -1 3 0 100.66 2.79 -1 3 0 101.25 2.81 0 -3 0 43.13 1.17 0 -3 0 43.77 1.18 0 -3 0 44.44 1.19 0 -3 0 42.17 1.17 0 -3 0 42.82 1.17 0 3 0 43.66 1.17 0 3 0 41.70 1.17 0 3 0 42.01 1.17 0 3 0 42.50 1.19 -1 -3 0 122.64 3.21 -1 -3 0 116.15 3.20 -1 -3 0 120.98 3.22 -1 -3 0 121.48 3.21 -1 -3 0 122.53 3.21 -1 -3 0 122.58 3.20 1 3 0 115.79 3.21 -2 -3 0 209.11 5.54 -2 -3 0 209.03 5.54 -2 -3 0 216.32 5.53 -2 -3 0 212.54 5.57 -2 -3 0 210.32 5.54 -2 -3 0 214.53 5.54 2 3 0 197.42 5.54 2 3 0 199.31 5.54 2 3 0 214.35 5.55 -3 -3 0 15.40 0.50 -3 -3 0 14.24 0.50 -3 -3 0 15.26 0.52 -3 -3 0 13.89 0.55 -3 -3 0 14.86 0.51 -3 -3 0 15.61 0.58 3 3 0 15.16 0.53 3 3 0 15.28 0.52 -4 -3 0 116.41 3.07 -4 -3 0 110.77 3.06 -4 -3 0 113.90 3.10 -4 -3 0 114.16 3.04 -4 -3 0 115.01 3.11 -4 -3 0 116.38 3.04 -4 -3 0 113.40 3.06 4 3 0 110.58 3.05 4 3 0 112.44 3.13 4 3 0 110.40 3.07 -5 -3 0 12.42 0.64 -5 -3 0 11.17 0.43 -5 -3 0 11.61 0.59 -5 -3 0 11.10 0.46 -5 -3 0 9.71 0.63 -5 -3 0 11.11 0.49 -5 -3 0 12.01 0.55 -5 -3 0 11.93 0.53 5 3 0 11.14 0.49 5 3 0 12.19 0.58 5 3 0 11.27 0.53 5 3 0 11.65 0.59 -6 -3 0 104.09 2.96 -6 -3 0 101.35 2.92 -6 -3 0 105.42 2.87 -6 -3 0 103.89 2.79 -6 -3 0 107.01 2.89 -6 -3 0 109.18 2.95 -6 -3 0 103.79 2.87 -6 -3 0 104.59 2.80 6 3 0 98.74 2.84 6 3 0 102.36 3.00 6 3 0 102.96 2.89 6 3 0 107.27 2.90 -7 -3 0 3.81 0.29 -7 -3 0 2.95 0.38 -7 -3 0 3.05 0.27 -7 -3 0 3.65 0.49 -7 -3 0 3.87 0.40 -7 -3 0 3.19 0.47 -7 -3 0 3.57 0.29 -7 -3 0 3.55 0.36 -7 -3 0 3.04 0.37 7 3 0 3.73 0.42 7 3 0 3.46 0.40 7 3 0 3.38 0.41 7 3 0 3.89 0.41 -8 -3 0 91.26 2.37 -8 -3 0 87.50 2.61 -8 -3 0 86.63 2.36 -8 -3 0 89.71 2.54 -8 -3 0 92.40 2.55 -8 -3 0 87.94 2.67 -8 -3 0 91.49 2.44 8 3 0 84.83 2.54 8 3 0 86.45 2.55 8 3 0 89.42 2.56 8 3 0 86.69 2.72 -9 -3 0 3.10 0.48 -9 -3 0 3.88 0.63 -9 -3 0 3.51 0.51 -9 -3 0 4.29 0.46 9 3 0 3.16 0.51 9 3 0 3.92 0.52 9 3 0 3.58 0.52 9 3 0 3.49 0.34 -10 -3 0 30.35 1.23 -10 -3 0 28.72 0.96 -10 -3 0 27.76 1.32 -10 -3 0 27.20 1.36 10 3 0 29.73 1.19 10 3 0 29.69 1.24 10 3 0 31.03 1.64 -11 -3 0 21.72 1.16 -11 -3 0 22.58 0.81 -11 -3 0 21.47 1.35 11 3 0 23.57 1.28 -12 -3 0 13.62 1.09 -12 -3 0 13.48 1.37 12 3 0 14.15 1.23 -13 -3 0 30.58 1.73 -13 -3 0 31.06 1.47 13 3 0 32.41 1.56 -14 -3 0 0.53 0.90 -14 -3 0 0.42 0.69 -15 -3 0 18.73 1.67 -15 -3 0 17.34 1.77 18 -4 0 27.31 1.77 18 -4 0 29.45 1.77 -18 4 0 23.19 1.96 -18 4 0 27.23 1.79 -18 4 0 30.32 1.75 17 -4 0 1.90 0.79 17 -4 0 0.80 0.80 -17 4 0 2.33 0.98 -17 4 0 1.94 0.97 -17 4 0 1.84 0.88 16 -4 0 23.45 1.88 -16 4 0 25.41 1.69 -16 4 0 27.59 1.57 15 -4 0 8.78 0.80 15 -4 0 10.22 1.11 -15 4 0 10.75 1.02 -15 4 0 10.50 1.24 14 -4 0 31.46 1.45 14 -4 0 35.00 1.11 14 -4 0 35.33 1.52 -14 4 0 33.69 1.56 -14 4 0 31.19 1.51 13 -4 0 48.08 1.75 13 -4 0 49.01 1.46 13 -4 0 47.65 1.69 -13 4 0 47.69 1.86 -13 4 0 47.09 1.75 12 -4 0 5.25 0.55 12 -4 0 4.62 0.31 12 -4 0 4.19 0.58 12 -4 0 4.37 0.54 12 -4 0 3.29 0.69 -12 4 0 5.10 0.65 -12 4 0 3.78 0.73 -12 4 0 4.80 0.65 11 -4 0 66.15 2.04 11 -4 0 67.23 1.91 11 -4 0 66.44 2.00 11 -4 0 69.29 1.84 11 -4 0 66.32 2.45 -11 4 0 67.16 2.10 -11 4 0 66.50 2.13 -11 4 0 63.15 2.42 -11 4 0 65.72 1.99 10 -4 0 0.63 0.21 10 -4 0 0.58 0.42 10 -4 0 -0.16 0.38 10 -4 0 0.39 0.39 10 -4 0 0.57 0.42 10 -4 0 0.12 0.44 10 -4 0 0.25 0.38 -10 4 0 0.46 0.48 -10 4 0 0.97 0.45 -10 4 0 1.34 0.38 -10 4 0 0.63 0.47 -10 4 0 0.66 0.35 -10 4 0 0.15 0.20 -10 4 0 -0.04 0.32 9 -4 0 90.79 2.61 9 -4 0 91.54 2.95 9 -4 0 92.10 2.65 9 -4 0 96.74 2.65 9 -4 0 95.64 2.53 9 -4 0 93.91 2.66 -9 4 0 88.58 2.67 -9 4 0 93.29 2.60 -9 4 0 89.24 2.67 -9 4 0 93.62 2.61 -9 4 0 90.58 2.51 -9 4 0 92.72 2.58 -9 4 0 93.96 2.95 8 -4 0 1.08 0.29 8 -4 0 1.33 0.32 8 -4 0 1.82 0.32 8 -4 0 1.93 0.22 8 -4 0 0.63 0.34 8 -4 0 0.88 0.40 8 -4 0 0.98 0.25 -8 4 0 1.22 0.39 -8 4 0 0.70 0.35 -8 4 0 1.33 0.22 -8 4 0 1.37 0.24 -8 4 0 1.57 0.28 -8 4 0 2.09 0.32 -8 4 0 1.29 0.44 7 -4 0 161.63 4.45 7 -4 0 160.79 4.44 7 -4 0 167.03 4.39 7 -4 0 165.88 4.42 7 -4 0 169.67 4.44 7 -4 0 167.70 4.71 7 -4 0 165.91 4.39 -7 4 0 168.23 4.44 -7 4 0 158.73 4.39 -7 4 0 162.98 4.47 -7 4 0 155.98 4.38 -7 4 0 170.82 4.42 -7 4 0 167.67 4.70 -7 4 0 154.12 4.45 6 -4 0 24.13 0.77 6 -4 0 23.18 0.79 6 -4 0 24.20 0.80 6 -4 0 24.76 0.78 6 -4 0 24.07 1.03 6 -4 0 26.04 0.84 6 -4 0 24.36 0.83 -6 4 0 24.31 0.74 -6 4 0 24.51 1.01 -6 4 0 23.25 0.85 -6 4 0 26.76 0.83 -6 4 0 25.75 0.79 -6 4 0 23.87 0.77 5 -4 0 130.30 3.33 5 -4 0 125.57 3.33 5 -4 0 130.20 3.34 5 -4 0 122.44 3.33 5 -4 0 110.22 3.39 5 -4 0 124.66 3.54 5 -4 0 129.36 3.36 -5 4 0 122.89 3.33 -5 4 0 129.13 3.33 -5 4 0 121.67 3.29 -5 4 0 124.01 3.54 -5 4 0 119.68 3.35 -5 4 0 110.64 3.38 -5 4 0 133.68 3.36 4 -4 0 54.85 1.61 4 -4 0 58.77 1.57 4 -4 0 60.06 1.58 4 -4 0 58.22 1.75 4 -4 0 57.09 1.60 4 -4 0 59.84 1.59 -4 4 0 55.15 1.53 -4 4 0 59.95 1.60 -4 4 0 56.82 1.75 -4 4 0 54.12 1.58 -4 4 0 55.16 1.61 -4 4 0 56.31 1.59 -4 4 0 58.27 1.57 3 -4 0 102.29 2.79 3 -4 0 100.99 2.67 3 -4 0 95.89 2.64 3 -4 0 98.83 2.67 3 -4 0 101.53 2.67 3 -4 0 104.62 2.65 -3 4 0 95.99 2.65 -3 4 0 96.99 2.64 -3 4 0 96.80 2.68 -3 4 0 102.63 2.67 -3 4 0 99.09 2.79 -3 4 0 91.46 2.67 2 -4 0 230.91 6.20 2 -4 0 250.38 6.24 2 -4 0 253.83 6.32 2 -4 0 237.01 6.22 2 -4 0 225.37 6.20 -2 4 0 230.61 6.24 -2 4 0 216.87 6.22 -2 4 0 238.25 6.20 -2 4 0 242.59 6.31 -2 4 0 225.08 6.20 1 -4 0 27.72 0.79 1 -4 0 29.12 0.84 1 -4 0 29.29 0.83 1 -4 0 29.39 0.82 1 -4 0 28.35 0.78 1 -4 0 27.44 0.79 1 -4 0 27.79 0.81 -1 4 0 27.78 0.84 -1 4 0 26.20 0.83 -1 4 0 28.07 0.82 -1 4 0 27.58 0.79 0 -4 0 267.62 6.99 0 -4 0 275.17 7.01 0 -4 0 266.19 6.98 0 -4 0 279.89 7.00 0 -4 0 264.26 6.99 0 4 0 265.78 6.98 0 4 0 253.35 6.99 0 4 0 251.82 6.98 0 4 0 255.73 7.00 -1 -4 0 33.99 0.98 -1 -4 0 34.92 0.99 -1 -4 0 34.62 1.00 -1 -4 0 35.04 1.02 -1 -4 0 35.35 1.01 -1 -4 0 35.13 0.99 -2 -4 0 253.92 6.60 -2 -4 0 254.26 6.57 -2 -4 0 248.10 6.57 -2 -4 0 243.29 6.57 -2 -4 0 245.90 6.57 -2 -4 0 251.46 6.56 2 4 0 237.35 6.57 -3 -4 0 72.59 1.94 -3 -4 0 69.86 1.99 -3 -4 0 59.83 2.03 -3 -4 0 73.32 1.94 -3 -4 0 75.09 1.96 -3 -4 0 71.00 1.92 3 4 0 71.93 1.94 3 4 0 70.19 1.95 -4 -4 0 106.76 2.93 -4 -4 0 111.19 2.92 -4 -4 0 110.54 2.92 -4 -4 0 109.12 3.00 -4 -4 0 111.08 2.95 -4 -4 0 106.90 2.94 4 4 0 100.59 2.94 4 4 0 108.64 2.97 4 4 0 108.08 2.96 -5 -4 0 27.59 0.93 -5 -4 0 28.51 0.87 -5 -4 0 27.98 1.01 -5 -4 0 28.83 0.87 -5 -4 0 28.64 0.92 -5 -4 0 28.05 0.90 -5 -4 0 28.30 1.03 -5 -4 0 27.46 0.93 5 4 0 28.46 0.96 5 4 0 26.81 0.94 -6 -4 0 54.54 1.54 -6 -4 0 52.81 1.70 -6 -4 0 53.98 1.52 -6 -4 0 54.89 1.62 -6 -4 0 55.34 1.56 -6 -4 0 53.66 1.72 -6 -4 0 55.66 1.60 -6 -4 0 54.67 1.65 -6 -4 0 54.66 1.61 6 4 0 53.72 1.59 6 4 0 54.39 1.65 6 4 0 56.61 1.70 -7 -4 0 48.77 1.59 -7 -4 0 49.79 1.42 -7 -4 0 51.50 1.46 -7 -4 0 47.64 1.61 -7 -4 0 49.41 1.41 -7 -4 0 52.25 1.54 -7 -4 0 50.36 1.54 7 4 0 49.58 1.57 7 4 0 51.15 1.49 7 4 0 51.01 1.65 -8 -4 0 0.09 0.39 -8 -4 0 0.70 0.34 -8 -4 0 0.18 0.53 -8 -4 0 0.22 0.18 -8 -4 0 0.68 0.28 -8 -4 0 0.38 0.19 8 4 0 0.46 0.31 8 4 0 0.11 0.35 8 4 0 0.59 0.44 -9 -4 0 42.55 1.30 -9 -4 0 42.63 1.14 -9 -4 0 41.21 1.57 -9 -4 0 40.77 1.55 -9 -4 0 43.37 1.46 9 4 0 44.19 1.55 -10 -4 0 0.27 0.50 -10 -4 0 0.94 0.32 -10 -4 0 0.50 0.68 10 4 0 0.77 0.56 -11 -4 0 32.45 1.56 -11 -4 0 35.21 1.41 -12 -4 0 2.81 1.19 -12 -4 0 2.63 0.65 -13 -4 0 26.56 1.77 -13 -4 0 30.52 1.43 -14 -4 0 4.26 0.78 -14 -4 0 2.35 0.95 18 -5 0 12.81 1.43 18 -5 0 13.15 1.11 -18 5 0 13.59 1.52 -18 5 0 15.00 1.77 17 -5 0 7.39 0.89 17 -5 0 7.33 0.88 -17 5 0 7.08 1.36 -17 5 0 5.20 1.01 -17 5 0 5.61 1.02 16 -5 0 7.25 1.15 -16 5 0 9.11 1.15 -16 5 0 9.25 0.97 15 -5 0 36.58 1.63 15 -5 0 35.15 1.18 15 -5 0 34.97 1.55 -15 5 0 35.74 1.75 -15 5 0 34.25 1.63 14 -5 0 0.71 0.34 14 -5 0 0.11 0.57 14 -5 0 0.44 0.62 -14 5 0 -0.19 0.73 -14 5 0 0.58 0.68 13 -5 0 54.17 1.65 13 -5 0 55.20 1.84 13 -5 0 55.45 1.53 13 -5 0 55.34 1.86 -13 5 0 55.15 1.93 -13 5 0 53.07 2.33 -13 5 0 53.47 1.93 12 -5 0 7.36 0.84 12 -5 0 7.06 0.61 12 -5 0 7.50 0.75 12 -5 0 8.90 0.53 12 -5 0 7.78 0.90 -12 5 0 6.79 0.71 -12 5 0 9.46 1.23 -12 5 0 7.70 0.75 -12 5 0 7.43 0.72 11 -5 0 38.05 1.33 11 -5 0 38.07 1.23 11 -5 0 39.05 1.38 11 -5 0 38.13 1.77 -11 5 0 38.32 1.47 -11 5 0 39.26 1.48 -11 5 0 39.29 1.16 -11 5 0 39.09 1.27 -11 5 0 37.05 1.76 10 -5 0 86.70 2.89 10 -5 0 87.11 2.55 10 -5 0 89.16 2.49 10 -5 0 87.51 2.48 10 -5 0 85.62 2.52 10 -5 0 87.01 2.52 10 -5 0 87.90 2.44 -10 5 0 85.47 2.58 -10 5 0 88.06 2.48 -10 5 0 89.42 2.45 -10 5 0 86.23 2.56 -10 5 0 83.26 2.40 -10 5 0 87.48 2.54 -10 5 0 86.45 2.88 9 -5 0 46.44 1.53 9 -5 0 46.22 1.46 9 -5 0 48.31 1.48 9 -5 0 49.39 1.54 9 -5 0 48.01 1.83 9 -5 0 48.13 1.43 9 -5 0 48.62 1.42 -9 5 0 50.57 1.47 -9 5 0 47.55 1.56 -9 5 0 49.81 1.83 -9 5 0 48.93 1.42 -9 5 0 46.01 1.54 -9 5 0 48.11 1.49 -9 5 0 45.21 1.39 8 -5 0 67.27 1.91 8 -5 0 62.13 1.83 8 -5 0 64.75 1.82 8 -5 0 64.95 1.90 8 -5 0 64.27 1.84 8 -5 0 64.81 2.18 8 -5 0 64.36 1.86 -8 5 0 64.39 1.83 -8 5 0 65.73 1.87 -8 5 0 61.26 1.81 -8 5 0 64.92 2.17 -8 5 0 61.98 1.92 -8 5 0 61.23 1.90 7 -5 0 33.25 1.31 7 -5 0 29.94 1.00 7 -5 0 32.82 1.05 7 -5 0 33.16 1.00 7 -5 0 32.33 1.07 7 -5 0 33.25 1.01 -7 5 0 32.35 1.00 -7 5 0 31.72 0.94 -7 5 0 30.02 1.03 -7 5 0 30.51 1.07 -7 5 0 32.13 1.03 -7 5 0 30.39 0.99 -7 5 0 33.80 1.31 6 -5 0 87.68 2.38 6 -5 0 89.80 2.43 6 -5 0 87.71 2.42 6 -5 0 88.51 2.45 6 -5 0 80.89 2.40 6 -5 0 91.00 2.40 6 -5 0 88.11 2.65 -6 5 0 86.03 2.33 -6 5 0 83.69 2.40 -6 5 0 89.21 2.42 -6 5 0 85.33 2.63 -6 5 0 85.72 2.39 -6 5 0 86.38 2.45 5 -5 0 8.53 0.40 5 -5 0 9.40 0.49 5 -5 0 8.59 0.50 5 -5 0 8.89 0.44 5 -5 0 7.89 0.45 5 -5 0 8.51 0.61 5 -5 0 8.55 0.40 -5 5 0 6.84 0.48 -5 5 0 8.36 0.43 -5 5 0 8.34 0.46 -5 5 0 8.72 0.59 -5 5 0 7.88 0.38 -5 5 0 8.86 0.28 -5 5 0 8.29 0.43 4 -5 0 77.95 2.26 4 -5 0 87.82 2.23 4 -5 0 84.80 2.26 4 -5 0 81.99 2.22 4 -5 0 85.48 2.42 -4 5 0 84.05 2.22 -4 5 0 75.06 2.27 -4 5 0 80.99 2.41 -4 5 0 77.80 2.23 -4 5 0 80.91 2.26 -4 5 0 85.92 2.25 3 -5 0 1.35 0.15 3 -5 0 1.22 0.20 3 -5 0 1.32 0.14 3 -5 0 2.13 0.26 -3 5 0 1.32 0.20 -3 5 0 1.09 0.22 -3 5 0 1.15 0.15 -3 5 0 1.64 0.22 -3 5 0 1.34 0.14 2 -5 0 198.08 5.08 2 -5 0 198.83 5.11 2 -5 0 190.08 5.11 2 -5 0 188.51 5.06 2 -5 0 186.32 5.08 2 -5 0 204.58 5.20 -2 5 0 186.66 5.13 -2 5 0 197.76 5.20 -2 5 0 190.61 5.11 -2 5 0 179.16 5.09 1 -5 0 57.89 1.54 1 -5 0 57.51 1.53 1 -5 0 57.08 1.57 1 -5 0 55.12 1.62 1 -5 0 57.06 1.53 -1 5 0 55.10 1.57 -1 5 0 54.89 1.53 -1 5 0 54.47 1.55 -1 5 0 53.74 1.58 0 -5 0 285.57 7.45 0 -5 0 278.26 7.52 0 -5 0 283.93 7.44 0 -5 0 286.48 7.46 0 -5 0 297.10 7.47 0 5 0 272.36 7.46 0 5 0 266.06 7.47 0 5 0 274.30 7.43 0 5 0 290.36 7.43 -1 -5 0 189.86 4.83 -1 -5 0 185.40 4.82 -1 -5 0 165.18 4.84 -1 -5 0 164.44 4.93 -1 -5 0 188.27 4.85 -1 -5 0 190.38 4.81 -2 -5 0 76.69 2.10 -2 -5 0 76.69 2.10 -2 -5 0 74.97 2.09 -2 -5 0 74.62 2.08 -2 -5 0 76.56 2.09 -2 -5 0 76.16 2.13 -2 -5 0 75.80 2.08 -3 -5 0 128.72 3.50 -3 -5 0 131.45 3.48 -3 -5 0 125.38 3.48 -3 -5 0 131.12 3.49 -3 -5 0 125.67 3.53 -3 -5 0 128.53 3.48 -3 -5 0 131.77 3.48 -4 -5 0 29.01 0.93 -4 -5 0 29.73 0.97 -4 -5 0 28.39 0.98 -4 -5 0 29.48 0.86 -4 -5 0 29.61 0.93 -4 -5 0 30.58 0.95 -4 -5 0 28.78 1.05 -4 -5 0 29.88 0.94 4 5 0 28.59 0.97 4 5 0 30.52 0.88 -5 -5 0 159.76 4.28 -5 -5 0 157.94 4.30 -5 -5 0 157.43 4.39 -5 -5 0 154.87 4.35 -5 -5 0 159.32 4.32 -5 -5 0 164.01 4.30 -5 -5 0 162.06 4.29 -5 -5 0 160.18 4.28 -5 -5 0 157.31 4.30 5 5 0 158.63 4.31 5 5 0 158.74 4.31 -6 -5 0 5.57 0.58 -6 -5 0 5.66 0.66 -6 -5 0 6.50 0.49 -6 -5 0 6.21 0.47 -6 -5 0 6.21 0.60 -6 -5 0 6.48 0.47 6 5 0 7.14 0.76 -7 -5 0 16.37 0.98 -7 -5 0 18.26 0.73 -7 -5 0 16.57 0.83 -7 -5 0 16.91 0.65 -7 -5 0 17.48 0.78 7 5 0 17.66 0.81 -8 -5 0 13.82 0.69 -8 -5 0 14.47 0.86 -8 -5 0 14.05 0.66 -8 -5 0 15.23 0.86 -8 -5 0 13.95 1.05 -8 -5 0 15.09 0.58 8 5 0 14.06 0.80 -9 -5 0 56.41 1.51 -9 -5 0 52.98 1.90 -9 -5 0 52.44 1.51 -9 -5 0 55.11 1.64 -9 -5 0 55.34 1.82 -9 -5 0 56.21 1.77 9 5 0 54.41 1.84 -10 -5 0 13.33 1.27 -10 -5 0 11.94 0.98 -11 -5 0 12.03 1.02 -11 -5 0 9.22 0.92 -12 -5 0 15.91 1.19 -12 -5 0 15.65 1.50 -13 -5 0 6.84 0.79 -13 -5 0 6.66 1.04 18 -6 0 -0.42 0.83 18 -6 0 -0.49 0.75 -18 6 0 0.03 0.98 -18 6 0 -0.65 0.79 -18 6 0 0.20 0.91 17 -6 0 8.02 0.92 17 -6 0 11.71 0.94 -17 6 0 10.91 0.92 -17 6 0 9.43 1.16 -17 6 0 7.02 1.05 16 -6 0 5.06 0.73 16 -6 0 5.06 0.44 16 -6 0 4.74 1.17 -16 6 0 4.33 0.88 -16 6 0 4.02 0.74 15 -6 0 14.20 1.16 15 -6 0 16.21 1.30 15 -6 0 14.41 0.79 -15 6 0 15.34 1.38 -15 6 0 14.40 1.29 14 -6 0 26.53 1.04 14 -6 0 27.82 1.40 14 -6 0 26.97 1.29 -14 6 0 27.68 1.42 -14 6 0 26.98 1.43 13 -6 0 16.28 1.54 13 -6 0 17.21 0.84 13 -6 0 18.20 0.72 13 -6 0 18.04 0.96 13 -6 0 16.27 1.14 -13 6 0 15.90 1.55 -13 6 0 17.13 1.10 -13 6 0 17.31 1.23 -13 6 0 17.76 1.22 12 -6 0 42.77 1.47 12 -6 0 41.14 1.57 12 -6 0 42.73 1.99 12 -6 0 43.15 1.37 12 -6 0 42.87 1.31 -12 6 0 41.31 1.38 -12 6 0 43.60 2.02 -12 6 0 42.32 1.63 -12 6 0 41.00 1.61 11 -6 0 11.85 0.64 11 -6 0 9.77 0.91 11 -6 0 12.11 0.79 11 -6 0 10.85 0.70 11 -6 0 13.07 1.21 -11 6 0 13.57 0.89 -11 6 0 13.93 0.65 -11 6 0 13.19 1.21 -11 6 0 13.32 1.00 -11 6 0 14.51 0.70 -11 6 0 13.55 0.82 10 -6 0 199.43 5.54 10 -6 0 201.53 5.59 10 -6 0 210.96 5.59 10 -6 0 200.56 5.96 10 -6 0 210.04 5.52 10 -6 0 200.88 5.61 10 -6 0 204.85 5.52 -10 6 0 200.53 5.62 -10 6 0 212.00 5.56 -10 6 0 198.49 5.62 -10 6 0 211.82 6.00 -10 6 0 210.01 5.50 -10 6 0 204.33 5.50 9 -6 0 20.07 0.83 9 -6 0 19.90 1.17 9 -6 0 20.70 0.77 9 -6 0 20.29 0.93 9 -6 0 20.50 0.82 9 -6 0 20.85 0.92 9 -6 0 20.68 0.80 -9 6 0 20.50 0.87 -9 6 0 20.92 0.94 -9 6 0 21.98 0.78 -9 6 0 20.60 0.74 -9 6 0 22.52 0.84 -9 6 0 20.43 1.19 -9 6 0 21.50 1.00 8 -6 0 107.27 2.88 8 -6 0 107.29 2.85 8 -6 0 104.40 2.85 8 -6 0 106.39 2.91 8 -6 0 102.33 2.85 8 -6 0 102.80 2.91 8 -6 0 104.07 3.20 -8 6 0 99.04 2.94 -8 6 0 101.40 2.85 -8 6 0 106.68 2.90 -8 6 0 101.74 2.79 -8 6 0 105.02 2.86 -8 6 0 95.54 2.88 -8 6 0 103.69 3.21 7 -6 0 24.09 0.87 7 -6 0 23.56 0.86 7 -6 0 23.93 0.81 7 -6 0 25.27 0.82 7 -6 0 24.99 1.13 7 -6 0 25.68 0.83 7 -6 0 23.24 0.81 -7 6 0 23.50 1.11 -7 6 0 23.01 0.90 -7 6 0 24.09 0.87 -7 6 0 23.31 0.86 -7 6 0 21.99 0.83 -7 6 0 23.40 0.71 -7 6 0 23.71 0.81 6 -6 0 81.76 2.24 6 -6 0 78.13 2.21 6 -6 0 84.46 2.22 6 -6 0 80.72 2.23 6 -6 0 81.63 2.27 6 -6 0 80.88 2.26 6 -6 0 84.53 2.50 -6 6 0 76.30 2.24 -6 6 0 79.55 2.48 -6 6 0 82.09 2.25 -6 6 0 76.69 2.27 -6 6 0 79.24 2.21 -6 6 0 78.94 2.14 -6 6 0 78.82 2.14 5 -6 0 84.21 2.29 5 -6 0 81.96 2.29 5 -6 0 81.52 2.23 5 -6 0 82.02 2.25 5 -6 0 80.49 2.47 5 -6 0 84.09 2.28 -5 6 0 78.77 2.24 -5 6 0 82.46 2.30 -5 6 0 81.03 2.47 -5 6 0 83.80 2.23 -5 6 0 84.99 2.28 -5 6 0 75.95 2.28 4 -6 0 57.17 1.61 4 -6 0 55.22 1.61 4 -6 0 57.02 1.56 4 -6 0 54.58 1.56 4 -6 0 57.18 1.77 4 -6 0 58.40 1.61 -4 6 0 55.66 1.62 -4 6 0 57.72 1.61 -4 6 0 54.12 1.63 -4 6 0 58.62 1.56 -4 6 0 56.50 1.76 -4 6 0 55.27 1.57 3 -6 0 121.64 3.34 3 -6 0 130.36 3.55 3 -6 0 121.50 3.34 3 -6 0 140.84 3.46 3 -6 0 118.72 3.44 3 -6 0 125.35 3.39 3 -6 0 131.12 3.39 3 -6 0 135.19 3.43 -3 6 0 126.50 3.45 -3 6 0 129.90 3.55 -3 6 0 117.08 3.48 -3 6 0 125.22 3.40 2 -6 0 197.23 5.13 2 -6 0 198.35 5.10 2 -6 0 197.32 5.21 2 -6 0 183.44 5.10 2 -6 0 204.32 5.16 2 -6 0 200.42 5.15 2 -6 0 184.02 5.08 -2 6 0 194.45 5.21 -2 6 0 180.49 5.10 -2 6 0 182.56 5.15 1 -6 0 219.65 5.60 1 -6 0 216.54 5.64 1 -6 0 227.18 5.65 1 -6 0 222.74 5.64 1 -6 0 213.25 5.62 1 -6 0 212.31 5.60 -1 6 0 200.42 5.60 -1 6 0 179.86 5.67 -1 6 0 203.92 5.65 -1 6 0 214.12 5.64 0 -6 0 15.88 0.56 0 -6 0 16.61 0.60 0 -6 0 15.61 0.57 0 -6 0 16.27 0.61 0 -6 0 16.39 0.56 0 -6 0 16.02 0.58 0 6 0 13.97 0.64 0 6 0 16.04 0.47 0 6 0 15.40 0.46 -1 -6 0 118.40 3.17 -1 -6 0 116.85 3.20 -1 -6 0 117.81 3.21 -1 -6 0 117.81 3.18 -1 -6 0 117.91 3.21 -1 -6 0 116.87 3.18 -2 -6 0 16.02 0.62 -2 -6 0 16.59 0.63 -2 -6 0 16.62 0.65 -2 -6 0 16.99 0.64 -2 -6 0 16.80 0.62 -2 -6 0 16.58 0.64 -2 -6 0 16.25 0.68 -3 -6 0 115.93 3.26 -3 -6 0 116.43 3.24 -3 -6 0 118.89 3.24 -3 -6 0 121.36 3.24 -3 -6 0 120.61 3.26 -3 -6 0 118.15 3.30 -3 -6 0 122.75 3.25 -4 -6 0 7.44 0.51 -4 -6 0 6.17 0.49 -4 -6 0 7.49 0.49 -4 -6 0 8.25 0.51 -4 -6 0 8.39 0.56 -4 -6 0 4.90 0.55 -4 -6 0 6.27 0.65 -5 -6 0 27.27 0.94 -5 -6 0 26.65 0.93 -5 -6 0 26.97 0.96 -5 -6 0 27.08 0.92 -5 -6 0 26.85 0.92 -5 -6 0 25.27 1.02 -6 -6 0 22.42 0.82 -6 -6 0 21.52 0.84 -6 -6 0 22.12 1.02 -6 -6 0 22.97 0.72 -6 -6 0 22.42 0.92 -6 -6 0 22.11 0.88 -7 -6 0 15.91 0.85 -7 -6 0 15.10 0.64 -7 -6 0 15.90 0.67 -7 -6 0 14.95 0.68 -7 -6 0 15.86 1.02 -7 -6 0 15.33 0.80 -7 -6 0 14.61 0.73 -8 -6 0 66.44 2.01 -8 -6 0 65.94 2.17 -8 -6 0 65.27 1.92 -8 -6 0 64.31 1.92 -8 -6 0 64.26 1.85 -9 -6 0 12.27 0.95 -9 -6 0 13.03 0.75 -9 -6 0 12.31 0.55 -9 -6 0 12.07 1.10 -10 -6 0 39.61 1.80 -10 -6 0 40.67 1.51 -11 -6 0 0.34 0.60 -11 -6 0 0.83 1.32 -12 -6 0 24.88 1.72 -12 -6 0 27.23 1.38 -13 -6 0 0.07 0.95 -13 -6 0 0.17 0.70 18 -7 0 6.78 0.94 18 -7 0 6.95 0.87 -18 7 0 9.17 1.00 -18 7 0 6.03 1.01 -18 7 0 6.26 1.08 17 -7 0 -0.17 0.77 17 -7 0 1.55 0.73 -17 7 0 0.98 0.91 -17 7 0 1.59 0.98 -17 7 0 1.38 0.70 16 -7 0 28.66 1.11 16 -7 0 23.61 2.17 16 -7 0 28.36 1.47 -16 7 0 29.87 1.39 -16 7 0 30.24 1.61 -16 7 0 28.46 1.67 15 -7 0 0.61 0.41 15 -7 0 0.37 0.59 15 -7 0 0.02 0.71 -15 7 0 0.76 0.79 -15 7 0 -0.43 0.77 -15 7 0 -0.08 0.54 14 -7 0 62.41 1.94 14 -7 0 62.70 2.20 14 -7 0 67.90 1.96 14 -7 0 61.33 2.06 -14 7 0 64.02 2.25 -14 7 0 61.80 2.25 13 -7 0 0.01 0.39 13 -7 0 -0.05 0.32 13 -7 0 -0.64 0.60 13 -7 0 0.07 0.73 13 -7 0 -0.09 0.51 -13 7 0 0.52 0.66 -13 7 0 -0.57 0.38 -13 7 0 0.30 1.13 -13 7 0 1.05 0.65 12 -7 0 59.66 1.93 12 -7 0 60.76 1.87 12 -7 0 60.42 1.77 12 -7 0 56.51 2.40 12 -7 0 59.82 1.80 -12 7 0 58.64 1.76 -12 7 0 58.92 2.03 -12 7 0 59.43 3.23 -12 7 0 56.73 1.95 11 -7 0 0.24 0.39 11 -7 0 0.40 0.50 11 -7 0 0.45 0.58 11 -7 0 1.25 0.33 11 -7 0 0.31 0.36 -11 7 0 1.54 0.58 -11 7 0 1.48 0.35 -11 7 0 2.09 0.65 -11 7 0 1.87 0.30 -11 7 0 1.77 0.41 -11 7 0 2.82 0.54 10 -7 0 42.35 1.49 10 -7 0 43.44 1.35 10 -7 0 41.11 1.37 10 -7 0 42.70 1.41 10 -7 0 43.23 1.37 10 -7 0 44.30 1.83 -10 7 0 43.57 1.36 -10 7 0 45.02 1.84 -10 7 0 40.93 1.49 -10 7 0 43.21 1.38 -10 7 0 40.65 1.48 -10 7 0 43.81 1.27 9 -7 0 11.50 1.01 9 -7 0 11.60 0.65 9 -7 0 11.31 0.66 9 -7 0 11.40 0.66 9 -7 0 10.83 0.74 9 -7 0 11.03 0.75 9 -7 0 11.91 0.62 -9 7 0 12.46 0.73 -9 7 0 11.94 0.80 -9 7 0 12.97 0.65 -9 7 0 12.98 1.04 -9 7 0 12.12 0.66 -9 7 0 12.40 0.75 -9 7 0 12.22 0.50 8 -7 0 48.69 1.49 8 -7 0 49.78 1.53 8 -7 0 51.66 1.48 8 -7 0 50.16 1.84 8 -7 0 48.84 1.46 8 -7 0 47.40 1.53 8 -7 0 51.44 1.48 -8 7 0 48.96 1.36 -8 7 0 48.31 1.37 -8 7 0 47.88 1.83 -8 7 0 47.35 1.51 -8 7 0 50.64 1.50 -8 7 0 50.63 1.52 -8 7 0 48.58 1.46 -8 7 0 48.27 1.56 7 -7 0 75.08 2.12 7 -7 0 76.73 2.42 7 -7 0 71.42 2.14 7 -7 0 73.95 2.13 7 -7 0 76.10 2.09 7 -7 0 73.45 2.07 7 -7 0 75.58 2.10 -7 7 0 72.37 2.11 -7 7 0 71.77 2.16 -7 7 0 71.37 2.12 -7 7 0 72.53 1.97 -7 7 0 75.05 1.98 -7 7 0 74.68 2.08 -7 7 0 76.56 2.42 -7 7 0 75.21 2.13 6 -7 0 43.21 1.19 6 -7 0 41.18 1.24 6 -7 0 42.54 1.49 6 -7 0 41.44 1.22 6 -7 0 39.37 1.24 6 -7 0 35.20 1.24 -6 7 0 40.44 1.23 -6 7 0 34.73 1.26 -6 7 0 38.58 1.24 -6 7 0 40.82 1.48 -6 7 0 40.27 1.17 -6 7 0 39.52 1.27 5 -7 0 205.81 5.32 5 -7 0 196.12 5.31 5 -7 0 203.13 5.32 5 -7 0 193.29 5.31 5 -7 0 197.52 5.27 5 -7 0 201.25 5.52 -5 7 0 204.71 5.31 -5 7 0 193.89 5.51 -5 7 0 189.61 5.33 -5 7 0 197.68 5.33 -5 7 0 191.27 5.28 4 -7 0 6.34 0.54 4 -7 0 5.46 0.35 4 -7 0 5.33 0.44 -4 7 0 5.72 0.46 -4 7 0 5.74 0.34 -4 7 0 6.39 0.36 3 -7 0 185.92 4.92 3 -7 0 173.12 4.75 3 -7 0 177.90 4.79 3 -7 0 190.50 4.82 3 -7 0 182.32 4.75 3 -7 0 192.93 4.83 3 -7 0 168.26 4.71 3 -7 0 183.58 4.79 3 -7 0 168.52 4.71 -3 7 0 168.04 4.76 -3 7 0 177.86 4.91 -3 7 0 180.04 4.81 -3 7 0 173.82 4.82 2 -7 0 16.04 0.53 2 -7 0 15.81 0.63 2 -7 0 16.51 0.62 2 -7 0 16.05 0.51 2 -7 0 14.96 0.63 2 -7 0 14.42 0.61 2 -7 0 16.04 0.55 -2 7 0 16.18 0.61 -2 7 0 14.01 0.66 -2 7 0 14.13 0.61 -2 7 0 15.36 0.55 1 -7 0 157.92 4.11 1 -7 0 158.14 4.10 1 -7 0 154.38 4.05 1 -7 0 155.53 4.07 -1 7 0 146.75 4.08 -1 7 0 147.72 4.08 -1 7 0 145.35 4.10 -1 7 0 144.74 4.05 0 -7 0 17.66 0.63 0 -7 0 17.02 0.68 0 -7 0 18.39 0.66 0 -7 0 18.31 0.70 0 -7 0 17.77 0.66 0 -7 0 18.45 0.62 0 7 0 17.84 0.68 -1 -7 0 20.41 0.74 -1 -7 0 21.36 0.78 -1 -7 0 22.09 0.74 -1 -7 0 20.85 0.76 -1 -7 0 21.61 0.78 -1 -7 0 21.59 0.75 -2 -7 0 73.64 2.09 -2 -7 0 73.97 2.06 -2 -7 0 70.77 2.10 -2 -7 0 75.74 2.06 -2 -7 0 72.78 2.05 -2 -7 0 72.89 2.05 -2 -7 0 70.24 2.06 -3 -7 0 5.79 0.51 -3 -7 0 6.30 0.53 -3 -7 0 6.41 0.51 -3 -7 0 4.99 0.51 -3 -7 0 5.40 0.45 -3 -7 0 5.64 0.54 -3 -7 0 5.25 0.49 -4 -7 0 43.43 1.33 -4 -7 0 39.66 1.43 -4 -7 0 42.88 1.34 -4 -7 0 43.97 1.35 -4 -7 0 43.34 1.32 -4 -7 0 42.45 1.36 -4 -7 0 42.93 1.38 -5 -7 0 8.23 0.62 -5 -7 0 7.88 0.61 -5 -7 0 8.48 0.61 -5 -7 0 7.62 0.76 -5 -7 0 9.33 0.68 -6 -7 0 89.65 2.59 -6 -7 0 93.06 2.61 -6 -7 0 92.52 2.58 -6 -7 0 89.92 2.70 -6 -7 0 92.28 2.62 -7 -7 0 0.69 0.51 -7 -7 0 0.26 0.33 -7 -7 0 0.17 0.45 -7 -7 0 0.25 0.56 -7 -7 0 0.39 0.34 -7 -7 0 0.67 0.40 -8 -7 0 100.42 2.84 -8 -7 0 86.10 2.44 -8 -7 0 86.43 2.58 -8 -7 0 82.02 2.54 -8 -7 0 83.42 2.74 -9 -7 0 1.16 0.72 -9 -7 0 1.16 0.56 -10 -7 0 39.60 1.53 -10 -7 0 38.28 1.85 -11 -7 0 5.18 0.70 -11 -7 0 5.22 0.92 -12 -7 0 9.47 1.08 -12 -7 0 11.42 1.16 18 -8 0 17.44 1.40 18 -8 0 17.10 1.45 -18 8 0 16.06 1.63 -18 8 0 14.63 1.32 -18 8 0 13.63 1.24 17 -8 0 1.90 0.99 17 -8 0 1.90 0.82 17 -8 0 1.96 0.59 -17 8 0 1.63 0.91 -17 8 0 1.69 0.65 -17 8 0 2.00 0.92 16 -8 0 39.56 1.42 16 -8 0 40.05 1.67 -16 8 0 43.18 1.92 -16 8 0 38.55 1.57 -16 8 0 39.46 1.92 15 -8 0 5.31 0.68 15 -8 0 4.47 0.52 15 -8 0 4.10 0.79 -15 8 0 4.80 0.58 -15 8 0 5.20 0.85 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89.74 3.06 9 -8 0 88.65 2.56 9 -8 0 91.00 2.55 9 -8 0 88.49 2.62 9 -8 0 90.99 2.55 9 -8 0 93.51 2.74 -9 8 0 94.83 2.82 -9 8 0 85.76 2.58 -9 8 0 90.49 2.96 -9 8 0 90.48 2.42 -9 8 0 89.41 2.67 -9 8 0 87.84 2.56 -9 8 0 87.84 2.53 -9 8 0 87.85 2.42 8 -8 0 0.54 0.41 8 -8 0 0.35 0.35 8 -8 0 0.89 0.44 8 -8 0 0.40 0.29 8 -8 0 1.02 0.29 8 -8 0 0.44 0.31 8 -8 0 0.83 0.35 -8 8 0 0.75 0.44 -8 8 0 0.60 0.37 -8 8 0 0.08 0.35 -8 8 0 0.22 0.26 -8 8 0 0.56 0.46 -8 8 0 0.75 0.33 7 -8 0 75.51 2.24 7 -8 0 75.41 2.20 7 -8 0 80.17 2.22 7 -8 0 79.25 2.16 7 -8 0 76.71 2.51 7 -8 0 77.44 2.15 7 -8 0 76.72 2.20 -7 8 0 75.56 2.15 -7 8 0 78.93 2.23 -7 8 0 76.45 2.27 -7 8 0 76.48 2.18 -7 8 0 77.19 2.50 -7 8 0 72.53 2.21 6 -8 0 9.03 0.61 6 -8 0 8.99 0.52 6 -8 0 9.99 0.49 6 -8 0 9.54 0.60 6 -8 0 10.69 0.79 6 -8 0 10.17 0.59 -6 8 0 9.10 0.67 -6 8 0 10.24 0.47 -6 8 0 8.70 0.74 -6 8 0 9.44 0.57 -6 8 0 9.04 0.53 -6 8 0 9.38 0.64 5 -8 0 121.24 3.31 5 -8 0 117.83 3.49 5 -8 0 122.98 3.24 5 -8 0 117.94 3.30 5 -8 0 121.97 3.30 -5 8 0 117.71 3.32 -5 8 0 116.58 3.32 -5 8 0 122.20 3.24 -5 8 0 119.41 3.50 4 -8 0 43.60 1.32 4 -8 0 44.19 1.47 4 -8 0 38.22 1.30 4 -8 0 45.72 1.34 4 -8 0 44.78 1.32 4 -8 0 45.09 1.33 4 -8 0 41.18 1.28 -4 8 0 43.63 1.35 -4 8 0 44.89 1.46 -4 8 0 41.71 1.26 -4 8 0 43.21 1.39 3 -8 0 129.65 3.45 3 -8 0 121.16 3.32 3 -8 0 123.98 3.41 3 -8 0 127.30 3.53 3 -8 0 124.42 3.32 3 -8 0 116.53 3.40 3 -8 0 131.62 3.42 3 -8 0 130.96 3.44 -3 8 0 126.99 3.53 -3 8 0 118.45 3.37 -3 8 0 125.49 3.43 -3 8 0 124.62 3.46 2 -8 0 141.19 3.63 2 -8 0 128.96 3.61 2 -8 0 128.20 3.56 2 -8 0 137.15 3.60 2 -8 0 134.43 3.54 2 -8 0 131.76 3.66 2 -8 0 141.86 3.65 2 -8 0 134.79 3.55 -2 8 0 132.54 3.62 -2 8 0 120.89 3.57 -2 8 0 129.34 3.65 -2 8 0 126.99 3.65 1 -8 0 44.95 1.30 1 -8 0 43.92 1.26 1 -8 0 41.43 1.36 1 -8 0 45.56 1.35 1 -8 0 43.99 1.28 1 -8 0 44.86 1.35 -1 8 0 41.67 1.36 -1 8 0 43.59 1.27 -1 8 0 42.90 1.33 -1 8 0 42.24 1.25 0 -8 0 79.89 2.22 0 -8 0 80.31 2.23 0 -8 0 80.64 2.25 0 -8 0 78.42 2.20 0 -8 0 78.29 2.20 0 -8 0 79.10 2.27 -1 -8 0 28.55 0.91 -1 -8 0 27.87 0.96 -1 -8 0 26.02 0.95 -1 -8 0 26.83 0.98 -1 -8 0 26.39 0.91 -1 -8 0 27.02 0.91 -2 -8 0 185.71 5.11 -2 -8 0 189.45 5.09 -2 -8 0 194.27 5.10 -2 -8 0 184.20 5.14 -2 -8 0 187.39 5.08 -2 -8 0 191.74 5.10 -2 -8 0 189.27 5.13 -3 -8 0 0.91 0.35 -3 -8 0 0.21 0.39 -3 -8 0 -0.01 0.34 -3 -8 0 0.47 0.33 -3 -8 0 -0.29 0.34 -3 -8 0 0.28 0.32 -3 -8 0 0.95 0.34 -4 -8 0 99.40 2.86 -4 -8 0 102.02 2.84 -4 -8 0 103.51 2.91 -4 -8 0 99.99 2.85 -5 -8 0 18.33 0.89 -5 -8 0 19.72 0.90 -5 -8 0 20.58 1.05 -5 -8 0 18.96 0.89 -5 -8 0 20.85 0.89 -6 -8 0 40.88 1.42 -6 -8 0 41.01 1.55 -6 -8 0 40.55 1.36 -7 -8 0 18.60 0.85 -7 -8 0 18.26 1.00 -7 -8 0 18.67 1.19 -8 -8 0 14.09 1.21 -8 -8 0 16.66 0.79 -8 -8 0 14.40 0.99 -9 -8 0 8.66 0.97 -9 -8 0 10.75 0.97 -9 -8 0 9.67 0.76 -10 -8 0 3.72 0.86 -10 -8 0 2.68 0.65 -11 -8 0 14.16 1.21 -11 -8 0 13.86 1.57 18 -9 0 9.02 1.03 18 -9 0 8.59 0.88 -18 9 0 7.94 1.09 -18 9 0 11.09 1.16 -18 9 0 11.79 1.16 17 -9 0 18.76 1.03 17 -9 0 19.65 1.55 -17 9 0 16.61 1.17 -17 9 0 21.38 1.69 -17 9 0 16.61 1.57 16 -9 0 17.29 1.20 16 -9 0 13.85 0.98 -16 9 0 14.39 1.03 -16 9 0 15.59 1.52 -16 9 0 18.70 1.66 15 -9 0 37.13 1.51 15 -9 0 35.44 1.70 15 -9 0 37.01 1.39 -15 9 0 37.20 1.37 -15 9 0 40.15 1.81 -15 9 0 35.77 1.75 14 -9 0 0.17 0.52 14 -9 0 -0.10 0.67 14 -9 0 -0.06 0.46 -14 9 0 0.07 0.39 -14 9 0 0.02 0.75 -14 9 0 -0.25 0.65 -14 9 0 1.21 0.87 13 -9 0 33.80 1.29 13 -9 0 35.88 1.33 13 -9 0 33.62 2.01 13 -9 0 36.81 1.54 13 -9 0 35.97 1.33 -13 9 0 34.35 1.16 -13 9 0 35.25 1.52 -13 9 0 38.31 2.03 -13 9 0 35.34 1.53 -13 9 0 34.19 1.19 12 -9 0 0.50 0.46 12 -9 0 1.00 0.57 12 -9 0 0.78 0.43 12 -9 0 0.00 0.70 12 -9 0 0.15 0.38 -12 9 0 1.12 0.43 -12 9 0 1.64 0.59 -12 9 0 1.57 0.29 -12 9 0 2.15 0.67 -12 9 0 1.20 0.71 11 -9 0 63.06 1.97 11 -9 0 64.66 2.06 11 -9 0 65.29 1.96 11 -9 0 65.29 2.54 11 -9 0 66.49 2.00 -11 9 0 65.85 2.13 -11 9 0 65.85 2.00 -11 9 0 65.08 2.07 -11 9 0 63.24 2.48 -11 9 0 66.06 1.98 -11 9 0 68.25 1.82 -11 9 0 63.63 1.82 10 -9 0 26.56 1.06 10 -9 0 25.83 1.46 10 -9 0 25.48 1.00 10 -9 0 26.19 1.01 10 -9 0 23.82 1.10 10 -9 0 25.69 0.98 -10 9 0 25.18 0.99 -10 9 0 26.69 0.76 -10 9 0 24.92 1.05 -10 9 0 24.78 1.44 -10 9 0 25.24 0.75 -10 9 0 24.45 1.08 -10 9 0 25.07 1.16 9 -9 0 98.44 2.76 9 -9 0 100.80 2.80 9 -9 0 95.66 2.79 9 -9 0 101.33 2.75 9 -9 0 99.06 3.18 9 -9 0 96.11 2.85 -9 9 0 98.02 2.83 -9 9 0 99.18 2.76 -9 9 0 99.08 3.21 -9 9 0 97.58 2.80 -9 9 0 94.81 2.87 8 -9 0 109.42 2.94 8 -9 0 105.99 2.93 8 -9 0 103.70 3.01 8 -9 0 104.92 3.01 8 -9 0 106.58 3.33 8 -9 0 103.94 2.99 8 -9 0 114.04 3.14 -8 9 0 102.83 3.32 -8 9 0 104.92 2.96 -8 9 0 102.97 3.06 -8 9 0 104.55 3.02 -8 9 0 107.40 3.03 -8 9 0 106.25 2.93 7 -9 0 25.26 0.99 7 -9 0 25.45 1.01 7 -9 0 26.72 0.90 7 -9 0 26.29 0.96 7 -9 0 25.26 0.98 7 -9 0 27.20 0.89 7 -9 0 25.70 1.25 -7 9 0 25.14 1.04 -7 9 0 25.71 0.93 -7 9 0 26.17 0.88 -7 9 0 25.52 1.02 -7 9 0 26.23 1.23 -7 9 0 26.02 1.02 6 -9 0 92.93 2.59 6 -9 0 92.84 2.90 6 -9 0 96.09 2.59 6 -9 0 95.34 2.67 6 -9 0 92.45 2.67 6 -9 0 97.26 2.68 -6 9 0 96.50 2.58 -6 9 0 92.89 2.90 -6 9 0 93.43 2.60 -6 9 0 92.60 2.70 -6 9 0 90.63 2.71 5 -9 0 19.62 0.86 5 -9 0 21.44 0.71 5 -9 0 21.57 0.85 5 -9 0 21.98 0.86 5 -9 0 20.81 0.99 5 -9 0 21.68 0.83 5 -9 0 18.74 0.73 -5 9 0 19.42 0.89 -5 9 0 19.00 0.74 -5 9 0 20.64 0.85 -5 9 0 20.73 0.96 4 -9 0 60.32 1.77 4 -9 0 58.71 1.59 4 -9 0 63.09 1.75 4 -9 0 63.41 1.80 4 -9 0 59.34 1.69 4 -9 0 58.18 1.59 4 -9 0 62.39 1.68 4 -9 0 58.12 1.76 4 -9 0 61.45 1.90 -4 9 0 58.79 1.77 -4 9 0 60.82 1.90 -4 9 0 60.07 1.84 -4 9 0 52.33 1.75 3 -9 0 6.63 0.54 3 -9 0 6.60 0.41 3 -9 0 7.71 0.53 3 -9 0 7.67 0.54 3 -9 0 7.35 0.33 3 -9 0 6.98 0.56 3 -9 0 8.18 0.57 3 -9 0 6.64 0.46 3 -9 0 7.96 0.34 -3 9 0 6.47 0.62 -3 9 0 6.53 0.70 -3 9 0 6.45 0.51 -3 9 0 5.50 0.48 2 -9 0 88.88 2.46 2 -9 0 83.27 2.37 2 -9 0 86.40 2.41 2 -9 0 85.79 2.43 2 -9 0 86.17 2.43 2 -9 0 86.48 2.44 2 -9 0 87.12 2.35 2 -9 0 88.60 2.35 -2 9 0 84.30 2.43 -2 9 0 83.96 2.37 -2 9 0 83.65 2.42 -2 9 0 84.25 2.47 1 -9 0 3.03 0.31 1 -9 0 2.84 0.38 1 -9 0 3.37 0.33 1 -9 0 3.08 0.28 1 -9 0 3.88 0.42 1 -9 0 3.59 0.39 1 -9 0 3.68 0.39 -1 9 0 3.96 0.25 -1 9 0 3.43 0.38 0 -9 0 72.45 2.14 0 -9 0 74.37 2.08 0 -9 0 73.03 2.10 0 -9 0 74.60 2.08 0 -9 0 73.97 2.11 0 -9 0 74.42 2.16 -1 -9 0 13.67 0.67 -1 -9 0 13.31 0.78 -1 -9 0 12.58 0.72 -1 -9 0 12.66 0.63 -1 -9 0 12.64 0.75 -1 -9 0 12.43 0.66 -2 -9 0 102.01 2.92 -2 -9 0 103.01 2.92 -2 -9 0 103.53 2.87 -2 -9 0 101.40 2.87 -2 -9 0 99.55 2.92 -2 -9 0 105.50 2.87 -3 -9 0 65.21 1.98 -3 -9 0 67.03 1.95 -3 -9 0 65.35 1.99 -4 -9 0 26.95 1.11 -4 -9 0 28.12 1.06 -5 -9 0 74.48 2.30 -5 -9 0 77.18 2.39 -5 -9 0 80.08 2.30 -6 -9 0 0.36 0.58 -6 -9 0 -0.28 0.47 -7 -9 0 32.81 1.32 -7 -9 0 33.52 1.54 -7 -9 0 33.15 1.21 -8 -9 0 3.74 0.46 -8 -9 0 4.10 0.81 -8 -9 0 4.47 0.63 -9 -9 0 7.19 0.95 -9 -9 0 10.94 1.02 -10 -9 0 4.68 0.96 -10 -9 0 5.44 0.74 18 -10 0 -1.05 0.68 18 -10 0 -0.66 0.85 -18 10 0 0.53 1.01 -18 10 0 -0.93 0.96 17 -10 0 29.03 1.63 17 -10 0 29.46 1.33 17 -10 0 25.46 2.03 -17 10 0 33.16 1.89 -17 10 0 33.04 1.85 -17 10 0 30.71 1.30 16 -10 0 2.28 0.55 16 -10 0 2.46 0.80 16 -10 0 2.27 0.62 -16 10 0 2.43 0.89 -16 10 0 2.39 0.49 15 -10 0 12.33 0.99 15 -10 0 13.43 1.20 15 -10 0 13.85 1.06 -15 10 0 14.11 1.42 -15 10 0 13.52 0.81 -15 10 0 12.73 1.31 14 -10 0 5.88 1.80 14 -10 0 3.66 0.58 14 -10 0 3.21 0.54 14 -10 0 2.92 0.71 -14 10 0 2.09 0.73 -14 10 0 3.50 0.38 -14 10 0 3.04 0.84 -14 10 0 2.62 0.99 13 -10 0 25.45 1.15 13 -10 0 25.71 1.11 13 -10 0 24.19 1.34 13 -10 0 25.98 1.88 -13 10 0 21.25 1.76 -13 10 0 25.37 1.06 -13 10 0 24.47 1.29 -13 10 0 26.69 1.47 12 -10 0 32.67 1.22 12 -10 0 33.15 1.87 12 -10 0 32.76 1.45 12 -10 0 32.24 1.29 -12 10 0 32.13 1.38 -12 10 0 32.32 0.97 -12 10 0 31.35 0.96 -12 10 0 33.01 1.29 -12 10 0 30.42 1.85 -12 10 0 31.62 1.45 11 -10 0 22.18 0.98 11 -10 0 22.04 1.55 11 -10 0 19.83 1.11 11 -10 0 22.01 1.06 -11 10 0 22.83 1.09 -11 10 0 23.98 1.10 -11 10 0 23.72 1.21 -11 10 0 24.49 1.00 -11 10 0 22.56 1.48 10 -10 0 85.80 2.60 10 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1.11 -1 -11 0 30.12 1.22 -4 -11 0 20.15 1.14 -5 -11 0 3.51 0.69 -5 -11 0 2.19 0.58 -6 -11 0 15.47 1.06 -6 -11 0 15.56 1.24 -7 -11 0 -0.25 0.94 -7 -11 0 0.12 0.60 -7 -11 0 -0.28 0.53 -8 -11 0 32.11 1.46 -8 -11 0 32.06 1.91 -8 -11 0 31.08 1.76 18 -12 0 11.51 1.24 18 -12 0 10.33 1.06 18 -12 0 11.71 0.93 -18 12 0 11.11 1.13 -18 12 0 11.63 1.24 17 -12 0 1.12 0.74 17 -12 0 0.90 0.85 17 -12 0 1.34 0.65 -17 12 0 1.27 1.01 -17 12 0 0.59 0.87 16 -12 0 31.15 1.41 16 -12 0 29.98 1.44 16 -12 0 31.22 1.62 -16 12 0 30.19 1.70 -16 12 0 31.68 1.89 15 -12 0 11.05 1.09 15 -12 0 12.00 1.02 15 -12 0 8.78 1.41 -15 12 0 10.97 1.28 14 -12 0 34.11 1.56 14 -12 0 31.99 1.44 14 -12 0 31.44 1.32 -14 12 0 32.17 1.54 -14 12 0 33.25 1.77 13 -12 0 29.32 1.44 13 -12 0 28.24 1.34 13 -12 0 31.13 1.22 13 -12 0 29.21 2.15 -13 12 0 28.42 1.65 -13 12 0 29.72 1.40 12 -12 0 19.71 0.98 12 -12 0 18.63 1.19 12 -12 0 19.49 1.77 12 -12 0 18.40 1.16 -12 12 0 19.18 1.14 -12 12 0 19.30 1.31 11 -12 0 22.31 1.30 11 -12 0 23.46 1.23 11 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92.07 2.87 5 -12 0 93.44 2.73 5 -12 0 95.92 2.61 5 -12 0 95.16 2.63 -5 12 0 93.17 2.87 -5 12 0 92.53 2.63 -5 12 0 93.40 2.77 4 -12 0 26.70 1.11 4 -12 0 27.19 0.97 4 -12 0 26.35 0.78 4 -12 0 26.16 0.91 4 -12 0 25.80 0.77 4 -12 0 25.40 1.14 -4 12 0 27.18 0.97 -4 12 0 25.52 1.08 -4 12 0 26.86 1.18 3 -12 0 65.20 1.84 3 -12 0 65.47 1.92 3 -12 0 66.84 2.04 3 -12 0 64.71 1.87 -3 12 0 65.91 2.05 -3 12 0 65.32 1.96 -3 12 0 63.30 1.94 2 -12 0 63.47 1.91 2 -12 0 67.19 1.86 2 -12 0 64.74 2.03 2 -12 0 62.34 1.87 2 -12 0 64.84 1.87 2 -12 0 65.12 1.91 -2 12 0 66.39 2.04 1 -12 0 23.44 0.97 1 -12 0 26.81 1.15 1 -12 0 24.26 0.94 1 -12 0 27.29 1.03 1 -12 0 25.88 0.96 0 -12 0 67.63 1.96 0 -12 0 62.97 1.91 0 -12 0 62.09 1.96 0 -12 0 64.38 1.95 -1 -12 0 5.43 0.55 -4 -12 0 17.95 1.16 -5 -12 0 6.01 0.83 -5 -12 0 6.41 0.66 -5 -12 0 8.86 0.83 -6 -12 0 22.94 1.26 -6 -12 0 25.41 1.61 -6 -12 0 22.49 1.46 -6 -12 0 24.19 1.28 -7 -12 0 8.84 1.02 -7 -12 0 8.78 0.93 18 -13 0 7.80 1.06 18 -13 0 10.93 1.20 -18 13 0 9.19 1.10 17 -13 0 7.86 0.80 17 -13 0 7.46 0.97 17 -13 0 7.51 0.85 -17 13 0 8.45 1.19 -17 13 0 6.98 0.96 16 -13 0 19.77 1.50 16 -13 0 21.95 1.36 16 -13 0 22.39 1.24 -16 13 0 23.42 1.57 -16 13 0 23.69 1.77 15 -13 0 36.16 1.73 15 -13 0 36.28 1.63 15 -13 0 38.60 1.47 -15 13 0 38.27 1.90 -15 13 0 36.04 1.72 14 -13 0 2.23 1.33 14 -13 0 4.65 0.74 14 -13 0 3.69 0.56 -14 13 0 4.48 0.74 13 -13 0 33.96 1.57 13 -13 0 34.15 1.49 13 -13 0 34.25 1.32 -13 13 0 35.00 1.50 -13 13 0 33.01 1.70 12 -13 0 0.21 0.43 12 -13 0 0.25 0.63 12 -13 0 0.10 0.68 -12 13 0 0.43 0.55 -12 13 0 0.26 0.78 11 -13 0 44.36 1.81 11 -13 0 45.82 1.53 11 -13 0 45.99 1.75 -11 13 0 48.63 1.65 -11 13 0 48.49 1.87 10 -13 0 -0.16 0.62 10 -13 0 0.04 0.39 10 -13 0 0.31 0.60 -10 13 0 0.88 0.41 -10 13 0 -0.12 0.68 -10 13 0 0.65 0.46 9 -13 0 21.81 1.16 9 -13 0 20.60 0.92 9 -13 0 21.06 0.92 9 -13 0 21.33 1.14 -9 13 0 21.43 1.33 -9 13 0 21.58 0.98 -9 13 0 20.39 1.20 8 -13 0 43.89 1.61 8 -13 0 42.58 1.71 8 -13 0 46.39 1.43 8 -13 0 45.92 1.44 -8 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1.17 -4 -13 0 15.96 1.25 -5 -13 0 44.90 1.87 -5 -13 0 49.17 1.76 -5 -13 0 43.32 1.94 -6 -13 0 0.69 0.84 -6 -13 0 0.28 0.69 -6 -13 0 0.17 0.67 -6 -13 0 0.77 0.79 17 -14 0 15.27 1.59 17 -14 0 12.72 1.42 17 -14 0 19.36 2.04 -17 14 0 16.13 1.81 -17 14 0 17.34 1.52 16 -14 0 0.05 0.89 16 -14 0 -0.47 0.57 16 -14 0 -0.21 0.83 -16 14 0 0.20 0.81 -16 14 0 -0.45 1.02 15 -14 0 18.35 1.13 15 -14 0 17.23 1.42 15 -14 0 19.40 1.37 -15 14 0 20.27 1.38 -15 14 0 17.15 1.72 14 -14 0 0.55 0.78 14 -14 0 0.35 0.52 14 -14 0 0.28 0.72 -14 14 0 0.94 0.95 -14 14 0 1.10 0.68 13 -14 0 14.47 1.23 13 -14 0 9.04 1.10 13 -14 0 13.33 0.93 -13 14 0 14.20 1.09 -13 14 0 9.83 1.69 12 -14 0 6.44 0.55 12 -14 0 6.60 0.81 12 -14 0 7.37 0.80 -12 14 0 6.61 0.93 -12 14 0 8.33 0.97 11 -14 0 24.25 1.05 11 -14 0 24.39 1.39 11 -14 0 23.02 1.32 -11 14 0 25.26 1.46 -11 14 0 24.81 1.18 10 -14 0 37.98 1.34 10 -14 0 38.14 1.67 10 -14 0 37.37 1.64 -10 14 0 39.04 1.42 -10 14 0 40.49 1.69 9 -14 0 1.35 0.40 9 -14 0 1.64 0.42 9 -14 0 1.50 0.66 9 -14 0 1.71 0.69 -9 14 0 1.52 0.76 -9 14 0 2.32 0.47 8 -14 0 84.00 2.42 8 -14 0 84.57 2.44 8 -14 0 84.03 2.65 8 -14 0 83.45 2.70 -8 14 0 85.54 2.72 -8 14 0 83.50 2.46 7 -14 0 -0.23 0.61 7 -14 0 0.40 0.34 7 -14 0 0.08 0.39 -7 14 0 -0.26 0.39 -7 14 0 -0.83 0.64 6 -14 0 64.50 1.91 6 -14 0 63.89 2.14 6 -14 0 65.31 1.94 -6 14 0 65.77 1.95 -6 14 0 64.47 2.19 5 -14 0 6.31 0.59 5 -14 0 5.93 0.49 5 -14 0 6.19 0.69 -5 14 0 6.30 0.71 -5 14 0 5.88 0.68 4 -14 0 33.38 0.97 4 -14 0 32.65 1.42 4 -14 0 32.18 0.95 4 -14 0 31.52 1.12 4 -14 0 33.24 1.19 -4 14 0 34.27 1.41 -4 14 0 32.33 1.22 3 -14 0 10.42 1.05 3 -14 0 10.84 0.57 3 -14 0 8.78 0.97 3 -14 0 10.13 0.79 3 -14 0 11.48 0.66 -3 14 0 11.00 1.00 2 -14 0 9.75 0.65 2 -14 0 9.41 0.79 2 -14 0 9.13 0.98 1 -14 0 15.15 0.95 1 -14 0 16.62 0.86 1 -14 0 15.88 1.15 0 -14 0 9.86 0.84 0 -14 0 6.82 0.62 0 -14 0 9.78 0.98 -1 -14 0 12.82 0.99 -1 -14 0 11.45 1.01 -2 -14 0 6.36 0.71 -2 -14 0 6.92 0.70 -3 -14 0 37.70 1.70 -4 -14 0 -0.18 0.66 -4 -14 0 -0.72 0.68 -4 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15 0 25.69 1.04 5 -15 0 29.44 1.15 5 -15 0 29.49 1.42 -5 15 0 28.39 1.45 4 -15 0 3.45 0.47 4 -15 0 2.62 0.66 4 -15 0 3.45 0.31 -4 15 0 3.11 0.66 3 -15 0 26.87 1.35 3 -15 0 23.76 1.09 3 -15 0 24.52 0.87 2 -15 0 1.09 0.50 2 -15 0 0.43 0.64 2 -15 0 0.73 0.36 1 -15 0 10.29 1.18 1 -15 0 10.39 0.92 1 -15 0 10.83 0.82 0 -15 0 3.57 0.56 0 -15 0 3.67 0.65 0 -15 0 3.18 0.77 -1 -15 0 14.73 1.09 -1 -15 0 14.21 1.15 -1 -15 0 12.59 1.44 -2 -15 0 1.38 0.74 -2 -15 0 2.16 0.66 -2 -15 0 0.15 0.64 -3 -15 0 21.54 1.55 -3 -15 0 21.92 1.42 -3 -15 0 23.41 1.41 16 -16 0 8.52 1.04 16 -16 0 9.64 1.03 16 -16 0 8.67 0.94 -16 16 0 12.14 1.34 -16 16 0 8.15 1.29 15 -16 0 1.67 0.55 15 -16 0 1.76 0.93 15 -16 0 1.57 0.82 -15 16 0 1.27 1.04 -15 16 0 1.44 0.76 14 -16 0 12.99 1.29 14 -16 0 12.19 0.98 14 -16 0 11.78 1.09 -14 16 0 13.79 1.27 -14 16 0 13.76 1.24 13 -16 0 10.09 1.01 13 -16 0 9.94 0.91 13 -16 0 12.02 1.37 -13 16 0 12.21 1.13 -13 16 0 10.54 1.20 12 -16 0 9.92 0.88 12 -16 0 10.68 0.97 12 -16 0 10.52 1.05 -12 16 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1.61 13 -17 0 28.19 1.22 13 -17 0 27.29 1.69 -13 17 0 28.50 1.40 -13 17 0 29.64 1.94 12 -17 0 0.37 0.87 12 -17 0 0.37 0.90 12 -17 0 0.22 0.48 -12 17 0 0.22 0.99 -12 17 0 1.04 0.59 11 -17 0 33.51 1.75 11 -17 0 31.27 1.27 11 -17 0 31.49 1.69 -11 17 0 31.67 1.95 -11 17 0 33.58 1.38 10 -17 0 -0.72 0.84 10 -17 0 -0.13 0.45 10 -17 0 -0.03 0.77 -10 17 0 -0.62 0.86 -10 17 0 0.41 0.50 9 -17 0 32.92 1.82 9 -17 0 32.14 1.65 9 -17 0 31.84 1.27 -9 17 0 36.22 1.85 -9 17 0 34.41 1.32 8 -17 0 7.58 1.02 8 -17 0 9.58 0.94 8 -17 0 9.89 0.86 -8 17 0 9.73 0.85 -8 17 0 8.26 0.95 7 -17 0 16.94 0.96 7 -17 0 14.88 1.35 7 -17 0 13.66 1.51 -7 17 0 17.55 1.57 6 -17 0 8.90 0.89 6 -17 0 8.50 1.01 6 -17 0 9.82 0.87 -6 17 0 6.02 1.37 5 -17 0 11.75 0.92 5 -17 0 9.44 0.91 -5 17 0 9.14 1.29 4 -17 0 38.50 1.47 4 -17 0 37.53 1.77 3 -17 0 0.19 0.74 3 -17 0 0.40 0.58 2 -17 0 32.27 1.66 2 -17 0 34.46 1.44 1 -17 0 1.44 0.80 13 -18 0 28.41 1.70 13 -18 0 27.87 1.70 -13 18 0 28.07 1.92 12 -18 0 0.98 0.89 12 -18 0 1.56 0.97 -12 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0.83 -5 4 -10 21.01 1.32 -5 4 -10 21.83 1.15 5 -4 10 20.82 0.91 5 -4 10 21.52 1.09 5 -4 10 17.90 1.26 5 -4 10 21.48 0.97 -6 4 -10 54.90 1.74 -6 4 -10 57.52 1.96 -6 4 -10 58.91 1.91 -6 4 -10 55.69 2.27 6 -4 10 55.78 2.23 6 -4 10 56.98 1.91 6 -4 10 56.77 1.83 6 -4 10 57.12 1.72 -7 4 -10 12.42 1.13 -7 4 -10 13.06 1.11 -7 4 -10 14.19 1.66 -7 4 -10 12.73 0.63 7 -4 10 11.92 0.99 7 -4 10 12.88 1.11 -8 4 -10 10.57 1.22 -8 4 -10 10.93 1.12 8 -4 10 8.89 0.94 8 -4 10 8.46 0.83 8 -4 10 9.48 0.82 8 -4 10 8.48 0.48 8 -4 10 9.88 0.50 -9 4 -10 25.39 1.48 -9 4 -10 25.43 1.53 9 -4 10 22.96 1.31 9 -4 10 23.50 1.35 -10 4 -10 2.61 0.83 -10 4 -10 2.99 0.89 10 -4 10 3.57 0.81 10 -4 10 0.82 0.86 -11 4 -10 19.21 1.62 -11 4 -10 22.48 1.64 11 -4 10 21.06 1.50 11 -4 10 19.72 1.44 -12 4 -10 3.81 1.00 -12 4 -10 2.18 1.01 12 -4 10 3.11 0.87 12 -4 10 3.35 1.03 -13 4 -10 25.48 1.91 -13 4 -10 21.93 1.87 13 -4 10 23.87 1.64 16 3 -10 6.10 0.93 -16 -3 10 4.21 0.67 -16 -3 10 5.73 1.07 -16 -3 10 4.60 1.06 15 3 -10 19.45 1.45 -15 -3 10 17.24 1.71 -15 -3 10 18.80 1.60 -15 -3 10 19.25 1.22 14 3 -10 0.41 0.82 -14 -3 10 1.17 1.13 -14 -3 10 0.29 1.17 -14 -3 10 0.54 0.63 13 3 -10 39.01 1.69 13 3 -10 38.22 1.66 -13 -3 10 37.28 1.62 -13 -3 10 36.82 1.52 -13 -3 10 35.49 1.78 12 3 -10 1.28 0.60 12 3 -10 0.95 0.67 -12 -3 10 1.64 0.30 -12 -3 10 0.90 0.76 -12 -3 10 1.15 0.61 11 3 -10 31.78 1.50 11 3 -10 30.07 1.34 -11 -3 10 32.20 1.37 -11 -3 10 31.75 1.42 10 3 -10 25.66 1.18 10 3 -10 27.11 1.25 -10 -3 10 25.94 1.33 -10 -3 10 26.79 1.18 -10 -3 10 23.15 1.49 -10 -3 10 21.26 1.73 9 3 -10 111.34 3.22 9 3 -10 114.02 3.29 -9 -3 10 107.72 3.57 -9 -3 10 116.47 3.58 -9 -3 10 109.49 3.24 -9 -3 10 114.28 3.25 -9 -3 10 110.01 2.96 8 3 -10 17.77 0.61 8 3 -10 16.50 0.91 8 3 -10 17.11 0.98 -8 -3 10 16.40 1.16 -8 -3 10 18.15 1.04 -8 -3 10 17.29 0.59 -8 -3 10 17.10 1.03 -8 -3 10 16.34 0.88 -8 -3 10 19.27 1.17 7 3 -10 29.73 1.17 7 3 -10 31.45 1.22 7 3 -10 35.22 1.51 -7 -3 10 31.59 1.27 -7 -3 10 31.27 1.11 -7 -3 10 31.08 1.42 -7 -3 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1.13 5 8 -20 8.47 1.11 5 8 -20 5.66 0.84 -5 -8 20 6.16 0.94 -5 -8 20 6.34 1.13 -5 -8 20 6.24 0.86 4 8 -20 2.44 0.79 4 8 -20 3.17 0.98 -4 -8 20 2.40 0.80 -4 -8 20 1.16 1.05 -4 -8 20 3.22 0.89 3 8 -20 17.65 1.40 3 8 -20 17.45 1.62 -3 -8 20 17.00 1.64 -3 -8 20 17.46 1.31 -3 -8 20 16.25 1.48 2 8 -20 6.85 0.87 2 8 -20 8.11 1.14 -2 -8 20 6.78 0.78 -2 -8 20 5.19 0.91 -2 -8 20 5.23 1.08 1 8 -20 9.42 1.16 1 8 -20 13.73 1.37 -1 -8 20 9.83 1.02 -1 -8 20 12.24 1.21 -1 -8 20 11.45 1.11 0 8 -20 5.90 0.90 0 8 -20 5.42 1.12 0 -8 20 4.68 0.97 0 -8 20 6.07 1.09 -1 8 -20 2.08 0.81 -1 8 -20 1.87 1.02 1 -8 20 1.32 0.97 1 -8 20 0.94 0.98 8 7 -20 1.97 0.70 8 7 -20 2.15 1.01 -8 -7 20 1.96 0.91 -8 -7 20 2.32 1.09 -8 -7 20 1.48 0.65 7 7 -20 9.19 0.78 7 7 -20 7.22 1.08 -7 -7 20 6.25 1.18 -7 -7 20 6.66 0.80 -7 -7 20 7.90 0.99 6 7 -20 7.95 0.76 6 7 -20 7.41 1.05 -6 -7 20 9.02 1.18 -6 -7 20 6.54 1.16 5 7 -20 6.11 1.02 5 7 -20 7.36 0.83 5 7 -20 7.33 0.81 -5 -7 20 7.38 1.15 -5 -7 20 7.35 0.85 -5 -7 20 8.26 0.90 4 7 -20 24.08 1.84 4 7 -20 28.57 1.49 -4 -7 20 27.57 1.46 -4 -7 20 26.28 1.56 -4 -7 20 28.33 1.92 3 7 -20 3.77 1.04 3 7 -20 2.34 0.75 -3 -7 20 3.17 0.70 -3 -7 20 2.09 1.09 -3 -7 20 2.28 0.85 2 7 -20 9.18 1.14 2 7 -20 11.79 1.27 -2 -7 20 14.39 1.62 -2 -7 20 14.11 1.48 -2 -7 20 12.73 1.08 1 7 -20 0.01 0.72 1 7 -20 -0.61 1.00 -1 -7 20 0.46 1.03 -1 -7 20 -1.01 0.90 0 7 -20 16.08 1.71 0 7 -20 16.92 1.38 0 -7 20 14.88 1.62 0 -7 20 14.40 1.66 -1 7 -20 2.04 1.09 -1 7 -20 1.42 0.82 1 -7 20 1.39 0.97 1 -7 20 2.48 1.00 9 6 -20 0.37 0.95 9 6 -20 0.22 0.77 -9 -6 20 -0.33 1.09 -9 -6 20 -0.18 0.92 -9 -6 20 0.29 0.61 8 6 -20 8.21 0.78 8 6 -20 9.17 1.09 -8 -6 20 8.35 0.96 -8 -6 20 7.55 1.14 -8 -6 20 6.49 0.74 7 6 -20 -0.73 0.94 7 6 -20 -0.01 0.62 -7 -6 20 -0.09 1.03 -7 -6 20 0.25 0.73 -7 -6 20 1.37 0.94 6 6 -20 22.53 1.82 6 6 -20 20.51 1.27 -6 -6 20 21.31 1.85 -6 -6 20 25.56 1.49 5 6 -20 0.41 0.58 5 6 -20 0.73 0.97 -5 -6 20 0.75 0.74 -5 -6 20 1.10 0.82 -5 -6 20 0.61 1.04 4 6 -20 15.30 1.11 4 6 -20 16.88 1.64 -4 -6 20 16.17 1.37 -4 -6 20 17.05 1.22 -4 -6 20 14.13 1.60 3 6 -20 0.08 0.94 3 6 -20 0.36 0.57 -3 -6 20 -0.03 0.61 -3 -6 20 -0.39 0.84 -3 -6 20 0.06 0.99 2 6 -20 11.88 1.06 2 6 -20 12.38 1.22 -2 -6 20 9.42 1.15 -2 -6 20 9.21 1.00 1 6 -20 17.07 1.64 1 6 -20 16.15 1.15 1 6 -20 15.15 1.32 -1 -6 20 14.17 1.26 -1 -6 20 14.48 1.44 0 6 -20 2.87 1.05 0 6 -20 3.50 1.10 0 6 -20 2.71 0.75 0 -6 20 1.60 0.94 0 -6 20 3.34 1.02 -1 6 -20 8.90 1.22 -1 6 -20 8.07 0.87 1 -6 20 10.34 1.13 1 -6 20 8.65 1.12 10 5 -20 18.24 1.73 10 5 -20 18.65 1.38 -10 -5 20 18.66 1.64 -10 -5 20 16.16 1.73 9 5 -20 1.99 0.97 -9 -5 20 0.63 0.89 -9 -5 20 1.12 0.64 -9 -5 20 0.96 1.10 8 5 -20 14.79 1.57 8 5 -20 13.94 1.21 -8 -5 20 13.24 1.44 -8 -5 20 14.30 1.17 -8 -5 20 13.89 1.32 7 5 -20 5.19 0.74 7 5 -20 2.40 0.96 -7 -5 20 4.47 1.11 -7 -5 20 2.95 0.96 -7 -5 20 5.18 0.88 6 5 -20 8.73 1.04 6 5 -20 7.76 0.77 -6 -5 20 8.65 1.18 -6 -5 20 8.90 1.13 -6 -5 20 11.57 1.26 5 5 -20 7.18 1.05 5 5 -20 6.73 0.72 5 5 -20 6.36 0.71 -5 -5 20 6.89 0.86 -5 -5 20 6.78 1.16 -5 -5 20 7.51 0.79 4 5 -20 1.35 0.98 4 5 -20 2.35 0.65 4 5 -20 0.96 0.63 -4 -5 20 1.38 0.65 -4 -5 20 1.65 1.06 -4 -5 20 1.80 0.82 3 5 -20 10.83 1.12 3 5 -20 12.45 1.13 3 5 -20 10.31 1.14 -3 -5 20 9.05 0.96 -3 -5 20 8.53 1.11 2 5 -20 -0.19 0.63 2 5 -20 0.06 0.66 2 5 -20 -0.43 0.96 -2 -5 20 -0.86 0.85 -2 -5 20 -0.72 0.97 1 5 -20 12.34 1.18 1 5 -20 10.83 1.18 -1 -5 20 11.79 1.12 -1 -5 20 14.65 1.71 0 5 -20 0.54 0.80 0 5 -20 0.27 0.67 0 5 -20 1.12 1.08 0 -5 20 0.33 0.96 0 -5 20 -0.28 1.01 -1 5 -20 9.97 1.26 -1 5 -20 11.62 1.25 1 -5 20 8.83 1.10 10 4 -20 7.29 0.84 10 4 -20 11.08 1.17 -10 -4 20 9.12 1.01 -10 -4 20 9.87 1.27 -10 -4 20 7.29 1.04 9 4 -20 7.82 0.87 9 4 -20 11.25 1.15 -9 -4 20 9.36 0.79 -9 -4 20 8.73 1.01 -9 -4 20 9.19 1.19 8 4 -20 5.77 1.29 8 4 -20 5.02 1.03 -8 -4 20 5.16 0.77 -8 -4 20 3.51 1.10 -8 -4 20 5.31 1.41 7 4 -20 25.61 1.47 7 4 -20 26.98 1.83 -7 -4 20 22.96 1.81 -7 -4 20 27.14 1.48 6 4 -20 0.49 0.91 6 4 -20 -0.15 0.68 -6 -4 20 0.01 0.71 -6 -4 20 -0.88 0.75 -6 -4 20 -0.78 1.00 5 4 -20 11.29 0.87 5 4 -20 13.75 1.07 5 4 -20 9.91 1.08 -5 -4 20 12.16 1.35 -5 -4 20 10.63 1.12 -5 -4 20 9.36 1.16 4 4 -20 1.27 0.69 4 4 -20 0.87 0.97 4 4 -20 1.32 0.61 -4 -4 20 0.61 0.81 -4 -4 20 1.43 1.05 3 4 -20 5.33 0.68 3 4 -20 5.47 0.75 3 4 -20 6.76 1.08 -3 -4 20 7.56 0.98 -3 -4 20 5.69 1.06 2 4 -20 10.64 1.14 2 4 -20 10.62 1.11 2 4 -20 8.40 0.82 -2 -4 20 10.85 1.16 -2 -4 20 10.53 1.05 1 4 -20 5.27 1.11 1 4 -20 4.69 0.78 1 4 -20 5.64 0.74 -1 -4 20 5.01 1.00 -1 -4 20 5.68 1.09 0 4 -20 16.14 1.36 0 -4 20 12.64 1.20 0 -4 20 10.94 1.17 10 3 -20 3.53 1.02 10 3 -20 2.85 0.82 -10 -3 20 2.93 1.11 -10 -3 20 1.76 0.63 -10 -3 20 2.32 0.93 9 3 -20 20.85 1.42 9 3 -20 17.89 1.75 -9 -3 20 20.36 2.46 -9 -3 20 18.73 1.88 -9 -3 20 18.35 1.25 8 3 -20 3.20 1.00 8 3 -20 3.55 0.88 -8 -3 20 1.82 0.91 -8 -3 20 4.19 1.15 -8 -3 20 2.63 0.83 7 3 -20 11.20 1.13 -7 -3 20 8.48 1.12 -7 -3 20 11.78 1.26 -7 -3 20 10.62 1.26 6 3 -20 6.93 0.97 6 3 -20 5.71 1.00 -6 -3 20 6.17 1.15 -6 -3 20 5.84 0.85 -6 -3 20 5.69 0.74 5 3 -20 5.60 0.62 5 3 -20 8.19 0.98 5 3 -20 7.40 1.03 -5 -3 20 5.34 0.86 -5 -3 20 6.08 1.09 4 3 -20 18.66 1.47 4 3 -20 16.95 1.70 4 3 -20 17.74 1.10 -4 -3 20 19.08 1.84 -4 -3 20 17.57 1.52 3 3 -20 3.22 0.64 3 3 -20 2.06 1.03 -3 -3 20 2.32 1.05 -3 -3 20 1.74 0.89 2 3 -20 33.17 2.03 2 3 -20 35.72 1.46 -2 -3 20 37.13 2.06 -2 -3 20 32.90 1.80 1 3 -20 1.15 1.04 1 3 -20 0.58 0.61 1 3 -20 -0.02 0.74 -1 -3 20 -0.21 0.93 -1 -3 20 0.33 0.97 11 2 -20 6.43 1.10 10 2 -20 3.64 1.01 10 2 -20 2.90 0.83 -10 -2 20 2.26 0.91 -10 -2 20 2.04 0.66 -10 -2 20 2.60 1.17 9 2 -20 2.20 0.97 9 2 -20 2.35 0.81 -9 -2 20 1.89 1.01 -9 -2 20 1.92 0.82 -9 -2 20 0.71 1.09 8 2 -20 7.42 1.07 8 2 -20 6.82 0.89 -8 -2 20 8.73 0.91 -8 -2 20 7.23 1.19 -8 -2 20 6.54 1.23 7 2 -20 0.47 0.94 7 2 -20 0.26 0.76 -7 -2 20 0.62 1.08 -7 -2 20 0.01 0.76 -7 -2 20 1.39 0.72 6 2 -20 15.29 1.67 6 2 -20 17.10 1.39 -6 -2 20 15.51 1.41 -6 -2 20 16.21 1.87 5 2 -20 1.15 0.88 5 2 -20 1.50 0.95 -5 -2 20 0.69 1.04 -5 -2 20 1.19 0.88 4 2 -20 32.38 1.96 4 2 -20 32.88 1.33 4 2 -20 33.61 1.70 -4 -2 20 33.38 1.74 -4 -2 20 36.03 2.13 3 2 -20 2.08 1.02 3 2 -20 2.40 0.82 3 2 -20 1.30 0.56 -3 -2 20 1.53 0.94 -3 -2 20 1.91 1.06 2 2 -20 16.69 1.76 2 2 -20 14.86 1.40 -2 -2 20 15.61 1.66 -2 -2 20 11.96 1.22 1 2 -20 1.42 0.80 1 2 -20 0.62 1.02 -1 -2 20 1.66 1.02 -1 -2 20 1.29 1.02 10 1 -20 5.64 1.03 10 1 -20 3.50 0.84 -10 -1 20 5.53 1.35 -10 -1 20 3.05 0.85 -10 -1 20 5.10 1.15 9 1 -20 0.20 0.95 9 1 -20 1.11 0.78 -9 -1 20 1.23 1.09 -9 -1 20 0.92 0.82 -9 -1 20 0.77 0.77 8 1 -20 11.42 1.14 8 1 -20 8.69 0.91 -8 -1 20 11.45 1.25 -8 -1 20 8.63 0.86 -8 -1 20 9.54 1.22 7 1 -20 1.46 0.96 7 1 -20 2.44 0.82 -7 -1 20 2.47 1.10 -7 -1 20 2.46 0.81 6 1 -20 17.57 1.68 6 1 -20 18.60 1.48 -6 -1 20 16.24 1.41 -6 -1 20 19.24 1.96 5 1 -20 8.61 1.06 5 1 -20 8.74 0.90 -5 -1 20 9.49 0.98 -5 -1 20 7.44 1.17 4 1 -20 4.07 1.05 4 1 -20 2.36 0.81 -4 -1 20 3.06 0.94 -4 -1 20 1.21 1.09 3 1 -20 2.50 1.01 3 1 -20 3.42 0.86 -3 -1 20 2.42 1.10 -3 -1 20 3.13 1.01 2 1 -20 4.71 1.13 2 1 -20 4.99 0.87 -2 -1 20 3.87 1.02 -2 -1 20 5.55 1.10 10 0 -20 15.56 1.66 10 0 -20 16.52 1.51 -10 0 20 16.11 1.94 -10 0 20 16.43 1.26 9 0 -20 13.73 1.47 9 0 -20 12.48 1.17 -9 0 20 14.61 1.36 -9 0 20 13.26 1.37 -9 0 20 12.02 1.30 8 0 -20 7.27 1.05 8 0 -20 6.72 0.94 -8 0 20 6.69 0.88 -8 0 20 7.73 1.25 7 0 -20 14.60 1.60 7 0 -20 15.84 1.50 -7 0 20 12.97 1.38 -7 0 20 15.32 1.76 6 0 -20 0.16 0.91 6 0 -20 -0.04 0.85 -6 0 20 -0.73 0.87 -6 0 20 0.01 1.11 5 0 -20 19.43 1.54 5 0 -20 18.57 1.25 5 0 -20 21.52 1.75 -5 0 20 15.86 1.82 -5 0 20 17.74 1.53 4 0 -20 -0.36 0.80 4 0 -20 0.15 0.98 -4 0 20 -0.51 0.92 -4 0 20 0.16 1.03 3 0 -20 8.88 1.15 9 -1 -20 21.66 1.67 9 -1 -20 18.97 1.57 -9 1 20 17.00 1.42 -9 1 20 22.59 2.07 8 -1 -20 0.09 0.88 8 -1 -20 -0.12 0.84 -8 1 20 0.32 0.82 -8 1 20 0.17 1.14 7 -1 -20 14.88 1.62 7 -1 -20 18.55 1.53 -7 1 20 18.07 1.49 -7 1 20 19.20 1.81 6 -1 -20 3.26 0.97 6 -1 -20 3.04 1.00 6 -1 -20 5.31 0.95 -6 1 20 4.68 0.92 -6 1 20 4.34 1.20 5 -1 -20 14.37 1.69 5 -1 -20 14.18 1.53 -5 1 20 10.05 1.26 -5 1 20 16.01 1.58 5 7 -21 0.92 0.75 5 7 -21 1.98 1.00 -5 -7 21 0.24 1.12 -5 -7 21 0.64 0.96 -5 -7 21 1.27 0.84 4 7 -21 14.60 1.32 4 7 -21 11.54 1.25 -4 -7 21 14.99 1.26 -4 -7 21 17.64 1.82 -4 -7 21 13.59 1.40 3 7 -21 0.66 1.01 3 7 -21 0.06 0.74 -3 -7 21 0.38 0.90 -3 -7 21 1.73 1.05 6 6 -21 18.59 1.80 6 6 -21 16.94 1.81 -6 -6 21 14.71 1.36 -6 -6 21 14.85 1.71 -6 -6 21 12.10 1.45 5 6 -21 -0.25 0.68 5 6 -21 0.59 1.00 -5 -6 21 0.15 0.80 -5 -6 21 0.07 0.75 -5 -6 21 0.52 1.06 4 6 -21 15.70 1.66 4 6 -21 15.82 1.28 -4 -6 21 15.61 1.85 -4 -6 21 12.55 1.38 3 6 -21 11.22 1.22 3 6 -21 8.64 0.87 -3 -6 21 6.68 0.98 -3 -6 21 7.25 1.18 7 5 -21 3.64 1.02 -7 -5 21 3.22 1.20 -7 -5 21 4.17 1.02 -7 -5 21 3.51 0.79 6 5 -21 7.73 1.10 6 5 -21 7.71 0.94 -6 -5 21 6.44 0.88 -6 -5 21 7.55 1.25 5 5 -21 12.62 1.38 5 5 -21 8.11 0.82 5 5 -21 11.88 1.23 -5 -5 21 10.89 1.26 -5 -5 21 8.17 0.91 4 5 -21 0.53 0.98 4 5 -21 -1.17 0.65 4 5 -21 0.99 0.78 -4 -5 21 -0.61 1.03 -4 -5 21 -0.34 0.87 3 5 -21 5.36 0.74 3 5 -21 7.90 0.82 3 5 -21 8.87 1.17 -3 -5 21 8.48 1.22 -3 -5 21 6.05 0.96 7 4 -21 6.91 1.09 7 4 -21 5.04 0.79 -7 -4 21 4.10 1.14 -7 -4 21 6.82 0.87 -7 -4 21 6.65 0.91 6 4 -21 3.53 1.00 6 4 -21 1.42 0.77 -6 -4 21 2.80 1.13 -6 -4 21 3.96 0.88 5 4 -21 2.27 0.91 5 4 -21 0.20 1.00 5 4 -21 2.31 0.66 -5 -4 21 1.84 0.87 -5 -4 21 0.71 1.13 4 4 -21 0.95 1.02 4 4 -21 -0.12 0.64 4 4 -21 0.13 1.04 -4 -4 21 1.97 1.08 -4 -4 21 0.73 0.85 3 4 -21 7.34 0.88 3 4 -21 8.58 1.16 7 3 -21 0.93 1.00 7 3 -21 0.11 0.77 -7 -3 21 0.85 0.78 -7 -3 21 -0.46 1.09 6 3 -21 6.35 0.86 6 3 -21 4.56 1.03 -6 -3 21 5.84 1.17 -6 -3 21 5.35 0.88 5 3 -21 1.71 1.02 5 3 -21 0.59 0.77 -5 -3 21 0.72 0.85 -5 -3 21 0.81 1.13 4 3 -21 13.88 1.49 4 3 -21 16.00 1.83 6 2 -21 22.52 1.76 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 96118 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.51113(15) -0.00989(14) 0.26515(12) 0.0138(3) Uani 1 1 d . . . . . C2 C 0.56328(15) 0.10573(15) 0.34623(13) 0.0160(3) Uani 1 1 d . . . . . H2 H 0.544200 0.114895 0.409348 0.019 Uiso 1 1 calc R U . . . C3 C 0.64402(15) 0.20974(15) 0.33649(13) 0.0148(3) Uani 1 1 d . . . . . C4 C 0.67063(17) 0.19179(16) 0.24259(14) 0.0201(3) Uani 1 1 d . . . . . H4 H 0.723874 0.260919 0.233995 0.024 Uiso 1 1 calc R U . . . C5 C 0.62188(18) 0.07622(16) 0.16128(14) 0.0208(3) Uani 1 1 d . . . . . H5 H 0.642495 0.066531 0.098954 0.025 Uiso 1 1 calc R U . . . C6 C 0.54244(16) -0.02451(15) 0.17340(13) 0.0163(3) Uani 1 1 d . . . . . C7 C 0.48213(16) -0.15508(15) 0.10523(13) 0.0164(3) Uani 1 1 d . . . . . C8 C 0.48546(18) -0.21688(16) 0.00769(14) 0.0211(3) Uani 1 1 d . . . . . H8 H 0.530013 -0.173201 -0.027218 0.025 Uiso 1 1 calc R U . . . C9 C 0.42220(18) -0.34381(16) -0.03744(14) 0.0209(3) Uani 1 1 d . . . . . H9 H 0.423162 -0.387030 -0.104294 0.025 Uiso 1 1 calc R U . . . C10 C 0.35724(16) -0.40912(15) 0.01348(13) 0.0166(3) Uani 1 1 d . . . . . C11 C 0.35325(16) -0.34632(15) 0.11093(13) 0.0169(3) Uani 1 1 d . . . . . H11 H 0.308618 -0.390020 0.145774 0.020 Uiso 1 1 calc R U . . . C12 C 0.41496(15) -0.22007(15) 0.15584(13) 0.0153(3) Uani 1 1 d . . . . . C13 C 0.42019(15) -0.13277(14) 0.25791(13) 0.0155(3) Uani 1 1 d . . . . . C14 C 0.28821(17) -0.14329(18) 0.23316(16) 0.0236(3) Uani 1 1 d . . . . . H14A H 0.266141 -0.120661 0.169916 0.028 Uiso 1 1 calc R U . . . H14B H 0.229302 -0.230094 0.211033 0.028 Uiso 1 1 calc R U . . . C15 C 0.2691(2) -0.0663(2) 0.32501(19) 0.0313(4) Uani 1 1 d . . . . . H15A H 0.328542 0.019851 0.349881 0.047 Uiso 1 1 calc R U . . . H15B H 0.281821 -0.093360 0.385698 0.047 Uiso 1 1 calc R U . . . H15C H 0.184612 -0.075848 0.298649 0.047 Uiso 1 1 calc R U . . . C16 C 0.46312(19) -0.16005(17) 0.35939(14) 0.0217(3) Uani 1 1 d . . . . . H16A H 0.472168 -0.095411 0.423557 0.026 Uiso 1 1 calc R U . . . H16B H 0.397862 -0.238650 0.350635 0.026 Uiso 1 1 calc R U . . . C17 C 0.5844(2) -0.1674(2) 0.38193(17) 0.0318(4) Uani 1 1 d . . . . . H17A H 0.575143 -0.234544 0.320921 0.048 Uiso 1 1 calc R U . . . H17B H 0.606588 -0.182256 0.448971 0.048 Uiso 1 1 calc R U . . . H17C H 0.649844 -0.090220 0.390459 0.048 Uiso 1 1 calc R U . . . C18 C 0.29522(16) -0.54300(15) -0.03275(13) 0.0173(3) Uani 1 1 d . . . . . C19 C 0.17297(19) -0.73365(17) -0.06225(15) 0.0248(4) Uani 1 1 d . . . . . C20 C 0.0828(3) -0.8308(2) -0.0536(2) 0.0448(7) Uani 1 1 d . . . . . H20 H 0.039658 -0.815977 -0.008560 0.054 Uiso 1 1 calc R U . . . C21 C 0.0575(3) -0.9493(2) -0.1121(2) 0.0533(8) Uani 1 1 d . . . . . H21 H -0.003599 -1.016014 -0.106864 0.064 Uiso 1 1 calc R U . . . C22 C 0.1201(3) -0.97202(19) -0.17831(19) 0.0422(6) Uani 1 1 d . . . . . H22 H 0.101769 -1.053980 -0.216741 0.051 Uiso 1 1 calc R U . . . C23 C 0.2082(2) -0.87778(18) -0.18922(17) 0.0311(4) Uani 1 1 d . . . . . H23 H 0.250875 -0.893407 -0.234542 0.037 Uiso 1 1 calc R U . . . C24 C 0.23261(18) -0.75875(16) -0.13143(15) 0.0220(3) Uani 1 1 d . . . . . C25 C 0.71055(15) 0.61120(15) 0.63915(14) 0.0166(3) Uani 1 1 d . . . . . H25 H 0.643555 0.593255 0.570298 0.020 Uiso 1 1 calc R U . . . C26 C 0.64578(18) 0.52693(17) 0.69023(17) 0.0232(3) Uani 1 1 d . . . . . H26A H 0.614781 0.440620 0.642460 0.028 Uiso 1 1 calc R U . . . H26B H 0.706027 0.543420 0.761583 0.028 Uiso 1 1 calc R U . . . C27 C 0.5376(2) 0.5471(2) 0.70601(19) 0.0295(4) Uani 1 1 d . . . . . H27A H 0.473292 0.522191 0.633931 0.035 Uiso 1 1 calc R U . . . H27B H 0.500250 0.495067 0.742697 0.035 Uiso 1 1 calc R U . . . C28 C 0.5795(2) 0.6802(2) 0.77379(17) 0.0284(4) Uani 1 1 d . . . . . H28A H 0.506609 0.691368 0.778011 0.034 Uiso 1 1 calc R U . . . H28B H 0.636022 0.702341 0.848773 0.034 Uiso 1 1 calc R U . . . C29 C 0.6456(2) 0.7643(2) 0.72444(18) 0.0285(4) Uani 1 1 d . . . . . H29A H 0.675910 0.850371 0.772368 0.034 Uiso 1 1 calc R U . . . H29B H 0.586240 0.748166 0.652775 0.034 Uiso 1 1 calc R U . . . C30 C 0.75493(18) 0.74564(17) 0.70978(17) 0.0245(4) Uani 1 1 d . . . . . H30A H 0.818110 0.768704 0.781894 0.029 Uiso 1 1 calc R U . . . H30B H 0.793463 0.798893 0.674517 0.029 Uiso 1 1 calc R U . . . C31 C 0.94371(16) 0.57788(16) 0.70946(13) 0.0175(3) Uani 1 1 d . . . . . H31 H 1.012336 0.580745 0.684478 0.021 Uiso 1 1 calc R U . . . C32 C 1.0016(2) 0.69310(18) 0.81338(15) 0.0283(4) Uani 1 1 d . . . . . H32A H 1.036072 0.766191 0.796280 0.034 Uiso 1 1 calc R U . . . H32B H 0.936387 0.696886 0.839859 0.034 Uiso 1 1 calc R U . . . C33 C 1.1041(2) 0.6953(2) 0.90314(16) 0.0310(4) Uani 1 1 d . . . . . H33A H 1.173997 0.701267 0.880412 0.037 Uiso 1 1 calc R U . . . H33B H 1.135067 0.767956 0.970319 0.037 Uiso 1 1 calc R U . . . C34 C 1.05589(19) 0.5803(2) 0.92613(16) 0.0274(4) Uani 1 1 d . . . . . H34A H 1.123665 0.582265 0.983571 0.033 Uiso 1 1 calc R U . . . H34B H 0.989342 0.576860 0.953032 0.033 Uiso 1 1 calc R U . . . C35 C 1.0058(2) 0.4674(2) 0.82382(17) 0.0286(4) Uani 1 1 d . . . . . H35A H 0.974926 0.393341 0.840313 0.034 Uiso 1 1 calc R U . . . H35B H 1.073300 0.469161 0.798727 0.034 Uiso 1 1 calc R U . . . C36 C 0.90077(18) 0.46175(18) 0.73354(16) 0.0252(4) Uani 1 1 d . . . . . H36A H 0.830206 0.452317 0.756026 0.030 Uiso 1 1 calc R U . . . H36B H 0.872052 0.389615 0.666575 0.030 Uiso 1 1 calc R U . . . C37 C 0.90385(15) 0.69666(15) 0.55699(13) 0.0160(3) Uani 1 1 d . . . . . H37 H 0.942138 0.774727 0.622133 0.019 Uiso 1 1 calc R U . . . C38 C 1.00756(18) 0.68509(19) 0.52380(18) 0.0256(4) Uani 1 1 d . . . . . H38A H 0.972209 0.608150 0.459488 0.031 Uiso 1 1 calc R U . . . H38B H 1.067542 0.681757 0.584149 0.031 Uiso 1 1 calc R U . . . C39 C 1.07456(19) 0.7940(2) 0.49648(19) 0.0305(4) Uani 1 1 d . . . . . H39A H 1.116265 0.870044 0.562767 0.037 Uiso 1 1 calc R U . . . H39B H 1.138867 0.783023 0.472313 0.037 Uiso 1 1 calc R U . . . C40 C 0.9849(2) 0.8061(2) 0.40739(19) 0.0309(4) Uani 1 1 d . . . . . H40A H 1.029699 0.880392 0.395377 0.037 Uiso 1 1 calc R U . . . H40B H 0.950741 0.734488 0.338509 0.037 Uiso 1 1 calc R U . . . C41 C 0.8797(2) 0.8141(2) 0.43806(19) 0.0295(4) Uani 1 1 d . . . . . H41A H 0.819887 0.816484 0.376840 0.035 Uiso 1 1 calc R U . . . H41B H 0.912972 0.890838 0.502046 0.035 Uiso 1 1 calc R U . . . C42 C 0.81282(17) 0.70543(18) 0.46481(16) 0.0226(3) Uani 1 1 d . . . . . H42A H 0.773424 0.629089 0.399092 0.027 Uiso 1 1 calc R U . . . H42B H 0.746839 0.714879 0.487031 0.027 Uiso 1 1 calc R U . . . Au1 Au 0.72510(2) 0.38075(2) 0.45674(2) 0.01484(2) Uani 1 1 d . . . . . N1 N 0.21091(16) -0.61060(14) -0.00631(13) 0.0238(3) Uani 1 1 d . . . . . P1 P 0.82247(4) 0.57071(4) 0.59473(3) 0.01357(7) Uani 1 1 d . . . . . S1 S 0.33646(5) -0.62296(4) -0.12792(4) 0.02486(9) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0155(7) 0.0117(6) 0.0130(6) 0.0040(5) 0.0061(5) 0.0054(5) C2 0.0178(7) 0.0147(7) 0.0139(6) 0.0034(5) 0.0065(6) 0.0070(6) C3 0.0156(7) 0.0135(7) 0.0163(7) 0.0053(5) 0.0066(6) 0.0077(6) C4 0.0245(8) 0.0132(7) 0.0199(7) 0.0053(6) 0.0111(7) 0.0046(6) C5 0.0288(9) 0.0154(7) 0.0177(7) 0.0052(6) 0.0143(7) 0.0070(7) C6 0.0215(7) 0.0118(7) 0.0150(7) 0.0041(5) 0.0089(6) 0.0066(6) C7 0.0211(7) 0.0125(7) 0.0144(6) 0.0042(5) 0.0084(6) 0.0061(6) C8 0.0308(9) 0.0152(7) 0.0170(7) 0.0052(6) 0.0139(7) 0.0078(7) C9 0.0303(9) 0.0146(7) 0.0164(7) 0.0036(6) 0.0119(7) 0.0084(7) C10 0.0196(7) 0.0117(7) 0.0147(7) 0.0025(5) 0.0053(6) 0.0060(6) C11 0.0185(7) 0.0140(7) 0.0151(7) 0.0044(5) 0.0067(6) 0.0050(6) C12 0.0176(7) 0.0131(7) 0.0127(6) 0.0031(5) 0.0061(5) 0.0059(6) C13 0.0192(7) 0.0117(6) 0.0143(6) 0.0039(5) 0.0083(6) 0.0052(6) C14 0.0190(8) 0.0221(8) 0.0254(8) 0.0048(7) 0.0106(7) 0.0067(7) C15 0.0297(10) 0.0309(10) 0.0365(11) 0.0092(9) 0.0210(9) 0.0142(9) C16 0.0330(9) 0.0174(8) 0.0163(7) 0.0071(6) 0.0121(7) 0.0110(7) C17 0.0415(12) 0.0349(11) 0.0222(9) 0.0109(8) 0.0082(8) 0.0239(10) C18 0.0195(7) 0.0138(7) 0.0139(7) 0.0024(5) 0.0041(6) 0.0066(6) C19 0.0293(9) 0.0144(8) 0.0185(8) 0.0018(6) 0.0081(7) 0.0014(7) C20 0.0597(16) 0.0195(10) 0.0347(12) 0.0020(8) 0.0284(12) -0.0040(10) C21 0.076(2) 0.0154(10) 0.0362(12) 0.0013(9) 0.0256(13) -0.0082(11) C22 0.0666(17) 0.0127(8) 0.0273(10) 0.0022(7) 0.0129(11) 0.0052(10) C23 0.0456(12) 0.0151(8) 0.0262(9) 0.0036(7) 0.0119(9) 0.0117(8) C24 0.0270(9) 0.0132(7) 0.0188(7) 0.0038(6) 0.0053(7) 0.0062(7) C25 0.0166(7) 0.0145(7) 0.0183(7) 0.0056(6) 0.0077(6) 0.0064(6) C26 0.0251(9) 0.0198(8) 0.0320(9) 0.0134(7) 0.0179(8) 0.0108(7) C27 0.0260(9) 0.0334(11) 0.0393(11) 0.0187(9) 0.0218(9) 0.0144(8) C28 0.0317(10) 0.0403(11) 0.0302(10) 0.0182(9) 0.0206(8) 0.0248(9) C29 0.0348(10) 0.0280(10) 0.0372(11) 0.0143(8) 0.0225(9) 0.0222(9) C30 0.0264(9) 0.0173(8) 0.0312(9) 0.0062(7) 0.0152(8) 0.0109(7) C31 0.0180(7) 0.0169(7) 0.0161(7) 0.0071(6) 0.0050(6) 0.0070(6) C32 0.0351(10) 0.0184(8) 0.0167(8) 0.0042(6) -0.0018(7) 0.0070(8) C33 0.0264(9) 0.0332(11) 0.0179(8) 0.0087(8) -0.0010(7) 0.0054(8) C34 0.0232(9) 0.0431(12) 0.0219(8) 0.0200(8) 0.0087(7) 0.0163(8) C35 0.0279(9) 0.0327(10) 0.0313(10) 0.0202(8) 0.0081(8) 0.0172(8) C36 0.0242(9) 0.0198(8) 0.0279(9) 0.0129(7) 0.0035(7) 0.0082(7) C37 0.0153(7) 0.0141(7) 0.0163(7) 0.0056(6) 0.0056(6) 0.0050(6) C38 0.0215(8) 0.0319(10) 0.0366(10) 0.0211(8) 0.0175(8) 0.0161(8) C39 0.0247(9) 0.0352(11) 0.0430(12) 0.0247(10) 0.0211(9) 0.0135(8) C40 0.0372(11) 0.0366(11) 0.0395(11) 0.0270(10) 0.0266(10) 0.0215(10) C41 0.0347(10) 0.0339(11) 0.0403(11) 0.0275(9) 0.0224(9) 0.0221(9) C42 0.0201(8) 0.0287(9) 0.0263(8) 0.0180(7) 0.0101(7) 0.0129(7) Au1 0.01480(3) 0.01151(3) 0.01481(3) 0.00262(2) 0.00446(2) 0.00514(2) N1 0.0277(8) 0.0127(6) 0.0212(7) 0.0006(5) 0.0113(6) 0.0021(6) P1 0.01408(17) 0.01128(17) 0.01339(16) 0.00376(14) 0.00466(14) 0.00496(14) S1 0.0299(2) 0.01334(18) 0.0307(2) 0.00415(16) 0.01766(19) 0.00825(17) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _citation_id _citation_doi _citation_year 1 10.1039/C9DT02312G 2019 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 C1 C6 119.66(15) . . ? C2 C1 C13 129.67(14) . . ? C6 C1 C13 110.67(13) . . ? C1 C2 C3 121.13(14) . . ? C1 C2 H2 119.4 . . ? C3 C2 H2 119.4 . . ? C4 C3 C2 117.50(15) . . ? C4 C3 Au1 120.71(12) . . ? C2 C3 Au1 121.76(11) . . ? C5 C4 C3 122.47(16) . . ? C5 C4 H4 118.8 . . ? C3 C4 H4 118.8 . . ? C6 C5 C4 118.57(15) . . ? C6 C5 H5 120.7 . . ? C4 C5 H5 120.7 . . ? C5 C6 C1 120.64(15) . . ? C5 C6 C7 130.85(15) . . ? C1 C6 C7 108.48(14) . . ? C8 C7 C12 120.49(15) . . ? C8 C7 C6 130.97(15) . . ? C12 C7 C6 108.52(14) . . ? C9 C8 C7 118.53(16) . . ? C9 C8 H8 120.7 . . ? C7 C8 H8 120.7 . . ? C8 C9 C10 121.31(15) . . ? C8 C9 H9 119.3 . . ? C10 C9 H9 119.3 . . ? C9 C10 C11 119.83(15) . . ? C9 C10 C18 120.68(15) . . ? C11 C10 C18 119.48(15) . . ? C12 C11 C10 119.23(15) . . ? C12 C11 H11 120.4 . . ? C10 C11 H11 120.4 . . ? C11 C12 C7 120.60(14) . . ? C11 C12 C13 128.62(15) . . ? C7 C12 C13 110.76(14) . . ? C12 C13 C1 101.20(12) . . ? C12 C13 C16 113.02(14) . . ? C1 C13 C16 113.15(14) . . ? C12 C13 C14 106.84(13) . . ? C1 C13 C14 111.32(14) . . ? C16 C13 C14 110.80(14) . . ? C15 C14 C13 116.70(16) . . ? C15 C14 H14A 108.1 . . ? C13 C14 H14A 108.1 . . ? C15 C14 H14B 108.1 . . ? C13 C14 H14B 108.1 . . ? H14A C14 H14B 107.3 . . ? C14 C15 H15A 109.5 . . ? C14 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? C14 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C17 C16 C13 114.57(15) . . ? C17 C16 H16A 108.6 . . ? C13 C16 H16A 108.6 . . ? C17 C16 H16B 108.6 . . ? C13 C16 H16B 108.6 . . ? H16A C16 H16B 107.6 . . ? C16 C17 H17A 109.5 . . ? C16 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C16 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? N1 C18 C10 124.53(15) . . ? N1 C18 S1 115.43(13) . . ? C10 C18 S1 120.02(13) . . ? N1 C19 C20 125.32(19) . . ? N1 C19 C24 115.49(16) . . ? C20 C19 C24 119.19(18) . . ? C21 C20 C19 118.8(2) . . ? C21 C20 H20 120.6 . . ? C19 C20 H20 120.6 . . ? C20 C21 C22 121.1(2) . . ? C20 C21 H21 119.5 . . ? C22 C21 H21 119.5 . . ? C23 C22 C21 121.2(2) . . ? C23 C22 H22 119.4 . . ? C21 C22 H22 119.4 . . ? C22 C23 C24 117.7(2) . . ? C22 C23 H23 121.2 . . ? C24 C23 H23 121.2 . . ? C23 C24 C19 122.02(18) . . ? C23 C24 S1 128.72(16) . . ? C19 C24 S1 109.24(13) . . ? C26 C25 C30 110.35(14) . . ? C26 C25 P1 112.47(12) . . ? C30 C25 P1 117.86(12) . . ? C26 C25 H25 105.0 . . ? C30 C25 H25 105.0 . . ? P1 C25 H25 105.0 . . ? C27 C26 C25 110.89(15) . . ? C27 C26 H26A 109.5 . . ? C25 C26 H26A 109.5 . . ? C27 C26 H26B 109.5 . . ? C25 C26 H26B 109.5 . . ? H26A C26 H26B 108.0 . . ? C28 C27 C26 111.41(17) . . ? C28 C27 H27A 109.3 . . ? C26 C27 H27A 109.3 . . ? C28 C27 H27B 109.3 . . ? C26 C27 H27B 109.3 . . ? H27A C27 H27B 108.0 . . ? C29 C28 C27 111.09(16) . . ? C29 C28 H28A 109.4 . . ? C27 C28 H28A 109.4 . . ? C29 C28 H28B 109.4 . . ? C27 C28 H28B 109.4 . . ? H28A C28 H28B 108.0 . . ? C28 C29 C30 111.73(16) . . ? C28 C29 H29A 109.3 . . ? C30 C29 H29A 109.3 . . ? C28 C29 H29B 109.3 . . ? C30 C29 H29B 109.3 . . ? H29A C29 H29B 107.9 . . ? C29 C30 C25 110.10(16) . . ? C29 C30 H30A 109.6 . . ? C25 C30 H30A 109.6 . . ? C29 C30 H30B 109.6 . . ? C25 C30 H30B 109.6 . . ? H30A C30 H30B 108.2 . . ? C32 C31 C36 111.37(15) . . ? C32 C31 P1 114.82(12) . . ? C36 C31 P1 112.39(12) . . ? C32 C31 H31 105.8 . . ? C36 C31 H31 105.8 . . ? P1 C31 H31 105.8 . . ? C33 C32 C31 112.03(17) . . ? C33 C32 H32A 109.2 . . ? C31 C32 H32A 109.2 . . ? C33 C32 H32B 109.2 . . ? C31 C32 H32B 109.2 . . ? H32A C32 H32B 107.9 . . ? C34 C33 C32 110.39(17) . . ? C34 C33 H33A 109.6 . . ? C32 C33 H33A 109.6 . . ? C34 C33 H33B 109.6 . . ? C32 C33 H33B 109.6 . . ? H33A C33 H33B 108.1 . . ? C35 C34 C33 110.58(16) . . ? C35 C34 H34A 109.5 . . ? C33 C34 H34A 109.5 . . ? C35 C34 H34B 109.5 . . ? C33 C34 H34B 109.5 . . ? H34A C34 H34B 108.1 . . ? C34 C35 C36 110.75(17) . . ? C34 C35 H35A 109.5 . . ? C36 C35 H35A 109.5 . . ? C34 C35 H35B 109.5 . . ? C36 C35 H35B 109.5 . . ? H35A C35 H35B 108.1 . . ? C35 C36 C31 110.95(16) . . ? C35 C36 H36A 109.4 . . ? C31 C36 H36A 109.4 . . ? C35 C36 H36B 109.4 . . ? C31 C36 H36B 109.4 . . ? H36A C36 H36B 108.0 . . ? C38 C37 C42 109.57(14) . . ? C38 C37 P1 112.82(12) . . ? C42 C37 P1 110.87(12) . . ? C38 C37 H37 107.8 . . ? C42 C37 H37 107.8 . . ? P1 C37 H37 107.8 . . ? C37 C38 C39 110.65(16) . . ? C37 C38 H38A 109.5 . . ? C39 C38 H38A 109.5 . . ? C37 C38 H38B 109.5 . . ? C39 C38 H38B 109.5 . . ? H38A C38 H38B 108.1 . . ? C40 C39 C38 111.38(17) . . ? C40 C39 H39A 109.4 . . ? C38 C39 H39A 109.4 . . ? C40 C39 H39B 109.4 . . ? C38 C39 H39B 109.4 . . ? H39A C39 H39B 108.0 . . ? C41 C40 C39 110.96(17) . . ? C41 C40 H40A 109.4 . . ? C39 C40 H40A 109.4 . . ? C41 C40 H40B 109.4 . . ? C39 C40 H40B 109.4 . . ? H40A C40 H40B 108.0 . . ? C40 C41 C42 111.50(16) . . ? C40 C41 H41A 109.3 . . ? C42 C41 H41A 109.3 . . ? C40 C41 H41B 109.3 . . ? C42 C41 H41B 109.3 . . ? H41A C41 H41B 108.0 . . ? C41 C42 C37 110.63(16) . . ? C41 C42 H42A 109.5 . . ? C37 C42 H42A 109.5 . . ? C41 C42 H42B 109.5 . . ? C37 C42 H42B 109.5 . . ? H42A C42 H42B 108.1 . . ? C3 Au1 P1 177.63(5) . . ? C18 N1 C19 110.49(15) . . ? C37 P1 C31 105.01(8) . . ? C37 P1 C25 104.17(7) . . ? C31 P1 C25 111.60(8) . . ? C37 P1 Au1 114.26(5) . . ? C31 P1 Au1 110.02(6) . . ? C25 P1 Au1 111.53(6) . . ? C24 S1 C18 89.32(9) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 C2 1.388(2) . ? C1 C6 1.405(2) . ? C1 C13 1.525(2) . ? C2 C3 1.409(2) . ? C2 H2 0.9500 . ? C3 C4 1.401(2) . ? C3 Au1 2.0498(16) . ? C4 C5 1.395(2) . ? C4 H4 0.9500 . ? C5 C6 1.391(2) . ? C5 H5 0.9500 . ? C6 C7 1.463(2) . ? C7 C8 1.392(2) . ? C7 C12 1.404(2) . ? C8 C9 1.389(2) . ? C8 H8 0.9500 . ? C9 C10 1.396(2) . ? C9 H9 0.9500 . ? C10 C11 1.400(2) . ? C10 C18 1.464(2) . ? C11 C12 1.381(2) . ? C11 H11 0.9500 . ? C12 C13 1.522(2) . ? C13 C16 1.536(2) . ? C13 C14 1.553(2) . ? C14 C15 1.521(3) . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C16 C17 1.519(3) . ? C16 H16A 0.9900 . ? C16 H16B 0.9900 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 N1 1.301(2) . ? C18 S1 1.7532(17) . ? C19 N1 1.388(2) . ? C19 C20 1.398(3) . ? C19 C24 1.399(3) . ? C20 C21 1.387(3) . ? C20 H20 0.9500 . ? C21 C22 1.390(4) . ? C21 H21 0.9500 . ? C22 C23 1.379(3) . ? C22 H22 0.9500 . ? C23 C24 1.394(3) . ? C23 H23 0.9500 . ? C24 S1 1.7265(19) . ? C25 C26 1.534(2) . ? C25 C30 1.538(2) . ? C25 P1 1.8512(17) . ? C25 H25 1.0000 . ? C26 C27 1.530(3) . ? C26 H26A 0.9900 . ? C26 H26B 0.9900 . ? C27 C28 1.521(3) . ? C27 H27A 0.9900 . ? C27 H27B 0.9900 . ? C28 C29 1.521(3) . ? C28 H28A 0.9900 . ? C28 H28B 0.9900 . ? C29 C30 1.530(3) . ? C29 H29A 0.9900 . ? C29 H29B 0.9900 . ? C30 H30A 0.9900 . ? C30 H30B 0.9900 . ? C31 C32 1.532(3) . ? C31 C36 1.532(2) . ? C31 P1 1.8481(17) . ? C31 H31 1.0000 . ? C32 C33 1.526(3) . ? C32 H32A 0.9900 . ? C32 H32B 0.9900 . ? C33 C34 1.517(3) . ? C33 H33A 0.9900 . ? C33 H33B 0.9900 . ? C34 C35 1.517(3) . ? C34 H34A 0.9900 . ? C34 H34B 0.9900 . ? C35 C36 1.528(3) . ? C35 H35A 0.9900 . ? C35 H35B 0.9900 . ? C36 H36A 0.9900 . ? C36 H36B 0.9900 . ? C37 C38 1.530(2) . ? C37 C42 1.534(2) . ? C37 P1 1.8422(17) . ? C37 H37 1.0000 . ? C38 C39 1.534(3) . ? C38 H38A 0.9900 . ? C38 H38B 0.9900 . ? C39 C40 1.520(3) . ? C39 H39A 0.9900 . ? C39 H39B 0.9900 . ? C40 C41 1.517(3) . ? C40 H40A 0.9900 . ? C40 H40B 0.9900 . ? C41 C42 1.526(3) . ? C41 H41A 0.9900 . ? C41 H41B 0.9900 . ? C42 H42A 0.9900 . ? C42 H42B 0.9900 . ? Au1 P1 2.2950(4) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C6 C1 C2 C3 2.2(2) . . . . ? C13 C1 C2 C3 -178.35(16) . . . . ? C1 C2 C3 C4 -0.7(2) . . . . ? C1 C2 C3 Au1 -178.59(12) . . . . ? C2 C3 C4 C5 -0.9(3) . . . . ? Au1 C3 C4 C5 176.98(14) . . . . ? C3 C4 C5 C6 1.0(3) . . . . ? C4 C5 C6 C1 0.6(3) . . . . ? C4 C5 C6 C7 -177.16(18) . . . . ? C2 C1 C6 C5 -2.2(3) . . . . ? C13 C1 C6 C5 178.30(16) . . . . ? C2 C1 C6 C7 176.03(15) . . . . ? C13 C1 C6 C7 -3.49(19) . . . . ? C5 C6 C7 C8 -0.7(3) . . . . ? C1 C6 C7 C8 -178.69(19) . . . . ? C5 C6 C7 C12 177.48(19) . . . . ? C1 C6 C7 C12 -0.49(19) . . . . ? C12 C7 C8 C9 -0.7(3) . . . . ? C6 C7 C8 C9 177.30(18) . . . . ? C7 C8 C9 C10 -0.5(3) . . . . ? C8 C9 C10 C11 1.2(3) . . . . ? C8 C9 C10 C18 -177.48(17) . . . . ? C9 C10 C11 C12 -0.6(3) . . . . ? C18 C10 C11 C12 178.11(16) . . . . ? C10 C11 C12 C7 -0.7(3) . . . . ? C10 C11 C12 C13 177.69(16) . . . . ? C8 C7 C12 C11 1.3(3) . . . . ? C6 C7 C12 C11 -177.09(15) . . . . ? C8 C7 C12 C13 -177.28(16) . . . . ? C6 C7 C12 C13 4.29(19) . . . . ? C11 C12 C13 C1 175.54(17) . . . . ? C7 C12 C13 C1 -5.97(18) . . . . ? C11 C12 C13 C16 54.2(2) . . . . ? C7 C12 C13 C16 -127.28(16) . . . . ? C11 C12 C13 C14 -67.9(2) . . . . ? C7 C12 C13 C14 110.59(16) . . . . ? C2 C1 C13 C12 -173.80(16) . . . . ? C6 C1 C13 C12 5.66(17) . . . . ? C2 C1 C13 C16 -52.6(2) . . . . ? C6 C1 C13 C16 126.88(15) . . . . ? C2 C1 C13 C14 73.0(2) . . . . ? C6 C1 C13 C14 -107.56(16) . . . . ? C12 C13 C14 C15 178.39(16) . . . . ? C1 C13 C14 C15 -72.0(2) . . . . ? C16 C13 C14 C15 54.9(2) . . . . ? C12 C13 C16 C17 52.9(2) . . . . ? C1 C13 C16 C17 -61.4(2) . . . . ? C14 C13 C16 C17 172.80(16) . . . . ? C9 C10 C18 N1 -163.64(18) . . . . ? C11 C10 C18 N1 17.7(3) . . . . ? C9 C10 C18 S1 18.2(2) . . . . ? C11 C10 C18 S1 -160.47(13) . . . . ? N1 C19 C20 C21 -177.9(3) . . . . ? C24 C19 C20 C21 1.6(4) . . . . ? C19 C20 C21 C22 0.0(5) . . . . ? C20 C21 C22 C23 -0.8(5) . . . . ? C21 C22 C23 C24 0.1(4) . . . . ? C22 C23 C24 C19 1.6(3) . . . . ? C22 C23 C24 S1 179.94(19) . . . . ? N1 C19 C24 C23 177.11(19) . . . . ? C20 C19 C24 C23 -2.4(3) . . . . ? N1 C19 C24 S1 -1.5(2) . . . . ? C20 C19 C24 S1 178.9(2) . . . . ? C30 C25 C26 C27 56.9(2) . . . . ? P1 C25 C26 C27 -169.27(14) . . . . ? C25 C26 C27 C28 -55.9(2) . . . . ? C26 C27 C28 C29 55.0(2) . . . . ? C27 C28 C29 C30 -55.8(2) . . . . ? C28 C29 C30 C25 56.8(2) . . . . ? C26 C25 C30 C29 -57.0(2) . . . . ? P1 C25 C30 C29 171.93(13) . . . . ? C36 C31 C32 C33 53.0(2) . . . . ? P1 C31 C32 C33 -177.82(14) . . . . ? C31 C32 C33 C34 -55.3(2) . . . . ? C32 C33 C34 C35 58.2(2) . . . . ? C33 C34 C35 C36 -59.3(2) . . . . ? C34 C35 C36 C31 56.5(2) . . . . ? C32 C31 C36 C35 -53.2(2) . . . . ? P1 C31 C36 C35 176.35(14) . . . . ? C42 C37 C38 C39 57.6(2) . . . . ? P1 C37 C38 C39 -178.35(14) . . . . ? C37 C38 C39 C40 -56.7(2) . . . . ? C38 C39 C40 C41 55.0(3) . . . . ? C39 C40 C41 C42 -55.4(3) . . . . ? C40 C41 C42 C37 57.1(2) . . . . ? C38 C37 C42 C41 -57.9(2) . . . . ? P1 C37 C42 C41 176.97(13) . . . . ? C10 C18 N1 C19 -178.38(17) . . . . ? S1 C18 N1 C19 -0.2(2) . . . . ? C20 C19 N1 C18 -179.4(2) . . . . ? C24 C19 N1 C18 1.1(3) . . . . ? C38 C37 P1 C31 59.09(14) . . . . ? C42 C37 P1 C31 -177.59(12) . . . . ? C38 C37 P1 C25 176.52(13) . . . . ? C42 C37 P1 C25 -60.15(14) . . . . ? C38 C37 P1 Au1 -61.54(14) . . . . ? C42 C37 P1 Au1 61.78(13) . . . . ? C32 C31 P1 C37 65.66(15) . . . . ? C36 C31 P1 C37 -165.68(13) . . . . ? C32 C31 P1 C25 -46.60(16) . . . . ? C36 C31 P1 C25 82.06(14) . . . . ? C32 C31 P1 Au1 -170.95(12) . . . . ? C36 C31 P1 Au1 -42.28(14) . . . . ? C26 C25 P1 C37 -171.57(13) . . . . ? C30 C25 P1 C37 -41.45(15) . . . . ? C26 C25 P1 C31 -58.79(15) . . . . ? C30 C25 P1 C31 71.33(15) . . . . ? C26 C25 P1 Au1 64.71(13) . . . . ? C30 C25 P1 Au1 -165.18(12) . . . . ? C23 C24 S1 C18 -177.4(2) . . . . ? C19 C24 S1 C18 1.15(15) . . . . ? N1 C18 S1 C24 -0.61(15) . . . . ? C10 C18 S1 C24 177.70(15) . . . . ?