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Information card for entry 7242947
Preview
| Coordinates | 7242947.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C30 H22 N4 |
|---|---|
| Calculated formula | C30 H22 N4 |
| Title of publication | Synthesis of tetrahydro-β-carbolines from 2-indolylmethyl azides and propargylic alcohols |
| Authors of publication | Yin, Haiting; Ma, Qin; Wang, Yushan; Gu, Xiaoxia; Feng, Zhijun; Wu, Yunjun; Wang, Ming; Wang, Shaoyin |
| Journal of publication | RSC Advances |
| Year of publication | 2021 |
| Journal volume | 11 |
| Journal issue | 32 |
| Pages of publication | 19639 - 19646 |
| a | 12.3091 ± 0.0008 Å |
| b | 14.2045 ± 0.0009 Å |
| c | 16.5877 ± 0.0011 Å |
| α | 90° |
| β | 101.973 ± 0.001° |
| γ | 90° |
| Cell volume | 2837.2 ± 0.3 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293.15 K |
| Number of distinct elements | 3 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0662 |
| Residual factor for significantly intense reflections | 0.0479 |
| Weighted residual factors for significantly intense reflections | 0.1336 |
| Weighted residual factors for all reflections included in the refinement | 0.1444 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.108 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 265663 (current) | 2021-06-02 | cif/ Adding structures of 7242947, 7242948 via cif-deposit CGI script. |
7242947.cif |
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Users of the data should acknowledge the original authors of the
structural data.