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Information card for entry 7246187
Preview
| Coordinates | 7246187.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C42 H48 N4 O2 Pd |
|---|---|
| Calculated formula | C42 H48 N4 O2 Pd |
| Title of publication | The role of a redox-active non-innocent ligand in additive-free C–C Glaser–Hay and Suzuki coupling reactions by an o-aminophenol palladium(ii) complex |
| Authors of publication | Pakpour, Fatemeh; Safaei, Elham; Azami, S. Mohammad; Wojtczak, Andrzej; Kaldunska, Karolina |
| Journal of publication | RSC Advances |
| Year of publication | 2023 |
| Journal volume | 13 |
| Journal issue | 5 |
| Pages of publication | 3278 - 3289 |
| a | 16.674 ± 0.002 Å |
| b | 8.0975 ± 0.0007 Å |
| c | 16.837 ± 0.002 Å |
| α | 90° |
| β | 119.02 ± 0.016° |
| γ | 90° |
| Cell volume | 1987.9 ± 0.5 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.1242 |
| Residual factor for significantly intense reflections | 0.0813 |
| Weighted residual factors for significantly intense reflections | 0.223 |
| Weighted residual factors for all reflections included in the refinement | 0.2611 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.159 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 280485 (current) | 2023-01-21 | cif/ Adding structures of 7246187 via cif-deposit CGI script. |
7246187.cif |
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