#------------------------------------------------------------------------------ #$Date: 2023-03-17 04:29:49 +0200 (Fri, 17 Mar 2023) $ #$Revision: 281927 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/64/7246464.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7246464 loop_ _publ_author_name 'Siedzielnik, Magdalena' 'Paw\/lowska, Monika' 'Da\'sko, Mateusz' 'Kleinschmidt, Hubert' 'Do\/l\;ega, Anna' _publ_section_title ; Reactions of cobalt(ii) chloride and cobalt(ii) acetate with hemisalen-type ligands: ligand transformation, oxidation of cobalt and complex formation. Preliminary study on the cytotoxicity of Co(ii) and Co(iii) hemisalen complexes ; _journal_issue 13 _journal_name_full 'RSC Advances' _journal_page_first 8830 _journal_page_last 8843 _journal_paper_doi 10.1039/D2RA07089H _journal_volume 13 _journal_year 2023 _chemical_formula_moiety 'C22 H20 N2 O4' _chemical_formula_sum 'C22 H20 N2 O4' _chemical_formula_weight 376.4 _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_cell_setting triclinic _symmetry_Int_Tables_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary other _audit_creation_date 2023-01-10T19:25:41-00:00 _audit_creation_method 'WinGX routine CIF_UPDATE' _audit_update_record ; 2023-01-23 deposited with the CCDC. 2023-03-08 downloaded from the CCDC. ; _cell_angle_alpha 87.538(4) _cell_angle_beta 85.441(4) _cell_angle_gamma 68.748(3) _cell_formula_units_Z 2 _cell_length_a 8.9262(4) _cell_length_b 9.3131(4) _cell_length_c 11.4785(5) _cell_measurement_reflns_used 20524 _cell_measurement_temperature 120(2) _cell_measurement_theta_max 29.6 _cell_measurement_theta_min 2.35 _cell_volume 886.41(7) _computing_cell_refinement ; X-Area Recipe 1.34.0.0 (STOE, 2019) ; _computing_data_collection ; X-Area WinXpose 2.0.22.0 (STOE, 2016) ; _computing_data_reduction ; X-Area Integrate 1.77.0.0 (STOE, 2019) X-Area X-Red32 1.65.0.0 (STOE, 2018) ; _computing_publication_material ; STOE & Cie GmbH, X-Area, software package for collecting single-crystal or multi-domain crystal data on STOE area-detector diffractometers, for image processing, for the correction and scaling of reflection intensities and for outlier rejection, version 1.88, Darmstadt 2019 ; _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _diffrn_ambient_temperature 120(2) _diffrn_detector 'image plate (34 cm diameter)' _diffrn_detector_area_resol_mean 6.67 _diffrn_detector_type 'STOE Imaging Plate' _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device '2-circle diffractometer' _diffrn_measurement_device_type 'STOE IPDS 2T' _diffrn_measurement_method 'rotation method, \w scans' _diffrn_radiation_monochromator 'parabolic x-ray mirror' _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0183 _diffrn_reflns_av_unetI/netI 0.0164 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 12586 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 29.185 _diffrn_reflns_theta_min 2.347 _diffrn_source 'GeniX Mo, 0.05 x 0.05 mm2 microfocus' _exptl_absorpt_coefficient_mu 0.098 _exptl_absorpt_correction_T_max 0.981 _exptl_absorpt_correction_T_min 0.9666 _exptl_absorpt_correction_type integration _exptl_absorpt_process_details ; STOE X-Red32, absorption correction by Gaussian integration, analogous to P. Coppens, "The Evaluation of Absorption and Extinction in Single-Crystal Structure Analysis", published in F. R. Ahmed (Editor), "Crystallographic Computing", Munksgaard, Copenhagen (1970), 255 - 270 ; _exptl_crystal_colour 'light green' _exptl_crystal_density_diffrn 1.41 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 396 _exptl_crystal_size_max 0.45 _exptl_crystal_size_mid 0.35 _exptl_crystal_size_min 0.293 _refine_diff_density_max 0.437 _refine_diff_density_min -0.2 _refine_diff_density_rms 0.049 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.04 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 256 _refine_ls_number_reflns 4767 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.04 _refine_ls_R_factor_all 0.0426 _refine_ls_R_factor_gt 0.038 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0569P)^2^+0.3278P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1018 _refine_ls_wR_factor_ref 0.1054 _reflns_Friedel_coverage 0 _reflns_number_gt 4276 _reflns_number_total 4767 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d2ra07089h2.cif _cod_data_source_block ms24_2022 _cod_database_code 7246464 _shelx_shelxl_version_number 2014/7 _shelx_res_file ; shelx.res created by SHELXL-2014/7 TITL ms24_2022_a.res in P-1 REM Old TITL REM SHELXT solution in P-1 REM R1 0.096, Rweak 0.004, Alpha 0.034, Orientation as input REM Formula found by SHELXT: C22 N2 O4 CELL 0.71073 8.9262 9.3131 11.4785 87.538 85.441 68.748 ZERR 2 0.0004 0.0004 0.0005 0.004 0.004 0.003 LATT 1 SFAC C H N O UNIT 44 40 4 8 L.S. 4 0 0 PLAN 5 CONF TEMP -153.15 BOND $H list 4 HTAB fmap 2 53 acta MORE -1 REM REM REM WGHT 0.056900 0.327800 FVAR 0.76460 O3 4 0.590178 0.590969 0.811778 11.00000 0.01483 0.01431 = 0.01245 -0.00049 0.00090 -0.00267 O1 4 0.889168 0.247304 0.665613 11.00000 0.01521 0.01279 = 0.01680 -0.00260 0.00296 -0.00571 O2 4 0.852014 -0.005986 0.621091 11.00000 0.02052 0.01318 = 0.01984 -0.00400 0.00131 -0.00610 O4 4 0.362100 0.820116 0.719954 11.00000 0.01583 0.01847 = 0.01809 -0.00061 -0.00023 -0.00061 N1 3 0.870622 0.435955 0.802270 11.00000 0.01352 0.01530 = 0.01278 -0.00214 0.00066 -0.00575 N2 3 1.093111 0.507672 0.780295 11.00000 0.01552 0.01944 = 0.01698 -0.00129 -0.00049 -0.00716 C9 1 0.604163 0.609730 0.692476 11.00000 0.01558 0.01445 = 0.01268 -0.00043 -0.00087 -0.00705 C17 1 0.947432 0.534762 0.834519 11.00000 0.01496 0.01342 = 0.01307 0.00175 -0.00298 -0.00502 C14 1 0.735500 0.517629 0.622300 11.00000 0.01526 0.01355 = 0.01389 -0.00071 0.00000 -0.00646 C1 1 0.773428 0.213729 0.734377 11.00000 0.01297 0.01441 = 0.01436 0.00109 -0.00099 -0.00504 C6 1 0.681264 0.308525 0.823891 11.00000 0.01367 0.01436 = 0.01463 -0.00002 -0.00062 -0.00505 C15 1 0.879702 0.402595 0.678621 11.00000 0.01417 0.01311 = 0.01330 -0.00205 0.00122 -0.00554 AFIX 13 H15 2 0.979796 0.413338 0.640337 11.00000 -1.20000 AFIX 0 C7 1 0.713360 0.451530 0.852583 11.00000 0.01352 0.01374 = 0.01271 -0.00036 -0.00001 -0.00426 AFIX 13 H7 2 0.713563 0.456588 0.939414 11.00000 -1.20000 AFIX 0 C2 1 0.753975 0.074421 0.711574 11.00000 0.01520 0.01361 = 0.01545 0.00008 -0.00268 -0.00379 C10 1 0.479232 0.731209 0.642495 11.00000 0.01514 0.01529 = 0.01740 -0.00117 -0.00070 -0.00558 C13 1 0.738066 0.540605 0.500841 11.00000 0.02071 0.01725 = 0.01398 -0.00200 0.00078 -0.00765 AFIX 43 H13 2 0.826540 0.476946 0.452479 11.00000 -1.20000 AFIX 0 C18 1 0.878218 0.648270 0.918745 11.00000 0.01571 0.01513 = 0.01583 -0.00085 -0.00117 -0.00479 AFIX 43 H18 2 0.773694 0.664620 0.954358 11.00000 -1.20000 AFIX 0 C11 1 0.483740 0.752070 0.521994 11.00000 0.02055 0.01948 = 0.01809 0.00205 -0.00533 -0.00493 AFIX 43 H11 2 0.398916 0.832433 0.487406 11.00000 -1.20000 AFIX 0 C19 1 0.964838 0.737034 0.949659 11.00000 0.02023 0.01458 = 0.01578 0.00063 -0.00416 -0.00582 C21 1 1.173960 0.595570 0.809721 11.00000 0.01736 0.02308 = 0.01941 -0.00060 -0.00037 -0.01000 AFIX 43 H21 2 1.277103 0.578398 0.771298 11.00000 -1.20000 AFIX 0 C5 1 0.566535 0.264863 0.891279 11.00000 0.01612 0.01870 = 0.01863 -0.00049 0.00219 -0.00576 AFIX 43 H5 2 0.503354 0.328306 0.953161 11.00000 -1.20000 AFIX 0 C3 1 0.638707 0.033380 0.778286 11.00000 0.01945 0.01639 = 0.02226 0.00202 -0.00303 -0.00869 AFIX 43 H3 2 0.623373 -0.059683 0.763211 11.00000 -1.20000 AFIX 0 C4 1 0.545247 0.129556 0.867766 11.00000 0.01861 0.02111 = 0.02228 0.00237 0.00171 -0.01022 AFIX 43 H4 2 0.466014 0.101468 0.913019 11.00000 -1.20000 AFIX 0 C12 1 0.612494 0.655406 0.451238 11.00000 0.02579 0.02204 = 0.01334 0.00050 -0.00257 -0.00775 AFIX 43 H12 2 0.613518 0.668822 0.368703 11.00000 -1.20000 AFIX 0 C20 1 1.116329 0.710004 0.892781 11.00000 0.02058 0.01948 = 0.01992 0.00042 -0.00444 -0.01043 AFIX 43 H20 2 1.178787 0.768861 0.910615 11.00000 -1.20000 AFIX 0 C8 1 0.852552 -0.156648 0.602003 11.00000 0.02983 0.01258 = 0.02586 -0.00272 -0.00217 -0.00772 AFIX 137 H8A 2 0.932555 -0.204927 0.538229 11.00000 -1.50000 H8B 2 0.745583 -0.149191 0.581183 11.00000 -1.50000 H8C 2 0.879886 -0.219247 0.673493 11.00000 -1.50000 AFIX 0 C22 1 0.894463 0.858997 1.041104 11.00000 0.02324 0.01884 = 0.02417 -0.00594 -0.00300 -0.00715 AFIX 137 H22A 2 0.816469 0.951036 1.006383 11.00000 -1.50000 H22B 2 0.980880 0.885441 1.070990 11.00000 -1.50000 H22C 2 0.840234 0.819899 1.105459 11.00000 -1.50000 AFIX 0 C16 1 0.234011 0.944630 0.671787 11.00000 0.02281 0.02735 = 0.02507 0.00072 -0.00304 0.00540 AFIX 137 H16A 2 0.184822 0.904963 0.613622 11.00000 -1.50000 H16B 2 0.276757 1.019712 0.634389 11.00000 -1.50000 H16C 2 0.152609 0.994610 0.734317 11.00000 -1.50000 AFIX 0 HKLF 4 REM ms24_2022_a.res in P-1 REM R1 = 0.0380 for 4276 Fo > 4sig(Fo) and 0.0426 for all 4767 data REM 256 parameters refined using 0 restraints END WGHT 0.0569 0.3280 REM Instructions for potential hydrogen bonds EQIV $1 -x+1, -y+1, -z+1 HTAB C11 O2_$1 EQIV $2 x+1, y, z HTAB C21 O4_$2 REM Highest difference peak 0.437, deepest hole -0.200, 1-sigma level 0.049 Q1 1 0.6727 0.5662 0.6589 11.00000 0.05 0.44 Q2 1 0.7272 0.2616 0.7802 11.00000 0.05 0.40 Q3 1 0.8027 0.4614 0.6503 11.00000 0.05 0.40 Q4 1 0.6962 0.3763 0.8363 11.00000 0.05 0.39 Q5 1 0.8006 0.4429 0.8324 11.00000 0.05 0.38 ; _shelx_res_checksum 99224 _shelx_hkl_file ; -11 -1 2 29.95 1.06 0 -10 -5 3 0.69 0.78 0 -10 -4 3 20.47 0.90 0 -10 0 2 0.41 0.72 0 -9 -9 2 1.40 0.83 0 -7 -10 1 41.62 1.01 0 -7 5 -1 91.69 0.57 0 -6 -8 2 27.82 0.75 0 -5 -7 2 415.56 1.85 0 -5 -4 3 60.41 0.71 0 -4 -12 -4 14.66 0.67 0 -4 -10 -1 4.51 0.49 0 -4 -9 0 13.59 0.52 0 -4 -6 2 47.75 0.62 0 -3 -8 0 72.60 0.71 0 -3 7 -4 -0.03 0.27 0 -2 -5 1 390.54 1.22 0 -2 8 -7 -0.21 0.52 0 -1 5 -2 781.73 1.34 0 -1 7 -5 1.00 0.32 0 -1 8 -8 -0.57 0.55 0 0 -9 -7 4.19 0.20 0 0 8 -11 9.63 0.94 0 0 8 -10 48.47 0.99 0 1 4 -3 3.19 0.23 0 1 5 -4 78.87 0.64 0 1 7 -8 197.01 1.42 0 2 6 -8 3.91 0.48 0 3 -4 -8 67.52 0.71 0 3 0 -5 561.45 1.62 0 3 1 -5 97.14 0.72 0 3 5 -13 0.09 0.86 0 3 5 -12 1.87 0.87 0 3 5 -11 3.68 0.77 0 3 5 -10 15.26 0.70 0 4 -1 -12 0.82 0.62 0 4 -1 -11 52.85 0.92 0 4 0 -13 0.17 0.75 0 4 0 -12 1.40 0.75 0 4 1 -13 6.74 0.82 0 4 1 -12 3.45 0.78 0 4 1 -11 3.40 0.68 0 4 1 -10 336.89 1.93 0 4 2 -10 48.81 0.88 0 -11 -6 3 28.95 1.30 0 -11 -5 3 7.10 0.98 0 -11 -4 3 11.43 1.08 0 -10 -7 3 38.50 1.14 0 -9 -1 3 11.11 0.69 0 -9 1 2 15.25 0.68 0 -7 -12 -1 12.88 0.85 0 -6 -6 3 187.94 1.36 0 -6 2 2 112.26 0.79 0 -5 -10 0 51.50 0.88 0 -5 -5 3 49.23 0.72 0 -4 -8 1 22.24 0.56 0 -3 -10 -2 3.48 0.41 0 -2 2 1 0.14 0.08 0 -1 -2 1 152.48 0.53 0 0 -2 0 47.97 0.19 0 0 5 -3 395.40 1.19 0 1 6 -6 259.99 1.38 0 1 7 -9 19.16 0.69 0 2 1 -3 669.47 1.43 0 2 3 -4 81.77 0.64 0 2 4 -5 625.45 1.88 0 2 6 -13 1.28 1.04 0 3 -4 -9 3.10 0.45 0 3 -3 -7 4.93 0.34 0 3 4 -14 23.46 1.21 0 3 4 -8 1.13 0.41 0 -11 -7 3 72.34 1.53 0 -11 -3 3 18.37 0.97 0 -10 -10 2 2.21 1.21 0 -10 -8 3 80.76 1.56 0 -10 3 0 4.59 0.67 0 -9 -11 1 2.60 0.96 0 -9 -8 3 14.72 1.00 0 -8 0 3 331.25 1.75 0 -8 4 0 0.18 0.39 0 -7 -9 2 46.14 0.94 0 -7 -7 3 215.24 1.62 0 -7 0 3 10.55 0.46 0 -7 2 2 83.77 0.79 0 -6 0 3 56.42 0.66 0 -5 -11 -1 5.96 0.60 0 -5 -9 1 66.31 0.86 0 -4 -11 -2 12.12 0.61 0 -4 -3 3 22.43 0.43 0 -4 -2 3 369.30 1.39 0 -3 -7 1 173.64 1.02 0 -3 -5 2 74.57 0.65 0 -2 -9 -2 37.15 0.48 0 -2 8 -8 13.20 0.68 0 -1 8 -10 12.61 0.88 0 0 4 -2 4.29 0.18 0 0 7 -7 139.35 1.13 0 1 7 -11 6.71 0.76 0 1 7 -10 4.82 0.63 0 2 -6 -8 50.96 0.59 0 2 5 -7 79.06 0.89 0 2 6 -12 55.83 1.19 0 2 6 -10 197.29 1.61 0 3 -4 -13 3.00 0.79 0 3 -4 -12 59.91 1.03 0 3 -4 -11 97.48 1.10 0 3 -4 -10 5.80 0.54 0 -11 -8 3 5.93 1.10 0 -11 -2 3 11.03 1.00 0 -11 0 2 5.55 0.91 0 -10 -1 3 0.92 0.79 0 -10 2 1 4.69 0.66 0 -9 -10 2 27.96 1.11 0 -8 -11 1 17.80 0.96 0 -8 -4 4 18.87 0.77 0 -6 -10 1 36.85 0.83 0 -6 -7 3 483.47 2.22 0 -5 -8 2 236.61 1.50 0 -5 -6 3 1.04 0.45 0 -4 -4 3 107.44 0.83 0 -4 8 -7 2.28 0.52 0 -3 1 2 486.29 1.15 0 -2 7 -5 34.13 0.53 0 -1 0 1 5235.96 2.45 0 0 6 -5 19.90 0.45 0 1 -7 -6 4.01 0.21 0 1 6 -7 226.01 1.40 0 2 5 -14 8.98 1.17 0 3 -3 -8 59.86 0.71 0 3 3 -14 3.14 0.93 0 3 4 -12 1.04 0.69 0 3 4 -10 6.34 0.59 0 -10 -9 3 1.05 1.13 0 -10 -4 4 8.33 0.95 0 -10 1 2 12.74 0.79 0 -9 -6 4 2.16 0.83 0 -9 -5 4 2.35 0.68 0 -9 -3 4 12.86 0.82 0 -9 0 3 35.16 0.83 0 -8 -5 4 16.72 0.72 0 -8 2 2 5.40 0.47 0 -7 -8 3 20.34 0.74 0 -7 -5 4 14.49 0.62 0 -7 -3 4 9.44 0.52 0 -6 -12 -1 0.83 0.73 0 -5 -12 -2 15.07 0.72 0 -4 2 2 16.24 0.30 0 -3 3 1 367.52 0.72 0 -3 8 -8 64.61 0.94 0 -2 -2 2 0.71 0.15 0 -2 8 -10 8.08 0.79 0 -2 8 -9 4.38 0.67 0 -1 -3 1 102.76 0.48 0 1 -8 -11 28.76 0.73 0 1 2 -2 607.19 1.17 0 2 -6 -9 3.05 0.43 0 2 4 -6 17.38 0.47 0 2 5 -13 40.88 1.24 0 2 5 -8 1.32 0.44 0 3 -3 -9 49.88 0.73 0 3 -2 -7 7.18 0.36 0 3 2 -14 0.96 0.99 0 3 3 -13 1.52 0.76 0 3 3 -9 3.58 0.53 0 -11 -5 4 8.85 1.14 0 -11 -1 3 52.11 1.22 0 -10 -6 4 18.45 0.99 0 -10 -3 4 1.79 0.84 0 -9 3 1 9.98 0.58 0 -8 -2 4 35.67 0.77 0 -7 -12 0 -0.56 0.84 0 -7 -11 1 24.30 0.89 0 -7 -10 2 2.93 0.76 0 -7 -6 4 244.25 1.71 0 -7 1 3 223.26 1.30 0 -6 -5 4 25.25 0.68 0 -6 -4 4 56.46 0.80 0 -6 -3 4 11.99 0.48 0 -6 -2 4 1.72 0.43 0 -4 -12 -3 10.23 0.65 0 -4 -5 3 97.23 0.83 0 -4 0 3 10.78 0.33 0 -4 8 -8 2.84 0.66 0 -3 -6 2 194.69 1.07 0 -3 8 -9 1.67 0.70 0 -2 -10 -3 0.13 0.32 0 -2 -6 1 50.30 0.51 0 -1 -7 -1 93.10 0.53 0 0 7 -12 4.10 0.85 0 1 6 -13 0.63 0.88 0 1 6 -8 18.54 0.59 0 2 -6 -10 20.60 0.60 0 2 2 -4 3.01 0.22 0 2 3 -5 0.97 0.24 0 2 5 -12 0.89 0.73 0 2 5 -10 35.02 0.83 0 3 -3 -12 13.99 0.72 0 3 -3 -10 3.83 0.56 0 3 -2 -14 1.57 0.81 0 3 -1 -14 58.29 1.36 0 3 0 -14 -0.33 0.93 0 3 1 -14 5.43 0.90 0 3 1 -7 399.32 1.64 0 3 2 -13 33.60 1.02 0 3 3 -11 10.58 0.66 0 3 3 -10 21.18 0.68 0 -11 -7 4 2.27 1.08 0 -11 -6 4 97.19 1.66 0 -11 -4 4 7.13 0.96 0 -10 0 3 8.54 0.83 0 -9 -11 2 12.56 1.09 0 -9 2 2 4.57 0.58 0 -8 -7 4 18.13 0.80 0 -8 -1 4 45.08 0.87 0 -8 1 3 5.62 0.54 0 -6 -8 3 17.96 0.64 0 -5 -10 1 30.74 0.76 0 -5 -7 3 118.48 1.07 0 -5 1 3 13.11 0.36 0 -4 -10 0 2.83 0.49 0 -1 -8 -2 87.52 0.50 0 -1 7 -7 0.71 0.45 0 0 -5 -1 8.09 0.14 0 1 3 -3 8.67 0.24 0 1 5 -6 22.94 0.52 0 1 6 -12 0.23 0.76 0 1 6 -10 -0.19 0.57 0 2 -5 -7 28.96 0.46 0 2 4 -14 8.02 0.99 0 2 4 -7 407.52 1.75 0 3 -2 -12 17.06 0.83 0 3 -1 -13 1.53 0.85 0 3 0 -13 158.62 1.66 0 3 0 -7 644.00 2.02 0 3 1 -13 222.48 1.88 0 3 1 -8 1.55 0.44 0 3 2 -12 207.63 1.74 0 3 2 -11 -0.29 0.56 0 3 2 -9 51.87 0.79 0 -10 -8 4 6.71 1.01 0 -9 -10 3 69.12 1.41 0 -9 -1 4 2.20 0.70 0 -9 4 0 0.75 0.48 0 -8 -11 2 7.81 0.91 0 -8 -8 4 4.28 0.85 0 -7 -9 3 1.02 0.64 0 -7 -7 4 104.14 1.22 0 -6 -11 1 155.39 1.49 0 -6 -6 4 223.81 1.52 0 -6 -1 4 119.94 0.98 0 -5 -11 0 59.08 0.95 0 -5 -9 2 2.42 0.55 0 -5 -4 4 150.14 1.10 0 -5 -2 4 77.87 0.77 0 -4 -11 -1 20.35 0.67 0 -4 -6 3 1.35 0.32 0 -3 -9 0 20.28 0.49 0 -3 -8 1 68.08 0.71 0 -3 -3 3 531.91 1.58 0 -3 -2 3 918.39 1.97 0 -2 -4 2 2.39 0.20 0 -2 0 2 1422.86 1.81 0 -2 7 -6 24.69 0.54 0 0 5 -4 0.28 0.25 0 1 5 -14 0.55 1.11 0 2 -2 -4 50.16 0.41 0 2 1 -4 195.18 0.87 0 2 4 -12 3.34 0.81 0 2 4 -8 147.43 1.19 0 3 -2 -11 31.83 0.75 0 3 -2 -10 1.71 0.44 0 3 -1 -11 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6 154.28 1.83 0 9 2 6 77.09 1.44 0 9 5 7 0.04 1.12 0 9 6 8 5.02 1.16 0 10 0 8 9.68 1.31 0 10 3 8 6.48 1.29 0 -10 -6 5 1.06 1.24 0 -9 -8 4 3.32 1.17 0 -9 -3 4 11.52 0.95 0 -8 -8 3 17.99 1.09 0 -8 2 7 14.69 1.01 0 -7 -3 2 119.71 1.35 0 -6 -11 4 13.19 1.14 0 -6 1 3 128.65 1.13 0 -6 3 5 23.32 0.64 0 -5 -9 2 2.15 0.67 0 -5 -7 1 106.19 1.20 0 -4 3 3 28.33 0.43 0 -3 1 1 60.08 0.49 0 -2 -11 4 61.15 1.15 0 -2 -9 2 17.35 0.67 0 -2 -5 0 129.09 0.86 0 0 9 9 14.24 0.69 0 3 4 2 16.30 0.48 0 3 8 6 74.19 1.02 0 3 10 10 0.27 1.00 0 4 -1 1 205.20 1.07 0 4 5 3 148.92 1.17 0 5 -3 2 1.44 0.40 0 5 2 2 9.54 0.45 0 6 -5 4 2.49 0.56 0 7 -3 4 19.98 0.79 0 8 -4 6 43.87 1.22 0 8 4 5 125.96 1.64 0 9 -3 7 3.17 1.25 0 9 -1 6 5.46 1.13 0 9 3 6 57.76 1.35 0 10 4 8 7.15 1.30 0 10 6 9 14.51 1.66 0 -10 -3 6 49.93 1.54 0 -10 -2 7 0.93 1.37 0 -9 -9 5 22.79 1.66 0 -9 -6 4 2.77 1.14 0 -9 -4 4 0.14 0.86 0 -9 -2 5 97.27 1.63 0 -9 1 8 16.97 1.36 0 -8 -7 3 46.00 1.22 0 -8 -3 3 31.61 0.95 0 -8 -1 4 44.28 1.01 0 -7 -11 5 -0.16 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168.73 1.44 0 7 1 3 103.12 1.20 0 7 2 3 53.24 1.01 0 7 6 5 48.81 1.10 0 8 -3 5 0.78 0.82 0 8 0 4 25.02 0.86 0 8 1 4 25.55 0.88 0 8 2 4 172.14 1.68 0 8 8 8 2.05 1.11 0 9 -2 6 -1.31 1.09 0 9 8 9 1.92 1.33 0 10 0 7 56.40 1.55 0 10 4 7 98.15 1.95 0 -10 -5 6 7.04 1.31 0 -9 -8 5 12.55 1.29 0 -8 -8 4 4.11 1.05 0 -8 -2 4 37.32 1.07 0 -7 -8 3 17.64 0.98 0 -6 -9 3 16.57 0.94 0 -6 4 7 9.37 0.70 0 -6 5 9 8.55 0.79 0 -5 -8 2 229.87 1.83 0 -5 -3 1 3.17 0.44 0 -5 5 7 59.80 0.79 0 -3 -7 1 175.26 1.27 0 -3 7 8 6.02 0.33 0 -2 -4 0 57.59 0.57 0 -1 5 3 28.64 0.20 0 2 -9 4 2.39 0.35 0 3 9 7 1.14 0.72 0 4 4 2 367.36 1.70 0 4 9 7 0.18 0.78 0 4 10 9 62.04 1.37 0 5 5 3 131.83 1.22 0 6 -4 3 24.53 0.66 0 6 -1 2 101.15 1.02 0 6 0 2 1.86 0.43 0 6 1 2 0.71 0.42 0 6 7 5 127.83 1.46 0 7 5 4 90.25 1.26 0 8 -1 4 5.79 0.77 0 8 3 4 263.80 2.06 0 8 9 9 1.63 1.22 0 9 0 5 143.42 1.78 0 9 1 5 32.25 1.08 0 9 2 5 19.05 0.99 0 9 3 5 31.78 1.25 0 9 5 6 7.61 1.02 0 10 -1 7 6.04 1.36 0 10 6 8 98.53 1.98 0 -9 -9 6 0.91 1.44 0 -9 -7 5 13.86 1.23 0 -9 -6 5 7.01 1.24 0 -9 -5 5 4.85 1.17 0 -9 -4 5 3.87 1.00 0 -9 -2 6 5.07 1.11 0 -8 -9 5 6.27 1.34 0 -8 2 8 41.78 1.29 0 -7 -2 3 5.67 0.68 0 -7 0 4 409.46 2.19 0 -7 1 5 92.66 1.19 0 -7 2 6 1.60 0.70 0 -6 -10 4 5.47 0.98 0 -6 -2 2 25.21 0.65 0 -5 0 2 156.74 1.11 0 -1 -4 0 292.88 0.98 0 1 0 0 121.27 0.42 0 3 10 9 5.97 0.89 0 5 9 7 -0.59 0.83 0 6 2 2 105.48 1.09 0 6 6 4 45.05 0.94 0 6 10 9 -0.43 1.16 0 7 -2 3 12.08 0.67 0 7 3 3 21.83 0.76 0 8 7 6 4.21 1.07 0 8 8 7 -0.56 1.15 0 9 -1 5 34.10 1.18 0 9 4 5 45.15 1.33 0 9 7 7 10.54 1.35 0 9 8 8 12.91 1.52 0 10 1 6 86.93 1.79 0 10 2 6 11.48 1.14 0 10 3 6 10.38 1.30 0 10 5 7 21.46 1.36 0 -10 -6 7 28.75 1.66 0 -10 -5 7 1.08 1.38 0 -9 -8 6 29.47 1.68 0 -9 -1 7 0.76 1.19 0 -9 0 8 1.10 1.19 0 -8 -10 6 6.80 1.44 0 -8 -7 4 18.91 1.04 0 -8 -6 4 10.08 1.03 0 -8 -3 4 32.96 1.01 0 -8 1 7 89.78 1.48 0 -7 -10 5 2.62 1.14 0 -6 -3 2 165.98 1.41 0 -5 -11 5 5.92 1.25 0 -5 -10 4 12.25 1.05 0 -5 -9 3 -0.25 0.68 0 -4 -1 1 109.79 0.84 0 1 3 1 16.88 0.26 0 2 -8 3 3.47 0.27 0 2 -1 0 11.19 0.20 0 2 6 3 67.77 0.71 0 2 9 7 1.67 0.61 0 3 6 3 33.54 0.63 0 3 7 4 1013.26 2.90 0 4 7 4 132.25 1.26 0 5 -4 2 1.29 0.37 0 6 -2 2 93.67 0.97 0 6 9 7 83.10 1.49 0 7 7 5 4.97 0.96 0 7 8 6 48.41 1.30 0 8 -2 4 10.51 0.86 0 8 6 5 13.42 0.92 0 8 9 8 9.67 1.37 0 9 -3 6 5.30 1.05 0 10 0 6 0.82 1.19 0 10 4 6 26.01 1.43 0 -8 -4 4 18.71 0.93 0 -8 0 6 36.07 1.04 0 -7 -6 3 32.41 0.96 0 -7 -5 3 64.69 1.20 0 -7 -4 3 28.68 0.92 0 -7 -3 3 86.95 1.17 0 -7 3 8 9.66 0.96 0 -6 -8 3 18.39 0.86 0 -6 3 6 7.66 0.67 0 -5 -7 2 419.10 2.27 0 -4 1 2 15.01 0.38 0 -3 -8 2 2.98 0.54 0 -2 -11 5 1.26 0.90 0 2 7 4 92.15 0.86 0 2 10 9 46.27 1.06 0 3 3 1 588.79 1.80 0 3 8 5 57.85 0.88 0 5 0 1 53.09 0.72 0 5 8 5 0.72 0.68 0 6 3 2 51.89 0.85 0 7 6 4 6.98 0.83 0 7 9 7 11.33 1.16 0 7 10 9 10.24 1.25 0 8 -4 5 0.90 0.82 0 9 -2 5 4.00 0.97 0 9 5 5 62.91 1.36 0 10 -1 6 5.54 1.22 0 10 5 6 6.18 1.31 0 11 2 7 4.83 1.36 0 11 3 7 0.12 1.31 0 -9 -5 6 1.01 1.22 0 -9 -2 7 22.17 1.37 0 -8 -9 6 18.16 1.57 0 -8 2 9 0.04 1.06 0 -7 -1 4 22.10 0.75 0 -6 -9 4 1.59 0.84 0 -6 1 4 298.46 1.69 0 -6 2 5 8.11 0.57 0 -4 -9 3 4.39 0.65 0 -4 -5 1 512.88 2.06 0 -4 -2 1 247.39 1.27 0 -3 -11 5 3.58 0.97 0 -2 -8 2 267.21 1.53 0 -1 -10 4 12.96 0.73 0 -1 -8 2 74.07 0.80 0 2 0 0 89.10 0.51 0 2 5 2 30.36 0.49 0 3 5 2 278.44 1.39 0 4 10 8 13.63 1.00 0 5 1 1 46.23 0.67 0 5 10 8 87.61 1.50 0 6 10 8 16.34 1.28 0 8 0 3 50.06 1.05 0 8 1 3 208.07 1.75 0 8 2 3 23.65 0.86 0 8 5 4 7.65 0.80 0 9 1 4 35.47 1.06 0 9 2 4 217.86 2.01 0 9 3 4 168.05 1.90 0 9 8 7 10.19 1.21 0 10 7 7 27.61 1.62 0 11 4 7 109.04 2.12 0 -9 -8 7 85.82 2.02 0 -8 -7 5 1.81 0.98 0 -8 -3 5 67.76 1.35 0 -7 -7 4 105.69 1.62 0 -7 2 7 0.66 0.82 0 -6 -7 3 498.87 2.70 0 -6 -1 3 4.95 0.48 0 -5 -8 3 57.78 1.16 0 -5 -6 2 39.00 0.81 0 -5 -1 2 34.25 0.61 0 -5 1 3 13.70 0.47 0 -5 4 6 238.92 1.34 0 -4 -4 1 89.90 0.88 0 -4 5 6 179.31 0.98 0 -3 -10 4 3.50 0.80 0 -3 -9 3 7.96 0.70 0 -3 0 1 578.92 1.51 0 -3 2 2 14.62 0.30 0 -1 -9 3 2.98 0.54 0 -1 -3 0 376.61 1.01 0 0 8 6 1.49 0.36 0 0 9 8 0.71 0.47 0 2 8 5 18.59 0.56 0 3 10 8 88.35 1.26 0 4 5 2 49.26 0.73 0 5 2 1 228.99 1.38 0 6 -6 4 2.87 0.54 0 6 4 2 78.02 1.07 0 6 8 5 15.12 0.82 0 7 0 2 44.99 0.90 0 7 1 2 190.48 1.52 0 7 2 2 248.15 1.78 0 8 -3 4 15.95 0.86 0 8 3 3 3.65 0.70 0 8 7 5 3.85 0.90 0 8 9 7 12.19 1.33 0 9 0 4 -0.05 0.75 0 9 4 4 11.84 1.05 0 9 6 5 29.01 1.17 0 9 9 8 -0.19 1.28 0 10 1 5 -0.08 0.96 0 10 2 5 5.44 1.03 0 10 3 5 6.48 1.04 0 11 5 7 -3.28 1.37 0 -9 -7 7 70.38 1.82 0 -8 -8 6 4.59 1.18 0 -8 -5 5 10.13 1.04 0 -8 -4 5 27.37 1.03 0 -8 0 7 15.51 1.05 0 -7 -2 4 4.31 0.61 0 -7 1 6 37.40 1.00 0 -5 -10 5 30.94 1.25 0 -4 -7 2 247.76 1.64 0 -2 -9 3 43.01 0.84 0 -1 -2 0 943.82 1.43 0 1 7 4 494.08 1.59 0 1 9 7 0.61 0.53 0 3 9 6 -0.30 0.60 0 5 -2 1 40.25 0.60 0 5 5 2 529.09 2.30 0 6 6 3 35.98 0.86 0 6 9 6 3.03 0.79 0 7 8 5 7.81 1.01 0 8 -1 3 10.40 0.70 0 8 4 3 106.82 1.46 0 8 6 4 114.87 1.55 0 9 -3 5 17.52 1.13 0 9 -1 4 22.52 1.08 0 10 0 5 11.60 1.06 0 10 4 5 10.67 1.13 0 11 1 6 48.98 1.74 0 11 2 6 3.20 1.25 0 11 3 6 59.75 1.68 0 11 4 6 2.11 1.46 0 11 6 7 13.71 1.50 0 -9 -2 8 48.79 1.49 0 -9 -1 9 5.95 1.21 0 -7 -10 7 12.75 1.60 0 -7 -9 6 -0.28 1.24 0 -7 -8 5 41.07 1.28 0 -7 -5 4 16.59 0.91 0 -7 -3 4 9.86 0.77 0 -7 3 9 0.77 0.92 0 -6 -10 6 3.85 1.26 0 -6 -8 4 0.75 0.74 0 -6 -6 3 193.11 1.67 0 -6 -2 3 8.40 0.53 0 -5 -2 2 125.60 1.06 0 -5 2 4 190.64 1.20 0 -5 3 5 337.04 1.57 0 -5 5 8 0.03 0.61 0 -1 -6 1 766.04 1.91 0 1 -10 5 48.27 0.81 0 1 10 9 0.34 0.67 0 3 -1 0 33.72 0.39 0 3 0 0 882.74 1.88 0 5 10 7 7.40 0.92 0 6 -5 3 8.36 0.53 0 6 10 7 4.79 1.06 0 7 -1 2 17.75 0.63 0 7 3 2 33.67 0.82 0 7 9 6 15.41 0.97 0 9 8 6 6.38 1.13 0 10 -1 5 4.55 1.13 0 10 5 5 256.63 2.49 0 10 7 6 25.67 1.56 0 11 5 6 73.56 1.89 0 -9 -6 8 62.96 1.94 0 -9 -3 8 68.56 1.66 0 -8 -7 6 99.53 1.74 0 -8 1 9 22.76 1.33 0 -7 -4 4 61.52 1.11 0 -6 -9 5 10.08 0.96 0 -6 -3 3 0.56 0.48 0 -6 0 4 9.76 0.59 0 -5 -11 7 43.09 1.66 0 -5 -7 3 126.85 1.43 0 -5 -3 2 186.98 1.31 0 -4 -10 5 123.19 1.66 0 -4 -8 3 241.30 1.79 0 -4 2 3 1.55 0.28 0 -4 6 8 0.27 0.46 0 -3 -11 6 3.53 1.10 0 -2 1 1 434.01 0.96 0 -1 -11 6 1.66 0.92 0 2 10 8 39.92 0.94 0 6 0 1 72.77 0.91 0 6 1 1 200.80 1.39 0 7 6 3 130.37 1.47 0 8 -5 5 0.64 0.88 0 8 -2 3 1.28 0.72 0 8 8 5 1.91 1.06 0 9 -2 4 29.66 1.06 0 9 7 5 -0.10 0.97 0 -9 -5 8 0.64 1.28 0 -9 -4 8 0.12 1.20 0 -9 -2 9 25.55 1.44 0 -8 -6 6 5.66 1.01 0 -8 -5 6 43.51 1.36 0 -8 -4 6 76.02 1.51 0 -8 0 8 3.76 1.07 0 -7 -7 5 4.01 0.88 0 -7 2 8 60.69 1.25 0 -6 -7 4 68.24 1.21 0 -5 0 3 1.35 0.42 0 -4 -9 4 59.27 1.09 0 -4 -6 2 46.72 0.78 0 -4 0 2 394.76 1.49 0 -4 4 5 89.74 0.74 0 -3 -1 1 1.25 0.22 0 -2 -11 6 0.00 0.94 0 3 1 0 197.48 0.95 0 4 -4 1 1.48 0.24 0 4 4 1 283.26 1.47 0 4 8 4 106.05 1.18 0 5 7 3 -0.36 0.51 0 6 -1 1 1.46 0.44 0 6 2 1 125.24 1.16 0 7 -2 2 1.67 0.54 0 8 -4 4 7.46 0.83 0 9 1 3 24.86 0.94 0 9 2 3 133.80 1.62 0 9 3 3 16.48 0.93 0 10 1 4 4.98 1.08 0 10 2 4 69.83 1.45 0 10 3 4 0.77 0.96 0 10 4 4 90.71 1.72 0 11 2 5 -0.07 1.33 0 11 3 5 3.12 1.37 0 11 6 6 69.13 1.84 0 -9 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242.10 2.03 0 -7 -4 5 17.93 0.91 0 -7 -3 5 8.74 0.83 0 -6 -9 6 24.46 1.19 0 -6 -1 4 115.95 1.16 0 -5 -6 3 1.50 0.54 0 -3 -3 1 269.87 1.23 0 -3 3 3 104.07 0.60 0 -2 -10 5 0.68 0.77 0 2 -10 6 8.15 0.69 0 3 6 2 4.74 0.43 0 4 -1 0 114.20 0.78 0 4 0 0 1044.39 2.35 0 5 -5 2 28.28 0.46 0 5 10 6 2.64 0.84 0 5 11 8 13.95 1.19 0 6 -4 2 1.95 0.44 0 6 10 6 45.66 1.30 0 7 8 4 73.69 1.30 0 7 9 5 20.81 1.02 0 8 4 2 248.49 2.03 0 9 -1 3 12.92 0.90 0 9 7 4 8.29 1.13 0 11 0 5 1.90 1.33 0 -8 -5 7 146.88 1.94 0 -7 -9 8 77.46 1.90 0 -7 -8 7 15.12 1.38 0 -7 -7 6 1.51 0.91 0 -7 -1 6 55.49 1.16 0 -7 2 9 80.60 1.47 0 -6 -10 8 7.87 1.55 0 -5 -1 3 470.03 1.96 0 -5 1 4 114.70 1.00 0 -5 4 7 26.52 0.69 0 -4 -10 6 63.91 1.47 0 -4 -7 3 450.86 2.24 0 -4 -1 2 1746.37 3.24 0 -3 -11 7 1.60 1.14 0 -2 -9 4 9.78 0.68 0 -2 -8 3 32.16 0.72 0 2 7 3 129.62 0.95 0 3 2 0 170.51 0.93 0 3 9 5 36.27 0.78 0 4 11 8 161.47 1.74 0 6 -2 1 207.18 1.30 0 7 1 1 21.53 0.67 0 7 2 1 14.04 0.63 0 8 -3 3 0.92 0.67 0 8 -1 2 6.94 0.71 0 9 -3 4 41.24 1.14 0 10 -1 4 0.87 1.12 0 11 6 5 1.45 1.26 0 -8 -6 8 108.26 1.90 0 -8 -2 8 15.62 1.07 0 -8 -1 9 2.57 1.24 0 -8 0 10 -0.05 1.27 0 -7 -6 6 19.86 1.00 0 -7 1 8 1.56 0.91 0 -6 -3 4 11.81 0.62 0 -6 0 5 445.46 2.20 0 -6 3 8 4.64 0.74 0 -5 -10 7 0.77 1.07 0 -5 -7 4 6.53 0.67 0 -4 -9 5 2.22 0.85 0 -4 -8 4 216.73 1.76 0 -4 -4 2 40.76 0.65 0 -3 4 4 184.01 0.79 0 -2 -11 7 4.70 1.04 0 -1 -9 4 40.98 0.84 0 0 -9 4 1.46 0.52 0 2 2 0 9999.99 5.91 0 2 8 4 22.74 0.57 0 4 5 1 37.00 0.68 0 4 10 6 1.03 0.75 0 7 0 1 121.90 1.19 0 7 3 1 81.87 1.08 0 8 5 2 1.93 0.68 0 8 7 3 0.02 0.90 0 8 10 6 1.07 1.10 0 9 6 3 347.03 2.59 0 10 1 3 12.59 1.08 0 10 2 3 0.39 0.87 0 10 3 3 4.48 0.94 0 10 4 3 44.35 1.45 0 10 8 5 26.64 1.44 0 11 2 4 0.92 1.27 0 11 3 4 5.19 1.15 0 11 4 4 19.29 1.45 0 11 7 5 80.13 2.01 0 -8 -7 9 5.91 1.40 0 -8 -5 8 0.41 1.11 0 -8 -3 8 1.28 1.00 0 -7 -8 8 18.70 1.54 0 -7 -5 6 30.88 1.05 0 -6 1 6 187.59 1.51 0 -6 2 7 0.48 0.64 0 -5 -8 5 38.39 1.03 0 -5 -2 3 239.33 1.46 0 -5 2 5 425.10 1.84 0 -5 3 6 45.36 0.75 0 -4 1 3 527.14 1.72 0 -3 -10 6 2.41 0.97 0 -3 1 2 488.79 1.36 0 -1 -8 3 108.51 0.98 0 0 6 3 2.91 0.21 0 1 4 1 1056.96 1.79 0 2 6 2 8.55 0.37 0 2 10 7 116.77 1.14 0 3 5 1 744.94 2.18 0 5 0 0 202.21 1.20 0 5 2 0 408.71 1.81 0 6 8 3 38.44 1.01 0 6 9 4 6.73 0.84 0 6 11 7 75.13 1.54 0 7 -1 1 117.50 1.18 0 7 11 7 13.06 1.20 0 9 -2 3 3.60 0.85 0 9 1 2 67.69 1.26 0 9 2 2 74.75 1.27 0 9 3 2 1.00 0.74 0 9 4 2 8.68 0.96 0 9 8 4 0.41 1.00 0 9 9 5 20.56 1.28 0 10 5 3 36.94 1.37 0 10 7 4 7.98 1.14 0 11 1 4 3.62 1.25 0 11 5 4 15.32 1.31 0 -8 -6 9 21.89 1.45 0 -8 -2 9 0.29 1.05 0 -8 -1 10 38.36 1.57 0 -7 -4 6 13.84 0.88 0 -7 -1 7 2.10 0.82 0 -6 -9 8 2.08 1.37 0 -6 -6 5 78.75 1.24 0 -4 -6 3 0.90 0.45 0 -4 5 7 16.67 0.55 0 -4 6 9 1.95 0.61 0 1 9 6 1.07 0.41 0 1 10 8 31.15 0.67 0 4 3 0 34.46 0.60 0 4 8 3 10.11 0.61 0 5 7 2 335.02 1.95 0 5 9 4 145.39 1.44 0 5 11 7 29.76 1.13 0 6 5 1 49.36 0.87 0 6 10 5 0.05 0.88 0 7 8 3 71.67 1.33 0 7 9 4 0.54 0.79 0 8 -2 2 25.29 0.84 0 8 2 1 122.00 1.42 0 8 6 2 362.45 2.49 0 9 0 2 9.47 0.89 0 10 -2 4 11.69 1.16 0 10 0 3 1.96 1.00 0 11 0 4 2.97 1.27 0 11 6 4 22.02 1.38 0 11 8 5 25.16 1.78 0 -8 -6 10 -1.33 1.42 0 -8 -5 9 13.07 1.30 0 -8 -4 9 4.05 1.19 0 -8 -3 9 92.12 1.75 0 -8 -2 10 63.16 1.85 0 -7 -8 9 15.49 1.48 0 -7 -6 7 63.79 1.39 0 -7 1 9 0.92 0.85 0 -6 -8 7 51.30 1.40 0 -6 -7 6 10.86 0.90 0 -6 -5 5 1.72 0.63 0 -6 -1 5 241.39 1.68 0 -6 3 9 13.45 0.93 0 -5 -9 7 0.97 1.08 0 -5 0 4 137.59 1.13 0 -3 -9 5 28.77 0.89 0 -3 -5 2 71.93 0.78 0 -2 -10 6 0.34 0.81 0 -2 0 1 437.66 1.07 0 -2 5 4 86.34 0.39 0 -2 8 9 0.60 0.39 0 0 7 4 646.46 1.30 0 0 9 7 4.95 0.33 0 2 9 5 18.19 0.57 0 3 10 6 36.02 0.84 0 4 9 4 58.59 0.99 0 5 10 5 2.51 0.83 0 6 -3 1 50.54 0.71 0 7 5 1 54.77 1.08 0 7 7 2 4.56 0.83 0 7 10 5 4.58 0.94 0 8 1 1 162.16 1.51 0 8 3 1 250.89 1.92 0 8 8 3 4.29 0.99 0 10 8 4 10.34 1.38 0 -8 -4 10 1.47 1.45 0 -8 -3 10 46.96 1.59 0 -7 -4 7 48.62 1.29 0 -7 -3 7 7.56 0.95 0 -7 -2 7 -0.07 0.71 0 -6 -9 9 13.05 1.44 0 -6 -4 5 78.81 1.15 0 -6 -3 5 32.59 0.91 0 -6 -2 5 2.90 0.55 0 -5 -8 6 76.57 1.42 0 -5 -7 5 53.54 1.08 0 -4 -9 6 72.22 1.30 0 -4 -7 4 93.31 1.16 0 -3 -10 7 43.51 1.32 0 -3 7 9 5.36 0.52 0 -2 -3 1 930.22 1.96 0 0 -10 6 19.18 0.89 0 2 5 1 993.24 2.19 0 4 11 7 7.13 0.87 0 6 0 0 158.35 1.22 0 6 2 0 162.53 1.28 0 6 11 6 1.93 1.02 0 7 -6 4 15.40 0.63 0 7 -5 3 26.02 0.69 0 7 -2 1 126.60 1.15 0 7 11 6 3.86 1.23 0 8 -4 3 23.78 0.83 0 8 0 1 447.09 2.35 0 8 4 1 315.89 2.17 0 8 11 6 6.75 1.33 0 9 -4 4 36.18 1.12 0 9 -1 2 35.80 1.06 0 9 6 2 6.37 0.99 0 9 10 5 43.91 1.72 0 10 -1 3 24.86 1.21 0 10 3 2 9.68 1.14 0 11 2 3 20.13 1.33 0 11 3 3 54.04 1.50 0 11 4 3 0.75 1.07 0 11 7 4 3.60 1.27 0 12 4 4 4.77 1.41 0 12 5 4 4.14 1.61 0 -8 -3 11 35.61 1.79 0 -7 -7 9 12.60 1.29 0 -7 -6 8 5.35 1.02 0 -7 -1 8 17.13 1.01 0 -7 1 10 2.93 0.96 0 -6 2 8 -0.08 0.75 0 -4 -10 8 6.83 1.11 0 -4 0 3 10.87 0.42 0 -4 2 4 115.95 0.86 0 -3 6 7 95.09 0.72 0 -2 -9 5 0.36 0.68 0 -2 -7 3 17.21 0.57 0 1 2 0 973.12 1.47 0 2 -9 5 13.17 0.57 0 2 3 0 565.99 1.50 0 3 7 2 8.32 0.46 0 3 8 3 23.90 0.61 0 4 6 1 221.67 1.42 0 4 10 5 1.14 0.69 0 5 -2 0 112.28 0.86 0 5 4 0 8.31 0.51 0 6 6 1 95.79 1.16 0 8 7 2 75.35 1.31 0 9 -3 3 -0.94 0.85 0 9 8 3 7.23 1.02 0 10 1 2 10.35 1.03 0 10 2 2 37.21 1.14 0 10 4 2 1.56 0.93 0 11 1 3 8.91 1.29 0 11 5 3 16.68 1.26 0 -7 -2 8 23.60 1.11 0 -7 1 11 1.76 1.30 0 -6 3 10 8.52 0.95 0 -5 -9 8 52.90 1.49 0 -5 1 5 236.01 1.43 0 -5 3 7 104.92 1.10 0 -4 -10 9 43.78 1.67 0 -4 3 5 30.90 0.56 0 -3 -9 6 179.13 1.78 0 -3 -6 3 12.30 0.57 0 -3 -4 2 36.97 0.56 0 -3 0 2 0.11 0.22 0 -2 -10 7 36.09 1.23 0 -2 -8 4 1.03 0.53 0 -2 -2 1 2.48 0.19 0 -2 -1 1 51.40 0.42 0 -1 -9 5 -0.77 0.64 0 1 7 3 0.11 0.27 0 3 9 4 0.73 0.50 0 4 4 0 326.15 1.56 0 5 11 6 65.94 1.31 0 6 -1 0 539.90 2.05 0 6 4 0 1.57 0.46 0 6 9 3 1.42 0.77 0 7 -4 2 6.47 0.53 0 7 1 0 35.92 0.83 0 7 2 0 5.78 0.54 0 7 3 0 134.56 1.37 0 7 9 3 8.41 0.99 0 8 -3 2 16.90 0.77 0 8 -1 1 33.52 0.87 0 9 2 1 183.18 1.75 0 9 3 1 127.30 1.55 0 9 4 1 250.73 2.15 0 10 5 2 -0.48 0.92 0 10 9 4 2.71 1.24 0 11 6 3 10.75 1.27 0 11 8 4 50.10 1.74 0 -7 -3 8 50.51 1.25 0 -7 0 10 131.58 1.87 0 -6 -8 9 15.89 1.34 0 -6 3 11 10.15 1.09 0 -5 -7 6 128.41 1.54 0 -5 2 6 1.62 0.49 0 -4 -9 7 71.68 1.38 0 -4 -6 4 270.74 1.74 0 -4 -1 3 51.26 0.67 0 -4 6 10 52.70 0.98 0 -3 -10 8 24.34 1.29 0 -1 -4 1 495.61 1.34 0 0 -9 5 5.87 0.63 0 1 -9 5 1.45 0.57 0 1 -5 1 323.22 0.79 0 1 6 2 140.53 0.75 0 3 -8 4 13.91 0.37 0 3 4 0 68.08 0.68 0 4 -3 0 206.53 0.88 0 5 9 3 1.87 0.67 0 6 8 2 15.59 0.75 0 6 10 4 6.35 0.90 0 7 0 0 50.36 0.88 0 7 8 2 481.12 2.71 0 7 10 4 -0.04 0.85 0 8 6 1 21.68 0.98 0 8 9 3 73.92 1.42 0 9 -2 2 8.07 0.86 0 9 1 1 16.36 0.82 0 9 5 1 4.84 0.94 0 10 -2 3 3.98 1.01 0 10 0 2 0.73 0.94 0 11 0 3 11.70 1.23 0 -7 -6 10 -0.10 1.22 0 -7 -5 9 16.87 1.20 0 -6 -8 10 48.53 1.88 0 -6 -3 6 9.81 0.68 0 -6 -2 6 39.99 0.89 0 -6 1 8 2.64 0.73 0 -6 2 9 15.38 0.82 0 -5 4 9 41.84 0.96 0 -4 -8 6 2.03 0.70 0 -4 -7 5 0.19 0.58 0 -4 -3 3 22.43 0.52 0 -4 -2 3 365.96 1.62 0 -4 5 8 14.43 0.60 0 -3 -7 4 77.76 1.00 0 -3 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-3 1 0.22 0.50 0 7 5 0 114.39 1.35 0 8 -2 1 18.59 0.78 0 8 1 0 208.77 1.71 0 8 2 0 0.62 0.58 0 8 3 0 21.12 0.79 0 8 4 0 2.91 0.76 0 9 6 1 8.83 0.88 0 9 8 2 9.16 1.00 0 10 -1 2 258.03 2.13 0 10 2 1 246.78 2.20 0 10 3 1 183.42 1.94 0 10 4 1 -1.04 1.00 0 10 9 3 21.53 1.53 0 10 10 4 136.08 2.18 0 11 6 2 68.65 1.78 0 12 6 3 64.98 1.88 0 -7 -5 11 0.37 1.33 0 -7 -4 10 17.09 1.24 0 -6 -7 10 5.75 1.43 0 -6 -6 8 3.16 0.90 0 -6 -1 7 5.13 0.65 0 -6 2 10 29.23 1.04 0 -5 -7 7 79.79 1.37 0 -5 -6 6 0.32 0.65 0 -5 4 10 37.29 1.05 0 -4 1 4 66.20 0.71 0 -3 7 10 32.08 0.79 0 -2 2 2 57.47 0.37 0 2 7 2 219.27 1.14 0 2 8 3 318.46 1.41 0 4 1 -1 110.61 0.85 0 5 11 5 10.26 0.88 0 7 -1 0 155.85 1.24 0 10 1 1 30.34 1.14 0 10 5 1 14.62 1.05 0 11 1 2 5.17 1.05 0 -7 -4 11 55.16 1.67 0 -7 -3 11 59.63 1.63 0 -7 -3 12 33.10 1.74 0 -7 -2 12 71.65 1.94 0 -6 -6 9 26.16 1.32 0 -6 -5 8 77.55 1.37 0 -6 -3 7 606.76 2.96 0 -6 0 8 11.54 0.74 0 -6 1 9 -0.16 0.69 0 -6 2 11 22.84 1.27 0 -5 -2 5 0.98 0.43 0 -5 1 6 155.43 1.24 0 -5 2 7 83.11 1.04 0 -4 -9 9 18.43 1.24 0 -4 -6 5 12.75 0.73 0 -3 5 6 0.81 0.34 0 -2 -10 9 28.55 1.45 0 -2 -8 5 345.71 1.99 0 -2 -6 3 40.81 0.66 0 -1 -10 8 86.92 1.49 0 0 -7 3 15.37 0.46 0 1 10 7 20.67 0.50 0 2 4 0 55.26 0.53 0 4 0 -1 68.58 0.66 0 4 10 4 6.01 0.68 0 5 1 -1 0.67 0.33 0 5 2 -1 524.13 2.01 0 6 -4 1 83.01 0.75 0 6 6 0 462.40 2.35 0 7 9 2 203.54 1.93 0 7 10 3 0.65 0.80 0 8 0 0 316.94 1.94 0 8 9 2 1.84 1.00 0 8 11 4 0.76 1.19 0 9 -4 3 3.50 0.80 0 9 -1 1 35.69 0.91 0 9 3 0 30.24 1.06 0 9 7 1 6.55 0.89 0 9 10 3 165.11 2.20 0 10 6 1 34.61 1.23 0 11 7 2 12.58 1.30 0 12 4 2 138.76 2.25 0 -6 -4 8 163.60 1.82 0 -6 -1 8 15.10 0.87 0 -6 1 10 6.03 0.97 0 -5 -8 10 16.07 1.35 0 -5 -7 8 66.41 1.38 0 -5 -6 7 9.82 0.91 0 -5 -5 6 4.76 0.62 0 -5 4 11 24.97 1.10 0 -4 5 9 26.44 0.80 0 -3 -9 8 31.96 1.15 0 -3 -7 5 10.44 0.70 0 -3 3 4 71.62 0.58 0 -2 -7 4 80.96 0.93 0 -2 -4 2 2.68 0.32 0 1 5 1 50.39 0.46 0 2 6 1 15.90 0.41 0 2 9 4 52.66 0.70 0 3 0 -1 614.18 1.54 0 3 5 0 18.15 0.44 0 5 0 -1 6.99 0.37 0 5 3 -1 3.32 0.38 0 5 6 0 7.51 0.51 0 6 1 -1 1.37 0.40 0 6 2 -1 189.72 1.37 0 6 3 -1 86.51 1.00 0 6 8 1 72.17 1.15 0 6 9 2 0.01 0.63 0 7 6 0 33.54 0.87 0 7 8 1 9.17 0.88 0 8 -5 3 62.53 0.91 0 8 -4 2 32.80 0.80 0 8 6 0 5.90 0.85 0 9 -3 2 15.48 0.88 0 9 1 0 125.98 1.50 0 9 2 0 40.45 1.00 0 9 4 0 2.24 0.77 0 9 5 0 4.73 0.92 0 9 9 2 7.38 1.07 0 9 11 4 5.04 1.25 0 10 0 1 74.16 1.38 0 11 0 2 2.03 0.97 0 11 3 1 45.11 1.48 0 11 4 1 35.33 1.45 0 12 3 2 130.89 2.09 0 12 5 2 13.92 1.44 0 12 6 2 1.38 1.54 0 -6 -6 11 5.02 1.45 0 -6 -5 9 45.51 1.27 0 -6 -3 8 300.21 2.24 0 -6 -2 8 -0.65 0.67 0 -6 0 9 1.56 0.72 0 -5 -8 11 -1.52 1.37 0 -5 -7 9 77.61 1.65 0 -5 0 6 475.84 2.16 0 -5 3 9 3.12 0.73 0 -4 -8 8 2.74 0.88 0 -4 3 6 23.26 0.55 0 -3 -4 3 1.84 0.32 0 -3 4 5 -0.21 0.25 0 -1 -3 1 103.19 0.57 0 0 -9 6 13.18 0.73 0 1 3 0 371.21 0.98 0 1 9 5 3.42 0.35 0 3 2 -1 296.96 1.21 0 3 8 2 18.61 0.55 0 3 9 3 43.40 0.77 0 5 10 3 -0.15 0.69 0 6 0 -1 180.85 1.27 0 6 4 -1 45.29 0.85 0 6 11 4 6.03 0.92 0 7 -2 0 209.66 1.39 0 7 2 -1 7.94 0.55 0 8 -1 0 264.25 1.75 0 9 8 1 14.86 1.22 0 10 -2 2 2.19 0.91 0 10 9 2 1.13 1.17 0 11 2 1 2.60 1.14 0 11 5 1 35.09 1.36 0 11 6 1 22.38 1.45 0 -6 -6 12 13.10 1.52 0 -6 -3 9 3.98 0.96 0 -6 -1 9 38.68 1.06 0 -6 0 10 3.54 0.99 0 -6 1 11 38.76 1.22 0 -5 -6 8 55.97 1.31 0 -5 1 7 286.45 1.78 0 -4 -7 7 3.41 0.73 0 -4 -5 5 1.95 0.49 0 -4 -1 4 30.03 0.55 0 -3 1 3 342.48 1.21 0 -1 -8 5 0.01 0.55 0 1 -9 6 0.21 0.65 0 3 -1 -1 58.95 0.49 0 3 7 1 1.89 0.39 0 3 11 6 12.49 0.72 0 4 6 0 33.46 0.63 0 4 11 5 0.31 0.70 0 5 -1 -1 65.24 0.70 0 5 4 -1 96.36 0.97 0 7 1 -1 0.58 0.45 0 7 4 -1 69.38 1.04 0 7 7 0 153.18 1.61 0 8 -3 1 9.25 0.66 0 9 -2 1 91.33 1.24 0 9 0 0 5.24 0.82 0 10 3 0 7.54 0.91 0 10 4 0 5.84 0.93 0 11 1 1 10.28 1.15 0 -6 -5 11 12.14 1.23 0 -6 -5 12 45.42 1.82 0 -6 -4 10 12.39 1.08 0 -6 -2 9 7.23 0.84 0 -5 -2 6 185.75 1.47 0 -5 3 10 91.54 1.34 0 -3 -9 10 2.24 1.31 0 -2 -9 8 116.95 1.57 0 -2 -8 6 470.36 2.40 0 -1 -9 7 24.13 0.93 0 2 -7 3 156.63 0.80 0 3 3 -1 264.56 1.19 0 4 4 -1 87.31 0.84 0 5 11 4 13.33 0.90 0 6 -3 0 20.43 0.52 0 6 5 -1 208.24 1.58 0 6 12 5 2.66 1.06 0 7 -5 2 3.59 0.49 0 7 5 -1 789.88 3.16 0 7 10 2 4.67 0.92 0 8 2 -1 107.97 1.27 0 8 3 -1 62.20 1.07 0 8 7 0 3.43 0.78 0 8 10 2 1.79 0.89 0 8 11 3 11.54 1.29 0 9 11 3 2.89 1.34 0 10 -1 1 30.65 1.12 0 10 2 0 62.17 1.26 0 10 6 0 44.56 1.41 0 10 8 1 8.20 1.13 0 11 7 1 18.82 1.33 0 11 9 2 3.04 1.37 0 12 4 1 -0.62 1.36 0 12 5 1 109.82 2.14 0 -6 -4 11 8.20 1.15 0 -6 -4 12 3.74 1.36 0 -6 -3 10 1.58 0.92 0 -6 -3 11 19.74 1.34 0 -6 -2 10 2.79 0.88 0 -6 0 12 -0.76 1.09 0 -5 -7 12 3.37 1.45 0 -5 -6 9 4.11 0.93 0 -5 -5 8 0.19 0.83 0 -5 0 7 59.91 0.99 0 -5 3 11 47.47 1.27 0 -4 -7 8 6.62 0.96 0 -4 4 8 5.24 0.55 0 -3 -8 8 1.96 0.95 0 -3 -7 6 21.68 0.75 0 -2 -9 9 0.31 1.05 0 -2 -7 5 263.04 1.68 0 -2 -3 2 0.31 0.21 0 0 -8 5 0.54 0.53 0 2 1 -1 52.37 0.44 0 2 11 7 13.03 0.58 0 3 10 4 3.74 0.55 0 4 9 2 44.86 0.83 0 5 5 -1 0.49 0.40 0 5 7 0 183.41 1.42 0 6 -1 -1 61.35 0.77 0 7 -4 1 0.20 0.46 0 7 9 1 33.10 0.99 0 7 11 3 27.35 1.19 0 8 1 -1 7.51 0.70 0 8 5 -1 48.30 1.11 0 9 7 0 29.86 1.10 0 9 9 1 3.12 0.99 0 10 1 0 61.80 1.23 0 10 10 2 87.39 1.84 0 11 8 1 11.30 1.48 0 12 3 1 53.70 1.60 0 12 6 1 1.35 1.31 0 -6 -3 12 5.96 1.23 0 -6 -2 11 7.31 1.06 0 -6 -2 12 1.51 1.29 0 -6 -2 13 -0.09 1.45 0 -6 -1 12 1.43 1.11 0 -5 -6 10 0.66 0.99 0 -5 1 8 63.25 1.03 0 -5 2 9 -0.20 0.58 0 -4 -6 7 16.37 0.87 0 -3 -2 3 884.77 2.23 0 -1 -9 8 14.52 1.01 0 2 0 -1 430.53 1.06 0 2 5 0 127.05 0.81 0 3 6 0 24.81 0.54 0 6 10 2 4.39 0.70 0 6 11 3 46.19 1.16 0 7 6 -1 459.74 2.51 0 7 8 0 16.92 0.95 0 7 12 4 7.53 1.15 0 8 -2 0 1.26 0.58 0 9 -1 0 6.32 0.77 0 9 2 -1 146.38 1.63 0 9 3 -1 17.62 0.84 0 10 7 0 0.35 0.96 0 10 9 1 1.50 1.17 0 11 0 1 -1.18 0.91 0 11 3 0 113.08 1.74 0 11 4 0 30.23 1.28 0 11 5 0 17.33 1.21 0 11 6 0 0.47 1.26 0 -5 -5 9 45.10 1.15 0 -5 -4 8 7.89 0.74 0 -5 -2 7 30.15 0.79 0 -4 -7 9 0.52 0.90 0 -4 0 5 231.11 1.34 0 -3 -7 7 32.03 0.99 0 -3 -1 3 60.47 0.60 0 -3 5 7 288.06 1.34 0 -3 6 9 86.53 0.96 0 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1.05 0 11 1 0 7.63 1.09 0 11 7 0 -0.32 1.14 0 12 4 0 1.69 1.35 0 12 5 0 6.51 1.48 0 -5 -5 12 3.15 1.19 0 -5 -5 13 2.02 1.37 0 -5 -4 9 39.55 1.07 0 -5 -2 8 29.12 0.85 0 -4 -7 11 10.71 1.23 0 -4 -7 12 -1.98 1.31 0 -4 -5 7 2.18 0.57 0 -3 -8 11 -0.17 1.16 0 -3 -7 8 3.08 0.85 0 -3 -6 6 0.19 0.51 0 -3 -5 5 217.23 1.45 0 -2 -8 8 213.28 1.89 0 -2 -7 6 10.34 0.67 0 -2 7 8 54.12 0.64 0 -1 -7 5 81.08 0.96 0 -1 -4 2 84.13 0.62 0 1 7 2 33.80 0.41 0 2 -8 5 8.14 0.50 0 2 -1 -1 439.67 0.95 0 2 8 2 7.98 0.40 0 5 1 -2 35.48 0.62 0 5 2 -2 122.57 1.01 0 5 3 -2 184.66 1.28 0 5 8 0 44.63 0.88 0 5 11 3 45.41 1.03 0 6 -2 -1 1.33 0.41 0 6 1 -2 28.93 0.67 0 6 2 -2 27.81 0.64 0 6 3 -2 163.74 1.31 0 7 2 -2 16.34 0.70 0 7 3 -2 116.77 1.23 0 7 4 -2 350.03 2.09 0 7 7 -1 5.46 0.68 0 7 11 2 3.17 1.05 0 8 9 0 45.09 1.30 0 9 -3 1 8.83 0.71 0 9 7 -1 137.72 1.80 0 10 2 -1 1.09 0.78 0 10 6 -1 0.73 0.93 0 10 10 1 5.94 1.25 0 11 -1 1 169.54 1.88 0 12 3 0 10.77 1.40 0 12 6 0 8.38 1.38 0 -5 -4 10 0.10 0.83 0 -5 -4 12 3.07 1.27 0 -5 -4 13 9.80 1.53 0 -5 -2 9 68.53 1.26 0 -5 -1 9 25.11 0.94 0 -4 -6 9 21.31 0.98 0 -4 3 8 33.09 0.75 0 -4 4 10 0.43 0.70 0 -3 -3 4 713.67 2.23 0 -3 3 5 77.81 0.68 0 -3 4 6 2.61 0.35 0 -3 6 10 11.01 0.72 0 -2 -6 5 32.83 0.72 0 -2 -1 2 83.94 0.55 0 -1 -8 7 461.33 2.44 0 0 -9 9 15.12 1.06 0 0 -8 6 20.54 0.74 0 1 -9 8 4.21 0.83 0 2 3 -1 968.77 1.94 0 2 7 1 1.23 0.30 0 2 9 3 27.30 0.54 0 3 -2 -1 66.25 0.44 0 6 4 -2 13.57 0.58 0 6 7 -1 640.42 2.74 0 7 1 -2 78.42 1.03 0 8 -1 -1 102.93 1.17 0 8 2 -2 6.48 0.71 0 8 3 -2 17.80 0.76 0 9 -2 0 127.68 1.37 0 9 0 -1 96.41 1.24 0 10 -1 0 82.38 1.35 0 10 1 -1 27.45 1.07 0 11 4 -1 78.63 1.66 0 11 5 -1 29.84 1.43 0 -5 -3 10 3.91 0.82 0 -5 -3 11 12.31 1.14 0 -5 -3 13 76.73 1.89 0 -5 -2 10 0.09 0.87 0 -5 -1 10 30.11 1.10 0 -5 0 10 3.55 0.73 0 -5 0 11 54.58 1.29 0 -5 1 13 6.68 1.14 0 -4 -6 10 120.11 1.71 0 -4 -6 11 32.86 1.43 0 -4 -6 13 1.49 1.54 0 -4 -5 8 68.14 1.14 0 -4 -2 6 25.50 0.67 0 -4 0 6 52.22 0.79 0 -4 4 11 0.48 0.84 0 -4 4 12 22.16 1.08 0 -3 -6 7 64.89 1.10 0 -3 1 4 9.25 0.34 0 -3 6 11 49.54 1.07 0 -2 -8 10 0.81 1.08 0 -1 -5 3 42.17 0.56 0 -1 -1 1 872.68 1.27 0 2 -9 8 -0.67 0.81 0 3 5 -1 187.65 1.09 0 4 1 -2 1796.97 3.17 0 4 2 -2 1295.49 2.81 0 4 6 -1 20.66 0.54 0 5 0 -2 150.67 1.04 0 5 4 -2 8.79 0.45 0 5 7 -1 100.73 1.13 0 6 0 -2 128.41 1.08 0 6 9 0 3.48 0.75 0 6 10 1 3.48 0.67 0 6 11 2 14.16 0.96 0 7 -2 -1 136.23 1.12 0 7 5 -2 135.27 1.38 0 8 -4 1 0.60 0.54 0 8 5 -2 151.29 1.57 0 8 8 -1 3.44 0.79 0 9 3 -2 77.27 1.34 0 11 0 0 14.75 1.12 0 11 3 -1 0.23 0.99 0 11 6 -1 6.30 1.15 0 11 9 0 0.02 1.28 0 -5 -2 11 29.86 1.11 0 -5 -2 12 13.99 1.13 0 -5 -2 13 39.86 1.47 0 -5 -1 12 4.62 1.13 0 -5 -1 13 18.09 1.40 0 -4 -5 9 49.07 1.11 0 -4 -1 6 361.56 1.78 0 -4 3 9 0.06 0.62 0 -3 -7 10 30.09 1.16 0 -3 -7 11 48.28 1.54 0 -3 -5 6 69.91 0.99 0 -3 -2 4 332.29 1.45 0 -3 5 8 8.32 0.51 0 -2 -8 11 26.47 1.44 0 -2 -7 7 13.24 0.70 0 -1 -8 8 50.03 1.17 0 1 -8 6 4.25 0.60 0 1 -7 4 6.34 0.38 0 1 6 1 40.31 0.42 0 3 10 3 -0.39 0.48 0 4 8 0 0.04 0.47 0 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0.73 0 -10 -8 -2 26.92 0.76 0 -9 -11 -3 4.29 1.06 0 -9 -9 -3 34.12 0.94 0 -8 -7 -3 0.65 0.49 0 -8 1 7 94.82 1.24 0 -7 2 9 79.61 1.43 0 -6 -11 -4 7.10 0.99 0 -6 -10 -4 6.29 0.90 0 -6 -8 -4 17.70 0.74 0 -6 -5 -3 0.31 0.32 0 -5 -11 -4 13.24 1.03 0 -5 -7 -4 6.09 0.50 0 -4 -11 -4 34.83 1.21 0 -4 -10 -4 6.80 0.93 0 -4 -7 -4 134.33 1.24 0 -3 -10 -4 3.94 0.78 0 -3 -9 -4 0.53 0.75 0 -3 -7 -4 1005.40 3.15 0 -2 -12 -3 235.15 2.44 0 -2 4 8 39.70 0.93 0 0 -9 -3 118.22 1.44 0 0 -8 -3 95.25 1.25 0 0 4 7 154.61 1.24 0 1 -10 -2 0.69 0.86 0 2 -10 -1 19.52 1.13 0 3 -10 0 4.00 0.96 0 3 -7 -1 253.41 1.71 0 3 -6 -1 393.43 1.90 0 3 -5 -1 360.38 1.65 0 4 -7 0 165.13 1.39 0 4 -6 0 146.32 1.22 0 4 -5 0 85.88 0.87 0 4 4 10 -0.14 0.50 0 -9 -10 -3 166.92 1.67 0 -9 0 6 19.92 0.77 0 -7 -6 -3 122.12 0.99 0 -7 -1 1 1.24 0.16 0 -6 -9 -4 7.02 0.69 0 -6 2 6 184.49 1.38 0 -6 3 11 10.33 1.23 0 -5 -10 -4 7.79 0.85 0 -5 -9 -4 148.11 1.55 0 -5 -8 -4 33.50 0.80 0 -5 3 8 7.40 0.68 0 -4 -9 -4 60.46 1.10 0 -4 -8 -4 105.47 1.21 0 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1.06 0 5 4 10 24.04 0.70 0 6 -4 3 23.86 0.48 0 7 -3 5 0.13 0.27 0 7 3 13 34.65 1.10 0 -10 -1 5 16.51 0.61 0 -7 -11 -3 27.32 1.09 0 -7 1 4 6.48 0.46 0 -6 -6 -3 35.66 0.64 0 -6 2 5 8.02 0.52 0 -6 3 8 6.21 0.82 0 -4 -5 -3 151.29 1.01 0 -4 2 3 1.25 0.29 0 -3 4 7 26.61 0.82 0 -2 -12 -2 180.39 2.17 0 -2 -9 -3 27.69 0.93 0 -2 -5 -3 0.07 0.30 0 -2 3 4 0.00 0.29 0 -2 5 11 11.57 0.95 0 -2 5 12 1.34 0.99 0 -1 -11 -2 5.60 0.97 0 0 5 9 176.31 1.56 0 1 -10 -1 9.63 0.91 0 1 -6 -2 85.86 0.93 0 1 -2 -1 2.84 0.16 0 1 5 9 89.80 1.14 0 2 -10 0 23.26 1.13 0 2 -8 -1 2.57 0.58 0 2 4 6 419.85 1.77 0 2 5 9 237.61 1.72 0 3 -10 1 1.27 0.91 0 3 -8 0 125.60 1.39 0 3 5 10 19.57 0.75 0 4 5 13 8.01 0.89 0 4 5 14 57.65 1.37 0 5 4 9 57.87 0.88 0 6 4 12 0.53 0.76 0 6 4 14 0.23 1.02 0 7 -4 5 25.64 0.50 0 7 3 12 42.38 0.99 0 -11 -7 0 -0.38 0.50 0 -11 -2 5 11.06 0.54 0 -10 -7 -1 25.42 0.66 0 -10 -2 3 17.12 0.36 0 -9 -11 -2 4.33 1.05 0 -9 -8 -2 8.23 0.66 0 -9 0 5 8.58 0.59 0 -9 1 8 18.42 1.01 0 -8 -6 -2 357.27 1.55 0 -7 -10 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1.48 0 4 -4 1 1.86 0.31 0 4 5 9 208.59 1.54 0 5 -7 3 72.40 1.04 0 5 3 6 5.17 0.34 0 6 1 5 0.76 0.17 0 6 2 6 0.41 0.26 0 -11 -9 0 1.19 0.80 0 -8 -9 -2 1.92 0.71 0 -8 -8 -2 82.06 1.07 0 -8 2 7 13.93 0.85 0 -7 -11 -2 2.10 0.88 0 -7 3 8 10.44 0.98 0 -6 -11 -2 14.93 1.11 0 -6 2 4 80.31 0.83 0 -6 3 6 7.23 0.65 0 -6 4 10 4.41 0.99 0 -5 -11 -2 0.28 0.87 0 -5 -2 -1 220.35 0.57 0 -5 2 3 0.49 0.33 0 -5 3 5 341.15 1.73 0 -4 -11 -2 12.85 0.97 0 -3 -10 -2 4.89 0.84 0 -3 5 8 8.69 0.81 0 -2 -9 -2 35.38 0.95 0 -2 6 12 7.11 1.29 0 -1 -12 0 4.50 1.16 0 -1 -8 -2 88.95 1.12 0 -1 -4 -2 62.52 0.61 0 -1 3 3 0.30 0.24 0 -1 6 11 25.20 1.10 0 0 -11 0 -0.05 0.97 0 0 6 10 8.87 0.80 0 1 -11 1 10.34 1.20 0 1 -3 -1 27.49 0.39 0 1 6 10 136.41 1.51 0 2 -8 0 184.42 1.56 0 2 4 5 8.30 0.37 0 2 5 7 0.03 0.41 0 2 6 10 35.38 0.94 0 3 -8 1 53.26 1.03 0 3 1 2 20.77 0.19 0 3 3 4 146.01 0.84 0 3 6 11 28.17 0.95 0 4 -9 3 54.37 1.25 0 4 6 14 66.07 1.49 0 5 5 10 16.34 0.68 0 6 -7 5 45.17 0.99 0 6 -5 4 2.56 0.46 0 6 4 9 1.17 0.51 0 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7.68 0.64 0 4 -8 3 53.93 1.10 0 4 6 10 29.73 0.86 0 5 6 12 21.38 0.94 0 6 4 8 41.14 0.70 0 7 4 10 24.58 0.77 0 -10 -10 0 11.93 0.98 0 -10 -7 0 0.27 0.54 0 -8 1 4 19.65 0.54 0 -7 -11 -1 32.95 1.24 0 -6 -8 -2 14.28 0.62 0 -6 -7 -2 60.71 0.87 0 -6 -6 -2 536.72 1.94 0 -6 1 2 133.59 0.75 0 -6 3 5 22.54 0.69 0 -5 -5 -2 516.27 1.73 0 -5 3 4 42.37 0.70 0 -5 5 9 4.49 1.02 0 -4 -11 -1 20.49 1.02 0 -4 -8 -2 0.63 0.59 0 -4 2 2 17.57 0.37 0 -3 -12 0 6.64 1.09 0 -3 6 10 10.94 1.02 0 -2 -5 -2 29.69 0.51 0 -2 4 4 57.08 0.75 0 -1 6 8 59.45 1.07 0 0 -11 1 9.32 1.02 0 0 -7 -1 18.50 0.66 0 1 -11 2 3.02 1.15 0 1 -8 0 1.21 0.67 0 1 4 4 131.30 0.93 0 1 7 11 0.80 0.99 0 1 7 12 0.50 0.99 0 2 -6 0 136.37 1.11 0 2 3 3 372.70 1.26 0 2 6 8 291.77 1.86 0 2 7 12 7.45 1.01 0 3 -6 1 12.43 0.54 0 3 7 12 46.04 1.36 0 4 -9 4 25.44 1.16 0 4 -6 2 93.19 1.00 0 4 5 7 24.42 0.67 0 5 -7 4 3.78 0.66 0 5 6 11 7.61 0.75 0 6 -6 5 8.06 0.62 0 8 3 11 51.62 0.87 0 -11 -7 1 53.28 0.86 0 -10 -9 0 41.76 1.04 0 -10 -8 0 1.22 0.66 0 -8 3 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0 -5 -6 0 6.30 0.46 0 -5 6 5 5.19 0.76 0 -4 -6 0 33.24 0.63 0 -4 4 2 122.14 0.96 0 -4 5 3 58.94 0.86 0 -3 -10 3 15.62 0.89 0 -3 3 1 372.55 1.31 0 -3 7 5 56.35 1.12 0 -2 8 6 28.65 1.09 0 -1 -8 2 69.98 1.01 0 -1 1 0 1635.48 1.51 0 0 -10 5 19.92 1.06 0 2 -9 6 4.98 0.96 0 2 -2 1 202.11 0.73 0 2 4 2 1375.95 2.60 0 3 -8 6 16.73 0.95 0 3 -3 2 17.21 0.35 0 3 8 6 75.74 1.12 0 3 10 10 1.44 1.12 0 5 9 9 1.78 0.86 0 6 7 7 49.23 0.92 0 7 8 10 13.96 0.92 0 9 4 10 13.88 0.61 0 -9 2 4 4.09 0.51 0 -8 -11 4 3.81 1.08 0 -8 -10 3 32.54 1.07 0 -8 -2 1 102.95 0.43 0 -7 -9 2 43.35 1.06 0 -7 4 4 3.75 0.58 0 -6 -5 0 71.45 0.71 0 -6 4 3 27.53 0.68 0 -4 -11 4 8.70 1.01 0 -4 -9 2 32.68 0.97 0 -4 6 4 7.87 0.67 0 -2 -11 5 1.33 1.03 0 -2 -5 0 131.82 0.92 0 -2 9 8 55.17 1.49 0 -1 -11 6 1.40 1.12 0 -1 -4 0 304.80 1.21 0 -1 5 2 25.88 0.57 0 -1 6 3 8.20 0.50 0 -1 7 4 89.61 1.16 0 0 -9 4 0.56 0.70 0 0 -8 3 45.93 0.98 0 0 -7 2 49.88 0.81 0 0 6 3 2.69 0.40 0 0 7 4 643.25 2.63 0 0 9 7 4.40 0.92 0 1 -4 1 336.13 1.31 0 1 6 3 124.52 1.07 0 1 7 4 460.39 2.20 0 1 9 7 0.15 0.81 0 1 10 9 0.40 1.13 0 2 -8 5 8.64 0.79 0 2 9 7 2.55 0.76 0 3 -7 5 58.86 1.03 0 3 5 3 0.01 0.29 0 4 -8 8 3.26 0.89 0 4 4 3 40.59 0.52 0 4 10 10 48.16 1.45 0 5 -6 7 1.34 0.67 0 5 -4 5 -0.05 0.41 0 5 6 5 4.87 0.42 0 5 7 6 24.26 0.68 0 5 8 7 53.86 1.07 0 6 6 6 1.48 0.41 0 6 8 8 2.34 0.78 0 7 -2 7 1.10 0.33 0 7 4 6 1.22 0.34 0 7 7 8 2.89 0.65 0 8 7 10 12.04 0.86 0 -10 -8 3 82.93 1.23 0 -9 -9 3 27.73 1.09 0 -9 -7 2 0.37 0.62 0 -9 3 5 0.95 0.65 0 -8 -6 1 3.42 0.43 0 -8 4 5 48.50 0.96 0 -7 -11 4 5.29 1.04 0 -7 -10 3 25.34 1.00 0 -7 2 2 84.03 0.68 0 -7 5 5 0.69 0.70 0 -6 -10 3 18.74 1.04 0 -6 5 4 105.57 1.20 0 -5 -11 4 31.07 1.18 0 -5 -10 3 0.60 0.89 0 -5 -9 2 2.89 0.65 0 -5 7 6 4.49 1.03 0 -4 8 7 2.96 0.99 0 -3 -5 0 17.57 0.45 0 -3 8 6 5.26 1.03 0 -2 -10 4 13.09 0.91 0 -2 5 2 24.95 0.58 0 -2 6 3 20.76 0.62 0 -2 7 4 0.51 0.63 0 -1 9 7 0.56 0.90 0 0 5 2 313.84 1.47 0 1 -10 7 5.53 1.20 0 1 -8 4 23.27 0.79 0 1 -7 3 18.52 0.63 0 1 3 1 16.93 0.32 0 1 8 5 7.30 0.66 0 2 -7 4 15.23 0.70 0 2 -6 3 101.05 0.99 0 2 7 4 93.56 1.05 0 3 9 7 1.61 0.75 0 3 10 9 6.74 1.07 0 4 6 4 2.81 0.45 0 4 7 5 48.23 0.82 0 5 -5 6 3.03 0.51 0 5 9 8 1.34 0.89 0 5 10 10 9.79 1.25 0 6 -5 8 -0.55 0.65 0 7 -4 9 48.83 0.85 0 7 6 7 180.98 1.35 0 9 5 10 56.31 0.92 0 -10 -9 4 7.84 0.99 0 -9 -10 4 17.87 1.06 0 -9 1 3 34.60 0.49 0 -8 -8 2 0.43 0.57 0 -8 -5 1 46.13 0.64 0 -8 1 2 453.89 1.20 0 -6 -7 1 630.84 2.41 0 -6 -2 0 155.19 0.53 0 -5 5 3 385.08 1.90 0 -4 -5 0 1065.66 2.50 0 -4 1 0 115.50 0.49 0 -4 3 1 106.88 0.76 0 -4 7 5 3.24 0.71 0 -3 6 3 0.53 0.53 0 -2 -9 3 43.31 0.98 0 -2 9 7 15.23 1.12 0 -1 -10 5 0.10 0.86 0 -1 8 5 0.85 0.67 0 0 -10 6 17.18 1.09 0 0 10 8 -1.24 1.24 0 1 5 2 94.76 0.83 0 1 10 8 32.65 1.28 0 2 -9 7 0.73 1.01 0 2 6 3 68.60 0.82 0 2 8 5 18.36 0.73 0 2 10 8 38.56 1.28 0 4 -7 7 6.46 0.79 0 4 9 7 -0.75 0.83 0 5 5 4 79.02 0.78 0 6 -3 6 31.46 0.53 0 -11 -7 4 2.32 0.82 0 -10 -7 3 39.59 0.91 0 -8 -9 3 4.42 0.86 0 -6 -3 0 192.49 0.78 0 -6 6 5 58.23 1.15 0 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1.12 0 3 4 2 15.96 0.36 0 3 9 6 -0.22 0.67 0 4 5 3 152.01 1.02 0 4 10 8 14.49 1.05 0 5 -6 8 10.76 0.81 0 5 7 5 25.51 0.72 0 5 9 7 -0.14 0.84 0 6 7 6 4.93 0.52 0 7 7 7 75.76 1.05 0 8 4 7 37.59 0.56 0 9 3 9 54.98 0.58 0 9 4 9 168.97 1.06 0 -11 -6 4 97.70 1.18 0 -10 -8 4 5.69 0.86 0 -10 -6 3 5.92 0.64 0 -10 1 4 24.30 0.48 0 -9 -9 4 0.55 0.95 0 -8 -7 2 17.40 0.66 0 -7 -9 3 0.18 0.66 0 -6 -10 4 5.38 0.87 0 -6 -9 3 17.79 0.91 0 -6 -8 2 25.30 0.74 0 -6 2 1 0.83 0.27 0 -5 -9 3 -0.10 0.75 0 -5 -8 2 236.43 1.68 0 -5 -4 0 8.51 0.28 0 -5 7 5 -0.67 0.76 0 -4 -11 6 65.95 1.65 0 -4 -9 3 3.79 0.67 0 -4 -4 0 322.46 1.23 0 -4 5 2 317.23 1.63 0 -4 6 3 36.44 0.84 0 -3 -4 0 63.79 0.58 0 -3 4 1 107.09 0.85 0 -3 8 5 2.71 0.78 0 -2 -11 7 3.83 1.18 0 -2 2 0 124.06 0.61 0 -2 9 6 0.52 0.91 0 -1 -10 6 7.52 0.98 0 -1 -5 1 1.18 0.34 0 -1 7 3 107.52 1.16 0 -1 8 4 142.66 1.53 0 0 -8 4 70.19 1.08 0 0 -7 3 15.01 0.59 0 0 7 3 86.72 1.04 0 0 8 4 28.66 0.83 0 0 10 7 12.83 1.13 0 1 -8 5 122.48 1.38 0 1 -3 1 78.56 0.56 0 1 7 3 -0.13 0.44 0 1 8 4 60.36 1.01 0 2 -9 8 0.23 0.96 0 3 -8 8 66.59 1.38 0 3 10 7 4.71 0.92 0 4 -2 3 80.58 0.53 0 4 9 6 -0.23 0.81 0 6 -5 9 12.24 0.78 0 6 2 4 1.26 0.16 0 6 6 5 3.83 0.47 0 7 9 9 4.26 0.86 0 8 -2 10 36.77 0.65 0 -9 -5 2 0.26 0.42 0 -8 4 4 14.86 0.72 0 -7 5 4 5.54 0.73 0 -6 -6 1 143.24 1.11 0 -5 -11 6 86.01 1.77 0 -4 7 4 70.94 1.12 0 -3 -11 7 0.62 1.29 0 -3 -10 5 26.86 1.04 0 -3 -6 1 262.99 1.43 0 -3 2 0 1.52 0.18 0 -2 -8 3 31.96 0.80 0 -2 7 3 66.32 1.04 0 -1 2 0 106.22 0.55 0 -1 6 2 85.84 0.93 0 -1 10 7 69.24 1.58 0 0 -4 1 632.94 1.76 0 0 6 2 0.11 0.37 0 0 9 5 5.80 0.79 0 1 -9 7 0.20 1.00 0 1 -6 3 699.80 2.43 0 1 4 1 1023.46 2.24 0 1 6 2 140.00 1.12 0 1 9 5 2.85 0.71 0 2 -7 5 34.87 0.81 0 2 7 3 128.96 1.21 0 2 9 5 20.75 0.84 0 3 -5 4 27.79 0.56 0 4 7 4 131.99 1.19 0 5 6 4 34.98 0.62 0 5 10 8 88.57 1.52 0 6 3 4 4.77 0.24 0 6 10 9 -0.88 0.96 0 7 6 6 49.36 0.77 0 8 5 7 131.93 1.02 0 8 7 8 68.83 1.03 0 8 8 9 35.08 1.09 0 9 5 9 1.27 0.52 0 9 7 10 61.05 1.16 0 -11 -5 4 9.41 0.65 0 -11 -3 4 17.17 0.50 0 -10 -5 3 1.36 0.54 0 -9 -7 3 13.91 0.70 0 -8 -9 4 9.13 0.99 0 -8 3 3 7.69 0.52 0 -7 -7 2 2.70 0.57 0 -7 -5 1 784.26 2.20 0 -6 -11 6 -1.07 1.10 0 -6 5 3 0.38 0.57 0 -6 6 4 15.56 0.82 0 -5 -6 1 267.75 1.45 0 -5 -3 0 15.99 0.30 0 -4 -10 5 124.29 1.71 0 -4 -6 1 21.58 0.53 0 -4 8 5 9.05 1.00 0 -3 -9 4 23.92 0.94 0 -3 9 6 11.96 1.10 0 -2 -10 6 1.22 0.92 0 -2 -3 0 560.46 1.37 0 -2 6 2 23.87 0.61 0 -2 8 4 28.31 0.89 0 -1 -10 7 8.71 1.20 0 -1 -9 5 -0.06 0.69 0 -1 9 5 12.96 0.91 0 0 -10 8 2.13 1.10 0 0 10 6 6.13 1.14 0 1 10 6 8.00 0.96 0 2 -8 7 0.56 0.91 0 2 3 1 1.04 0.18 0 3 8 4 248.13 1.74 0 3 9 5 35.96 1.03 0 3 11 8 7.51 1.19 0 5 -6 9 9.51 0.85 0 5 -4 6 107.00 0.97 0 6 4 4 21.49 0.42 0 6 8 6 41.65 0.96 0 8 -1 9 22.80 0.44 0 -11 -4 4 8.27 0.54 0 -10 -7 4 4.43 0.80 0 -9 -4 2 28.72 0.51 0 -8 -6 2 12.37 0.55 0 -7 -10 5 3.17 0.93 0 -7 -9 4 0.79 0.81 0 -7 3 2 69.43 0.72 0 -7 6 5 3.57 0.85 0 -6 -10 5 5.84 0.93 0 -6 4 2 177.85 1.17 0 -5 -10 5 30.18 1.10 0 -5 6 3 2.46 0.63 0 -4 -11 7 69.95 1.66 0 -3 -8 3 17.78 0.69 0 -3 6 2 22.14 0.69 0 -3 7 3 6.82 0.61 0 -3 8 4 44.47 1.10 0 -2 -5 1 406.36 1.60 0 -2 9 5 7.73 0.90 0 -1 -8 4 126.92 1.34 0 -1 -2 0 961.73 1.45 0 -1 5 1 8.90 0.39 0 -1 10 6 0.03 1.15 0 0 1 0 1537.61 1.38 0 1 -8 6 4.45 0.80 0 2 6 2 7.41 0.46 0 3 -8 9 1.56 0.94 0 3 -7 7 34.42 0.99 0 3 10 6 34.17 1.10 0 4 -7 9 0.77 0.97 0 4 -6 7 1.76 0.56 0 4 11 8 162.85 2.08 0 5 8 5 1.73 0.54 0 5 9 6 -0.17 0.66 0 6 -4 8 8.84 0.58 0 7 -3 9 10.56 0.59 0 7 8 7 48.56 0.94 0 7 9 8 28.35 0.98 0 8 6 7 4.09 0.54 0 9 6 9 117.29 1.16 0 -10 -8 5 183.31 1.82 0 -10 -4 3 19.61 0.54 0 -10 -2 3 15.80 0.34 0 -9 -8 4 3.36 0.71 0 -9 -3 2 78.45 0.61 0 -6 -7 2 144.72 1.24 0 -6 7 5 81.23 1.35 0 -5 -11 7 40.99 1.48 0 -5 -9 4 6.69 0.73 0 -5 -7 2 408.27 1.99 0 -5 5 2 2.56 0.49 0 -5 7 4 64.82 1.20 0 -4 -8 3 230.76 1.69 0 -4 -7 2 241.55 1.55 0 -4 -3 0 36.86 0.39 0 -3 -10 6 1.43 0.90 0 -3 -3 0 979.50 1.79 0 -2 -9 5 0.58 0.68 0 -2 5 1 25.34 0.53 0 -1 -10 8 83.24 1.76 0 0 -5 2 266.35 1.35 0 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0 -9 -9 6 1.16 1.06 0 -9 -7 4 35.05 0.91 0 -7 -9 5 82.08 1.34 0 -7 5 3 131.44 1.26 0 -7 6 4 7.17 0.87 0 -6 3 1 122.92 0.84 0 -6 6 3 42.94 0.96 0 -5 4 1 321.98 1.44 0 -4 -10 7 10.41 1.17 0 -3 -8 4 271.74 1.86 0 -2 -9 6 52.96 1.17 0 -1 -8 5 0.46 0.61 0 -1 6 1 92.01 0.97 0 0 -3 1 91.76 0.60 0 0 3 0 58.13 0.50 0 0 6 1 62.22 0.81 0 0 11 6 4.34 1.19 0 1 -8 7 0.65 0.72 0 2 7 2 215.06 1.46 0 2 11 6 187.16 2.12 0 3 -5 5 12.56 0.49 0 3 8 3 25.66 0.72 0 3 11 6 11.07 1.07 0 5 8 4 35.71 0.85 0 5 11 7 30.55 1.25 0 6 -4 9 38.99 0.85 0 6 6 4 43.72 0.65 0 6 8 5 15.95 0.65 0 6 11 8 3.42 1.08 0 7 6 5 48.66 0.72 0 7 8 6 47.12 0.91 0 8 9 8 9.96 0.99 0 9 4 8 9.32 0.41 0 9 5 8 12.88 0.53 0 9 6 8 4.88 0.60 0 9 8 9 2.38 0.84 0 -10 -7 5 0.46 0.85 0 -9 -8 5 13.32 0.85 0 -8 5 4 3.27 0.77 0 -7 -8 4 190.65 1.64 0 -6 -9 5 9.83 0.84 0 -6 -6 2 113.62 1.01 0 -6 7 4 5.10 0.87 0 -5 -10 7 1.68 1.14 0 -5 -9 5 0.27 0.70 0 -5 7 3 45.05 1.03 0 -4 -8 4 217.13 1.72 0 -4 5 1 136.25 1.09 0 -3 -6 2 205.68 1.30 0 -3 7 2 0.43 0.61 0 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0 5 -5 9 49.51 1.02 0 6 7 4 72.34 0.93 0 6 10 6 46.53 1.14 0 6 11 7 70.31 1.59 0 7 10 7 61.22 1.35 0 8 4 6 34.05 0.48 0 8 6 6 221.55 1.36 0 9 7 8 1.10 0.63 0 -10 -5 4 16.50 0.70 0 -8 -8 5 32.45 1.03 0 -8 -7 4 19.09 0.79 0 -8 -6 3 84.15 0.96 0 -8 -4 2 33.44 0.55 0 -7 -9 6 -0.09 0.85 0 -7 2 1 150.82 0.76 0 -6 -10 8 8.51 1.33 0 -5 -1 0 126.45 0.34 0 -5 2 0 111.70 0.62 0 -4 -10 8 3.52 1.09 0 -4 -9 6 73.39 1.30 0 -4 -2 0 104.80 0.48 0 -4 7 2 1.38 0.65 0 -4 8 3 10.19 0.95 0 -3 -2 0 168.55 0.60 0 -3 4 0 1.80 0.33 0 -3 6 1 408.73 1.92 0 -2 -9 7 111.56 1.56 0 -2 9 3 3.26 0.94 0 -1 -9 8 15.23 1.05 0 -1 -8 6 0.22 0.65 0 -1 8 2 242.05 1.78 0 -1 10 4 2.39 0.92 0 0 -8 7 49.49 1.11 0 0 4 0 417.18 1.45 0 0 11 5 1.79 1.12 0 2 6 1 14.14 0.50 0 3 3 1 577.05 1.38 0 3 4 1 5325.96 4.91 0 3 10 4 4.00 0.79 0 3 11 5 85.77 1.52 0 4 6 2 277.45 1.45 0 5 -3 6 9.29 0.40 0 5 -2 5 83.88 0.63 0 5 7 3 -0.25 0.41 0 5 9 4 144.34 1.51 0 5 10 5 2.10 0.77 0 6 9 5 23.01 0.82 0 8 9 7 12.61 0.90 0 8 10 8 13.18 1.11 0 -11 -4 5 0.49 0.63 0 -9 -8 6 28.34 1.12 0 -9 -6 4 2.47 0.59 0 -8 -9 7 4.38 1.14 0 -7 -8 5 42.40 1.06 0 -6 -9 6 26.49 1.02 0 -5 -9 6 111.00 1.52 0 -5 -4 1 98.91 0.74 0 -5 5 1 0.89 0.48 0 -4 -10 9 49.85 1.57 0 -4 9 4 3.63 0.96 0 -3 -9 7 10.53 1.00 0 -3 -8 5 30.68 0.84 0 -3 -4 1 44.09 0.51 0 -2 -5 2 10.66 0.41 0 -2 8 2 1.47 0.60 0 -2 10 4 41.50 1.28 0 -1 7 1 295.97 1.78 0 0 -9 10 173.40 2.16 0 0 7 1 18.02 0.60 0 1 -8 9 48.42 1.34 0 1 -6 5 274.04 1.68 0 1 3 0 386.74 1.18 0 2 -6 6 63.61 0.93 0 3 -7 10 138.77 1.78 0 3 2 1 105.96 0.48 0 4 11 5 -0.40 1.04 0 6 -4 10 5.45 0.72 0 6 -3 8 30.38 0.63 0 7 -3 11 94.86 1.17 0 7 8 5 8.51 0.68 0 8 7 6 2.72 0.55 0 9 8 8 13.21 0.80 0 -10 -7 6 245.44 2.02 0 -10 -6 5 0.00 0.71 0 -9 -7 5 13.16 0.77 0 -8 3 2 0.21 0.41 0 -7 -7 4 106.39 1.23 0 -7 -6 3 31.51 0.72 0 -6 -8 5 76.24 1.26 0 -6 4 1 0.19 0.41 0 -4 -8 5 206.45 1.71 0 -4 -4 1 90.57 0.69 0 -4 6 1 11.52 0.60 0 -3 8 2 3.15 0.75 0 -3 9 3 4.15 0.94 0 -2 -9 8 116.94 1.67 0 -2 -8 6 453.49 2.55 0 -2 5 0 273.64 1.41 0 -2 7 1 8.68 0.63 0 -1 -9 9 24.56 1.20 0 -1 -7 5 79.12 1.10 0 -1 5 0 545.50 1.90 0 0 5 0 47.93 0.65 0 0 10 3 3.95 0.99 0 1 -7 7 0.23 0.69 0 1 -3 2 56.74 0.52 0 1 2 0 944.92 1.48 0 1 4 0 299.18 1.23 0 1 7 1 104.28 1.07 0 1 10 3 12.50 0.98 0 2 -2 2 3008.60 2.90 0 3 -6 8 0.78 0.70 0 3 -5 6 21.60 0.58 0 3 5 1 787.20 2.16 0 3 8 2 18.73 0.65 0 4 -4 6 1.32 0.40 0 4 7 2 0.48 0.48 0 5 -5 10 62.85 1.19 0 5 8 3 23.25 0.75 0 6 10 5 -0.62 0.86 0 6 11 6 1.57 1.10 0 7 -2 9 202.63 1.21 0 7 10 6 15.94 1.05 0 8 3 6 0.82 0.22 0 8 8 6 11.75 0.71 0 -10 -4 4 7.57 0.54 0 -9 -4 3 7.12 0.46 0 -8 -8 6 5.37 0.92 0 -7 -2 1 7.54 0.23 0 -7 6 3 10.99 0.76 0 -6 -9 7 24.40 1.09 0 -6 -5 2 3.95 0.39 0 -6 6 2 5.82 0.69 0 -6 7 3 2.71 0.81 0 -5 -9 7 1.48 0.87 0 -5 8 3 0.29 0.94 0 -4 4 0 112.30 0.85 0 -1 -9 10 6.79 1.32 0 -1 -8 7 450.40 2.60 0 -1 9 2 24.40 0.99 0 -1 10 3 0.93 0.98 0 0 -8 8 82.30 1.34 0 0 -7 6 0.41 0.56 0 0 9 2 122.32 1.43 0 0 11 4 15.96 1.19 0 1 -5 4 2.51 0.37 0 1 9 2 285.13 2.01 0 1 11 4 15.64 1.10 0 2 -7 9 32.54 1.10 0 2 -5 5 24.79 0.62 0 2 7 1 1.72 0.42 0 2 11 4 4.73 0.95 0 3 6 1 405.41 1.76 0 3 11 4 6.58 1.07 0 4 -5 8 0.40 0.64 0 4 -3 5 3.34 0.35 0 5 -4 8 9.12 0.60 0 5 10 4 7.75 0.92 0 5 11 5 10.19 1.00 0 6 5 3 -0.33 0.31 0 8 10 7 12.56 1.05 0 9 6 7 0.74 0.50 0 -11 -3 5 39.15 0.72 0 -9 -8 7 82.52 1.48 0 -8 -7 5 2.55 0.72 0 -8 -5 3 8.21 0.49 0 -8 5 3 0.73 0.66 0 -7 5 2 70.07 0.95 0 -6 -7 4 68.90 0.99 0 -6 -6 3 186.97 1.32 0 -5 -7 4 6.37 0.56 0 -5 -5 2 126.75 0.98 0 -5 3 0 85.71 0.66 0 -5 7 2 17.19 0.79 0 -4 -7 4 88.64 1.06 0 -4 -5 2 51.84 0.68 0 -3 -8 6 663.67 3.02 0 -3 5 0 146.13 1.05 0 -3 7 1 253.65 1.69 0 -1 11 4 1.57 1.10 0 0 8 1 81.24 1.15 0 1 -4 3 53.73 0.60 0 1 5 0 569.17 1.89 0 2 -6 7 1.39 0.61 0 3 -4 5 18.98 0.49 0 3 10 3 0.59 0.73 0 4 -6 11 5.10 1.03 0 5 -5 11 3.32 0.94 0 5 5 2 539.33 1.76 0 6 -4 11 78.73 1.24 0 6 -2 7 2.76 0.36 0 6 4 3 17.11 0.35 0 6 6 3 36.98 0.64 0 7 5 4 91.06 0.76 0 7 6 4 7.28 0.45 0 7 9 5 18.63 0.79 0 8 9 6 6.31 0.80 0 9 5 7 -0.31 0.41 0 9 7 7 11.78 0.66 0 -9 -7 6 52.26 1.22 0 -8 -6 4 11.48 0.65 0 -8 -3 2 17.00 0.40 0 -7 -9 8 76.69 1.55 0 -7 -8 6 48.26 1.08 0 -7 -4 2 338.86 1.40 0 -7 3 1 17.29 0.43 0 -6 -9 8 2.59 1.14 0 -6 -8 6 105.24 1.43 0 -4 -8 6 2.36 0.68 0 -4 -6 3 1.28 0.39 0 -4 8 2 2.04 0.79 0 -4 9 3 27.58 1.09 0 -3 -9 9 20.41 1.27 0 -2 -8 7 11.14 0.79 0 -2 -7 5 247.92 1.70 0 -2 6 0 148.25 1.20 0 -2 9 2 1.98 0.71 0 -2 10 3 1.54 0.93 0 -1 -8 8 52.16 1.26 0 -1 -4 2 79.06 0.69 0 -1 6 0 1.31 0.38 0 -1 8 1 67.45 1.03 0 1 -7 8 1.49 0.78 0 2 -7 10 7.90 1.04 0 2 -3 3 189.17 0.94 0 3 -6 9 15.16 0.92 0 3 -2 3 457.54 1.22 0 3 7 1 2.69 0.50 0 3 9 2 142.23 1.45 0 4 8 2 0.43 0.48 0 4 10 3 33.85 1.06 0 4 11 4 31.77 1.15 0 4 12 5 37.28 1.41 0 5 4 2 7.97 0.31 0 5 6 2 380.16 1.67 0 6 -3 9 66.94 0.93 0 6 7 3 166.90 1.28 0 7 4 4 43.90 0.49 0 7 7 4 156.36 1.25 0 7 11 6 2.66 1.10 0 8 0 9 1.16 0.34 0 9 8 7 11.70 0.78 0 -11 -2 5 12.58 0.58 0 -10 -6 6 16.80 0.91 0 -9 -6 5 7.81 0.73 0 -9 -5 4 2.42 0.54 0 -6 5 1 3.05 0.51 0 -5 -8 6 76.62 1.22 0 -5 6 1 70.91 0.96 0 -4 -9 9 17.66 1.27 0 -4 5 0 86.17 0.88 0 -4 7 1 1.40 0.67 0 -3 9 2 5.51 0.92 0 -3 10 3 4.59 1.15 0 -2 8 1 2.77 0.59 0 -1 -7 6 9.78 0.64 0 0 -8 10 48.45 1.42 0 0 -7 7 142.77 1.46 0 0 -2 1 452.98 1.05 0 0 10 2 116.91 1.62 0 0 11 3 1.76 1.14 0 1 6 0 75.71 0.83 0 1 10 2 180.76 1.88 0 1 11 3 105.94 1.64 0 2 8 1 195.31 1.52 0 2 11 3 112.61 1.65 0 2 12 4 3.25 1.31 0 3 -5 7 109.70 1.14 0 4 -5 9 1.38 0.71 0 5 -4 9 27.37 0.76 0 5 -3 7 30.72 0.63 0 5 7 2 316.27 1.72 0 5 11 4 15.13 1.12 0 5 12 5 19.76 1.39 0 6 0 5 3.45 0.16 0 6 10 4 6.28 0.93 0 7 10 5 5.27 0.78 0 8 6 5 13.65 0.51 0 8 10 6 0.61 0.89 0 9 9 7 3.22 0.86 0 -10 -3 4 2.10 0.48 0 -9 -3 3 1.57 0.39 0 -7 -8 7 15.76 1.03 0 -7 -6 4 248.97 1.62 0 -7 -5 3 62.04 0.80 0 -6 -9 9 11.00 1.18 0 -6 -7 5 13.04 0.74 0 -6 1 0 537.11 0.91 0 -5 -9 9 179.54 2.11 0 -5 4 0 430.47 1.59 0 -3 -8 7 82.36 1.27 0 -3 -7 5 10.62 0.61 0 -3 6 0 273.68 1.56 0 -3 8 1 56.70 1.07 0 -2 -3 1 938.38 1.83 0 -1 7 0 1.83 0.54 0 -1 10 2 1.11 0.96 0 -1 11 3 25.60 1.37 0 0 7 0 124.44 1.19 0 1 -7 9 5.03 0.91 0 2 -7 11 14.09 1.19 0 2 4 0 54.64 0.55 0 2 5 0 129.79 0.92 0 3 -6 10 95.22 1.47 0 3 11 3 54.62 1.31 0 4 -4 7 30.81 0.66 0 4 5 1 37.07 0.53 0 4 9 2 46.76 0.95 0 5 3 2 47.97 0.42 0 6 3 3 71.62 0.47 0 6 8 3 38.94 0.79 0 8 5 5 6.52 0.40 0 -9 -7 7 68.90 1.40 0 -8 -8 8 5.45 1.00 0 -8 -7 6 97.38 1.31 0 -8 4 2 14.35 0.54 0 -6 -8 7 49.29 1.16 0 -6 2 0 590.33 1.31 0 -6 7 2 8.07 0.81 0 -5 -9 10 73.46 1.79 0 -5 -8 7 176.73 1.81 0 -5 -7 5 54.36 0.94 0 -5 -3 1 3.08 0.23 0 -5 8 2 3.04 0.90 0 -4 -9 10 7.64 1.17 0 -4 -8 7 8.28 0.79 0 -4 -7 5 -0.08 0.51 0 -2 -7 6 10.12 0.71 0 -2 7 0 483.88 2.25 0 -2 10 2 0.03 1.00 0 -1 9 1 13.36 0.88 0 0 9 1 -0.45 0.65 0 1 -5 5 31.10 0.67 0 1 7 0 0.70 0.43 0 2 -5 6 17.90 0.56 0 2 6 0 18.89 0.49 0 2 9 1 238.89 1.86 0 3 8 1 52.05 0.88 0 3 10 2 5.24 0.75 0 4 4 1 295.98 1.15 0 4 6 1 225.56 1.31 0 4 11 3 1.55 1.01 0 5 8 2 0.15 0.48 0 7 9 4 1.06 0.68 0 7 11 5 2.77 1.05 0 9 4 7 0.70 0.30 0 -9 4 3 16.12 0.61 0 -8 -6 5 35.51 0.91 0 -8 -4 3 69.71 0.76 0 -7 4 1 1.29 0.41 0 -7 6 2 5.04 0.68 0 -6 -4 2 13.18 0.40 0 -4 -3 1 105.82 0.65 0 -4 6 0 147.12 1.22 0 -4 9 2 14.30 1.06 0 -3 -8 8 1.71 0.78 0 -3 -3 1 257.16 0.97 0 -2 -8 9 3.00 0.98 0 -2 -4 2 2.47 0.26 0 -2 9 1 197.83 1.84 0 -1 -7 7 365.58 2.21 0 0 -7 8 10.80 0.76 0 0 -6 6 370.85 2.00 0 0 -4 3 221.76 1.13 0 1 -7 10 7.13 1.06 0 1 -6 7 22.40 0.72 0 1 -1 1 342.64 0.69 0 1 1 0 373.88 0.65 0 3 -6 11 50.72 1.29 0 3 -5 8 77.11 1.06 0 3 -4 6 0.17 0.41 0 4 -5 10 107.93 1.33 0 4 10 2 0.20 0.80 0 6 -3 10 12.06 0.70 0 6 11 4 6.43 0.95 0 8 9 5 27.17 0.85 0 8 11 6 6.02 0.99 0 9 7 6 10.64 0.64 0 9 8 6 5.28 0.71 0 10 8 8 4.02 0.74 0 -10 -5 6 7.33 0.79 0 -10 -4 5 2.67 0.59 0 -9 -6 6 105.39 1.34 0 -9 -4 4 1.05 0.51 0 -8 -5 4 15.52 0.62 0 -8 -2 2 6.83 0.30 0 -7 -1 1 0.56 0.15 0 -6 -5 3 3.48 0.37 0 -6 3 0 20.28 0.40 0 -6 6 1 79.89 1.02 0 -5 -8 8 18.90 1.07 0 -5 -6 4 78.70 0.94 0 -5 5 0 283.65 1.47 0 -5 7 1 0.78 0.55 0 -4 -8 8 2.55 0.80 0 -4 -6 4 270.26 1.60 0 -4 8 1 1.33 0.76 0 -3 -7 6 20.58 0.72 0 -3 -5 3 58.96 0.70 0 -3 3 -1 81.16 0.61 0 -3 7 0 23.05 0.74 0 -3 10 2 5.34 1.10 0 -1 -8 11 12.33 1.19 0 -1 3 -1 81.58 0.59 0 -1 4 -1 335.73 1.33 0 -1 8 0 0.62 0.67 0 0 8 0 35.87 0.82 0 0 11 2 52.66 1.37 0 1 8 0 47.77 0.93 0 1 11 2 4.41 0.98 0 1 12 3 14.49 1.27 0 2 -6 9 102.04 1.31 0 2 7 0 108.96 1.07 0 2 11 2 12.82 0.99 0 2 12 3 230.13 2.40 0 3 -6 12 9.60 1.21 0 3 9 1 27.17 0.81 0 3 12 3 0.10 1.03 0 4 -5 11 4.80 0.89 0 4 3 1 49.74 0.43 0 4 8 1 6.06 0.61 0 5 -2 6 -0.09 0.27 0 5 9 2 32.15 0.85 0 5 11 3 44.96 1.22 0 6 -2 8 225.10 1.25 0 6 10 3 3.94 0.84 0 7 -2 11 209.70 1.51 0 7 0 7 1.09 0.25 0 7 10 4 -0.49 0.72 0 8 10 5 2.32 0.93 0 9 6 6 85.08 0.86 0 9 9 6 5.76 0.84 0 -10 -2 4 16.10 0.49 0 -9 -5 5 3.63 0.61 0 -8 -7 7 -0.77 0.76 0 -7 -3 2 115.80 0.77 0 -5 -7 6 128.94 1.38 0 -5 -5 3 48.67 0.67 0 -5 -4 2 8.65 0.33 0 -4 -7 6 0.86 0.56 0 -4 -4 2 40.70 0.55 0 -4 -1 0 0.38 0.09 0 -3 -8 9 37.00 1.14 0 -3 -4 2 35.35 0.49 0 -3 2 -1 38.18 0.37 0 -3 4 -1 34.09 0.53 0 -3 9 1 14.27 0.96 0 -2 -8 10 0.77 0.97 0 -2 -7 7 12.87 0.71 0 -2 2 -1 200.77 0.75 0 -2 5 -1 72.31 0.78 0 -2 8 0 174.93 1.58 0 -1 -7 8 206.33 1.84 0 -1 5 -1 328.13 1.49 0 -1 10 1 12.30 1.02 0 -1 11 2 3.73 1.03 0 0 -7 9 2.39 0.75 0 0 4 -1 620.16 1.78 0 0 10 1 122.24 1.56 0 1 10 1 22.97 0.94 0 2 -4 5 569.83 1.97 0 2 10 1 57.57 1.16 0 3 5 0 17.47 0.42 0 3 6 0 23.18 0.53 0 3 11 2 25.98 1.08 0 4 -4 8 37.47 0.78 0 4 12 3 9.21 1.11 0 5 -3 8 7.95 0.53 0 6 6 2 555.50 1.98 0 6 7 2 64.02 0.87 0 6 12 4 7.07 1.23 0 7 3 4 36.18 0.34 0 7 6 3 127.55 1.01 0 7 7 3 120.78 1.10 0 8 1 8 1.13 0.25 0 8 4 5 128.48 0.71 0 -9 -2 3 54.19 0.58 0 -8 5 2 2.83 0.61 0 -7 -7 7 117.85 1.52 0 -7 -6 5 5.91 0.56 0 -7 5 1 1.74 0.53 0 -6 -8 9 15.75 1.06 0 -6 -2 1 180.89 0.72 0 -6 4 0 -0.32 0.38 0 -5 -8 9 133.03 1.75 0 -4 7 0 156.38 1.39 0 -3 -8 10 0.95 1.08 0 -3 5 -1 39.71 0.63 0 -2 -8 11 27.12 1.27 0 0 -7 10 35.20 1.22 0 0 3 -1 93.30 0.62 0 0 5 -1 399.96 1.62 0 1 -7 12 1.20 1.07 0 1 -6 8 4.18 0.62 0 2 -6 10 170.70 1.72 0 2 -5 7 248.41 1.60 0 2 8 0 225.04 1.62 0 3 4 0 68.68 0.60 0 3 7 0 93.97 0.99 0 3 10 1 28.31 1.01 0 4 -5 12 9.24 1.05 0 4 9 1 144.90 1.44 0 4 11 2 12.41 0.95 0 5 10 2 3.05 0.73 0 6 8 2 14.12 0.67 0 7 8 3 70.02 0.96 0 7 11 4 0.13 0.86 0 8 7 4 76.88 0.93 0 8 8 4 1.67 0.59 0 8 11 5 33.80 1.24 0 9 10 6 1.59 0.81 0 -9 -6 7 11.85 0.85 0 -8 -7 8 9.95 0.95 0 -8 -6 6 6.83 0.67 0 -7 -5 4 16.85 0.61 0 -7 -4 3 26.22 0.55 0 -6 -8 10 44.10 1.52 0 -6 -7 7 46.22 1.12 0 -6 -6 5 77.32 1.04 0 -5 -8 10 18.56 1.29 0 -5 6 0 38.20 0.79 0 -5 8 1 0.62 0.85 0 -4 -8 10 18.19 1.11 0 -4 -7 7 3.43 0.75 0 -4 3 -1 78.72 0.61 0 -3 -8 11 0.46 1.21 0 -3 -7 7 31.30 0.86 0 -3 8 0 136.30 1.43 0 -2 -7 8 168.04 1.68 0 -2 6 -1 2.93 0.40 0 -2 10 1 22.16 1.03 0 -1 -4 3 3.50 0.33 0 -1 9 0 136.94 1.49 0 0 6 -1 0.66 0.36 0 0 9 0 38.39 0.96 0 1 -5 6 10.72 0.51 0 1 -3 3 427.89 1.38 0 1 5 -1 1.20 0.34 0 1 9 0 65.22 1.10 0 1 12 2 3.90 1.17 0 2 -6 11 4.99 1.04 0 2 12 2 185.92 2.17 0 3 -3 5 77.84 0.72 0 3 8 0 72.95 1.05 0 5 -4 12 1.77 0.94 0 5 6 1 314.39 1.51 0 5 7 1 274.64 1.57 0 6 -3 12 1.13 0.84 0 6 5 2 1.21 0.30 0 6 9 2 -0.72 0.67 0 7 5 3 -0.38 0.33 0 7 9 3 7.80 0.64 0 8 6 4 115.36 0.96 0 8 9 4 52.39 1.07 0 9 5 6 8.12 0.40 0 10 8 7 0.98 0.72 0 -10 -4 6 6.35 0.74 0 -10 -3 5 53.63 0.85 0 -8 -7 9 6.06 1.13 0 -8 -5 5 11.06 0.65 0 -8 2 1 15.07 0.28 0 -7 -7 8 0.71 0.92 0 -6 7 1 0.95 0.72 0 -5 -7 7 77.43 1.19 0 -5 -6 5 266.73 1.68 0 -4 -8 11 0.18 1.09 0 -4 -6 5 12.13 0.56 0 -4 2 -1 24.34 0.31 0 -4 9 1 0.87 0.80 0 -3 -1 0 185.76 0.44 0 -3 6 -1 13.04 0.58 0 -2 9 0 24.63 0.97 0 -1 -2 1 154.03 0.62 0 -1 7 -1 12.43 0.57 0 0 -7 11 16.24 1.06 0 0 -7 12 4.97 1.24 0 0 11 1 25.73 1.16 0 1 -6 9 1.64 0.66 0 1 -2 2 144.47 0.65 0 1 4 -1 463.18 1.52 0 1 6 -1 771.62 2.45 0 1 11 1 14.84 1.03 0 2 -6 12 8.87 1.15 0 2 -3 4 131.19 0.84 0 2 9 0 234.63 1.80 0 3 -4 7 65.04 0.86 0 3 12 2 57.85 1.47 0 4 -4 9 26.54 0.78 0 4 10 1 4.25 0.73 0 5 5 1 5.73 0.32 0 5 11 2 0.66 0.87 0 7 12 4 8.55 1.24 0 8 10 4 8.16 0.93 0 10 7 7 27.85 0.73 0 -10 -1 4 1.40 0.39 0 -9 -6 8 63.06 1.35 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1.76 0 -4 3 -6 19.50 0.46 0 -4 5 -8 -0.18 0.55 0 -3 2 13 7.87 1.10 0 -3 6 -9 16.63 0.82 0 -2 0 9 133.83 1.19 0 -1 1 12 7.46 0.69 0 -1 7 -10 7.24 0.83 0 0 1 12 6.01 0.67 0 1 7 -10 4.70 0.80 0 2 3 -6 13.57 0.42 0 2 3 15 -0.26 0.99 0 3 5 -8 0.25 0.57 0 4 4 -6 9.67 0.46 0 5 2 10 108.52 1.03 0 6 2 4 1.05 0.14 0 6 2 6 -0.01 0.24 0 7 4 12 17.48 0.81 0 9 5 0 4.52 0.34 0 9 5 10 53.71 0.86 0 -8 3 7 2.99 0.79 0 -7 6 -6 11.79 0.64 0 -6 1 7 6.85 0.59 0 -6 2 10 29.51 1.01 0 -5 1 9 0.22 0.56 0 -5 2 11 11.90 1.01 0 -4 1 10 4.00 0.76 0 -3 0 8 229.06 1.45 0 -3 1 11 14.52 0.76 0 -2 3 -7 0.52 0.38 0 -2 4 -8 354.30 1.78 0 -2 7 -10 7.90 0.85 0 -1 3 -7 9.64 0.41 0 -1 5 -9 55.30 0.93 0 1 0 7 146.90 0.97 0 1 1 11 5.06 0.58 0 1 2 -5 1290.72 2.54 0 2 2 13 5.57 0.77 0 2 7 -10 0.58 0.77 0 3 4 -7 61.02 0.82 0 3 6 -9 23.27 0.80 0 4 8 -10 19.03 1.06 0 6 3 11 42.95 0.85 0 6 4 -4 56.94 0.68 0 6 6 -7 99.91 1.18 0 7 3 8 13.77 0.45 0 7 7 -7 127.45 1.41 0 7 8 -8 18.69 1.06 0 8 4 0 3.57 0.27 0 8 8 -7 30.93 1.09 0 10 6 0 45.53 0.61 0 10 8 -4 6.27 0.82 0 -8 3 6 6.43 0.73 0 -7 2 7 0.00 0.64 0 -6 3 11 11.54 1.15 0 -4 0 1 67.79 0.36 0 -4 0 6 50.52 0.66 0 -4 2 -5 333.46 1.19 0 -4 3 13 70.65 1.64 0 -4 6 -9 81.68 1.19 0 -3 4 -8 65.17 0.87 0 -3 7 -10 140.88 1.67 0 -2 2 13 2.32 0.86 0 -1 1 11 9.20 0.62 0 -1 2 13 54.63 1.26 0 0 8 -11 9.92 1.06 0 1 2 13 95.87 1.35 0 1 8 -11 13.82 1.10 0 2 1 -2 81.45 0.45 0 3 3 14 2.20 0.84 0 3 7 -10 28.70 0.99 0 5 3 12 143.65 1.46 0 5 4 14 -0.28 1.00 0 5 5 -7 177.06 1.43 0 5 6 -8 56.31 1.00 0 5 7 -9 76.81 1.28 0 6 4 13 153.85 1.64 0 6 5 -6 210.42 1.48 0 6 8 -9 15.26 0.99 0 8 5 -3 8.02 0.46 0 8 5 12 2.99 0.78 0 9 6 -3 21.25 0.64 0 9 8 -6 27.91 1.04 0 11 8 -2 7.40 0.76 0 -7 3 9 -0.14 0.79 0 -6 4 -6 4.76 0.42 0 -5 3 12 21.48 1.17 0 -4 0 5 235.41 1.19 0 -3 1 10 1.73 0.58 0 -3 2 12 16.55 0.92 0 -3 3 -7 100.97 0.89 0 -3 5 -9 1.77 0.64 0 -2 3 14 17.66 1.17 0 0 0 7 299.48 1.39 0 1 3 -7 28.87 0.56 0 2 2 12 41.97 0.99 0 2 5 -9 26.67 0.76 0 2 6 -10 201.36 1.79 0 3 4 15 0.26 1.12 0 3 8 -11 0.94 1.08 0 4 1 5 43.57 0.42 0 4 3 -5 197.28 1.14 0 7 4 11 13.44 0.68 0 7 5 -5 255.27 1.53 0 8 6 -5 35.60 0.82 0 9 5 9 1.08 0.46 0 9 7 -5 12.55 0.76 0 11 7 0 -0.27 0.48 0 -8 3 5 19.41 0.69 0 -8 5 -4 12.22 0.41 0 -7 2 6 1.38 0.57 0 -6 3 -5 187.60 0.92 0 -5 2 10 97.77 1.32 0 -5 3 -6 9.13 0.38 0 -4 0 2 402.20 1.05 0 -4 1 9 0.82 0.52 0 -4 2 11 -0.63 0.74 0 -3 0 6 33.01 0.53 0 -3 3 13 25.05 1.29 0 -2 1 -4 12.70 0.25 0 -2 1 10 -0.02 0.58 0 -1 3 14 0.40 0.94 0 -1 7 -11 8.81 1.05 0 0 3 14 40.08 1.21 0 1 0 5 1206.57 2.19 0 1 3 14 7.66 0.96 0 1 7 -11 7.63 0.91 0 3 1 8 4.54 0.35 0 4 1 3 1.82 0.12 0 4 2 10 0.01 0.50 0 4 4 -7 93.84 1.03 0 5 3 -4 39.90 0.54 0 5 4 -6 10.21 0.53 0 6 3 10 38.98 0.75 0 7 4 -3 27.49 0.51 0 7 5 13 80.98 1.34 0 -8 3 1 11.76 0.37 0 -7 2 5 0.82 0.52 0 -7 4 -5 25.40 0.48 0 -6 1 1 61.40 0.43 0 -6 2 8 0.36 0.65 0 -6 3 10 8.99 0.88 0 -6 6 -8 4.00 0.74 0 -5 1 7 285.62 1.64 0 -4 3 -7 5.06 0.40 0 -4 4 -8 36.75 0.71 0 -3 0 0 795.81 0.73 0 -2 0 6 1.63 0.34 0 -2 7 -11 15.20 1.08 0 -1 1 10 5.38 0.53 0 -1 2 12 -0.05 0.65 0 -1 4 -9 160.21 1.36 0 0 0 6 365.85 1.39 0 0 1 10 27.87 0.68 0 0 2 -6 17.10 0.40 0 0 2 12 1.03 0.62 0 0 4 -9 45.93 0.86 0 0 5 -10 8.76 0.75 0 1 0 2 49.61 0.27 0 1 0 4 19.20 0.28 0 1 2 12 3.02 0.63 0 1 4 15 0.65 1.08 0 2 3 -7 40.70 0.64 0 3 1 -1 0.71 0.10 0 3 3 13 1.53 0.72 0 3 5 -9 0.96 0.56 0 4 2 -3 376.54 1.24 0 4 4 14 4.56 0.87 0 4 8 -11 0.56 1.00 0 5 2 8 45.77 0.63 0 6 4 -5 83.17 0.89 0 6 4 12 1.05 0.73 0 6 6 -8 4.23 0.65 0 6 7 -9 4.13 0.80 0 7 7 -8 0.90 0.73 0 7 8 -9 16.69 1.02 0 8 4 8 279.39 1.28 0 8 5 11 27.95 0.83 0 8 7 -7 -0.59 0.77 0 8 8 -8 4.46 1.00 0 10 6 -1 -0.03 0.43 0 10 8 -5 182.72 1.69 0 11 8 -3 5.87 0.77 0 -8 3 2 0.97 0.37 0 -8 3 3 7.26 0.48 0 -6 1 2 139.76 0.73 0 -6 1 3 136.00 0.83 0 -5 6 -9 8.51 0.77 0 -4 1 8 107.97 1.09 0 -4 2 10 15.55 0.84 0 -3 0 5 575.99 1.73 0 -3 1 -4 2834.22 2.85 0 -2 3 13 3.88 0.92 0 -2 4 -9 0.32 0.46 0 -2 4 14 42.83 1.53 0 -2 5 -10 34.72 0.93 0 -1 3 -8 114.44 1.01 0 -1 5 -10 18.34 0.74 0 0 1 -4 7.02 0.23 0 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44.85 0.91 0 -1 2 11 49.42 0.94 0 -1 7 -12 0.13 1.06 0 0 0 4 260.15 0.94 0 0 2 11 6.26 0.59 0 0 7 -12 4.77 0.97 0 1 3 -8 11.67 0.49 0 1 7 -12 134.81 1.78 0 2 1 -3 696.92 1.47 0 2 4 -9 1.64 0.49 0 2 4 14 16.90 1.04 0 2 6 -11 35.45 1.02 0 3 3 -7 16.13 0.49 0 3 3 12 3.07 0.61 0 4 4 13 0.06 0.80 0 5 3 -5 5.51 0.41 0 5 4 -7 8.47 0.56 0 6 5 13 17.50 0.97 0 7 4 -4 61.79 0.73 0 9 5 -2 0.66 0.38 0 10 6 -2 10.74 0.54 0 -7 3 6 20.09 0.75 0 -7 4 8 27.32 0.96 0 -6 2 6 185.96 1.34 0 -6 5 -8 -0.36 0.54 0 -5 2 8 12.26 0.60 0 -5 3 -7 30.37 0.58 0 -5 4 11 24.97 1.12 0 -5 5 -9 49.31 0.93 0 -4 2 9 11.11 0.69 0 -4 4 12 23.28 1.14 0 -3 0 1 582.14 0.94 0 -3 0 2 0.77 0.13 0 -3 0 3 48.39 0.42 0 -3 2 10 1.64 0.59 0 -2 0 4 122.60 0.71 0 -2 2 -7 219.27 1.19 0 -2 3 12 1.52 0.76 0 -2 4 13 -0.74 1.06 0 -1 2 -7 11.72 0.39 0 0 2 -7 72.11 0.76 0 2 2 -6 316.35 1.40 0 2 2 10 0.97 0.51 0 2 3 -8 78.33 0.92 0 2 7 -12 123.50 1.73 0 3 1 6 0.24 0.21 0 3 5 -10 15.99 0.74 0 3 6 -11 0.38 0.76 0 4 3 11 26.53 0.71 0 5 2 -2 127.31 0.67 0 5 4 12 13.91 0.71 0 5 6 -10 0.37 0.83 0 6 4 -6 46.10 0.76 0 6 4 11 24.92 0.70 0 6 6 -9 25.86 0.88 0 6 7 -10 6.98 0.91 0 7 6 -8 5.61 0.75 0 8 4 -2 32.67 0.51 0 8 5 10 6.31 0.60 0 8 6 12 0.59 0.80 0 8 7 -8 10.05 0.82 0 -6 2 -4 10.06 0.25 0 -6 3 -6 31.84 0.50 0 -6 3 8 6.20 0.66 0 -5 6 -10 12.59 0.85 0 -4 1 -4 1.93 0.18 0 -4 3 -8 37.49 0.65 0 -4 4 -9 24.98 0.65 0 -4 5 -10 115.79 1.32 0 -3 3 11 2.44 0.84 0 -2 1 -5 134.42 0.74 0 -2 2 10 28.59 0.76 0 -2 4 -10 29.69 0.83 0 -1 0 4 162.97 0.77 0 -1 5 -11 8.26 0.73 0 0 0 3 35.22 0.31 0 0 4 -10 14.55 0.65 0 0 5 -11 0.17 0.64 0 0 6 -12 15.90 1.07 0 1 3 12 -0.32 0.61 0 1 4 -10 2.36 0.61 0 3 4 -9 7.10 0.55 0 3 4 13 0.62 0.73 0 3 7 -12 37.76 1.23 0 4 2 8 7.71 0.41 0 5 5 -9 48.16 0.95 0 5 7 -11 38.21 1.20 0 6 3 8 1.20 0.35 0 7 3 -1 16.85 0.31 0 7 4 9 141.69 1.09 0 8 5 -5 10.54 0.58 0 9 6 -5 7.72 0.57 0 9 6 10 14.81 0.68 0 10 7 -5 1.39 0.75 0 -8 5 -5 0.86 0.37 0 -7 3 5 34.52 0.76 0 -7 4 7 1.46 0.80 0 -7 5 -7 2.17 0.53 0 -6 4 9 23.03 0.95 0 -5 3 9 3.53 0.64 0 -4 1 6 49.52 0.66 0 -4 6 -11 5.80 0.90 0 -3 2 -7 124.60 0.89 0 -3 2 9 0.52 0.58 0 -2 0 3 14.11 0.24 0 -2 3 -9 244.93 1.51 0 -2 5 -11 9.05 0.74 0 -1 0 -1 1133.81 0.83 0 -1 2 10 90.61 1.07 0 -1 3 -9 59.62 0.83 0 -1 4 13 -0.21 0.83 0 -1 6 -12 4.48 0.88 0 0 1 -5 9.95 0.29 0 0 2 10 35.23 0.75 0 0 4 13 3.60 0.95 0 1 2 -7 1.00 0.30 0 1 2 10 18.67 0.60 0 2 4 13 9.39 0.82 0 2 5 -11 6.45 0.72 0 3 1 5 195.89 0.84 0 3 5 14 1.14 0.90 0 4 5 -10 1.21 0.62 0 4 6 -11 32.72 1.05 0 4 7 -12 -2.01 1.09 0 5 5 13 26.46 0.93 0 6 5 12 71.75 1.17 0 7 4 -5 20.56 0.58 0 7 5 -7 354.85 1.98 0 7 5 11 -0.04 0.63 0 9 5 -3 46.13 0.69 0 10 6 7 26.75 0.52 0 -8 4 3 5.93 0.56 0 -6 3 7 -0.04 0.64 0 -5 4 10 38.56 1.08 0 -4 2 8 52.65 0.84 0 -4 4 11 0.89 0.81 0 -3 1 -5 303.45 1.06 0 -3 4 -10 17.73 0.65 0 -3 5 -11 125.24 1.44 0 -2 1 7 111.12 0.95 0 -2 6 -12 9.52 0.91 0 -1 0 3 759.29 1.41 0 0 0 2 1990.91 1.75 0 1 1 7 1386.48 2.85 0 1 5 14 22.63 1.13 0 3 3 -8 2.07 0.43 0 5 3 -6 10.01 0.43 0 5 3 9 90.73 0.92 0 5 4 -8 9.13 0.56 0 5 4 11 75.07 1.04 0 6 4 10 1.33 0.55 0 6 6 -10 37.59 1.13 0 6 7 -11 19.45 1.21 0 8 7 -9 4.35 0.97 0 -5 1 -3 1.86 0.13 0 -5 2 -6 -0.41 0.29 0 -5 4 -9 27.13 0.73 0 -4 1 5 0.90 0.33 0 -3 1 6 2.53 0.36 0 -3 3 10 4.10 0.76 0 -3 6 -12 8.62 1.06 0 -2 0 2 1391.68 1.68 0 -2 2 9 4.52 0.48 0 -2 4 12 4.45 0.85 0 -1 2 -8 4.98 0.37 0 -1 3 11 169.33 1.55 0 0 2 -8 0.21 0.38 0 1 1 -5 137.40 0.80 0 1 3 11 1.75 0.63 0 2 1 6 85.66 0.66 0 2 2 -7 13.61 0.43 0 2 2 9 0.98 0.38 0 2 3 -9 29.09 0.72 0 2 3 11 42.01 0.84 0 3 4 -10 6.14 0.68 0 3 5 -11 2.75 0.71 0 3 6 -12 6.96 0.91 0 4 2 -5 441.90 1.59 0 4 5 13 6.99 0.81 0 4 6 14 64.98 1.46 0 5 2 -3 248.44 1.03 0 5 6 -11 13.50 0.91 0 6 4 -7 4.77 0.48 0 7 3 -2 114.72 0.72 0 7 6 -9 16.24 0.84 0 7 6 12 9.85 0.84 0 8 4 -3 71.05 0.71 0 8 5 -6 43.60 0.86 0 8 5 9 8.72 0.51 0 8 6 11 18.08 0.79 0 9 6 -6 100.99 1.20 0 10 7 -6 247.56 1.84 0 -8 4 2 14.83 0.53 0 -7 4 6 7.57 0.69 0 -6 4 -8 8.03 0.52 0 -6 4 8 0.28 0.67 0 -6 5 -9 11.33 0.68 0 -6 5 9 7.99 0.90 0 -5 2 6 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105.91 1.29 0 -3 6 8 2.08 0.73 0 -3 8 9 1.25 0.87 0 -2 0 -8 50.10 0.60 0 -2 3 6 10.26 0.43 0 -2 5 8 28.70 0.77 0 -1 1 3 266.41 0.85 0 -1 3 -15 29.82 1.09 0 1 3 -15 233.27 2.17 0 1 5 9 88.55 1.05 0 1 8 11 19.98 0.98 0 2 4 8 14.22 0.51 0 3 1 -10 391.83 1.98 0 3 6 10 0.27 0.52 0 5 1 -5 23.38 0.42 0 5 1 -2 34.49 0.33 0 5 2 -10 -0.07 0.51 0 5 8 11 1.11 0.71 0 7 2 -4 3.97 0.33 0 7 2 -3 4.86 0.28 0 7 4 5 -0.03 0.22 0 7 8 10 15.16 0.79 0 -5 1 -9 11.01 0.43 0 -5 3 -13 0.49 0.77 0 -5 3 3 106.54 0.80 0 -4 0 -5 12.12 0.26 0 -4 6 7 0.28 0.56 0 -3 0 -8 12.60 0.41 0 -2 7 9 7.58 0.86 0 -1 0 -9 2.83 0.36 0 -1 1 -12 20.18 0.68 0 0 0 -9 53.82 0.70 0 0 1 -12 54.37 0.91 0 0 2 -14 32.26 1.06 0 0 7 10 0.27 0.66 0 2 0 -7 31.17 0.50 0 2 1 -11 3.46 0.52 0 2 5 9 245.52 1.54 0 2 8 11 17.66 0.92 0 3 8 11 39.90 1.06 0 4 2 -12 32.82 0.96 0 4 3 -14 4.07 1.02 0 4 8 11 187.51 1.72 0 5 1 -6 100.39 0.83 0 5 3 -13 75.66 1.33 0 5 7 10 0.64 0.61 0 6 2 -9 6.57 0.62 0 6 9 11 0.79 0.79 0 7 2 -5 13.35 0.43 0 7 6 8 13.16 0.52 0 8 6 7 4.47 0.40 0 9 4 -8 0.49 0.57 0 -6 2 -10 68.70 0.81 0 -6 6 4 15.55 0.66 0 -5 4 4 6.51 0.44 0 -5 7 6 6.06 0.77 0 -4 1 -11 24.41 0.65 0 -4 5 6 172.29 1.35 0 -3 3 5 78.01 0.73 0 -3 5 7 290.43 1.70 0 -2 1 -12 5.22 0.54 0 -2 2 -14 69.61 1.17 0 1 2 -14 81.94 1.28 0 1 2 5 55.20 0.50 0 1 7 10 21.29 0.88 0 2 0 -8 5.39 0.42 0 2 9 11 -0.18 0.99 0 3 0 -5 558.42 1.61 0 3 0 -4 437.65 1.29 0 3 2 -13 33.72 0.96 0 4 7 10 62.64 1.05 0 5 1 -7 181.42 1.16 0 5 5 8 9.82 0.42 0 5 9 11 159.65 1.75 0 6 3 -12 4.59 0.79 0 8 3 -8 1.43 0.61 0 8 7 8 65.15 0.86 0 9 4 -9 17.58 0.84 0 -4 7 7 0.92 0.65 0 -3 1 -12 18.73 0.64 0 -2 8 9 0.70 0.80 0 -1 3 6 8.75 0.35 0 -1 4 7 7.43 0.42 0 0 6 9 8.23 0.59 0 0 8 10 0.21 0.76 0 2 1 -12 7.24 0.61 0 2 2 -14 21.74 0.93 0 2 7 10 76.52 1.11 0 3 0 -6 32.18 0.48 0 3 9 11 0.71 0.85 0 4 1 -10 336.50 1.85 0 4 4 7 150.21 0.96 0 6 8 10 3.22 0.64 0 7 3 -11 57.77 1.09 0 ; _shelx_hkl_checksum 25741 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O3 O 0.59018(8) 0.59097(8) 0.81178(6) 0.01468(15) Uani 1 1 d . . . . . O1 O 0.88917(8) 0.24730(8) 0.66561(6) 0.01491(15) Uani 1 1 d . . . . . O2 O 0.85201(9) -0.00599(8) 0.62109(6) 0.01788(16) Uani 1 1 d . . . . . O4 O 0.36210(9) 0.82012(9) 0.71995(6) 0.01906(16) Uani 1 1 d . . . . . N1 N 0.87062(10) 0.43595(10) 0.80227(7) 0.01375(16) Uani 1 1 d . . . . . N2 N 1.09311(10) 0.50767(10) 0.78029(8) 0.01708(17) Uani 1 1 d . . . . . C9 C 0.60416(12) 0.60973(11) 0.69248(8) 0.01378(18) Uani 1 1 d . . . . . C17 C 0.94743(11) 0.53476(11) 0.83452(8) 0.01379(18) Uani 1 1 d . . . . . C14 C 0.73550(12) 0.51763(11) 0.62230(8) 0.01392(18) Uani 1 1 d . . . . . C1 C 0.77343(11) 0.21373(11) 0.73438(8) 0.01392(18) Uani 1 1 d . . . . . C6 C 0.68126(11) 0.30853(11) 0.82389(8) 0.01425(18) Uani 1 1 d . . . . . C15 C 0.87970(11) 0.40259(11) 0.67862(8) 0.01342(18) Uani 1 1 d . . . . . H15 H 0.9798 0.4133 0.6403 0.016 Uiso 1 1 calc R U . . . C7 C 0.71336(11) 0.45153(11) 0.85258(8) 0.01355(18) Uani 1 1 d . . . . . H7 H 0.7136 0.4566 0.9394 0.016 Uiso 1 1 calc R U . . . C2 C 0.75398(12) 0.07442(11) 0.71157(8) 0.01506(19) Uani 1 1 d . . . . . C10 C 0.47923(12) 0.73121(11) 0.64250(9) 0.01591(19) Uani 1 1 d . . . . . C13 C 0.73807(13) 0.54061(12) 0.50084(9) 0.01715(19) Uani 1 1 d . . . . . H13 H 0.8265 0.4769 0.4525 0.021 Uiso 1 1 calc R U . . . C18 C 0.87822(12) 0.64827(11) 0.91875(8) 0.01575(19) Uani 1 1 d . . . . . H18 H 0.7737 0.6646 0.9544 0.019 Uiso 1 1 calc R U . . . C11 C 0.48374(13) 0.75207(12) 0.52199(9) 0.0199(2) Uani 1 1 d . . . . . H11 H 0.3989 0.8324 0.4874 0.024 Uiso 1 1 calc R U . . . C19 C 0.96484(13) 0.73703(11) 0.94966(9) 0.01685(19) Uani 1 1 d . . . . . C21 C 1.17396(13) 0.59557(13) 0.80972(9) 0.0192(2) Uani 1 1 d . . . . . H21 H 1.2771 0.5784 0.7713 0.023 Uiso 1 1 calc R U . . . C5 C 0.56653(12) 0.26486(12) 0.89128(9) 0.0182(2) Uani 1 1 d . . . . . H5 H 0.5034 0.3283 0.9532 0.022 Uiso 1 1 calc R U . . . C3 C 0.63871(13) 0.03338(12) 0.77829(9) 0.0187(2) Uani 1 1 d . . . . . H3 H 0.6234 -0.0597 0.7632 0.022 Uiso 1 1 calc R U . . . C4 C 0.54525(13) 0.12956(12) 0.86777(9) 0.0201(2) Uani 1 1 d . . . . . H4 H 0.466 0.1015 0.913 0.024 Uiso 1 1 calc R U . . . C12 C 0.61249(14) 0.65541(13) 0.45124(9) 0.0206(2) Uani 1 1 d . . . . . H12 H 0.6135 0.6688 0.3687 0.025 Uiso 1 1 calc R U . . . C20 C 1.11633(13) 0.71000(12) 0.89278(9) 0.0189(2) Uani 1 1 d . . . . . H20 H 1.1788 0.7689 0.9106 0.023 Uiso 1 1 calc R U . . . C8 C 0.85255(14) -0.15665(12) 0.60200(10) 0.0226(2) Uani 1 1 d . . . . . H8A H 0.9326 -0.2049 0.5382 0.034 Uiso 1 1 calc R U . . . H8B H 0.7456 -0.1492 0.5812 0.034 Uiso 1 1 calc R U . . . H8C H 0.8799 -0.2192 0.6735 0.034 Uiso 1 1 calc R U . . . C22 C 0.89446(14) 0.85900(13) 1.04110(10) 0.0220(2) Uani 1 1 d . . . . . H22A H 0.8165 0.951 1.0064 0.033 Uiso 1 1 calc R U . . . H22B H 0.9809 0.8854 1.071 0.033 Uiso 1 1 calc R U . . . H22C H 0.8402 0.8199 1.1055 0.033 Uiso 1 1 calc R U . . . C16 C 0.23401(15) 0.94463(14) 0.67179(11) 0.0291(3) Uani 1 1 d . . . . . H16A H 0.1848 0.905 0.6136 0.044 Uiso 1 1 calc R U . . . H16B H 0.2768 1.0197 0.6344 0.044 Uiso 1 1 calc R U . . . H16C H 0.1526 0.9946 0.7343 0.044 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O3 0.0148(3) 0.0143(3) 0.0124(3) -0.0005(2) 0.0009(2) -0.0027(3) O1 0.0152(3) 0.0128(3) 0.0168(3) -0.0026(2) 0.0030(3) -0.0057(3) O2 0.0205(4) 0.0132(3) 0.0198(4) -0.0040(3) 0.0013(3) -0.0061(3) O4 0.0158(3) 0.0185(4) 0.0181(3) -0.0006(3) -0.0002(3) -0.0006(3) N1 0.0135(4) 0.0153(4) 0.0128(4) -0.0021(3) 0.0007(3) -0.0057(3) N2 0.0155(4) 0.0194(4) 0.0170(4) -0.0013(3) -0.0005(3) -0.0072(3) C9 0.0156(4) 0.0144(4) 0.0127(4) -0.0004(3) -0.0009(3) -0.0071(3) C17 0.0150(4) 0.0134(4) 0.0131(4) 0.0017(3) -0.0030(3) -0.0050(3) C14 0.0153(4) 0.0136(4) 0.0139(4) -0.0007(3) 0.0000(3) -0.0065(3) C1 0.0130(4) 0.0144(4) 0.0144(4) 0.0011(3) -0.0010(3) -0.0050(3) C6 0.0137(4) 0.0144(4) 0.0146(4) 0.0000(3) -0.0006(3) -0.0050(3) C15 0.0142(4) 0.0131(4) 0.0133(4) -0.0021(3) 0.0012(3) -0.0055(3) C7 0.0135(4) 0.0137(4) 0.0127(4) -0.0004(3) 0.0000(3) -0.0043(3) C2 0.0152(4) 0.0136(4) 0.0155(4) 0.0001(3) -0.0027(3) -0.0038(3) C10 0.0151(4) 0.0153(4) 0.0174(4) -0.0012(3) -0.0007(3) -0.0056(4) C13 0.0207(5) 0.0173(5) 0.0140(4) -0.0020(3) 0.0008(3) -0.0076(4) C18 0.0157(4) 0.0151(4) 0.0158(4) -0.0008(3) -0.0012(3) -0.0048(4) C11 0.0205(5) 0.0195(5) 0.0181(5) 0.0020(4) -0.0053(4) -0.0049(4) C19 0.0202(5) 0.0146(4) 0.0158(4) 0.0006(3) -0.0042(3) -0.0058(4) C21 0.0174(5) 0.0231(5) 0.0194(5) -0.0006(4) -0.0004(4) -0.0100(4) C5 0.0161(4) 0.0187(5) 0.0186(5) -0.0005(4) 0.0022(4) -0.0058(4) C3 0.0195(5) 0.0164(5) 0.0223(5) 0.0020(4) -0.0030(4) -0.0087(4) C4 0.0186(5) 0.0211(5) 0.0223(5) 0.0024(4) 0.0017(4) -0.0102(4) C12 0.0258(5) 0.0220(5) 0.0133(4) 0.0005(4) -0.0026(4) -0.0078(4) C20 0.0206(5) 0.0195(5) 0.0199(5) 0.0004(4) -0.0044(4) -0.0104(4) C8 0.0298(6) 0.0126(5) 0.0259(5) -0.0027(4) -0.0022(4) -0.0077(4) C22 0.0232(5) 0.0188(5) 0.0242(5) -0.0059(4) -0.0030(4) -0.0072(4) C16 0.0228(5) 0.0273(6) 0.0251(6) 0.0007(4) -0.0030(4) 0.0054(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 3 2 6 0.139 4 1 4 0.138 5 -1 -3 0.247 0 -1 -4 0.178 -3 -2 -8 0.17 -5 -1 -3 0.241 -3 1 5 0.227 1 1 -1 0.142 1 8 -2 0.154 -7 1 6 0.203 -2 -8 3 0.152 2 -9 -1 0.195 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C9 O3 C7 112.23(7) . . ? C1 O1 C15 112.51(7) . . ? C2 O2 C8 117.26(8) . . ? C10 O4 C16 116.57(8) . . ? C17 N1 C7 120.76(8) . . ? C17 N1 C15 117.37(8) . . ? C7 N1 C15 108.74(7) . . ? C17 N2 C21 117.05(9) . . ? O3 C9 C14 123.04(9) . . ? O3 C9 C10 116.69(8) . . ? C14 C9 C10 120.25(9) . . ? N2 C17 C18 123.26(9) . . ? N2 C17 N1 114.34(8) . . ? C18 C17 N1 122.37(9) . . ? C9 C14 C13 119.57(9) . . ? C9 C14 C15 119.62(8) . . ? C13 C14 C15 120.63(8) . . ? O1 C1 C6 122.74(9) . . ? O1 C1 C2 116.33(8) . . ? C6 C1 C2 120.91(9) . . ? C1 C6 C5 119.20(9) . . ? C1 C6 C7 119.83(8) . . ? C5 C6 C7 120.85(9) . . ? O1 C15 N1 109.51(7) . . ? O1 C15 C14 111.93(8) . . ? N1 C15 C14 109.64(8) . . ? O1 C15 H15 108.6 . . ? N1 C15 H15 108.6 . . ? C14 C15 H15 108.6 . . ? N1 C7 O3 111.82(7) . . ? N1 C7 C6 107.97(8) . . ? O3 C7 C6 111.79(8) . . ? N1 C7 H7 108.4 . . ? O3 C7 H7 108.4 . . ? C6 C7 H7 108.4 . . ? O2 C2 C3 126.40(9) . . ? O2 C2 C1 114.33(8) . . ? C3 C2 C1 119.25(9) . . ? O4 C10 C11 125.43(9) . . ? O4 C10 C9 115.32(9) . . ? C11 C10 C9 119.25(9) . . ? C12 C13 C14 120.21(9) . . ? C12 C13 H13 119.9 . . ? C14 C13 H13 119.9 . . ? C19 C18 C17 118.97(9) . . ? C19 C18 H18 120.5 . . ? C17 C18 H18 120.5 . . ? C10 C11 C12 120.34(10) . . ? C10 C11 H11 119.8 . . ? C12 C11 H11 119.8 . . ? C18 C19 C20 117.99(9) . . ? C18 C19 C22 120.28(9) . . ? C20 C19 C22 121.73(9) . . ? N2 C21 C20 124.02(10) . . ? N2 C21 H21 118 . . ? C20 C21 H21 118 . . ? C4 C5 C6 120.00(9) . . ? C4 C5 H5 120 . . ? C6 C5 H5 120 . . ? C2 C3 C4 119.72(9) . . ? C2 C3 H3 120.1 . . ? C4 C3 H3 120.1 . . ? C5 C4 C3 120.90(9) . . ? C5 C4 H4 119.5 . . ? C3 C4 H4 119.5 . . ? C13 C12 C11 120.25(9) . . ? C13 C12 H12 119.9 . . ? C11 C12 H12 119.9 . . ? C21 C20 C19 118.69(9) . . ? C21 C20 H20 120.7 . . ? C19 C20 H20 120.7 . . ? O2 C8 H8A 109.5 . . ? O2 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? O2 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C19 C22 H22A 109.5 . . ? C19 C22 H22B 109.5 . . ? H22A C22 H22B 109.5 . . ? C19 C22 H22C 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? O4 C16 H16A 109.5 . . ? O4 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? O4 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O3 C9 1.3746(11) . ? O3 C7 1.4523(11) . ? O1 C1 1.3680(11) . ? O1 C15 1.4314(11) . ? O2 C2 1.3611(12) . ? O2 C8 1.4276(12) . ? O4 C10 1.3628(12) . ? O4 C16 1.4289(13) . ? N1 C17 1.4074(12) . ? N1 C7 1.4338(12) . ? N1 C15 1.4556(12) . ? N2 C17 1.3375(12) . ? N2 C21 1.3401(13) . ? C9 C14 1.3926(13) . ? C9 C10 1.4085(13) . ? C17 C18 1.3976(13) . ? C14 C13 1.4010(13) . ? C14 C15 1.5151(13) . ? C1 C6 1.3889(13) . ? C1 C2 1.4077(13) . ? C6 C5 1.4005(13) . ? C6 C7 1.5145(13) . ? C15 H15 1 . ? C7 H7 1 . ? C2 C3 1.3877(14) . ? C10 C11 1.3879(14) . ? C13 C12 1.3799(14) . ? C13 H13 0.95 . ? C18 C19 1.3926(14) . ? C18 H18 0.95 . ? C11 C12 1.3983(15) . ? C11 H11 0.95 . ? C19 C20 1.3947(15) . ? C19 C22 1.5056(14) . ? C21 C20 1.3861(15) . ? C21 H21 0.95 . ? C5 C4 1.3812(14) . ? C5 H5 0.95 . ? C3 C4 1.3980(15) . ? C3 H3 0.95 . ? C4 H4 0.95 . ? C12 H12 0.95 . ? C20 H20 0.95 . ? C8 H8A 0.98 . ? C8 H8B 0.98 . ? C8 H8C 0.98 . ? C22 H22A 0.98 . ? C22 H22B 0.98 . ? C22 H22C 0.98 . ? C16 H16A 0.98 . ? C16 H16B 0.98 . ? C16 H16C 0.98 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C7 O3 C9 C14 -8.96(12) . . . . ? C7 O3 C9 C10 172.53(8) . . . . ? C21 N2 C17 C18 -0.11(14) . . . . ? C21 N2 C17 N1 -178.30(9) . . . . ? C7 N1 C17 N2 -179.66(8) . . . . ? C15 N1 C17 N2 -42.84(12) . . . . ? C7 N1 C17 C18 2.13(14) . . . . ? C15 N1 C17 C18 138.95(9) . . . . ? O3 C9 C14 C13 177.75(8) . . . . ? C10 C9 C14 C13 -3.80(14) . . . . ? O3 C9 C14 C15 -7.13(14) . . . . ? C10 C9 C14 C15 171.32(8) . . . . ? C15 O1 C1 C6 -12.89(12) . . . . ? C15 O1 C1 C2 168.48(8) . . . . ? O1 C1 C6 C5 -179.20(9) . . . . ? C2 C1 C6 C5 -0.63(14) . . . . ? O1 C1 C6 C7 -3.24(14) . . . . ? C2 C1 C6 C7 175.33(9) . . . . ? C1 O1 C15 N1 49.59(10) . . . . ? C1 O1 C15 C14 -72.21(9) . . . . ? C17 N1 C15 O1 145.19(8) . . . . ? C7 N1 C15 O1 -73.20(9) . . . . ? C17 N1 C15 C14 -91.65(10) . . . . ? C7 N1 C15 C14 49.97(10) . . . . ? C9 C14 C15 O1 107.65(10) . . . . ? C13 C14 C15 O1 -77.29(11) . . . . ? C9 C14 C15 N1 -14.07(12) . . . . ? C13 C14 C15 N1 160.99(9) . . . . ? C17 N1 C7 O3 70.05(11) . . . . ? C15 N1 C7 O3 -70.03(9) . . . . ? C17 N1 C7 C6 -166.58(8) . . . . ? C15 N1 C7 C6 53.35(10) . . . . ? C9 O3 C7 N1 47.43(10) . . . . ? C9 O3 C7 C6 -73.76(9) . . . . ? C1 C6 C7 N1 -17.73(12) . . . . ? C5 C6 C7 N1 158.16(9) . . . . ? C1 C6 C7 O3 105.66(10) . . . . ? C5 C6 C7 O3 -78.45(11) . . . . ? C8 O2 C2 C3 -8.91(15) . . . . ? C8 O2 C2 C1 172.71(9) . . . . ? O1 C1 C2 O2 -1.56(12) . . . . ? C6 C1 C2 O2 179.78(8) . . . . ? O1 C1 C2 C3 179.93(9) . . . . ? C6 C1 C2 C3 1.27(14) . . . . ? C16 O4 C10 C11 0.06(15) . . . . ? C16 O4 C10 C9 179.79(9) . . . . ? O3 C9 C10 O4 2.69(13) . . . . ? C14 C9 C10 O4 -175.86(9) . . . . ? O3 C9 C10 C11 -177.56(9) . . . . ? C14 C9 C10 C11 3.89(14) . . . . ? C9 C14 C13 C12 1.06(15) . . . . ? C15 C14 C13 C12 -174.01(9) . . . . ? N2 C17 C18 C19 -0.87(15) . . . . ? N1 C17 C18 C19 177.18(9) . . . . ? O4 C10 C11 C12 178.48(10) . . . . ? C9 C10 C11 C12 -1.24(16) . . . . ? C17 C18 C19 C20 1.27(14) . . . . ? C17 C18 C19 C22 -179.29(9) . . . . ? C17 N2 C21 C20 0.68(16) . . . . ? C1 C6 C5 C4 -0.51(15) . . . . ? C7 C6 C5 C4 -176.42(9) . . . . ? O2 C2 C3 C4 -179.09(9) . . . . ? C1 C2 C3 C4 -0.78(15) . . . . ? C6 C5 C4 C3 1.00(16) . . . . ? C2 C3 C4 C5 -0.35(16) . . . . ? C14 C13 C12 C11 1.59(16) . . . . ? C10 C11 C12 C13 -1.48(17) . . . . ? N2 C21 C20 C19 -0.24(16) . . . . ? C18 C19 C20 C21 -0.76(15) . . . . ? C22 C19 C20 C21 179.81(10) . . . . ?