#------------------------------------------------------------------------------ #$Date: 2023-05-05 04:27:30 +0300 (Fri, 05 May 2023) $ #$Revision: 283216 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/64/7246468.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7246468 loop_ _publ_author_name 'Angevine, Devin J.' 'Mitchell, Travis' 'Zhang, Xiaotong' 'Benedict, Jason B.' _publ_section_title ; Unusual single crystal to single crystal phase transition of a nicotine salt monitored using temperature dependent single crystal X-ray diffraction ; _journal_issue 15 _journal_name_full CrystEngComm _journal_page_first 2181 _journal_page_last 2184 _journal_paper_doi 10.1039/D3CE00042G _journal_volume 25 _journal_year 2023 _chemical_absolute_configuration rm _chemical_formula_moiety 'C10 H15 N2, C7 H5 O4' _chemical_formula_sum 'C17 H20 N2 O4' _chemical_formula_weight 316.35 _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2022-11-30 _audit_creation_method ; Olex2 1.5 (compiled 2021.12.09 svn.r5202d8cf for OlexSys, GUI svn.r6439) ; _audit_update_record ; 2023-03-03 deposited with the CCDC. 2023-03-17 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 101.9950(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 9.9691(4) _cell_length_b 11.5520(4) _cell_length_c 13.8196(5) _cell_measurement_reflns_used 6299 _cell_measurement_temperature 90 _cell_measurement_theta_max 27.30 _cell_measurement_theta_min 2.31 _cell_volume 1556.76(10) _computing_cell_refinement 'SAINT V8.38A (?, 2016)' _computing_data_reduction 'SAINT V8.38A (?, 2016)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 90 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0299 _diffrn_reflns_av_unetI/netI 0.0293 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 28199 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.366 _diffrn_reflns_theta_min 2.088 _exptl_absorpt_coefficient_mu 0.097 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_correction_T_min 0.7173 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1064 before and 0.0467 after correction. The Ratio of minimum to maximum transmission is 0.9619. The \l/2 correction factor is Not present. ; _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.350 _exptl_crystal_description block _exptl_crystal_F_000 672 _exptl_crystal_size_max 0.22 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.06 _refine_diff_density_max 0.244 _refine_diff_density_min -0.221 _refine_diff_density_rms 0.038 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.033 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 435 _refine_ls_number_reflns 7777 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.033 _refine_ls_R_factor_all 0.0379 _refine_ls_R_factor_gt 0.0335 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0511P)^2^+0.0326P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0844 _refine_ls_wR_factor_ref 0.0874 _reflns_Friedel_coverage 0.902 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.994 _reflns_number_gt 7118 _reflns_number_total 7777 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d3ce00042g2.cif _cod_data_source_block LT_Salt _cod_depositor_comments 'Adding full bibliography for 7246467--7246468.cif.' _cod_database_code 7246468 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups, All C(H,H,H,H,H,H) groups 2.a Ternary CH refined with riding coordinates: C6(H6), C16(H16) 2.b Secondary CH2 refined with riding coordinates: C9(H9A,H9B), C19(H19A,H19B), C17(H17A,H17B), C18(H18A,H18B), C7(H7A,H7B), C8(H8A,H8B) 2.c Aromatic/amide H refined with riding coordinates: C5(H5), C15(H15), C11(H11), C2(H2), C13(H13), C31(H31), C1(H1A), C3(H3A), C12(H12), C25(H25), C32(H32), C33(H33), C24(H24), C26(H26) 2.d Idealised Me refined as rotating group: C20(H20A,H20B,H20C), C10(H10A,H10B,H10C) ; _shelx_res_file ; TITL dja_111903_0m_a.res in P2(1) dja_111903_0m.res created by SHELXL-2018/3 at 13:58:49 on 30-Nov-2022 REM Old TITL dja_111903_0m in P21/m #11 REM SHELXT solution in P2(1): R1 0.082, Rweak 0.012, Alpha 0.001 REM 0.981 for 7 systematic absences, Orientation as input REM Flack x = -0.309 ( 0.262 ) from 2698 Parsons' quotients REM Formula found by SHELXT: C34 N4 O8 CELL 0.71073 9.9691 11.552 13.8196 90 101.995 90 ZERR 4 0.0004 0.0004 0.0005 0 0.001 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H N O UNIT 68 80 8 16 EQIV $1 2-X,-0.5+Y,-Z EQIV $2 2-X,0.5+Y,-Z EQIV $3 -1+X,+Y,-1+Z EQIV $4 1-X,0.5+Y,-Z EQIV $5 +X,+Y,1+Z EQIV $6 1-X,-0.5+Y,-Z L.S. 15 PLAN 5 TEMP 0 CONF HTAB C11 O2_$1 HTAB C31 O6 HTAB C17 O1 HTAB C7 O6_$2 HTAB C20 N2_$3 HTAB C8 O7_$4 HTAB N1 O6_$5 HTAB N1 O5_$5 HTAB N3 O1_$6 HTAB O4 O2 HTAB O8 O6 HTAB O3 O1 HTAB O7 O5 BOND list 4 MORE -1 BOND $H fmap 2 53 acta REM REM REM WGHT 0.051100 0.032600 FVAR 0.60411 O1 4 0.617988 1.248036 -0.092724 11.00000 0.01581 0.01676 = 0.01651 -0.00159 0.00499 0.00077 O6 4 0.878788 0.753886 -0.415394 11.00000 0.01546 0.01518 = 0.01592 0.00075 0.00411 -0.00139 O2 4 0.835874 1.192158 -0.047089 11.00000 0.01664 0.02366 = 0.02144 -0.00384 -0.00119 -0.00072 O5 4 0.667577 0.688796 -0.474619 11.00000 0.01742 0.02409 = 0.01989 0.00405 -0.00154 -0.00149 O3 4 0.465641 1.168733 -0.248738 11.00000 0.01516 0.02251 = 0.01804 -0.00320 -0.00117 0.00445 O4 4 0.941576 1.061471 -0.158934 11.00000 0.01288 0.02950 = 0.03833 -0.00881 0.00330 0.00333 O8 4 1.011061 0.690174 -0.245972 11.00000 0.02043 0.02361 = 0.01669 0.00209 -0.00208 -0.00612 O7 4 0.558370 0.542629 -0.378416 11.00000 0.01587 0.02888 = 0.03718 0.00897 0.00221 -0.00499 N3 3 0.349799 0.831128 -0.091927 11.00000 0.01628 0.01587 = 0.01288 0.00210 -0.00034 -0.00314 N1 3 0.863979 0.817971 0.394934 11.00000 0.01518 0.01431 = 0.01336 0.00183 0.00069 -0.00233 N4 3 0.772410 0.849633 0.107296 11.00000 0.01629 0.02438 = 0.02414 0.00507 0.00073 0.00055 N2 3 1.264909 0.848072 0.617997 11.00000 0.01862 0.02627 = 0.01908 0.00215 -0.00044 -0.00335 C21 1 0.774498 0.692152 -0.407993 11.00000 0.01459 0.01221 = 0.01594 -0.00075 0.00492 0.00155 C28 1 0.722399 1.190432 -0.106935 11.00000 0.01635 0.01199 = 0.01567 0.00209 0.00403 -0.00176 C22 1 0.783517 0.620718 -0.317447 11.00000 0.01567 0.01207 = 0.01532 0.00047 0.00524 0.00217 C34 1 0.577149 1.110571 -0.264529 11.00000 0.01786 0.01295 = 0.01341 0.00302 0.00412 0.00061 C29 1 0.705322 1.120039 -0.198775 11.00000 0.01455 0.01231 = 0.01511 0.00064 0.00473 -0.00101 C30 1 0.817291 1.056993 -0.220092 11.00000 0.01536 0.01646 = 0.02519 -0.00014 0.00778 0.00040 C14 1 0.602490 0.879735 -0.043197 11.00000 0.01554 0.01565 = 0.01824 0.00256 0.00434 -0.00312 C4 1 1.112510 0.867787 0.458367 11.00000 0.01455 0.01499 = 0.01675 0.00233 0.00361 -0.00351 C27 1 0.673704 0.547228 -0.307565 11.00000 0.01613 0.01733 = 0.02402 0.00204 0.00687 0.00009 C23 1 0.902890 0.620910 -0.241348 11.00000 0.01910 0.01313 = 0.01471 -0.00223 0.00368 0.00158 C5 1 1.145214 0.880384 0.560782 11.00000 0.01515 0.02072 = 0.01709 -0.00007 0.00392 -0.00176 AFIX 43 H5 2 1.079792 0.913339 0.591455 11.00000 -1.20000 AFIX 0 C6 1 0.976569 0.907101 0.397199 11.00000 0.01573 0.01440 = 0.01434 0.00236 0.00351 -0.00239 AFIX 13 H6 2 0.987848 0.919766 0.329225 11.00000 -1.20000 AFIX 0 C15 1 0.645906 0.879997 0.059525 11.00000 0.01399 0.02169 = 0.01750 0.00147 0.00348 0.00011 AFIX 43 H15 2 0.583314 0.902615 0.097264 11.00000 -1.20000 AFIX 0 C16 1 0.460951 0.920211 -0.092936 11.00000 0.01684 0.01715 = 0.01294 0.00368 0.00154 -0.00345 AFIX 13 H16 2 0.461928 0.938907 -0.161956 11.00000 -1.20000 AFIX 0 C11 1 0.860633 0.817804 0.051113 11.00000 0.01299 0.01913 = 0.03592 0.00013 0.00473 -0.00025 AFIX 43 H11 2 0.949227 0.797644 0.082744 11.00000 -1.20000 AFIX 0 C2 1 1.337331 0.786779 0.470753 11.00000 0.01862 0.02159 = 0.03321 -0.00260 0.00854 0.00090 AFIX 43 H2 2 1.405414 0.755075 0.441993 11.00000 -1.20000 AFIX 0 C13 1 0.696533 0.844877 -0.098815 11.00000 0.02197 0.02034 = 0.02003 -0.00220 0.00766 -0.00653 AFIX 43 H13 2 0.671635 0.842844 -0.167487 11.00000 -1.20000 AFIX 0 C9 1 0.730420 0.881142 0.353745 11.00000 0.01374 0.02040 = 0.01944 0.00429 -0.00164 0.00036 AFIX 23 H9A 2 0.660598 0.860154 0.390091 11.00000 -1.20000 H9B 2 0.697387 0.862295 0.284487 11.00000 -1.20000 AFIX 0 C31 1 0.800815 0.987082 -0.303709 11.00000 0.02431 0.01969 = 0.02873 -0.00307 0.01513 0.00122 AFIX 43 H31 2 0.874894 0.946045 -0.317496 11.00000 -1.20000 AFIX 0 C1 1 1.358281 0.802325 0.571779 11.00000 0.01449 0.02033 = 0.02993 0.00169 -0.00110 0.00053 AFIX 43 H1A 2 1.442194 0.779729 0.610167 11.00000 -1.20000 AFIX 0 C3 1 1.211799 0.819753 0.413118 11.00000 0.02029 0.02014 = 0.01894 -0.00262 0.00562 -0.00272 AFIX 43 H3A 2 1.194301 0.809796 0.344867 11.00000 -1.20000 AFIX 0 C19 1 0.216204 0.896059 -0.124293 11.00000 0.01505 0.02115 = 0.02214 0.00361 -0.00278 -0.00096 AFIX 23 H19A 2 0.147558 0.867347 -0.089814 11.00000 -1.20000 H19B 2 0.181808 0.887581 -0.194928 11.00000 -1.20000 AFIX 0 C17 1 0.402518 1.023847 -0.046974 11.00000 0.01629 0.01546 = 0.02116 0.00306 -0.00072 -0.00218 AFIX 23 H17A 2 0.446534 1.095188 -0.060516 11.00000 -1.20000 H17B 2 0.414047 1.014560 0.024038 11.00000 -1.20000 AFIX 0 C12 1 0.827864 0.813132 -0.051063 11.00000 0.01996 0.02192 = 0.03667 -0.00615 0.01368 -0.00200 AFIX 43 H12 2 0.892249 0.789307 -0.086887 11.00000 -1.20000 AFIX 0 C18 1 0.250414 1.023459 -0.097535 11.00000 0.01792 0.01950 = 0.02597 0.00652 -0.00253 0.00035 AFIX 23 H18A 2 0.234651 1.071277 -0.156513 11.00000 -1.20000 H18B 2 0.194600 1.052345 -0.053058 11.00000 -1.20000 AFIX 0 C7 1 0.909618 1.014234 0.430460 11.00000 0.01745 0.01541 = 0.02813 0.00243 0.00480 -0.00089 AFIX 23 H7A 2 0.957152 1.084170 0.417989 11.00000 -1.20000 H7B 2 0.907602 1.010227 0.500253 11.00000 -1.20000 AFIX 0 C25 1 0.803461 0.477198 -0.152870 11.00000 0.03654 0.01876 = 0.01841 0.00578 0.01282 0.00359 AFIX 43 H25 2 0.810533 0.428358 -0.098546 11.00000 -1.20000 AFIX 0 C32 1 0.673056 0.979126 -0.366274 11.00000 0.03460 0.01740 = 0.01734 -0.00388 0.01133 -0.00195 AFIX 43 H32 2 0.662390 0.931964 -0.421890 11.00000 -1.20000 AFIX 0 C33 1 0.560920 1.039522 -0.348165 11.00000 0.02468 0.01882 = 0.01476 -0.00049 0.00061 -0.00179 AFIX 43 H33 2 0.475964 1.032978 -0.390987 11.00000 -1.20000 AFIX 0 C24 1 0.912701 0.548714 -0.159045 11.00000 0.02800 0.01942 = 0.01373 0.00067 0.00299 0.00238 AFIX 43 H24 2 0.991387 0.548733 -0.109222 11.00000 -1.20000 AFIX 0 C26 1 0.683828 0.475934 -0.224972 11.00000 0.02532 0.01856 = 0.03062 0.00548 0.01330 -0.00191 AFIX 43 H26 2 0.611228 0.428123 -0.218330 11.00000 -1.20000 AFIX 0 C20 1 0.358673 0.725197 -0.150759 11.00000 0.02508 0.02108 = 0.01720 -0.00308 -0.00082 -0.00333 AFIX 137 H20A 2 0.347307 0.745357 -0.219376 11.00000 -1.50000 H20B 2 0.287814 0.672097 -0.142529 11.00000 -1.50000 H20C 2 0.446646 0.689515 -0.128483 11.00000 -1.50000 AFIX 0 C10 1 0.880129 0.709572 0.341257 11.00000 0.02402 0.01632 = 0.01962 -0.00208 -0.00029 -0.00142 AFIX 137 H10A 2 0.878468 0.726935 0.273085 11.00000 -1.50000 H10B 2 0.806391 0.657644 0.345506 11.00000 -1.50000 H10C 2 0.965994 0.673878 0.370391 11.00000 -1.50000 AFIX 0 C8 1 0.764794 1.009691 0.366295 11.00000 0.01820 0.02000 = 0.04021 0.00900 0.00172 0.00180 AFIX 23 H8A 2 0.700201 1.049046 0.398648 11.00000 -1.20000 H8B 2 0.762364 1.045877 0.302616 11.00000 -1.20000 AFIX 0 H1 2 0.864362 0.796911 0.460788 11.00000 -1.50000 H3 2 0.359069 0.805986 -0.028040 11.00000 -1.50000 H4 2 0.927030 1.105785 -0.105635 11.00000 -1.50000 H8 2 0.982513 0.725345 -0.304807 11.00000 -1.50000 H3B 2 0.500413 1.210692 -0.189285 11.00000 -1.50000 H7 2 0.574815 0.594146 -0.422930 11.00000 -1.50000 HKLF 4 REM dja_111903_0m_a.res in P2(1) REM wR2 = 0.0874, GooF = S = 1.033, Restrained GooF = 1.033 for all data REM R1 = 0.0335 for 7118 Fo > 4sig(Fo) and 0.0379 for all 7777 data REM 435 parameters refined using 1 restraints END WGHT 0.0511 0.0326 REM Highest difference peak 0.244, deepest hole -0.221, 1-sigma level 0.038 Q1 1 0.7082 1.1565 -0.1594 11.00000 0.05 0.24 Q2 1 0.6485 1.1373 -0.2387 11.00000 0.05 0.22 Q3 1 0.5760 1.0804 -0.3047 11.00000 0.05 0.21 Q4 1 0.6709 0.5325 -0.2552 11.00000 0.05 0.21 Q5 1 0.7646 1.0994 -0.2175 11.00000 0.05 0.21 ; _shelx_res_checksum 74192 _shelx_hkl_file ; -1 0 0 0.30 0.20 -1 0 0 1.00 0.20 1 0 0 0.20 0.20 1 0 0 0.40 0.20 1 0 0 0.80 0.30 -1 0 0 0.40 0.20 -1 0 0 0.30 0.10 -2 0 0 2766.22 44.70 -2 0 0 2725.73 44.80 2 0 0 2787.92 44.40 2 0 0 2771.22 45.20 -2 0 0 2825.92 46.90 3 0 0 0.20 0.40 -3 0 0 0.20 0.30 3 0 0 0.30 0.50 -3 0 0 -0.50 0.40 -4 0 0 456.05 8.60 4 0 0 469.95 10.20 4 0 0 476.85 9.80 -4 0 0 477.35 10.20 5 0 0 18.90 2.10 5 0 0 20.60 2.10 -5 0 0 16.80 2.00 -5 0 0 15.20 1.30 6 0 0 20.00 2.40 -6 0 0 26.80 1.60 6 0 0 26.80 2.60 -6 0 0 20.30 2.30 7 0 0 5.40 1.40 -7 0 0 6.40 1.60 -7 0 0 4.00 0.90 7 0 0 4.80 1.40 -8 0 0 1.50 0.80 8 0 0 0.90 1.20 8 0 0 2.40 1.30 -8 0 0 0.60 1.10 9 0 0 281.57 9.60 9 0 0 290.77 10.00 -9 0 0 288.67 7.60 -9 0 0 278.87 10.00 10 0 0 11.80 2.60 10 0 0 12.70 2.70 -10 0 0 16.30 2.10 -10 0 0 17.00 3.20 -11 0 0 1.10 1.50 11 0 0 -0.50 1.40 11 0 0 -0.90 1.40 12 0 0 8.10 2.60 -12 0 0 7.10 2.80 12 0 0 5.70 2.30 -13 0 0 0.20 2.10 13 0 0 0.90 2.10 13 0 0 -2.00 1.60 0 -1 0 0.20 0.20 0 -1 0 0.10 0.10 0 -1 0 0.00 0.10 0 -1 0 0.20 0.10 0 -1 0 0.00 0.10 0 1 0 0.30 0.20 0 1 0 0.20 0.20 1 -1 0 4.10 0.60 1 -1 0 5.10 0.40 1 -1 0 5.10 0.50 -1 -1 0 4.00 0.50 -1 -1 0 5.00 0.50 -1 -1 0 4.50 0.50 -1 -1 0 5.20 0.30 1 1 0 4.70 0.30 1 1 0 3.90 0.50 -1 1 0 5.50 0.40 -1 1 0 4.50 0.50 -1 1 0 4.90 0.70 -1 1 0 5.20 0.60 1 1 0 5.10 0.60 1 1 0 5.10 0.50 2 -1 0 1347.07 22.50 2 -1 0 1363.96 22.10 -2 -1 0 1370.86 22.20 -2 -1 0 1340.17 21.70 2 -1 0 1351.76 21.50 2 1 0 1335.87 22.20 -2 1 0 1339.57 22.10 -2 1 0 1313.87 21.50 2 1 0 1351.06 22.20 3 -1 0 22.50 1.10 -3 -1 0 23.70 1.20 3 -1 0 24.10 2.00 -3 -1 0 20.90 1.50 3 -1 0 22.20 1.50 -3 1 0 21.80 1.10 3 1 0 24.50 1.60 -3 1 0 22.60 1.50 3 1 0 25.80 1.60 -4 -1 0 199.68 5.60 4 -1 0 201.98 5.80 4 -1 0 206.88 5.50 -4 -1 0 198.58 4.80 -4 1 0 198.58 5.60 4 1 0 194.88 5.50 -4 1 0 203.68 4.20 4 1 0 196.28 5.60 5 -1 0 8.00 1.30 5 -1 0 5.00 1.30 -5 -1 0 8.00 1.00 -5 -1 0 7.00 1.40 -5 1 0 7.00 0.80 5 1 0 7.30 1.40 5 1 0 7.30 1.30 -5 1 0 4.90 1.20 6 -1 0 363.86 9.30 -6 -1 0 355.26 8.10 6 -1 0 374.56 9.90 -6 -1 0 375.56 9.90 6 1 0 372.76 9.60 6 1 0 373.56 9.70 -6 1 0 362.36 7.50 -6 1 0 366.46 9.80 -7 -1 0 18.80 1.90 7 -1 0 15.00 2.30 7 -1 0 19.20 2.40 -7 -1 0 19.50 2.60 -7 1 0 17.20 1.50 7 1 0 20.90 2.60 7 1 0 17.10 2.40 -7 1 0 11.90 2.10 8 -1 0 277.97 9.40 -8 -1 0 290.67 9.50 -8 -1 0 278.27 7.40 8 -1 0 261.57 8.50 8 1 0 275.67 9.10 8 1 0 285.57 9.30 -8 1 0 279.47 9.40 -8 1 0 277.37 6.70 -9 -1 0 2.60 1.50 9 -1 0 1.30 1.20 -9 -1 0 5.10 1.30 9 -1 0 2.40 1.50 -9 1 0 3.90 1.10 -9 1 0 7.10 2.10 9 1 0 2.40 1.60 9 1 0 3.80 1.80 10 -1 0 120.39 6.20 -10 -1 0 132.69 7.00 -10 -1 0 113.79 5.00 10 -1 0 118.59 6.60 -10 1 0 125.09 6.50 10 1 0 122.59 6.50 -10 1 0 123.09 6.80 10 1 0 130.19 6.80 11 -1 0 12.70 3.10 11 -1 0 12.10 2.80 -11 -1 0 13.10 2.20 -11 -1 0 14.00 3.20 -11 1 0 13.80 3.10 11 1 0 8.00 2.40 11 1 0 14.00 3.10 -12 -1 0 46.50 5.60 12 -1 0 50.89 5.90 12 1 0 45.60 5.60 12 1 0 41.60 5.10 -12 1 0 45.50 5.70 13 -1 0 11.20 3.20 13 1 0 8.30 2.80 0 -2 0 302.17 6.30 0 -2 0 326.27 5.80 0 -2 0 299.87 6.60 0 -2 0 309.07 5.80 0 2 0 306.17 6.30 0 2 0 323.67 5.90 1 -2 0 45.10 1.40 -1 -2 0 45.40 1.30 1 -2 0 43.50 1.30 1 -2 0 44.50 1.90 -1 -2 0 44.30 1.30 -1 -2 0 42.80 1.60 1 2 0 42.70 1.30 1 2 0 43.50 1.80 -1 2 0 42.20 1.30 1 2 0 42.90 1.80 1 2 0 44.70 1.30 -1 2 0 43.70 1.30 -1 2 0 45.50 2.00 -2 -2 0 1276.17 20.80 -2 -2 0 1259.57 20.80 2 -2 0 1269.87 21.80 2 -2 0 1263.77 20.00 -2 -2 0 1252.87 19.70 2 2 0 1231.28 21.40 2 2 0 1276.77 21.50 -2 2 0 1269.17 20.00 2 2 0 1254.27 19.80 -2 2 0 1244.38 20.80 -2 2 0 1254.47 22.00 3 -2 0 36.80 1.40 3 -2 0 39.10 2.10 -3 -2 0 37.70 1.80 3 -2 0 37.80 2.20 -3 -2 0 37.90 2.00 -3 2 0 39.40 2.00 3 2 0 39.40 2.10 3 2 0 37.10 2.10 -3 2 0 39.20 1.40 3 2 0 38.00 1.20 4 -2 0 840.62 15.90 4 -2 0 850.11 14.20 -4 -2 0 845.12 16.00 -4 -2 0 833.92 15.20 4 -2 0 833.62 16.50 -4 2 0 847.72 14.30 4 2 0 824.12 16.10 -4 2 0 833.62 16.00 4 2 0 832.42 16.20 5 -2 0 20.60 2.40 -5 -2 0 18.00 1.70 -5 -2 0 21.90 2.30 5 -2 0 18.70 2.00 5 2 0 25.50 2.50 -5 2 0 19.60 2.10 5 2 0 19.10 2.20 -5 2 0 21.10 1.10 6 -2 0 548.85 13.10 6 -2 0 539.35 12.30 -6 -2 0 541.75 11.40 -6 -2 0 550.04 12.90 -6 2 0 526.65 12.70 6 2 0 550.94 12.80 6 2 0 553.64 12.80 -6 2 0 547.55 9.90 -7 -2 0 24.20 2.90 -7 -2 0 21.50 2.30 7 -2 0 15.90 2.40 7 -2 0 21.60 2.60 7 2 0 13.10 2.20 -7 2 0 20.80 1.40 7 2 0 23.10 2.90 -7 2 0 16.30 2.40 -8 -2 0 660.23 16.20 8 -2 0 683.03 15.60 8 -2 0 651.73 16.40 -8 -2 0 663.63 14.20 -8 2 0 655.03 16.20 8 2 0 627.14 15.70 8 2 0 656.63 16.00 -8 2 0 661.43 12.40 -9 -2 0 2.50 1.20 9 -2 0 0.40 1.20 9 -2 0 0.00 1.10 -9 -2 0 3.20 1.60 -9 2 0 1.40 0.70 9 2 0 0.80 1.30 -9 2 0 4.10 1.80 9 2 0 0.60 1.20 -10 -2 0 36.90 3.50 10 -2 0 31.90 4.20 10 -2 0 40.20 4.20 -10 -2 0 39.20 4.50 10 2 0 35.40 4.30 -10 2 0 38.60 4.70 10 2 0 35.90 4.30 -11 -2 0 6.40 1.70 11 -2 0 14.20 2.90 -11 -2 0 9.60 2.80 11 -2 0 5.30 2.10 -11 2 0 9.60 2.60 11 2 0 5.20 2.30 11 2 0 13.40 3.00 12 -2 0 44.10 5.50 -12 -2 0 40.90 5.40 12 -2 0 53.99 5.80 -12 2 0 54.59 6.30 12 2 0 58.09 6.30 12 2 0 51.59 5.80 0 -3 0 -0.30 0.30 0 -3 0 0.10 0.60 0 3 0 0.70 0.50 0 3 0 -0.10 0.60 -1 -3 0 36.60 1.20 -1 -3 0 36.90 1.70 1 -3 0 34.20 1.20 1 -3 0 35.10 2.00 -1 -3 0 40.00 1.70 1 -3 0 37.90 1.50 -1 3 0 34.70 2.00 1 3 0 34.90 1.50 1 3 0 34.00 2.00 1 3 0 37.50 2.00 -1 3 0 36.50 1.20 1 3 0 34.70 1.20 -2 -3 0 2413.76 38.30 2 -3 0 2436.06 40.50 -2 -3 0 2479.55 39.60 -2 -3 0 2406.76 40.30 2 -3 0 2498.75 39.20 -2 3 0 2473.85 38.80 2 3 0 2440.06 40.20 2 3 0 2467.85 40.30 -2 3 0 2485.25 40.70 -2 3 0 2425.86 39.70 2 3 0 2432.46 39.00 -3 -3 0 3.50 0.80 3 -3 0 3.20 0.90 -3 -3 0 3.00 0.80 3 -3 0 2.40 0.50 3 3 0 2.70 0.90 3 3 0 3.60 0.50 -3 3 0 3.10 0.60 -3 3 0 2.80 0.70 3 3 0 2.70 0.80 -4 -3 0 85.29 3.40 -4 -3 0 82.79 3.20 4 -3 0 87.29 2.40 4 -3 0 84.29 3.90 4 -3 0 89.89 3.60 -4 3 0 89.29 3.50 -4 3 0 83.99 2.40 4 3 0 86.19 3.80 4 3 0 87.39 2.20 4 3 0 84.39 3.70 -5 -3 0 22.50 2.30 5 -3 0 28.70 3.00 -5 -3 0 23.10 2.20 5 -3 0 24.80 2.40 5 -3 0 25.20 1.30 -5 3 0 27.90 2.70 5 3 0 23.40 1.20 5 3 0 25.40 2.60 5 3 0 23.60 2.50 -6 -3 0 377.76 9.80 6 -3 0 357.46 10.30 -6 -3 0 358.46 8.90 6 -3 0 357.96 9.50 6 3 0 362.06 10.00 -6 3 0 361.26 6.80 6 3 0 370.56 7.00 -6 3 0 360.26 9.70 6 3 0 368.66 10.00 7 -3 0 9.40 1.80 -7 -3 0 12.40 2.20 7 -3 0 10.30 2.10 -7 -3 0 12.10 1.90 -7 3 0 12.20 2.10 7 3 0 10.70 2.20 7 3 0 11.00 1.10 -7 3 0 13.50 1.20 7 3 0 15.90 2.60 8 -3 0 672.73 15.70 8 -3 0 666.23 17.00 -8 -3 0 682.23 16.50 -8 -3 0 661.33 14.80 8 3 0 661.73 16.40 -8 3 0 675.43 16.50 8 3 0 666.23 16.50 -8 3 0 671.93 12.20 8 3 0 662.93 12.20 9 -3 0 9.90 2.10 -9 -3 0 14.80 2.20 9 -3 0 13.30 2.60 -9 -3 0 9.80 2.30 9 3 0 9.90 2.30 -9 3 0 10.00 2.30 9 3 0 7.90 2.20 -10 -3 0 21.10 2.80 -10 -3 0 27.10 3.90 10 -3 0 19.50 3.10 10 -3 0 20.30 3.50 -10 3 0 20.20 3.30 10 3 0 27.90 3.90 10 3 0 22.60 3.70 -11 -3 0 1.20 1.60 11 -3 0 1.60 1.80 11 -3 0 0.30 1.60 -11 -3 0 0.20 1.10 11 3 0 0.90 1.70 -11 3 0 0.70 1.70 11 3 0 3.60 2.20 12 -3 0 29.20 4.60 12 -3 0 34.50 4.50 -12 -3 0 34.10 5.10 -12 -3 0 28.60 3.70 12 3 0 27.30 4.60 12 3 0 28.80 4.50 -12 3 0 21.90 4.00 0 -4 0 555.14 10.50 0 -4 0 535.35 11.40 0 4 0 546.95 10.50 0 4 0 563.44 11.80 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66.69 2.60 1 5 0 62.29 3.40 1 5 0 65.19 3.50 -1 5 0 67.79 1.60 -1 5 0 69.09 3.60 1 5 0 63.89 1.60 2 -5 0 2092.69 34.40 -2 -5 0 2148.09 35.40 2 -5 0 2051.39 36.70 -2 -5 0 2091.69 33.50 2 5 0 2092.99 36.40 -2 5 0 2076.79 34.10 2 5 0 2132.69 36.70 2 5 0 2049.70 34.00 -2 5 0 2128.59 37.00 3 -5 0 5.40 1.50 -3 -5 0 3.60 1.00 -3 -5 0 4.60 0.80 3 -5 0 2.60 0.70 -3 5 0 4.80 1.60 3 5 0 3.50 1.30 3 5 0 4.10 1.30 3 5 0 3.20 0.70 -3 5 0 3.40 0.80 -4 -5 0 230.58 6.20 4 -5 0 238.28 7.90 -4 -5 0 232.38 6.80 4 -5 0 234.68 5.40 4 5 0 247.68 7.60 4 5 0 232.38 5.00 -4 5 0 230.78 6.20 -4 5 0 227.78 8.00 4 5 0 226.38 7.50 -5 -5 0 23.70 2.50 -5 -5 0 29.50 2.70 5 -5 0 23.30 3.00 5 -5 0 27.40 2.90 5 -5 0 23.20 1.40 5 5 0 22.00 2.70 5 5 0 25.00 3.00 5 5 0 24.10 1.20 -5 5 0 21.10 2.20 -6 -5 0 221.28 7.10 6 -5 0 210.88 4.70 6 -5 0 221.08 8.30 6 -5 0 212.68 7.40 -6 -5 0 220.78 7.10 -6 5 0 205.78 6.90 6 5 0 211.98 4.50 6 5 0 211.38 7.80 6 5 0 219.48 8.00 7 -5 0 52.79 4.30 -7 -5 0 50.99 3.60 7 -5 0 45.70 4.60 -7 -5 0 52.59 3.40 7 5 0 47.10 1.80 7 5 0 52.09 4.60 -7 5 0 49.80 4.20 -7 5 0 47.70 1.50 7 5 0 47.70 4.60 -8 -5 0 30.30 3.40 8 -5 0 37.90 4.40 8 -5 0 25.30 3.20 -8 -5 0 37.30 4.10 -8 5 0 24.60 3.20 8 5 0 25.50 3.70 8 5 0 27.80 3.70 -9 -5 0 -0.10 1.20 9 -5 0 1.50 1.50 9 -5 0 -1.10 1.10 -9 -5 0 -0.10 1.00 -9 5 0 1.10 1.40 9 5 0 0.40 1.30 9 5 0 -0.40 1.30 10 -5 0 50.39 5.00 10 -5 0 48.40 5.50 -10 -5 0 50.39 5.50 -10 -5 0 40.60 4.30 10 5 0 51.99 5.50 -10 5 0 38.20 4.60 10 5 0 52.99 5.80 -11 -5 0 1.40 1.50 11 -5 0 2.90 2.00 -11 -5 0 4.10 2.00 11 -5 0 6.50 2.50 11 5 0 4.50 2.40 -11 5 0 5.60 2.30 11 5 0 3.60 2.30 12 -5 0 44.10 5.90 -12 -5 0 45.40 5.10 12 -5 0 50.39 5.40 -12 -5 0 46.60 5.80 -12 5 0 42.30 5.60 12 5 0 34.00 5.10 12 5 0 45.50 6.10 0 -6 0 2598.84 42.70 0 -6 0 2534.15 44.30 0 6 0 2570.24 44.60 1 -6 0 4.40 1.00 -1 -6 0 6.00 1.40 -1 -6 0 6.80 1.30 1 -6 0 5.80 1.40 -1 6 0 5.70 1.50 1 6 0 7.10 1.80 1 6 0 5.00 1.00 -2 -6 0 810.42 13.90 -2 -6 0 807.02 16.20 2 -6 0 799.82 15.30 2 -6 0 807.72 17.50 -2 6 0 807.42 17.70 2 6 0 791.12 17.40 -2 6 0 809.42 13.80 2 6 0 808.72 14.90 2 6 0 829.32 17.60 3 -6 0 29.10 1.90 -3 -6 0 32.90 2.80 -3 -6 0 32.30 1.80 3 -6 0 30.00 3.20 3 6 0 34.60 1.80 -3 6 0 39.60 3.90 3 6 0 39.80 3.70 3 6 0 38.40 3.70 -3 6 0 32.90 1.80 4 -6 0 94.89 3.30 4 -6 0 100.39 5.20 -4 -6 0 99.19 3.70 -4 -6 0 102.69 4.40 -4 6 0 97.49 3.70 4 6 0 105.69 5.20 -4 6 0 107.29 5.50 4 6 0 104.09 3.10 4 6 0 103.69 5.00 5 -6 0 11.50 2.10 -5 -6 0 9.20 1.80 5 -6 0 14.00 1.40 -5 -6 0 12.40 1.80 5 -6 0 11.50 2.30 5 6 0 12.00 2.30 5 6 0 14.10 1.20 5 6 0 12.60 2.30 -5 6 0 12.80 1.80 -6 -6 0 104.09 4.90 6 -6 0 100.39 2.90 6 -6 0 99.99 5.10 6 -6 0 101.79 5.70 -6 -6 0 96.69 4.50 6 6 0 97.89 5.60 6 6 0 88.09 5.10 -6 6 0 97.19 4.50 6 6 0 96.89 2.60 -7 -6 0 17.00 2.60 7 -6 0 18.10 2.90 -7 -6 0 18.40 2.70 7 -6 0 13.20 2.80 -7 6 0 14.70 2.40 7 6 0 15.20 2.90 7 6 0 12.70 2.50 8 -6 0 27.80 3.50 8 -6 0 23.40 3.80 -8 -6 0 28.70 3.50 -8 -6 0 26.40 3.30 8 6 0 39.00 4.70 8 6 0 25.20 3.80 -8 6 0 24.00 3.20 9 -6 0 21.60 3.30 9 -6 0 19.10 3.60 -9 -6 0 14.70 2.70 -9 -6 0 12.10 2.60 -9 6 0 14.80 2.90 9 6 0 17.00 3.50 9 6 0 17.90 3.30 10 -6 0 12.70 2.70 -10 -6 0 18.60 3.20 10 -6 0 16.40 3.70 -10 -6 0 18.20 3.40 10 6 0 21.70 4.00 10 6 0 18.60 3.50 -10 6 0 15.20 3.10 11 -6 0 10.80 3.30 11 -6 0 3.40 2.00 -11 -6 0 5.40 2.30 -11 -6 0 8.60 2.50 -11 6 0 8.20 2.60 11 6 0 9.40 2.90 11 6 0 10.00 3.00 12 -6 0 37.80 5.50 0 -7 0 1.50 1.00 0 -7 0 0.80 0.70 0 7 0 0.90 1.20 -1 -7 0 46.90 3.40 1 -7 0 48.40 3.50 -1 -7 0 45.40 2.90 1 -7 0 42.40 2.60 -1 7 0 41.50 3.80 1 7 0 43.60 3.90 -2 -7 0 280.37 5.60 2 -7 0 289.47 9.20 2 -7 0 278.27 5.70 -2 -7 0 284.67 8.10 2 -7 0 272.67 7.30 -2 7 0 271.57 9.10 2 7 0 277.37 6.90 2 7 0 281.97 5.80 2 7 0 276.47 9.00 -2 7 0 276.07 5.60 2 7 0 294.57 9.30 -3 -7 0 67.79 2.60 3 -7 0 66.49 3.10 -3 -7 0 72.19 3.80 3 -7 0 66.89 4.30 3 7 0 74.49 4.50 3 7 0 64.19 2.80 3 7 0 67.19 4.30 -3 7 0 61.49 4.30 -3 7 0 66.79 2.60 4 -7 0 63.69 2.90 4 -7 0 72.99 4.70 -4 -7 0 71.09 3.90 -4 -7 0 65.29 2.90 -4 7 0 69.79 3.10 -4 7 0 52.79 4.80 4 7 0 66.09 2.60 4 7 0 62.89 4.30 4 7 0 61.39 4.20 5 -7 0 5.00 1.80 -5 -7 0 6.20 1.40 5 -7 0 7.00 1.10 -5 -7 0 10.10 1.90 5 7 0 4.70 1.80 5 7 0 7.80 2.00 -5 7 0 6.20 1.30 5 7 0 6.50 1.00 -5 7 0 4.30 1.90 6 -7 0 74.99 6.20 6 -7 0 58.79 2.40 -6 -7 0 64.79 3.70 -6 -7 0 66.89 4.20 6 -7 0 69.99 4.60 6 7 0 68.59 3.10 -6 7 0 67.49 3.80 6 7 0 69.29 4.70 6 7 0 74.59 5.10 -7 -7 0 1.80 1.40 7 -7 0 5.10 1.90 7 -7 0 5.40 1.80 -7 -7 0 1.60 1.20 7 7 0 6.70 2.10 -7 7 0 3.00 1.30 7 7 0 4.10 2.00 8 -7 0 130.99 6.50 8 -7 0 123.89 7.30 -8 -7 0 127.09 6.20 -8 -7 0 121.69 6.20 -8 7 0 137.59 6.40 8 7 0 149.59 7.80 8 7 0 125.89 7.00 9 -7 0 7.70 2.30 -9 -7 0 12.40 2.60 -9 -7 0 5.60 2.10 9 -7 0 10.70 3.10 9 7 0 8.50 2.60 -9 7 0 8.60 2.40 9 7 0 12.20 3.00 10 -7 0 33.90 4.90 -10 -7 0 40.10 4.90 10 -7 0 35.20 4.50 -10 -7 0 42.60 4.80 10 7 0 32.90 4.90 10 7 0 35.40 4.80 -10 7 0 37.70 4.70 11 -7 0 8.40 2.90 11 -7 0 3.00 2.00 -11 -7 0 3.60 2.30 -11 -7 0 3.90 2.30 11 7 0 2.20 2.30 -11 7 0 1.40 1.90 11 7 0 5.10 2.70 0 -8 0 41.70 2.80 0 -8 0 35.90 3.80 0 8 0 39.50 4.20 1 -8 0 53.69 4.70 -1 -8 0 53.49 3.40 -1 -8 0 64.49 4.20 1 -8 0 52.99 3.20 1 8 0 52.09 4.80 -1 8 0 60.79 5.30 2 -8 0 356.96 11.10 -2 -8 0 360.86 6.50 -2 -8 0 366.96 10.00 2 -8 0 363.76 9.30 -2 8 0 348.17 6.60 -2 8 0 369.76 11.50 2 8 0 373.86 11.40 3 -8 0 21.20 3.10 3 -8 0 17.20 2.10 -3 -8 0 20.20 1.70 -3 -8 0 16.30 2.40 -3 8 0 19.00 1.60 3 8 0 19.60 2.90 3 8 0 23.50 3.20 -3 8 0 19.50 3.10 -4 -8 0 50.19 2.50 4 -8 0 58.39 5.40 4 -8 0 50.69 2.80 -4 -8 0 46.20 4.00 4 8 0 46.10 4.50 -4 8 0 42.90 4.60 -4 8 0 47.80 2.50 4 8 0 45.70 4.70 -5 -8 0 6.80 1.40 5 -8 0 4.80 2.00 -5 -8 0 6.80 1.80 5 -8 0 7.10 1.20 5 8 0 5.30 1.80 -5 8 0 8.30 2.40 5 8 0 8.20 2.30 -5 8 0 5.10 1.20 -6 -8 0 261.87 8.00 -6 -8 0 261.67 9.20 6 -8 0 272.37 9.70 6 -8 0 268.07 10.50 6 8 0 272.37 10.40 -6 8 0 268.37 8.10 6 8 0 267.07 10.10 -7 -8 0 2.30 1.50 7 -8 0 3.80 2.00 7 -8 0 4.30 1.80 -7 -8 0 3.60 1.50 -7 8 0 2.80 1.40 7 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4 -9 0 10.10 2.50 -4 9 0 9.40 1.30 4 9 0 9.20 2.50 4 9 0 9.90 2.50 -4 9 0 8.70 2.50 5 -9 0 52.19 2.90 5 -9 0 46.80 5.20 -5 -9 0 48.50 2.90 -5 -9 0 54.79 4.80 5 9 0 57.19 5.70 -5 9 0 47.10 5.50 5 9 0 43.60 4.80 -5 9 0 45.60 2.80 6 -9 0 10.90 2.70 -6 -9 0 13.00 2.00 -6 -9 0 9.30 2.30 6 -9 0 11.30 2.80 6 9 0 11.00 2.70 6 9 0 5.00 2.20 -6 9 0 11.70 1.90 -7 -9 0 0.70 1.30 7 -9 0 0.80 1.50 -7 -9 0 0.80 1.10 7 -9 0 1.80 1.60 7 9 0 -0.60 1.40 -7 9 0 2.10 1.30 7 9 0 -1.10 1.10 8 -9 0 18.00 3.30 -8 -9 0 23.30 3.20 8 -9 0 23.20 4.10 -8 -9 0 25.80 3.80 8 9 0 22.10 3.90 -8 9 0 22.90 3.30 8 9 0 21.80 4.20 9 -9 0 0.80 1.80 -9 -9 0 4.10 2.00 -9 -9 0 3.70 1.80 9 -9 0 1.40 1.80 -9 9 0 1.10 1.60 9 9 0 2.10 2.10 9 9 0 2.90 2.20 -10 -9 0 9.40 3.00 -10 -9 0 13.30 2.90 10 -9 0 13.40 3.80 10 -9 0 11.10 3.00 10 9 0 15.10 3.80 10 9 0 12.70 3.80 -10 9 0 14.70 3.20 0 -10 0 63.09 4.00 0 -10 0 52.99 5.30 0 10 0 56.39 5.60 -1 -10 0 37.50 3.80 -1 -10 0 30.90 4.00 1 -10 0 33.90 4.20 1 -10 0 35.60 3.50 1 10 0 37.40 4.60 -1 10 0 39.20 4.70 -2 -10 0 24.20 3.60 2 -10 0 32.70 4.20 -2 -10 0 20.70 3.00 2 -10 0 26.40 3.10 2 10 0 27.00 4.00 -2 10 0 23.40 3.90 -3 -10 0 17.30 3.10 -3 -10 0 16.60 2.80 3 -10 0 18.90 2.50 3 -10 0 19.70 3.40 -3 10 0 19.10 3.60 3 10 0 15.30 3.10 -4 -10 0 18.60 3.30 4 -10 0 11.70 2.80 4 -10 0 14.90 2.20 -4 10 0 13.10 3.20 4 10 0 13.90 3.30 4 10 0 14.20 3.20 5 -10 0 45.70 5.40 -5 -10 0 42.90 4.70 5 10 0 53.99 5.90 5 10 0 32.30 4.30 -5 10 0 44.40 5.60 -6 -10 0 98.29 6.00 6 -10 0 93.79 6.60 6 10 0 91.59 6.40 6 10 0 84.69 7.60 7 -10 0 2.60 2.00 -7 -10 0 2.30 1.70 7 -10 0 3.60 2.00 7 10 0 1.60 1.90 7 10 0 0.70 1.70 8 -10 0 24.70 4.70 -8 -10 0 24.10 4.10 8 -10 0 24.60 3.90 8 10 0 21.20 3.90 8 10 0 25.50 4.80 9 -10 0 10.00 3.00 9 -10 0 13.80 3.50 -9 -10 0 9.30 2.80 9 10 0 10.70 3.60 9 10 0 15.50 3.70 0 -11 0 0.70 1.30 0 -11 0 -0.10 1.00 0 11 0 0.20 1.40 1 -11 0 12.10 2.40 -1 -11 0 7.50 2.30 -1 -11 0 15.60 2.80 1 -11 0 11.10 2.80 -1 11 0 13.00 3.20 1 11 0 7.90 2.60 2 -11 0 201.58 9.40 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4.20 2.00 10 -8 -3 3.20 2.20 -10 -8 3 2.60 1.80 -10 8 3 -0.70 1.40 10 8 -3 -0.50 1.40 10 8 -3 -0.10 2.10 9 -8 -3 9.10 2.60 -9 -8 3 9.50 2.40 -9 -8 3 8.80 2.70 9 -8 -3 7.50 2.50 9 8 -3 6.80 2.70 -9 8 3 11.70 2.70 9 8 -3 9.70 2.60 -8 -8 3 13.00 2.70 -8 -8 3 18.70 3.20 8 -8 -3 13.70 3.20 8 -8 -3 13.30 3.10 8 8 -3 11.00 2.60 -8 8 3 8.10 2.20 8 8 -3 17.30 3.50 7 -8 -3 149.29 7.60 -7 -8 3 155.38 7.30 7 -8 -3 160.58 8.00 -7 -8 3 161.08 6.80 7 8 -3 153.68 5.30 -7 8 3 155.48 6.60 7 8 -3 162.38 8.20 7 8 -3 148.69 7.00 6 -8 -3 60.59 5.50 -6 -8 3 59.89 3.80 6 -8 -3 75.59 6.40 -6 -8 3 63.89 5.30 -6 8 3 56.39 3.70 6 8 -3 63.69 5.70 6 8 -3 68.49 3.50 6 8 -3 54.89 4.90 5 -8 -3 108.39 4.50 -5 -8 3 129.29 6.30 5 -8 -3 119.59 6.40 -5 -8 3 130.29 5.20 5 8 -3 125.39 6.10 5 8 -3 116.29 4.70 -5 8 3 130.49 7.60 5 8 -3 127.79 6.70 -5 8 3 130.79 5.10 -4 -8 3 72.19 4.30 4 -8 -3 69.39 2.90 -4 -8 3 82.39 3.70 4 -8 -3 80.89 5.20 -4 -8 3 78.39 4.70 4 8 -3 67.59 4.70 4 8 -3 73.39 3.80 -4 8 3 69.89 3.40 -4 8 3 72.99 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17.70 3.80 9 8 3 36.60 5.30 -9 8 -3 32.30 4.30 9 8 3 42.30 5.70 -10 -8 -3 0.20 1.70 -10 -8 -3 0.80 1.70 10 -8 3 2.60 2.40 -10 8 -3 1.00 1.60 10 8 3 2.20 2.60 10 8 3 1.60 2.20 10 -9 -3 1.00 2.00 -10 -9 3 -0.30 2.00 10 -9 -3 -0.40 1.50 -10 -9 3 -0.80 1.50 -10 9 3 2.50 2.00 10 9 -3 0.70 1.80 10 9 -3 3.30 2.60 9 -9 -3 29.20 4.60 -9 -9 3 32.70 4.50 -9 -9 3 29.20 4.10 9 -9 -3 34.50 4.90 9 9 -3 39.00 4.80 -9 9 3 29.40 4.10 8 -9 -3 2.20 2.00 -8 -9 3 3.20 1.50 8 -9 -3 2.80 1.90 -8 -9 3 1.00 1.50 -8 9 3 3.10 1.80 8 9 -3 1.30 1.80 8 9 -3 -0.30 1.40 -7 -9 3 108.49 6.50 7 -9 -3 111.09 7.00 7 -9 -3 131.09 7.30 -7 -9 3 117.39 5.70 7 9 -3 119.99 6.70 7 9 -3 124.69 7.40 -7 9 3 115.29 5.70 6 -9 -3 47.20 5.30 -6 -9 3 40.20 3.80 -6 -9 3 44.30 4.90 6 9 -3 44.60 4.80 6 9 -3 40.70 3.30 6 9 -3 29.60 4.30 -6 9 3 40.90 3.70 -5 -9 3 3.60 1.30 5 -9 -3 4.10 2.00 -5 -9 3 3.50 1.60 5 9 -3 3.30 1.30 5 9 -3 4.90 2.00 -5 9 3 5.10 1.50 -5 9 3 3.60 2.30 -4 -9 3 1.20 1.20 -4 -9 3 2.50 1.00 4 -9 -3 0.40 1.30 -4 -9 3 1.30 1.20 4 -9 -3 2.90 1.00 4 9 -3 3.40 1.20 -4 9 3 2.20 1.70 -4 9 3 1.80 1.00 4 9 -3 -0.10 1.20 3 -9 -3 126.99 6.70 -3 -9 3 132.89 6.40 3 -9 -3 117.29 4.50 -3 -9 3 122.49 6.10 -3 -9 3 118.09 4.20 3 9 -3 124.49 5.30 3 9 -3 119.99 6.50 -3 9 3 121.49 4.00 -3 9 3 133.19 7.50 -2 -9 3 65.39 2.50 -2 -9 3 68.39 4.50 2 -9 -3 69.19 6.00 -2 -9 3 72.29 4.60 2 -9 -3 65.89 3.40 -2 9 3 65.89 6.00 2 9 -3 71.19 4.90 2 9 -3 59.89 3.80 1 -9 -3 58.89 3.30 -1 -9 3 59.69 4.30 -1 -9 3 62.89 5.20 1 -9 -3 61.99 5.50 1 9 -3 54.59 5.00 1 9 -3 58.69 3.80 -1 9 3 62.79 5.70 0 -9 -3 11.30 1.90 0 -9 -3 9.10 2.30 0 -9 3 14.00 2.50 0 -9 3 10.80 2.30 0 9 3 8.70 2.40 0 9 -3 9.20 2.00 0 9 -3 9.70 2.30 1 -9 3 388.96 11.20 1 -9 3 385.36 11.90 -1 -9 -3 378.96 10.10 -1 9 -3 390.56 12.00 -1 9 -3 369.86 6.90 1 9 3 382.96 12.70 -1 9 -3 379.06 10.90 2 -9 3 12.90 2.60 -2 -9 -3 15.30 1.30 2 -9 3 14.40 2.40 -2 -9 -3 13.90 2.30 2 9 3 14.20 2.90 -2 9 -3 14.20 2.40 2 9 3 7.70 2.20 -2 9 -3 13.00 1.30 -2 9 -3 18.70 3.10 3 -9 3 351.06 10.20 3 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6 -13 -3 3.50 2.60 -6 -13 3 1.00 2.00 -6 13 3 1.80 2.90 6 13 -3 5.70 3.10 5 -13 -3 109.99 9.40 -5 -13 3 96.19 8.30 -5 -13 3 106.29 7.20 5 13 -3 122.59 10.20 -5 13 3 129.39 11.30 -4 -13 3 0.40 1.60 4 -13 -3 -0.20 1.70 -4 -13 3 0.20 1.40 4 13 -3 -0.60 2.10 -4 13 3 -1.80 1.90 -3 -13 3 14.00 3.20 3 -13 -3 14.80 3.70 -3 -13 3 20.80 4.00 3 13 -3 17.30 4.10 -3 13 3 11.90 3.60 -2 -13 3 0.10 1.70 2 -13 -3 -0.30 1.70 -2 -13 3 0.50 1.60 2 -13 -3 -1.40 1.00 -2 13 3 -2.00 1.50 2 13 -3 -1.70 1.70 -1 -13 3 0.20 1.70 -1 -13 3 1.20 1.60 1 -13 -3 1.60 1.50 1 -13 -3 0.40 1.70 -1 13 3 -2.50 1.70 1 13 -3 1.40 2.00 0 -13 3 8.70 2.60 0 -13 -3 3.30 1.80 0 -13 -3 4.50 2.30 0 -13 3 3.40 2.30 0 13 3 4.20 2.60 0 13 -3 3.80 2.50 -1 -13 -3 75.89 7.50 1 -13 3 73.69 7.30 -1 -13 -3 78.79 5.40 1 -13 3 82.69 7.00 1 13 3 90.69 8.90 -1 13 -3 94.79 8.40 -2 -13 -3 3.80 1.80 2 -13 3 5.30 2.30 -2 -13 -3 4.20 2.30 2 -13 3 2.00 1.80 2 13 3 0.60 2.00 -2 13 -3 6.30 2.80 -3 -13 -3 16.30 3.90 3 -13 3 11.90 3.40 -3 -13 -3 19.80 3.50 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10.20 2.70 11 -1 -4 12.30 2.60 11 -1 -4 11.60 2.80 11 1 -4 12.60 2.50 -11 1 4 10.10 2.90 11 1 -4 6.40 2.50 10 -1 -4 432.66 12.20 10 -1 -4 444.86 13.50 -10 -1 4 435.36 11.10 -10 -1 4 429.16 14.00 10 1 -4 413.36 13.40 10 1 -4 422.56 11.80 -10 1 4 440.26 14.10 9 -1 -4 33.20 3.90 -9 -1 4 39.60 3.30 9 -1 -4 36.40 3.60 -9 -1 4 27.80 3.70 -9 1 4 37.90 2.30 9 1 -4 37.00 3.40 -9 1 4 33.80 4.20 9 1 -4 36.30 4.20 -8 -1 4 26.70 2.60 8 -1 -4 35.50 3.80 -8 -1 4 32.60 3.80 8 -1 -4 28.40 3.00 -8 1 4 29.00 1.90 -8 1 4 27.40 3.60 8 1 -4 32.00 3.60 8 1 -4 31.00 2.90 -7 -1 4 22.10 2.20 7 -1 -4 25.60 2.90 -7 -1 4 25.90 3.20 7 -1 -4 24.60 2.50 7 1 -4 22.30 2.30 -7 1 4 26.70 3.20 -7 1 4 24.40 1.90 7 1 -4 26.20 3.00 -6 -1 4 165.68 6.30 -6 -1 4 169.28 5.20 6 -1 -4 166.78 6.10 6 -1 -4 163.98 5.20 -6 1 4 154.78 6.10 6 1 -4 173.58 6.20 6 1 -4 165.78 4.80 -6 1 4 159.58 4.30 -5 -1 4 0.20 0.80 -5 -1 4 0.40 0.60 5 -1 -4 0.80 0.60 5 -1 -4 1.00 0.80 -5 1 4 0.50 0.50 5 1 -4 1.00 0.80 5 1 -4 0.90 0.50 -5 1 4 1.80 1.00 -4 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4.20 12 -2 -4 44.90 5.40 12 2 -4 40.80 5.20 -12 2 4 33.70 5.00 12 2 -4 35.90 5.00 -11 -2 4 1.20 1.60 11 -2 -4 -0.70 1.20 -11 -2 4 0.30 1.30 11 -2 -4 -0.10 1.70 11 2 -4 -1.10 1.00 -11 2 4 0.40 1.80 11 2 -4 1.20 1.20 11 2 -4 0.10 1.70 -10 -2 4 362.06 10.50 10 -2 -4 379.76 12.40 10 -2 -4 386.36 11.50 -10 -2 4 402.56 13.30 10 2 -4 370.56 10.90 -10 2 4 384.06 13.00 10 2 -4 345.77 12.30 -9 -2 4 132.29 5.60 9 -2 -4 128.29 6.00 -9 -2 4 133.59 6.90 9 -2 -4 138.19 6.70 9 2 -4 135.49 5.60 -9 2 4 148.99 7.20 9 2 -4 141.09 7.00 -8 -2 4 74.69 3.90 -8 -2 4 65.79 4.50 8 -2 -4 79.99 4.30 8 -2 -4 77.19 4.70 -8 2 4 70.09 4.70 -8 2 4 74.29 2.40 8 2 -4 78.59 4.80 8 2 -4 82.79 4.00 7 -2 -4 5.00 1.40 -7 -2 4 7.30 1.50 -7 -2 4 4.50 1.50 7 -2 -4 6.60 1.70 -7 2 4 7.90 1.90 7 2 -4 5.30 1.20 -7 2 4 4.60 0.70 -7 2 4 4.60 0.70 7 2 -4 3.30 1.40 6 -2 -4 195.38 6.90 -6 -2 4 206.48 7.20 6 -2 -4 199.28 6.20 -6 -2 4 207.98 6.30 -6 2 4 206.88 7.20 -6 2 4 202.28 4.20 6 2 -4 210.88 5.70 6 2 -4 205.48 5.80 6 2 -4 202.78 7.00 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4 12.30 1.90 -5 -2 -4 6.70 1.60 5 -2 4 10.10 2.00 5 2 4 9.00 1.60 5 2 4 12.40 0.90 5 2 4 11.10 2.20 -5 2 -4 8.90 1.90 6 -2 4 46.50 3.10 -6 -2 -4 48.70 3.50 6 -2 4 49.30 2.70 -6 -2 -4 52.39 3.00 6 -2 4 45.30 4.20 -6 2 -4 51.79 3.70 6 2 4 52.99 4.70 6 2 4 52.89 3.30 6 2 4 53.99 2.50 7 -2 4 1.20 1.20 7 -2 4 0.50 0.90 7 -2 4 1.50 1.10 -7 -2 -4 1.60 0.90 -7 -2 -4 0.80 1.30 -7 2 -4 2.40 1.30 7 2 4 -0.80 0.90 7 2 4 1.40 1.20 8 -2 4 308.77 9.30 -8 -2 -4 312.97 10.70 8 -2 4 311.57 11.20 8 -2 4 313.87 8.90 -8 -2 -4 317.77 9.00 8 2 4 317.47 11.30 -8 2 -4 307.37 10.60 8 2 4 307.17 9.60 9 -2 4 22.20 3.80 -9 -2 -4 29.10 3.10 -9 -2 -4 31.40 4.30 9 -2 4 22.30 2.90 9 2 4 27.00 3.50 9 2 4 21.90 3.60 -9 2 -4 24.80 3.70 -9 2 -4 27.30 2.60 -10 -2 -4 26.40 4.10 10 -2 4 29.50 3.60 -10 -2 -4 34.70 3.60 10 -2 4 31.20 4.70 -10 2 -4 25.10 3.80 -10 2 -4 27.90 2.90 10 2 4 31.70 4.70 10 2 4 29.90 3.90 -11 -2 -4 18.60 2.90 -11 -2 -4 26.50 4.50 11 -2 4 20.40 4.00 11 2 4 22.80 3.80 11 2 4 22.70 4.30 -11 2 -4 21.70 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4 43.80 2.90 6 -3 -4 32.70 3.20 6 3 -4 41.50 2.40 -6 3 4 41.10 3.70 6 3 -4 40.40 3.70 6 3 -4 40.70 2.40 -5 -3 4 2.90 1.00 -5 -3 4 4.00 1.20 5 -3 -4 5.00 1.40 5 -3 -4 6.00 1.30 5 3 -4 3.80 1.40 5 3 -4 3.90 0.90 5 3 -4 3.50 1.00 -5 3 4 3.30 1.20 4 -3 -4 93.29 4.20 4 -3 -4 85.39 3.70 -4 -3 4 97.89 4.20 4 -3 -4 89.89 2.10 -4 -3 4 94.89 4.00 4 3 -4 92.19 3.00 -4 3 4 88.19 4.00 4 3 -4 95.19 4.10 -4 3 4 89.79 2.00 4 3 -4 94.59 3.50 3 -3 -4 34.10 2.20 3 -3 -4 33.70 1.50 3 -3 -4 39.80 2.60 -3 -3 4 31.90 2.70 -3 -3 4 38.00 2.50 -3 3 4 29.40 2.50 3 3 -4 38.20 2.30 3 3 -4 33.80 2.10 -3 3 4 34.80 1.40 -2 -3 4 755.52 15.20 -2 -3 4 737.03 13.10 2 -3 -4 737.33 14.50 -2 -3 4 753.12 14.80 -2 3 4 749.53 14.80 2 3 -4 756.22 14.30 2 3 -4 750.82 14.20 -2 3 4 744.23 13.30 -2 3 4 756.22 15.80 -1 -3 4 146.29 4.80 -1 -3 4 137.89 3.80 -1 -3 4 141.89 4.70 -1 3 4 136.69 4.00 1 3 -4 147.69 4.40 -1 3 4 130.09 4.50 1 3 -4 131.39 3.90 -1 3 4 131.39 4.80 -1 3 4 139.29 4.70 0 -3 4 760.12 15.10 0 -3 4 761.42 15.20 0 -3 4 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3.70 2.40 11 4 -4 2.10 1.60 -11 4 4 0.60 1.60 -10 -4 4 121.89 7.00 -10 -4 4 127.69 6.30 10 -4 -4 120.19 6.70 10 -4 -4 112.49 6.30 -10 4 4 121.79 7.00 10 4 -4 112.39 5.50 10 4 -4 129.39 6.20 10 4 -4 104.39 6.60 9 -4 -4 35.20 4.10 -9 -4 4 20.30 3.30 -9 -4 4 32.40 3.70 9 -4 -4 29.80 3.80 9 4 -4 29.90 4.00 9 4 -4 29.10 2.70 9 4 -4 32.00 3.50 -9 4 4 26.60 3.80 -8 -4 4 93.09 5.30 8 -4 -4 97.19 5.30 8 -4 -4 97.59 5.60 -8 -4 4 97.89 5.00 8 4 -4 88.49 5.40 8 4 -4 93.69 4.00 -8 4 4 95.99 5.40 8 4 -4 96.79 4.60 7 -4 -4 3.50 1.50 -7 -4 4 4.40 1.50 7 -4 -4 3.40 1.40 -7 -4 4 2.30 1.40 7 4 -4 3.00 1.20 7 4 -4 2.50 1.00 7 4 -4 3.60 1.60 -7 4 4 1.20 1.30 6 -4 -4 137.19 5.80 -6 -4 4 149.99 5.90 6 -4 -4 154.78 6.40 -6 -4 4 156.78 6.20 -6 4 4 153.68 6.20 6 4 -4 153.98 5.00 6 4 -4 156.08 6.30 6 4 -4 152.78 5.20 -5 -4 4 5.20 1.40 5 -4 -4 2.80 1.20 5 -4 -4 2.90 1.30 -5 -4 4 4.60 1.40 -5 4 4 3.10 1.10 5 4 -4 6.00 1.50 5 4 -4 5.80 1.20 5 4 -4 6.30 1.20 -4 -4 4 693.53 14.80 4 -4 -4 676.83 11.40 -4 -4 4 718.43 15.20 4 -4 -4 707.33 15.60 4 -4 -4 698.43 11.20 4 -4 -4 711.43 15.00 4 4 -4 698.03 13.90 4 4 -4 703.73 15.10 4 4 -4 693.23 13.50 -4 4 4 704.83 14.80 -3 -4 4 128.69 4.60 3 -4 -4 126.29 4.80 3 -4 -4 130.79 2.90 -3 -4 4 125.49 4.90 -3 -4 4 120.39 3.80 -3 4 4 124.19 5.70 3 4 -4 130.09 4.80 -3 4 4 125.89 4.60 3 4 -4 132.59 4.40 -2 -4 4 1225.18 22.90 2 -4 -4 1214.78 20.10 -2 -4 4 1225.58 22.10 2 -4 -4 1204.08 22.50 -2 -4 4 1233.48 21.20 -2 4 4 1239.28 22.10 2 4 -4 1209.08 22.00 2 4 -4 1193.88 21.80 -2 4 4 1198.68 23.60 -1 -4 4 85.59 3.60 1 -4 -4 84.79 2.70 -1 -4 4 91.89 4.00 -1 -4 4 84.79 3.30 -1 4 4 83.19 4.10 1 4 -4 85.19 3.40 1 4 -4 83.49 3.50 -1 4 4 86.49 3.60 -1 4 4 90.99 4.00 0 -4 4 655.33 13.90 0 -4 4 668.43 13.70 0 -4 -4 673.43 12.40 0 -4 4 635.74 13.20 0 4 4 669.53 14.20 0 4 4 642.34 13.40 0 4 4 670.33 14.30 0 4 -4 679.73 13.60 0 4 -4 664.33 12.90 1 -4 4 52.29 2.90 -1 -4 -4 52.59 2.60 1 -4 4 49.10 2.80 -1 -4 -4 53.49 2.50 1 4 4 50.79 3.10 -1 4 -4 51.99 2.40 1 4 4 51.89 3.00 -1 4 -4 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40.60 3.40 8 -4 4 43.10 4.90 8 -4 4 46.90 3.90 8 4 4 49.60 4.70 8 4 4 49.70 5.40 -8 4 -4 39.40 4.30 9 -4 4 19.60 2.70 -9 -4 -4 26.10 3.30 9 -4 4 18.30 3.50 -9 -4 -4 19.80 3.40 -9 4 -4 19.20 3.40 9 4 4 21.60 3.90 9 4 4 19.80 3.30 -10 -4 -4 41.80 4.30 -10 -4 -4 39.50 5.00 10 -4 4 53.19 6.30 10 4 4 49.40 5.20 -10 4 -4 45.50 5.40 10 4 4 35.00 5.10 -11 -4 -4 1.00 1.60 -11 -4 -4 2.80 1.70 11 -4 4 4.40 2.30 -11 4 -4 3.80 2.10 11 4 4 0.90 2.20 11 4 4 1.40 2.00 12 -5 -4 89.49 7.60 -12 -5 4 92.29 6.10 -12 -5 4 79.69 7.70 12 -5 -4 76.59 7.10 12 5 -4 85.19 8.10 -12 5 4 82.69 7.80 11 -5 -4 18.50 3.50 -11 -5 4 17.50 3.20 11 -5 -4 22.10 3.80 -11 -5 4 12.00 3.10 -11 5 4 15.00 3.50 11 5 -4 19.10 4.00 -10 -5 4 62.89 5.60 10 -5 -4 62.89 5.70 10 -5 -4 63.49 6.00 -10 -5 4 66.89 6.20 10 5 -4 61.49 6.10 -10 5 4 63.09 6.00 10 5 -4 61.99 4.40 -9 -5 4 2.20 1.50 9 -5 -4 1.40 1.60 -9 -5 4 3.80 1.70 9 -5 -4 5.70 2.00 -9 5 4 4.80 1.90 9 5 -4 2.60 1.10 9 5 -4 5.00 1.70 9 5 -4 2.50 1.80 -8 -5 4 196.28 7.80 -8 -5 4 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13.40 3.20 10 8 4 9.40 3.50 -10 -9 4 9.40 2.90 10 -9 -4 8.70 2.80 -10 -9 4 3.30 2.10 10 -9 -4 7.90 2.80 10 9 -4 6.30 3.00 -10 9 4 11.80 3.10 9 -9 -4 6.70 2.40 -9 -9 4 0.30 1.50 -9 -9 4 3.70 1.90 9 -9 -4 4.10 2.20 -9 9 4 7.60 2.40 9 9 -4 3.10 2.10 9 9 -4 3.40 1.90 8 -9 -4 81.89 7.40 -8 -9 4 82.69 5.30 8 -9 -4 71.89 6.70 -8 -9 4 78.09 6.90 -8 9 4 70.19 5.00 8 9 -4 77.39 7.20 8 9 -4 88.49 5.70 7 -9 -4 24.10 4.00 -7 -9 4 17.30 3.20 7 -9 -4 16.50 3.30 -7 -9 4 17.20 2.90 -7 9 4 18.60 3.00 7 9 -4 22.70 2.60 7 9 -4 23.60 3.50 7 9 -4 21.10 3.90 6 -9 -4 3.00 1.80 -6 -9 4 3.70 1.90 6 -9 -4 5.50 2.20 -6 -9 4 2.00 1.40 -6 9 4 2.90 1.40 6 9 -4 2.50 1.30 6 9 -4 3.90 2.00 -5 -9 4 1.60 1.30 -5 -9 4 3.40 1.80 -5 -9 4 3.80 1.40 5 -9 -4 5.20 2.10 -5 9 4 3.00 2.10 5 9 -4 4.00 1.50 5 9 -4 2.00 1.90 -5 9 4 3.80 1.30 -4 -9 4 40.80 4.50 -4 -9 4 47.80 3.00 -4 -9 4 54.09 4.80 4 -9 -4 47.70 2.60 4 -9 -4 43.60 4.70 4 9 -4 49.80 4.00 -4 9 4 56.69 6.10 -4 9 4 51.49 3.10 4 9 -4 44.40 4.80 3 -9 -4 6.00 2.10 -3 -9 4 8.90 1.60 3 -9 -4 6.80 1.30 -3 -9 4 7.60 2.10 -3 -9 4 8.10 2.00 3 9 -4 7.30 2.20 3 9 -4 10.00 2.00 -3 9 4 8.50 1.50 -3 9 4 8.10 2.60 2 -9 -4 199.78 6.20 -2 -9 4 178.38 7.30 2 -9 -4 188.78 8.30 -2 -9 4 207.08 8.20 -2 -9 4 185.88 5.40 2 9 -4 194.28 8.30 -2 9 4 210.08 9.40 -2 9 4 193.78 5.10 2 9 -4 201.98 7.30 1 -9 -4 47.60 5.00 1 -9 -4 41.20 1.70 1 -9 -4 41.10 2.80 -1 -9 4 40.30 4.20 -1 -9 4 40.50 4.00 -1 9 4 39.40 4.70 1 9 -4 43.90 1.90 1 9 -4 36.90 4.10 1 9 -4 34.30 3.70 0 -9 4 0.30 1.10 0 -9 4 0.90 1.20 0 -9 -4 1.40 1.30 0 -9 -4 0.10 0.40 0 -9 -4 0.30 0.80 0 9 -4 0.00 1.00 0 9 -4 -0.20 0.40 0 9 4 0.70 1.70 0 9 -4 0.60 1.20 1 -9 4 9.20 2.10 -1 -9 -4 11.20 1.90 1 -9 4 9.90 2.20 -1 -9 -4 12.00 1.20 -1 9 -4 8.20 2.20 1 9 4 13.10 3.00 -1 9 -4 15.90 1.50 1 9 4 14.10 2.90 -1 9 -4 13.30 2.30 -2 -9 -4 24.80 1.70 2 -9 4 26.90 3.70 2 -9 4 22.10 3.10 -2 -9 -4 27.60 3.00 2 9 4 24.30 3.80 -2 9 -4 27.50 1.80 -2 9 -4 29.30 3.70 2 9 4 23.60 3.60 -2 9 -4 25.10 3.20 -3 -9 -4 35.80 3.60 -3 -9 -4 37.00 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23.70 4.70 8 10 4 27.50 4.90 9 -11 -4 22.70 4.40 -9 -11 4 34.30 5.20 9 -11 -4 24.80 4.70 9 11 -4 26.80 5.30 8 -11 -4 0.10 2.10 -8 -11 4 1.60 1.70 -8 -11 4 0.70 1.70 8 -11 -4 4.80 2.60 8 11 -4 0.50 2.00 -7 -11 4 -0.70 1.30 7 -11 -4 4.10 2.20 7 -11 -4 3.80 2.40 -7 -11 4 4.00 2.00 7 11 -4 9.80 3.40 6 -11 -4 14.00 3.60 -6 -11 4 12.30 3.00 -6 -11 4 9.70 2.60 -6 11 4 8.50 3.30 6 11 -4 9.00 3.00 5 -11 -4 42.70 5.40 -5 -11 4 43.50 5.00 -5 -11 4 37.50 4.90 -5 11 4 39.60 5.80 5 11 -4 41.80 3.90 5 11 -4 43.30 5.40 -4 -11 4 58.69 5.60 4 -11 -4 57.89 6.40 -4 -11 4 59.29 5.90 4 11 -4 64.19 6.50 -4 11 4 67.49 7.20 4 11 -4 51.59 4.50 3 -11 -4 6.20 2.30 3 -11 -4 6.70 1.60 -3 -11 4 5.90 2.20 -3 -11 4 4.50 2.10 3 11 -4 2.40 1.90 3 11 -4 5.20 1.70 -3 11 4 3.00 2.20 2 -11 -4 153.38 6.00 -2 -11 4 140.99 7.20 -2 -11 4 125.79 7.10 2 -11 -4 146.19 8.10 -2 11 4 133.19 8.30 2 11 -4 145.69 6.60 2 11 -4 144.19 7.90 -1 -11 4 3.40 1.90 1 -11 -4 2.80 1.80 -1 -11 4 2.40 1.70 1 -11 -4 2.90 1.40 1 11 -4 3.40 1.60 1 11 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8 -12 -4 3.90 2.70 8 12 -4 0.60 2.30 7 -12 -4 -1.40 1.90 -7 -12 4 1.20 1.80 -7 -12 4 2.10 1.80 7 -12 -4 0.70 2.10 7 12 -4 -0.30 2.10 -6 -12 4 28.80 4.40 6 -12 -4 9.70 3.20 -6 -12 4 19.30 3.80 -6 12 4 8.50 3.60 6 12 -4 19.50 4.20 -5 -12 4 20.40 3.90 5 -12 -4 17.60 3.70 -5 -12 4 16.60 3.30 -5 12 4 18.40 4.60 5 12 -4 27.00 3.40 5 12 -4 18.20 4.10 -4 -12 4 99.49 6.70 -4 -12 4 103.29 6.60 4 -12 -4 102.49 8.80 4 12 -4 105.39 5.60 4 12 -4 96.79 8.40 -4 12 4 94.69 8.80 -3 -12 4 23.90 3.90 3 -12 -4 25.20 4.30 3 -12 -4 29.20 3.60 -3 -12 4 23.90 4.10 3 12 -4 26.70 3.50 3 12 -4 23.50 4.20 -3 12 4 29.40 5.20 2 -12 -4 161.38 6.60 -2 -12 4 167.18 8.40 2 -12 -4 166.18 9.10 -2 -12 4 187.38 9.00 2 12 -4 155.58 8.80 2 12 -4 158.78 7.20 -2 12 4 155.68 9.40 1 -12 -4 2.80 2.10 -1 -12 4 0.90 1.50 -1 -12 4 5.00 2.30 1 -12 -4 4.70 1.60 1 12 -4 7.00 2.20 1 12 -4 6.80 2.70 -1 12 4 1.50 2.20 0 -12 -4 49.70 5.80 0 -12 4 55.99 5.80 0 -12 4 58.99 5.80 0 -12 -4 73.49 4.70 0 12 4 50.79 6.30 0 12 -4 62.39 6.30 0 12 -4 59.29 5.40 -1 -12 -4 17.60 2.90 1 -12 4 20.90 3.60 1 -12 4 22.50 3.90 -1 -12 -4 17.80 3.60 -1 12 -4 16.80 3.60 1 12 4 20.40 4.20 -2 -12 -4 5.50 2.50 2 -12 4 5.90 2.30 2 -12 4 -0.30 1.30 -2 -12 -4 8.80 2.40 2 12 4 1.20 2.10 -2 12 -4 6.30 2.70 3 -12 4 21.60 4.10 -3 -12 -4 21.40 3.40 3 -12 4 28.20 3.90 -3 12 -4 24.90 4.30 3 12 4 19.90 4.30 4 -12 4 41.80 4.50 -4 -12 -4 45.00 5.00 4 -12 4 44.30 5.80 -4 12 -4 37.70 5.30 4 12 4 44.10 6.00 4 12 4 42.50 6.00 5 -12 4 2.90 2.00 -5 -12 -4 5.60 2.20 -5 12 -4 3.70 2.50 5 12 4 3.90 2.40 5 12 4 6.10 3.10 6 -12 4 32.10 5.60 6 -12 4 40.00 5.00 -6 -12 -4 34.90 4.80 6 12 4 40.00 6.00 6 12 4 30.90 5.30 7 -12 4 23.30 4.90 -7 -12 -4 12.50 3.20 7 12 4 19.70 4.50 7 12 4 15.70 4.20 7 -13 -4 2.50 2.40 -7 -13 4 4.50 2.40 -7 -13 4 3.40 2.30 -6 -13 4 129.29 8.40 -6 -13 4 113.69 7.40 6 -13 -4 106.19 9.40 6 13 -4 121.29 10.40 -6 13 4 118.69 11.40 -5 -13 4 1.20 2.00 5 -13 -4 3.00 2.20 -5 -13 4 3.20 2.10 -5 13 4 2.70 3.10 5 13 -4 6.50 3.00 4 -13 -4 125.39 8.40 -4 -13 4 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75.39 3.70 5 2 -9 82.49 4.30 -5 2 9 88.59 5.60 5 2 -9 81.49 4.30 4 -2 -9 13.30 1.60 -4 -2 9 12.20 2.20 4 -2 -9 11.90 2.00 -4 -2 9 9.90 2.40 -4 2 9 11.80 1.90 4 2 -9 9.60 1.80 4 2 -9 14.30 2.00 -4 2 9 11.90 2.70 3 -2 -9 11.00 1.80 -3 -2 9 15.30 2.40 -3 -2 9 17.30 2.90 -3 2 9 17.50 2.30 -3 2 9 13.20 2.80 3 2 -9 14.90 2.10 3 2 -9 16.60 2.00 2 -2 -9 34.00 2.80 -2 -2 9 31.40 1.60 -2 -2 9 29.00 3.30 -2 -2 9 30.80 3.80 2 -2 -9 34.20 3.00 -2 2 9 32.60 3.20 2 2 -9 29.20 2.40 -2 2 9 30.40 3.80 -2 2 9 35.10 2.40 2 2 -9 42.30 3.60 1 -2 -9 90.39 3.70 1 -2 -9 96.69 4.10 -1 -2 9 95.49 5.00 -1 -2 9 93.89 3.40 -1 -2 9 87.79 5.60 1 2 -9 93.89 3.10 -1 2 9 89.79 5.50 -1 2 9 87.99 4.00 1 2 -9 94.99 4.50 -1 2 9 86.09 4.60 0 -2 -9 5.90 1.30 0 -2 9 6.90 1.80 0 -2 9 6.40 1.30 0 -2 9 4.80 1.90 0 2 -9 5.90 0.70 0 2 -9 5.50 1.50 0 2 9 8.20 2.30 0 2 9 6.60 1.50 0 2 9 4.90 1.60 0 2 -9 7.50 0.90 1 -2 9 49.40 3.10 -1 -2 -9 46.30 4.40 -1 -2 -9 36.50 2.50 1 -2 9 50.89 4.50 -1 2 -9 43.90 4.40 1 2 9 46.40 4.00 1 2 9 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-0.30 1.60 -9 -2 -9 7.90 2.80 -9 -2 -9 8.80 2.30 9 -2 9 11.70 3.00 9 -2 9 17.80 3.90 -9 2 -9 8.80 2.90 9 2 9 7.30 2.90 12 -3 -9 6.60 2.80 -12 -3 9 11.10 3.70 12 3 -9 10.50 3.00 -12 3 9 12.40 4.00 12 3 -9 11.90 2.70 -11 -3 9 13.30 3.50 11 -3 -9 10.10 3.10 -11 3 9 16.30 4.20 11 3 -9 9.60 3.00 11 3 -9 17.20 3.00 -10 -3 9 3.80 1.90 -10 -3 9 5.60 2.60 10 -3 -9 1.20 1.70 -10 3 9 0.80 1.80 10 3 -9 4.80 1.90 10 3 -9 2.00 2.00 -9 -3 9 5.90 2.10 9 -3 -9 6.40 2.10 -9 -3 9 2.40 1.90 -9 3 9 7.10 2.70 9 3 -9 9.60 2.20 9 3 -9 7.00 2.30 8 -3 -9 1.50 1.00 -8 -3 9 0.50 1.50 -8 -3 9 3.00 1.60 8 -3 -9 1.40 1.50 8 3 -9 1.80 1.60 -8 3 9 2.40 1.90 8 3 -9 2.50 1.30 -7 -3 9 48.30 5.20 7 -3 -9 44.10 4.50 7 -3 -9 46.00 2.90 -7 -3 9 50.19 4.60 -7 3 9 46.30 2.50 7 3 -9 46.10 4.50 -7 3 9 41.30 4.80 7 3 -9 55.29 4.60 6 -3 -9 93.49 4.00 -6 -3 9 101.19 5.40 -6 -3 9 96.19 6.10 6 -3 -9 91.69 5.30 6 3 -9 88.99 5.00 -6 3 9 92.29 6.00 6 3 -9 93.19 4.80 -6 3 9 94.39 3.80 -5 -3 9 92.99 5.20 -5 -3 9 100.29 5.90 5 -3 -9 100.29 4.10 5 -3 -9 100.29 5.10 -5 3 9 101.19 4.20 5 3 -9 101.19 5.00 5 3 -9 107.89 5.10 -5 3 9 91.49 5.70 -4 -3 9 43.50 4.30 -4 -3 9 34.00 4.20 4 -3 -9 41.80 2.60 4 -3 -9 40.30 3.60 4 3 -9 37.40 3.30 -4 3 9 42.40 4.80 4 3 -9 46.90 3.90 -4 3 9 44.20 2.90 3 -3 -9 35.90 2.50 -3 -3 9 34.20 4.10 3 -3 -9 29.10 2.90 -3 -3 9 31.10 3.50 -3 3 9 25.10 3.50 3 3 -9 28.90 2.60 -3 3 9 32.80 3.00 3 3 -9 39.00 3.60 2 -3 -9 28.50 2.90 -2 -3 9 26.50 3.60 -2 -3 9 38.00 1.80 -2 -3 9 34.40 3.60 2 3 -9 32.00 2.10 -2 3 9 31.70 3.00 -2 3 9 36.00 4.30 2 3 -9 36.80 3.30 -2 3 9 29.20 2.90 -1 -3 9 161.58 4.90 -1 -3 9 176.38 7.70 -1 -3 9 168.18 6.90 1 -3 -9 165.48 5.50 -1 3 9 174.98 6.20 -1 3 9 162.38 6.40 1 3 -9 167.78 6.30 -1 3 9 159.78 7.50 1 3 -9 158.78 4.50 0 -3 9 21.80 2.30 0 -3 -9 20.40 2.20 0 -3 9 20.50 3.30 0 -3 9 26.90 3.40 0 3 -9 27.50 3.10 0 3 9 19.90 3.20 0 3 9 23.80 2.80 0 3 -9 24.00 1.30 0 3 9 22.60 2.90 0 3 9 23.90 2.60 1 -3 9 55.19 3.40 -1 -3 -9 48.40 4.50 1 -3 9 59.39 5.10 -1 -3 -9 53.59 2.80 -1 3 -9 57.19 3.70 -1 3 -9 58.59 4.20 1 3 9 55.19 3.80 1 3 9 55.39 4.60 1 3 9 53.19 3.20 2 -3 9 156.38 6.30 2 -3 9 149.88 6.90 -2 -3 -9 161.78 7.10 -2 -3 -9 153.18 5.00 2 3 9 157.98 6.90 -2 3 -9 165.18 7.20 -2 3 -9 156.08 6.20 2 3 9 161.08 6.90 2 3 9 152.28 5.50 -3 -3 -9 1771.32 34.70 3 -3 9 1795.72 33.90 3 -3 9 1761.42 34.60 -3 -3 -9 1711.13 30.10 -3 3 -9 1773.22 32.90 3 3 9 1715.83 31.20 -3 3 -9 1807.42 35.00 3 3 9 1762.92 34.90 3 3 9 1764.62 34.60 -4 -3 -9 433.56 9.40 4 -3 9 435.56 12.90 -4 -3 -9 429.76 13.00 4 -3 9 444.16 13.20 4 3 9 428.06 13.10 4 3 9 430.26 10.60 4 3 9 437.66 13.60 -4 3 -9 415.86 11.50 -4 3 -9 434.86 13.10 5 -3 9 527.65 15.00 -5 -3 -9 490.35 14.50 5 -3 9 524.65 14.80 5 3 9 495.65 11.90 -5 3 -9 484.95 12.90 -5 3 -9 502.15 14.70 5 3 9 475.45 14.50 5 3 9 522.55 15.60 -6 -3 -9 39.20 4.60 6 -3 9 40.10 4.80 6 -3 9 39.40 4.60 -6 3 -9 46.50 5.10 -6 3 -9 48.50 4.30 6 3 9 39.60 4.90 6 3 9 46.10 4.90 -7 -3 -9 21.40 3.80 7 -3 9 20.70 3.80 7 -3 9 25.90 3.80 7 3 9 25.10 4.30 -7 3 -9 26.30 4.20 -8 -3 -9 10.10 2.90 -8 -3 -9 14.40 2.80 8 -3 9 11.00 2.90 8 -3 9 12.20 3.10 8 3 9 12.70 3.60 -8 3 -9 11.70 3.10 -9 -3 -9 4.20 1.90 -9 -3 -9 1.90 2.00 9 -3 9 10.00 3.30 9 -3 9 2.80 2.00 9 3 9 1.50 2.10 -9 3 -9 3.80 2.30 -12 -4 9 46.60 6.80 12 -4 -9 37.90 5.40 12 4 -9 33.20 5.20 -12 4 9 40.10 6.10 -11 -4 9 -0.20 1.70 11 -4 -9 1.40 1.90 -11 -4 9 2.80 2.10 11 4 -9 -1.10 1.60 -11 4 9 2.70 2.50 11 4 -9 0.60 1.50 -10 -4 9 18.40 4.10 -10 -4 9 14.40 3.10 10 -4 -9 14.50 3.30 -10 4 9 13.50 3.50 10 4 -9 9.40 2.70 10 4 -9 21.70 3.30 9 -4 -9 107.79 6.60 -9 -4 9 105.59 7.10 -9 -4 9 107.19 6.30 -9 4 9 103.79 7.20 9 4 -9 118.59 7.00 9 4 -9 103.69 5.70 8 -4 -9 20.60 3.40 -8 -4 9 19.60 3.10 8 -4 -9 16.20 2.40 -8 -4 9 16.60 3.40 8 4 -9 16.10 2.70 8 4 -9 21.30 3.40 -8 4 9 14.70 3.30 7 -4 -9 246.08 9.40 -7 -4 9 245.48 10.20 7 -4 -9 224.48 7.40 -7 -4 9 235.38 9.10 -7 4 9 239.48 10.10 7 4 -9 238.78 9.00 7 4 -9 226.58 8.20 -6 -4 9 66.39 6.00 6 -4 -9 68.39 4.70 -6 -4 9 75.69 4.90 6 -4 -9 77.69 4.00 6 4 -9 83.59 4.90 -6 4 9 74.59 5.40 -6 4 9 72.99 3.10 6 4 -9 85.59 4.80 5 -4 -9 259.97 7.70 -5 -4 9 249.18 9.10 5 -4 -9 248.28 8.80 -5 -4 9 244.38 9.60 5 4 -9 247.88 8.40 -5 4 9 234.18 6.70 -5 4 9 267.87 10.00 5 4 -9 234.18 8.10 -4 -4 9 4.70 1.70 4 -4 -9 3.40 1.50 -4 -4 9 4.80 1.90 4 -4 -9 2.20 1.10 4 4 -9 1.90 1.20 -4 4 9 1.90 1.40 -4 4 9 3.80 1.20 4 4 -9 3.80 1.30 -3 -4 9 128.59 3.30 3 -4 -9 129.99 5.70 -3 -4 9 127.89 6.70 3 -4 -9 127.59 5.20 -3 -4 9 139.59 6.40 3 4 -9 127.49 5.00 -3 4 9 122.69 6.60 -3 4 9 128.29 5.10 3 4 -9 134.79 5.90 -2 -4 9 23.00 3.30 -2 -4 9 28.70 3.90 -2 -4 9 24.20 1.70 -2 4 9 24.80 2.80 2 4 -9 29.20 3.20 -2 4 9 18.90 2.50 -2 4 9 21.00 3.20 2 4 -9 22.50 2.20 -1 -4 9 21.20 3.00 -1 -4 9 24.60 3.70 -1 -4 9 23.10 2.20 -1 4 9 22.90 3.40 -1 4 9 20.80 2.70 -1 4 9 21.20 3.00 1 4 -9 28.50 2.30 -1 4 9 26.80 3.00 1 4 -9 23.10 2.90 0 -4 9 56.89 5.00 0 -4 -9 57.99 3.00 0 -4 9 49.70 3.00 0 -4 9 51.89 5.10 0 4 9 54.69 3.80 0 4 -9 49.30 2.20 0 4 9 52.59 3.70 0 4 9 56.39 3.80 0 4 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3.60 7 4 9 26.00 4.60 -7 4 -9 28.80 4.40 8 -4 9 8.40 3.10 8 -4 9 3.10 1.90 -8 -4 -9 9.30 2.30 -8 -4 -9 4.70 2.40 8 4 9 2.60 2.10 -8 4 -9 8.10 2.70 -9 -4 -9 11.30 2.60 9 -4 9 4.20 2.20 9 -4 9 7.20 2.90 -9 -4 -9 3.70 2.40 -9 4 -9 9.80 3.20 9 4 9 7.60 3.20 11 -5 -9 28.00 4.50 -11 -5 9 18.70 3.70 -11 -5 9 31.70 5.40 11 5 -9 24.30 4.40 11 5 -9 23.20 3.40 -11 5 9 23.60 4.70 -10 -5 9 20.20 3.60 -10 -5 9 11.80 3.30 10 -5 -9 17.80 3.50 10 5 -9 18.60 3.20 10 5 -9 12.70 3.30 -10 5 9 11.10 3.40 9 -5 -9 86.59 7.20 9 -5 -9 76.29 4.70 -9 -5 9 84.49 5.80 -9 -5 9 66.29 6.70 9 5 -9 87.69 7.20 9 5 -9 85.19 5.20 -9 5 9 91.99 8.00 -8 -5 9 2.70 1.80 8 -5 -9 0.30 1.40 8 -5 -9 2.10 1.30 -8 -5 9 2.20 1.80 8 5 -9 0.20 1.30 -8 5 9 1.90 1.70 8 5 -9 2.60 1.70 -7 -5 9 61.99 5.70 -7 -5 9 56.59 5.70 7 -5 -9 51.69 3.80 7 -5 -9 59.69 5.50 -7 5 9 51.69 5.50 7 5 -9 63.39 4.30 7 5 -9 56.79 5.20 6 -5 -9 100.79 5.00 -6 -5 9 93.49 5.80 -6 -5 9 119.09 6.70 6 -5 -9 97.49 5.80 -6 5 9 99.99 6.30 6 5 -9 102.59 5.60 6 5 -9 105.09 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12.90 5 -6 -9 409.96 11.70 -5 -6 9 402.86 13.10 5 -6 -9 399.86 12.60 -5 6 9 406.46 13.20 5 6 -9 404.76 11.80 5 6 -9 400.56 11.70 -4 -6 9 141.19 7.20 4 -6 -9 136.59 6.70 -4 -6 9 126.09 6.80 -4 -6 9 134.39 4.00 4 -6 -9 140.09 6.30 4 6 -9 132.19 6.00 4 6 -9 139.69 6.40 -4 6 9 120.49 6.70 -3 -6 9 278.07 10.10 3 -6 -9 276.97 9.30 -3 -6 9 264.77 6.90 -3 -6 9 271.97 10.10 -3 6 9 277.17 8.00 -3 6 9 264.77 10.00 -3 6 9 274.07 10.90 3 6 -9 277.17 9.30 3 6 -9 266.77 8.50 -2 -6 9 10.70 2.50 -2 -6 9 13.50 2.70 -2 -6 9 9.70 1.60 -2 6 9 12.90 2.70 -2 6 9 8.60 1.80 -2 6 9 10.70 2.30 2 6 -9 8.00 1.70 -2 6 9 10.70 2.60 2 6 -9 9.10 2.10 -1 -6 9 43.30 4.60 -1 -6 9 47.00 3.10 -1 -6 9 43.60 4.60 -1 6 9 44.70 4.00 -1 6 9 46.60 4.90 1 6 -9 43.40 4.20 1 6 -9 43.90 2.90 -1 6 9 48.20 4.80 -1 6 9 41.10 4.20 0 -6 9 2.20 1.50 0 -6 -9 5.20 1.80 0 -6 9 5.20 1.50 0 6 -9 5.60 1.90 0 6 9 9.00 2.00 0 6 9 7.50 2.00 0 6 -9 6.90 2.00 0 6 -9 7.50 1.50 0 6 9 6.40 2.10 1 -6 9 82.19 5.30 -1 -6 -9 83.39 3.50 -1 -6 -9 81.99 4.90 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19.20 3.60 5 -9 -9 50.99 5.50 -5 -9 9 54.49 5.60 -5 -9 9 61.29 6.40 5 9 -9 40.90 4.90 -5 9 9 67.19 6.00 5 9 -9 54.29 5.20 4 -9 -9 22.80 3.80 -4 -9 9 18.30 3.30 -4 -9 9 24.10 4.20 4 9 -9 26.30 3.70 -4 9 9 20.30 3.40 4 9 -9 25.70 3.80 -4 9 9 30.30 5.10 -3 -9 9 174.08 6.60 3 -9 -9 163.48 5.70 -3 -9 9 165.18 8.60 -3 -9 9 183.78 8.00 3 -9 -9 181.28 8.60 3 9 -9 166.98 7.60 -3 9 9 175.38 9.80 3 9 -9 170.18 7.90 -3 9 9 155.28 7.40 -2 -9 9 21.30 3.80 2 -9 -9 21.20 2.40 2 -9 -9 15.20 3.10 -2 -9 9 15.90 2.50 -2 -9 9 20.30 3.40 -2 9 9 15.00 2.70 2 9 -9 18.00 3.30 -2 9 9 18.70 4.00 2 9 -9 18.60 3.10 1 -9 -9 178.98 7.00 -1 -9 9 168.58 7.20 -1 -9 9 179.28 8.80 1 -9 -9 167.18 6.30 1 -9 -9 189.18 8.80 1 9 -9 172.78 7.00 1 9 -9 178.08 8.10 1 9 -9 167.58 7.30 -1 9 9 186.38 9.50 0 -9 -9 32.30 3.30 0 -9 9 39.60 5.10 0 -9 -9 33.60 3.60 0 -9 9 35.90 4.20 0 9 -9 26.70 3.90 0 9 9 25.20 4.20 0 9 9 32.20 4.80 0 9 -9 27.60 3.40 0 9 -9 30.20 3.50 1 -9 9 84.69 5.50 -1 -9 -9 80.09 4.60 -1 -9 -9 88.19 4.70 1 -9 9 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3 -2 10 69.49 5.80 -3 -2 -10 57.69 3.20 3 2 10 63.49 2.90 -3 2 -10 50.49 4.10 3 2 10 64.59 4.70 -3 2 -10 55.39 5.30 3 2 10 59.19 5.20 -4 -2 -10 4.10 2.00 -4 -2 -10 3.30 1.20 4 -2 10 4.10 1.70 4 -2 10 6.70 2.30 -4 2 -10 4.80 1.60 4 2 10 4.70 2.00 -4 2 -10 2.70 1.60 4 2 10 6.20 2.20 5 -2 10 30.10 4.00 5 -2 10 21.20 3.50 -5 -2 -10 24.60 3.70 -5 2 -10 23.60 3.60 5 2 10 26.20 3.80 -5 2 -10 24.60 3.00 5 2 10 23.70 3.80 -6 -2 -10 50.39 5.40 6 -2 10 58.39 6.00 6 -2 10 45.90 5.10 -6 2 -10 55.69 3.80 -6 2 -10 55.79 5.90 6 2 10 46.80 5.40 6 2 10 56.39 5.90 -7 -2 -10 9.40 2.80 7 -2 10 6.70 2.40 7 -2 10 8.60 2.60 -7 2 -10 6.00 2.40 7 2 10 3.30 1.80 7 2 10 4.30 2.30 8 -2 10 26.10 4.50 -8 -2 -10 32.60 4.80 8 -2 10 22.60 3.90 -8 2 -10 26.30 4.50 8 2 10 24.80 4.60 9 -2 10 16.00 4.10 -9 -2 -10 10.30 2.40 -9 -2 -10 17.60 3.70 9 -2 10 17.70 3.60 9 2 10 13.20 3.70 -9 2 -10 9.90 2.90 -12 -3 10 33.50 5.50 12 -3 -10 23.80 4.40 -12 3 10 19.20 4.60 12 3 -10 25.80 3.80 12 3 -10 21.20 4.30 -11 -3 10 24.80 4.80 11 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494.65 11.20 -4 3 10 485.75 15.10 4 3 -10 487.05 12.80 -4 3 10 467.65 11.90 4 3 -10 489.95 12.00 -3 -3 10 47.60 4.60 -3 -3 10 38.10 4.50 -3 -3 10 46.90 1.50 3 -3 -10 45.50 3.80 -3 3 10 44.80 3.80 3 3 -10 49.10 2.90 -3 3 10 50.99 5.20 3 3 -10 49.30 4.10 -2 -3 10 21.10 3.10 2 -3 -10 13.20 1.90 -2 -3 10 12.90 2.90 -2 -3 10 13.70 1.40 2 -3 -10 13.20 2.10 -2 3 10 15.40 2.40 2 3 -10 12.70 1.60 2 3 -10 11.70 2.20 -2 3 10 17.00 3.20 -2 3 10 15.70 2.30 -1 -3 10 22.40 3.30 -1 -3 10 26.60 4.00 1 -3 -10 20.80 2.50 1 -3 -10 20.80 2.40 -1 -3 10 23.10 2.20 -1 3 10 19.20 2.70 -1 3 10 12.90 2.90 -1 3 10 21.00 2.70 1 3 -10 23.10 1.90 1 3 -10 21.60 2.90 0 -3 10 5.20 1.30 0 -3 -10 4.00 1.20 0 -3 10 4.00 1.90 0 -3 10 3.80 1.60 0 3 10 4.70 2.20 0 3 -10 6.30 1.80 0 3 -10 5.50 0.70 0 3 10 4.10 1.70 0 3 10 4.40 1.50 0 3 10 6.30 1.60 -1 -3 -10 5.70 2.10 -1 -3 -10 9.60 1.60 1 -3 10 7.60 1.70 1 -3 10 5.50 1.80 1 3 10 9.10 2.10 1 3 10 6.10 1.90 1 3 10 8.00 1.70 -1 3 -10 8.90 2.20 -1 3 -10 9.70 2.10 -2 -3 -10 -1.00 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3.00 2.30 9 -3 10 1.60 2.00 9 -3 10 0.60 1.90 -9 -3 -10 4.90 2.00 -9 3 -10 7.40 2.70 9 3 10 0.30 2.00 11 -4 -10 7.00 2.70 -11 -4 10 8.80 2.70 -11 -4 10 7.10 3.20 11 4 -10 8.30 2.90 11 4 -10 6.40 2.30 -11 4 10 7.20 3.40 10 -4 -10 20.50 3.80 -10 -4 10 26.80 4.00 -10 -4 10 34.00 5.40 -10 4 10 37.20 5.60 10 4 -10 28.50 3.80 10 4 -10 21.50 3.80 9 -4 -10 25.70 4.00 -9 -4 10 23.60 3.70 -9 -4 10 23.00 4.40 -9 4 10 20.70 4.20 9 4 -10 24.60 3.40 9 4 -10 25.20 4.10 -8 -4 10 82.69 5.60 8 -4 -10 74.09 6.30 -8 -4 10 80.89 7.40 -8 4 10 96.19 8.10 8 4 -10 83.59 5.50 8 4 -10 84.89 5.30 7 -4 -10 6.70 1.50 -7 -4 10 5.60 2.10 7 -4 -10 6.50 2.30 -7 -4 10 7.80 2.50 -7 4 10 11.50 3.20 7 4 -10 7.50 2.00 7 4 -10 10.50 2.50 6 -4 -10 174.98 6.20 -6 -4 10 178.08 8.70 -6 -4 10 183.68 8.00 6 -4 -10 179.18 7.70 6 4 -10 184.38 7.40 6 4 -10 186.68 7.50 -6 4 10 184.48 8.80 -6 4 10 178.18 5.70 -5 -4 10 31.00 4.40 -5 -4 10 41.60 4.50 5 -4 -10 40.40 4.10 5 -4 -10 35.30 3.20 5 4 -10 40.40 4.00 -5 4 10 38.70 3.20 5 4 -10 36.10 3.90 -5 4 10 27.80 4.10 4 -4 -10 150.48 5.80 -4 -4 10 151.28 7.80 -4 -4 10 162.98 7.40 4 -4 -10 144.29 6.40 -4 4 10 148.59 7.80 4 4 -10 147.09 5.80 4 4 -10 152.18 6.50 -4 4 10 147.79 5.70 -3 -4 10 72.69 2.30 3 -4 -10 73.49 4.00 -3 -4 10 77.89 5.50 -3 -4 10 76.69 5.00 3 -4 -10 74.29 4.40 3 4 -10 74.69 3.80 -3 4 10 69.79 4.00 3 4 -10 75.39 4.60 -3 4 10 87.79 5.80 -2 -4 10 101.09 3.60 2 -4 -10 111.69 5.20 -2 -4 10 122.49 6.80 -2 -4 10 108.09 5.90 2 4 -10 113.99 5.50 -2 4 10 109.19 6.40 -2 4 10 108.29 5.20 2 4 -10 113.79 4.30 -2 4 10 120.69 5.50 -1 -4 10 9.60 2.70 -1 -4 10 9.40 2.30 -1 -4 10 12.10 1.70 1 -4 -10 9.10 1.70 1 4 -10 8.00 2.10 -1 4 10 10.80 2.10 -1 4 10 11.10 2.20 -1 4 10 7.30 2.10 -1 4 10 10.70 2.70 1 4 -10 10.10 1.40 0 -4 10 54.19 5.20 0 -4 10 48.40 3.10 0 -4 -10 46.00 2.90 0 4 -10 45.30 4.10 0 4 -10 43.30 2.00 0 4 10 41.60 4.10 0 4 10 48.40 4.10 0 4 10 49.80 4.40 -1 -4 -10 13.60 2.70 1 -4 10 13.30 2.20 -1 -4 -10 16.10 2.00 1 -4 10 16.60 3.00 1 4 10 13.50 2.60 1 4 10 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3.50 1.40 4 -5 -10 7.10 2.00 -4 -5 10 1.20 1.60 4 5 -10 4.10 1.60 4 5 -10 4.80 1.70 -4 5 10 4.30 2.00 -4 5 10 6.30 1.50 -3 -5 10 19.80 1.70 3 -5 -10 20.70 3.10 -3 -5 10 17.30 3.20 3 -5 -10 17.80 2.70 -3 -5 10 22.10 3.50 -3 5 10 17.20 2.40 -3 5 10 22.90 3.90 3 5 -10 19.40 3.10 3 5 -10 22.20 2.60 -2 -5 10 53.89 5.20 -2 -5 10 55.39 5.50 -2 -5 10 53.79 2.70 -2 5 10 49.30 5.00 2 5 -10 49.80 3.10 2 5 -10 57.89 5.00 -2 5 10 55.89 4.50 -2 5 10 41.00 4.70 -2 5 10 46.80 4.30 -1 -5 10 3.50 1.10 -1 -5 10 7.00 2.20 -1 -5 10 7.60 2.40 1 5 -10 7.60 2.00 -1 5 10 3.80 2.00 1 5 -10 4.40 1.20 -1 5 10 3.20 1.50 -1 5 10 6.60 1.80 -1 5 10 1.70 1.40 0 -5 -10 6.50 1.40 0 -5 10 5.50 1.40 0 -5 -10 4.70 1.70 0 -5 10 5.50 2.00 0 5 10 9.80 2.20 0 5 10 3.20 1.60 0 5 -10 4.30 1.90 0 5 -10 6.50 1.20 0 5 10 4.70 1.70 0 5 -10 8.70 2.10 -1 -5 -10 59.29 3.10 1 -5 10 60.89 5.50 -1 -5 -10 63.39 4.50 1 -5 10 60.69 3.90 1 5 10 55.29 4.70 1 5 10 52.09 4.80 -1 5 -10 60.89 5.40 -1 5 -10 55.49 4.80 1 5 10 58.99 5.30 2 -5 10 59.39 5.60 -2 -5 -10 63.79 4.60 -2 -5 -10 70.09 3.30 2 -5 10 77.19 4.70 2 5 10 65.09 4.30 2 5 10 75.99 5.30 2 5 10 72.29 5.00 -2 5 -10 67.89 5.80 -2 5 -10 60.09 5.10 -3 -5 -10 15.50 2.90 -3 -5 -10 17.70 1.90 3 -5 10 18.90 3.30 3 -5 10 20.60 3.20 -3 5 -10 15.20 2.60 3 5 10 18.00 3.20 -3 5 -10 17.50 3.10 3 5 10 12.40 2.40 3 5 10 21.80 3.50 4 -5 10 42.70 4.90 -4 -5 -10 31.50 4.10 4 -5 10 33.50 4.30 -4 5 -10 33.80 4.20 4 5 10 27.80 3.90 4 5 10 40.60 5.20 -4 5 -10 30.10 3.80 4 5 10 32.40 3.60 -5 -5 -10 1.00 1.60 5 -5 10 1.40 1.70 5 -5 10 0.80 1.80 5 5 10 1.70 1.80 5 5 10 1.00 2.50 -5 5 -10 2.30 1.80 -5 5 -10 2.60 1.60 6 -5 10 6.40 2.30 -6 -5 -10 10.00 2.80 -6 -5 -10 5.60 2.00 6 -5 10 8.40 2.70 6 5 10 9.50 2.90 -6 5 -10 6.60 2.10 -6 5 -10 10.40 2.80 -7 -5 -10 2.10 1.60 7 -5 10 5.90 2.50 7 -5 10 3.10 1.90 -7 -5 -10 4.60 2.50 7 5 10 8.40 3.00 -7 5 -10 5.60 2.40 -8 -5 -10 1.20 1.40 -8 -5 -10 0.50 1.80 8 -5 10 1.30 1.80 8 -5 10 3.90 2.60 -8 5 -10 0.30 1.90 8 5 10 0.20 2.00 -11 -6 10 40.00 5.60 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5.50 2.40 3 -5 -14 6.20 1.80 3 -5 -14 7.10 2.00 -3 -5 14 12.20 3.70 3 5 -14 7.40 2.30 -3 5 14 2.90 2.50 -3 5 14 4.70 2.00 -2 -5 14 28.30 5.10 -2 -5 14 13.20 3.30 2 -5 -14 25.10 3.30 2 -5 -14 23.30 3.10 -2 5 14 21.40 3.50 -2 5 14 20.20 3.30 -2 5 14 18.40 4.10 2 5 -14 22.90 3.80 1 -5 -14 5.00 1.70 1 -5 -14 6.90 2.60 1 -5 -14 10.60 2.30 -1 -5 14 8.90 2.90 1 5 -14 4.10 2.00 -1 5 14 12.10 2.90 -1 5 14 10.40 2.70 0 -5 -14 17.30 3.70 0 -5 -14 19.00 2.80 0 -5 14 17.50 3.70 0 5 -14 17.70 3.50 0 5 14 17.20 3.50 0 5 14 22.30 3.70 0 5 -14 24.10 4.30 -1 -5 -14 27.30 3.20 1 -5 14 35.80 5.30 -1 -5 -14 31.30 4.70 1 -5 14 31.60 3.80 -1 5 -14 27.50 4.60 -1 5 -14 29.60 4.20 1 5 14 29.00 4.50 1 5 14 32.20 4.50 2 -5 14 152.38 7.40 -2 -5 -14 159.88 8.90 2 -5 14 153.98 9.00 -2 5 -14 155.68 8.80 -2 5 -14 144.39 7.80 2 5 14 165.58 8.80 2 5 14 138.99 8.30 3 -5 14 33.60 4.40 3 -5 14 26.30 4.60 -3 -5 -14 39.20 5.30 3 5 14 27.00 4.50 3 5 14 41.10 5.40 -3 5 -14 27.40 4.60 -3 5 -14 34.60 4.70 4 -5 14 2.10 2.20 -4 -5 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2.70 8 7 -14 1.10 2.00 8 7 -14 -0.60 1.90 -7 -7 14 23.60 5.00 -7 -7 14 28.50 4.90 7 -7 -14 25.10 4.40 7 7 -14 26.30 4.20 -7 7 14 28.10 5.40 7 7 -14 31.70 4.60 -6 -7 14 66.59 7.80 -6 -7 14 45.90 6.00 6 -7 -14 53.69 6.00 6 7 -14 58.59 6.30 -6 7 14 49.90 6.70 6 7 -14 59.29 5.80 5 -7 -14 24.00 3.90 -5 -7 14 27.10 5.30 -5 -7 14 24.20 4.50 5 7 -14 15.00 3.50 -5 7 14 29.60 5.30 -4 -7 14 74.89 7.40 4 -7 -14 77.79 6.60 4 -7 -14 82.09 5.70 -4 -7 14 85.99 8.60 -4 7 14 80.89 5.10 -4 7 14 95.39 9.10 4 7 -14 72.39 6.70 -3 -7 14 3.30 2.60 3 -7 -14 0.20 1.50 -3 -7 14 3.60 2.40 3 -7 -14 3.00 1.90 3 7 -14 3.60 2.00 -3 7 14 2.70 2.60 -3 7 14 2.60 1.60 2 -7 -14 33.80 4.30 -2 -7 14 36.10 5.60 -2 -7 14 24.40 4.60 2 -7 -14 31.70 3.70 2 7 -14 31.10 4.50 -2 7 14 38.20 4.60 -1 -7 14 21.50 4.20 1 -7 -14 19.30 3.30 1 -7 -14 12.70 2.50 1 -7 -14 11.70 3.20 -1 7 14 16.00 3.20 1 7 -14 10.80 3.30 -1 7 14 12.90 3.30 1 7 -14 11.60 3.00 0 -7 -14 19.80 3.80 0 -7 -14 21.40 3.00 0 -7 14 15.60 3.60 0 7 -14 14.60 3.20 0 7 14 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3.60 -4 -5 16 7.90 3.20 4 -5 -16 7.50 2.30 4 -5 -16 11.40 2.70 -4 5 16 9.50 2.70 -4 5 16 10.90 4.20 4 5 -16 6.50 2.50 -3 -5 16 44.50 7.10 -3 -5 16 34.40 5.30 3 -5 -16 37.00 4.40 3 5 -16 38.50 5.10 -3 5 16 38.90 4.80 -3 5 16 28.20 5.60 2 -5 -16 112.19 6.30 -2 -5 16 119.29 8.20 2 5 -16 87.59 7.80 -2 5 16 93.49 6.50 1 -5 -16 65.79 7.30 -1 -5 16 76.79 7.70 1 -5 -16 64.79 5.60 1 5 -16 66.09 7.40 -1 5 16 72.79 6.70 1 5 -16 68.79 6.90 -1 5 16 72.49 7.10 0 -5 -16 22.60 3.40 0 -5 -16 17.70 4.30 0 -5 16 17.30 4.10 0 5 -16 21.90 4.00 0 5 16 27.60 4.80 0 5 16 14.60 3.30 0 5 -16 19.20 4.50 1 -5 16 125.29 8.60 -1 -5 -16 121.29 8.30 1 5 16 117.29 7.70 -1 5 -16 130.59 8.70 1 5 16 112.39 7.80 -1 5 -16 122.99 7.70 -2 -5 -16 74.89 8.00 2 -5 16 60.89 7.10 -2 5 -16 76.09 7.10 -2 5 -16 75.69 7.90 2 5 16 73.59 7.40 2 5 16 68.19 7.40 -6 -6 16 31.20 5.20 -6 -6 16 30.40 6.10 6 -6 -16 26.90 4.20 6 -6 -16 25.80 4.00 -6 6 16 27.70 5.50 6 6 -16 27.80 4.70 5 -6 -16 2.20 2.00 5 -6 -16 1.00 1.70 -5 -6 16 1.40 2.40 -5 -6 16 4.70 3.40 -5 6 16 4.60 3.30 5 6 -16 1.60 2.10 4 -6 -16 0.60 1.50 -4 -6 16 1.60 2.30 -4 -6 16 -0.10 2.10 4 -6 -16 1.50 1.60 -4 6 16 2.00 2.00 4 6 -16 1.60 2.10 -4 6 16 0.30 2.50 3 -6 -16 12.00 2.90 -3 -6 16 15.60 4.70 -3 -6 16 7.90 3.20 3 -6 -16 8.70 3.90 -3 6 16 11.60 3.00 3 6 -16 10.00 3.20 -3 6 16 12.60 4.40 -2 -6 16 95.09 8.70 2 -6 -16 95.39 8.50 2 -6 -16 103.69 6.10 2 6 -16 102.49 8.50 -2 6 16 107.19 7.10 -1 -6 16 7.50 2.90 1 -6 -16 9.60 2.50 1 -6 -16 10.70 3.40 -1 6 16 8.30 2.90 1 6 -16 9.50 3.20 1 6 -16 6.70 2.80 -1 6 16 12.00 3.30 0 -6 16 30.60 5.10 0 -6 -16 24.80 4.60 0 6 16 27.80 4.80 0 6 16 21.70 4.20 0 6 -16 24.50 4.70 0 6 -16 26.60 4.60 -1 -6 -16 4.80 2.70 1 -6 16 0.90 2.00 1 6 16 2.00 2.30 -1 6 -16 3.00 2.30 -1 6 -16 0.90 2.20 1 6 16 6.60 2.90 -5 -7 16 10.10 3.70 5 -7 -16 0.40 1.80 -5 -7 16 3.10 2.60 -5 7 16 5.10 3.10 -4 -7 16 10.90 3.60 4 -7 -16 9.60 2.70 4 -7 -16 12.30 3.00 -4 -7 16 8.30 3.70 -4 7 16 11.50 3.80 4 7 -16 11.10 3.40 -3 -7 16 1.30 2.00 3 -7 -16 -1.00 1.30 -3 -7 16 0.00 2.20 3 -7 -16 1.70 1.80 -3 7 16 -1.70 1.50 -3 7 16 0.60 2.60 3 7 -16 -2.00 1.60 -2 -7 16 5.50 3.10 2 -7 -16 3.70 2.40 2 -7 -16 2.50 1.70 2 7 -16 4.00 2.70 2 7 -16 1.00 2.10 -2 7 16 1.10 1.90 1 -7 -16 14.90 4.00 1 -7 -16 11.10 2.60 -1 -7 16 10.00 3.60 -1 7 16 8.40 3.00 1 7 -16 10.20 3.10 1 7 -16 10.30 3.40 -1 7 16 10.90 3.10 0 -7 16 21.80 4.80 0 -7 -16 21.50 4.40 0 7 16 21.70 4.20 0 7 -16 23.10 4.40 0 7 16 31.60 5.00 0 7 -16 21.30 4.40 -7 0 17 5.40 2.50 7 0 -17 4.10 2.20 -7 0 17 7.20 3.70 7 0 -17 1.90 2.00 6 0 -17 0.40 1.60 -6 0 17 0.20 1.60 -6 0 17 -1.20 2.10 5 0 -17 15.20 3.50 -5 0 17 18.20 3.90 -5 0 17 15.10 4.70 -4 0 17 7.90 2.90 4 0 -17 6.00 2.50 -4 0 17 2.20 3.00 -3 0 17 7.40 3.70 -3 0 17 2.60 2.40 3 0 -17 5.70 2.30 2 0 -17 11.80 2.90 -2 0 17 11.00 3.90 -2 0 17 15.90 3.70 1 0 -17 11.20 3.00 -1 0 17 12.60 3.50 1 0 -17 12.00 3.60 0 0 -17 7.20 2.90 0 0 -17 5.30 2.30 0 0 17 6.80 3.00 -1 0 -17 30.30 4.40 -1 0 -17 23.10 4.70 1 0 17 23.60 4.60 2 0 17 0.20 2.10 -2 0 -17 1.80 1.90 -2 0 -17 -0.10 2.20 7 -1 -17 25.00 4.40 -7 -1 17 31.90 4.70 -7 -1 17 27.60 5.80 7 -1 -17 28.70 4.00 7 1 -17 31.30 4.70 -7 1 17 37.40 6.70 -7 1 17 27.00 5.90 -6 -1 17 15.30 3.40 6 -1 -17 8.60 2.70 -6 -1 17 8.10 3.70 6 1 -17 15.90 3.50 -6 1 17 13.00 4.40 -6 1 17 20.30 3.90 5 -1 -17 26.30 4.00 -5 -1 17 27.80 5.60 -5 -1 17 27.50 4.50 -5 1 17 34.10 4.90 5 1 -17 21.70 4.00 -5 1 17 27.20 5.70 -4 -1 17 41.20 5.60 -4 -1 17 28.40 5.90 4 -1 -17 35.50 4.80 -4 1 17 35.70 4.90 -4 1 17 43.80 7.10 4 1 -17 34.80 4.70 -3 -1 17 17.70 3.80 -3 -1 17 27.20 5.90 3 -1 -17 25.20 4.10 3 1 -17 30.80 4.50 -3 1 17 29.50 4.60 -3 1 17 31.20 6.20 2 -1 -17 2.20 1.60 -2 -1 17 0.40 2.30 -2 -1 17 0.60 1.90 -2 1 17 0.70 1.70 -2 1 17 4.80 3.40 2 1 -17 -0.40 1.50 1 -1 -17 -0.40 2.00 1 -1 -17 3.40 2.10 -1 -1 17 -0.80 1.60 1 1 -17 -0.60 1.40 -1 1 17 -1.30 1.60 1 1 -17 1.10 2.10 0 -1 -17 77.39 8.40 0 -1 -17 64.59 5.90 0 -1 17 77.49 7.70 0 1 -17 77.69 8.20 0 1 -17 63.89 6.30 0 1 17 58.99 6.80 -1 -1 -17 201.78 9.00 1 -1 17 187.98 10.60 -1 -1 -17 185.88 10.90 -1 1 -17 209.38 11.50 1 1 17 194.68 10.60 -1 1 -17 215.38 9.50 2 -1 17 8.70 3.40 -2 -1 -17 23.30 3.70 -2 -1 -17 13.50 4.10 2 1 17 14.00 3.80 2 1 17 15.80 3.60 -2 1 -17 12.80 3.20 -2 1 -17 19.20 4.60 -7 -2 17 4.20 3.60 7 -2 -17 8.70 3.00 7 -2 -17 7.70 2.70 -7 -2 17 9.30 2.90 7 2 -17 6.40 2.60 -7 2 17 8.30 3.90 -6 -2 17 2.90 2.40 -6 -2 17 2.50 2.70 6 -2 -17 3.90 2.10 6 -2 -17 5.70 3.10 6 2 -17 -1.00 1.70 -6 2 17 -1.00 1.50 -6 2 17 6.90 3.50 -5 -2 17 52.09 6.30 5 -2 -17 44.90 5.10 -5 -2 17 50.29 7.50 -5 2 17 49.50 5.70 -5 2 17 37.20 6.50 5 2 -17 61.29 6.50 -4 -2 17 9.80 3.30 -4 -2 17 6.40 3.70 4 -2 -17 7.70 2.50 4 2 -17 5.70 2.50 -4 2 17 11.30 4.20 -4 2 17 14.60 3.40 3 -2 -17 1.30 1.80 -3 -2 17 2.10 2.40 -3 -2 17 4.80 3.50 -3 2 17 4.40 2.30 -3 2 17 4.00 3.30 3 2 -17 2.20 2.10 -2 -2 17 27.60 4.80 2 -2 -17 26.80 4.00 -2 -2 17 31.20 5.90 2 2 -17 30.30 4.60 -2 2 17 22.50 4.20 -2 2 17 23.10 5.30 1 -2 -17 21.00 3.50 1 -2 -17 14.40 4.00 -1 -2 17 19.30 4.30 -1 2 17 18.00 3.80 1 2 -17 15.40 3.40 1 2 -17 14.80 3.90 0 -2 -17 14.30 4.10 0 -2 -17 16.60 3.20 0 -2 17 17.20 4.00 0 2 17 19.30 4.30 0 2 -17 12.10 3.70 0 2 -17 11.20 3.10 1 -2 17 17.00 4.10 -1 -2 -17 25.90 3.80 -1 -2 -17 18.70 4.60 1 2 17 21.20 4.40 -1 2 -17 21.50 4.00 -1 2 -17 12.50 3.80 2 -2 17 59.49 7.10 -2 -2 -17 90.49 9.20 -2 2 -17 64.99 7.50 -2 2 -17 69.89 6.50 2 2 17 75.79 8.00 2 2 17 76.89 7.10 6 -3 -17 22.80 3.60 6 -3 -17 32.30 4.70 -6 -3 17 21.30 5.20 -6 -3 17 37.40 5.50 6 3 -17 23.90 4.40 -6 3 17 36.50 6.80 -5 -3 17 8.00 3.00 -5 -3 17 7.60 3.50 5 -3 -17 8.60 2.70 -5 3 17 5.60 2.50 -5 3 17 5.30 3.60 5 3 -17 4.60 2.50 -4 -3 17 8.00 4.00 4 -3 -17 12.20 3.00 -4 -3 17 13.90 3.70 -4 3 17 15.80 4.60 -4 3 17 10.00 2.80 4 3 -17 10.90 3.20 -3 -3 17 17.50 5.10 3 -3 -17 10.10 2.60 -3 -3 17 7.10 2.80 3 3 -17 10.30 3.10 -3 3 17 11.30 4.10 -3 3 17 13.60 3.40 -2 -3 17 2.70 2.40 2 -3 -17 7.00 2.40 2 3 -17 3.00 2.00 -2 3 17 3.40 2.50 1 -3 -17 1.20 2.20 -1 -3 17 2.70 2.40 1 -3 -17 4.20 2.10 -1 3 17 2.90 2.20 1 3 -17 2.70 2.50 1 3 -17 1.40 2.00 0 -3 -17 5.90 2.30 0 -3 -17 4.60 3.00 0 -3 17 1.00 2.50 0 3 -17 3.10 2.40 0 3 -17 1.50 2.60 0 3 17 2.00 2.30 -1 -3 -17 5.90 3.00 1 -3 17 7.90 3.20 -1 -3 -17 11.90 3.60 1 3 17 7.50 3.10 -1 3 -17 6.70 3.20 1 3 17 2.70 3.30 -1 3 -17 7.60 2.80 -6 -4 17 6.50 3.10 -6 -4 17 4.60 2.80 6 -4 -17 -0.30 1.60 6 -4 -17 0.30 1.70 6 4 -17 1.20 2.30 -6 4 17 -2.10 2.70 -5 -4 17 15.40 4.50 -5 -4 17 19.70 4.30 5 -4 -17 23.80 4.00 -5 4 17 11.90 4.40 5 4 -17 25.10 4.60 -5 4 17 25.50 4.10 -4 -4 17 18.00 5.10 -4 -4 17 18.80 4.10 4 -4 -17 19.90 3.50 -4 4 17 15.10 3.30 4 4 -17 22.50 4.20 -4 4 17 17.60 4.90 3 -4 -17 37.10 4.70 -3 -4 17 44.20 6.20 -3 -4 17 57.59 8.20 -3 4 17 43.10 7.00 3 4 -17 56.79 6.20 -3 4 17 49.30 5.60 2 -4 -17 5.80 2.30 -2 -4 17 5.70 3.00 2 4 -17 2.60 2.40 -2 4 17 2.60 2.30 -1 -4 17 1.30 1.90 1 -4 -17 1.00 1.60 1 -4 -17 3.20 2.60 1 4 -17 2.80 2.30 -1 4 17 2.70 2.40 1 4 -17 3.70 2.70 0 -4 -17 17.20 3.20 0 -4 17 12.00 3.70 0 -4 -17 18.00 4.30 0 4 -17 14.60 4.00 0 4 17 14.50 3.70 0 4 -17 10.00 3.00 -1 -4 -17 9.80 3.30 1 -4 17 5.70 3.10 1 4 17 9.40 3.20 -1 4 -17 10.90 3.60 1 4 17 11.10 3.40 -1 4 -17 8.80 2.90 5 -5 -17 11.50 3.50 -5 -5 17 6.90 3.60 -5 -5 17 14.00 3.80 5 -5 -17 9.10 2.80 -5 5 17 14.40 4.50 5 5 -17 7.60 2.90 -4 -5 17 1.50 2.30 -4 -5 17 1.80 2.70 4 -5 -17 3.70 2.10 -4 5 17 0.80 2.80 -4 5 17 1.50 2.00 4 5 -17 3.60 2.50 3 -5 -17 15.90 3.20 -3 -5 17 10.20 3.60 -3 -5 17 11.00 3.80 3 5 -17 19.90 4.00 -3 5 17 11.80 3.30 -3 5 17 8.40 3.90 2 -5 -17 9.90 3.60 2 -5 -17 14.90 3.20 -2 -5 17 13.00 3.70 -2 5 17 13.20 3.50 2 5 -17 13.40 3.40 2 5 -17 11.60 3.60 -1 -5 17 15.20 3.90 1 -5 -17 14.90 3.00 1 -5 -17 16.70 4.20 1 5 -17 15.70 4.30 -1 5 17 12.70 3.60 1 5 -17 11.80 3.10 0 -5 -17 33.20 5.70 0 -5 17 17.50 4.10 0 5 17 22.30 4.40 0 5 -17 13.80 3.50 0 5 -17 25.60 5.00 -5 0 18 2.90 2.20 -5 0 18 5.70 3.50 5 0 -18 1.80 1.90 4 0 -18 1.90 2.20 -4 0 18 7.20 2.90 -4 0 18 -0.70 2.80 -3 0 18 10.30 3.10 -3 0 18 10.20 4.30 3 0 -18 10.70 3.10 2 0 -18 1.90 2.20 -2 0 18 -3.50 1.20 1 0 -18 4.90 2.70 -1 0 18 8.60 3.00 1 0 -18 2.10 2.10 0 0 18 8.50 3.30 0 0 -18 6.10 2.60 0 0 -18 5.00 3.30 5 -1 -18 33.90 4.90 -5 -1 18 45.30 7.50 -5 -1 18 37.10 5.40 -5 1 18 49.00 7.90 5 1 -18 33.10 4.80 -5 1 18 36.80 5.20 -4 -1 18 16.20 4.90 4 -1 -18 11.80 3.20 -4 -1 18 19.50 4.30 -4 1 18 12.40 3.30 4 1 -18 16.40 3.80 -4 1 18 13.00 4.30 -3 -1 18 39.60 6.90 3 -1 -18 44.30 5.50 -3 -1 18 36.10 5.50 -3 1 18 37.70 5.50 3 1 -18 42.50 5.40 -3 1 18 49.50 7.70 2 -1 -18 4.10 2.30 -2 -1 18 5.30 2.80 2 1 -18 7.70 2.60 -2 1 18 8.60 3.20 1 -1 -18 1.00 1.90 -1 -1 18 -0.20 2.20 1 -1 -18 -1.20 2.20 -1 1 18 3.70 2.60 1 1 -18 4.00 2.20 1 1 -18 3.00 2.70 0 -1 -18 48.50 6.90 0 1 -18 51.09 7.30 0 1 18 31.10 5.30 -4 -2 18 6.30 3.80 -4 -2 18 10.40 3.50 4 -2 -18 7.90 2.60 -4 2 18 8.10 4.20 -4 2 18 8.60 3.10 4 2 -18 9.00 3.00 3 -2 -18 26.20 4.30 -3 -2 18 18.10 5.00 -3 -2 18 20.70 4.50 -3 2 18 25.60 5.70 -3 2 18 24.10 4.40 3 2 -18 22.90 4.20 -2 -2 18 14.00 3.50 2 -2 -18 11.90 2.90 -2 2 18 12.80 3.60 2 2 -18 9.50 3.00 1 -2 -18 5.20 2.90 -1 -2 18 9.60 3.40 1 -2 -18 7.50 2.40 1 2 -18 4.60 3.00 1 2 -18 9.10 3.00 -1 2 18 3.60 2.50 -4 -3 18 12.50 4.50 -4 3 18 18.50 5.20 -3 -3 18 3.90 3.00 -3 -3 18 0.20 2.30 3 -3 -18 2.30 1.80 -3 3 18 0.70 1.90 -3 3 18 -0.30 2.50 3 3 -18 3.50 2.40 2 -3 -18 7.70 2.60 -2 -3 18 6.20 2.90 2 -3 -18 6.80 3.20 -2 3 18 2.60 2.20 2 3 -18 6.20 3.60 2 3 -18 3.10 2.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 97398 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.61799(12) 1.24804(11) -0.09272(9) 0.0161(3) Uani 1 1 d . . . . . O6 O 0.87879(12) 0.75389(10) -0.41539(9) 0.0154(3) Uani 1 1 d . . . . . O2 O 0.83587(13) 1.19216(13) -0.04709(9) 0.0213(3) Uani 1 1 d . . . . . O5 O 0.66758(13) 0.68880(13) -0.47462(9) 0.0212(3) Uani 1 1 d . . . . . O3 O 0.46564(13) 1.16873(12) -0.24874(9) 0.0192(3) Uani 1 1 d . . . . . O4 O 0.94158(13) 1.06147(14) -0.15893(12) 0.0272(3) Uani 1 1 d . . . . . O8 O 1.01106(13) 0.69017(12) -0.24597(9) 0.0211(3) Uani 1 1 d . . . . . O7 O 0.55837(14) 0.54263(14) -0.37842(12) 0.0278(3) Uani 1 1 d . . . . . N3 N 0.34980(15) 0.83113(13) -0.09193(11) 0.0155(3) Uani 1 1 d . . . . . N1 N 0.86398(15) 0.81797(13) 0.39493(11) 0.0146(3) Uani 1 1 d . . . . . N4 N 0.77241(16) 0.84963(15) 0.10730(12) 0.0221(4) Uani 1 1 d . . . . . N2 N 1.26491(16) 0.84807(15) 0.61800(12) 0.0220(4) Uani 1 1 d . . . . . C21 C 0.77450(17) 0.69215(16) -0.40799(12) 0.0140(3) Uani 1 1 d . . . . . C28 C 0.72240(17) 1.19043(16) -0.10694(12) 0.0146(3) Uani 1 1 d . . . . . C22 C 0.78352(17) 0.62072(16) -0.31745(12) 0.0141(3) Uani 1 1 d . . . . . C34 C 0.57715(17) 1.11057(15) -0.26453(12) 0.0146(3) Uani 1 1 d . . . . . C29 C 0.70532(17) 1.12004(16) -0.19877(13) 0.0138(3) Uani 1 1 d . . . . . C30 C 0.81729(18) 1.05699(17) -0.22009(14) 0.0185(4) Uani 1 1 d . . . . . C14 C 0.60249(18) 0.87974(16) -0.04320(13) 0.0164(4) Uani 1 1 d . . . . . C4 C 1.11251(18) 0.86779(16) 0.45837(13) 0.0154(3) Uani 1 1 d . . . . . C27 C 0.67370(18) 0.54723(16) -0.30756(14) 0.0188(4) Uani 1 1 d . . . . . C23 C 0.90289(18) 0.62091(15) -0.24135(13) 0.0156(3) Uani 1 1 d . . . . . C5 C 1.14521(18) 0.88038(17) 0.56078(13) 0.0176(4) Uani 1 1 d . . . . . H5 H 1.079792 0.913339 0.591455 0.021 Uiso 1 1 calc R U . . . C6 C 0.97657(17) 0.90710(15) 0.39720(12) 0.0148(3) Uani 1 1 d . . . . . H6 H 0.987848 0.919766 0.329225 0.018 Uiso 1 1 calc R U . . . C15 C 0.64591(18) 0.88000(17) 0.05952(13) 0.0177(4) Uani 1 1 d . . . . . H15 H 0.583314 0.902615 0.097264 0.021 Uiso 1 1 calc R U . . . C16 C 0.46095(18) 0.92021(16) -0.09294(13) 0.0159(4) Uani 1 1 d . . . . . H16 H 0.461928 0.938907 -0.161956 0.019 Uiso 1 1 calc R U . . . C11 C 0.86063(18) 0.81780(17) 0.05111(15) 0.0227(4) Uani 1 1 d . . . . . H11 H 0.949227 0.797644 0.082744 0.027 Uiso 1 1 calc R U . . . C2 C 1.33733(19) 0.78678(18) 0.47075(15) 0.0240(4) Uani 1 1 d . . . . . H2 H 1.405414 0.755075 0.441993 0.029 Uiso 1 1 calc R U . . . C13 C 0.69653(19) 0.84488(17) -0.09881(14) 0.0203(4) Uani 1 1 d . . . . . H13 H 0.671635 0.842844 -0.167487 0.024 Uiso 1 1 calc R U . . . C9 C 0.73042(18) 0.88114(16) 0.35374(14) 0.0186(4) Uani 1 1 d . . . . . H9A H 0.660598 0.860154 0.390091 0.022 Uiso 1 1 calc R U . . . H9B H 0.697387 0.862295 0.284487 0.022 Uiso 1 1 calc R U . . . C31 C 0.8008(2) 0.98708(17) -0.30371(15) 0.0228(4) Uani 1 1 d . . . . . H31 H 0.874894 0.946045 -0.317496 0.027 Uiso 1 1 calc R U . . . C1 C 1.35828(18) 0.80232(17) 0.57178(15) 0.0224(4) Uani 1 1 d . . . . . H1A H 1.442194 0.779729 0.610167 0.027 Uiso 1 1 calc R U . . . C3 C 1.21180(18) 0.81975(17) 0.41312(13) 0.0196(4) Uani 1 1 d . . . . . H3A H 1.194301 0.809796 0.344867 0.023 Uiso 1 1 calc R U . . . C19 C 0.21620(18) 0.89606(17) -0.12429(14) 0.0204(4) Uani 1 1 d . . . . . H19A H 0.147558 0.867347 -0.089814 0.024 Uiso 1 1 calc R U . . . H19B H 0.181808 0.887581 -0.194928 0.024 Uiso 1 1 calc R U . . . C17 C 0.40252(18) 1.02385(16) -0.04697(14) 0.0183(4) Uani 1 1 d . . . . . H17A H 0.446534 1.095188 -0.060516 0.022 Uiso 1 1 calc R U . . . H17B H 0.414047 1.014560 0.024038 0.022 Uiso 1 1 calc R U . . . C12 C 0.8279(2) 0.81313(18) -0.05106(16) 0.0251(4) Uani 1 1 d . . . . . H12 H 0.892249 0.789307 -0.086887 0.030 Uiso 1 1 calc R U . . . C18 C 0.25041(19) 1.02346(17) -0.09754(14) 0.0222(4) Uani 1 1 d . . . . . H18A H 0.234651 1.071277 -0.156513 0.027 Uiso 1 1 calc R U . . . H18B H 0.194600 1.052345 -0.053058 0.027 Uiso 1 1 calc R U . . . C7 C 0.90962(18) 1.01423(16) 0.43046(14) 0.0203(4) Uani 1 1 d . . . . . H7A H 0.957152 1.084170 0.417989 0.024 Uiso 1 1 calc R U . . . H7B H 0.907602 1.010227 0.500253 0.024 Uiso 1 1 calc R U . . . C25 C 0.8035(2) 0.47720(17) -0.15287(14) 0.0235(4) Uani 1 1 d . . . . . H25 H 0.810533 0.428358 -0.098546 0.028 Uiso 1 1 calc R U . . . C32 C 0.6731(2) 0.97913(17) -0.36627(14) 0.0223(4) Uani 1 1 d . . . . . H32 H 0.662390 0.931964 -0.421890 0.027 Uiso 1 1 calc R U . . . C33 C 0.5609(2) 1.03952(16) -0.34817(13) 0.0199(4) Uani 1 1 d . . . . . H33 H 0.475964 1.032978 -0.390987 0.024 Uiso 1 1 calc R U . . . C24 C 0.9127(2) 0.54871(17) -0.15904(13) 0.0206(4) Uani 1 1 d . . . . . H24 H 0.991387 0.548733 -0.109222 0.025 Uiso 1 1 calc R U . . . C26 C 0.6838(2) 0.47593(17) -0.22497(15) 0.0237(4) Uani 1 1 d . . . . . H26 H 0.611228 0.428123 -0.218330 0.028 Uiso 1 1 calc R U . . . C20 C 0.3587(2) 0.72520(17) -0.15076(13) 0.0219(4) Uani 1 1 d . . . . . H20A H 0.347307 0.745357 -0.219376 0.033 Uiso 1 1 calc R U . . . H20B H 0.287814 0.672097 -0.142529 0.033 Uiso 1 1 calc R U . . . H20C H 0.446646 0.689515 -0.128483 0.033 Uiso 1 1 calc R U . . . C10 C 0.8801(2) 0.70957(16) 0.34126(13) 0.0207(4) Uani 1 1 d . . . . . H10A H 0.878468 0.726935 0.273085 0.031 Uiso 1 1 calc R U . . . H10B H 0.806391 0.657644 0.345506 0.031 Uiso 1 1 calc R U . . . H10C H 0.965994 0.673878 0.370391 0.031 Uiso 1 1 calc R U . . . C8 C 0.7648(2) 1.00969(17) 0.36630(16) 0.0268(4) Uani 1 1 d . . . . . H8A H 0.700201 1.049046 0.398648 0.032 Uiso 1 1 calc R U . . . H8B H 0.762364 1.045877 0.302616 0.032 Uiso 1 1 calc R U . . . H1 H 0.864(3) 0.797(3) 0.461(2) 0.040 Uiso 1 1 d . U . . . H3 H 0.359(3) 0.806(3) -0.028(2) 0.040 Uiso 1 1 d . U . . . H4 H 0.927(3) 1.106(3) -0.1056(19) 0.040 Uiso 1 1 d . U . . . H8 H 0.983(3) 0.725(2) -0.305(2) 0.040 Uiso 1 1 d . U . . . H3B H 0.500(3) 1.211(3) -0.1893(19) 0.040 Uiso 1 1 d . U . . . H7 H 0.575(3) 0.594(3) -0.4229(19) 0.040 Uiso 1 1 d . U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0158(6) 0.0168(6) 0.0165(6) -0.0016(5) 0.0050(5) 0.0008(5) O6 0.0155(6) 0.0152(6) 0.0159(6) 0.0008(5) 0.0041(5) -0.0014(5) O2 0.0166(6) 0.0237(7) 0.0214(6) -0.0038(6) -0.0012(5) -0.0007(5) O5 0.0174(6) 0.0241(7) 0.0199(6) 0.0041(6) -0.0015(5) -0.0015(5) O3 0.0152(6) 0.0225(7) 0.0180(6) -0.0032(5) -0.0012(5) 0.0045(5) O4 0.0129(6) 0.0295(8) 0.0383(8) -0.0088(7) 0.0033(6) 0.0033(6) O8 0.0204(6) 0.0236(8) 0.0167(6) 0.0021(6) -0.0021(5) -0.0061(6) O7 0.0159(6) 0.0289(8) 0.0372(8) 0.0090(7) 0.0022(6) -0.0050(6) N3 0.0163(7) 0.0159(8) 0.0129(7) 0.0021(6) -0.0003(6) -0.0031(6) N1 0.0152(7) 0.0143(7) 0.0134(7) 0.0018(6) 0.0007(5) -0.0023(6) N4 0.0163(8) 0.0244(9) 0.0241(8) 0.0051(7) 0.0007(6) 0.0005(6) N2 0.0186(8) 0.0263(9) 0.0191(7) 0.0021(6) -0.0004(6) -0.0034(7) C21 0.0146(8) 0.0122(8) 0.0159(8) -0.0008(7) 0.0049(6) 0.0016(7) C28 0.0164(8) 0.0120(8) 0.0157(8) 0.0021(7) 0.0040(6) -0.0018(7) C22 0.0157(8) 0.0121(8) 0.0153(8) 0.0005(6) 0.0052(6) 0.0022(6) C34 0.0179(8) 0.0130(8) 0.0134(8) 0.0030(6) 0.0041(6) 0.0006(7) C29 0.0146(8) 0.0123(8) 0.0151(8) 0.0006(6) 0.0047(6) -0.0010(6) C30 0.0154(8) 0.0165(9) 0.0252(9) -0.0001(7) 0.0078(7) 0.0004(7) C14 0.0155(8) 0.0156(9) 0.0182(8) 0.0026(7) 0.0043(7) -0.0031(7) C4 0.0146(8) 0.0150(9) 0.0167(8) 0.0023(6) 0.0036(6) -0.0035(7) C27 0.0161(8) 0.0173(9) 0.0240(9) 0.0020(7) 0.0069(7) 0.0001(7) C23 0.0191(8) 0.0131(8) 0.0147(8) -0.0022(6) 0.0037(7) 0.0016(7) C5 0.0152(8) 0.0207(9) 0.0171(8) -0.0001(7) 0.0039(7) -0.0018(7) C6 0.0157(8) 0.0144(8) 0.0143(8) 0.0024(6) 0.0035(6) -0.0024(7) C15 0.0140(8) 0.0217(10) 0.0175(8) 0.0015(7) 0.0035(7) 0.0001(7) C16 0.0168(8) 0.0172(9) 0.0129(8) 0.0037(6) 0.0015(6) -0.0035(7) C11 0.0130(8) 0.0191(10) 0.0359(11) 0.0001(8) 0.0047(8) -0.0003(7) C2 0.0186(9) 0.0216(10) 0.0332(10) -0.0026(8) 0.0085(8) 0.0009(8) C13 0.0220(9) 0.0203(10) 0.0200(9) -0.0022(7) 0.0077(7) -0.0065(7) C9 0.0137(8) 0.0204(10) 0.0194(8) 0.0043(7) -0.0016(7) 0.0004(7) C31 0.0243(10) 0.0197(10) 0.0287(10) -0.0031(8) 0.0151(8) 0.0012(8) C1 0.0145(8) 0.0203(10) 0.0299(10) 0.0017(8) -0.0011(7) 0.0005(7) C3 0.0203(9) 0.0201(10) 0.0189(8) -0.0026(7) 0.0056(7) -0.0027(7) C19 0.0151(8) 0.0211(10) 0.0221(9) 0.0036(7) -0.0028(7) -0.0010(7) C17 0.0163(8) 0.0155(9) 0.0212(9) 0.0031(7) -0.0007(7) -0.0022(7) C12 0.0200(9) 0.0219(10) 0.0367(11) -0.0062(8) 0.0137(8) -0.0020(8) C18 0.0179(9) 0.0195(10) 0.0260(9) 0.0065(8) -0.0025(7) 0.0004(7) C7 0.0174(9) 0.0154(9) 0.0281(9) 0.0024(8) 0.0048(7) -0.0009(7) C25 0.0365(11) 0.0188(10) 0.0184(9) 0.0058(7) 0.0128(8) 0.0036(8) C32 0.0346(11) 0.0174(9) 0.0173(8) -0.0039(7) 0.0113(8) -0.0019(8) C33 0.0247(9) 0.0188(10) 0.0148(8) -0.0005(7) 0.0006(7) -0.0018(8) C24 0.0280(10) 0.0194(10) 0.0137(8) 0.0007(7) 0.0030(7) 0.0024(8) C26 0.0253(10) 0.0186(10) 0.0306(10) 0.0055(8) 0.0133(8) -0.0019(8) C20 0.0251(10) 0.0211(10) 0.0172(9) -0.0031(7) -0.0008(7) -0.0033(8) C10 0.0240(9) 0.0163(9) 0.0196(8) -0.0021(7) -0.0003(7) -0.0014(7) C8 0.0182(9) 0.0200(10) 0.0402(12) 0.0090(9) 0.0017(8) 0.0018(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C34 O3 H3B 103.1(16) . . ? C30 O4 H4 104.0(16) . . ? C23 O8 H8 101.8(17) . . ? C27 O7 H7 102.9(16) . . ? C16 N3 H3 107.3(18) . . ? C19 N3 C16 105.14(13) . . ? C19 N3 H3 110.4(17) . . ? C20 N3 C16 115.39(14) . . ? C20 N3 C19 113.36(14) . . ? C20 N3 H3 105.2(18) . . ? C6 N1 C9 105.55(13) . . ? C6 N1 H1 107.5(17) . . ? C9 N1 H1 108.2(16) . . ? C10 N1 C6 115.26(14) . . ? C10 N1 C9 113.32(14) . . ? C10 N1 H1 106.7(18) . . ? C11 N4 C15 116.70(17) . . ? C5 N2 C1 116.71(16) . . ? O6 C21 C22 117.90(15) . . ? O5 C21 O6 122.50(16) . . ? O5 C21 C22 119.59(16) . . ? O1 C28 C29 117.46(15) . . ? O2 C28 O1 122.62(16) . . ? O2 C28 C29 119.92(15) . . ? C27 C22 C21 120.14(15) . . ? C27 C22 C23 118.53(16) . . ? C23 C22 C21 121.29(15) . . ? O3 C34 C29 121.45(15) . . ? O3 C34 C33 117.78(15) . . ? C33 C34 C29 120.77(16) . . ? C34 C29 C28 121.34(15) . . ? C34 C29 C30 118.34(16) . . ? C30 C29 C28 120.27(15) . . ? O4 C30 C29 120.80(16) . . ? O4 C30 C31 118.52(16) . . ? C31 C30 C29 120.66(17) . . ? C15 C14 C16 121.70(16) . . ? C13 C14 C15 117.45(17) . . ? C13 C14 C16 120.80(16) . . ? C5 C4 C6 122.06(16) . . ? C3 C4 C5 117.41(16) . . ? C3 C4 C6 120.51(15) . . ? O7 C27 C22 120.95(16) . . ? O7 C27 C26 118.51(16) . . ? C26 C27 C22 120.53(17) . . ? O8 C23 C22 121.37(15) . . ? O8 C23 C24 117.98(16) . . ? C24 C23 C22 120.65(17) . . ? N2 C5 C4 124.21(17) . . ? N2 C5 H5 117.9 . . ? C4 C5 H5 117.9 . . ? N1 C6 H6 108.2 . . ? N1 C6 C7 100.89(13) . . ? C4 C6 N1 112.40(14) . . ? C4 C6 H6 108.2 . . ? C4 C6 C7 118.32(15) . . ? C7 C6 H6 108.2 . . ? N4 C15 C14 124.10(17) . . ? N4 C15 H15 118.0 . . ? C14 C15 H15 118.0 . . ? N3 C16 H16 108.3 . . ? N3 C16 C17 100.71(13) . . ? C14 C16 N3 113.69(14) . . ? C14 C16 H16 108.3 . . ? C14 C16 C17 117.06(15) . . ? C17 C16 H16 108.3 . . ? N4 C11 H11 118.0 . . ? N4 C11 C12 123.94(17) . . ? C12 C11 H11 118.0 . . ? C1 C2 H2 120.9 . . ? C1 C2 C3 118.24(18) . . ? C3 C2 H2 120.9 . . ? C14 C13 H13 120.3 . . ? C12 C13 C14 119.47(17) . . ? C12 C13 H13 120.3 . . ? N1 C9 H9A 110.7 . . ? N1 C9 H9B 110.7 . . ? N1 C9 C8 105.42(14) . . ? H9A C9 H9B 108.8 . . ? C8 C9 H9A 110.7 . . ? C8 C9 H9B 110.7 . . ? C30 C31 H31 120.3 . . ? C32 C31 C30 119.42(17) . . ? C32 C31 H31 120.3 . . ? N2 C1 C2 123.97(17) . . ? N2 C1 H1A 118.0 . . ? C2 C1 H1A 118.0 . . ? C4 C3 H3A 120.3 . . ? C2 C3 C4 119.45(16) . . ? C2 C3 H3A 120.3 . . ? N3 C19 H19A 110.7 . . ? N3 C19 H19B 110.7 . . ? N3 C19 C18 105.41(14) . . ? H19A C19 H19B 108.8 . . ? C18 C19 H19A 110.7 . . ? C18 C19 H19B 110.7 . . ? C16 C17 H17A 111.0 . . ? C16 C17 H17B 111.0 . . ? C16 C17 C18 103.60(15) . . ? H17A C17 H17B 109.0 . . ? C18 C17 H17A 111.0 . . ? C18 C17 H17B 111.0 . . ? C11 C12 C13 118.34(17) . . ? C11 C12 H12 120.8 . . ? C13 C12 H12 120.8 . . ? C19 C18 H18A 110.7 . . ? C19 C18 H18B 110.7 . . ? C17 C18 C19 105.15(15) . . ? C17 C18 H18A 110.7 . . ? C17 C18 H18B 110.7 . . ? H18A C18 H18B 108.8 . . ? C6 C7 H7A 111.3 . . ? C6 C7 H7B 111.3 . . ? C6 C7 C8 102.55(15) . . ? H7A C7 H7B 109.2 . . ? C8 C7 H7A 111.3 . . ? C8 C7 H7B 111.3 . . ? C24 C25 H25 118.9 . . ? C24 C25 C26 122.18(17) . . ? C26 C25 H25 118.9 . . ? C31 C32 H32 119.1 . . ? C33 C32 C31 121.73(17) . . ? C33 C32 H32 119.1 . . ? C34 C33 H33 120.5 . . ? C32 C33 C34 119.08(17) . . ? C32 C33 H33 120.5 . . ? C23 C24 H24 120.5 . . ? C25 C24 C23 118.93(17) . . ? C25 C24 H24 120.5 . . ? C27 C26 H26 120.4 . . ? C25 C26 C27 119.17(17) . . ? C25 C26 H26 120.4 . . ? N3 C20 H20A 109.5 . . ? N3 C20 H20B 109.5 . . ? N3 C20 H20C 109.5 . . ? H20A C20 H20B 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? N1 C10 H10A 109.5 . . ? N1 C10 H10B 109.5 . . ? N1 C10 H10C 109.5 . . ? H10A C10 H10B 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C9 C8 C7 105.18(15) . . ? C9 C8 H8A 110.7 . . ? C9 C8 H8B 110.7 . . ? C7 C8 H8A 110.7 . . ? C7 C8 H8B 110.7 . . ? H8A C8 H8B 108.8 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C28 1.284(2) . ? O6 C21 1.282(2) . ? O2 C28 1.255(2) . ? O5 C21 1.256(2) . ? O3 C34 1.355(2) . ? O3 H3B 0.95(3) . ? O4 C30 1.348(2) . ? O4 H4 0.93(3) . ? O8 C23 1.355(2) . ? O8 H8 0.90(3) . ? O7 C27 1.347(2) . ? O7 H7 0.90(3) . ? N3 C16 1.514(2) . ? N3 C19 1.513(2) . ? N3 C20 1.482(2) . ? N3 H3 0.92(3) . ? N1 C6 1.519(2) . ? N1 C9 1.521(2) . ? N1 C10 1.481(2) . ? N1 H1 0.94(3) . ? N4 C15 1.343(2) . ? N4 C11 1.340(3) . ? N2 C5 1.340(2) . ? N2 C1 1.342(3) . ? C21 C22 1.486(2) . ? C28 C29 1.487(2) . ? C22 C27 1.414(2) . ? C22 C23 1.415(2) . ? C34 C29 1.410(2) . ? C34 C33 1.399(2) . ? C29 C30 1.414(2) . ? C30 C31 1.391(3) . ? C14 C15 1.395(2) . ? C14 C16 1.510(2) . ? C14 C13 1.390(3) . ? C4 C5 1.392(2) . ? C4 C6 1.510(2) . ? C4 C3 1.391(3) . ? C27 C26 1.394(3) . ? C23 C24 1.397(2) . ? C5 H5 0.9300 . ? C6 H6 0.9800 . ? C6 C7 1.522(3) . ? C15 H15 0.9300 . ? C16 H16 0.9800 . ? C16 C17 1.526(3) . ? C11 H11 0.9300 . ? C11 C12 1.383(3) . ? C2 H2 0.9300 . ? C2 C1 1.380(3) . ? C2 C3 1.390(3) . ? C13 H13 0.9300 . ? C13 C12 1.387(3) . ? C9 H9A 0.9700 . ? C9 H9B 0.9700 . ? C9 C8 1.526(3) . ? C31 H31 0.9300 . ? C31 C32 1.386(3) . ? C1 H1A 0.9300 . ? C3 H3A 0.9300 . ? C19 H19A 0.9700 . ? C19 H19B 0.9700 . ? C19 C18 1.538(3) . ? C17 H17A 0.9700 . ? C17 H17B 0.9700 . ? C17 C18 1.532(2) . ? C12 H12 0.9300 . ? C18 H18A 0.9700 . ? C18 H18B 0.9700 . ? C7 H7A 0.9700 . ? C7 H7B 0.9700 . ? C7 C8 1.530(3) . ? C25 H25 0.9300 . ? C25 C24 1.384(3) . ? C25 C26 1.386(3) . ? C32 H32 0.9300 . ? C32 C33 1.384(3) . ? C33 H33 0.9300 . ? C24 H24 0.9300 . ? C26 H26 0.9300 . ? C20 H20A 0.9600 . ? C20 H20B 0.9600 . ? C20 H20C 0.9600 . ? C10 H10A 0.9600 . ? C10 H10B 0.9600 . ? C10 H10C 0.9600 . ? C8 H8A 0.9700 . ? C8 H8B 0.9700 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag C11 H11 O2 0.93 2.60 3.367(2) 140.2 2_745 yes C31 H31 O6 0.93 2.60 3.278(2) 129.7 . yes C17 H17A O1 0.97 2.56 3.505(2) 164.7 . yes C7 H7A O6 0.97 2.56 3.513(2) 168.0 2_755 yes C20 H20A N2 0.96 2.52 3.444(2) 160.7 1_454 yes C8 H8A O7 0.97 2.54 3.283(2) 133.8 2_655 yes N1 H1 O6 0.94(3) 1.76(3) 2.6981(19) 175(2) 1_556 yes N1 H1 O5 0.94(3) 2.63(3) 3.283(2) 127(2) 1_556 yes N3 H3 O1 0.92(3) 1.77(3) 2.6825(19) 176(3) 2_645 yes O4 H4 O2 0.93(3) 1.67(3) 2.5408(19) 154(2) . yes O8 H8 O6 0.90(3) 1.69(3) 2.5454(17) 157(3) . yes O3 H3B O1 0.95(3) 1.64(3) 2.5364(17) 155(2) . yes O7 H7 O5 0.90(3) 1.68(3) 2.531(2) 157(2) . yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C28 C29 C34 -4.2(2) . . . . ? O1 C28 C29 C30 178.36(16) . . . . ? O6 C21 C22 C27 -177.23(16) . . . . ? O6 C21 C22 C23 0.3(2) . . . . ? O2 C28 C29 C34 176.09(16) . . . . ? O2 C28 C29 C30 -1.4(3) . . . . ? O5 C21 C22 C27 1.6(3) . . . . ? O5 C21 C22 C23 179.13(16) . . . . ? O3 C34 C29 C28 2.6(3) . . . . ? O3 C34 C29 C30 -179.87(16) . . . . ? O3 C34 C33 C32 179.93(17) . . . . ? O4 C30 C31 C32 178.47(17) . . . . ? O8 C23 C24 C25 -179.94(17) . . . . ? O7 C27 C26 C25 178.11(17) . . . . ? N3 C16 C17 C18 -43.02(16) . . . . ? N3 C19 C18 C17 -2.2(2) . . . . ? N1 C6 C7 C8 -44.77(17) . . . . ? N1 C9 C8 C7 -9.7(2) . . . . ? N4 C11 C12 C13 1.0(3) . . . . ? C21 C22 C27 O7 -1.6(3) . . . . ? C21 C22 C27 C26 177.02(17) . . . . ? C21 C22 C23 O8 3.1(3) . . . . ? C21 C22 C23 C24 -176.60(17) . . . . ? C28 C29 C30 O4 -1.4(3) . . . . ? C28 C29 C30 C31 177.29(17) . . . . ? C22 C27 C26 C25 -0.5(3) . . . . ? C22 C23 C24 C25 -0.3(3) . . . . ? C34 C29 C30 O4 -178.96(16) . . . . ? C34 C29 C30 C31 -0.3(3) . . . . ? C29 C34 C33 C32 -0.6(3) . . . . ? C29 C30 C31 C32 -0.2(3) . . . . ? C30 C31 C32 C33 0.3(3) . . . . ? C14 C16 C17 C18 -166.79(15) . . . . ? C14 C13 C12 C11 -0.2(3) . . . . ? C4 C6 C7 C8 -167.75(15) . . . . ? C27 C22 C23 O8 -179.35(17) . . . . ? C27 C22 C23 C24 1.0(3) . . . . ? C23 C22 C27 O7 -179.18(16) . . . . ? C23 C22 C27 C26 -0.6(3) . . . . ? C5 N2 C1 C2 -0.3(3) . . . . ? C5 C4 C6 N1 -83.1(2) . . . . ? C5 C4 C6 C7 33.9(2) . . . . ? C5 C4 C3 C2 0.0(3) . . . . ? C6 N1 C9 C8 -18.43(18) . . . . ? C6 C4 C5 N2 -179.21(17) . . . . ? C6 C4 C3 C2 178.47(17) . . . . ? C6 C7 C8 C9 34.05(19) . . . . ? C15 N4 C11 C12 -1.0(3) . . . . ? C15 C14 C16 N3 -79.2(2) . . . . ? C15 C14 C16 C17 37.7(2) . . . . ? C15 C14 C13 C12 -0.5(3) . . . . ? C16 N3 C19 C18 -25.01(18) . . . . ? C16 C14 C15 N4 -177.04(18) . . . . ? C16 C14 C13 C12 177.08(17) . . . . ? C16 C17 C18 C19 28.16(18) . . . . ? C11 N4 C15 C14 0.2(3) . . . . ? C13 C14 C15 N4 0.5(3) . . . . ? C13 C14 C16 N3 103.34(19) . . . . ? C13 C14 C16 C17 -139.79(18) . . . . ? C9 N1 C6 C4 166.26(14) . . . . ? C9 N1 C6 C7 39.27(16) . . . . ? C31 C32 C33 C34 0.1(3) . . . . ? C1 N2 C5 C4 0.9(3) . . . . ? C1 C2 C3 C4 0.5(3) . . . . ? C3 C4 C5 N2 -0.8(3) . . . . ? C3 C4 C6 N1 98.57(19) . . . . ? C3 C4 C6 C7 -144.42(17) . . . . ? C3 C2 C1 N2 -0.4(3) . . . . ? C19 N3 C16 C14 168.22(15) . . . . ? C19 N3 C16 C17 42.16(16) . . . . ? C33 C34 C29 C28 -176.83(17) . . . . ? C33 C34 C29 C30 0.7(3) . . . . ? C24 C25 C26 C27 1.3(3) . . . . ? C26 C25 C24 C23 -0.9(3) . . . . ? C20 N3 C16 C14 -66.11(19) . . . . ? C20 N3 C16 C17 167.83(14) . . . . ? C20 N3 C19 C18 -151.93(15) . . . . ? C10 N1 C6 C4 -67.89(18) . . . . ? C10 N1 C6 C7 165.12(14) . . . . ? C10 N1 C9 C8 -145.47(16) . . . . ?