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Information card for entry 7246511
Preview
| Coordinates | 7246511.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C28 H26 N4 Ni O8 |
|---|---|
| Calculated formula | C28 H23.9998 N4 Ni O8 |
| Title of publication | Square-planar and octahedral nickel complexes of an acylhydrazone ligand and the serendipitous isolation of a potential octahedral nickel acylhydrazone precursor |
| Authors of publication | Carballo, Rosa; Lago, Ana Belén; Vázquez-Toirán, María; Estévez, Laura; Vázquez-López, Ezequiel M. |
| Journal of publication | CrystEngComm |
| Year of publication | 2023 |
| Journal volume | 25 |
| Journal issue | 16 |
| Pages of publication | 2463 - 2472 |
| a | 20.668 ± 0.0018 Å |
| b | 5.9629 ± 0.0005 Å |
| c | 23.892 ± 0.002 Å |
| α | 90° |
| β | 103.289 ± 0.003° |
| γ | 90° |
| Cell volume | 2865.6 ± 0.4 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0735 |
| Residual factor for significantly intense reflections | 0.0556 |
| Weighted residual factors for significantly intense reflections | 0.1314 |
| Weighted residual factors for all reflections included in the refinement | 0.1414 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.039 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 283207 (current) | 2023-05-05 | cif/ Updating files of 7246508, 7246509, 7246510, 7246511 Original log message: Adding full bibliography for 7246508--7246511.cif. |
7246511.cif |
| 282094 | 2023-03-29 | cif/ Adding structures of 7246508, 7246509, 7246510, 7246511 via cif-deposit CGI script. |
7246511.cif |
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Users of the data should acknowledge the original authors of the
structural data.