#------------------------------------------------------------------------------ #$Date: 2023-11-10 04:00:10 +0200 (Fri, 10 Nov 2023) $ #$Revision: 287506 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/76/7247692.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7247692 loop_ _publ_author_name 'Atceken, Nurunnisa' 'Hemingway, Jack' 'Bull, Craig L.' 'Liu, Xiaojiao' 'Michalchuk, Adam A.L.' 'Konar, Sumit' 'Morrison, Carole' 'Pulham, Colin R.' _publ_section_title ; High-pressure Structural Studies and Pressure-induced Sensitisation of 3,4,5-trinitro-1H-pyrazole ; _journal_name_full 'Physical Chemistry Chemical Physics' _journal_paper_doi 10.1039/D3CP04526A _journal_year 2023 _chemical_formula_moiety '3(C3 N5 O6)' _chemical_formula_sum 'C9 N15 O18' _chemical_formula_weight 606.24 _space_group_crystal_system monoclinic _space_group_IT_number 9 _space_group_name_Hall 'C -2yc' _space_group_name_H-M_alt 'C 1 c 1' _atom_sites_solution_primary dual _audit_block_doi 10.5517/ccdc.csd.cc29gp2k _audit_creation_date 2021-12-16 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408) ; _audit_update_record ; 2021-12-16 deposited with the CCDC. 2023-11-08 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 127.661(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 19.5713(11) _cell_length_b 7.6509(8) _cell_length_c 14.6982(9) _cell_measurement_reflns_used 2276 _cell_measurement_temperature 298.4 _cell_measurement_theta_max 25.99 _cell_measurement_theta_min 2.81 _cell_volume 1742.3(2) _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 298.4 _diffrn_measured_fraction_theta_full 0.546 _diffrn_measured_fraction_theta_max 0.503 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0326 _diffrn_reflns_av_unetI/netI 0.0414 _diffrn_reflns_Laue_measured_fraction_full 0.546 _diffrn_reflns_Laue_measured_fraction_max 0.503 _diffrn_reflns_limit_h_max 23 _diffrn_reflns_limit_h_min -24 _diffrn_reflns_limit_k_max 6 _diffrn_reflns_limit_k_min -6 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 4862 _diffrn_reflns_point_group_measured_fraction_full 0.510 _diffrn_reflns_point_group_measured_fraction_max 0.464 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.379 _diffrn_reflns_theta_min 2.629 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.226 _exptl_absorpt_correction_T_max 0.7454 _exptl_absorpt_correction_T_min 0.6498 _exptl_absorpt_correction_type multi-scan _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 2.311 _exptl_crystal_description block _exptl_crystal_F_000 1212 _refine_diff_density_max 0.172 _refine_diff_density_min -0.193 _refine_diff_density_rms 0.044 _refine_ls_abs_structure_details ; Flack x determined using 637 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -4.5(10) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.069 _refine_ls_hydrogen_treatment undef _refine_ls_matrix_type full _refine_ls_number_parameters 379 _refine_ls_number_reflns 1652 _refine_ls_number_restraints 308 _refine_ls_restrained_S_all 0.978 _refine_ls_R_factor_all 0.0458 _refine_ls_R_factor_gt 0.0399 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0834P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1013 _refine_ls_wR_factor_ref 0.1053 _reflns_Friedel_coverage 0.844 _reflns_Friedel_fraction_full 0.473 _reflns_Friedel_fraction_max 0.425 _reflns_number_gt 1493 _reflns_number_total 1652 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d3cp04526a2.cif _cod_data_source_block 2tnp_p08_cc _cod_database_code 7247692 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Rigid body (RIGU) restrains All non-hydrogen atoms with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 ; _shelx_res_file ; TITL 2tnp_p08_cc_a.res in Cc 2tnp_p08_cc.res created by SHELXL-2018/3 at 15:47:17 on 28-Jul-2020 REM Old TITL 2tnp_p08_cc_a.res in Cc REM SHELXT solution in Cc REM R1 0.225, Rweak 0.041, Alpha 0.066, Orientation as input REM Flack x = -0.400 ( 1.238 ) from Parsons' quotients REM Formula found by SHELXT: C23 N5 O8 CELL 0.71073 19.5713 7.6509 14.6982 90 127.661 90 ZERR 4 0.0011 0.0008 0.0009 0 0.002 0 LATT -7 SYMM +X,-Y,0.5+Z SFAC C N O UNIT 36 60 72 RIGU L.S. 10 PLAN 20 TEMP 25.25 CONF list 4 MORE -1 fmap 2 53 acta OMIT -2 0 2 REM REM REM WGHT 0.083400 FVAR 0.58552 O001 3 0.663363 0.909722 0.886976 11.00000 0.05240 0.05409 = 0.02910 -0.02044 0.03324 -0.02421 N002 2 0.811643 0.887415 0.790714 11.00000 0.01462 0.00744 = 0.01903 0.00323 0.00708 0.00234 O003 3 0.334164 1.048790 0.151629 11.00000 0.02235 0.02173 = 0.02575 -0.00690 0.01273 -0.00293 O004 3 0.860311 0.832234 0.771380 11.00000 0.01835 0.01004 = 0.03534 -0.00301 0.01846 -0.00363 N005 2 0.486908 0.241894 0.598326 11.00000 0.01915 0.03087 = 0.01576 0.00701 0.00820 -0.00052 N006 2 0.337002 -0.008380 0.421621 11.00000 0.01813 0.03070 = 0.01720 -0.01311 0.00836 -0.00049 O 3 0.821551 1.017230 0.845031 11.00000 0.02310 0.01982 = 0.03100 -0.00949 0.01446 -0.00426 O008 3 0.492749 0.798529 0.665205 11.00000 0.02849 0.05674 = 0.02916 -0.01091 0.02291 -0.00540 O009 3 0.331697 -0.157254 0.450309 11.00000 0.03781 0.02387 = 0.02763 -0.00461 0.01236 0.00565 C00A 1 0.663807 0.831875 0.739105 11.00000 0.01007 0.02005 = 0.00993 -0.00243 0.00204 0.00059 O00B 3 0.506500 0.842933 0.429675 11.00000 0.02725 0.03143 = 0.02602 0.00625 0.01629 -0.00323 N00C 2 0.646495 1.173666 0.560246 11.00000 0.01881 0.00916 = 0.02471 0.00198 0.01385 -0.00173 O00D 3 0.314685 1.334543 0.125601 11.00000 0.02426 0.02029 = 0.04115 0.01456 0.01521 0.00425 O00E 3 0.464226 0.621105 0.530225 11.00000 0.02027 0.01409 = 0.02694 -0.00101 0.00749 -0.00713 C00F 1 0.564260 1.224676 0.452134 11.00000 0.02026 0.01266 = 0.02170 -0.00250 0.01601 -0.00080 O00G 3 0.687310 1.288731 0.630614 11.00000 0.02408 0.01254 = 0.03539 -0.01182 0.01373 -0.00626 O00H 3 0.131516 0.189339 0.425050 11.00000 0.02314 0.02585 = 0.03856 -0.00152 0.02235 0.00356 C00I 1 0.730472 0.794335 0.733322 11.00000 0.01520 0.00877 = 0.01792 0.00504 0.00768 0.00192 N00J 2 0.630245 0.633901 0.612421 11.00000 0.01249 0.01341 = 0.02764 -0.00522 0.01032 0.00044 N00K 2 0.466620 1.393527 0.328701 11.00000 0.01598 0.01029 = 0.02910 -0.00224 0.01104 0.00057 O00L 3 0.491303 0.867130 0.272152 11.00000 0.03695 0.03491 = 0.01826 -0.00845 0.01354 0.00360 O00M 3 0.537628 0.355429 0.663396 11.00000 0.02612 0.02099 = 0.03721 0.00200 0.01101 -0.00645 O00N 3 0.168764 -0.019599 0.362646 11.00000 0.02936 0.02695 = 0.03998 -0.01480 0.01578 0.00051 O00O 3 0.505054 0.111076 0.566199 11.00000 0.02118 0.04766 = 0.03020 -0.00460 0.01828 0.00027 N00P 2 0.661367 0.959914 0.806520 11.00000 0.01183 0.02735 = 0.02250 -0.00325 0.00762 0.00326 N00Q 2 0.498738 0.931046 0.355635 11.00000 0.01277 0.02643 = 0.01677 -0.00225 0.00701 -0.00202 O00R 3 0.667263 1.022546 0.568437 11.00000 0.02344 0.01579 = 0.02499 0.00689 0.01453 0.00205 N00S 2 0.356379 1.200005 0.179973 11.00000 0.01664 0.02500 = 0.01599 0.00333 0.01125 0.00115 N00T 2 0.290368 0.334299 0.539147 11.00000 0.01994 0.02597 = 0.01652 -0.00053 0.00720 0.00414 O00U 3 0.659875 1.112234 0.782708 11.00000 0.03078 0.02804 = 0.02353 -0.00370 0.01003 0.01182 N00V 2 0.711567 0.669955 0.658647 11.00000 0.01696 0.00831 = 0.02962 -0.00657 0.01239 -0.00880 C00W 1 0.599736 0.727308 0.657065 11.00000 0.01292 0.01308 = 0.01435 0.00196 0.00713 0.00083 C00X 1 0.397735 0.255629 0.553515 11.00000 0.02231 0.01894 = 0.02265 0.00422 0.01413 0.00444 O00Y 3 0.345673 0.025886 0.347597 11.00000 0.03154 0.06894 = 0.02788 -0.01402 0.02295 -0.01566 C00Z 1 0.500502 1.115010 0.365223 11.00000 0.02130 0.01454 = 0.01846 0.00211 0.01639 0.00479 N010 2 0.372495 0.376350 0.589779 11.00000 0.02237 0.02304 = 0.02927 0.00213 0.01352 0.00158 N1 2 0.544029 1.387062 0.431974 11.00000 0.01927 0.01438 = 0.02214 0.00049 0.00987 0.00868 C2 1 0.439825 1.233248 0.288234 11.00000 0.01993 0.02039 = 0.01622 0.00157 0.01330 -0.00040 N3 2 0.511564 0.712560 0.613971 11.00000 0.01636 0.02431 = 0.01788 0.00281 0.01063 -0.00132 N4 2 0.182465 0.115942 0.417033 11.00000 0.01975 0.01437 = 0.02629 0.00201 0.01345 -0.00029 C5 1 0.334714 0.136197 0.480984 11.00000 0.02439 0.01583 = 0.02013 0.00448 0.01569 0.00403 C6 1 0.266458 0.191828 0.474805 11.00000 0.01956 0.01756 = 0.01747 0.00247 0.01167 0.00188 HKLF 4 REM 2tnp_p08_cc_a.res in Cc REM wR2 = 0.105304, GooF = S = 1.06884, Restrained GooF = 0.97839 for all data REM R1 = 0.039863 for 1493 Fo > 4sig(Fo) and 0.045824 for all 1652 data REM 379 parameters refined using 308 restraints END WGHT 0.0833 0.0000 REM Highest difference peak 0.172, deepest hole -0.193, 1-sigma level 0.044 Q1 1 0.2403 0.4024 0.5253 11.00000 0.05 0.17 Q2 1 0.6610 0.7321 0.5803 11.00000 0.05 0.17 Q3 1 0.4406 1.4777 0.2829 11.00000 0.05 0.17 Q4 1 0.1401 0.3596 0.4147 11.00000 0.05 0.15 Q5 1 0.4959 0.7249 0.2815 11.00000 0.05 0.15 Q6 1 0.7400 0.6246 0.7357 11.00000 0.05 0.15 Q7 1 0.8357 1.0234 0.9463 11.00000 0.05 0.14 Q8 1 0.6944 1.3983 0.5211 11.00000 0.05 0.14 Q9 1 0.4019 1.4110 0.2962 11.00000 0.05 0.14 Q10 1 0.6413 0.9381 0.6655 11.00000 0.05 0.13 Q11 1 0.3480 0.0372 0.2780 11.00000 0.05 0.13 Q12 1 0.8712 0.6666 0.7797 11.00000 0.05 0.13 Q13 1 0.4574 0.8016 0.5178 11.00000 0.05 0.13 Q14 1 0.3582 0.9082 0.2418 11.00000 0.05 0.13 Q15 1 0.5404 1.1573 0.3597 11.00000 0.05 0.13 Q16 1 0.3192 1.3224 0.0581 11.00000 0.05 0.13 Q17 1 0.7290 0.9912 0.9438 11.00000 0.05 0.13 Q18 1 0.4607 1.3200 0.2461 11.00000 0.05 0.12 Q19 1 0.5469 1.5132 0.4104 11.00000 0.05 0.12 Q20 1 0.4534 0.7961 0.6887 11.00000 0.05 0.12 ; _shelx_res_checksum 98048 _shelx_hkl_file ; 2 0 0 55.99 2.40 2 0 0 56.79 4.10 -2 0 0 56.99 2.50 -2 0 0 51.09 3.80 2 0 0 53.49 3.60 2 0 0 58.19 2.70 2 0 0 53.59 2.60 2 0 0 55.49 2.40 -2 0 0 58.99 3.60 -2 0 0 54.79 3.80 -2 0 0 53.59 2.80 -2 0 0 60.29 2.50 -2 0 0 54.29 2.40 4 0 0 152.08 9.20 4 0 0 143.49 6.70 4 0 0 149.88 6.20 -4 0 0 171.18 9.00 -4 0 0 148.59 9.40 -4 0 0 127.59 6.10 -4 0 0 130.09 6.10 -4 0 0 152.08 6.20 -4 0 0 150.68 9.90 4 0 0 141.59 6.80 4 0 0 148.49 6.10 4 0 0 144.69 10.60 8 0 0 93.29 6.00 -8 0 0 96.89 10.70 8 0 0 85.99 6.40 8 0 0 81.89 7.00 -8 0 0 83.99 5.90 -10 0 0 237.68 10.90 10 0 0 199.28 21.40 -10 0 0 208.68 18.90 10 0 0 172.08 24.60 10 0 0 227.38 13.00 10 0 0 219.48 10.80 10 0 0 194.68 10.70 -10 0 0 246.38 11.80 12 0 0 2016.00 73.09 -12 0 0 2188.18 88.69 12 0 0 1856.51 95.99 -12 0 0 2244.08 81.79 -12 0 0 2284.97 82.59 12 0 0 1907.11 95.29 12 0 0 2080.19 73.99 12 0 0 2074.29 73.99 -12 0 0 2269.27 81.99 -14 0 0 15.40 5.40 14 0 0 15.60 8.00 -14 0 0 16.10 12.60 -14 0 0 15.80 9.30 -14 0 0 19.60 6.20 14 0 0 14.50 6.20 -16 0 0 22.60 11.60 16 0 0 24.70 9.60 18 0 0 414.86 25.90 -3 -1 0 150.88 7.10 -3 -1 0 150.28 7.00 3 1 0 163.28 7.10 3 1 0 133.09 6.90 -5 -1 0 1343.57 49.30 -5 -1 0 1298.47 48.20 -5 -1 0 1314.77 49.20 5 1 0 1200.38 43.10 5 1 0 1280.07 46.50 5 1 0 1153.78 44.70 5 1 0 1140.09 44.50 -7 -1 0 6539.45 235.98 7 1 0 6295.87 236.78 7 1 0 6471.05 236.68 7 1 0 6352.66 231.88 7 1 0 6609.14 235.18 9 -1 0 134.69 9.10 9 -1 0 116.39 8.90 -9 -1 0 126.59 10.30 9 -1 0 115.59 8.70 -9 -1 0 121.39 9.80 9 1 0 129.49 16.90 9 1 0 120.19 13.90 -9 1 0 112.99 14.10 -9 1 0 102.39 8.60 -9 1 0 146.59 17.20 9 1 0 115.79 8.90 9 1 0 125.49 9.60 11 -1 0 857.71 32.40 11 -1 0 816.92 32.00 11 -1 0 821.32 33.60 11 -1 0 782.52 33.80 -11 -1 0 922.51 37.50 11 -1 0 845.02 32.30 11 1 0 813.42 34.20 -11 1 0 821.82 45.80 -11 1 0 823.72 42.80 -11 1 0 909.31 35.30 11 1 0 687.73 41.60 -11 1 0 883.41 35.30 11 1 0 760.92 48.40 13 -1 0 4339.47 159.38 13 -1 0 4327.57 156.98 -13 -1 0 4852.61 173.98 13 -1 0 4728.63 162.58 -13 1 0 4652.33 178.28 13 1 0 3793.82 173.08 13 1 0 4311.47 160.18 13 1 0 4376.66 159.18 13 1 0 4292.07 179.38 -13 1 0 4641.34 181.78 -13 1 0 4734.43 171.78 -15 -1 0 60.69 12.60 15 1 0 42.00 11.00 15 1 0 34.90 29.80 17 1 0 106.09 15.40 17 1 0 108.89 31.50 19 1 0 748.43 39.70 -4 -2 0 1554.44 58.99 -4 -2 0 1597.24 58.89 4 2 0 1544.85 57.09 4 2 0 1456.05 56.79 -6 -2 0 2310.57 83.29 -6 -2 0 2305.17 84.79 -6 -2 0 2249.68 84.79 6 2 0 2285.27 83.69 6 2 0 2299.27 83.99 6 2 0 2145.89 82.99 6 2 0 2234.18 84.79 -8 -2 0 1167.88 46.10 8 2 0 1112.89 43.90 8 2 0 1111.99 44.20 8 2 0 1079.19 46.60 -10 -2 0 796.72 35.20 10 2 0 706.73 31.40 10 2 0 715.93 39.60 10 2 0 703.13 31.10 10 2 0 666.83 39.70 -12 -2 0 669.73 33.00 12 2 0 582.34 29.30 12 2 0 622.64 45.60 -14 -2 0 371.46 27.10 14 2 0 349.67 38.30 14 2 0 321.07 23.30 16 2 0 161.18 33.50 16 2 0 180.08 18.90 18 2 0 117.09 18.70 18 2 0 117.19 35.60 -7 -3 0 276.17 15.70 -7 -3 0 298.57 13.70 -7 -3 0 280.47 17.10 7 3 0 272.07 17.00 7 3 0 295.07 18.20 -9 -3 0 79.79 7.80 -9 -3 0 83.49 10.50 9 3 0 87.79 12.30 9 3 0 74.09 12.40 9 3 0 59.19 11.10 -11 -3 0 755.22 35.60 11 3 0 681.83 33.70 11 3 0 627.84 40.40 -13 -3 0 1187.08 53.09 -13 -3 0 1171.08 51.39 13 3 0 1190.08 68.39 13 3 0 1152.88 65.09 -15 -3 0 64.59 16.00 15 3 0 93.99 27.60 15 3 0 33.70 15.10 17 3 0 302.37 26.60 17 3 0 281.87 42.60 -12 -4 0 521.35 30.40 12 4 0 401.96 35.90 -14 -4 0 19.90 13.40 -14 -4 0 19.90 13.10 14 4 0 18.40 20.60 14 4 0 27.80 22.40 -16 -4 0 28.60 16.40 16 4 0 28.90 26.80 18 0 -1 -12.50 9.60 16 0 -1 3.50 8.70 -16 0 1 -8.30 9.60 14 0 -1 8.90 7.70 14 0 -1 20.50 7.60 -14 0 1 28.70 9.60 14 0 -1 6.50 5.20 14 0 -1 4.60 5.60 -14 0 1 24.50 11.90 -14 0 1 8.00 6.50 -14 0 1 8.40 5.70 12 0 -1 -1.10 5.40 -12 0 1 -11.30 6.30 12 0 -1 -20.40 12.00 -12 0 1 -9.60 8.50 -12 0 1 -3.20 5.00 12 0 -1 -2.10 4.10 12 0 -1 -6.20 5.00 12 0 -1 -18.20 15.70 12 0 -1 4.30 4.10 -12 0 1 0.10 4.40 10 0 -1 0.90 3.30 10 0 -1 -4.00 9.10 -10 0 1 2.10 6.80 -10 0 1 -6.30 3.60 10 0 -1 2.40 2.90 10 0 -1 -1.00 4.00 10 0 -1 0.00 11.70 -10 0 1 2.90 3.30 10 0 -1 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949.11 42.30 6 -2 -13 877.91 49.10 -6 2 13 848.12 38.10 -6 2 13 862.11 35.50 -21 3 13 125.19 19.00 -21 3 13 87.69 16.10 -19 3 13 74.09 16.30 -19 3 13 78.59 13.80 17 -3 -13 12.20 16.90 -17 3 13 14.70 13.00 -17 3 13 0.40 10.20 15 -3 -13 75.59 17.70 -15 3 13 44.00 11.80 -15 3 13 49.30 13.50 13 -3 -13 34.20 15.70 -13 3 13 47.50 12.40 -13 3 13 50.19 11.20 -13 3 13 42.90 11.00 -13 3 13 55.09 11.10 11 -3 -13 73.29 16.40 -11 3 13 75.49 13.00 -11 3 13 54.99 11.50 -11 3 13 83.69 11.70 -11 3 13 71.59 11.70 9 -3 -13 155.28 18.50 9 -3 -13 138.29 15.20 -9 3 13 132.69 13.20 -9 3 13 126.19 14.40 -9 3 13 71.89 29.20 -9 3 13 94.69 12.90 7 -3 -13 74.99 15.30 7 -3 -13 101.49 14.80 -7 3 13 64.79 11.80 -7 3 13 169.58 39.90 -7 3 13 43.50 11.50 -7 3 13 65.99 11.20 5 -3 -13 182.38 18.80 5 -3 -13 155.28 18.20 5 -3 -13 172.58 23.20 -5 3 13 120.19 14.70 -5 3 13 185.28 43.90 -5 3 13 139.79 13.90 -5 3 13 155.08 12.10 3 -3 -13 107.59 15.90 3 -3 -13 104.99 17.10 3 -3 -13 98.59 22.40 -3 3 13 61.59 10.40 -3 3 13 105.29 12.60 -3 3 13 81.59 40.80 -3 3 13 93.59 14.20 1 -3 -13 22.10 20.50 1 -3 -13 79.29 17.70 -1 3 13 46.90 14.10 -1 3 13 51.89 70.39 -1 3 13 45.70 10.70 18 -4 -13 91.19 15.70 -18 4 13 117.99 15.80 -18 4 13 79.59 17.00 16 -4 -13 128.09 16.60 -16 4 13 145.79 17.90 -16 4 13 145.99 23.10 14 -4 -13 51.19 13.40 -14 4 13 54.19 12.70 -14 4 13 51.29 14.80 -12 4 13 7.70 10.10 -12 4 13 10.70 23.50 -12 4 13 66.09 18.20 -12 4 13 34.80 13.20 -12 4 13 1.90 11.60 -12 4 13 17.80 12.90 -10 4 13 52.89 13.80 -10 4 13 83.89 31.00 -10 4 13 25.60 12.70 -10 4 13 61.79 11.80 -8 4 13 10.40 28.40 -8 4 13 8.60 11.50 -8 4 13 3.20 11.60 -8 4 13 5.30 9.40 -6 4 13 150.38 39.00 -6 4 13 118.49 15.90 -6 4 13 103.79 13.90 -6 4 13 108.69 12.20 -4 4 13 471.15 59.79 -4 4 13 406.16 30.20 2 -4 -13 30.80 16.10 -2 4 13 33.60 15.00 -2 4 13 17.30 41.50 17 -5 -13 17.90 13.20 -17 5 13 -0.10 12.20 -17 5 13 16.70 16.10 15 -5 -13 173.78 17.80 -15 5 13 199.48 18.20 -15 5 13 166.28 26.30 13 -5 -13 23.40 12.70 -13 5 13 21.50 11.60 -13 5 13 11.90 14.60 11 -5 -13 41.10 12.90 -11 5 13 3.70 24.70 -11 5 13 27.40 12.20 -11 5 13 -3.00 13.40 -9 5 13 24.00 14.00 -9 5 13 69.49 18.20 -9 5 13 72.09 31.00 -9 5 13 41.10 11.50 -7 5 13 53.09 11.50 -7 5 13 71.79 32.50 -7 5 13 60.29 17.40 -7 5 13 29.20 14.20 -5 5 13 71.39 14.90 -5 5 13 82.09 11.70 -5 5 13 81.39 18.40 -5 5 13 61.39 33.10 -3 5 13 -14.70 15.00 -3 5 13 32.80 34.90 12 -6 -13 55.19 17.30 12 -6 -13 84.99 15.00 -12 6 13 62.99 13.90 10 -6 -13 37.40 14.30 8 -6 -13 134.09 19.90 8 -6 -13 129.49 15.60 -8 6 13 109.69 14.70 -8 6 13 163.48 35.90 6 -6 -13 94.49 19.90 -6 6 13 97.29 13.70 -6 6 13 113.99 36.10 23 -1 -14 79.59 25.50 -23 1 14 60.59 15.40 -23 1 14 67.19 16.60 21 -1 -14 13.90 18.40 21 -1 -14 -18.20 17.00 -21 1 14 27.40 18.20 -21 1 14 -15.50 11.50 -21 1 14 -6.50 16.10 19 -1 -14 393.46 31.00 19 -1 -14 341.37 27.60 -19 1 14 351.86 25.40 -19 1 14 402.66 27.80 -19 1 14 375.76 26.60 17 -1 -14 70.89 15.70 -17 1 14 60.59 12.00 -17 1 14 38.30 12.70 22 -2 -14 27.80 25.60 -22 2 14 39.60 17.30 -22 2 14 18.00 15.00 20 -2 -14 48.00 19.80 -20 2 14 53.19 14.30 -20 2 14 58.89 17.30 18 -2 -14 490.25 35.30 18 -2 -14 404.76 33.90 -18 2 14 370.96 25.10 -18 2 14 324.87 26.40 -18 2 14 400.16 28.20 16 -2 -14 17.90 15.20 16 -2 -14 22.00 16.20 -16 2 14 27.30 11.40 -16 2 14 47.80 13.60 -16 2 14 46.40 13.60 14 -2 -14 73.29 17.10 14 -2 -14 67.49 9.90 14 -2 -14 37.20 15.30 -14 2 14 40.20 9.30 -14 2 14 48.10 9.20 -14 2 14 53.29 13.50 -14 2 14 33.50 12.70 -14 2 14 60.89 17.20 12 -2 -14 544.25 32.40 12 -2 -14 510.15 27.30 12 -2 -14 513.15 31.20 -12 2 14 435.16 23.30 -12 2 14 446.46 20.10 -12 2 14 492.35 26.80 -12 2 14 410.46 23.20 -12 2 14 470.95 27.50 10 -2 -14 46.90 15.50 10 -2 -14 28.90 13.60 -10 2 14 45.50 11.90 -10 2 14 61.49 8.00 8 -2 -14 437.86 27.90 -8 2 14 404.26 24.50 -19 3 14 293.97 21.20 -19 3 14 263.77 24.00 15 -3 -14 33.80 18.10 -15 3 14 22.60 11.50 -15 3 14 30.50 13.70 13 -3 -14 1.80 15.90 -13 3 14 17.30 12.60 -13 3 14 28.70 11.60 -13 3 14 33.30 10.80 -13 3 14 30.10 10.30 11 -3 -14 196.38 21.60 -11 3 14 133.99 14.50 -11 3 14 162.68 17.00 9 -3 -14 272.37 20.50 9 -3 -14 264.07 23.10 -9 3 14 208.98 16.80 -9 3 14 238.38 18.60 -9 3 14 191.18 16.80 7 -3 -14 -1.70 14.00 7 -3 -14 33.80 17.40 7 -3 -14 27.80 13.20 -7 3 14 7.30 10.70 -7 3 14 27.10 8.40 -7 3 14 10.50 11.10 5 -3 -14 250.27 21.70 5 -3 -14 251.17 28.00 5 -3 -14 246.78 22.70 -5 3 14 184.38 16.20 -5 3 14 216.88 14.80 -5 3 14 219.18 18.70 3 -3 -14 151.68 25.60 3 -3 -14 142.79 19.80 -3 3 14 135.49 16.90 -3 3 14 119.49 12.80 -18 4 14 41.90 13.00 -18 4 14 24.00 14.90 -16 4 14 451.25 28.20 -14 4 14 239.58 24.20 -14 4 14 230.48 19.10 -12 4 14 38.50 13.90 -12 4 14 24.60 22.40 -12 4 14 40.40 11.90 -10 4 14 414.66 28.40 -10 4 14 441.06 53.39 -10 4 14 438.26 27.40 -10 4 14 420.06 25.80 -8 4 14 288.87 24.00 -8 4 14 355.66 22.70 -8 4 14 391.56 52.89 -8 4 14 354.66 27.50 -6 4 14 224.18 18.80 -6 4 14 238.38 49.30 -6 4 14 229.98 21.00 4 -4 -14 322.97 26.40 -4 4 14 347.77 25.90 15 -5 -14 37.10 14.00 -15 5 14 42.10 16.70 -15 5 14 20.00 13.10 13 -5 -14 149.59 17.80 -13 5 14 79.89 14.40 -13 5 14 68.79 28.10 -11 5 14 24.60 29.50 -11 5 14 9.20 11.40 -11 5 14 14.20 14.10 -9 5 14 94.09 13.30 -9 5 14 80.19 17.90 -9 5 14 100.29 36.80 -9 5 14 78.59 16.20 -7 5 14 94.59 16.40 -7 5 14 139.09 41.40 -7 5 14 71.39 18.40 -7 5 14 80.19 12.90 -5 5 14 75.69 11.80 -5 5 14 39.40 17.70 -5 5 14 37.30 37.60 -5 5 14 56.29 15.30 12 -6 -14 16.80 14.40 -12 6 14 30.40 15.70 10 -6 -14 80.59 15.40 -10 6 14 57.79 13.70 20 -2 -15 341.97 29.90 -20 2 15 295.07 24.20 -20 2 15 265.17 22.10 -18 2 15 126.79 16.30 16 -2 -15 86.39 19.20 16 -2 -15 89.99 18.20 -16 2 15 60.49 14.80 -16 2 15 66.09 13.60 -16 2 15 62.59 14.40 14 -2 -15 357.76 26.90 14 -2 -15 356.56 27.70 -14 2 15 283.37 23.50 -14 2 15 270.97 21.30 12 -2 -15 361.96 28.90 -12 2 15 253.07 20.00 19 -3 -15 2.00 20.10 -19 3 15 10.20 12.80 -19 3 15 6.80 15.20 17 -3 -15 119.19 21.60 -17 3 15 136.49 18.40 -17 3 15 129.49 16.80 13 -3 -15 271.77 25.60 -13 3 15 144.39 15.30 -13 3 15 199.08 19.20 -13 3 15 196.38 17.40 11 -3 -15 242.28 19.60 11 -3 -15 278.67 24.80 -11 3 15 209.58 17.40 -11 3 15 214.98 20.00 -11 3 15 236.38 18.60 9 -3 -15 39.40 14.60 9 -3 -15 45.70 17.10 -9 3 15 31.60 12.20 -9 3 15 38.70 13.00 7 -3 -15 252.97 23.20 7 -3 -15 281.77 29.20 7 -3 -15 281.87 23.90 -7 3 15 202.58 18.10 -7 3 15 168.78 13.70 -7 3 15 176.28 17.00 -16 4 15 77.29 18.30 -16 4 15 89.99 15.20 -14 4 15 7.50 11.80 -12 4 15 8.50 11.40 -12 4 15 17.20 13.80 -12 4 15 5.20 13.70 -10 4 15 98.99 15.80 -10 4 15 91.29 15.70 -10 4 15 81.39 13.60 -8 4 15 165.08 17.70 -8 4 15 110.79 17.60 -8 4 15 180.88 41.20 -6 4 15 80.19 16.50 -6 4 15 72.29 14.50 -13 5 15 60.99 14.10 -13 5 15 92.09 18.50 -11 5 15 34.60 32.10 -11 5 15 -22.50 15.60 -11 5 15 8.90 11.50 -9 5 15 82.59 39.30 -9 5 15 53.29 17.80 -9 5 15 41.00 15.70 -9 5 15 46.30 12.60 18 -2 -16 253.17 25.40 18 -2 -16 258.57 25.30 -18 2 16 205.48 20.60 -18 2 16 220.98 20.30 -18 2 16 241.38 22.10 17 -3 -16 55.89 21.70 -17 3 16 81.29 14.90 -17 3 16 49.80 16.50 15 -3 -16 49.10 20.40 -15 3 16 27.50 14.50 -15 3 16 18.90 12.90 13 -3 -16 191.58 24.20 -13 3 16 169.98 17.40 -13 3 16 173.48 19.30 11 -3 -16 34.90 18.20 -11 3 16 35.80 14.30 -14 4 16 66.79 17.00 -14 4 16 66.49 14.60 -12 4 16 45.50 15.50 -12 4 16 39.50 16.60 -12 4 16 44.20 12.90 -10 4 16 147.89 18.50 -8 4 16 145.79 19.50 15 -3 -17 78.99 36.10 -15 3 17 68.79 25.70 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 80001 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O001 O 0.6634(5) 0.9097(15) 0.8870(6) 0.040(3) Uani 1 1 d . . . . . N002 N 0.8116(5) 0.8874(16) 0.7907(7) 0.016(2) Uani 1 1 d . . . . . O003 O 0.3342(4) 1.0488(14) 0.1516(6) 0.025(2) Uani 1 1 d . . . . . O004 O 0.8603(4) 0.8322(11) 0.7714(5) 0.020(2) Uani 1 1 d . . . . . N005 N 0.4869(5) 0.2419(16) 0.5983(7) 0.024(2) Uani 1 1 d . . . . . N006 N 0.3370(5) -0.0084(16) 0.4216(7) 0.024(3) Uani 1 1 d . . . . . O O 0.8216(4) 1.0172(14) 0.8450(7) 0.026(3) Uani 1 1 d . . . . . O008 O 0.4927(4) 0.7985(13) 0.6652(5) 0.035(3) Uani 1 1 d . . . . . O009 O 0.3317(5) -0.1573(15) 0.4503(6) 0.035(3) Uani 1 1 d . . . . . C00A C 0.6638(5) 0.8319(17) 0.7391(7) 0.016(2) Uani 1 1 d . . . . . O00B O 0.5065(4) 0.8429(14) 0.4297(5) 0.028(3) Uani 1 1 d . . . . . N00C N 0.6465(5) 1.1737(17) 0.5602(6) 0.017(2) Uani 1 1 d . . . . . O00D O 0.3147(4) 1.3345(14) 0.1256(6) 0.032(3) Uani 1 1 d . . . . . O00E O 0.4642(4) 0.6211(13) 0.5302(6) 0.025(2) Uani 1 1 d . . . . . C00F C 0.5643(6) 1.2247(17) 0.4521(8) 0.016(2) Uani 1 1 d . . . . . O00G O 0.6873(4) 1.2887(13) 0.6306(6) 0.027(2) Uani 1 1 d . . . . . O00H O 0.1315(4) 0.1893(12) 0.4251(5) 0.027(2) Uani 1 1 d . . . . . C00I C 0.7305(6) 0.7943(17) 0.7333(7) 0.016(3) Uani 1 1 d . . . . . N00J N 0.6302(4) 0.6339(14) 0.6124(6) 0.019(3) Uani 1 1 d . . . . . N00K N 0.4666(4) 1.3935(15) 0.3287(6) 0.020(2) Uani 1 1 d . . . . . O00L O 0.4913(4) 0.8671(14) 0.2722(5) 0.032(3) Uani 1 1 d . . . . . O00M O 0.5376(4) 0.3554(14) 0.6634(6) 0.034(3) Uani 1 1 d . . . . . O00N O 0.1688(5) -0.0196(16) 0.3626(7) 0.036(3) Uani 1 1 d . . . . . O00O O 0.5051(4) 0.1111(13) 0.5662(5) 0.031(3) Uani 1 1 d . . . . . N00P N 0.6614(5) 0.9599(18) 0.8065(7) 0.022(3) Uani 1 1 d . . . . . N00Q N 0.4987(6) 0.9310(13) 0.3556(8) 0.020(2) Uani 1 1 d . . . . . O00R O 0.6673(4) 1.0225(14) 0.5684(6) 0.022(2) Uani 1 1 d . . . . . N00S N 0.3564(5) 1.2000(16) 0.1800(6) 0.018(3) Uani 1 1 d . . . . . N00T N 0.2904(5) 0.3343(16) 0.5391(7) 0.023(3) Uani 1 1 d . . . . . O00U O 0.6599(5) 1.1122(15) 0.7827(6) 0.032(3) Uani 1 1 d . . . . . N00V N 0.7116(5) 0.6700(15) 0.6586(7) 0.019(3) Uani 1 1 d . . . . . C00W C 0.5997(5) 0.7273(16) 0.6571(7) 0.014(3) Uani 1 1 d . . . . . C00X C 0.3977(6) 0.2556(18) 0.5535(8) 0.021(3) Uani 1 1 d . . . . . O00Y O 0.3457(5) 0.0259(13) 0.3476(6) 0.040(3) Uani 1 1 d . . . . . C00Z C 0.5005(7) 1.1150(15) 0.3652(8) 0.015(2) Uani 1 1 d . . . . . N010 N 0.3725(5) 0.3763(16) 0.5898(7) 0.026(3) Uani 1 1 d . . . . . N1 N 0.5440(5) 1.3871(15) 0.4320(6) 0.020(2) Uani 1 1 d . . . . . C2 C 0.4398(5) 1.2332(16) 0.2882(7) 0.017(3) Uani 1 1 d . . . . . N3 N 0.5116(5) 0.7126(15) 0.6140(6) 0.019(3) Uani 1 1 d . . . . . N4 N 0.1825(5) 0.1159(17) 0.4170(7) 0.021(2) Uani 1 1 d . . . . . C5 C 0.3347(6) 0.1362(17) 0.4810(8) 0.019(3) Uani 1 1 d . . . . . C6 C 0.2665(6) 0.1918(19) 0.4748(8) 0.018(3) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O001 0.052(4) 0.054(11) 0.029(5) -0.020(3) 0.033(4) -0.024(5) N002 0.015(4) 0.007(10) 0.019(5) 0.003(3) 0.007(3) 0.002(4) O003 0.022(4) 0.022(9) 0.026(4) -0.007(3) 0.013(3) -0.003(4) O004 0.018(3) 0.010(9) 0.035(4) -0.003(3) 0.018(3) -0.004(3) N005 0.019(4) 0.031(10) 0.016(4) 0.007(3) 0.008(4) -0.001(4) N006 0.018(4) 0.031(10) 0.017(5) -0.013(4) 0.008(4) 0.000(5) O 0.023(4) 0.020(10) 0.031(5) -0.009(3) 0.014(3) -0.004(4) O008 0.028(3) 0.057(10) 0.029(4) -0.011(4) 0.023(3) -0.005(4) O009 0.038(4) 0.024(10) 0.028(5) -0.005(4) 0.012(3) 0.006(4) C00A 0.010(4) 0.020(10) 0.010(5) -0.002(3) 0.002(4) 0.001(4) O00B 0.027(4) 0.031(9) 0.026(4) 0.006(3) 0.016(3) -0.003(4) N00C 0.019(4) 0.009(9) 0.025(5) 0.002(3) 0.014(4) -0.002(4) O00D 0.024(4) 0.020(10) 0.041(5) 0.015(4) 0.015(4) 0.004(4) O00E 0.020(3) 0.014(9) 0.027(4) -0.001(3) 0.007(3) -0.007(4) C00F 0.020(4) 0.013(9) 0.022(5) -0.003(4) 0.016(3) -0.001(4) O00G 0.024(3) 0.013(9) 0.035(5) -0.012(3) 0.014(3) -0.006(4) O00H 0.023(4) 0.026(9) 0.039(5) -0.002(3) 0.022(3) 0.004(4) C00I 0.015(4) 0.009(11) 0.018(5) 0.005(4) 0.008(4) 0.002(4) N00J 0.012(4) 0.013(10) 0.028(5) -0.005(3) 0.010(4) 0.000(4) N00K 0.016(3) 0.010(9) 0.029(5) -0.002(3) 0.011(3) 0.001(4) O00L 0.037(4) 0.035(10) 0.018(4) -0.008(3) 0.014(3) 0.004(4) O00M 0.026(4) 0.021(10) 0.037(5) 0.002(3) 0.011(4) -0.006(4) O00N 0.029(4) 0.027(11) 0.040(5) -0.015(4) 0.016(4) 0.001(4) O00O 0.021(3) 0.048(10) 0.030(4) -0.005(3) 0.018(3) 0.000(4) N00P 0.012(4) 0.027(10) 0.023(5) -0.003(4) 0.008(4) 0.003(4) N00Q 0.013(3) 0.026(8) 0.017(4) -0.002(4) 0.007(3) -0.002(5) O00R 0.023(4) 0.016(8) 0.025(4) 0.007(3) 0.015(3) 0.002(4) N00S 0.017(4) 0.025(10) 0.016(4) 0.003(3) 0.011(3) 0.001(5) N00T 0.020(4) 0.026(11) 0.017(5) -0.001(3) 0.007(3) 0.004(4) O00U 0.031(4) 0.028(9) 0.024(4) -0.004(4) 0.010(3) 0.012(5) N00V 0.017(4) 0.008(10) 0.030(5) -0.007(4) 0.012(4) -0.009(4) C00W 0.013(4) 0.013(11) 0.014(5) 0.002(3) 0.007(4) 0.001(4) C00X 0.022(4) 0.019(11) 0.023(6) 0.004(4) 0.014(4) 0.004(5) O00Y 0.032(4) 0.069(11) 0.028(4) -0.014(3) 0.023(4) -0.016(4) C00Z 0.021(3) 0.015(7) 0.018(5) 0.002(4) 0.016(3) 0.005(5) N010 0.022(4) 0.023(11) 0.029(6) 0.002(4) 0.014(4) 0.002(4) N1 0.019(3) 0.014(8) 0.022(4) 0.000(3) 0.010(3) 0.009(4) C2 0.020(4) 0.020(9) 0.016(5) 0.002(3) 0.013(4) 0.000(4) N3 0.016(4) 0.024(9) 0.018(4) 0.003(3) 0.011(3) -0.001(4) N4 0.020(4) 0.014(10) 0.026(5) 0.002(3) 0.013(4) 0.000(4) C5 0.024(5) 0.016(10) 0.020(5) 0.004(3) 0.016(4) 0.004(5) C6 0.020(4) 0.018(11) 0.017(6) 0.002(4) 0.012(4) 0.002(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O004 N002 C00I 115.3(9) . . ? O N002 O004 127.0(10) . . ? O N002 C00I 117.5(8) . . ? O00M N005 O00O 125.7(8) . . ? O00M N005 C00X 118.8(11) . . ? O00O N005 C00X 115.5(10) . . ? O009 N006 C5 117.6(10) . . ? O00Y N006 O009 125.7(11) . . ? O00Y N006 C5 116.7(13) . . ? C00I C00A N00P 128.4(10) . . ? C00W C00A C00I 102.6(9) . . ? C00W C00A N00P 128.8(8) . . ? O00G N00C C00F 116.5(13) . . ? O00R N00C C00F 116.3(9) . . ? O00R N00C O00G 127.1(10) . . ? C00Z C00F N00C 127.5(12) . . ? N1 C00F N00C 119.2(10) . . ? N1 C00F C00Z 113.2(9) . . ? C00A C00I N002 126.8(10) . . ? N00V C00I N002 119.2(8) . . ? N00V C00I C00A 113.7(9) . . ? N00V N00J C00W 113.3(8) . . ? C2 N00K N1 109.8(10) . . ? O001 N00P C00A 117.8(13) . . ? O00U N00P O001 124.3(11) . . ? O00U N00P C00A 117.9(10) . . ? O00B N00Q O00L 122.9(11) . . ? O00B N00Q C00Z 118.9(9) . . ? O00L N00Q C00Z 118.1(8) . . ? O003 N00S O00D 127.3(10) . . ? O003 N00S C2 118.1(9) . . ? O00D N00S C2 114.6(11) . . ? C6 N00T N010 112.1(9) . . ? N00J N00V C00I 102.4(8) . . ? C00A C00W N3 130.7(9) . . ? N00J C00W C00A 107.9(7) . . ? N00J C00W N3 121.4(9) . . ? N010 C00X N005 121.2(10) . . ? N010 C00X C5 113.8(8) . . ? C5 C00X N005 124.6(11) . . ? C00F C00Z N00Q 130.1(9) . . ? C2 C00Z C00F 101.5(10) . . ? C2 C00Z N00Q 128.4(9) . . ? C00X N010 N00T 103.3(9) . . ? C00F N1 N00K 105.9(10) . . ? N00K C2 N00S 121.9(10) . . ? N00K C2 C00Z 109.6(9) . . ? C00Z C2 N00S 128.4(11) . . ? O008 N3 C00W 115.0(8) . . ? O00E N3 O008 127.5(7) . . ? O00E N3 C00W 117.4(8) . . ? O00H N4 O00N 125.9(10) . . ? O00H N4 C6 118.0(11) . . ? O00N N4 C6 116.1(9) . . ? C00X C5 N006 129.9(8) . . ? C6 C5 N006 127.0(10) . . ? C6 C5 C00X 103.0(10) . . ? N00T C6 N4 122.2(9) . . ? N00T C6 C5 107.9(10) . . ? C5 C6 N4 129.9(12) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O001 N00P 1.221(12) . ? N002 O004 1.224(10) . ? N002 O 1.213(13) . ? N002 C00I 1.451(14) . ? O003 N00S 1.216(13) . ? N005 O00M 1.223(14) . ? N005 O00O 1.247(13) . ? N005 C00X 1.444(12) . ? N006 O009 1.241(14) . ? N006 O00Y 1.228(12) . ? N006 C5 1.426(15) . ? O008 N3 1.214(11) . ? C00A C00I 1.388(12) . ? C00A N00P 1.415(16) . ? C00A C00W 1.349(15) . ? O00B N00Q 1.208(12) . ? N00C C00F 1.464(12) . ? N00C O00G 1.214(13) . ? N00C O00R 1.207(14) . ? O00D N00S 1.252(13) . ? O00E N3 1.212(12) . ? C00F C00Z 1.395(15) . ? C00F N1 1.282(15) . ? O00H N4 1.211(11) . ? C00I N00V 1.323(15) . ? N00J N00V 1.323(11) . ? N00J C00W 1.333(12) . ? N00K N1 1.339(10) . ? N00K C2 1.323(15) . ? O00L N00Q 1.244(12) . ? O00N N4 1.235(16) . ? N00P O00U 1.212(14) . ? N00Q C00Z 1.413(13) . ? N00S C2 1.445(12) . ? N00T N010 1.334(11) . ? N00T C6 1.327(16) . ? C00W N3 1.434(10) . ? C00X N010 1.305(16) . ? C00X C5 1.373(16) . ? C00Z C2 1.366(15) . ? N4 C6 1.433(14) . ? C5 C6 1.351(13) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N002 C00I N00V N00J -171.2(9) . . . . ? O003 N00S C2 N00K -175.8(6) . . . . ? O003 N00S C2 C00Z 1.6(13) . . . . ? O004 N002 C00I C00A -178.9(11) . . . . ? O004 N002 C00I N00V -5.6(16) . . . . ? N005 C00X N010 N00T -173.2(10) . . . . ? N005 C00X C5 N006 -10(2) . . . . ? N005 C00X C5 C6 172.6(10) . . . . ? N006 C5 C6 N00T -177.3(13) . . . . ? N006 C5 C6 N4 6(2) . . . . ? O N002 C00I C00A -4.1(19) . . . . ? O N002 C00I N00V 169.1(13) . . . . ? O009 N006 C5 C00X 113.5(14) . . . . ? O009 N006 C5 C6 -69.1(16) . . . . ? C00A C00I N00V N00J 2.9(15) . . . . ? C00A C00W N3 O008 -6.3(17) . . . . ? C00A C00W N3 O00E 171.9(11) . . . . ? O00B N00Q C00Z C00F 58.4(14) . . . . ? O00B N00Q C00Z C2 -123.9(10) . . . . ? N00C C00F C00Z N00Q -2.4(15) . . . . ? N00C C00F C00Z C2 179.4(7) . . . . ? N00C C00F N1 N00K -179.8(7) . . . . ? O00D N00S C2 N00K 4.1(11) . . . . ? O00D N00S C2 C00Z -178.6(8) . . . . ? C00F C00Z C2 N00K -0.6(10) . . . . ? C00F C00Z C2 N00S -178.2(7) . . . . ? O00G N00C C00F C00Z -170.3(9) . . . . ? O00G N00C C00F N1 7.4(11) . . . . ? O00H N4 C6 N00T 2.5(19) . . . . ? O00H N4 C6 C5 179.0(12) . . . . ? C00I C00A N00P O001 -109.3(14) . . . . ? C00I C00A N00P O00U 68.6(16) . . . . ? C00I C00A C00W N00J 2.2(12) . . . . ? C00I C00A C00W N3 -175.0(11) . . . . ? N00J C00W N3 O008 176.8(10) . . . . ? N00J C00W N3 O00E -5.0(16) . . . . ? O00L N00Q C00Z C00F -119.9(10) . . . . ? O00L N00Q C00Z C2 57.9(13) . . . . ? O00M N005 C00X N010 -6.8(17) . . . . ? O00M N005 C00X C5 -179.2(11) . . . . ? O00N N4 C6 N00T -177.8(15) . . . . ? O00N N4 C6 C5 -1(2) . . . . ? O00O N005 C00X N010 172.9(11) . . . . ? O00O N005 C00X C5 0.5(16) . . . . ? N00P C00A C00I N002 -4(2) . . . . ? N00P C00A C00I N00V -177.9(12) . . . . ? N00P C00A C00W N00J 176.8(13) . . . . ? N00P C00A C00W N3 0(2) . . . . ? N00Q C00Z C2 N00K -178.9(7) . . . . ? N00Q C00Z C2 N00S 3.5(15) . . . . ? O00R N00C C00F C00Z 11.4(12) . . . . ? O00R N00C C00F N1 -170.8(7) . . . . ? N00V N00J C00W C00A -0.6(13) . . . . ? N00V N00J C00W N3 176.9(10) . . . . ? C00W C00A C00I N002 170.3(10) . . . . ? C00W C00A C00I N00V -3.3(15) . . . . ? C00W C00A N00P O001 77.4(15) . . . . ? C00W C00A N00P O00U -104.6(15) . . . . ? C00W N00J N00V C00I -1.4(14) . . . . ? C00X C5 C6 N00T 0.6(15) . . . . ? C00X C5 C6 N4 -176.3(12) . . . . ? O00Y N006 C5 C00X -65.2(16) . . . . ? O00Y N006 C5 C6 112.1(13) . . . . ? C00Z C00F N1 N00K -1.8(9) . . . . ? N010 N00T C6 N4 176.5(9) . . . . ? N010 N00T C6 C5 -0.7(17) . . . . ? N010 C00X C5 N006 177.5(12) . . . . ? N010 C00X C5 C6 -0.3(14) . . . . ? N1 C00F C00Z N00Q 179.7(8) . . . . ? N1 C00F C00Z C2 1.5(10) . . . . ? N1 N00K C2 N00S 177.4(7) . . . . ? N1 N00K C2 C00Z -0.4(9) . . . . ? C2 N00K N1 C00F 1.3(8) . . . . ? C5 C00X N010 N00T -0.1(14) . . . . ? C6 N00T N010 C00X 0.5(15) . . . . ?