#------------------------------------------------------------------------------ #$Date: 2024-01-06 09:58:57 +0200 (Sat, 06 Jan 2024) $ #$Revision: 288793 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/77/7247763.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7247763 loop_ _publ_author_name 'Jones, Isabelle M.' 'Turner, Gemma F.' 'Pitts, Kari' 'Powell, Rees' 'Riboldi-Tunnicliffe, Alan' 'Williamson, Rachel' 'Boer, Stephanie' 'Allen, Lauren' 'Moggach, Stephen A.' _publ_section_title ; High-pressure induced guest-mediated gate opening behaviour of the Co-based framework ZIF-67 ; _journal_issue 47 _journal_name_full CrystEngComm _journal_page_first 6533 _journal_page_last 6538 _journal_paper_doi 10.1039/D3CE00979C _journal_volume 25 _journal_year 2023 _chemical_absolute_configuration ad _chemical_formula_moiety 'C8 H10 Co N4, 12.889(N0.5)' _chemical_formula_sum 'C8 H10 Co N10.44' _chemical_formula_weight 311.41 _chemical_name_common ZIF-67 _space_group_crystal_system cubic _space_group_IT_number 217 _space_group_name_Hall 'I -4 2 3' _space_group_name_H-M_alt 'I -4 3 m' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2023-10-03 _audit_creation_method ; Olex2 1.5 (compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817) ; _audit_update_record ; 2023-10-04 deposited with the CCDC. 2023-11-21 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 12 _cell_length_a 16.9979(6) _cell_length_b 16.9979(6) _cell_length_c 16.9979(6) _cell_measurement_reflns_used 1983 _cell_measurement_temperature 293 _cell_measurement_theta_max 20.7810 _cell_measurement_theta_min 3.3720 _cell_volume 4911.2(3) _computing_cell_refinement 'CrysAlisPro 1.171.42.58a (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.42.58a (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.58a (Rigaku OD, 2022)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _diffrn_ambient_temperature 293 _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.990 _diffrn_measured_fraction_theta_max 0.990 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -36.00 29.00 0.50 75.00 -- -24.44 -53.00 38.00 130 2 \w -27.00 -3.00 0.50 75.00 -- 24.20 19.00-150.00 48 3 \w -23.00 16.00 0.50 75.00 -- 24.20 67.00 -23.00 78 4 \w -36.00 -16.00 0.50 75.00 -- -24.44 38.00 150.00 40 5 \w -4.00 18.00 0.50 75.00 -- -24.44 -57.00 30.00 44 6 \w -36.00 -16.00 0.50 75.00 -- -24.44 38.00 -30.00 40 7 \w -36.00 -16.00 0.50 75.00 -- 24.20 38.00 30.00 40 8 \w 30.00 55.00 0.50 75.00 -- 24.20 -99.00 30.00 50 9 \w 30.00 71.00 0.50 75.00 -- 24.20 -99.00-150.00 82 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Single source at home/near, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0147531000 _diffrn_orient_matrix_UB_12 0.0070913000 _diffrn_orient_matrix_UB_13 -0.0383535000 _diffrn_orient_matrix_UB_21 0.0040678000 _diffrn_orient_matrix_UB_22 0.0411162000 _diffrn_orient_matrix_UB_23 0.0059826000 _diffrn_orient_matrix_UB_31 0.0388200000 _diffrn_orient_matrix_UB_32 -0.0016011000 _diffrn_orient_matrix_UB_33 -0.0152482000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0906 _diffrn_reflns_av_unetI/netI 0.0491 _diffrn_reflns_Laue_measured_fraction_full 0.990 _diffrn_reflns_Laue_measured_fraction_max 0.990 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 10 _diffrn_reflns_limit_l_min -11 _diffrn_reflns_number 5119 _diffrn_reflns_point_group_measured_fraction_full 0.992 _diffrn_reflns_point_group_measured_fraction_max 0.992 _diffrn_reflns_theta_full 20.781 _diffrn_reflns_theta_max 20.781 _diffrn_reflns_theta_min 3.390 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Mo) X-ray Source' _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 1.054 _exptl_absorpt_correction_T_max 0.7445 _exptl_absorpt_correction_T_min 0.4799 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1078 before and 0.0816 after correction. The Ratio of minimum to maximum transmission is 0.6446. The \l/2 correction factor is Not present. ; _exptl_crystal_colour 'bluish violet' _exptl_crystal_colour_modifier bluish _exptl_crystal_colour_primary violet _exptl_crystal_density_diffrn 1.264 _exptl_crystal_description block _exptl_crystal_F_000 1897 _exptl_crystal_recrystallization_method 'Re-crystallisation from solvent' _exptl_crystal_size_max 0.14 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.09 _refine_diff_density_max 0.830 _refine_diff_density_min -0.378 _refine_diff_density_rms 0.150 _refine_ls_abs_structure_details ; Flack x determined using 182 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.13(3) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.114 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 43 _refine_ls_number_reflns 505 _refine_ls_number_restraints 8 _refine_ls_restrained_S_all 1.120 _refine_ls_R_factor_all 0.0847 _refine_ls_R_factor_gt 0.0801 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1966P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2325 _refine_ls_wR_factor_ref 0.2398 _reflns_Friedel_coverage 0.778 _reflns_Friedel_fraction_full 0.995 _reflns_Friedel_fraction_max 0.995 _reflns_number_gt 463 _reflns_number_total 505 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL zif67_ln2_1300_a.res in I-43m zif67_ln2_1300.res created by SHELXL-2018/3 at 14:55:36 on 03-Oct-2023 REM Old TITL ZIF67_LN2_1300 in I-43m REM SHELXT solution in I-43m: R1 0.115, Rweak 0.052, Alpha 0.139 REM 0.000 for 0 systematic absences, Orientation as input REM Flack x = 0.113 ( 0.037 ) from 179 Parsons' quotients REM Formula found by SHELXT: C37 N17 Co3 CELL 0.71073 16.9979 16.9979 16.9979 90 90 90 ZERR 12 0.0006 0.0006 0.0006 0 0 0 LATT -2 SYMM -X,-Y,+Z SYMM -X,+Y,-Z SYMM +X,-Y,-Z SYMM +Z,+X,+Y SYMM +Z,-X,-Y SYMM -Z,-X,+Y SYMM -Z,+X,-Y SYMM +Y,+Z,+X SYMM -Y,+Z,-X SYMM +Y,-Z,-X SYMM -Y,-Z,+X SYMM +Y,+X,+Z SYMM -Y,-X,+Z SYMM +Y,-X,-Z SYMM -Y,+X,-Z SYMM +X,+Z,+Y SYMM -X,+Z,-Y SYMM -X,-Z,+Y SYMM +X,-Z,-Y SYMM +Z,+Y,+X SYMM +Z,-Y,-X SYMM -Z,+Y,-X SYMM -Z,-Y,+X SFAC C H Co N UNIT 96 120 12 125.33 DFIX 1.55 C2 C3 DFIX 1.337 0.01 N1 C2 DFIX 1.387 0.01 N1 C1 DFIX 2.175 0.01 C1 C2 EADP N1 C1 C2 RIGU C2 C3 FLAT C1 N1 C2 C3 EADP N11 N10 EADP N4 N5 EADP N3 N2 EADP N9 N8 EADP N6 N7 L.S. 10 0 0 PLAN 1 SIZE 0.09 0.1 0.14 TEMP 19.85 CONF BOND list 4 MORE -1 BOND $H fmap 2 53 acta REM REM REM WGHT 0.196600 FVAR 0.14777 CO1 3 0.500000 0.250000 0.000000 10.25000 0.03838 0.03592 = 0.03838 0.00000 0.00000 0.00000 N1 4 0.587390 0.319544 0.035454 11.00000 0.03574 0.04823 = 0.03549 0.00210 -0.00031 -0.00335 C2 1 0.632418 0.367582 -0.008119 10.50000 0.03574 0.04823 = 0.03549 0.00210 -0.00031 -0.00335 C1 1 0.605903 0.337995 0.112273 11.00000 0.03574 0.04823 = 0.03549 0.00210 -0.00031 -0.00335 AFIX 43 1.0770 H1 2 0.579842 0.311891 0.163790 11.00000 -1.20000 AFIX 0 C3 1 0.627381 0.372619 -0.096350 10.50000 0.05232 0.05232 = 0.04470 0.00754 -0.00754 -0.02189 PART -1 AFIX 33 1.0830 H3A 2 0.584599 0.330469 -0.117621 10.50000 -1.50000 H3B 2 0.609526 0.431389 -0.113282 10.50000 -1.50000 H3C 2 0.684392 0.359626 -0.121654 10.50000 -1.50000 AFIX 0 PART 0 N2 4 0.500000 0.500000 0.000000 10.08333 0.09065 N5 4 0.500000 0.500000 -0.231903 10.25000 0.13749 N8 4 0.777383 0.222617 0.070244 10.25000 0.06434 N3 4 0.500000 0.500000 -0.038895 10.16667 0.09065 N9 4 0.770227 0.229773 0.026801 10.25000 0.06434 N6 4 0.758299 0.241701 -0.241701 10.11111 0.08114 N4 4 0.527905 0.472095 -0.232951 10.16667 0.13749 N7 4 0.742291 0.257709 -0.257709 10.05556 0.08114 N10 4 0.574677 0.425323 -0.425323 10.11112 0.10424 N11 4 0.596666 0.442577 -0.442577 10.08333 0.10424 N12 4 0.873207 0.126793 -0.126793 10.08333 0.08305 HKLF 4 REM zif67_ln2_1300_a.res in I-43m REM wR2 = 0.2398, GooF = S = 1.114, Restrained GooF = 1.120 for all data REM R1 = 0.0801 for 463 Fo > 4sig(Fo) and 0.0847 for all 505 data REM 43 parameters refined using 8 restraints END WGHT 0.1969 0.0000 REM Highest difference peak 0.830, deepest hole -0.378, 1-sigma level 0.150 Q1 1 0.8618 0.1382 -0.1553 10.50000 0.05 0.83 REM The information below was added by Olex2. REM REM R1 = 0.0801 for 463 Fo > 4sig(Fo) and 0.0847 for all 5119 data REM 43 parameters refined using n/a restraints REM Highest difference peak 0.83, deepest hole -0.38 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0847 REM R1_gt = 0.0801 REM wR_ref = 0.2398 REM GOOF = 1.114 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 5119 REM Reflections_gt = 463 REM Parameters = 43 REM Hole = -0.38 REM Peak = 0.83 REM Flack = 0.13(3) ; _cod_data_source_file d3ce00979c2.cif _cod_data_source_block zif67_ln2_1300 _cod_depositor_comments 'Adding full bibliography for 7247762--7247779.cif.' _cod_original_cell_volume 4911.2(5) _cod_database_code 7247763 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'Co C8 H10 N4' _chemical_oxdiff_usercomment 'ZIF67 @ 1.3 GPa' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.911 _shelx_estimated_absorpt_t_min 0.866 _diffrn_orient_matrix_axis[1] matrixX _diffrn_orient_matrix_axis[2] matrixY _diffrn_orient_matrix_axis[3] matrixZ _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances C2-C3 1.55 with sigma of 0.02 N1-C2 1.337 with sigma of 0.01 N1-C1 1.387 with sigma of 0.01 C1-C2 2.175 with sigma of 0.01 3. Restrained planarity C1, N1, C2, C3 with sigma of 0.1 4. Uiso/Uaniso restraints and constraints Uanis(N1) = Uanis(C1) = Uanis(C2) Uiso(N11) = Uiso(N10) Uiso(N4) = Uiso(N5) Uiso(N3) = Uiso(N2) Uiso(N9) = Uiso(N8) Uiso(N6) = Uiso(N7) 5. Rigid body (RIGU) restrains C2, C3 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 6. Others Fixed Sof: H3A(0.5) H3B(0.5) H3C(0.5) N2(0.083333) N8(0.25) N3(0.166667) N9(0.25) N6(0.11111) N4(0.166667) N7(0.05556) N10(0.11112) N11(0.083333) N12(0.083333) 7.a Me refined with riding coordinates: C3(H3A,H3B,H3C) 7.b Aromatic/amide H refined with riding coordinates: C1(H1) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 3.598 _oxdiff_exptl_absorpt_empirical_full_min 0.614 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, z' '-y, -x, z' 'y, -x, -z' '-y, x, -z' 'x, z, y' '-x, z, -y' '-x, -z, y' 'x, -z, -y' 'z, y, x' 'z, -y, -x' '-z, y, -x' '-z, -y, x' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' 'z+1/2, x+1/2, y+1/2' 'z+1/2, -x+1/2, -y+1/2' '-z+1/2, -x+1/2, y+1/2' '-z+1/2, x+1/2, -y+1/2' 'y+1/2, z+1/2, x+1/2' '-y+1/2, z+1/2, -x+1/2' 'y+1/2, -z+1/2, -x+1/2' '-y+1/2, -z+1/2, x+1/2' 'y+1/2, x+1/2, z+1/2' '-y+1/2, -x+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' 'x+1/2, z+1/2, y+1/2' '-x+1/2, z+1/2, -y+1/2' '-x+1/2, -z+1/2, y+1/2' 'x+1/2, -z+1/2, -y+1/2' 'z+1/2, y+1/2, x+1/2' 'z+1/2, -y+1/2, -x+1/2' '-z+1/2, y+1/2, -x+1/2' '-z+1/2, -y+1/2, x+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co1 Co 0.500000 0.250000 0.000000 0.0376(18) Uani 1 4 d S T P . . N1 N 0.5874(6) 0.3195(6) 0.0355(5) 0.040(3) Uani 1 1 d D . . . . C2 C 0.6324(7) 0.3676(7) -0.0081(8) 0.040(3) Uani 1 2 d DS T P . . C1 C 0.6059(8) 0.3380(10) 0.1123(6) 0.040(3) Uani 1 1 d D . . . . H1 H 0.579842 0.311891 0.163790 0.048 Uiso 1 1 calc R U . . . C3 C 0.6274(10) 0.3726(10) -0.0964(12) 0.050(6) Uani 1 2 d DS T P . . H3A H 0.584599 0.330469 -0.117621 0.075 Uiso 0.5 1 calc R U P A -1 H3B H 0.609526 0.431389 -0.113282 0.075 Uiso 0.5 1 calc R U P A -1 H3C H 0.684392 0.359626 -0.121654 0.075 Uiso 0.5 1 calc R U P A -1 N2 N 0.500000 0.500000 0.000000 0.091(10) Uiso 0.6666 8 d S . P . . N5 N 0.500000 0.500000 -0.232(5) 0.137(19) Uiso 1 4 d S . P . . N8 N 0.7774(18) 0.2226(18) 0.070(2) 0.064(8) Uiso 0.5 2 d S . P . . N3 N 0.500000 0.500000 -0.039(3) 0.091(10) Uiso 0.6667 4 d S . P . . N9 N 0.770(2) 0.230(2) 0.027(2) 0.064(8) Uiso 0.5 2 d S . P . . N6 N 0.758(3) 0.242(3) -0.242(3) 0.081(15) Uiso 0.6667 6 d S . P . . N4 N 0.528(6) 0.472(6) -0.233(10) 0.137(19) Uiso 0.3333 2 d S . P . . N7 N 0.742(5) 0.258(5) -0.258(5) 0.081(15) Uiso 0.3334 6 d S . P . . N10 N 0.575(5) 0.425(5) -0.425(5) 0.10(3) Uiso 0.6667 6 d S . P . . N11 N 0.597(14) 0.443(12) -0.443(12) 0.10(3) Uiso 0.1667 2 d S . P . . N12 N 0.873(3) 0.127(3) -0.127(3) 0.08(3) Uiso 0.5 6 d S . P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Co1 0.038(2) 0.036(2) 0.038(2) 0.000 0.000 0.000 N1 0.036(5) 0.048(6) 0.035(4) 0.002(5) 0.000(4) -0.003(4) C2 0.036(5) 0.048(6) 0.035(4) 0.002(5) 0.000(4) -0.003(4) C1 0.036(5) 0.048(6) 0.035(4) 0.002(5) 0.000(4) -0.003(4) C3 0.052(10) 0.052(10) 0.045(9) 0.008(7) -0.008(7) -0.022(13) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _axis.id _axis.type _axis.equipment _axis.parity _axis.depends_on _axis.zero _axis.vector[1] _axis.vector[2] _axis.vector[3] source . source . . . 1.00000000 0.00000000 0.00003403 omega rotation goniometer -1 . 0.12240000 0.00000000 0.00000000 1.00000000 kappa rotation goniometer -1 omega 0.28425000 -0.76560404 0.00000000 0.64331210 phi rotation goniometer -1 kappa . -0.00006266 0.00000000 1.00000000 theta rotation goniometer -1 . 0.19892000 0.00000000 0.00000000 1.00000000 matrixX general general . phi . 1.00000000 0.00000000 0.00000000 matrixY general general . phi . 0.00000000 1.00000000 0.00000000 matrixZ general general . phi . 0.00000000 0.00000000 1.00000000 dacX translation general . phi . 0.00000000 1.00000000 0.00000000 dacY translation general . phi . -1.00000000 0.00000000 0.00000000 dacZ translation general . phi . 0.00000000 0.00000000 1.00000000 loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u _diffrn_refln_scale_group_code -2 0 2 186.382 13.1374 1 -2 -2 0 178.868 13.0442 2 -2 -2 0 172.874 12.9358 5 -2 0 2 167.577 12.3206 3 2 0 -2 178.518 12.7178 1 -2 2 2 2518.68 166.109 3 -2 2 2 2214.22 171.892 7 -2 -2 2 2125.76 165.605 1 2 -2 -2 2434.85 193.444 9 2 -2 -2 2636.87 176.255 2 0 3 1 434.134 30.6971 3 0 -3 -1 459.078 31.4634 5 0 3 -1 452.529 34.7362 4 0 3 1 429.161 36.8913 9 0 -3 1 462.155 35.5175 6 0 -3 -1 455.874 31.375 1 -3 -1 0 434.951 31.327 1 3 0 -1 385.132 30.4354 7 3 0 -1 482.416 33.4233 6 1 3 0 385.728 29.1261 3 -3 0 1 430.229 29.9977 1 -3 0 1 429.843 29.4271 3 -1 3 0 449.575 33.0197 4 -3 0 1 400.301 30.0008 5 1 3 0 412.117 30.1215 8 -2 1 3 68.6057 4.98212 3 1 3 -2 67.6254 6.49139 4 3 2 -1 70.7526 4.93611 8 -1 -3 -2 71.1209 4.94229 1 -1 3 2 80.1273 5.46488 7 -3 -2 -1 74.8583 5.07321 1 3 2 -1 72.6023 5.70523 9 -1 3 2 77.6368 4.61791 1 1 -3 -2 63.9125 6.74814 9 3 -2 -1 68.717 5.0035 8 1 -3 -2 68.0672 4.97932 1 1 -3 -2 70.7432 5.4204 2 3 -2 -1 62.7472 6.54408 9 -3 -2 1 63.2315 5.31835 1 3 2 1 59.0685 5.19541 7 -3 -2 1 62.1018 5.32026 5 1 3 2 63.3433 5.57809 7 -3 1 2 77.0209 4.48855 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140.063 10.8212 5 7 -3 -2 140.56 14.7912 6 7 -3 -2 138.248 14.2993 9 -7 -3 2 141.591 10.6754 2 2 -7 -3 123.995 14.505 9 -7 -3 2 145.898 10.8255 1 -7 -3 2 124.87 9.77534 3 2 7 3 148.215 11.8538 7 2 -7 -3 134.041 12.6442 1 -2 7 5 38.5217 6.60283 7 -2 -7 -5 31.8196 4.56181 1 -7 -5 -2 34.4994 5.11522 1 -7 5 2 33.9523 5.28932 3 -2 -7 -5 33.4157 5.68108 2 7 5 -2 35.87 6.33996 9 -2 7 5 30.1318 4.67012 3 7 5 -2 31.4144 5.37294 8 -7 -5 2 25.8928 4.66269 5 -7 -5 2 30.0978 4.73066 1 7 -5 -2 37.7196 8.52062 6 2 -7 -5 36.6248 3.16709 1 -7 -5 2 20.1232 5.13568 2 7 -5 -2 30.4858 8.61636 9 2 -7 -5 30.08 3.10586 5 2 -7 -5 31.4117 4.87325 2 2 7 5 27.3421 6.08571 7 -7 0 3 20.6151 3.45086 3 3 -7 0 35.7799 7.35284 6 -3 -7 0 15.2246 3.49528 5 3 -7 0 20.9688 6.37523 9 -7 0 3 19.9742 3.06478 1 -7 0 3 19.5991 2.98555 5 7 0 -3 36.3484 7.2588 9 -3 -7 0 25.7752 3.67883 1 3 7 -2 128.971 10.1493 8 7 2 -3 128.526 12.6453 4 -3 -7 -2 138.068 10.5092 5 7 2 -3 132.54 10.3702 8 -3 -7 -2 128.372 11.1637 2 -3 7 2 131.48 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53.6009 5.2217 8 4 -7 -3 60.1567 8.8948 9 7 5 -4 97.6263 11.7182 4 7 5 -4 103.872 12.0703 9 -4 7 5 109.482 10.9421 7 -5 4 7 115.142 9.71811 3 -7 5 4 112.624 9.44807 3 -7 5 4 107.978 10.2842 7 7 5 -4 105.299 9.36646 8 7 -5 -4 108.582 8.11164 2 5 -4 -7 80.7592 7.67295 1 7 -5 -4 130.158 13.3551 9 7 -5 -4 114.984 8.35633 8 -7 -5 4 106.664 9.49072 1 4 -7 -5 100.649 8.85879 2 4 -7 -5 114.551 13.0678 9 -7 0 5 184.907 13.4739 3 -5 -7 0 176.113 14.523 2 5 -7 0 167.858 18.8368 9 -7 0 5 192.994 13.6044 1 5 7 0 167.399 16.2922 9 7 0 -5 184.134 13.8736 8 7 0 -5 185.021 17.9123 9 5 7 -2 34.5768 4.64077 8 -7 2 5 31.2817 5.17238 3 -7 2 5 36.907 3.86309 1 -5 -7 -2 37.062 5.08268 1 -5 7 2 35.358 4.52911 4 7 2 -5 30.6233 7.76214 9 -5 -7 -2 28.0086 4.94458 5 -5 -7 -2 22.997 5.56612 2 -5 -7 2 21.0102 4.70975 1 -7 -2 5 35.8825 4.99501 1 5 7 2 27.9778 4.92183 7 7 -2 -5 34.0589 4.6346 8 -5 -7 2 30.1743 4.74511 6 5 -7 -2 23.6309 7.80997 9 7 4 -5 113.021 9.94124 8 5 7 -4 110.027 9.82674 8 -7 4 5 117.554 10.0496 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7.56492 3 -7 6 7 42.1315 7.58259 3 7 7 -6 40.3878 7.94677 8 -7 7 6 62.7462 8.31578 3 7 -7 -6 49.0843 11.2542 9 7 -6 -7 49.6929 10.8791 9 -7 -7 6 12.1774 16.1359 1 7 -7 -6 51.7505 5.48993 8 0 -8 0 2189.91 161.395 1 0 -8 0 1916.26 163.904 9 0 -8 2 49.2968 12.2142 6 0 -8 -2 57.8327 5.94143 1 0 8 2 58.7151 5.91263 3 -8 -2 0 73.5232 6.69655 1 0 8 -2 77.1322 8.43622 4 0 8 4 616.228 46.2627 7 0 -8 -4 603.879 44.4276 2 0 -8 -4 591.359 43.8625 1 -8 -4 0 619.373 43.7989 5 -8 -4 0 597.527 43.9369 1 0 -8 -4 624.032 43.3026 5 0 8 4 612.92 41.8647 3 -8 -6 0 221.744 18.3161 1 -8 -6 0 233.962 18.1567 5 -8 -6 0 241.751 18.3002 2 0 8 6 217.204 20.3045 7 8 6 0 237.27 21.5497 9 0 -8 -6 243.966 18.4723 2 0 -8 -6 246.935 17.7241 1 -1 8 1 90.4988 7.4381 3 1 8 -1 86.665 9.37896 4 8 1 -1 96.6235 10.768 9 -1 -8 -1 114.141 8.19497 1 1 -8 1 116.231 10.9853 6 -8 1 1 105.023 7.68703 1 1 -8 1 71.2106 9.65078 9 1 8 -1 79.2631 6.65669 8 -1 8 -1 88.3433 8.8915 4 -1 -8 1 64.9825 7.93045 9 8 -1 -1 88.3917 10.6752 9 1 8 1 82.7543 6.73399 3 -1 -8 1 84.345 8.48923 6 1 -8 -1 75.3218 9.31155 9 -1 -8 1 72.206 12.5515 1 -8 -1 1 88.7314 7.46519 1 -1 -8 -3 132.301 11.5882 2 -8 -3 -1 149.164 11.7407 1 1 8 -3 143.061 13.4596 4 -1 -8 -3 136.465 10.93 1 -1 8 3 132.105 10.7356 3 -1 -8 -3 143.073 10.9711 5 8 3 -1 132.892 14.132 9 1 -8 -3 147.231 11.476 2 8 -3 -1 127.586 15.6226 9 -8 -3 1 144.692 11.4763 1 -8 -3 1 129.713 10.1842 3 1 8 3 145.234 12.7296 7 1 -8 -3 147.692 11.0043 1 -8 -3 1 139.476 11.3348 5 1 8 3 141.976 10.5075 3 -1 -8 -5 98.0172 8.10723 1 -1 -8 -5 91.5678 8.92655 2 -1 8 5 92.3087 8.14366 3 8 5 -1 82.9126 10.1945 9 -8 -5 -1 79.2092 8.7054 1 1 -8 -5 86.4635 8.79371 2 1 -8 -5 100.288 7.59265 1 -8 -5 1 89.9877 9.02763 2 -8 -5 1 84.3196 8.72507 1 1 -8 -5 97.9746 7.26543 5 -8 -5 1 79.0832 6.72965 3 8 -5 -1 97.3698 13.5845 9 1 8 5 99.7681 9.99414 7 -8 -5 1 99.9165 8.79375 5 -8 -7 -1 117.308 10.6221 1 8 7 -1 124.191 12.4067 9 -8 -7 -1 117.606 10.8363 2 8 7 1 101.235 8.98058 7 -8 -7 1 110.613 10.2973 2 -8 -7 1 123.975 10.427 1 -8 -7 1 88.7728 9.71797 5 8 -7 -1 106.437 22.4698 6 8 -7 -1 106.593 16.4673 9 8 0 -2 67.362 6.97964 4 8 0 -2 54.8895 8.88871 9 -2 8 0 69.3066 7.39523 4 2 -8 0 59.4864 7.67474 6 2 -8 0 68.2227 8.41396 9 2 8 0 58.5334 5.13269 3 -8 0 2 49.3403 5.62724 3 -2 -8 0 67.9942 6.71211 1 -8 0 2 60.1698 5.94188 5 -8 0 2 64.6248 5.93001 1 -2 -8 -2 130.722 9.62119 1 2 8 -2 112.011 11.8508 4 8 2 -2 108.011 9.82683 8 -2 8 2 120.251 9.38068 3 -8 2 2 121.988 9.11886 1 -8 2 2 123.52 9.53478 3 -2 -8 -2 117.165 9.3477 5 2 8 -2 116.815 9.00582 8 8 2 -2 126.29 12.7324 9 -2 -8 2 105.832 11.8347 6 -2 -8 2 95.3222 14.7458 1 2 -8 -2 109.888 11.4231 9 -8 -2 2 113.211 8.99852 5 2 8 2 121.774 8.37504 3 -8 -2 2 120.348 9.16548 1 -8 -2 2 117.938 8.36589 3 -2 -8 -4 132.105 11.1945 2 -2 -8 -4 114.411 10.0444 1 -8 4 2 111.556 10.8303 7 -2 8 4 142.097 11.8103 7 -2 -8 -4 117.675 9.93554 5 8 4 -2 123.651 10.5769 8 -2 8 4 138.4 10.4653 3 8 4 -2 105.53 13.0843 9 -8 -4 2 106.348 9.06056 3 8 -4 -2 146.32 15.0631 9 2 -8 -4 133.97 10.8439 2 -8 -4 2 119.039 10.5667 2 2 -8 -4 129.019 10.4411 1 8 -4 -2 132.073 18.2341 6 -8 -4 2 117.71 10.4652 5 2 8 4 128.221 11.7525 7 -8 -4 2 125.921 10.9118 1 8 6 -2 17.7311 6.75572 9 -8 6 2 16.6746 5.87218 3 8 6 -2 21.862 5.77721 8 -2 8 6 20.822 7.09634 7 -2 8 6 9.90181 5.14628 3 -8 -6 -2 23.8486 5.92728 1 -8 -6 2 20.9417 5.76772 2 2 -8 -6 32.9753 3.27299 1 2 -8 -6 28.9727 3.17165 5 -8 -6 2 24.7355 5.23636 5 2 -8 -6 25.3026 5.28263 2 8 -6 -2 30.7311 11.0851 9 8 -6 -2 25.7428 12.1331 6 -8 -6 2 23.8845 5.21823 1 -3 -8 -1 130.539 10.7009 5 3 8 -1 127.772 10.2882 8 -3 8 1 138.564 11.771 4 -8 1 3 133.435 10.4871 3 3 8 -1 122.037 9.52842 3 8 1 -3 128.661 14.2247 9 -3 -8 -1 129.699 10.8829 1 8 1 -3 125.614 12.5206 4 -8 1 3 143.626 10.3115 5 3 -8 1 140.073 17.692 6 -8 1 3 132.283 10.3301 1 3 -8 -1 129.582 12.0005 6 -8 -1 3 125.305 10.2868 3 8 -1 -3 142.109 10.6192 8 3 8 1 112.618 9.63817 3 -8 -1 3 140.311 10.4052 5 8 -1 -3 133.619 14.3903 9 -8 -1 3 124.194 10.4627 1 -3 -8 1 146.466 11.4821 1 8 -1 -3 131.482 17.1598 6 3 -8 -1 120.09 13.5466 9 8 3 -3 32.7955 6.63135 4 -3 -8 -3 26.8258 4.76949 1 3 8 -3 30.7113 4.42227 8 8 3 -3 30.5002 6.89323 9 8 3 -3 30.5194 5.09322 8 -8 3 3 30.6782 3.30699 1 -3 8 3 33.3067 5.1296 3 -3 -8 -3 24.9164 4.49461 5 3 8 -3 22.215 6.62879 4 -8 3 3 29.4439 3.24136 5 -8 3 3 28.8901 4.9276 3 3 -8 -3 26.8523 7.72923 9 -8 -3 3 33.2123 4.44325 5 8 -3 -3 31.9885 8.42631 9 8 -3 -3 39.4618 8.56602 6 3 8 3 40.4625 6.09176 7 -8 -3 3 31.9409 3.45978 3 -8 -3 3 29.9634 4.53022 1 8 -3 -3 37.5675 4.80484 8 -8 -3 3 39.1223 4.64551 2 8 5 -3 86.3452 8.51188 8 8 5 -3 74.7765 10.3429 4 -3 8 5 77.0459 10.2272 7 -3 8 5 79.39 8.44537 3 -8 5 3 92.0828 8.73719 3 8 5 -3 86.2278 11.0823 9 -3 -8 -5 87.6793 8.31687 1 -8 5 3 83.6234 7.00563 1 -8 5 3 98.2196 9.19442 7 -3 -8 -5 71.0358 9.06916 2 -8 5 3 85.1664 6.77713 5 8 -5 -3 103.397 11.8328 6 8 -5 -3 108.13 13.2402 9 -8 -5 3 94.3575 8.71781 1 3 -8 -5 101.556 8.66846 2 -8 -5 3 87.4471 8.83213 2 3 8 5 119.67 10.4649 7 -8 7 3 230.981 19.1401 7 8 7 -3 218.208 17.615 8 8 7 -3 243.31 22.4358 9 -8 7 3 246.904 18.1658 3 8 7 -3 241.805 20.863 4 -3 8 7 235.735 17.4338 3 -8 -7 3 210.319 17.7917 2 3 -8 -7 222.849 15.8578 5 -8 -7 3 213.178 17.4809 1 8 -7 -3 244.512 20.7452 6 8 -7 -3 228.242 22.8878 9 -4 -8 0 599.38 42.8327 5 8 0 -4 608.697 53.7964 9 8 0 -4 658.117 48.7719 6 -8 0 4 641.757 42.4198 3 -4 -8 0 581.897 42.9623 1 -4 8 0 589.301 42.9704 8 4 -8 0 615.068 47.4393 6 4 -8 0 518.099 52.0053 9 -8 0 4 597.336 42.8285 1 8 0 -4 607.49 41.536 8 -4 -8 -2 110.703 10.9873 2 4 8 -2 105.772 12.3963 4 -4 8 2 127.076 11.0286 4 4 8 -2 113.962 9.73382 8 8 2 -4 119.896 13.4558 4 -8 2 4 122.513 9.38078 1 -8 2 4 116.593 10.2057 3 -4 8 2 126.388 10.6075 3 -4 -8 -2 129.157 10.409 5 8 2 -4 112.47 14.1189 9 -4 -8 -2 131.065 10.6847 1 -4 -8 2 124.647 11.825 6 8 -2 -4 130.892 10.1168 8 4 -8 -2 138.071 14.3488 9 -8 -2 4 136.39 10.0484 2 -8 -2 4 131.246 10.2773 1 8 -2 -4 137.047 11.6981 6 -8 -2 4 127.526 9.57767 3 -4 8 4 1493.76 101.234 3 4 8 -4 1493.52 115.205 4 -8 4 4 1504.91 102.604 3 4 8 -4 1457.47 105.05 8 -4 8 4 1509.48 107.363 7 8 4 -4 1452.03 100.133 8 -8 4 4 1349.59 102.776 1 -4 -8 -4 1502.31 102.626 1 8 4 -4 1488.49 117.977 4 8 4 -4 1377.76 130 9 -4 -8 -4 1252.48 104.165 2 -8 -4 4 1442.69 106.184 2 8 -4 -4 1588.33 130.248 9 4 -8 -4 1589.77 107.703 2 8 -4 -4 1584.75 104.771 8 4 -8 -4 1583.93 128.244 9 4 8 4 1502.03 110.051 7 4 -8 -4 1460.52 102.664 8 8 -4 -4 1545.5 108.789 6 -4 -8 4 1067.66 124.651 1 -8 -4 4 1509.33 106.458 1 8 6 -4 50.7154 8.61643 9 -8 6 4 43.271 7.53816 7 8 6 -4 56.0647 9.63941 4 -4 8 6 53.0702 7.13907 3 8 6 -4 58.1713 7.13029 8 -4 8 6 47.8806 8.61304 7 -8 6 4 44.9386 7.21754 3 -8 -6 4 48.418 6.90824 1 8 -6 -4 44.5931 5.68045 8 8 -6 -4 50.4494 8.36559 6 4 -8 -6 50.3542 6.10597 2 8 -6 -4 58.2221 11.9009 9 -5 -8 -1 100.949 8.89372 1 -8 1 5 91.9064 7.34042 1 8 1 -5 82.1386 12.5434 9 8 1 -5 88.7783 8.07503 6 -5 -8 -1 86.2606 9.29664 2 -5 -8 -1 88.9455 8.71298 5 -8 1 5 101.923 8.54828 3 -8 -1 5 97.6416 7.92021 1 -8 -1 5 91.504 8.01462 3 8 -1 -5 88.9584 8.31389 8 -8 -1 5 103.701 7.54433 2 5 -8 -1 86.4015 13.3542 9 8 -1 -5 95.1386 12.2875 9 5 8 -3 86.1604 8.13509 8 8 3 -5 83.2851 8.64946 8 -5 -8 -3 74.1638 9.24146 2 -5 8 3 76.729 8.52878 3 -5 -8 -3 76.6071 8.67705 1 -8 3 5 87.2828 6.74612 1 -5 -8 -3 92.357 8.5737 5 -8 3 5 91.9552 8.53419 3 8 3 -5 83.606 11.5772 9 5 -8 -3 87.2021 12.2698 9 5 8 3 98.4474 9.10787 7 -8 -3 5 93.2428 8.7326 1 8 -3 -5 96.5033 8.08006 8 -5 -8 3 94.8629 10.8742 1 -8 5 5 109.32 10.8027 3 8 5 -5 104.368 11.1676 8 5 8 -5 117.645 11.0119 8 8 5 -5 132.196 14.5923 4 -5 8 5 117.082 11.0138 3 -5 8 5 98.8247 12.0337 7 5 -8 -5 126.439 10.4273 2 8 -5 -5 117.626 15.4437 9 -8 -5 5 92.7838 11.1194 1 5 -8 -5 122.384 9.14197 8 5 -8 -5 146.716 16.5137 9 8 -5 -5 126.472 9.85557 8 8 7 -5 101.692 13.475 4 -8 7 5 86.7053 11.0604 7 -8 7 5 97.6854 10.7264 3 8 7 -5 118.713 10.5899 8 -7 5 8 108.854 10.5144 3 8 -7 -5 107.068 8.80118 8 -8 -7 5 98.7101 12.4612 1 -6 -8 0 240.981 18.6738 2 -8 0 6 248.323 17.6046 3 -6 -8 0 241.379 18.1918 5 6 8 0 214.475 21.3018 9 8 0 -6 257.966 23.5137 9 8 0 -6 261.127 18.2234 8 6 -8 0 207.911 25.7379 9 -8 0 6 224.714 19.6208 1 -6 -8 -2 18.7892 5.2356 5 8 2 -6 14.7507 7.56518 9 -6 -8 -2 16.1902 6.16262 2 -8 2 6 15.8604 5.27764 3 6 8 -2 17.973 5.2044 8 -8 2 6 11.0005 7.23727 1 -6 -8 -2 17.3596 5.28965 1 -6 -8 2 18.719 5.26681 1 8 -2 -6 26.0886 4.81242 8 -6 -8 2 19.5449 4.85355 6 6 8 2 23.6418 5.29777 7 -8 -2 6 21.7761 6.32 1 6 -8 -2 37.3616 10.5475 9 6 -8 -2 37.0503 8.6962 6 -6 8 4 47.0844 8.08625 7 6 8 -4 42.1127 7.0785 8 -8 4 6 56.9479 7.41845 3 -6 -8 -4 36.4206 6.94914 1 8 4 -6 59.7822 7.86924 8 8 -4 -6 53.3874 10.7505 9 -6 -8 4 48.1499 9.83893 1 6 -8 -4 59.657 11.3977 9 -8 -4 6 49.8286 9.77892 1 8 -4 -6 37.157 5.88345 8 -6 6 8 62.2437 8.12503 3 -8 6 6 55.0055 8.26656 3 -6 8 6 50.3757 8.77097 7 6 8 -6 50.3644 8.66099 8 8 6 -6 57.8327 8.30474 8 6 -8 -6 57.2049 5.39857 8 6 -8 -6 49.9328 12.0029 9 6 -8 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6.72359 8 -8 -8 0 1263.55 81.0453 1 8 8 0 1133.51 98.5205 9 -8 -8 0 1130.79 79.9218 2 8 -8 0 1006.84 103.396 9 -8 -8 -2 107.704 11.3761 2 8 8 -2 124.782 12.7385 9 -8 8 2 132.439 12.1991 3 8 8 2 108.479 10.4476 7 -8 -8 2 130.39 12.5188 2 8 -8 -2 122.99 18.2645 9 -8 -8 2 122.739 11.5041 1 8 -8 -2 105.272 17.7614 6 -4 8 8 448.816 30.9387 3 -8 8 4 412.864 31.5856 3 8 8 -4 406.284 31.6401 8 -8 8 4 412.149 33.8546 7 -8 4 8 430.865 30.9694 3 8 8 -4 405.359 35.546 4 4 -8 -8 399.571 29.8562 5 -8 -8 4 429.218 31.7385 1 8 -8 -4 439.159 32.2729 6 -8 8 6 97.8084 10.2552 3 -8 8 6 85.5702 11.4072 7 8 8 -6 80.2282 10.8513 8 -8 6 8 88.8254 10.156 3 8 -6 -8 85.7734 8.52455 8 -8 -8 6 77.2705 19.0919 1 8 -8 -6 87.2649 7.78353 8 -8 8 8 364.838 26.9982 3 8 -8 -8 323.042 24.8189 8 0 -9 1 143.973 13.9089 6 0 9 1 135.494 10.617 3 -9 -1 0 130.444 11.4612 1 0 9 -1 144.534 9.9413 8 0 9 -1 138.282 13.6799 4 0 -9 -1 143.283 14.3637 1 0 -9 1 115.58 13.2406 9 -9 -3 0 38.5301 5.53432 1 0 -9 -3 37.4699 6.29365 2 0 9 3 30.4859 4.92412 3 0 -9 -3 36.133 4.45494 1 0 9 5 13.4758 6.86729 7 0 9 5 0.80238 4.26326 3 0 -9 -5 4.85588 5.21011 2 -9 -5 0 1.86259 4.91637 1 0 -9 -5 1.00666 2.90782 5 -9 -5 0 2.58561 4.76824 5 0 -9 -5 0.23733 2.97985 1 -9 -7 0 79.0436 8.54804 1 9 7 0 71.5056 9.41748 9 9 7 0 68.2646 6.38938 7 -9 -7 0 60.613 8.32595 2 -9 -7 0 72.8629 8.39208 5 9 -7 0 54.2618 16.6387 9 1 -9 0 128.645 14.3909 9 1 9 0 136.594 10.8458 3 -1 -9 0 161.313 14.7809 1 9 0 -1 155.877 15.3279 9 -1 9 0 143.098 13.4209 4 -9 0 1 152.063 11.711 1 1 -9 0 134.128 12.6962 6 -1 9 2 94.7209 7.84739 3 9 2 -1 93.842 11.4899 9 -1 -9 -2 96.4159 7.95214 1 1 9 -2 84.562 9.73241 4 1 9 -2 93.0893 7.03077 8 1 -9 2 71.0419 15.8365 6 -9 -2 1 76.5349 7.72316 5 1 9 2 82.6524 7.36282 3 -9 -2 1 82.9913 8.08395 1 1 -9 -2 72.9328 11.6054 1 -1 9 -2 89.0033 9.82528 4 -1 -9 2 61.8479 11.8667 6 -9 -4 -1 32.9136 6.08084 1 -1 9 4 32.7089 5.59884 3 9 4 -1 35.36 7.95892 9 -1 -9 -4 35.597 4.88616 1 -1 -9 -4 33.3845 6.14017 2 -1 -9 -4 35.9037 4.94944 5 1 9 4 38.4778 7.74241 7 -9 -4 1 44.3698 5.7252 5 1 9 4 47.978 5.32348 3 1 -9 -4 49.7399 6.49164 2 1 -9 -4 47.8858 4.81588 1 -9 -4 1 44.0254 3.95908 3 -9 -4 1 41.605 6.22239 1 9 -4 -1 48.0303 11.2793 9 -1 -9 -6 7.36476 5.54843 2 -9 -6 -1 11.2666 5.88051 1 -1 9 6 6.95789 5.23164 3 -9 -6 -1 10.9611 5.63938 5 -1 -9 -6 11.9407 4.04835 1 9 6 -1 8.40356 7.32699 9 -9 -6 1 10.2723 5.41891 5 1 -9 -6 -2.6883 5.35632 2 1 -9 -6 1.68112 2.74087 5 1 9 6 14.2981 7.27275 7 -9 -6 1 4.32272 5.57803 1 9 -6 -1 13.4866 12.5065 9 1 -9 -6 4.46773 2.99269 1 -9 -6 1 2.21442 5.87943 2 9 8 -1 89.3039 11.2538 9 -9 -8 -1 93.0431 9.95529 1 -9 -8 -1 95.1863 9.7068 2 -9 -8 1 84.855 9.42339 5 -9 -8 1 91.9634 9.72976 1 9 8 1 77.1002 7.96738 7 -9 -8 1 82.6342 10.1523 2 -9 1 2 95.9949 7.49352 1 -9 1 2 100.756 7.49684 5 2 9 -1 93.8114 7.2235 8 2 -9 1 79.6861 12.8854 6 9 1 -2 84.6712 11.2126 9 2 -9 1 68.9232 11.1732 9 2 9 -1 75.1459 10.0613 4 -9 1 2 77.2663 7.63755 3 -2 9 1 97.4068 8.01524 3 -2 -9 -1 91.7455 7.93817 1 -9 -1 2 84.533 7.6047 5 -9 -1 2 75.1421 7.05964 3 2 9 1 76.7238 6.75707 3 -2 -9 1 72.0427 10.9342 1 9 -1 -2 76.9945 10.7055 9 9 -1 -2 81.0269 8.54791 4 2 -9 -1 68.5629 10.5552 9 -2 -9 1 79.2079 8.45202 6 -2 9 -1 92.9671 9.77657 4 -9 -1 2 83.6733 7.50415 1 9 3 -2 6.05839 1.67678 7 9 3 -2 3.20768 7.37832 9 -2 -9 -3 5.27736 3.42341 5 -9 3 2 8.34814 4.46592 3 -2 9 3 3.90472 4.54609 3 -9 3 2 13.2894 2.97944 1 2 9 -3 7.79291 3.75883 8 2 9 -3 9.36762 6.60145 4 -2 -9 -3 2.67019 5.22956 2 -2 -9 -3 9.51285 3.5302 1 2 -9 -3 4.36323 7.27865 9 -9 -3 2 5.49023 4.13034 5 2 9 3 4.637 5.92838 7 -9 -3 2 4.49883 4.10886 1 -9 -3 2 9.58725 2.80436 3 2 9 3 7.62186 3.23058 3 -2 -9 -5 118.371 11.5629 2 9 5 -2 125.948 14.1697 9 -9 5 2 109.634 11.3698 7 -2 -9 -5 132.814 10.6722 1 -2 -9 -5 130.868 10.6031 5 -2 9 5 140.924 10.9892 3 9 -5 -2 85.8674 21.7404 6 2 9 5 149.318 12.8901 7 2 -9 -5 127.567 10.4055 1 -9 -5 2 141.84 11.5712 1 -9 -5 2 137.632 11.69 2 9 -5 -2 137.518 17.4793 9 -9 -5 2 111.521 9.17826 3 -9 -5 2 114.358 11.1135 5 2 -9 -5 124.292 11.2032 2 9 7 -2 86.1202 11.7096 9 -2 9 7 90.0638 10.0067 3 -9 7 2 85.7708 10.1903 3 -9 -7 -2 84.5228 9.38504 5 -9 -7 -2 97.7946 10.2571 1 9 -7 -2 119.425 21.166 6 9 -7 -2 95.2186 17.5899 9 -9 -7 2 96.9505 9.3631 5 2 -9 -7 94.6487 7.39814 5 2 -9 -7 79.0039 7.3822 1 -9 -7 2 75.3688 9.23763 1 -9 -7 2 83.0733 9.70057 2 3 -9 0 36.7268 9.22586 6 -3 9 0 42.039 6.58052 4 -3 -9 0 38.9038 5.41194 1 -9 0 3 34.0599 4.61197 1 -9 0 3 40.6612 4.69604 5 9 0 -3 26.3121 7.37846 4 3 -9 0 31.7937 8.63825 9 9 0 -3 39.2665 8.79053 9 3 9 0 39.1141 3.84264 3 9 0 -3 43.0553 5.7171 8 -9 0 3 29.4539 4.93469 3 -9 2 3 6.92278 2.9879 1 9 2 -3 10.8594 7.53212 9 -3 -9 -2 10.352 5.62089 2 -3 -9 -2 13.5714 3.67222 5 3 9 -2 4.52035 3.44786 8 -3 -9 -2 6.76453 3.7988 1 -3 9 2 8.58545 4.66657 3 9 2 -3 1.64739 5.86153 4 -9 2 3 5.41745 4.1776 3 -9 2 3 7.70386 2.70046 5 3 9 -2 6.93616 6.46597 4 -3 -9 2 6.11717 6.52768 6 -9 -2 3 2.02494 3.42165 5 -9 -2 3 5.65634 3.31054 3 -3 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-14 3 16.0223 21.6764 1 -14 -3 7 -8.4395 7.90324 1 14 -3 -7 24.7063 15.452 9 7 -14 -3 9.00015 21.6068 9 14 5 -7 17.928 14.5945 9 -7 -14 -5 12.2814 7.96819 5 -14 5 7 20.3253 9.77935 3 -7 14 5 12.2574 12.0321 7 14 5 -7 12.3127 10.5937 8 7 14 -5 3.53209 12.9577 4 -7 14 5 5.63151 10.2954 3 7 -14 -5 20.1205 22.9532 9 -14 -5 7 13.3423 10.5465 1 7 -14 -5 12.3446 9.64001 2 14 -5 -7 6.91209 25.9697 6 -8 -14 0 38.4283 11.0074 1 -14 0 8 34.4411 8.27657 3 14 0 -8 61.3505 10.1638 8 8 -14 0 -22.445 33.2768 9 14 0 -8 40.183 16.521 9 -8 14 0 51.0558 12.6811 3 -8 -14 0 56.768 14.6172 2 -8 -14 -2 2.95258 11.533 2 8 14 -2 6.26471 14.4772 4 -14 2 8 17.6189 8.67169 3 -8 -14 -2 -0.7724 8.67311 1 14 2 -8 6.00828 9.63393 8 14 2 -8 10.7486 14.4882 9 -8 14 2 -7.9429 11.1107 3 -8 -14 2 8.15069 13.678 1 14 -2 -8 19.9042 14.9415 9 8 -14 -2 9.85747 25.9173 9 -8 -14 2 13.626 18.7141 2 14 -2 -8 4.36829 8.82985 8 8 14 2 -8.5748 8.88329 7 -8 -14 -4 15.9879 8.75082 1 8 14 -4 1.64847 13.997 4 -8 -14 -4 2.56444 9.86895 2 -8 14 4 13.2969 10.7036 3 -8 14 4 5.39209 12.1314 7 -14 4 8 15.6189 9.42453 3 -8 -14 -4 18.0925 8.58911 5 8 -14 -4 -3.7931 23.3259 9 -14 -4 8 23.923 13.7933 1 14 -4 -8 2.58086 15.146 9 14 -4 -8 15.7448 9.02578 8 8 14 4 10.1364 9.085 7 -9 14 1 5.11592 12.2144 3 -9 -14 -1 10.1056 12.1798 2 14 1 -9 18.9918 10.4396 8 -9 -14 -1 14.0035 9.13345 1 9 14 -1 5.02158 15.9254 4 -9 -14 1 15.6748 15.1416 2 -9 -14 1 15.9865 11.1497 1 9 -14 -1 14.7236 32.1688 9 14 -1 -9 26.5286 9.76195 8 14 -1 -9 3.51689 15.0497 9 9 14 1 8.39155 8.90044 7 14 3 -9 26.8441 11.98 8 -9 14 3 13.9117 12.7454 7 -9 -14 -3 23.0809 9.76636 1 -9 -14 -3 9.37265 8.75238 5 -9 -14 -3 31.9744 11.0037 2 -14 3 9 13.7424 9.39887 3 -9 14 3 0.723 11.552 3 14 -3 -9 9.78374 9.28653 8 9 -14 -3 17.3564 25.7772 6 -9 -14 3 17.6357 21.2441 2 9 -14 -3 3.73517 28.2877 9 14 -3 -9 20.6655 17.046 9 15 1 0 -8.8851 15.4486 9 0 15 1 14.3719 12.2816 4 0 15 -1 1.35905 7.41051 3 0 15 1 -9.8526 7.59977 3 0 15 -1 0.98447 11.4847 4 0 -15 -1 -0.3818 11.6949 6 0 -15 1 -19.303 19.9489 6 0 -15 -3 65.6816 12.6174 2 15 3 0 14.2942 15.3466 9 0 15 3 54.1251 8.35224 3 -15 -3 0 14.883 8.81674 1 -15 -3 0 52.3652 9.41054 5 15 5 0 33.1771 15.9944 9 -15 -5 0 42.6705 9.11706 5 -15 -5 0 49.6098 10.6318 1 0 15 5 42.8825 8.5825 3 0 -15 -5 40.6913 10.3349 2 0 15 5 49.1426 13.5521 7 15 7 0 12.6968 14.6981 9 0 15 7 21.3343 12.3147 7 -15 -7 0 13.6707 9.65416 1 -15 -7 0 8.33989 9.69175 5 0 -15 -7 7.91142 9.1108 2 -15 0 1 -3.3954 7.25421 1 1 15 0 -0.705 6.63399 3 15 0 -1 15.6143 15.0539 9 -1 15 0 2.18648 10.3988 4 -15 0 1 8.98118 7.0598 3 -1 15 0 -6.2536 8.00632 3 1 15 0 -1.041 13.1676 4 -1 -15 0 -0.4604 13.3917 6 1 -15 0 -7.4031 16.3939 6 -15 0 1 -3.7917 6.85014 5 15 2 -1 42.8462 14.5799 9 1 15 -2 12.7686 12.4139 4 1 -15 2 -3.5908 19.7165 6 1 15 -2 44.0529 7.68638 3 -1 15 2 46.3216 8.96725 3 -1 15 2 46.3522 11.9925 4 -1 -15 -2 34.4808 13.6785 2 15 -2 -1 12.8203 16.8112 9 -1 -15 2 52.2784 25.5202 6 -15 -2 1 39.8249 8.42506 5 -15 -2 1 26.7818 8.16044 1 1 15 2 44.9951 7.90473 3 1 -15 -2 25.2513 12.011 6 -1 15 4 0.33717 12.1199 7 -1 15 4 19.8843 7.94015 3 -1 -15 -4 13.0828 10.4681 2 -1 -15 -4 -4.6272 13.3112 1 15 4 -1 9.05828 15.0877 9 1 -15 -4 16.6018 11.0615 2 1 15 4 32.1636 12.1567 7 -15 -4 1 7.21764 8.06069 1 1 15 4 6.09495 7.05896 3 -15 -4 1 21.3481 7.58897 5 -1 15 6 14.2467 8.60505 3 -15 -6 -1 18.2111 9.48506 5 -1 15 6 19.5124 12.0472 7 -1 -15 -6 22.1822 10.4238 2 15 6 -1 41.9397 15.326 9 1 15 6 22.0911 12.1811 7 -15 -6 1 12.6261 8.98446 1 -15 -6 1 22.6933 8.89305 5 15 6 1 1.56139 13.8253 9 1 -15 -6 25.5772 9.91607 2 15 -6 -1 3.61267 21.5203 9 15 1 -2 49.5742 16.706 9 2 15 -1 6.88977 13.0506 4 -2 -15 -1 36.7505 11.2916 6 -2 -15 -1 1.44883 21.078 1 -15 1 2 35.4843 7.69307 1 -15 1 2 34.1784 6.96312 5 2 -15 1 29.489 27.6992 6 -2 15 1 40.1881 10.8386 4 -15 1 2 26.5368 7.74847 3 15 1 -2 1.36951 10.1569 4 -2 15 1 23.5161 8.7318 3 -15 -1 2 34.2794 8.3448 1 -2 15 -1 56.6153 9.30802 3 2 15 1 3.3922 15.1186 4 15 -1 -2 51.8228 17.736 9 2 15 1 40.3571 7.33148 3 -2 15 -1 48.5566 11.2087 4 -2 -15 1 16.9377 17.3547 6 -15 -1 2 30.2952 7.05632 5 2 -15 -1 33.8074 15.4831 6 -2 15 3 20.3235 8.49803 3 -2 15 3 14.2751 11.2594 4 15 3 -2 8.83264 13.7943 9 2 15 -3 -0.2767 11.1419 4 -2 -15 -3 21.7175 14.2243 1 -15 3 2 13.6692 7.7814 3 15 3 -2 12.9383 10.6185 4 -2 -15 -3 12.0814 11.2035 2 15 -3 -2 14.2294 18.5903 9 2 15 3 11.0707 11.4331 7 2 15 3 9.70155 6.51896 3 -15 -3 2 17.151 7.22476 1 -15 -3 2 24.112 7.49831 5 2 -15 -3 22.67 11.6254 6 -2 15 5 41.1516 12.9354 7 15 5 -2 34.9852 14.7711 9 -15 5 2 23.9908 9.59936 3 15 5 -2 35.9565 11.9564 4 -2 -15 -5 10.1663 8.33682 1 -2 15 5 55.4083 9.65004 3 -2 -15 -5 24.6832 10.3684 2 -15 -5 2 24.7428 7.89859 5 2 15 5 34.5718 12.6799 7 2 -15 -5 33.2396 10.6313 2 -15 -5 2 38.3498 9.32928 1 -2 15 7 71.4922 13.9641 7 -2 15 7 51.6898 10.2814 3 15 7 -2 42.3911 13.7177 4 -2 -15 -7 35.71 9.80147 2 -15 7 2 28.8731 10.7423 3 15 7 -2 34.7017 15.6273 9 2 -15 -7 53.6514 10.3533 2 -15 -7 2 36.9429 9.80148 1 2 15 7 15.9002 12.6131 7 15 -7 -2 28.9211 24.2501 9 -15 -7 2 61.3538 9.94545 5 -15 0 3 54.7724 7.60323 1 -15 0 3 36.3361 7.93009 3 -15 0 3 41.8878 7.29238 5 -3 -15 0 51.3559 25.0298 1 -3 -15 0 37.3916 12.6754 6 15 0 -3 53.3514 16.5063 9 -3 15 0 50.1036 10.0012 3 -3 15 0 58.9367 11.3162 4 3 -15 0 66.3695 24.3681 6 3 15 0 5.00083 15.8578 4 -3 15 2 17.7 10.4056 4 -3 15 2 22.1984 8.62096 3 -15 2 3 12.7313 7.79407 3 15 2 -3 24.1655 14.4106 9 15 2 -3 -1.6729 10.9258 4 3 15 -2 -0.539 12.2256 4 -3 -15 -2 16.6545 13.4843 1 -15 -2 3 21.9501 6.95773 1 3 -15 -2 27.1686 14.0415 6 -15 -2 3 24.3991 6.69359 5 -3 -15 2 15.6965 21.155 6 15 -2 -3 19.9642 16.8146 9 -3 15 4 15.3594 9.21476 3 15 4 -3 11.2715 11.9053 4 15 4 -3 6.35715 14.3083 9 -15 4 3 9.45766 8.38274 3 -3 -15 -4 18.0968 10.6879 2 -3 -15 -4 8.04262 8.26255 1 15 -4 -3 16.9884 18.2502 9 -15 -4 3 11.3158 7.44161 1 3 -15 -4 1.23254 10.6869 2 3 15 4 26.8299 11.4857 7 -15 -4 3 4.36297 7.03925 5 15 6 -3 19.7647 12.5438 4 -15 6 3 30.543 9.73934 3 -3 -15 -6 20.7619 9.76468 2 -3 15 6 42.7697 9.11466 3 15 6 -3 25.9197 15.3473 9 3 -15 -6 16.7102 9.29024 2 3 15 6 13.8793 11.7837 7 15 -6 -3 26.2884 21.0966 9 -15 -6 3 35.6216 8.30218 5 -15 -6 3 28.2696 8.71424 1 4 15 -1 1.49614 14.4805 4 -4 15 1 12.1096 9.2367 3 4 -15 1 33.6547 25.8967 6 15 1 -4 21.3516 14.5405 9 -15 1 4 7.99922 6.9976 3 -4 -15 -1 7.35916 14.6527 1 -4 -15 -1 5.59896 14.1788 2 -15 -1 4 17.7405 6.23798 5 -4 -15 1 10.0091 13.8135 6 4 -15 -1 19.0582 19.5383 6 -4 -15 1 22.023 25.5102 1 15 -1 -4 19.0157 15.6059 9 -15 -1 4 9.74136 6.44374 1 4 15 -3 0.29687 12.3044 4 15 3 -4 -5.9034 14.0773 9 15 3 -4 -14.017 12.3296 4 -15 3 4 -5.9725 7.98273 3 -4 -15 -3 6.47027 9.02096 1 -4 15 3 5.58284 9.18241 3 4 -15 -3 18.1519 13.2218 6 -15 -3 4 13.0407 7.19334 1 15 -3 -4 7.29399 17.1932 9 4 15 3 3.07568 10.5522 7 -15 -3 4 6.45089 6.47168 5 -15 5 4 11.3602 9.38166 3 15 5 -4 18.1592 15.4409 9 -4 15 5 43.1022 13.0552 7 -4 15 5 23.5947 10.1708 3 15 5 -4 15.4491 11.7537 4 -4 -15 -5 7.70628 7.45681 1 -4 -15 -5 33.8627 10.7651 2 4 15 5 17.8954 11.6767 7 4 -15 -5 25.0982 10.304 2 -15 -5 4 13.6015 7.78021 1 -5 -15 0 50.5426 11.7982 6 -5 -15 0 65.9715 16.9598 1 -5 15 0 57.815 11.0495 3 5 15 0 9.52495 16.254 4 -5 -15 0 48.5583 16.8033 2 5 -15 0 16.8949 29.225 6 -15 0 5 50.9813 8.9862 3 15 0 -5 43.6787 15.9397 9 -5 15 2 39.8683 9.90822 3 5 15 -2 3.07485 14.8065 4 -5 -15 -2 34.1493 13.4001 2 15 2 -5 36.847 15.9155 9 -15 2 5 35.3952 8.88371 3 -5 -15 -2 37.6698 10.2963 1 -5 -15 2 -18.675 27.6528 1 15 -2 -5 27.6043 17.0955 9 -15 -2 5 30.654 7.05748 1 5 -15 -2 44.8647 18.8683 6 15 4 -5 6.93674 13.4806 4 -5 15 4 2.62969 9.82531 3 -5 15 4 13.8456 12.7086 7 5 15 -4 7.36233 12.7727 4 -15 4 5 12.8542 8.92181 3 -5 -15 -4 14.4477 7.859 1 15 4 -5 10.8392 14.3328 9 15 -4 -5 28.7277 17.9071 9 -15 -4 5 7.26106 6.87667 1 5 -15 -4 -1.8452 11.0886 2 5 -15 -4 11.0888 12.4183 6 5 15 4 7.88118 10.8532 7 15 6 -5 41.9513 17.5229 9 15 6 -5 32.5578 14.7881 4 -5 15 6 14.1578 10.5909 3 -5 -15 -6 -6.9374 7.77046 5 -5 -15 -6 -2.1409 9.52307 2 -5 15 6 11.5385 13.4271 7 -15 6 5 -2.3843 9.74724 3 5 15 6 9.54777 11.4171 7 -15 -6 5 -3.6269 7.67898 1 15 -6 -5 -8.2618 19.5881 9 5 -15 -6 0.49637 9.30531 2 6 15 -1 1.5829 14.9545 4 15 1 -6 23.7784 15.9154 9 -6 15 1 33.0388 11.1809 3 -15 1 6 32.8588 8.54719 3 -6 -15 -1 50.5444 11.789 1 -6 -15 -1 14.1685 13.9305 2 -6 -15 1 51.6684 18.8122 1 15 -1 -6 35.0277 15.9339 9 6 -15 -1 4.36674 26.1101 6 -6 -15 1 29.3281 18.7956 2 -6 15 3 26.8304 10.7719 3 6 15 -3 2.78359 13.7044 4 -6 -15 -3 34.3478 11.9952 2 -15 3 6 16.056 9.51904 3 15 3 -6 29.8004 16.678 9 -6 -15 -3 20.1895 8.5525 1 6 15 3 16.8533 10.5601 7 15 -3 -6 25.8725 16.6933 9 6 -15 -3 -4.8481 17.0185 6 -15 -3 6 18.958 7.11132 1 -6 -15 -5 2.3867 7.36129 5 -6 15 5 19.5837 13.552 7 -6 -15 -5 -3.143 7.9975 1 -6 15 5 21.361 11.4125 3 6 15 -5 1.02449 12.832 4 -15 5 6 -1.7808 9.93723 3 15 5 -6 42.0275 18.9988 9 6 15 5 11.7594 11.3049 7 6 -15 -5 -10.969 13.2679 6 6 -15 -5 0.27639 10.463 2 -15 -5 6 0.34625 7.71357 1 -7 15 0 -0.7429 11.8483 3 -7 -15 0 -4.7056 15.6231 2 15 0 -7 23.9985 9.4913 8 -7 -15 0 14.1709 12.7055 1 15 0 -7 5.96081 14.9036 9 7 15 0 -5.5362 16.3281 4 15 2 -7 32.1093 11.1817 8 7 15 -2 6.3757 17.4898 4 -7 -15 -2 45.0696 12.8983 2 -7 -15 -2 50.6113 10.305 1 15 2 -7 41.5596 16.8212 9 -7 15 2 39.204 11.8016 3 -15 2 7 43.8972 9.29493 3 -7 -15 2 12.8513 21.5537 2 7 15 2 31.073 11.3959 7 15 -2 -7 35.1872 16.8128 9 7 -15 -2 36.7385 26.2223 6 -7 -15 2 41.4578 22.1214 1 0 16 0 156.918 14.8441 3 0 -16 0 182.917 25.3953 6 0 16 -2 4.87191 12.8799 4 0 16 -2 26.3943 8.45943 3 0 16 2 52.5278 9.49147 3 16 2 0 -4.0981 15.9122 9 0 -16 2 1.24236 18.9286 6 -16 -2 0 1.42507 8.21715 5 0 16 2 46.3633 13.5021 4 0 -16 -2 36.1025 13.0295 6 -16 -4 0 143.545 15.9776 5 0 -16 -4 158.774 18.0734 2 0 16 4 173.654 14.6452 3 0 16 4 175.999 19.4202 7 1 -16 1 31.7458 29.2249 6 -16 1 1 38.4546 8.52679 5 -1 -16 -1 42.6582 14.3545 6 -1 16 1 59.0184 9.67502 3 16 1 -1 46.737 17.7461 9 -16 1 1 66.2523 9.42538 3 1 16 -1 7.51106 12.9376 4 -1 16 1 55.2376 13.4669 4 1 16 1 7.67619 15.418 4 -1 -16 1 57.8009 24.5228 6 1 16 1 65.0803 9.32529 3 16 -1 -1 12.2366 16.5443 9 -16 -1 1 54.5022 8.86206 5 -1 16 -1 49.5226 9.7974 3 -1 16 -1 40.0916 13.4277 4 1 -16 -1 60.5167 17.153 6 -16 -1 1 47.7295 8.91681 1 -1 -16 -3 20.9403 13.2712 2 -1 16 3 39.884 9.23933 3 -1 16 3 35.8213 13.7187 4 16 3 -1 18.5392 15.8959 9 -16 3 1 12.1795 8.58654 3 1 16 3 29.6489 13.2216 7 -16 -3 1 31.253 8.52369 5 1 -16 -3 29.3309 13.739 2 1 -16 -3 26.265 13.2357 6 1 16 3 18.9929 7.84488 3 16 -3 -1 10.6394 18.0433 9 -16 -3 1 16.2488 8.88082 1 16 5 -1 3.44761 16.7597 9 -16 5 1 8.24321 8.93235 3 -1 16 5 11.6505 13.9322 7 -1 16 5 27.4876 9.42891 3 -1 -16 -5 21.3307 10.8126 2 1 -16 -5 13.7051 11.5581 2 1 16 5 -4.9084 13.5198 7 -16 -5 1 2.5334 8.73919 1 -16 -5 1 14.4788 9.09214 5 16 0 -2 43.1316 18.5832 9 2 -16 0 41.1859 21.7471 6 -16 0 2 33.0941 8.34733 1 -16 0 2 38.6017 7.61183 5 -2 16 0 40.4523 9.11055 3 -2 16 0 54.8896 12.4135 4 2 16 0 1.20387 15.555 4 -2 -16 0 41.9958 16.8175 6 -2 -16 -2 13.0569 15.1531 2 -16 2 2 39.0685 8.57692 3 -2 -16 -2 7.52852 23.4696 1 2 16 -2 4.80059 13.5774 4 -2 16 2 22.3453 12.5452 4 16 2 -2 25.2584 16.5024 9 -2 16 2 11.7878 9.11233 3 -2 16 -2 31.2532 9.78745 3 -2 -16 2 14.9034 25.9046 6 2 -16 -2 46.2954 14.8911 6 16 -2 -2 58.2039 19.9064 9 -16 -2 2 55.7814 8.48893 5 -16 -2 2 31.5833 8.29849 1 -2 -16 -4 20.9958 11.6852 2 -2 -16 -4 12.8302 14.464 1 -2 16 4 4.25428 9.07926 3 -16 4 2 14.3634 8.57824 3 16 4 -2 -5.2912 15.9266 9 16 4 -2 -12.089 11.4371 4 -2 16 4 29.9956 13.7048 7 -16 -4 2 2.27602 7.71395 5 2 16 4 5.65292 12.3899 7 16 -4 -2 9.56968 21.1649 9 2 -16 -4 13.8739 12.5068 2 -16 -4 2 17.923 8.10989 1 -3 -16 -1 15.8535 25.3606 1 -3 16 1 25.7225 9.51505 3 3 16 -1 4.26327 14.4546 4 3 -16 1 -9.653 30.6094 6 -16 1 3 34.0163 8.01359 3 -3 -16 -1 42.7937 12.1177 6 16 1 -3 0.29212 16.0968 9 -16 -1 3 20.5542 7.33458 1 3 16 1 3.65645 15.3996 4 16 -1 -3 21.1897 16.8634 9 -3 -16 1 18.6404 17.6633 6 -3 16 -1 42.2539 9.6749 3 -16 -1 3 22.7798 7.13397 5 3 -16 -1 20.312 20.4267 6 -3 16 3 26.1282 9.28813 3 3 16 -3 6.3184 14.0983 4 16 3 -3 31.3012 15.983 9 -3 -16 -3 37.7536 15.3671 1 16 3 -3 -7.6315 12.0765 4 -3 -16 -3 20.2317 12.4457 2 -16 3 3 38.7744 8.90968 3 -16 -3 3 21.8276 7.98159 1 16 -3 -3 26.8337 19.0064 9 -16 -3 3 16.266 7.08961 5 3 -16 -3 7.93586 13.7092 6 3 16 3 26.8951 12.4116 7 -4 -16 0 126.525 23.4693 2 -4 -16 0 165.8 20.6299 6 -4 16 0 150.267 15.9027 3 4 -16 0 162.615 36.7892 6 16 0 -4 160.802 23.2567 9 -4 -16 0 135.151 32.1564 1 -16 2 4 7.24757 8.41344 3 -4 16 2 11.3557 9.68222 3 4 16 -2 4.9232 13.3127 4 -4 -16 -2 -1.5305 13.5397 1 16 2 -4 4.16689 16.8809 9 4 -16 -2 5.94788 18.6632 6 -16 -2 4 28.3855 6.72394 5 16 -2 -4 13.2726 16.6248 9 -16 -2 4 4.57008 6.88499 1 16 4 -4 123.737 20.9613 9 -4 -16 -4 93.351 13.2916 1 -4 16 4 114.23 13.1842 3 -4 -16 -4 88.5295 14.8044 2 -16 4 4 80.5276 12.108 3 4 -16 -4 111.308 17.3547 6 -16 -4 4 83.6559 11.1844 1 4 16 4 108.772 16.4354 7 16 -4 -4 115.443 23.1907 9 4 -16 -4 72.9102 15.4559 2 -5 16 1 12.7799 10.5317 3 -5 -16 -1 38.066 17.0425 1 -5 -16 -1 20.1469 15.9671 2 -16 1 5 15.9925 8.34378 3 5 16 -1 -1.396 17.2419 4 16 1 -5 -12.251 17.6979 9 5 16 1 -4.1746 17.81 4 -5 16 -1 8.57225 10.6759 3 16 -1 -5 -13.99 17.9282 9 -5 -16 1 5.59724 27.6459 1 5 -16 -1 12.6749 25.6015 6 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Co1 N1 110.6(3) 46 3_655 ? N1 Co1 N1 107.2(6) 3_655 . ? N1 Co1 N1 110.6(3) 46 . ? N1 Co1 N1 107.2(6) 46 48_554 ? N1 Co1 N1 110.6(3) 48_554 . ? N1 Co1 N1 110.6(3) 3_655 48_554 ? C2 N1 Co1 128.3(7) . . ? C2 N1 C1 104.7(10) . . ? C1 N1 Co1 126.3(9) . . ? N1 C2 N1 112.9(12) 14_665 . ? N1 C2 C3 123.5(6) . . ? N1 C2 C3 123.5(6) 14_665 . ? N1 C1 H1 125.6 . . ? C1 C1 N1 108.8(7) 14_665 . ? C1 C1 H1 125.6 14_665 . ? C2 C3 H3A 109.5 . . ? C2 C3 H3B 109.5 . . ? C2 C3 H3C 109.5 . . ? H3A C3 H3B 109.5 . . ? H3A C3 H3C 109.5 . . ? H3B C3 H3C 109.5 . . ? N3 N2 N3 180.0 3_655 . ? N4 N5 N4 177(10) 2_665 . ? N2 N3 N3 0.000(3) . 3_655 ? N5 N4 N4 2(10) . 2_665 ? N11 N10 N11 115(10) . 12_654 ? N11 N10 N11 115(10) . 6_665 ? N11 N10 N11 115(10) 6_665 12_654 ? N10 N11 N11 32(10) . 6_665 ? N10 N11 N11 32(10) . 12_654 ? N11 N11 N11 60.00(8) 6_665 12_654 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Co1 N1 1.992(10) 46 ? Co1 N1 1.992(10) . ? Co1 N1 1.992(10) 3_655 ? Co1 N1 1.992(10) 48_554 ? N1 C2 1.342(10) . ? N1 C1 1.379(11) . ? C2 C3 1.50(2) . ? C1 C1 1.35(3) 14_665 ? C1 H1 1.0770 . ? C3 H3A 1.0830 . ? C3 H3B 1.0830 . ? C3 H3C 1.0830 . ? N2 N3 0.66(4) 3_655 ? N2 N3 0.66(4) . ? N5 N4 0.67(14) . ? N5 N4 0.67(14) 2_665 ? N8 N9 0.76(5) . ? N3 N3 1.32(9) 3_655 ? N4 N4 1.3(3) 2_665 ? N10 N11 0.6(2) 12_654 ? N10 N11 0.6(2) . ? N10 N11 0.6(2) 6_665 ? N11 N11 0.9(4) 6_665 ? N11 N11 0.9(4) 12_654 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Co1 N1 C2 N1 173.2(5) . . . 14_665 ? Co1 N1 C2 C3 -5(2) . . . . ? Co1 N1 C1 C1 -172.3(6) . . . 14_665 ? C2 N1 C1 C1 -1.6(11) . . . 14_665 ? C1 N1 C2 N1 2.7(19) . . . 14_665 ? C1 N1 C2 C3 -175.1(15) . . . . ? N11 N10 N11 N11 -138(100) 12_654 . . 6_665 ? N11 N10 N11 N11 138(100) 6_665 . . 12_654 ?