#------------------------------------------------------------------------------ #$Date: 2023-11-23 01:39:40 +0200 (Thu, 23 Nov 2023) $ #$Revision: 287746 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/77/7247766.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7247766 loop_ _publ_author_name 'Jones, Isabelle M.' 'Turner, Gemma F.' 'Pitts, Kari' 'Powell, Rees' 'Riboldi-Tunnicliffe, Alan' 'Williamson, Rachel' 'Boer, Stephanie' 'Allen, Lauren' 'Moggach, Stephen A.' _publ_section_title ; High-pressure induced guest-mediated gate opening behaviour of the Co-based framework ZIF-67 ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D3CE00979C _journal_year 2023 _chemical_formula_moiety 'C8 H10 Co N4, 18(N0.5)' _chemical_formula_sum 'C8 H10 Co N13' _chemical_formula_weight 347.22 _chemical_name_common ZIF-67 _space_group_crystal_system cubic _space_group_IT_number 217 _space_group_name_Hall 'I -4 2 3' _space_group_name_H-M_alt 'I -4 3 m' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2023-10-03 _audit_creation_method ; Olex2 1.5 (compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817) ; _audit_update_record ; 2023-10-04 deposited with the CCDC. 2023-11-21 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 12 _cell_length_a 16.9247(6) _cell_length_b 16.9247(6) _cell_length_c 16.9247(6) _cell_measurement_reflns_used 1908 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 20.7650 _cell_measurement_theta_min 3.3910 _cell_volume 4848.0(3) _computing_cell_refinement 'CrysAlisPro 1.171.42.58a (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.42.58a (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.58a (Rigaku OD, 2022)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _diffrn_ambient_temperature 293(2) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.989 _diffrn_measured_fraction_theta_max 0.989 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -37.00 29.00 0.50 75.00 -- -24.44 -52.00 38.00 132 2 \w -27.00 -3.00 0.50 75.00 -- 24.20 19.00-150.00 48 3 \w -23.00 16.00 0.50 75.00 -- 24.20 67.00 -23.00 78 4 \w -36.00 -16.00 0.50 75.00 -- -24.44 38.00 150.00 40 5 \w -4.00 18.00 0.50 75.00 -- -24.44 -57.00 30.00 44 6 \w -36.00 -16.00 0.50 75.00 -- -24.44 38.00 -30.00 40 7 \w -36.00 -16.00 0.50 75.00 -- 24.20 38.00 30.00 40 8 \w 30.00 55.00 0.50 75.00 -- 24.20 -99.00 30.00 50 9 \w 30.00 71.00 0.50 75.00 -- 24.20 -99.00-150.00 82 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Single source at home/near, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0150047000 _diffrn_orient_matrix_UB_12 0.0070899000 _diffrn_orient_matrix_UB_13 -0.0384553000 _diffrn_orient_matrix_UB_21 0.0041370000 _diffrn_orient_matrix_UB_22 0.0412825000 _diffrn_orient_matrix_UB_23 0.0059706000 _diffrn_orient_matrix_UB_31 0.0389285000 _diffrn_orient_matrix_UB_32 -0.0016528000 _diffrn_orient_matrix_UB_33 -0.0154844000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0942 _diffrn_reflns_av_unetI/netI 0.0517 _diffrn_reflns_Laue_measured_fraction_full 0.989 _diffrn_reflns_Laue_measured_fraction_max 0.989 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 10 _diffrn_reflns_limit_l_min -11 _diffrn_reflns_number 5113 _diffrn_reflns_point_group_measured_fraction_full 0.990 _diffrn_reflns_point_group_measured_fraction_max 0.990 _diffrn_reflns_theta_full 20.799 _diffrn_reflns_theta_max 20.799 _diffrn_reflns_theta_min 3.405 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Mo) X-ray Source' _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 1.080 _exptl_absorpt_correction_T_max 0.7445 _exptl_absorpt_correction_T_min 0.5158 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1139 before and 0.0835 after correction. The Ratio of minimum to maximum transmission is 0.6928. The \l/2 correction factor is Not present. ; _exptl_crystal_colour 'clear bluish violet' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier bluish _exptl_crystal_colour_primary violet _exptl_crystal_density_diffrn 1.427 _exptl_crystal_description block _exptl_crystal_F_000 2112 _exptl_crystal_recrystallization_method 'Re-crystallisation from solvent' _exptl_crystal_size_max 0.14 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.09 _refine_diff_density_max 0.730 _refine_diff_density_min -0.831 _refine_diff_density_rms 0.143 _refine_ls_abs_structure_details ; Flack x determined using 172 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.08(3) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.113 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 45 _refine_ls_number_reflns 501 _refine_ls_number_restraints 10 _refine_ls_restrained_S_all 1.149 _refine_ls_R_factor_all 0.0867 _refine_ls_R_factor_gt 0.0816 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1666P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2091 _refine_ls_wR_factor_ref 0.2136 _reflns_Friedel_coverage 0.777 _reflns_Friedel_fraction_full 0.991 _reflns_Friedel_fraction_max 0.991 _reflns_number_gt 458 _reflns_number_total 501 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL zif67_ln2_1600_a.res in I-43m zif67_ln2_1600.res created by SHELXL-2018/3 at 14:43:25 on 03-Oct-2023 REM Old TITL ZIF67_LN2_1600 in I-43m REM SHELXT solution in I-43m: R1 0.110, Rweak 0.047, Alpha 0.132 REM 0.000 for 0 systematic absences, Orientation as input REM Flack x = 0.028 ( 0.036 ) from 174 Parsons' quotients REM Formula found by SHELXT: C9 N11 Co CELL 0.71073 16.924681 16.924681 16.924681 90 90 90 ZERR 12 0.000606 0.000606 0.000606 0 0 0 LATT -2 SYMM -X,-Y,+Z SYMM -X,+Y,-Z SYMM +X,-Y,-Z SYMM +Z,+X,+Y SYMM +Z,-X,-Y SYMM -Z,-X,+Y SYMM -Z,+X,-Y SYMM +Y,+Z,+X SYMM -Y,+Z,-X SYMM +Y,-Z,-X SYMM -Y,-Z,+X SYMM +Y,+X,+Z SYMM -Y,-X,+Z SYMM +Y,-X,-Z SYMM -Y,+X,-Z SYMM +X,+Z,+Y SYMM -X,+Z,-Y SYMM -X,-Z,+Y SYMM +X,-Z,-Y SYMM +Z,+Y,+X SYMM +Z,-Y,-X SYMM -Z,+Y,-X SYMM -Z,-Y,+X SFAC C H Co N UNIT 96 120 12 156 EQIV $1 1-Y,1-X,+Z DFIX 1.55 C2 C3 DFIX 1.337 0.01 N1 C2 DFIX 1.387 0.01 N1 C1 DFIX 2.175 0.01 C1 C2 EADP N1 C1 C2 EADP N11 N10 RIGU C2 C3 FLAT C1 N1 C2 C3 EADP N6 N7 EADP N4 N5 DFIX 1.08 N4 N5 DFIX 1.09 N9 N8 L.S. 10 0 0 PLAN 5 SIZE 0.09 0.1 0.14 CONF BIND C2 C3 FREE C2 C1_$1 FREE C2 C1 BOND list 4 MORE -1 BOND $H fmap 2 53 acta REM REM REM WGHT 0.166600 FVAR 0.13953 CO1 3 0.500000 0.250000 0.000000 10.25000 0.03531 0.03539 = 0.03531 0.00000 0.00000 0.00000 N1 4 0.586948 0.319833 0.036097 11.00000 0.03428 0.04046 = 0.03854 0.00344 -0.00373 -0.00549 C2 1 0.632601 0.367399 -0.006976 10.50000 0.03428 0.04046 = 0.03854 0.00344 -0.00373 -0.00549 C1 1 0.604529 0.338004 0.113937 11.00000 0.03428 0.04046 = 0.03854 0.00344 -0.00373 -0.00549 AFIX 43 1.0770 H1 2 0.577882 0.311749 0.165415 11.00000 -1.20000 AFIX 0 C3 1 0.627473 0.372527 -0.095328 10.50000 0.04227 0.04227 = 0.04592 0.01022 -0.01022 -0.01341 PART -1 AFIX 33 1.0830 H3A 2 0.670278 0.414994 -0.116748 10.50000 -1.50000 H3B 2 0.639801 0.315125 -0.120776 10.50000 -1.50000 H3C 2 0.568639 0.391163 -0.112232 10.50000 -1.50000 AFIX 0 PART 0 N2 4 0.500000 0.500000 0.000000 10.08333 0.06063 N5 4 0.500000 0.500000 -0.231580 10.25000 0.11671 N8 4 0.779355 0.220645 0.070901 10.50000 0.13091 N3 4 0.500000 0.500000 -0.035952 10.16667 0.07799 N9 4 0.764807 0.235193 0.016607 10.50000 0.13036 N6 4 0.768378 0.231622 -0.231622 10.04167 0.07445 N4 4 0.543927 0.456073 -0.228872 10.25000 0.11671 N7 4 0.748888 0.251112 -0.251112 10.12500 0.07445 N10 4 0.576333 0.423667 -0.423667 10.08333 0.07458 N11 4 0.602581 0.444556 -0.444556 10.08333 0.07458 N12 4 0.875811 0.124189 -0.124189 10.16667 0.13893 HKLF 4 REM zif67_ln2_1600_a.res in I-43m REM wR2 = 0.2136, GooF = S = 1.113, Restrained GooF = 1.149 for all data REM R1 = 0.0816 for 458 Fo > 4sig(Fo) and 0.0867 for all 501 data REM 45 parameters refined using 10 restraints END WGHT 0.1668 0.0000 REM Highest difference peak 0.730, deepest hole -0.831, 1-sigma level 0.143 Q1 1 0.7603 0.2397 -0.2068 10.50000 0.05 0.73 Q2 1 0.8678 0.1322 -0.1530 10.50000 0.05 0.73 Q3 1 0.7474 0.2526 -0.2166 10.50000 0.05 0.69 Q4 1 0.7384 0.2616 -0.2972 10.50000 0.05 0.64 Q5 1 0.5156 0.5156 -0.2434 10.50000 0.05 0.53 REM The information below was added by Olex2. REM REM R1 = 0.0816 for 458 Fo > 4sig(Fo) and 0.0867 for all 5113 data REM 45 parameters refined using n/a restraints REM Highest difference peak 0.73, deepest hole -0.83 REM Mean Shift 0, Max Shift -0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0867 REM R1_gt = 0.0816 REM wR_ref = 0.2136 REM GOOF = 1.113 REM Shift_max = -0.001 REM Shift_mean = 0 REM Reflections_all = 5113 REM Reflections_gt = 458 REM Parameters = 45 REM Hole = -0.83 REM Peak = 0.73 REM Flack = 0.08(3) ; _cod_data_source_file d3ce00979c2.cif _cod_data_source_block zif67_ln2_1600 _cod_original_cell_volume 4848.0(5) _cod_database_code 7247766 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'Co C8 H10 N4' _chemical_oxdiff_usercomment 'ZIF67 @ 1.59 GPa in LN2' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.909 _shelx_estimated_absorpt_t_min 0.864 _diffrn_orient_matrix_axis[1] matrixX _diffrn_orient_matrix_axis[2] matrixY _diffrn_orient_matrix_axis[3] matrixZ _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances C2-C3 1.55 with sigma of 0.02 N1-C2 1.337 with sigma of 0.01 N1-C1 1.387 with sigma of 0.01 C1-C2 2.175 with sigma of 0.01 N4-N5 1.08 with sigma of 0.02 N9-N8 1.09 with sigma of 0.02 3. Restrained planarity C1, N1, C2, C3 with sigma of 0.1 4. Uiso/Uaniso restraints and constraints Uanis(N1) = Uanis(C1) = Uanis(C2) Uiso(N11) = Uiso(N10) Uiso(N6) = Uiso(N7) Uiso(N4) = Uiso(N5) 5. Rigid body (RIGU) restrains C2, C3 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 6. Others Fixed Sof: H3A(0.5) H3B(0.5) H3C(0.5) N2(0.083333) N3(0.166667) N6(0.041667) N4(0.25) N7(0.125) N10(0.083333) N11(0.083333) 7.a Me refined with riding coordinates: C3(H3A,H3B,H3C) 7.b Aromatic/amide H refined with riding coordinates: C1(H1) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 7.228 _oxdiff_exptl_absorpt_empirical_full_min 0.666 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, z' '-y, -x, z' 'y, -x, -z' '-y, x, -z' 'x, z, y' '-x, z, -y' '-x, -z, y' 'x, -z, -y' 'z, y, x' 'z, -y, -x' '-z, y, -x' '-z, -y, x' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' 'z+1/2, x+1/2, y+1/2' 'z+1/2, -x+1/2, -y+1/2' '-z+1/2, -x+1/2, y+1/2' '-z+1/2, x+1/2, -y+1/2' 'y+1/2, z+1/2, x+1/2' '-y+1/2, z+1/2, -x+1/2' 'y+1/2, -z+1/2, -x+1/2' '-y+1/2, -z+1/2, x+1/2' 'y+1/2, x+1/2, z+1/2' '-y+1/2, -x+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' 'x+1/2, z+1/2, y+1/2' '-x+1/2, z+1/2, -y+1/2' '-x+1/2, -z+1/2, y+1/2' 'x+1/2, -z+1/2, -y+1/2' 'z+1/2, y+1/2, x+1/2' 'z+1/2, -y+1/2, -x+1/2' '-z+1/2, y+1/2, -x+1/2' '-z+1/2, -y+1/2, x+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co1 Co 0.500000 0.250000 0.000000 0.0353(16) Uani 1 4 d S T P . . N1 N 0.5869(6) 0.3198(6) 0.0361(5) 0.038(2) Uani 1 1 d D . . . . C2 C 0.6326(6) 0.3674(6) -0.0070(8) 0.038(2) Uani 1 2 d DS T P . . C1 C 0.6045(8) 0.3380(9) 0.1139(6) 0.038(2) Uani 1 1 d D . . . . H1 H 0.577882 0.311749 0.165415 0.045 Uiso 1 1 calc R U . . . C3 C 0.6275(9) 0.3725(9) -0.0953(12) 0.043(6) Uani 1 2 d DS T P . . H3A H 0.670278 0.414994 -0.116748 0.065 Uiso 0.5 1 calc R U P A -1 H3B H 0.639801 0.315125 -0.120776 0.065 Uiso 0.5 1 calc R U P A -1 H3C H 0.568639 0.391163 -0.112232 0.065 Uiso 0.5 1 calc R U P A -1 N2 N 0.500000 0.500000 0.000000 0.061(19) Uiso 0.6666 8 d S . P . . N5 N 0.500000 0.500000 -0.232(2) 0.117(11) Uiso 1 4 d DS . P . . N8 N 0.7794(13) 0.2206(13) 0.0709(19) 0.131(11) Uiso 1 2 d DS . P . . N3 N 0.500000 0.500000 -0.036(3) 0.078(11) Uiso 0.6667 4 d S . P . . N9 N 0.7648(14) 0.2352(14) 0.017(2) 0.130(12) Uiso 1 2 d DS . P . . N6 N 0.768(6) 0.232(6) -0.232(6) 0.074(14) Uiso 0.25 6 d S . P . . N4 N 0.5439(11) 0.4561(11) -0.229(4) 0.117(11) Uiso 0.5 2 d DS . P . . N7 N 0.749(3) 0.251(3) -0.251(3) 0.074(14) Uiso 0.75 6 d S . P . . N10 N 0.576(4) 0.424(4) -0.424(4) 0.07(3) Uiso 0.5 6 d S . P . . N11 N 0.603(9) 0.445(7) -0.445(7) 0.07(3) Uiso 0.1667 2 d S . P . . N12 N 0.8758(19) 0.1242(19) -0.1242(19) 0.14(2) Uiso 1 6 d S . P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Co1 0.0353(18) 0.035(2) 0.0353(18) 0.000 0.000 0.000 N1 0.034(5) 0.040(6) 0.039(4) 0.003(4) -0.004(4) -0.005(4) C2 0.034(5) 0.040(6) 0.039(4) 0.003(4) -0.004(4) -0.005(4) C1 0.034(5) 0.040(6) 0.039(4) 0.003(4) -0.004(4) -0.005(4) C3 0.042(8) 0.042(8) 0.046(9) 0.010(7) -0.010(7) -0.013(12) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _axis.id _axis.type _axis.equipment _axis.parity _axis.depends_on _axis.zero _axis.vector[1] _axis.vector[2] _axis.vector[3] source . source . . . 1.00000000 0.00000000 0.00003403 omega rotation goniometer -1 . 0.12240000 0.00000000 0.00000000 1.00000000 kappa rotation goniometer -1 omega 0.28425000 -0.76560404 0.00000000 0.64331210 phi rotation goniometer -1 kappa . -0.00006266 0.00000000 1.00000000 theta rotation goniometer -1 . 0.19892000 0.00000000 0.00000000 1.00000000 matrixX general general . phi . 1.00000000 0.00000000 0.00000000 matrixY general general . phi . 0.00000000 1.00000000 0.00000000 matrixZ general general . phi . 0.00000000 0.00000000 1.00000000 dacX translation general . phi . 0.00000000 1.00000000 0.00000000 dacY translation general . phi . -1.00000000 0.00000000 0.00000000 dacZ translation general . phi . 0.00000000 0.00000000 1.00000000 loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u _diffrn_refln_scale_group_code -2 0 2 165.037 11.337 1 2 0 -2 154.102 10.7465 1 -2 0 2 151.161 11.1548 3 -2 -2 0 161.631 11.7037 5 -2 -2 0 160.157 10.7448 2 2 -2 -2 2448.24 177.507 9 2 -2 -2 2245.87 151.223 2 -2 -2 2 2162.08 156.618 1 -2 2 2 2526.39 160.382 3 -2 2 2 2328.54 160.294 7 -3 -1 0 406.096 29.0003 1 0 -3 -1 433.903 28.8683 1 -1 3 0 458.11 31.7441 4 0 3 1 428.989 28.2914 3 0 3 -1 433.963 31.5982 4 3 0 -1 367.22 28.1949 7 -3 0 1 442.425 29.26 5 0 3 1 407.858 31.9267 9 1 3 0 410.746 27.5186 8 1 3 0 383.279 28.2555 3 3 0 -1 488.437 29.0217 6 -3 0 1 380.442 28.9178 1 -3 0 1 406.841 28.2634 3 0 -3 -1 453.283 29.1235 5 0 -3 1 393.922 29.7784 6 1 3 2 71.8106 5.54994 7 -3 -2 1 59.3219 5.42964 5 -2 -3 -1 79.466 5.25566 2 2 3 -1 75.6072 5.22003 8 -3 1 2 81.3153 5.29293 1 -3 -2 1 65.3861 5.4435 1 3 -2 -1 72.2771 6.40828 9 1 -3 -2 70.4526 4.82975 2 3 -2 -1 71.354 5.33639 6 1 -3 -2 64.1636 6.29593 9 1 -3 -2 68.0692 4.94617 1 3 -2 -1 68.7767 4.99715 8 -3 1 2 82.1639 5.56858 3 3 2 1 54.8113 5.11178 7 3 1 -2 79.24 6.47134 9 -1 2 3 53.1454 5.89491 3 3 1 -2 78.9267 7.4516 4 1 3 -2 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247.911 18.1652 7 1 -6 -5 265.433 17.5028 1 -6 -5 -1 256.477 16.7217 2 -1 6 5 260.797 18.3672 3 -5 -6 1 243.947 18.6564 1 6 5 -1 246.537 18.8587 9 5 -6 -1 275.994 21.9666 9 -6 -5 -1 257.215 18.0441 1 -6 -5 -1 234.071 18.3686 5 -6 -1 5 240.746 19.5747 1 -6 3 5 120.256 10.5447 3 -5 6 3 103.588 7.4953 1 -5 6 3 101.281 10.0002 7 -5 -6 -3 109.837 9.97026 1 3 -6 -5 104.749 7.52758 1 3 -6 -5 93.9151 7.50944 5 5 6 -3 109.166 8.9654 8 -5 -6 -3 117.395 9.08344 2 6 -5 -3 117.312 8.55257 8 -6 -5 3 111.065 9.58707 1 3 -6 -5 115.012 8.08209 2 5 -3 -6 90.4891 7.54132 1 6 -5 -3 118.576 11.73 9 -6 -3 5 105.156 11.347 1 3 -5 -6 98.18 7.48579 1 6 5 -3 104.488 8.93776 8 6 5 -3 110.976 10.0405 9 -5 3 6 122.948 11.0562 3 -6 5 3 109.12 9.53783 3 5 -6 -3 110.635 11.9914 9 6 5 -3 109.043 12.0347 4 6 -3 -5 107.997 11.4288 9 5 -6 -3 109.395 7.92373 8 -6 5 3 105.002 9.79798 7 5 6 3 108.239 9.23673 7 -5 -6 3 92.6828 10.097 1 -3 6 5 116.436 10.5883 7 5 -6 -5 31.1699 3.466 2 -6 5 5 25.5708 6.47414 3 6 -5 -5 24.6017 2.90851 2 -5 5 6 21.0645 6.65422 3 -5 6 5 14.8761 5.4565 7 6 -5 -5 31.3757 4.13619 8 6 -5 -5 27.3068 7.61147 9 5 -6 -5 31.5459 7.33834 9 6 5 -5 22.0428 5.9466 8 -5 6 5 16.3118 6.62192 3 -6 -5 5 31.6256 9.15895 1 -5 -6 5 18.2831 12.3129 1 -6 -6 0 138.241 10.4852 2 6 -6 0 138.173 19.2996 6 -6 -6 0 133.723 11.7069 1 2 -6 -6 1085.28 73.1414 1 -6 -6 2 980.599 74.3332 6 6 6 -2 1088.24 71.5731 8 6 6 2 1028.23 75.0258 7 6 -6 -2 1180.22 83.6924 9 -2 6 6 1117.36 77.9582 3 6 -6 -2 1072.57 74.5641 6 -6 6 2 1103.82 72.6199 3 -6 -6 2 1033.13 75.3058 1 -6 -6 -2 1055.55 70.9222 2 6 6 -2 1045.41 82.8829 9 -6 2 6 1217.92 75.9614 3 -6 6 4 42.5057 6.33935 7 6 -4 -6 46.8023 8.72418 9 6 6 -4 42.9843 6.21372 8 -6 6 4 39.4147 6.85374 3 -6 -4 6 19.8309 13.4331 1 6 6 -4 45.8952 10.7431 4 6 -6 -4 46.8105 4.80073 8 -6 4 6 42.5252 7.40022 3 6 -6 -4 42.1353 8.56265 9 -6 -6 4 37.8088 7.69961 1 -6 6 6 624.02 47.0241 3 6 -6 -6 714.989 47.8791 9 0 7 -1 327.56 24.4112 4 1 -7 0 314.958 22.5967 6 0 -7 1 296.828 22.9521 6 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10.5032 7 -1 -7 -2 160.118 10.8809 1 -1 7 2 145.37 10.9676 3 -7 -1 2 135.229 10.8596 1 -2 -7 1 122.958 10.8397 6 0 7 3 26.1418 5.23393 7 7 0 -3 36.7044 5.12617 8 -7 0 3 19.6407 3.76875 3 -7 -3 0 14.928 4.40595 1 3 -7 0 14.2741 5.9782 9 -3 -7 0 13.4398 3.64681 5 -3 -7 0 16.0988 3.83429 1 0 -7 -3 18.4621 2.98078 5 -7 0 3 16.3344 3.15639 1 -7 0 3 15.3224 3.05719 5 0 -7 -3 16.0463 3.48038 2 0 -7 -3 19.8523 3.21285 1 3 -7 0 19.2966 6.07072 6 -3 7 0 27.7268 7.36517 4 7 0 -3 24.7079 6.56571 9 0 7 3 31.2908 5.11444 3 7 2 -3 109.878 10.1284 8 -7 2 3 114.89 9.34556 1 7 -3 -2 134.019 12.7583 6 2 -7 -3 141.335 11.2317 1 -7 -3 2 124.672 10.5975 1 3 7 -2 115.111 9.29865 8 -7 2 3 130.753 10.0669 3 -3 7 2 131.045 10.2953 3 3 7 -2 108.564 12.6805 4 -3 -7 -2 131.174 9.76436 2 7 2 -3 125.319 12.0058 9 -3 -7 -2 129.963 10.2041 5 -7 -3 2 137.178 9.2964 2 7 -3 -2 130.478 13.1244 9 7 2 -3 133.148 12.9445 4 2 -7 -3 135.297 12.7036 9 -3 -7 -2 126.331 10.3513 1 -7 -3 2 119.866 9.16361 3 2 7 3 140.511 10.8894 7 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44.8372 4.31594 1 -3 7 4 44.0288 6.59577 3 -7 -3 4 50.3602 5.60125 1 4 -7 -3 44.9236 4.01024 8 -7 4 3 54.3939 6.22151 3 7 4 -3 42.2178 8.53581 4 -3 -7 -4 50.334 6.28298 1 7 4 -3 49.5045 7.14431 9 -7 4 3 58.112 5.9179 7 0 -7 -5 186.12 13.0546 2 7 0 -5 186.014 13.5333 8 -7 -5 0 182.667 13.2546 2 -7 0 5 170.685 14.1473 3 -7 -5 0 175.228 14.6951 5 0 -7 -5 186.1 13.5195 1 -7 -5 0 181.415 14.8259 1 5 -7 0 167.628 18.5714 9 0 7 5 214.266 15.3599 7 -7 0 5 189.244 13.7681 1 7 0 -5 189.438 16.4449 9 -5 -7 0 167.43 13.6708 2 5 7 0 164.346 14.414 9 2 -7 -5 35.9343 3.34374 1 2 -7 -5 34.01 4.051 2 -7 2 5 37.2339 4.15383 1 -7 2 5 38.8789 6.68971 3 7 2 -5 31.3543 6.59564 9 -7 -5 2 29.8131 5.2161 1 -5 -7 -2 30.9932 4.75368 2 -5 7 2 37.9884 5.62416 4 -7 -5 2 31.4108 4.48094 2 -7 -5 2 30.7603 5.29506 5 7 -5 -2 38.9757 7.8099 6 2 -7 -5 33.5464 3.33399 5 -5 -7 -2 31.7234 5.65358 5 2 7 5 21.808 6.23449 7 5 7 -2 35.7506 5.22707 8 -5 -7 -2 35.351 5.73908 1 7 -5 -2 41.7209 9.24049 9 -2 7 5 32.1057 6.49296 7 -7 5 2 29.9793 5.67225 3 5 7 2 26.9756 4.63022 7 5 -7 -2 35.2077 7.982 9 -7 -5 -2 31.1642 5.8889 1 -5 -7 2 29.6788 5.50294 1 -5 -7 2 27.9903 4.56217 6 7 5 -2 32.7874 5.88467 8 -7 -2 5 35.1864 5.21959 1 7 5 -2 33.9547 5.73338 9 -2 -7 -5 25.7448 4.53644 2 -2 -7 -5 23.0627 4.80577 1 -2 7 5 39.5399 6.48714 3 7 -2 -5 31.3658 5.21245 8 7 -5 -4 94.9289 7.26822 2 -4 5 7 95.9288 11.3779 3 5 7 -4 106.812 9.40709 8 4 -7 -5 99.8067 7.84538 2 4 -7 -5 101.772 12.3404 9 7 4 -5 102.79 9.55868 8 -7 -5 4 107.103 10.2157 1 7 -5 -4 119.881 12.699 9 -5 7 4 117.269 10.4303 7 -7 4 5 102.224 10.337 3 7 -5 -4 106.701 8.72846 8 -7 5 4 113.15 9.79545 7 7 5 -4 95.1781 10.2251 9 -5 4 7 107.377 11.0632 3 -7 -4 5 116.838 10.9534 1 7 -4 -5 105.427 12.0062 9 7 -4 -5 97.3306 8.81537 8 -4 7 5 106.713 10.5326 7 5 -7 -4 107.456 7.9135 8 7 5 -4 102.027 9.64222 8 7 5 -4 98.046 13.5316 4 -5 -7 4 92.619 14.2103 1 5 -7 -4 109.836 12.1787 9 -7 5 4 99.8463 9.8728 3 -7 1 6 143.766 12.5092 3 1 -7 -6 146.917 10.7392 1 -6 -7 -1 141.439 11.058 2 6 7 -1 132.402 11.7455 9 7 1 -6 143.896 14.0922 9 -7 -6 1 138.628 12.3173 1 7 -6 -1 145.983 16.8907 9 -7 -6 1 136.14 12.2034 5 7 6 1 139.614 10.8838 7 -7 -6 1 150.215 10.9485 2 7 -6 -1 151.408 17.6061 6 -7 -1 6 92.7896 14.3453 1 -6 -7 1 147.926 11.4978 2 -6 -7 1 150.573 12.1756 1 -7 -6 -1 136.886 12.3539 1 -7 -6 -1 138.113 12.4659 5 6 -7 -1 137.838 15.74 9 6 -7 -1 162.997 14.8977 6 7 -1 -6 144.283 14.4124 9 7 6 -1 133.54 12.7046 9 -7 -6 -1 151.741 10.9975 2 3 -7 -6 85.6401 6.28148 5 -6 -7 -3 81.4448 7.6693 2 7 -6 -3 86.8433 8.99672 6 -6 7 3 79.5873 8.79735 7 -6 7 3 96.5172 8.24605 4 3 -7 -6 100.774 7.17103 2 -7 -6 3 67.3819 8.65547 1 6 7 -3 85.9915 8.5096 8 7 -6 -3 104.061 11.8357 9 6 7 -3 72.6027 11.4643 4 3 -7 -6 87.339 6.22749 1 -6 -7 -3 77.0811 9.07144 1 -7 3 6 90.6517 9.4607 3 7 6 -3 81.4427 11.7047 4 -6 -7 3 86.2149 9.16458 1 7 6 -3 79.7996 8.36236 8 6 7 3 80.8498 7.97845 7 6 -7 -3 86.925 11.5467 9 -6 3 7 71.5528 10.0512 3 7 6 -3 75.8782 8.49131 9 -3 7 6 82.0977 10.044 3 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237.927 17.0973 1 -7 -7 2 222.774 16.1584 2 7 -7 -2 230.407 19.1956 6 7 -7 -2 231.844 20.6604 9 7 7 -4 36.0972 7.08218 8 -7 -7 4 44.1796 7.89636 1 7 7 -4 35.3666 11.0722 4 -7 4 7 33.9248 9.04348 3 7 -7 -4 53.8579 10.554 9 -7 7 4 24.3525 7.63848 3 -7 7 4 32.4508 6.62529 7 7 -4 -7 49.806 10.0728 9 7 -7 -4 47.9484 5.7261 8 -6 7 7 45.077 9.66883 3 -7 6 7 52.3618 9.47911 3 -7 7 6 34.955 9.41071 3 -7 -7 6 33.2181 16.272 1 7 -7 -6 45.3254 5.60434 8 7 -6 -7 46.5076 10.7919 9 7 7 -6 36.6033 9.16246 8 7 -7 -6 42.4695 10.2538 9 7 -7 -6 25.8953 4.30023 2 0 -8 0 1814.78 154.998 9 0 -8 0 2489.22 145.435 1 8 -1 -1 98.9747 11.3867 9 -1 -8 -1 108.423 8.55146 1 1 8 1 73.8513 7.06223 3 -1 -8 1 99.1285 13.4716 1 -1 8 -1 96.4565 10.3725 4 -8 -1 1 97.1322 8.21648 1 1 8 -1 92.7342 10.65 4 1 8 -1 86.1539 6.90896 8 1 -8 -1 77.1407 8.59343 9 1 -8 1 76.6975 9.99465 9 8 1 -1 102.069 11.0488 9 -8 1 1 103.049 8.57538 1 -1 8 1 98.4635 7.77753 3 -1 -8 1 83.1928 8.18588 6 1 -8 1 113.871 10.676 6 2 8 0 56.6632 5.27488 3 2 -8 0 53.3728 7.35737 6 -8 0 2 65.0194 6.15475 5 0 8 2 65.4682 6.40066 3 8 0 -2 67.1812 7.21425 4 8 0 -2 67.1772 9.15027 9 -8 0 2 63.0239 6.46828 1 -8 0 2 57.2009 5.91886 3 0 -8 -2 62.3421 6.12912 1 0 -8 2 49.0054 11.3262 6 0 8 -2 63.6116 10.1586 4 -8 -2 0 58.8857 6.93475 1 -2 8 0 71.4923 8.58129 4 -2 -8 0 68.6821 7.20288 1 2 -8 0 53.2961 8.00097 9 -8 -2 2 114.703 9.2969 5 2 8 -2 113.309 8.44491 8 -8 2 2 112.351 9.26216 3 -8 2 2 120.687 9.23518 1 -2 8 2 119.131 9.33833 3 -2 -8 -2 107.951 9.23097 1 8 2 -2 103.775 9.95753 8 2 8 -2 120.994 12.6572 4 -8 -2 2 113.359 9.3573 1 2 -8 -2 107.869 10.8837 9 -2 -8 -2 104.072 9.1824 5 -2 -8 2 103.701 14.7279 1 8 2 -2 119.368 12.184 9 -2 -8 2 106.524 10.7845 6 -8 -2 2 98.2988 8.24685 3 2 8 2 108.123 8.78938 3 1 -8 -3 156.769 10.4867 2 3 8 -1 112.339 9.45599 3 1 8 3 133.465 12.0318 7 3 8 -1 132.43 10.162 8 8 1 -3 129.857 14.0716 4 -3 8 1 145.475 12.6855 4 -3 -8 -1 130.372 11.1428 1 -3 -8 -1 134.577 11.0195 5 -8 1 3 132.834 11.0123 3 1 8 3 128.421 11.1264 3 3 -8 1 119.39 15.2773 6 -8 -3 1 143.408 11.7404 1 -8 -3 1 145.056 11.7775 5 1 -8 -3 141.44 10.5694 1 8 1 -3 135.252 13.6313 9 -8 1 3 131.196 10.4368 5 -8 -3 1 135.685 9.81452 3 -8 1 3 132.655 10.4402 1 8 -3 -1 144.207 15.2291 9 -8 -1 3 138.572 11.1528 1 -1 -8 -3 137.645 10.6332 5 -8 -1 3 137.823 10.8043 3 -3 -8 1 131.002 11.9663 1 8 -1 -3 139.122 11.0898 8 1 8 -3 145.427 15.4079 4 8 3 -1 128.302 13.3825 9 -1 8 3 146.031 11.1549 3 8 -1 -3 136.983 13.4897 9 8 -1 -3 166.716 17.0259 6 3 8 1 120.25 9.99116 3 3 -8 -1 136.989 12.0269 6 -1 -8 -3 143.839 10.6112 1 -1 -8 -3 147.233 10.3168 2 3 -8 -1 110.501 13.2931 9 -8 -1 3 135.668 10.7264 5 -8 -3 -1 126.531 11.9389 1 8 -3 -3 24.7893 8.00075 9 8 3 -3 26.5508 6.73543 9 -3 -8 -3 24.31 5.11343 1 8 3 -3 31.7597 6.04674 8 3 8 3 24.1388 5.35201 7 -8 -3 3 33.3738 3.74001 2 3 8 -3 27.9342 4.67669 8 -3 -8 -3 23.1952 4.9202 5 -8 3 3 25.6529 3.58326 1 -8 -3 3 23.0296 4.7481 5 -8 3 3 28.4996 5.3589 3 8 -3 -3 30.5618 5.49443 8 -8 -3 3 23.4493 4.77589 1 3 -8 -3 32.0007 7.11736 9 3 8 -3 14.095 8.47102 4 8 -3 -3 33.4099 7.76305 6 -8 -3 3 26.4684 3.95435 3 -3 8 3 25.6627 5.78303 3 -8 3 3 27.7347 3.30054 5 8 3 -3 27.3625 7.65111 4 8 0 -4 672.903 41.1689 6 4 -8 0 500.578 48.791 9 -8 -4 0 577.121 42.792 5 0 -8 -4 559.277 40.3514 1 0 -8 -4 602.548 39.2194 2 4 -8 0 564.148 45.9089 6 8 0 -4 606.319 47.0174 9 8 0 -4 604.278 40.7274 8 -4 8 0 585.02 38.0966 8 0 8 4 603.988 42.8264 7 0 -8 -4 597.063 40.8425 5 0 8 4 616.356 41.7167 3 -8 -4 0 564.138 42.1506 1 -4 -8 0 584.319 42.0685 1 -4 -8 0 572.576 41.1582 5 -8 0 4 564.589 40.7 3 -8 0 4 577.138 41.4014 1 4 8 -2 113.442 9.28192 8 2 -8 -4 121.925 9.56458 1 -4 -8 -2 115.558 10.3746 1 -8 -4 2 112.639 10.4118 5 2 8 4 114.501 10.8866 7 2 -8 -4 119.389 8.99075 2 -8 2 4 115.201 10.592 3 -8 -4 2 103.034 8.65194 3 8 2 -4 112.654 12.4755 9 -4 8 2 122.224 10.1725 3 8 -4 -2 122.344 14.0192 9 8 2 -4 112.045 15.858 4 -8 2 4 119.931 9.02018 1 -4 8 2 132.376 11.1883 4 -4 -8 -2 115.998 9.52361 2 -4 -8 -2 113.284 10.1596 5 8 -4 -2 143.016 16.4956 6 4 8 -2 94.2525 12.9538 4 -8 -4 2 117.525 9.07266 2 -8 -4 2 118.659 10.5353 1 -2 -8 -4 119.64 9.45999 2 8 -2 -4 118.982 9.94131 8 -8 -2 4 110.109 9.68106 3 -8 -2 4 118.885 8.60095 2 8 4 -2 114.197 10.6971 8 -8 -2 4 124.337 9.93146 1 8 4 -2 112.018 11.7 9 -2 -8 -4 107.495 9.82106 5 -8 4 2 104.274 9.80914 7 -2 -8 -4 123.946 10.0562 1 4 -8 -2 119.68 12.7205 9 -4 -8 2 107.797 10.4732 6 -2 8 4 114.743 10.8701 7 8 -2 -4 123.545 9.89769 6 -2 8 4 122.336 10.9018 3 4 -8 -4 1527.34 112.546 9 -8 4 4 1332.75 98.0998 1 4 8 4 1540.56 100.627 7 4 -8 -4 1474.21 92.0212 2 -8 -4 4 1448.97 95.0542 2 8 -4 -4 1540.86 108.422 9 -4 -8 -4 1389.68 97.7537 1 4 8 -4 1347.42 106.525 4 4 8 -4 1466.45 91.6963 8 8 -4 -4 1438.58 94.7391 6 8 -4 -4 1431.99 95.6215 8 8 4 -4 1369.62 103.781 4 8 4 -4 1330.27 93.2668 8 -8 -4 4 1397.74 99.9909 1 4 -8 -4 1469.59 94.884 8 -4 8 4 1399.04 97.1236 3 8 4 -4 1368.93 108.043 9 -4 8 4 1504.01 98.1849 7 -8 4 4 1475.66 96.0782 3 -4 -8 4 1053.19 109.597 1 -8 -5 1 77.2988 6.49492 3 8 1 -5 95.5175 7.39224 6 -5 -8 -1 96.9293 8.56629 2 -8 -5 1 96.0939 7.70824 2 1 -8 -5 96.5856 7.58024 2 -8 1 5 87.6177 7.46051 1 1 -8 -5 93.8041 7.1848 5 8 -5 -1 99.7982 13.7802 9 1 8 5 100.723 9.93942 7 -5 -8 -1 76.3538 8.84844 5 -5 -8 -1 95.9597 9.16989 1 -8 -5 1 106.661 9.31206 5 8 1 -5 84.9427 10.9484 9 1 -8 -5 86.5142 7.25636 1 -8 -5 1 84.5536 9.26999 1 -8 1 5 92.568 9.43496 3 8 -1 -5 89.9702 11.0152 9 -8 -5 -1 88.8663 9.51024 1 -1 -8 -5 99.9366 7.94083 2 -1 -8 -5 100.244 8.41453 1 5 -8 -1 91.7368 12.5141 9 8 -1 -5 93.4873 8.74807 8 8 5 -1 88.1607 10.2062 9 -8 -1 5 70.341 6.51582 2 -1 8 5 98.7276 9.80534 3 -8 -1 5 85.8659 8.66965 3 -8 -1 5 93.4644 8.15819 1 3 -8 -5 103.406 7.39287 2 -8 -5 3 96.2958 8.77844 1 -5 -8 -3 73.9062 9.01439 1 5 8 -3 83.6569 7.79942 8 -5 -8 -3 77.5377 9.07018 5 8 -5 -3 97.184 10.9751 6 -5 8 3 85.0183 8.84518 3 8 3 -5 84.0943 10.1592 9 -8 3 5 85.2847 9.55042 3 -8 -5 3 88.7664 7.81918 2 8 3 -5 85.2967 8.60305 8 -5 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19.4593 1 0 8 6 207.233 20.6067 7 -8 -6 0 248.268 18.5287 5 -6 -8 0 246.96 17.4149 2 -8 0 6 250.484 18.6732 3 -8 -6 0 242.71 17.1046 2 6 8 0 232.384 19.2783 9 -6 -8 0 242.706 18.2246 5 2 -8 -6 30.9137 3.48788 1 2 -8 -6 26.1187 3.44545 5 8 2 -6 22.2486 7.99369 9 -8 -6 2 24.6583 5.29091 2 2 -8 -6 24.9845 4.26513 2 -6 -8 -2 10.334 5.70714 1 8 -6 -2 27.9241 10.623 9 -6 -8 -2 25.4955 5.15504 2 -8 -6 2 20.8876 5.67574 5 8 -6 -2 30.996 10.5347 6 -8 2 6 21.7308 7.13752 3 6 8 -2 25.0989 6.10732 8 -8 -6 2 26.1587 5.60317 1 -8 2 6 18.3123 8.81754 1 -6 -8 -2 15.8079 6.04714 5 6 8 2 24.9943 4.95585 7 6 -8 -2 28.1711 9.57971 9 6 -8 -2 26.3906 7.65472 6 -2 8 6 20.6087 6.99395 7 -8 6 2 21.9355 6.34251 3 -2 8 6 23.6884 7.4358 3 -8 -6 -2 17.2489 6.45731 1 8 -2 -6 21.3186 5.58679 8 8 6 -2 22.9707 6.37127 9 -6 -8 2 25.5257 4.7549 6 -8 -2 6 19.6744 7.42136 1 8 6 -2 14.8823 6.7558 8 -6 -8 2 21.4225 5.9822 1 -6 -8 -4 25.7057 6.84354 1 8 -6 -4 38.7358 6.22744 8 -8 -6 4 42.2128 7.43428 1 4 -8 -6 49.2363 5.0255 2 8 -6 -4 46.0321 10.5074 9 8 -6 -4 45.9528 7.25561 6 -6 8 4 42.9498 7.2018 7 6 8 -4 38.4568 7.07175 8 8 4 -6 62.3053 8.10259 8 -8 4 6 45.1815 8.81499 3 -6 4 8 16.1231 8.24939 3 -8 -4 6 27.2964 9.43514 1 -8 6 4 44.5377 7.74555 3 8 6 -4 32.9444 11.1643 4 8 -4 -6 41.5962 9.5419 9 8 6 -4 50.1731 7.67906 8 -6 -8 4 37.6791 10.3999 1 -4 8 6 44.8814 8.97774 3 8 6 -4 41.5362 7.64639 9 6 -8 -4 38.9982 9.76168 9 -4 8 6 50.6271 8.21732 7 8 -4 -6 41.7836 6.35415 8 -8 6 4 46.976 6.82955 7 8 -6 -6 58.6762 10.6441 9 6 -8 -6 34.5864 5.25147 2 8 6 -6 34.022 8.98435 8 6 8 -6 53.3249 8.80387 8 6 -8 -6 53.5721 5.39952 8 -6 6 8 53.4769 10.9409 3 -8 6 6 59.5481 9.67612 3 -8 -6 6 46.7672 13.1243 1 8 -6 -6 58.9897 6.71943 8 -6 8 6 54.6411 9.13425 7 -8 1 7 110.644 11.7905 3 -8 -7 1 97.6334 10.2164 1 -7 -8 -1 94.6355 9.55406 2 -8 -7 1 96.9598 8.94794 2 7 8 -1 107.88 9.6149 9 8 -7 -1 110.996 20.316 6 8 -7 -1 91.7683 15.4491 9 -8 -7 1 109.492 9.99234 5 8 7 1 93.5016 8.22044 7 8 7 -1 122.915 10.9988 9 8 -1 -7 115.588 12.7976 9 -7 -8 1 94.4682 10.1646 1 7 -8 -1 89.4322 14.835 9 -8 -7 -1 94.6452 10.9716 1 -8 -7 -1 104.899 9.30658 2 7 -8 -1 92.8151 15.5495 6 -7 -8 1 96.683 9.61591 2 7 8 -3 192.505 20.3709 4 -7 -8 -3 206.703 17.5166 5 -8 -7 3 192.73 16.3368 1 -7 -8 -3 225.707 17.6675 1 3 -8 -7 210.21 13.7984 5 -8 3 7 250.23 18.7389 3 7 8 -3 199.79 16.195 8 8 3 -7 224.097 16.6781 8 -8 -7 3 213.62 15.5914 2 8 -7 -3 233.865 20.0118 9 -7 8 3 225.051 17.205 7 -7 -8 -3 213.404 15.9927 2 8 -7 -3 226.046 18.5875 6 7 8 3 196.619 15.5724 7 7 -8 -3 188.831 16.8354 6 8 7 -3 218.4 17.4053 9 -8 7 3 219.288 17.0446 7 7 -8 -3 203.956 19.4426 9 -8 -3 7 144.049 23.2151 1 -3 8 7 193.16 18.2405 3 8 7 -3 208.048 16.7037 8 -7 -8 3 194.303 17.0413 1 -8 7 3 244.885 17.2751 3 8 -3 -7 211.367 15.2229 8 8 7 -3 196.693 20.2927 4 -7 8 5 99.525 11.0401 7 7 8 -5 106.059 10.6572 8 7 8 -5 89.9756 16.6278 4 8 -7 -5 110.768 13.6987 9 8 5 -7 104.041 11.4756 8 8 -7 -5 88.9075 8.64327 8 -8 -7 5 84.4516 12.6412 1 -8 5 7 85.1312 11.6439 3 -7 5 8 94.284 13.3968 3 8 -5 -7 82.8541 8.84161 8 8 7 -5 98.1694 10.611 8 -8 -5 7 35.5258 19.7285 1 -8 7 5 108.12 11.4219 3 8 -5 -7 103.113 13.3325 9 -7 -8 5 86.9398 15.4779 1 -8 7 5 87.6374 10.5893 7 8 7 -5 95.0335 17.3637 4 7 -8 -5 97.8525 8.15414 8 8 7 -7 57.7018 11.3544 8 -7 8 7 50.1964 10.7742 3 -8 -7 7 1.66484 22.0695 1 8 -7 -7 51.149 6.91737 8 -7 7 8 38.3769 11.9825 3 7 -8 -7 50.0663 6.06767 8 -8 7 7 58.3544 11.6752 3 8 -7 -7 65.9559 12.6667 9 -8 -8 0 1315.68 83.2132 1 8 8 0 1179.46 92.5195 9 8 -8 0 1071.46 96.5449 9 -8 -8 0 1188.36 79.1222 2 -8 -8 2 111.866 11.7147 1 -8 -8 2 122.982 10.5067 2 8 8 2 110.782 9.77432 7 8 -8 -2 119.013 16.6338 6 8 8 -2 121.905 11.4667 9 -8 8 2 115.876 12.0332 3 -8 -8 -2 106.986 10.1134 2 -4 8 8 409.775 31.1449 3 -8 8 4 382.374 28.8451 7 -8 4 8 399.163 30.3984 3 4 -8 -8 396.788 26.4491 5 8 8 -4 315.296 31.6091 4 -8 -8 4 403.65 30.6425 1 -8 8 4 387.466 28.0084 3 8 8 -4 341.086 26.5989 8 8 -8 -4 368.763 29.7804 6 -8 -8 6 43.7084 18.7004 1 -8 6 8 69.5585 12.7682 3 8 -8 -6 76.5714 7.6899 8 -8 8 6 93.568 12.0544 3 8 -6 -8 66.3053 8.0199 8 8 8 -6 81.263 11.4049 8 -8 8 6 85.054 11.4178 7 -8 8 8 357.943 27.2941 3 8 -8 -8 300.083 22.6491 8 0 9 1 119.512 9.42842 3 9 0 -1 124.274 13.748 9 0 -9 1 123.192 12.2209 6 1 -9 0 120.366 11.0512 6 0 -9 1 87.0966 10.8916 9 -9 -1 0 128.837 10.9957 1 -1 -9 0 140.154 13.5874 1 0 -9 -1 124.49 12.9739 1 1 -9 0 92.5545 11.3814 9 1 9 0 124.012 9.19651 3 0 9 -1 130.821 8.36724 8 -9 0 1 126.81 10.4504 1 0 9 -1 114.353 13.0321 4 -1 9 0 128.271 12.1192 4 2 -9 1 65.6764 11.0593 9 -9 1 2 89.0969 7.79018 5 -2 9 1 92.1509 8.38013 3 -2 9 1 81.9557 10.0863 4 9 1 -2 100.839 11.4995 9 -1 -9 2 59.5673 10.9262 6 -2 -9 -1 92.281 8.59474 1 2 9 -1 93.3253 7.33155 8 -9 1 2 96.9493 8.21685 3 -9 -2 1 78.8028 8.60118 1 -1 9 -2 78.418 12.3756 4 -9 1 2 87.5026 7.85302 1 2 9 -1 79.5111 10.859 4 1 -9 -2 75.6881 11.474 1 2 -9 1 88.8042 11.9112 6 1 9 2 83.5306 7.71717 3 -9 -2 1 77.8333 8.55513 5 1 9 -2 89.7651 6.77997 8 -1 -9 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7.2269 3.4945 1 -3 9 2 6.62953 5.3602 3 -3 -9 -2 7.11864 4.323 1 2 9 3 6.61874 5.2245 7 -3 -9 -2 6.1877 4.0778 5 -9 2 3 4.87765 4.92453 3 2 -9 -3 2.65095 8.35946 1 2 9 -3 9.96888 3.86968 8 -9 -2 3 3.76499 4.1746 5 9 3 -2 3.8088 1.46052 7 -2 9 3 3.90771 5.70331 3 -9 3 2 4.94215 3.50867 1 -3 -9 2 2.34179 6.44413 6 -9 -2 3 6.91755 4.32035 1 -2 -9 -3 4.77993 4.74594 2 9 3 -2 5.545 6.65558 9 9 -2 -3 7.65814 6.14208 8 -9 -2 3 9.10056 3.98447 3 -2 -9 -3 8.91145 4.14737 1 -2 -9 -3 5.93195 4.02769 5 -3 -9 2 7.87378 9.13266 1 3 -9 -2 3.79142 6.79676 9 9 -2 -3 2.14 13.0395 6 2 9 -3 14.1815 9.86194 4 9 1 -4 42.5895 8.82844 9 9 -4 -1 37.8105 11.4105 9 -9 1 4 34.4942 4.74799 5 9 1 -4 30.7127 6.99517 8 -4 -9 -1 29.0088 6.16768 1 -4 -9 -1 41.1862 6.39154 2 -4 -9 -1 30.692 5.81525 5 4 9 -1 28.7997 3.66203 3 9 1 -4 41.2075 15.4722 4 1 9 4 49.4528 6.95925 3 -9 1 4 34.8698 6.19204 3 -4 9 1 33.702 7.96736 4 1 9 4 50.7954 7.15054 7 -9 -4 1 37.7077 6.34635 5 -9 -4 1 40.8472 4.13856 3 -9 -4 1 56.9228 7.27041 1 4 -9 1 17.3373 14.9132 6 -9 1 4 35.1815 4.6261 1 1 -9 -4 40.1461 5.03174 1 1 -9 -4 39.6733 5.38748 2 9 -1 -4 38.0046 8.97093 9 -9 -1 4 46.4101 6.43699 3 4 -9 -1 43.723 7.77646 6 4 -9 -1 40.8367 8.81604 9 -9 -4 -1 29.427 6.69026 1 -9 -1 4 48.644 5.31258 1 -1 -9 -4 40.7274 5.45667 5 9 -1 -4 66.2651 12.0329 6 9 -1 -4 53.0595 6.74536 8 -9 -1 4 37.0608 5.31825 5 -1 -9 -4 32.043 5.24737 1 -1 -9 -4 37.4714 5.41953 2 -4 -9 1 37.3514 6.91063 1 -1 9 4 43.3898 6.90391 3 9 4 -1 33.8308 8.74103 9 -4 -9 -3 109.852 9.73906 5 3 -9 -4 104.418 8.63654 2 -4 -9 -3 86.5096 8.9443 2 9 3 -4 95.4661 14.7196 4 -9 3 4 108.526 8.13958 5 9 3 -4 90.7806 9.58043 8 -4 9 3 104.164 10.1703 3 9 3 -4 88.915 11.9532 9 -9 -4 3 106.69 8.43209 2 3 9 4 108.583 10.6456 7 4 9 -3 93.2287 13.7533 4 -9 -4 3 96.218 8.33399 3 9 -4 -3 112.429 13.549 9 -9 -4 3 99.8392 9.78105 1 -4 -9 -3 108.803 10.0791 1 4 9 -3 98.1187 8.84812 8 9 -4 -3 124.598 15.1546 6 3 -9 -4 84.2397 12.8415 9 3 -9 -4 101.8 7.08321 8 -9 3 4 105.072 8.14491 1 -9 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440.986 32.7362 3 -4 -12 -4 475.504 33.1202 1 -12 1 5 67.3299 7.37113 1 12 1 -5 84.8714 11.9058 8 5 -12 1 46.6681 23.4077 6 -12 1 5 91.0953 10.314 3 12 1 -5 84.6606 14.7649 9 -12 -5 1 68.892 10.3165 1 -12 -5 1 57.8274 10.2422 5 -5 -12 -1 66.9981 10.3481 2 -5 -12 -1 80.78 10.2985 1 12 -5 -1 82.0713 18.928 9 1 -12 -5 72.1628 8.64966 2 1 12 5 86.679 11.0854 7 -5 12 1 101.52 11.8801 3 5 -12 -1 71.1229 15.8056 6 -1 12 5 96.2241 11.7394 3 -12 -1 5 71.605 8.10798 1 -12 -5 -1 78.2194 11.0639 1 -1 12 5 94.271 11.8074 7 12 -1 -5 87.105 11.5925 8 -12 -5 -1 40.3904 10.6237 5 -12 -1 5 66.0333 9.81917 3 12 -1 -5 95.2322 14.9423 9 5 -12 -1 35.6202 14.2153 9 -1 -12 -5 80.7404 8.99905 1 -5 -12 1 66.9336 12.4589 1 -1 -12 -5 70.6034 8.56102 2 -5 -12 1 72.0057 9.33481 6 -1 -12 -5 74.0438 8.24777 5 12 5 -1 73.9302 14.0991 9 12 3 -5 80.1027 13.6546 9 -5 -12 -3 94.6146 10.3219 1 -12 -5 3 72.8569 10.668 1 -12 3 5 85.8254 11.4205 3 3 -12 -5 93.0791 9.08751 2 12 -5 -3 106.347 17.8095 9 -5 12 3 78.6989 11.9631 3 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14 -5 -7 9.59385 66.8787 6 -5 14 7 17.0886 10.922 7 7 -14 -5 11.5986 7.46129 2 -5 14 7 18.3381 12.7599 3 14 7 -5 11.9508 19.8825 4 -14 -5 7 7.24516 11.4074 1 14 7 -5 9.47943 12.9608 9 7 -14 -5 21.0438 18.4682 9 -14 7 5 0.92174 11.1605 3 -8 -14 0 49.395 12.3802 1 -8 -14 0 52.8824 11.8092 2 -14 -8 0 30.7716 11.5782 5 14 0 -8 26.5027 11.6933 8 0 14 8 5.75874 8.57704 7 0 -14 -8 21.6566 6.30512 2 -14 0 8 48.3772 12.1884 3 -14 -8 0 37.5684 11.1972 1 8 -14 0 16.813 24.019 9 14 0 -8 35.9518 14.1175 9 -8 14 0 93.0389 18.8009 3 14 2 -8 2.47284 13.6178 9 14 2 -8 -11.335 12.1126 8 8 14 -2 3.56963 19.8911 4 -14 2 8 5.40021 12.6087 3 -14 -8 2 0.32222 9.85246 5 2 -14 -8 4.86549 6.48646 2 -14 -8 2 9.39096 9.24023 1 14 -8 -2 -1.7206 21.7049 9 -8 -14 -2 1.01085 9.9143 1 -8 14 2 6.76847 13.9359 3 -8 -14 -2 13.1828 9.34862 2 -8 -14 2 -7.2954 13.7453 2 -14 8 2 9.89045 11.1476 3 14 -2 -8 0.25307 13.5439 9 8 -14 -2 6.94459 19.8838 9 14 -2 -8 14.1678 11.4981 8 14 8 -2 7.48588 15.1712 4 -2 14 8 8.73973 12.2004 7 -8 -14 2 11.8532 16.43 1 8 14 2 -4.6599 8.35933 7 -8 -14 -4 18.6172 9.54006 5 8 14 -4 -2.1135 20.3936 4 -8 -14 -4 20.6741 9.69602 1 14 -8 -4 2.19681 18.8486 9 -14 -8 4 13.3466 9.61394 1 -14 4 8 3.20135 12.313 3 -8 14 4 3.54074 13.2238 3 4 -14 -8 -0.4083 5.95247 2 -8 -14 -4 14.9133 7.99048 2 -8 14 4 11.289 9.75692 7 8 14 4 4.78164 8.87902 7 -4 14 8 -4.1925 11.6907 7 -14 -4 8 10.2023 15.4111 1 14 8 -4 -1.0381 17.275 4 -4 14 8 11.2718 13.4006 3 14 -4 -8 -2.0182 11.0828 8 8 -14 -4 3.67684 17.5013 9 -14 8 4 7.61817 11.5288 3 14 -4 -8 9.33525 14.589 9 9 14 -1 22.9953 21.37 4 -14 -9 1 15.715 10.6529 5 -9 -14 -1 2.85278 10.2265 2 -14 -9 1 19.828 10.4456 1 14 1 -9 9.59359 12.3472 8 -9 -14 -1 19.3087 10.9346 1 -9 14 1 13.6473 16.7661 3 9 -14 -1 12.2547 25.8973 9 -9 -14 1 3.06466 12.414 1 -14 -9 -1 12.4356 11.0315 1 14 -1 -9 22.6197 14.8707 9 14 -1 -9 8.79498 11.0818 8 -14 -9 -1 12.3536 10.8773 5 -9 -14 1 20.6322 12.1709 2 -9 14 3 5.59049 10.1159 7 14 3 -9 64.5233 14.7211 8 -14 -9 3 12.7902 10.7066 1 -9 -14 -3 11.8234 10.177 1 -9 14 3 45.0825 15.1679 3 -9 -14 -3 21.3417 10.1605 5 -14 3 9 19.8085 14.0033 3 14 -3 -9 22.9351 11.1887 8 -14 9 3 5.76324 12.2395 3 9 -14 -3 2.84029 23.2781 6 1 15 0 4.31382 16.2338 4 0 -15 1 4.70433 17.7525 6 1 -15 0 -12.837 15.8086 6 -1 -15 0 4.95406 13.2962 6 -1 15 0 5.41323 8.12605 3 1 15 0 3.50602 8.38711 3 0 15 1 29.9244 8.82481 3 -15 0 1 6.58407 8.85293 1 0 15 -1 12.1759 7.84881 3 0 -15 -1 11.9716 11.3183 6 -15 0 1 5.05099 8.09524 5 0 15 1 0.28274 15.0325 4 0 15 -1 -0.32 16.5014 4 15 0 -1 22.606 15.1669 9 -15 0 1 6.50331 7.3399 3 -1 15 0 -7.3981 15.4119 4 15 1 0 -10.16 14.7585 9 2 15 -1 9.44828 17.4359 4 -15 -2 1 31.9448 9.0194 1 -2 15 1 34.2767 10.3206 3 -2 -15 -1 40.7331 10.9519 6 -2 -15 -1 53.0467 27.2215 1 -15 -2 1 35.4595 9.22369 5 -2 15 1 28.077 14.7198 4 -15 1 2 20.9423 7.94807 5 1 15 2 73.4392 10.4246 3 2 -15 1 25.4067 24.7466 6 15 1 -2 -5.9633 11.3296 4 15 1 -2 52.9775 16.4344 9 -1 -15 2 54.7889 25.9728 6 15 -2 -1 24.2384 16.6602 9 -15 1 2 28.83 8.3502 1 -15 1 2 33.3724 8.64451 3 1 -15 -2 40.053 11.9597 6 -2 -15 1 31.581 16.2005 6 -1 15 2 30.5997 14.3959 4 2 15 1 51.1273 10.1918 3 -15 -1 2 35.8305 8.98171 1 2 15 1 9.73785 17.3826 4 -1 -15 -2 5.84546 26.8487 1 15 -1 -2 65.503 17.3877 9 -2 15 -1 26.6758 16.3554 4 -1 15 2 41.0168 9.8138 3 -1 -15 -2 31.7069 11.1117 2 -15 -1 2 37.4607 8.48094 5 15 2 -1 61.0577 16.975 9 1 15 -2 2.8717 18.4904 4 2 -15 -1 43.4316 15.5564 6 -2 15 -1 39.8586 10.5544 3 1 15 -2 45.2827 8.11372 3 1 -15 2 -0.8828 25.9147 6 15 3 0 18.3796 16.2923 9 3 15 0 7.37597 18.3281 4 -3 -15 0 52.9325 28.5953 1 3 -15 0 20.4992 20.1926 6 -3 15 0 44.769 10.9716 3 0 15 3 37.1555 10.2206 3 -15 -3 0 29.828 10.2088 5 15 0 -3 42.8485 15.6906 9 -15 0 3 36.8008 8.26611 5 -3 -15 0 45.5812 12.1696 6 0 -15 -3 67.1846 10.859 2 -15 0 3 44.3245 8.89291 1 -3 15 0 37.0412 16.6753 4 -15 0 3 60.0493 9.40967 3 2 15 3 17.8881 10.6968 7 -15 2 3 22.7237 8.35217 3 -3 15 2 24.0077 14.2815 4 15 2 -3 10.8029 15.2844 9 -3 -15 -2 10.4807 16.008 1 2 15 3 30.9644 10.2754 3 15 2 -3 -1.9587 14.7051 4 -3 -15 -2 16.4399 10.0365 2 3 15 -2 0.67898 17.4065 4 -15 -3 2 17.6283 9.00708 1 2 -15 -3 35.519 12.2109 6 -15 -3 2 20.6888 9.05858 5 -3 15 2 4.90222 9.79151 3 15 -3 -2 14.2912 17.2026 9 -2 15 3 16.5283 12.8061 4 -2 -15 -3 16.6527 16.6611 1 -15 3 2 15.3128 8.77201 3 -15 -2 3 18.0036 8.45751 1 -2 15 3 30.9501 10.5476 3 3 -15 -2 28.4723 14.0995 6 2 15 -3 0.74749 17.6252 4 -3 -15 2 28.2016 20.1262 6 -2 -15 -3 13.1776 9.20027 2 15 -2 -3 21.7365 15.7916 9 -15 -2 3 23.1068 7.96428 5 15 3 -2 13.4876 12.1641 4 15 3 -2 30.5679 16.1063 9 4 15 -1 -1.7491 17.9737 4 -4 -15 -1 19.434 11.8929 2 -15 -4 1 4.35735 8.90001 5 4 -15 1 3.88977 28.2116 6 1 15 4 8.93582 10.269 7 1 -15 -4 12.2164 8.55757 2 -15 1 4 3.54487 9.25381 3 -4 15 1 19.1207 10.9669 3 -4 -15 -1 -18.717 17.0117 1 -15 -4 1 11.4809 9.37389 1 1 15 4 17.397 10.7868 3 15 1 -4 17.5743 14.553 9 -1 15 4 -1.7706 10.7074 7 -1 -15 -4 14.0944 15.0871 1 -4 -15 1 17.5575 13.8666 6 -1 -15 -4 16.9429 9.20303 2 15 -1 -4 12.6171 15.052 9 15 4 -1 28.8277 17.4969 9 -15 -1 4 7.49474 7.36139 1 -1 15 4 14.843 9.83212 3 -15 -1 4 8.60518 6.78014 5 -4 -15 1 1.08389 29.5426 1 -4 15 -1 23.082 11.7669 3 4 -15 -1 -6.9048 17.9513 6 15 -4 -3 12.2518 17.2062 9 -15 -4 3 11.1881 8.79512 1 -4 15 3 3.1392 10.4224 3 -15 -4 3 12.1238 8.60034 5 -4 -15 -3 16.3209 11.1171 1 15 3 -4 22.4107 19.7295 4 15 3 -4 11.8305 14.9325 9 3 -15 -4 12.4178 9.08528 2 -15 3 4 11.6415 9.2919 3 3 15 4 13.2275 9.55717 7 4 15 -3 3.4674 18.5304 4 -3 -15 -4 0.70599 10.4838 1 4 -15 -3 2.23323 12.7364 6 -3 15 4 9.88017 11.0459 3 -3 -15 -4 9.41864 8.4033 2 15 -3 -4 14.2677 16.6611 9 -15 4 3 8.35698 9.44621 3 15 4 -3 16.5429 14.467 4 4 15 3 0.56716 9.25868 7 15 4 -3 6.65418 14.6367 9 -15 -3 4 7.64193 7.65181 5 -15 -3 4 9.80913 7.73951 1 15 5 0 33.502 18.6681 9 0 -15 -5 59.8826 9.67383 2 -15 -5 0 47.3823 10.9667 1 0 15 5 54.9926 11.9558 7 15 0 -5 37.996 16.1237 9 -5 15 0 57.0074 14.0435 3 5 -15 0 12.6885 28.0507 6 0 15 5 48.918 11.7867 3 -15 0 5 56.532 11.0731 3 -5 -15 0 47.3832 13.2854 2 -5 -15 0 79.3984 19.8818 1 5 15 0 8.8997 19.9699 4 -5 -15 0 52.8613 11.2666 6 -5 -15 -2 42.8037 12.1055 1 15 2 -5 28.9105 14.3729 9 -15 -5 2 31.8797 10.2221 1 2 15 5 41.8384 10.9863 7 2 -15 -5 25.4857 8.5304 2 -5 15 2 16.8449 11.619 3 -15 2 5 40.7727 9.89117 3 -5 -15 -2 30.1053 10.5445 2 5 15 -2 1.87873 19.632 4 -15 -5 2 17.1904 10.2745 5 -15 -2 5 28.8559 7.73069 1 15 5 -2 27.4686 13.5901 4 5 -15 -2 25.2564 17.7534 6 -2 -15 -5 29.7398 8.72083 2 -2 -15 -5 -3.6412 10.2134 1 -5 -15 2 -11.658 32.3108 1 -15 5 2 35.8028 10.3698 3 15 -2 -5 51.7073 15.8136 9 15 5 -2 36.824 15.46 9 -2 15 5 40.1105 11.4777 7 -2 15 5 42.6126 12.2724 3 4 -15 -5 20.1677 8.10132 2 -15 -5 4 22.067 9.29869 1 5 15 -4 0.86224 20.1837 4 15 4 -5 5.31659 14.6984 9 15 4 -5 -12.454 24.8091 4 -5 15 4 14.9835 11.0063 7 -15 4 5 1.75586 11.1044 3 4 15 5 14.5684 10.3353 7 -5 15 4 17.1917 11.831 3 -5 -15 -4 9.04858 9.76397 1 15 -4 -5 8.6024 15.9426 9 -4 15 5 10.2887 12.8274 3 -15 -4 5 11.892 8.32236 1 15 5 -4 14.6707 14.225 9 5 -15 -4 18.4702 9.68204 2 -4 -15 -5 8.67651 9.53483 1 -4 -15 -5 12.7847 8.12245 2 -4 15 5 12.2797 11.0008 7 -15 5 4 26.625 10.2207 3 5 -15 -4 5.56688 12.7815 6 5 15 4 8.40658 9.41834 7 15 5 -4 15.7186 17.3193 4 -15 -6 1 18.5782 10.5174 5 1 -15 -6 18.7688 7.88539 2 -6 -15 -1 32.1429 11.5487 2 -6 15 1 48.7865 14.162 3 15 6 1 -0.8442 15.8521 9 -15 -6 1 22.7646 10.464 1 -6 -15 -1 31.0389 12.8946 1 1 15 6 25.0735 11.2644 7 6 15 -1 -0.3915 20.1138 4 -15 1 6 15.1883 11.3308 3 15 1 -6 24.5683 15.4147 9 15 6 -1 17.6785 16.5428 9 -6 -15 1 1.47385 20.5014 1 -1 15 6 25.6331 11.8925 3 -1 -15 -6 30.0447 8.11104 2 -15 -6 -1 5.21216 10.0577 5 -1 15 6 24.608 11.1564 7 6 -15 -1 9.02648 24.8481 6 15 -1 -6 44.8076 15.3634 9 -6 -15 1 36.0196 14.4894 2 -6 15 3 36.3558 13.1011 3 3 15 6 16.8392 11.212 7 6 15 -3 -1.961 19.3627 4 15 -6 -3 -1.7744 19.014 9 -15 -6 3 19.2335 9.42711 1 -6 -15 -3 21.2897 10.1198 2 15 3 -6 33.2219 15.2622 9 -15 -6 3 21.8186 10.4076 5 -6 -15 -3 43.1691 11.1745 1 -15 3 6 40.9562 11.8361 3 3 -15 -6 16.3769 7.72668 2 -15 6 3 38.0749 10.902 3 -3 -15 -6 29.8485 8.62813 2 15 6 -3 16.3954 15.0277 9 6 -15 -3 16.5522 16.9505 6 15 -3 -6 27.3396 16.0903 9 -15 -3 6 32.3955 8.2875 1 -6 -15 3 26.8704 35.7923 1 -3 15 6 32.6533 12.6508 3 6 15 3 18.132 9.32588 7 15 6 -3 32.0636 15.8051 4 -6 15 5 15.9828 14.2662 3 -6 -15 -5 1.41988 9.21947 5 -15 -6 5 -1.9963 9.30296 1 -6 15 5 28.9213 11.9002 7 -6 -15 -5 7.03978 9.402 1 -15 5 6 8.41063 12.0418 3 5 15 6 11.711 11.8034 7 -5 -15 -6 0.5231 8.3979 5 -5 15 6 16.2094 12.3732 7 -5 15 6 -2.7407 14.1411 3 6 15 5 2.45713 11.1358 7 -15 6 5 10.7549 11.956 3 6 -15 -5 1.14127 13.3166 6 -15 -5 6 9.57149 9.76277 1 15 0 -7 13.4543 14.8517 9 -15 -7 0 8.70421 10.2079 1 0 15 7 16.6419 11.1752 7 15 0 -7 17.2264 12.5477 8 -15 -7 0 6.20402 10.5476 5 -7 15 0 32.4155 16.6348 3 0 -15 -7 8.39602 7.22168 2 -7 -15 0 -2.0566 12.3422 2 7 15 0 -3.707 20.4913 4 15 7 0 2.39928 16.3916 9 -7 -15 0 18.6572 14.3176 1 -15 -7 2 18.6309 10.9733 5 -7 -15 -2 46.9301 12.4207 1 -15 2 7 55.9411 12.3287 3 15 2 -7 10.4318 14.1038 8 2 -15 -7 35.7591 8.18723 2 2 15 7 46.8968 13.1029 7 -7 -15 -2 40.6078 11.3173 2 15 2 -7 36.8729 17.2658 9 15 -7 -2 -8.3446 22.5141 9 7 15 -2 2.47922 20.643 4 -7 15 2 50.8608 14.8371 3 -15 -7 2 45.5067 11.1277 1 -7 -15 2 26.2271 16.1252 2 -2 15 7 26.3248 14.661 3 -2 -15 -7 32.296 7.91334 2 -15 7 2 37.8722 11.4485 3 -7 -15 2 50.1305 23.5913 1 15 7 -2 22.4661 16.1938 4 7 15 2 26.0227 10.2047 7 15 -2 -7 40.3361 15.9821 9 -2 15 7 49.1175 12.1854 7 7 -15 -2 46.1255 22.7175 6 15 7 -2 20.0454 15.6583 9 0 16 0 142.802 13.5463 3 0 -16 0 133.42 22.6245 6 -16 -1 1 41.2739 9.76681 1 -1 16 -1 0.35764 18.0617 4 1 -16 -1 44.7856 16.688 6 16 -1 -1 15.0576 16.2358 9 1 -16 1 44.4073 27.8467 6 -1 16 1 65.2682 17.363 4 16 1 -1 43.1178 16.9467 9 1 16 1 2.28358 18.0393 4 -16 1 1 27.3311 8.94435 3 1 16 -1 0.71948 18.4011 4 -16 1 1 43.0829 9.10953 5 -1 -16 -1 37.7928 13.9674 6 1 16 1 54.2892 10.6197 3 -1 16 -1 43.4407 10.5631 3 -1 16 1 50.8763 10.8586 3 -16 -1 1 59.006 10.0815 5 -1 -16 1 41.1208 21.0279 6 0 16 2 48.9234 11.1029 3 2 -16 0 39.1408 20.0014 6 0 16 2 9.41192 17.5274 4 -2 -16 0 42.5513 16.1797 6 16 0 -2 42.5889 16.964 9 0 -16 2 17.6771 26.0608 6 -16 0 2 40.9044 8.82965 5 2 16 0 0.35368 18.8772 4 0 16 -2 1.14687 19.3527 4 0 16 -2 25.6884 8.78417 3 -2 16 0 38.3275 18.4464 4 -2 16 0 30.8782 10.1734 3 -16 0 2 43.6685 9.65823 1 0 -16 -2 40.648 12.6201 6 -16 2 2 33.2183 9.17714 3 16 -2 -2 47.9032 17.9984 9 2 16 -2 7.35311 19.2837 4 2 -16 -2 48.2696 15.1328 6 -2 -16 2 39.1558 28.1342 6 -2 -16 -2 6.268 29.4325 1 -16 -2 2 30.7763 10.0555 1 -2 16 2 33.1322 11.1757 3 -16 -2 2 44.0197 9.54618 5 -2 16 -2 45.2748 10.9217 3 -2 -16 -2 20.6843 12.3425 2 16 2 -2 18.2189 17.2189 9 -2 16 2 31.2477 16.6538 4 -3 -16 -1 29.6418 11.966 6 -16 -3 1 15.4652 9.66332 5 1 -16 -3 38.478 12.9547 6 16 1 -3 25.3047 16.5853 9 1 16 3 19.0662 12.0247 7 3 -16 1 13.8943 31.1871 6 -16 1 3 31.6266 9.35264 3 16 -3 -1 -2.0014 16.4339 9 3 16 -1 1.86063 19.2259 4 -3 16 1 50.0985 10.9901 3 1 16 3 38.1361 11.8301 3 -16 -3 1 17.9064 9.94752 1 1 -16 -3 30.8414 11.24 2 -3 -16 -1 40.0893 29.8826 1 -1 16 3 29.3634 11.1164 3 16 3 -1 27.6145 18.1174 9 -3 16 -1 28.9866 11.8933 3 -3 -16 1 35.0412 17.6437 6 -16 -1 3 23.0359 8.89185 1 3 -16 -1 49.3061 19.5 6 -16 -1 3 30.7947 8.72324 5 16 -1 -3 28.7292 16.6873 9 -1 -16 -3 -8.476 29.3912 1 3 16 1 1.46206 18.7687 4 -1 16 3 33.1301 16.3924 4 -1 -16 -3 32.7997 10.9616 2 -16 3 1 28.6506 8.75792 3 3 16 3 18.0733 11.1432 7 3 -16 -3 27.7262 13.5811 6 -3 -16 -3 29.8144 10.9789 2 -16 3 3 31.4825 9.91581 3 16 3 -3 -1.458 15.31 4 16 -3 -3 37.0748 17.494 9 -3 16 3 6.54351 11.4059 3 -16 -3 3 19.5318 8.62402 5 -16 -3 3 32.9392 9.66852 1 3 16 -3 -0.4273 20.2503 4 16 3 -3 33.1523 17.308 9 -3 -16 -3 35.9212 18.2113 1 -4 -16 0 141.448 19.2052 6 0 16 4 144.981 17.1259 7 -4 -16 0 110.142 33.9853 1 4 -16 0 132.035 31.4659 6 16 0 -4 149.889 20.5849 9 -4 16 0 160.5 16.9291 3 0 -16 -4 159.652 15.079 2 -4 -16 0 120.819 18.3349 2 -16 -4 0 97.8701 15.3841 5 0 16 4 166.23 16.7198 3 -16 2 4 29.7079 9.42851 3 -16 -4 2 2.64137 9.42849 1 4 16 -2 -1.1579 19.4654 4 -4 16 2 2.33033 11.5433 3 -16 -4 2 5.10781 9.24804 5 16 -4 -2 20.4142 18.1731 9 16 2 -4 7.1361 15.3452 9 -4 -16 -2 17.2998 17.6808 1 2 -16 -4 12.3741 9.88985 2 2 16 4 -7.2532 11.4335 7 16 4 -2 2.75833 16.8685 9 -16 -2 4 4.56461 7.91771 1 16 -2 -4 9.57067 16.213 9 4 -16 -2 5.98952 18.2284 6 -2 -16 -4 -1.2833 18.5151 1 -2 16 4 8.89641 11.5612 7 16 4 -2 -20.564 14.1628 4 -16 4 2 18.0418 9.12428 3 -2 16 4 -2.5843 11.4879 3 -16 -2 4 17.4234 8.70852 5 -2 -16 -4 18.0628 10.0416 2 -5 -16 -1 13.553 12.4244 2 16 1 -5 36.2913 18.0105 9 -16 -5 1 22.7779 10.548 1 -5 -16 -1 -6.708 19.3137 1 1 -16 -5 12.9624 9.56498 2 -5 16 1 17.5802 13.2984 3 5 16 -1 0.82206 21.1385 4 -16 1 5 7.59658 10.1924 3 -16 -5 1 8.03394 10.1834 5 1 16 5 21.2279 12.5228 7 -5 -16 1 25.9569 32.7267 1 16 -1 -5 0.88145 17.1315 9 -1 16 5 27.1402 13.4916 3 -1 16 5 11.5683 12.7704 7 5 16 1 3.25595 21.7146 4 5 -16 -1 33.2688 24.4316 6 16 5 -1 8.3005 17.7119 9 -1 -16 -5 32.2213 9.22906 2 -5 16 -1 4.03396 15.3501 3 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Co1 N1 106.9(6) 46 48_554 ? N1 Co1 N1 110.8(3) 48_554 . ? N1 Co1 N1 110.8(3) 46 . ? N1 Co1 N1 110.8(3) 46 3_655 ? N1 Co1 N1 110.8(3) 48_554 3_655 ? N1 Co1 N1 106.9(6) 3_655 . ? C2 N1 Co1 128.4(7) . . ? C2 N1 C1 105.2(9) . . ? C1 N1 Co1 125.8(8) . . ? N1 C2 N1 113.6(11) . 14_665 ? N1 C2 C3 123.1(6) 14_665 . ? N1 C2 C3 123.1(6) . . ? N1 C1 H1 126.0 . . ? C1 C1 N1 108.0(7) 14_665 . ? C1 C1 H1 126.0 14_665 . ? C2 C3 H3A 109.5 . . ? C2 C3 H3B 109.5 . . ? C2 C3 H3C 109.5 . . ? H3A C3 H3B 109.5 . . ? H3A C3 H3C 109.5 . . ? H3B C3 H3C 109.5 . . ? N3 N2 N3 180.0 3_655 . ? N4 N5 N4 175(10) 2_665 . ? N2 N3 N3 0.000(4) . 3_655 ? N11 N10 N11 115(10) 6_665 12_654 ? N11 N10 N11 115(10) 12_654 . ? N11 N10 N11 115(10) 6_665 . ? N10 N11 N11 32(8) . 6_665 ? N10 N11 N11 32(8) . 12_654 ? N11 N11 N11 60.00(3) 6_665 12_654 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Co1 N1 1.984(9) 46 ? Co1 N1 1.984(9) . ? Co1 N1 1.984(9) 48_554 ? Co1 N1 1.984(9) 3_655 ? N1 C2 1.333(10) . ? N1 C1 1.385(11) . ? C2 C3 1.50(2) . ? C1 C1 1.38(3) 14_665 ? C1 H1 1.0770 . ? C3 H3A 1.0830 . ? C3 H3B 1.0830 . ? C3 H3C 1.0830 . ? N2 N3 0.61(5) 3_655 ? N2 N3 0.61(5) . ? N5 N4 1.05(3) . ? N5 N4 1.05(3) 2_665 ? N8 N9 0.98(2) . ? N3 N3 1.22(10) 3_655 ? N6 N7 0.57(19) . ? N10 N11 0.67(15) . ? N10 N11 0.67(15) 6_665 ? N10 N11 0.67(15) 12_654 ? N11 N11 1.1(2) 6_665 ? N11 N11 1.1(2) 12_654 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Co1 N1 C2 N1 173.1(5) . . . 14_665 ? Co1 N1 C2 C3 -3(2) . . . . ? Co1 N1 C1 C1 -172.6(6) . . . 14_665 ? C2 N1 C1 C1 -1.2(10) . . . 14_665 ? C1 N1 C2 N1 2.1(18) . . . 14_665 ? C1 N1 C2 C3 -174.5(13) . . . . ? N11 N10 N11 N11 -137(63) 12_654 . . 6_665 ? N11 N10 N11 N11 137(63) 6_665 . . 12_654 ?