#------------------------------------------------------------------------------ #$Date: 2023-11-23 01:39:40 +0200 (Thu, 23 Nov 2023) $ #$Revision: 287746 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/77/7247767.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7247767 loop_ _publ_author_name 'Jones, Isabelle M.' 'Turner, Gemma F.' 'Pitts, Kari' 'Powell, Rees' 'Riboldi-Tunnicliffe, Alan' 'Williamson, Rachel' 'Boer, Stephanie' 'Allen, Lauren' 'Moggach, Stephen A.' _publ_section_title ; High-pressure induced guest-mediated gate opening behaviour of the Co-based framework ZIF-67 ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D3CE00979C _journal_year 2023 _chemical_absolute_configuration ad _chemical_formula_moiety 'C8 H10 Co N4, 18.667(N0.5)' _chemical_formula_sum 'C8 H10 Co N13.33' _chemical_formula_weight 351.89 _chemical_name_common ZIF-67 _space_group_crystal_system cubic _space_group_IT_number 217 _space_group_name_Hall 'I -4 2 3' _space_group_name_H-M_alt 'I -4 3 m' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2023-10-04 _audit_creation_method ; Olex2 1.5 (compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817) ; _audit_update_record ; 2023-10-04 deposited with the CCDC. 2023-11-21 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 12 _cell_length_a 16.6284(4) _cell_length_b 16.6284(4) _cell_length_c 16.6284(4) _cell_measurement_reflns_used 3710 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 23.0470 _cell_measurement_theta_min 3.4470 _cell_volume 4597.81(19) _computing_cell_refinement 'CrysAlisPro 1.171.42.58a (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.42.58a (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.58a (Rigaku OD, 2022)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _diffrn_ambient_temperature 293(2) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.978 _diffrn_measured_fraction_theta_max 0.975 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -47.00 32.00 0.50 60.00 -- 13.12 26.00 -8.00 158 2 \w -96.00 -68.00 0.50 60.00 -- 13.12-178.00 90.00 56 3 \w -22.00 57.00 0.50 60.00 -- 13.12 -53.00-162.00 158 4 \w -3.00 76.00 0.50 60.00 -- 13.12 -97.00-143.00 158 5 \w -27.00 -3.00 0.50 60.00 -- 13.12 19.00-150.00 48 6 \w -96.00 -68.00 0.50 60.00 -- 13.12-178.00 -90.00 56 7 \w -61.00 16.00 0.50 60.00 -- -13.27 67.00 -23.00 154 8 \w -12.00 40.00 0.50 60.00 -- -13.27 -53.00-162.00 104 9 \w 32.00 58.00 0.50 60.00 -- -13.27-114.00-135.00 52 10 \w -38.00 -13.00 0.50 60.00 -- -13.27 77.00 -30.00 50 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Single source at home/near, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0390816000 _diffrn_orient_matrix_UB_12 0.0152303000 _diffrn_orient_matrix_UB_13 0.0076773000 _diffrn_orient_matrix_UB_21 -0.0065473000 _diffrn_orient_matrix_UB_22 -0.0043421000 _diffrn_orient_matrix_UB_23 0.0419340000 _diffrn_orient_matrix_UB_31 0.0157898000 _diffrn_orient_matrix_UB_32 -0.0395993000 _diffrn_orient_matrix_UB_33 -0.0016444000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0743 _diffrn_reflns_av_unetI/netI 0.0513 _diffrn_reflns_Laue_measured_fraction_full 0.978 _diffrn_reflns_Laue_measured_fraction_max 0.975 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 8667 _diffrn_reflns_point_group_measured_fraction_full 0.961 _diffrn_reflns_point_group_measured_fraction_max 0.960 _diffrn_reflns_theta_full 23.207 _diffrn_reflns_theta_max 23.207 _diffrn_reflns_theta_min 3.465 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Mo) X-ray Source' _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 1.140 _exptl_absorpt_correction_T_max 0.7449 _exptl_absorpt_correction_T_min 0.6338 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0907 before and 0.0782 after correction. The Ratio of minimum to maximum transmission is 0.8509. The \l/2 correction factor is Not present. ; _exptl_crystal_colour 'clear bluish violet' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier bluish _exptl_crystal_colour_primary violet _exptl_crystal_density_diffrn 1.525 _exptl_crystal_description block _exptl_crystal_F_000 2140 _exptl_crystal_recrystallization_method 'Re-crystallisation from solvent' _exptl_crystal_size_max 0.14 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.09 _refine_diff_density_max 0.848 _refine_diff_density_min -0.811 _refine_diff_density_rms 0.153 _refine_ls_abs_structure_details ; Flack x determined using 180 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.07(2) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.178 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 49 _refine_ls_number_reflns 619 _refine_ls_number_restraints 11 _refine_ls_restrained_S_all 1.207 _refine_ls_R_factor_all 0.1064 _refine_ls_R_factor_gt 0.0871 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1508P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2123 _refine_ls_wR_factor_ref 0.2224 _reflns_Friedel_coverage 0.754 _reflns_Friedel_fraction_full 0.940 _reflns_Friedel_fraction_max 0.940 _reflns_number_gt 491 _reflns_number_total 619 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL zif67_ln2_2750_a.res in I-43m zif67_ln2_2750.res created by SHELXL-2018/3 at 10:49:05 on 04-Oct-2023 REM Old TITL ZIF67_LN2_2750 in I-43m REM SHELXT solution in I-43m: R1 0.115, Rweak 0.064, Alpha 0.142 REM 0.000 for 0 systematic absences, Orientation as input REM Flack x = 0.147 ( 0.022 ) from 184 Parsons' quotients REM Formula found by SHELXT: C7 N11 Co CELL 0.71073 16.6284 16.6284 16.6284 90 90 90 ZERR 12 0.0004 0.0004 0.0004 0 0 0 LATT -2 SYMM -X,-Y,+Z SYMM -X,+Y,-Z SYMM +X,-Y,-Z SYMM +Z,+X,+Y SYMM +Z,-X,-Y SYMM -Z,-X,+Y SYMM -Z,+X,-Y SYMM +Y,+Z,+X SYMM -Y,+Z,-X SYMM +Y,-Z,-X SYMM -Y,-Z,+X SYMM +Y,+X,+Z SYMM -Y,-X,+Z SYMM +Y,-X,-Z SYMM -Y,+X,-Z SYMM +X,+Z,+Y SYMM -X,+Z,-Y SYMM -X,-Z,+Y SYMM +X,-Z,-Y SYMM +Z,+Y,+X SYMM +Z,-Y,-X SYMM -Z,+Y,-X SYMM -Z,-Y,+X SFAC C H Co N UNIT 96 120 12 160 EQIV $1 1-Y,1-X,+Z EQIV $2 1+Z,1-X,-Y EQIV $3 1-Y,-Z,-1+X EQIV $4 1+Z,+Y,-1+X EQIV $5 +X,-Z,-Y EQIV $6 0.5+Y,0.5+Z,-0.5+X EQIV $7 0.5-Z,0.5-Y,-0.5+X DFIX 1.55 C3 C2 DFIX 1.337 0.01 N1 C2 DFIX 1.387 0.01 C1 N1 EADP C1 C2 N1 DFIX 2.175 0.01 C1 C2 FLAT C1 C2 N1 C3 RIGU C3 C2 EADP N15 N13 EADP N4 N5 DFIX 1.08 N9 N8 DFIX 1.08 N4 N5 EADP N3 N2 EADP N6 N7 EADP N9 N8 DFIX 1.09 N8 N9 L.S. 10 0 0 PLAN 5 CONF FREE N10 N10_$2 FREE N10 N10_$1 FREE N9 N10_$6 FREE N9 N10_$7 FREE N12 N10 FREE N12 N10_$1 FREE N12 N12_$3 FREE N12 N12_$4 FREE N12 N12_$2 FREE N12 N12_$5 FREE N12 N12_$1 BOND list 4 MORE -1 BOND $H fmap 2 53 acta REM REM REM WGHT 0.150800 FVAR 0.13932 CO1 3 0.500000 0.250000 0.000000 10.25000 0.03652 0.03533 = 0.03652 0.00000 0.00000 0.00000 N1 4 0.585522 0.319582 0.040912 11.00000 0.03696 0.03708 = 0.03573 0.00219 -0.00407 -0.00424 C2 1 0.632590 0.367410 -0.003299 10.50000 0.03696 0.03708 = 0.03573 0.00219 -0.00407 -0.00424 C1 1 0.602711 0.338287 0.119940 11.00000 0.03696 0.03708 = 0.03573 0.00219 -0.00407 -0.00424 AFIX 43 1.0770 H1 2 0.575226 0.311805 0.172268 11.00000 -1.20000 AFIX 0 C3 1 0.628424 0.371576 -0.094486 10.50000 0.04558 0.04558 = 0.04556 0.01120 -0.01120 -0.01267 PART -1 AFIX 33 1.0830 H3A 2 0.672321 0.414466 -0.116286 10.50000 -1.50000 H3B 2 0.641197 0.312818 -0.119508 10.50000 -1.50000 H3C 2 0.568785 0.390413 -0.112655 10.50000 -1.50000 AFIX 0 PART 0 N2 4 0.500000 0.500000 0.000000 10.08333 0.05976 N5 4 0.500000 0.500000 -0.232173 10.25000 0.12234 N8 4 0.783922 0.216078 0.077892 10.50000 0.12188 N3 4 0.500000 0.500000 -0.039320 10.16667 0.05976 N9 4 0.763067 0.236933 0.024881 10.50000 0.12188 N6 4 0.745023 0.254977 -0.254977 10.05555 0.06384 N4 4 0.544076 0.455924 -0.228696 10.25000 0.12234 N11 4 0.584801 0.415199 -0.415199 10.08333 0.09407 PART 2 N12 4 0.575888 0.424112 -0.461299 10.08333 0.03645 PART 0 N7 4 0.764298 0.235702 -0.235702 10.11112 0.06384 N13 4 0.875540 0.124460 -0.124460 10.08333 0.07363 PART 1 N10 4 0.556152 0.443848 -0.388784 10.08333 0.08043 PART 0 N15 4 0.835262 0.116385 -0.116385 10.08335 0.07363 HKLF 4 REM zif67_ln2_2750_a.res in I-43m REM wR2 = 0.2224, GooF = S = 1.178, Restrained GooF = 1.207 for all data REM R1 = 0.0871 for 491 Fo > 4sig(Fo) and 0.1064 for all 619 data REM 49 parameters refined using 11 restraints END WGHT 0.1664 0.0000 REM Highest difference peak 0.848, deepest hole -0.811, 1-sigma level 0.153 Q1 1 0.7528 0.2472 -0.2189 10.50000 0.05 0.85 Q2 1 0.5068 0.5209 -0.2417 11.00000 0.05 0.84 Q3 1 0.7574 0.2426 -0.2806 10.50000 0.05 0.81 Q4 1 0.8845 0.1485 -0.1485 10.50000 0.05 0.80 Q5 1 0.8011 0.2447 0.0541 11.00000 0.05 0.67 REM The information below was added by Olex2. REM REM R1 = 0.0871 for 491 Fo > 4sig(Fo) and 0.1064 for all 8667 data REM 49 parameters refined using n/a restraints REM Highest difference peak 0.85, deepest hole -0.81 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.1064 REM R1_gt = 0.0871 REM wR_ref = 0.2224 REM GOOF = 1.178 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 8667 REM Reflections_gt = 491 REM Parameters = 49 REM Hole = -0.81 REM Peak = 0.85 REM Flack = 0.07(2) ; _cod_data_source_file d3ce00979c2.cif _cod_data_source_block zif67_ln2_2750 _cod_original_cell_volume 4597.8(3) _cod_database_code 7247767 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'Co C8 H10 N4' _chemical_oxdiff_usercomment 'ZIF67 @ 2.75GPa in LN2' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _diffrn_orient_matrix_axis[1] matrixX _diffrn_orient_matrix_axis[2] matrixY _diffrn_orient_matrix_axis[3] matrixZ _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances C3-C2 1.55 with sigma of 0.02 N1-C2 1.337 with sigma of 0.01 C1-N1 1.387 with sigma of 0.01 C1-C2 2.175 with sigma of 0.01 N9-N8 1.08 with sigma of 0.02 N4-N5 1.08 with sigma of 0.02 N8-N9 1.09 with sigma of 0.02 3. Restrained planarity C1, C2, N1, C3 with sigma of 0.1 4. Uiso/Uaniso restraints and constraints Uanis(C1) = Uanis(C2) = Uanis(N1) Uiso(N15) = Uiso(N13) Uiso(N4) = Uiso(N5) Uiso(N3) = Uiso(N2) Uiso(N6) = Uiso(N7) Uiso(N9) = Uiso(N8) 5. Rigid body (RIGU) restrains C3, C2 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 6. Others Fixed Sof: H3A(0.5) H3B(0.5) H3C(0.5) N2(0.083333) N3(0.166667) N6(0.05555) N4(0.25) N11(0.083333) N12(0.083333) N7(0.11112) N13(0.083333) N10(0.083333) N15(0.08335) 7.a Me refined with riding coordinates: C3(H3A,H3B,H3C) 7.b Aromatic/amide H refined with riding coordinates: C1(H1) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 4.631 _oxdiff_exptl_absorpt_empirical_full_min 0.666 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, z' '-y, -x, z' 'y, -x, -z' '-y, x, -z' 'x, z, y' '-x, z, -y' '-x, -z, y' 'x, -z, -y' 'z, y, x' 'z, -y, -x' '-z, y, -x' '-z, -y, x' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' 'z+1/2, x+1/2, y+1/2' 'z+1/2, -x+1/2, -y+1/2' '-z+1/2, -x+1/2, y+1/2' '-z+1/2, x+1/2, -y+1/2' 'y+1/2, z+1/2, x+1/2' '-y+1/2, z+1/2, -x+1/2' 'y+1/2, -z+1/2, -x+1/2' '-y+1/2, -z+1/2, x+1/2' 'y+1/2, x+1/2, z+1/2' '-y+1/2, -x+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' 'x+1/2, z+1/2, y+1/2' '-x+1/2, z+1/2, -y+1/2' '-x+1/2, -z+1/2, y+1/2' 'x+1/2, -z+1/2, -y+1/2' 'z+1/2, y+1/2, x+1/2' 'z+1/2, -y+1/2, -x+1/2' '-z+1/2, y+1/2, -x+1/2' '-z+1/2, -y+1/2, x+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co1 Co 0.500000 0.250000 0.000000 0.0361(14) Uani 1 4 d S T P . . N1 N 0.5855(6) 0.3196(6) 0.0409(5) 0.037(2) Uani 1 1 d D . . . . C2 C 0.6326(6) 0.3674(6) -0.0033(8) 0.037(2) Uani 1 2 d DS T P . . C1 C 0.6027(8) 0.3383(8) 0.1199(6) 0.037(2) Uani 1 1 d D . . . . H1 H 0.575226 0.311805 0.172268 0.044 Uiso 1 1 calc R U . . . C3 C 0.6284(8) 0.3716(8) -0.0945(11) 0.046(5) Uani 1 2 d DS T P . . H3A H 0.672321 0.414466 -0.116286 0.068 Uiso 0.5 1 calc R U P A -1 H3B H 0.641197 0.312818 -0.119508 0.068 Uiso 0.5 1 calc R U P A -1 H3C H 0.568785 0.390413 -0.112655 0.068 Uiso 0.5 1 calc R U P A -1 N2 N 0.500000 0.500000 0.000000 0.060(7) Uiso 0.6666 8 d S . P . . N5 N 0.500000 0.500000 -0.232(2) 0.122(11) Uiso 1 4 d DS . P . . N8 N 0.7839(12) 0.2161(12) 0.0779(17) 0.122(7) Uiso 1 2 d DS . P . . N3 N 0.500000 0.500000 -0.0393(17) 0.060(7) Uiso 0.6667 4 d S . P . . N9 N 0.7631(12) 0.2369(12) 0.0249(17) 0.122(7) Uiso 1 2 d DS . P . . N6 N 0.745(4) 0.255(4) -0.255(4) 0.064(11) Uiso 0.3333 6 d S . P . . N4 N 0.5441(11) 0.4559(11) -0.229(4) 0.122(11) Uiso 0.5 2 d DS . P . . N11 N 0.585(5) 0.415(5) -0.415(5) 0.09(4) Uiso 0.5 6 d S . P . . N12 N 0.576(3) 0.424(3) -0.461(6) 0.04(3) Uiso 0.1667 2 d S . P B 2 N7 N 0.7643(17) 0.2357(17) -0.2357(17) 0.064(11) Uiso 0.6667 6 d S . P . . N13 N 0.876(3) 0.124(3) -0.124(3) 0.07(2) Uiso 0.5 6 d S . P . . N10 N 0.556(7) 0.444(7) -0.389(10) 0.08(4) Uiso 0.1667 2 d S . P B 1 N15 N 0.835(8) 0.116(6) -0.116(6) 0.07(2) Uiso 0.1667 2 d S . P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Co1 0.0365(15) 0.035(2) 0.0365(15) 0.000 0.000 0.000 N1 0.037(4) 0.037(5) 0.036(4) 0.002(4) -0.004(4) -0.004(3) C2 0.037(4) 0.037(5) 0.036(4) 0.002(4) -0.004(4) -0.004(3) C1 0.037(4) 0.037(5) 0.036(4) 0.002(4) -0.004(4) -0.004(3) C3 0.046(8) 0.046(8) 0.046(8) 0.011(6) -0.011(6) -0.013(11) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _axis.id _axis.type _axis.equipment _axis.parity _axis.depends_on _axis.zero _axis.vector[1] _axis.vector[2] _axis.vector[3] source . source . . . 1.00000000 0.00000000 0.00003403 omega rotation goniometer -1 . 0.12240000 0.00000000 0.00000000 1.00000000 kappa rotation goniometer -1 omega 0.28425000 -0.76560404 0.00000000 0.64331210 phi rotation goniometer -1 kappa . -0.00006266 0.00000000 1.00000000 theta rotation goniometer -1 . 0.19892000 0.00000000 0.00000000 1.00000000 matrixX general general . phi . 1.00000000 0.00000000 0.00000000 matrixY general general . phi . 0.00000000 1.00000000 0.00000000 matrixZ general general . phi . 0.00000000 0.00000000 1.00000000 dacX translation general . phi . 0.00000000 1.00000000 0.00000000 dacY translation general . phi . -1.00000000 0.00000000 0.00000000 dacZ translation general . phi . 0.00000000 0.00000000 1.00000000 loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u _diffrn_refln_scale_group_code 2 0 -2 141.98 10.5876 3 0 2 2 130.233 9.88569 3 0 -2 -2 126.952 9.5225 7 0 -2 -2 133.196 8.33595 4 0 2 2 141.852 9.49477 7 0 2 -2 119.215 8.15011 1 -2 0 2 156.184 10.0922 5 0 2 -2 118.31 8.18252 2 0 -2 -2 124.592 8.17453 8 0 -2 2 113 8.19948 1 2 -2 0 128.236 10.2473 3 2 0 -2 131.693 9.15802 7 0 2 2 131.06 7.94554 8 0 2 2 135.983 8.28949 1 -2 2 0 123.262 9.91791 3 0 -2 2 124.443 7.87092 2 0 2 -2 122.563 8.80598 6 0 -2 2 124.968 7.69971 9 -2 2 0 123.344 9.29314 7 2 -2 0 139.1 8.48396 6 -2 2 0 130.253 8.45884 4 2 0 -2 144.35 7.79313 1 0 -2 -2 124.594 9.8185 3 -2 0 2 135.084 7.85434 1 2 -2 -2 2473.27 154.2 10 2 -2 -2 2391.83 153.523 1 2 -2 -2 2443.63 156.512 4 -2 2 2 2567.48 191.691 3 2 -2 -2 2591.72 155.33 6 -2 2 2 2619.51 150.281 1 -2 2 2 2811.46 146.582 6 2 -2 -2 2622.33 182.17 5 2 -2 -2 2461.43 175.316 7 -2 2 2 2577.21 180.177 7 -2 2 2 2517.87 157.27 8 -1 0 -3 384.985 24.678 1 1 0 -3 376.868 22.0521 10 -1 3 0 354.601 27.6676 3 0 -1 3 327.58 23.0944 8 0 3 1 390.791 26.2828 7 0 3 1 386.335 23.173 4 0 -1 3 339.94 24.7192 6 1 -3 0 398.492 26.2147 7 0 1 3 403.652 22.3812 4 1 -3 0 374.648 21.7279 2 0 -1 -3 377.213 22.7595 1 1 0 -3 361.655 23.3799 4 1 -3 0 397.288 22.4775 10 1 -3 0 375.236 22.6093 8 0 -3 1 386.872 21.9576 2 0 1 -3 377.548 22.7144 8 -1 3 0 358.495 22.5041 9 -1 3 0 398.176 26.2843 7 1 0 -3 365.911 27.9175 3 0 -3 -1 419.552 22.1974 8 0 -3 1 365.649 23.8595 4 -1 3 0 366.307 23.5365 4 0 -1 3 339.059 27.3314 3 1 -3 0 377.517 27.5134 3 0 1 3 433.69 21.6926 1 0 -3 -1 400.319 22.6187 2 -1 3 0 395.749 22.0024 6 0 -1 -3 352.005 22.9664 8 0 1 -3 373.243 27.7088 3 0 3 1 376.009 23.0912 1 -1 3 0 379.767 22.5498 8 0 -1 -3 342.392 24.659 4 1 0 -3 377.598 22.7324 8 0 -3 -1 383.877 23.6434 4 0 3 -1 392.456 22.9788 4 -1 0 3 384.085 22.2823 4 0 1 -3 347.777 23.8844 1 0 1 -3 338.437 25.9016 7 0 -1 3 348.128 25.9598 7 0 3 1 363.212 28.0474 3 0 -1 3 348.185 23.8802 1 -1 0 -3 395.409 27.6966 3 -1 0 3 398.838 26.2445 7 1 0 -3 355.215 25.9891 7 -1 3 0 410.407 22.0424 10 0 -1 -3 385.632 27.5296 3 0 -3 1 426.281 28.428 5 1 0 -3 384.385 22.3602 1 0 1 -3 359.152 24.3979 6 0 -1 -3 358.809 26.1678 7 0 3 -1 384.151 26.436 7 2 -1 -3 92.1225 6.43183 5 -1 3 -2 70.0112 5.26444 2 -2 3 1 89.3565 5.98861 4 2 -1 -3 84.8739 5.83244 8 2 -1 -3 77.6923 5.99829 7 -1 3 -2 76.7321 5.14166 9 -2 3 1 84.6074 6.26695 7 -1 2 3 87.7196 5.56377 4 -2 3 1 89.0807 5.53562 8 2 -3 1 74.2617 5.6726 10 -1 3 -2 74.4074 5.85141 6 1 -3 -2 71.6209 5.42145 1 2 -3 1 83.3699 6.2252 7 -2 3 1 88.9414 5.14877 1 2 -1 -3 77.9944 5.05377 6 -1 2 3 95.0906 6.89825 3 -2 -1 3 63.0972 6.49062 3 -1 3 -2 65.889 5.56423 4 -3 1 2 87.1743 7.32801 3 1 -3 -2 75.0542 5.83881 4 -2 3 1 87.3845 5.46672 9 -1 2 3 87.4303 5.60944 8 1 -2 3 87.2372 5.54765 1 -2 -1 3 76.4239 6.5534 5 2 -1 -3 82.2004 5.22777 10 2 -1 -3 80.0087 5.50732 4 -1 2 3 98.8218 5.59979 1 -2 3 1 88.1826 6.91485 3 1 2 -3 87.5723 5.53762 1 1 -3 -2 78.0605 5.2202 9 1 -2 3 86.1762 6.07625 6 3 -2 -1 78.649 6.29492 4 2 -1 -3 84.6656 7.06187 3 2 -3 1 86.2715 6.01265 4 2 -3 1 87.2004 6.47817 6 1 2 -3 97.2374 7.02783 5 -1 2 -3 74.7967 6.20691 3 2 -3 -1 87.7789 5.38281 8 -2 1 3 92.5957 5.48104 1 1 -3 2 90.5662 5.28051 9 -3 2 1 97.0348 6.51049 7 3 -1 -2 83.8812 7.36311 3 1 -2 -3 75.4717 5.93107 7 2 1 -3 91.7405 5.4033 1 -2 3 -1 69.914 5.3709 9 -1 3 2 91.1062 6.6995 3 -1 3 2 85.8488 5.67871 1 -1 2 -3 70.5621 5.24066 8 2 -3 -1 73.8912 5.23143 1 -1 3 2 90.1581 5.38642 8 -1 3 2 85.3178 6.24538 7 3 -1 -2 73.2407 6.02414 7 2 -3 -1 81.2982 6.66088 3 -1 2 -3 71.5986 5.62013 1 1 -3 2 80.0476 5.39655 10 -2 3 -1 67.156 6.30093 3 1 -2 -3 73.743 6.51508 3 -3 2 1 87.9261 6.23442 4 -1 -2 3 73.1608 5.45482 1 -2 3 -1 77.1878 5.88428 6 -1 3 2 90.7907 5.44504 2 2 -3 -1 82.9373 5.66028 6 1 -2 -3 82.136 5.54019 4 -1 3 2 97.4216 5.54905 10 1 -2 -3 78.6629 5.17019 9 -1 -2 3 71.2542 6.3022 3 -3 2 1 92.3913 7.31528 3 1 -2 -3 70.8805 5.42679 10 -2 3 -1 75.4033 5.82688 7 1 -2 -3 78.9422 5.45405 8 2 -3 -1 83.205 5.68737 4 -2 3 -1 77.1825 5.67981 4 1 -2 -3 76.0554 5.13417 2 1 -3 2 81.9414 5.96617 4 0 3 -3 122.768 8.82899 4 0 -3 -3 134.55 8.75256 4 0 3 3 133.425 8.78749 1 0 3 -3 130.485 10.3329 5 0 -3 -3 138.662 8.95798 1 3 0 -3 138.127 8.48542 1 3 -3 0 141.337 9.17988 6 -3 3 0 142.631 8.90476 4 0 -3 3 127.47 8.21294 2 0 -3 -3 137.582 9.79072 7 0 -3 3 129.528 7.99314 9 -3 0 3 143.708 10.2881 5 -3 3 0 127.727 10.5176 3 -3 0 3 137.645 8.62327 1 0 3 3 149.93 9.81098 7 3 -3 0 134.043 9.74255 7 0 -3 3 135.189 8.31529 4 -3 3 0 133.443 9.68841 7 0 3 -3 128.237 9.08915 6 0 3 -3 113.391 8.54452 2 0 -3 3 119.888 8.32517 1 0 3 3 126.646 10.4102 3 0 3 -3 124.714 8.35571 1 0 -3 -3 145.099 8.36899 2 0 3 3 128.382 8.61397 8 3 -2 -3 486.883 29.4337 1 2 -3 -3 482.843 29.8383 1 2 -3 -3 457.784 33.5035 7 2 -3 3 510.119 31.3732 6 3 -2 -3 500.099 30.8289 6 2 -3 3 490.278 30.6053 1 -3 3 2 467.634 30.2675 1 -3 3 -2 410.015 33.4229 4 -3 2 3 494.583 29.6172 8 2 -3 -3 468.6 29.4239 9 2 -3 -3 485.176 30.2268 10 -3 3 2 509.364 34.8451 7 3 -3 -2 502.345 30.8466 6 -2 3 3 494.534 29.7511 1 -3 2 3 490.992 29.9746 4 -2 3 3 534.242 28.816 2 -3 3 2 493.653 30.0343 8 -2 3 3 506.293 36.6349 3 -2 3 -3 453.656 31.9642 4 3 -3 -2 456.835 30.0975 1 3 -3 -2 468.566 30.2533 10 2 -3 -3 495.978 29.7768 4 -2 3 3 489.092 34.388 7 3 -2 -3 523.257 29.5278 4 -2 3 3 475.777 31.5653 6 -2 3 3 471.639 30.3905 8 -3 3 2 515.318 36.6827 3 3 -2 -3 501.08 34.0999 7 -2 3 3 463.412 30.1593 9 3 -3 -2 502.572 30.9298 4 -3 2 3 513.174 36.6567 3 3 -2 -3 505.172 37.3326 3 -3 2 3 519.93 29.2337 1 3 -2 -3 520.619 35.1944 5 0 -4 0 679.402 48.0031 3 0 0 4 612.794 39.83 8 0 4 0 668.152 46.0808 7 0 0 -4 665.852 39.8853 1 0 0 4 670.441 45.9835 7 0 4 0 690.252 39.0573 4 0 0 -4 611.398 42.4845 4 0 0 -4 687.291 47.6967 3 0 0 4 649.297 39.7568 10 0 -4 0 671.193 38.8356 8 0 0 -4 686.346 38.6688 8 0 -4 0 717.932 38.0736 2 0 0 4 594.489 47.3812 3 0 0 -4 567.238 45.6404 7 0 -4 0 714.51 47.4212 7 1 1 -4 151.345 10.32 8 -1 1 4 162.655 9.73425 1 1 -1 -4 141.717 9.44106 8 1 -4 1 164.101 9.44844 9 -1 4 -1 131.545 9.78954 4 -1 4 1 165.615 11.6694 3 1 -4 1 158.422 10.0095 4 1 -4 -1 138.8 10.552 7 -1 -1 4 130.341 11.1424 3 1 -4 1 145.589 11.4517 3 1 -1 -4 146.028 9.1693 10 1 -4 1 158.701 10.8684 7 1 -1 -4 129.827 10.5569 7 1 -1 -4 138.848 9.63697 1 1 -4 1 153.336 9.30897 2 -1 4 1 172.083 9.2918 2 -1 1 -4 144.359 9.20652 8 -1 4 -1 133.457 10.9409 5 1 -4 -1 153.189 9.51133 1 -1 4 -1 148.886 9.17375 8 -1 -1 -4 161.35 11.1331 1 1 -1 -4 142.57 8.99171 2 -1 1 4 162.021 9.27822 10 1 1 -4 144.107 12.1576 3 -1 -1 4 136.674 9.56155 1 1 -1 -4 146.049 9.52212 4 1 -4 -1 132.899 10.9306 3 -1 1 4 159.573 11.0194 7 -1 4 1 174.066 9.35245 10 -1 -1 4 139.204 9.31853 8 1 1 4 129.218 11.5035 3 -1 4 1 163.132 9.56541 1 -1 4 1 154.64 10.874 7 -1 4 -1 138.92 9.79799 6 1 -4 -1 146.922 9.28436 9 -1 1 -4 142.005 11.1354 3 1 1 -4 152.368 10.7027 7 1 -1 -4 144.674 11.4061 3 1 -1 4 155.716 9.84748 1 -1 4 1 162.695 9.29166 8 1 -4 1 154.618 9.33772 8 -1 4 1 165.12 9.8427 4 -1 4 -1 135.653 9.41224 10 -1 1 4 161.906 9.62449 4 -1 1 -4 127.292 10.2948 1 1 -1 -4 137.354 9.01025 9 -1 4 -1 135.707 9.61563 2 1 -4 -1 151.047 9.23462 2 -1 4 -1 144.208 9.21187 9 1 1 -4 156.591 9.33915 10 -1 -1 4 151.852 10.502 7 1 1 -4 170.661 9.43165 1 -1 1 4 173.665 9.10882 2 1 1 4 148.109 10.7523 7 -1 4 -1 140.998 11.2279 3 1 -1 4 146.777 11.0818 7 -1 4 -1 132.919 10.3412 7 1 -4 -1 135.411 9.48442 8 2 0 -4 14.2422 2.91268 3 0 2 4 12.9524 2.30341 1 0 -4 2 13.8046 1.84604 2 0 2 -4 13.1095 1.85586 6 2 -4 0 13.2641 1.31262 1 -2 0 4 13.8284 2.39609 8 0 -4 2 12.1619 1.78853 4 2 -4 0 15.3391 2.46275 3 0 -4 -2 13.318 2.28746 4 0 2 -4 11.2992 1.77532 3 2 0 -4 15.0363 1.93346 7 -2 4 0 16.2086 1.70284 10 0 2 -4 14.2536 1.54701 8 -2 0 4 15.0795 2.00224 7 0 2 4 14.51 2.07768 4 0 -2 -4 14.3282 2.03077 7 2 -4 0 14.0335 2.65343 6 2 0 -4 14.8395 2.56211 5 2 -4 0 13.8112 1.97293 10 0 -2 4 12.766 1.97217 1 -2 4 0 12.3155 1.88712 9 0 4 2 14.0853 2.0965 3 0 4 -2 14.2811 1.36705 1 0 4 -2 14.4279 1.40385 7 -2 4 0 12.9896 1.67471 8 0 -4 2 19.0936 2.53937 5 0 -4 -2 16.944 2.5297 3 -2 4 0 13.2512 1.96991 3 0 4 -2 12.817 1.78163 4 2 0 -4 14.6482 2.15634 1 -2 0 4 13.3983 2.62215 3 0 -2 4 14.6728 1.32767 7 2 -4 0 14.1585 2.1858 8 -2 4 0 11.7395 2.25223 4 -2 4 0 12.1063 1.7055 7 0 -2 4 14.0912 1.75934 3 -2 0 4 16.9965 1.9783 4 0 -2 -4 12.2986 2.06935 4 2 0 -4 14.1503 2.12309 4 0 -2 -4 12.133 2.38575 3 0 4 2 14.2126 2.0722 7 0 2 -4 14.7199 1.76166 1 0 4 2 15.0467 2.21705 4 0 2 -4 13.53 1.29571 7 0 -2 -4 13.3607 1.96364 8 0 -4 2 16.0608 1.70385 9 2 -4 0 16.7275 1.9337 7 -2 4 0 13.5885 1.40292 1 0 -2 -4 12.987 1.73386 2 0 4 2 14.377 1.84034 1 0 -2 4 12.8397 1.49155 8 0 -4 -2 13.6605 2.00726 8 2 0 -4 15.9311 2.42885 8 0 4 -2 10.8738 2.42719 5 -2 -2 4 66.8881 6.30377 3 -2 4 2 78.7497 6.26839 3 -2 4 -2 66.645 5.26507 7 -2 4 -2 67.1751 5.06377 9 -2 4 -2 64.3289 5.91248 6 2 -2 -4 68.9682 5.56926 4 -2 4 2 77.3049 5.78819 7 -2 4 -2 60.0831 5.48009 3 2 2 -4 76.1329 7.07128 5 2 -4 2 75.725 4.94963 10 2 -2 4 84.2214 5.53757 1 -2 2 4 77.3294 5.11798 2 -2 4 -2 62.5986 5.36847 4 2 -2 -4 70.552 5.13793 10 2 -4 2 68.7105 5.4438 7 2 -4 -2 66.4097 6.42894 3 -2 2 4 83.5434 4.77747 6 -2 4 2 78.5423 5.40614 8 2 -4 -2 70.7699 5.71584 4 2 -4 -2 70.3309 5.1392 9 2 -4 2 69.3238 6.10249 4 -2 2 4 76.6896 5.68694 4 -2 2 4 71.3156 5.0802 9 2 -4 -2 73.0921 4.91099 1 -2 4 2 75.6312 5.18037 10 -2 4 2 85.1064 5.326 2 2 -2 -4 69.7691 5.64245 7 2 -4 -2 71.1206 5.26475 8 -2 2 4 78.1857 5.57058 1 -2 -2 4 60.7508 5.40217 1 2 2 -4 81.1452 5.48705 1 2 -2 -4 70.6538 5.3901 8 -2 4 -2 57.8676 4.7287 8 -2 4 2 79.2691 6.04449 6 -2 4 2 86.6436 5.00326 1 -2 -2 4 76.7699 6.56268 5 -2 4 2 77.5325 5.81859 4 2 -2 -4 71.9259 6.52724 3 -3 4 1 421.668 24.4912 4 3 -4 1 408.787 28.376 7 -1 4 -3 396.102 23.8098 2 -1 3 4 446.837 23.2162 2 1 -4 -3 423.818 23.5681 2 -3 4 1 405.295 25.1613 6 1 -3 4 365.715 25.0986 1 -1 -4 3 378.109 23.8664 2 -1 4 -3 367.302 24.7342 1 -1 4 -3 359.516 26.169 6 1 3 -4 337.58 27.2404 7 1 -3 4 389.011 25.4187 6 -3 4 1 403.041 24.392 9 -1 3 4 417.825 24.3632 1 -3 4 1 401.421 29.8772 3 1 -4 -3 406.898 23.2935 9 3 -1 -4 433.15 30.4269 3 -1 3 4 410.127 29.5587 3 4 -3 -1 417.651 25.9019 4 3 -1 -4 431.643 28.6072 5 -3 -1 4 434.462 28.9652 5 3 -1 -4 434.039 27.6388 7 -3 4 1 402.91 24.2854 8 3 -1 -4 436.376 25.2057 4 3 -4 1 429.111 24.966 6 3 -4 1 364.008 26.5453 4 -1 4 -3 395.837 23.6982 9 -3 -1 4 404.821 29.6508 3 -3 4 1 417.578 28.1511 7 -1 3 4 394.1 24.1437 8 1 -4 -3 389.579 24.9693 4 1 3 -4 386.368 24.8825 1 -1 -4 3 448.948 29.481 5 1 -4 -3 435.225 23.3076 1 1 3 -4 407.971 29.4608 5 -1 3 4 398.662 24.3133 4 -3 4 1 362.525 24.5119 1 -1 4 -3 382.232 24.7868 4 1 -3 -4 368.582 24.7258 9 -1 -3 4 402.816 23.0394 1 1 -3 -4 410.727 27.6645 7 1 -3 -4 388.6 23.9518 2 3 -4 -1 399.485 23.7627 10 -1 -3 4 332.635 29.3821 3 -1 -3 4 351.275 25.4541 8 -4 3 1 379.879 30.273 3 -3 4 -1 390.856 24.7185 8 1 4 -3 398.971 24.3365 1 -1 4 3 384.751 24.2918 8 3 -4 -1 410.828 23.4983 1 -1 3 -4 358.835 25.1729 4 -3 1 4 410.305 23.7193 1 1 -4 3 379.949 24.8657 4 -3 1 4 410.68 24.3408 4 1 -3 -4 414.529 23.8099 8 -3 4 -1 366.834 27.1693 7 1 -3 -4 387.726 25.445 4 -1 3 -4 376.407 25.5124 6 -3 4 -1 396.734 24.0279 9 -1 4 3 395.67 25.0862 1 -3 1 4 434.762 27.9322 7 -3 4 -1 406.527 24.0588 4 -4 3 1 432.834 28.5092 7 1 4 -3 432.652 28.8857 5 -1 4 3 411.284 29.2148 3 -4 3 1 424.733 25.7312 4 -1 3 -4 376.35 23.7436 9 -3 4 -1 379.197 29.6918 3 1 -3 -4 411.424 29.7041 3 -1 3 -4 355.345 28.7894 3 1 -4 3 360.288 25.0987 1 -1 4 3 407.707 24.5773 2 1 -4 3 361.304 24.6375 9 -1 -3 4 384.582 23.9235 2 1 -3 -4 392.669 23.9919 1 -1 3 -4 357.75 24.2494 8 -1 4 3 401.589 24.2737 10 -1 3 -4 377.798 24.6488 1 3 -4 -1 424.881 27.3379 7 3 -4 -1 413.929 30.0345 3 -1 4 3 412.449 27.7859 7 3 -4 -1 428.335 23.7505 6 3 1 -4 423.105 23.0734 1 -3 4 3 1414.91 101.494 3 3 -4 -3 1391.58 81.3087 1 -4 3 3 1378 81.0182 8 3 -3 -4 1408.47 79.7382 10 3 -4 -3 1290.41 86.4689 4 -3 3 4 1391.92 81.5106 1 3 -3 -4 1249.55 84.547 4 3 -3 -4 1303.07 81.9245 1 3 -4 -3 1247.36 86.44 6 -3 4 3 1404.67 82.5817 8 3 -3 -4 1378.41 94.65 7 -3 4 -3 1254.94 86.045 4 4 -3 -3 1362.29 83.9618 4 -3 4 3 1321.62 82.6031 1 3 -3 -4 1445.07 98.7078 5 -3 3 4 1380.01 78.3096 2 -3 4 3 1410.93 79.0513 2 -3 4 3 1411.12 80.5478 9 3 -3 4 1340.2 88.0747 6 3 -3 -4 1320.39 85.6096 6 4 -3 -3 1361.69 79.67 1 3 -4 -3 1396.48 80.8684 8 -3 3 4 1348.04 82.7067 8 3 -4 -3 1371.54 81.6083 10 -4 3 3 1295.54 83.8674 1 -4 3 3 1440.04 94.5681 7 -4 3 3 1382.82 99.8018 3 -3 3 4 1422.16 79.4729 9 4 -3 -3 1404.28 87.4336 6 -3 4 3 1437.63 83.0291 6 -3 3 4 1355.89 100.473 3 3 -4 3 1362.75 88.5289 6 -3 4 3 1297.19 95.3357 7 -3 3 4 1299.85 85.5221 4 4 -3 -3 1356.44 94.2522 7 3 -4 -3 1377.32 97.5491 5 3 -4 -3 1435.11 100.508 3 4 -4 0 9598.78 641.028 7 0 -4 -4 9209.93 556.237 1 0 4 4 9346.05 548.553 1 4 -4 0 9999.99 564.221 6 0 4 4 9106.32 639.132 7 -4 4 0 9230.06 638.967 7 -4 4 0 9629.39 683.038 3 0 -4 4 8568.7 544.848 2 0 -4 4 8744.35 559.844 4 0 -4 4 8686.67 545.321 9 0 4 4 9352.94 672.134 3 -4 4 0 9840.45 541.204 4 0 4 -4 8883.51 571.718 6 0 4 -4 9318.97 552.834 1 0 4 -4 9031.28 657.082 5 0 -4 4 8718.38 556.235 1 0 -4 -4 9133.55 636.36 7 0 4 4 9228.06 558.238 4 0 -4 -4 9814.08 540.839 2 0 -4 -4 9672.83 552.751 4 2 -4 -4 453.82 32.1673 7 2 -4 -4 473.172 28.2056 1 2 4 -4 453.138 33.6714 5 -4 2 4 488.273 27.2887 8 4 -2 -4 475.401 33.4323 5 -2 4 4 462.14 28.3488 8 -2 4 -4 400.68 30.0972 6 -2 4 4 472.456 34.95 3 -4 4 2 469.937 28.2808 8 4 -2 -4 480.793 27.5062 1 -4 2 4 484.205 28.5829 4 2 -4 4 418.239 30.8628 6 2 -4 4 412.905 28.2855 10 -4 4 2 451.434 28.8039 1 4 -4 -2 449.08 29.2642 4 -2 4 4 460.028 28.645 4 4 -4 -2 473.982 27.4864 1 -2 4 4 457.17 31.9817 7 2 -4 4 446.811 28.8242 1 4 -2 -4 434.285 32.5407 4 -4 4 -2 453.111 29.9782 4 -2 4 4 449.807 29.2748 6 -4 2 4 483.059 27.2749 1 -4 4 2 492.617 34.7872 3 4 -2 -4 482.869 35.3977 3 4 -2 -4 488.875 32.6159 7 4 -4 -2 465.534 30.3414 6 -4 4 2 464.081 32.3581 7 -2 4 4 506.091 27.0103 2 -2 4 4 472.859 28.5671 1 2 -4 -4 484.344 28.2727 4 -2 4 -4 405.974 30.6276 4 -4 4 2 485.081 28.9292 4 -4 2 4 481.336 34.3753 3 4 -4 -2 464.877 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30.9476 3.35544 8 -3 2 5 35.8913 3.67657 2 2 -5 3 37.1648 4.69717 4 2 -3 -5 42.3742 3.94689 10 -3 2 5 38.8366 3.58277 9 -3 2 5 37.4484 4.19494 7 -3 5 -2 38.4271 3.67229 7 -2 -3 5 43.0342 4.28399 1 3 -5 -2 42.471 3.61191 1 2 -3 -5 45.8354 4.40951 7 -2 5 3 46.9403 4.23667 2 2 -3 -5 39.9923 3.57403 9 -3 2 5 34.2046 4.45145 4 -3 5 -2 41.2635 4.12379 9 3 -5 -2 38.1841 4.14975 7 2 -3 -5 33.9708 4.58156 4 -3 5 -2 37.0421 4.55154 4 3 -5 -2 43.0451 4.51644 8 -2 3 -5 32.7779 4.87229 4 -2 -3 5 41.0614 4.96361 3 3 -5 -2 41.0936 5.06944 4 2 -5 3 36.7326 3.12089 7 3 -5 -2 44.181 5.59016 3 -3 5 -2 40.6844 5.1278 6 3 -5 -2 40.1511 4.19028 9 2 -3 -5 46.2499 4.47951 8 -3 5 -2 39.5464 3.89947 3 -2 3 -5 46.7544 4.4563 3 -2 -3 5 41.9092 4.33038 8 3 2 -5 42.8283 4.33016 1 2 -5 3 34.4188 5.09298 6 -2 5 3 33.7324 4.0681 7 2 -5 3 37.5361 3.13208 10 -3 2 5 37.9717 4.50993 1 2 -3 -5 42.3615 5.42609 3 -2 5 3 32.8103 4.34602 3 -2 5 3 35.4535 3.77739 8 -2 5 3 28.2408 3.91639 1 2 -3 -5 42.4769 4.18185 1 -1 -4 -5 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88.2564 7.40406 9 4 -4 -6 85.8013 7.83502 5 -4 4 6 91.2118 7.32751 1 6 -4 -4 73.8372 10.751 3 4 -4 -6 98.1394 8.32386 4 4 -6 -4 87.1489 9.94489 3 4 -6 -4 84.5512 7.14558 5 -6 4 4 86.5052 8.2432 8 4 -6 -4 87.5779 8.87178 4 6 -4 -4 79.5869 7.77579 6 -4 6 -4 83.8531 8.04281 4 -4 6 4 104.804 7.88748 6 -4 6 4 81.7994 7.62979 2 -4 6 -4 70.3987 7.40159 3 -4 4 6 93.9591 6.82212 9 4 -4 -6 81.5887 7.74505 7 -4 4 6 82.2362 7.17784 2 -1 6 -5 204.058 13.8791 2 -1 5 6 182.178 15.1221 8 -1 -6 5 210.427 13.2209 9 6 -5 -1 222.564 15.9984 7 5 -6 1 207.236 14.3157 10 5 -1 -6 227.299 16.0989 7 5 -6 1 210.998 16.5349 4 -1 -6 5 215.416 13.3437 4 -1 6 -5 224.405 15.0279 6 -1 5 6 203.734 14.6271 1 1 -6 -5 212.615 17.1019 3 5 -1 -6 222.311 17.0339 5 5 -6 1 218.119 15.7422 7 1 5 -6 192.015 17.0481 5 -1 6 -5 222.904 17.1487 5 5 -1 -6 236.608 18.8932 3 1 5 -6 218.426 13.7033 1 1 5 -6 191.888 14.884 7 1 5 -6 231.495 14.2854 6 -1 -6 5 212.589 13.4186 2 -5 6 1 201.981 16.8997 3 1 -6 -5 222.098 15.187 4 1 -5 6 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109.16 8.5495 7 -2 3 7 111.064 7.01978 6 2 -7 -3 111.006 9.80662 3 3 -7 -2 116.16 7.19368 1 2 -7 3 102.989 7.85669 7 -2 7 3 96.1139 8.57987 2 -2 3 -7 113.265 8.9474 3 -3 7 -2 102.391 9.53559 6 -3 2 7 87.2055 8.69632 1 3 -7 -2 103.374 10.1192 3 -2 7 3 102.244 7.92983 8 -3 2 7 105.831 8.51036 8 -3 7 -2 93.8668 8.78954 5 -2 -3 7 88.0073 9.11796 3 2 -3 -7 108.384 7.23139 9 -3 7 -2 101.565 8.22203 7 -2 7 3 102.256 9.39819 6 3 2 -7 101.113 10.4526 3 2 -3 -7 109.681 10.3992 3 -3 2 7 107.377 7.1257 9 -3 2 7 100.174 8.17839 4 -3 7 -2 102.367 8.23216 3 -2 3 -7 101.619 7.25397 8 -3 7 -2 115.773 7.76629 9 2 -3 -7 101.157 8.7398 7 -3 7 -2 95.413 8.25909 2 -2 3 -7 90.4613 9.19933 1 -3 7 -2 107.608 6.74665 8 2 -3 -7 110.32 8.34412 4 3 2 -7 111.455 8.21545 7 -2 -3 7 102.998 7.76261 8 2 -7 3 93.9366 8.66876 4 -2 -3 7 96.7451 8.4224 1 3 -7 -2 107.64 8.53674 7 3 -2 7 109.297 8.65256 1 -3 2 7 111.082 7.50984 2 -2 7 3 99.5429 7.55859 1 -1 -4 -7 139.739 13.7383 3 4 -7 1 92.1483 7.85028 10 1 4 -7 87.2455 7.82723 1 1 4 -7 89.9621 6.44546 10 -4 -1 7 110.036 8.42813 8 1 -7 -4 116.759 9.9477 3 4 -1 -7 112.457 8.73848 7 4 -1 -7 109.518 9.82797 5 4 -7 1 87.3558 9.9052 4 4 -1 -7 100.507 11.2631 3 1 -7 -4 102.635 8.87143 7 4 -1 -7 96.8979 7.38917 6 -1 7 -4 105.021 9.80504 5 1 4 -7 93.4045 7.37166 7 -1 7 -4 97.3787 7.50058 7 -1 7 -4 99.4722 6.77095 1 4 -7 1 92.721 9.84228 3 -1 -7 4 108.078 7.84419 4 -1 -7 4 101.282 7.95597 2 1 4 -7 82.2903 9.16787 3 -4 7 1 99.2734 7.74681 8 -4 7 1 95.5807 9.18926 6 -1 7 -4 99.2159 8.0501 2 4 -1 -7 119.532 7.46581 10 -4 7 1 100.013 9.18425 3 1 4 -7 84.1114 8.19903 6 -1 7 -4 117.229 9.40777 6 1 4 -7 82.5991 9.67526 5 -4 -1 7 119.237 7.58961 4 -4 -1 7 108.791 8.66119 1 -4 7 1 101.022 7.75612 9 1 -7 -4 106.872 9.37245 4 4 -1 -7 115.861 9.21659 4 1 -4 7 99.7733 7.88331 1 -1 7 -4 101.549 6.80632 10 4 -7 1 97.927 8.14858 7 4 -7 1 90.4719 6.73537 1 -1 7 -4 105.675 7.69741 4 -1 4 7 92.6474 8.76824 1 4 -7 -1 110.306 10.7786 3 1 -4 -7 116.387 8.79675 4 -1 4 -7 106.704 6.90221 2 -4 7 -1 116.219 7.96312 2 4 -7 -1 111.734 7.09117 1 4 -7 -1 109.422 8.16131 10 1 4 7 100.561 8.77013 1 4 -7 -1 106.651 9.64983 4 -4 7 -1 120.606 7.84764 9 -1 7 4 104.827 7.81435 1 -1 4 -7 104.078 7.74902 1 4 -7 -1 111.287 8.5897 7 1 -4 -7 114.378 10.4018 3 1 7 -4 97.0825 7.19916 1 -4 7 -1 102.467 8.30897 5 1 -7 4 101.848 7.66248 9 4 1 -7 108.936 10.9464 3 -1 4 -7 101.275 8.61501 3 1 -7 4 100.806 8.16588 4 4 1 -7 108.954 10.5826 5 1 -4 -7 106.855 7.48992 9 -4 1 7 98.2591 8.34434 1 -4 7 -1 104.072 8.87454 3 -1 -4 7 109.41 7.17703 8 -1 4 -7 96.1449 7.19443 8 -1 -4 7 107.234 8.48888 3 -1 -4 7 106.173 7.83282 1 1 -4 -7 99.304 7.55994 2 -4 1 7 93.4031 6.92511 9 1 -4 -7 102.975 8.69685 7 -4 7 -1 105.615 9.34817 6 -4 7 -1 103.799 7.4468 8 -4 1 7 91.6248 8.20024 4 -1 7 4 97.7677 7.77207 8 -4 7 -1 108.388 8.32728 7 -4 1 7 100.493 8.38598 8 4 1 -7 106.151 8.1403 7 3 4 -7 54.2575 4.67931 7 -4 -3 7 42.8463 6.22057 8 -3 4 7 48.2218 6.19549 1 4 -3 -7 50.0893 6.4857 4 -3 7 -4 40.8091 5.29109 9 -3 7 -4 45.0309 5.46029 2 -4 7 3 50.8441 6.62888 6 -4 7 3 53.7676 5.30991 8 -4 7 3 50.7434 5.07885 1 -3 7 -4 42.5067 6.75306 6 4 -3 -7 52.0174 5.71116 7 3 -7 -4 48.1366 5.81067 7 4 -3 -7 50.8194 5.41555 10 4 -3 -7 52.8375 6.23688 5 3 -7 -4 50.6047 4.89453 1 -3 4 7 54.2636 5.57911 2 3 -7 -4 42.5313 7.00053 4 -3 4 7 56.0211 4.57489 6 4 -7 3 44.8362 7.55689 4 4 -3 -7 50.5384 8.61266 3 -3 7 -4 51.6117 5.62217 4 4 -7 3 51.3371 5.00911 10 4 -7 3 54.6175 4.84901 7 -3 7 -4 47.191 5.99588 5 -4 7 3 49.535 6.14085 2 3 4 -7 56.9136 7.43855 5 3 -7 -4 48.7085 7.18783 3 3 -4 7 52.9448 5.55892 1 3 -4 -7 40.5677 5.27138 10 -3 4 -7 55.4175 6.77291 3 -4 7 -3 34.7944 5.519 2 4 -7 -3 49.5936 4.89761 1 4 -7 -3 47.3735 7.59255 4 -3 7 4 48.4008 6.1251 2 3 -4 -7 41.87 5.51528 7 -4 7 -3 37.8453 4.06931 8 -4 7 -3 37.3417 5.49258 9 4 -7 -3 47.8709 5.9151 7 -4 3 7 51.1157 5.21183 2 3 -4 -7 37.7084 7.29527 3 3 -4 -7 44.2345 6.38179 4 3 -7 4 45.1886 4.14559 7 -3 -4 7 42.5741 5.5411 1 -4 3 7 53.9022 4.72023 9 -3 7 4 50.1295 5.67943 8 -3 -4 7 41.4911 6.27025 3 3 -7 4 46.0881 6.6489 4 -3 4 -7 39.1018 5.57474 8 4 -7 -3 35.8389 7.64045 3 -3 -4 7 56.1169 5.54256 8 -4 3 7 47.1084 5.93608 1 -3 7 4 52.6392 6.55583 6 -3 7 4 55.0842 5.22383 1 -4 7 -3 35.5095 6.15817 6 4 -7 -3 48.6062 5.6509 10 -4 7 -3 34.1598 4.59611 3 5 -7 0 178.01 15.335 4 0 -5 7 184.248 11.7903 8 -5 0 7 208.597 13.0329 8 0 7 -5 205.836 13.7625 6 0 -5 -7 218.486 17.1296 3 0 7 -5 190.417 15.9114 5 0 -7 5 207.909 11.9074 9 0 -7 -5 188.382 14.3369 4 5 0 -7 187.884 14.2571 7 0 5 -7 189.268 12.5642 1 -5 7 0 196.898 15.414 3 0 -5 -7 183.048 15.1398 7 -5 7 0 188.771 12.6358 8 0 7 -5 170.796 12.1067 10 -5 0 7 190.23 12.8836 4 0 7 -5 190.803 12.0798 1 0 -5 -7 191.578 13.9176 4 5 -7 0 208.806 12.8457 10 5 -7 0 178.407 16.9075 3 0 -5 7 183.557 12.7679 1 0 -7 -5 203.506 16.2865 3 0 7 5 191.167 13.0977 1 5 -7 0 179.34 14.1954 7 0 5 -7 175.561 13.6949 6 -5 7 0 193.022 13.0595 9 0 -7 5 177.039 12.2305 2 0 5 7 161.353 14.5003 1 5 -7 0 192.1 12.0507 1 0 5 -7 182.984 16.3377 5 5 0 -7 205.595 17.886 3 0 7 -5 164.785 13.1371 7 0 -7 5 197.76 12.4242 4 0 -5 7 185.171 14.4103 3 5 0 -7 223.928 16.6319 5 -2 7 -5 32.5854 5.93067 5 -2 5 7 50.3141 5.23283 6 -5 7 2 42.381 5.50268 2 5 -7 2 31.8083 4.92967 10 5 -2 -7 43.0397 7.16577 5 5 -7 2 40.6754 4.89117 7 2 5 -7 47.8294 3.88508 7 5 -2 -7 46.2762 6.62397 4 5 -2 -7 42.9545 5.16309 10 -2 5 7 46.6815 5.87829 1 -2 5 7 42.9297 5.57061 8 5 -2 -7 56.0362 5.71659 7 -5 7 2 48.4459 5.4449 8 -2 7 -5 42.4406 4.75536 4 2 5 -7 37.4945 7.79338 5 -2 7 -5 35.8821 7.05129 6 5 -2 -7 40.6676 4.26072 6 5 -7 2 35.224 7.57387 4 2 -5 7 39.1478 4.92912 1 -2 -7 5 40.3778 5.18953 2 -2 7 -5 47.9523 5.22722 2 2 -7 -5 40.7873 6.92334 3 2 -7 -5 40.3555 6.33518 4 5 -2 -7 40.4216 7.88693 3 5 -7 -2 47.3894 4.46842 1 -2 5 -7 44.5147 4.06875 9 -2 -5 7 41.3565 5.48327 1 -5 7 -2 34.2015 5.12412 3 -2 5 -7 39.8257 4.22495 2 2 -7 5 35.2661 3.44262 1 2 -5 -7 43.6274 7.25373 3 -5 2 7 50.3441 4.60844 9 -2 7 5 34.4436 5.26333 8 -2 5 -7 38.7429 3.51628 8 -2 5 -7 39.5487 3.87187 4 -2 -5 7 44.4876 3.50341 4 -5 7 -2 39.3414 6.05194 9 -2 -5 7 34.7443 3.75045 2 -2 -5 7 38.6344 4.60855 8 2 -5 -7 43.4789 5.70099 7 -2 5 -7 39.7686 4.22228 3 2 -7 5 42.784 5.44878 4 5 -7 -2 53.8184 8.44255 3 5 2 -7 38.4294 7.63709 5 -2 -5 7 28.3078 5.06344 3 -5 7 -2 41.9867 4.59731 8 -2 5 -7 32.3512 5.31415 1 -2 7 5 50.2101 6.48021 6 2 -5 -7 45.1327 6.50125 4 5 -7 -2 37.9101 5.69136 10 -2 7 5 48.4958 5.3511 1 5 -7 -2 43.7124 5.61307 7 -5 2 7 40.1366 6.21138 1 -2 7 5 58.969 6.34154 2 -7 4 5 75.0343 9.13911 8 -5 7 4 84.2718 8.20115 6 7 -5 -4 64.1383 10.0844 4 -4 7 -5 88.8258 7.87888 2 -4 5 7 89.5164 7.95602 2 4 -7 -5 80.8314 7.11533 5 4 -7 -5 85.7936 10.3482 3 4 -7 -5 89.4874 9.43604 4 5 -7 4 87.6286 7.22189 7 -4 7 -5 89.303 7.56688 9 -4 7 -5 88.3013 8.11457 4 -5 7 4 82.0599 8.161 2 4 -7 -5 82.6216 7.96619 10 -4 7 -5 72.074 6.70707 3 -5 7 4 79.8148 7.7993 9 -5 7 4 85.9513 7.75564 1 5 -4 -7 81.4766 11.4246 3 5 -4 -7 92.8817 9.58946 4 5 -4 -7 86.9888 8.85713 5 5 -7 4 89.0998 6.50298 10 -4 5 7 80.2303 8.23438 1 5 -4 -7 99.2875 8.53913 7 5 -4 -7 78.185 7.41463 6 7 -5 -4 81.5244 11.9072 3 5 -4 -7 84.8606 7.88963 10 -4 5 7 90.6731 7.8547 8 -4 7 -5 70.0424 5.71097 8 -4 5 7 79.1609 7.12013 9 -5 7 4 89.4398 7.93264 8 4 -5 7 82.5851 7.10505 1 -5 4 7 87.2699 7.2191 9 -5 4 7 84.7157 7.72624 2 -4 7 5 85.7252 8.51065 6 -5 4 7 84.1833 8.10803 1 4 -7 5 85.5009 6.40201 10 4 -7 5 79.1228 6.57685 7 5 -7 -4 91.0739 11.425 3 -7 5 4 85.2117 8.18709 9 5 -7 -4 74.6007 9.87199 4 4 -5 -7 98.3164 9.10543 4 -4 7 5 91.5831 7.32496 9 -4 7 5 86.3362 7.83853 8 -5 7 -4 93.5127 8.31858 9 7 -4 -5 84.707 8.44106 7 4 -7 5 77.4181 6.07854 1 -4 5 -7 80.9898 12.0003 4 4 -5 -7 93.6453 8.40508 7 -5 4 7 91.0479 8.65929 8 5 -7 -4 85.1613 8.32569 7 -5 7 -4 86.5114 8.25809 3 -5 7 -4 74.979 7.22727 8 4 -5 -7 91.0023 7.59527 10 -4 7 5 83.8443 7.91358 1 4 -5 -7 79.742 10.9025 3 -7 5 4 89.2125 8.82764 8 -4 7 5 76.8836 8.54559 2 1 6 -7 150.277 14.2356 5 -1 7 -6 137.431 10.6687 4 1 -7 -6 173.3 11.9221 4 1 -7 -6 154.617 12.3646 7 6 -7 1 149.281 12.0465 7 6 -1 -7 178.544 15.711 3 1 6 -7 170.322 11.9491 6 -1 -7 6 146.501 10.2649 4 1 -7 -6 165.702 13.7051 3 1 -6 7 148.493 10.5035 1 -1 7 -6 152.732 12.2818 6 -6 7 1 155.835 11.1986 8 6 -7 1 165.523 10.9636 10 -1 -7 6 132.45 9.9274 8 1 6 -7 149.257 10.6388 1 -1 -7 6 134.85 11.7461 3 -1 6 7 148.732 10.9643 8 -1 -7 6 152.404 9.88776 9 -6 7 1 135.202 11.7811 9 -1 -7 6 146.581 10.0455 2 -1 7 -6 158.434 9.76539 1 6 -7 1 143.103 13.6522 4 -1 7 -6 133.039 10.6795 2 6 -1 -7 157.262 12.1852 7 -1 6 7 150.618 11.6503 1 -1 7 -6 143.927 13.3375 5 6 -7 -1 153.096 10.1304 1 1 -6 -7 159.8 12.2557 7 1 7 -6 151.346 10.2275 1 1 -7 6 130.092 10.4312 1 -6 7 -1 141.361 12.9238 3 -6 7 -1 143.345 10.8514 8 -1 -6 7 147.794 10.6957 1 -1 -6 7 150.42 11.6891 3 -1 7 6 163.571 11.2064 1 1 -6 -7 163.705 12.3735 4 -6 7 -1 154.287 11.8245 9 -1 -6 7 152.177 9.60205 8 -1 7 6 163.232 10.7878 8 1 -7 6 143.094 10.9117 4 -1 -6 7 142.768 9.8195 4 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6.38236 9 5 -6 7 48.294 5.57682 1 6 -5 -7 54.0427 7.17996 5 7 -5 -6 55.6955 6.61415 10 5 -6 -7 59.6749 6.47773 5 5 -6 -7 44.6946 8.90174 4 -5 6 -7 42.989 10.3278 9 5 -6 -7 44.0434 7.06106 10 -6 5 7 44.8201 6.29288 9 5 -6 -7 39.3147 7.14268 7 -7 6 5 46.3395 7.5983 8 5 -7 6 43.9174 4.80827 7 -5 7 6 35.2394 6.89039 8 -7 6 5 44.9678 6.9428 9 5 -7 6 45.2164 4.62023 10 -6 5 7 42.2646 6.57824 2 -5 7 6 47.8222 6.29534 1 -6 5 7 57.1679 7.96658 8 -5 7 6 49.8316 6.50673 9 6 -7 -5 41.3706 7.06605 7 6 -7 -5 57.9966 11.1704 3 6 -7 -5 50.9566 9.16964 4 7 -5 -6 49.677 7.18701 7 -5 6 -7 50.5267 13.2495 4 7 -5 -6 48.2053 9.09634 4 -6 7 -5 48.3542 11.1984 9 5 -7 6 50.4373 4.86053 1 -5 7 6 49.5472 7.09007 2 -6 5 7 47.5818 7.33084 1 0 -7 7 -1.9337 3.2615 9 7 -7 0 -1.5406 4.22257 7 0 -7 7 -2.0527 2.84963 1 0 -7 7 1.47692 3.20454 4 0 -7 -7 1.6825 4.77923 7 0 7 -7 -1.9152 5.89838 6 0 7 -7 5.56242 3.26651 1 7 -7 0 -5.2577 4.68376 10 0 7 7 0.20395 4.96321 1 0 -7 -7 2.40128 6.28522 4 -7 7 0 5.21515 5.64245 8 7 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6.25394 7 7 -7 -4 40.6439 10.6297 3 7 -4 -7 39.458 6.4788 7 7 -4 -7 44.6821 6.41645 10 7 -4 -7 19.6276 9.74431 3 -4 7 7 16.8132 6.55341 2 -7 7 4 26.1248 6.99333 8 7 -7 -4 40.4517 9.51609 4 -4 7 7 28.0924 5.96085 6 6 -7 -7 32.2412 9.06225 4 7 -6 -7 30.728 10.1939 4 -7 6 7 40.329 8.58567 8 -6 7 7 26.3372 6.44906 9 7 -7 -6 37.9147 11.4872 3 -6 7 7 38.4157 7.55763 2 -7 7 6 35.0123 7.79002 2 -7 7 6 43.643 7.00867 9 6 -7 -7 11.572 11.5959 3 7 -6 -7 22.2668 7.16507 10 7 -6 -7 19.1429 11.2793 3 -7 7 6 39.7936 7.33719 1 6 -7 -7 39.5327 6.99158 10 -6 7 -7 29.0778 13.199 9 7 -7 -6 25.8511 9.95141 4 -7 6 7 43.1952 7.78465 1 6 -7 -7 31.6806 7.11034 7 -7 7 6 37.2549 8.32197 8 7 -6 -7 34.9622 7.22685 7 -7 6 7 30.8964 7.44081 2 -6 7 7 33.4344 7.95579 8 -6 7 7 33.5045 7.41528 1 -7 6 7 40.8273 6.8234 9 7 -7 -6 32.0034 7.47446 10 0 8 0 2391.26 144.317 7 0 -8 0 2133.59 149.043 3 0 0 -8 2031.06 129.233 4 0 0 8 2025.84 128.5 6 0 0 8 2115.5 121.587 10 0 0 8 2091.77 142.068 7 0 0 -8 1908.34 129.631 2 0 0 8 2011.61 120.354 8 0 0 -8 2221.96 143.609 7 0 0 -8 1933.58 128.248 9 0 0 8 2230.51 120.922 1 0 0 -8 2192.42 151.922 3 0 -8 0 2056.23 121.306 8 0 -8 0 2182.1 120.767 4 1 -8 -1 110.682 9.87587 3 -1 8 -1 102.818 7.79115 1 -1 8 1 127.071 8.30986 1 -1 1 -8 107.862 8.7548 8 1 1 -8 112.878 9.16184 8 1 -1 -8 121.089 8.57933 4 -1 1 -8 111.256 10.3074 3 -1 8 1 143.862 10.6808 3 1 1 -8 128.17 8.23856 4 -1 -1 8 106.56 10.1815 3 -1 1 8 128.603 8.31057 10 1 -1 8 117.58 9.3265 7 -1 1 8 128.814 8.6434 4 -1 -1 8 124.455 9.257 1 -1 8 -1 134.644 10.5888 6 -1 1 8 130.55 8.90469 8 -1 1 -8 105.738 8.28391 4 1 1 -8 122.008 9.45493 7 -1 8 -1 109.236 8.91089 7 -1 -1 8 94.575 8.90359 7 1 -8 1 138.553 9.78008 4 1 -8 1 137.821 10.7202 5 -1 -1 8 103.382 8.87594 8 1 -1 -8 115.126 7.54048 9 1 -8 -1 111.825 10.2759 4 1 1 8 94.1114 10.1403 1 1 -8 1 118.064 10.0166 3 -1 -1 -8 130.404 11.639 3 1 -1 -8 113.833 9.39883 7 1 -1 8 125.964 10.6123 3 1 -1 8 117.625 8.18705 10 1 -8 -1 104.669 8.23559 8 -1 -1 -8 143.557 9.32964 4 1 -1 8 126.209 8.816 6 1 -8 1 124.697 8.31523 8 1 -8 1 125.019 10.2336 7 1 1 -8 133.79 11.1829 3 1 -1 8 132.109 9.5955 1 1 -8 -1 120.469 9.74861 7 1 -1 -8 125.426 10.9004 3 -1 -8 1 115.484 9.40649 4 -1 8 -1 113.937 8.36436 10 2 0 -8 86.5632 8.68453 3 0 2 -8 78.3691 6.52287 8 0 -2 -8 74.2192 7.21917 7 -2 0 8 73.3274 7.67468 1 2 0 -8 92.878 6.50038 4 0 -8 2 72.5077 5.40038 8 2 -8 0 77.829 6.11606 8 2 0 8 81.9713 7.65726 1 0 -2 -8 63.5361 5.7538 2 -2 8 0 70.1407 5.47593 1 2 -8 0 77.1723 6.67949 7 0 -8 2 77.5277 7.38103 4 0 -8 2 77.4072 8.40834 5 2 -8 0 70.7183 6.7377 5 0 8 -2 83.9961 6.50721 7 2 0 8 74.5291 6.6699 7 0 -2 8 76.0683 6.23118 7 0 2 -8 70.9392 7.97824 3 -2 8 0 83.6523 7.19484 3 0 -2 -8 71.5646 8.46493 3 0 -2 8 69.8322 7.41241 3 -2 0 8 94.0722 6.68109 8 2 0 -8 73.6029 6.6869 7 0 -2 8 76.3976 7.21403 1 0 2 -8 77.3814 6.64408 7 -2 0 8 81.7313 5.77015 4 0 -2 -8 69.3718 6.97293 4 2 -8 0 81.0457 7.60033 3 -2 8 0 63.4788 7.06257 2 0 2 8 73.7484 6.73208 8 0 -8 -2 78.0132 7.81468 3 0 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7.88425 4 1 -3 8 121.091 10.355 3 1 3 -8 108.39 9.23688 6 1 3 -8 129.743 9.42588 7 -1 -3 -8 141.91 13.6495 3 1 -3 8 117.766 9.62082 6 3 -8 1 126.18 10.8676 4 -1 8 -3 132.564 8.57735 10 -1 8 -3 134.061 11.3711 6 -3 8 1 130.905 8.85997 8 -1 -3 -8 122.676 11.2328 4 -3 -1 8 119.303 9.97154 7 -3 8 1 138.582 10.9754 6 -1 3 8 122.43 9.66304 4 1 -3 8 115.415 9.81293 1 3 -1 -8 119.91 9.98022 7 -3 8 1 133.728 10.8064 3 1 3 -8 127.394 11.6919 3 1 -8 -3 112.666 11.136 3 3 -8 1 125.633 10.0071 7 -1 8 -3 112.261 9.58165 2 -1 3 8 118.15 9.59263 8 -1 8 -3 117.611 9.73431 4 -3 -1 8 131.423 8.78917 4 -1 -8 3 127.787 10.0181 4 3 -1 -8 126.972 9.0915 10 -3 8 1 127.926 8.22491 1 3 -8 1 134.82 11.599 3 3 -1 -8 153.934 13.0859 3 1 -3 8 113.766 9.24832 7 -3 -1 8 119.094 7.9573 9 3 -1 -8 137.403 10.283 4 1 -8 -3 118.741 10.4984 7 -3 -1 8 116.001 8.11999 2 -3 -1 8 127.787 9.74395 1 -1 3 8 117.1 10.5532 1 -1 8 -3 121.859 9.33974 7 -3 -1 8 127.674 9.67475 8 3 -8 -1 127.44 11.465 3 1 -3 -8 114.735 8.688 2 3 1 -8 135.185 11.7772 5 3 1 -8 137.294 9.90257 7 -3 8 -1 121.715 9.57058 9 3 -8 -1 118.837 9.53442 8 -1 3 -8 134.747 10.9663 3 -3 1 8 131.07 8.1931 9 3 -8 -1 142.32 10.4746 7 -3 8 -1 137.951 9.84964 7 -3 8 -1 132.035 11.0414 6 -3 8 -1 130.154 10.0052 2 -3 1 8 126.61 10.0894 8 3 -8 -1 127.11 8.90556 1 -1 -3 8 129.6 8.69452 8 -1 8 3 113.135 9.52438 1 1 -3 -8 123.793 8.69461 9 -1 -3 8 127.029 9.68811 7 3 -8 -1 142.676 11.2053 4 -1 -3 8 121.115 10.4224 3 -1 3 -8 129.571 8.80589 8 1 -8 3 137.482 10.1862 4 -3 1 8 128.502 9.31865 4 -1 -3 8 122.931 9.97151 1 1 -3 -8 131.863 10.3252 7 1 -3 -8 129.753 10.1013 4 3 1 -8 122.1 12.1147 3 -3 8 -1 131.407 10.3257 3 3 1 -8 127.933 8.52662 10 1 -8 3 115.063 9.76731 3 1 3 8 127.94 10.5293 1 -1 3 -8 121.357 8.00829 2 1 -3 -8 121.672 12.2082 3 -3 8 -1 138.917 8.2943 8 -3 1 8 127.492 8.29376 2 1 -8 3 120.578 8.05284 8 3 -3 -8 22.1933 5.64229 4 -3 -3 8 21.0688 2.87583 4 -3 8 3 18.26 6.29891 6 -3 8 -3 26.886 5.043 2 -3 8 -3 17.8632 6.5098 6 -3 3 8 16.2146 5.09859 8 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33.8446 8 0 4 -8 544.54 42.2294 3 0 8 -4 489.782 38.2689 7 -4 0 8 569.14 33.2207 4 -4 0 8 576.016 33.2674 8 4 -8 0 587.164 42.4544 3 4 0 -8 594.858 38.1475 7 0 -8 -4 552.311 35.1921 4 0 8 -4 573.656 35.2338 6 0 -8 -4 543.267 40.9459 7 -4 8 0 589.933 32.6327 9 4 -8 0 565.116 32.8198 1 0 -4 -8 543.607 40.1408 7 -4 0 8 525.07 32.9745 9 4 -8 0 579.774 33.4056 10 0 -4 -8 614.741 42.1958 3 4 -8 0 555.781 34.7039 4 0 -4 8 561.072 41.6126 3 4 -8 0 580.057 38.7531 7 -4 8 2 112.61 8.97549 9 2 4 -8 99.4004 8.38556 7 -2 8 -4 108.791 10.7875 5 4 -8 2 118.69 8.45751 10 -2 8 -4 110.411 8.40876 7 4 -8 2 102.424 10.4392 4 4 -2 -8 114.639 8.77687 10 2 4 -8 109.645 9.00817 6 2 -8 -4 112.734 9.76644 7 -4 8 2 109.331 8.24984 1 -2 8 -4 110.89 11.1554 6 -2 4 8 115.479 9.78643 1 -2 8 -4 121.679 8.81058 4 2 -4 8 93.5587 10.1712 6 4 -2 -8 117.311 10.8759 5 2 -8 -4 114.127 10.405 4 -4 8 2 107.999 10.3484 6 2 -4 8 93.1821 7.99551 7 2 4 -8 100.003 11.0276 5 -4 -2 8 128.507 9.51068 1 2 4 -8 92.9654 7.5438 10 -4 -2 8 117.111 9.41189 8 -4 8 2 122.14 9.31756 2 4 -2 -8 117.6 12.7418 3 -2 4 8 106.075 8.39012 6 -2 8 -4 103.917 9.03362 2 2 -8 -4 124.62 11.6704 3 -4 -2 8 115.623 8.27801 4 4 -2 -8 121.537 9.75009 7 2 -4 8 105.892 9.19827 1 4 -2 -8 141.839 10.0186 4 -4 8 2 105.876 8.62506 8 4 -8 2 107.038 9.01704 7 4 -8 -2 121.666 9.24704 10 -4 2 8 123.334 9.40976 1 -2 -4 8 111.044 9.62361 1 -2 4 -8 106.303 7.61245 9 -2 8 4 112.035 8.6163 1 -4 8 -2 120.039 9.52111 3 -2 4 -8 105.441 8.00808 4 -4 8 -2 119.254 7.75552 8 2 -8 4 120.846 9.75395 4 -2 8 4 114.565 8.92384 8 -2 8 4 118.646 10.5481 6 -4 8 -2 114.357 9.01615 7 -2 4 -8 117.533 10.0056 3 4 -8 -2 117.538 8.02275 1 -4 8 -2 115.283 9.22298 9 4 -8 -2 114.793 12.3273 3 4 -8 -2 120.638 9.89472 7 2 -4 -8 128.579 9.87846 4 -2 -4 8 109.812 10.2382 3 4 2 -8 115.546 11.8972 5 -2 4 -8 116.155 8.12488 8 -4 8 -2 111.551 9.39162 2 -4 2 8 119.176 7.97465 2 -4 2 8 112.712 7.87987 9 -4 8 -2 100.763 9.75287 5 4 2 -8 118.629 9.25823 7 -4 2 8 116.035 9.42129 8 2 -4 -8 106.324 10.0439 7 -2 -4 8 123.156 8.42908 8 -2 8 4 127.964 9.60039 2 2 -4 -8 113.406 11.6715 3 -4 8 -2 112.621 10.7426 6 4 -4 -8 1366.61 78.0937 4 -4 4 8 1319.42 75.8031 2 4 -4 -8 1386.13 94.7431 5 4 -8 4 1199.5 88.4138 7 4 -8 -4 1260.39 95.2256 3 4 -8 -4 1359.02 89.1409 7 -4 8 -4 1237.04 93.4685 3 -4 8 -4 1294.33 96.8611 5 4 -4 -8 1327.01 89.928 7 -4 8 4 1285.14 77.499 2 4 -4 -8 1365.54 97.8529 3 -4 8 4 1247.23 82.1758 6 -4 4 8 1350.68 73.3916 9 4 -4 8 1255.1 80.143 1 4 -4 -8 1312.09 77.7994 10 -4 4 8 1259.65 78.6623 1 -4 8 4 1256.84 76.1253 8 4 -8 4 1233.98 78.189 10 -4 -4 8 1251.33 78.1925 8 4 -8 -4 1347.34 78.7132 4 -4 8 -4 1334.83 76.1898 2 -4 8 -4 1357.4 76.2337 9 -4 8 4 1254.34 76.785 1 4 -8 4 1202.37 85.6642 4 -4 8 4 1292.66 76.074 9 -4 8 -4 1193.76 80.693 6 -4 8 -4 1213.63 77.1194 8 -5 8 1 108.392 8.48358 9 5 -8 1 96.2641 8.33379 7 1 -5 8 88.2348 8.24949 1 1 -8 -5 113.686 10.4375 3 -1 5 8 89.8809 9.2893 1 1 -8 -5 108.681 9.82763 4 -5 -1 8 92.2693 7.8688 4 5 -8 1 101.717 10.7964 4 -5 8 1 98.7219 7.99811 8 5 -1 -8 119.789 11.1925 5 1 -8 -5 96.1217 9.05449 7 -5 -1 8 100.196 8.82338 1 1 5 -8 96.6859 10.9027 5 -1 -5 -8 100.111 17.2081 3 5 -8 1 100.987 8.3345 10 -1 8 -5 105.323 10.0871 5 5 -8 1 92.6328 6.70125 1 1 5 -8 91.2669 8.32148 6 5 -1 -8 96.5806 6.98626 6 -1 8 -5 92.3065 6.55782 10 -5 -1 8 97.1418 9.2463 8 -1 8 -5 86.4706 7.91648 4 -5 8 1 99.3658 9.5596 6 -1 8 -5 100.285 10.6895 6 5 -1 -8 94.3583 8.85848 7 5 -1 -8 99.7564 7.80662 10 1 5 -8 86.985 7.08876 7 -1 -8 5 93.526 8.18155 4 -1 8 -5 93.0515 6.63269 1 5 -1 -8 105.322 11.8252 3 -1 8 -5 89.1688 7.10719 7 1 -8 5 97.2092 8.69798 4 1 5 8 97.9069 9.18394 1 -1 -5 8 94.8792 8.35292 3 5 1 -8 87.9229 8.43918 7 -1 5 -8 90.6688 8.69267 3 1 -5 -8 91.2546 8.93366 7 5 -8 -1 104.464 11.2559 4 5 -8 -1 105.07 8.72262 7 -5 8 -1 106.567 8.40688 9 -1 5 -8 86.5709 7.7457 1 1 -5 -8 105.281 9.47541 4 -5 1 8 96.6635 7.05814 9 -5 1 8 105.739 8.89361 1 -5 8 -1 95.1354 9.05539 3 5 -8 -1 97.0273 8.48977 10 -1 8 5 103.971 8.12078 1 -5 8 -1 92.93 8.65811 2 5 1 -8 98.9457 11.1701 5 1 -5 -8 95.2106 10.9136 3 -1 -5 8 94.6718 8.31261 1 -5 8 -1 99.9282 7.62372 8 5 -8 -1 111.995 11.6371 3 -1 -5 8 93.6763 7.01937 8 1 8 -5 100.174 7.04402 1 -1 5 -8 90.2964 6.91316 2 5 -8 -1 101.26 6.93234 1 -5 1 8 91.1385 9.17413 8 5 -8 3 82.1037 10.0444 4 -3 5 8 89.6972 7.36891 6 3 -8 -5 96.0878 10.11 4 -3 5 8 78.2671 8.60477 2 -3 5 8 70.6108 8.46208 1 -3 8 -5 106.211 7.97417 4 5 -3 -8 103.421 9.66783 5 -3 8 -5 99.488 7.86348 9 5 -3 -8 89.32 8.727 7 -3 5 8 76.1531 8.47809 8 -5 8 3 75.3296 7.54515 1 -5 8 3 75.5489 7.93369 8 5 -8 3 76.4444 7.57051 7 3 5 -8 70.4534 10.3665 5 5 -3 -8 108.374 10.1622 4 3 -5 8 69.5301 6.37131 7 3 5 -8 90.8144 7.05886 7 -3 8 -5 95.5394 10.2199 6 -5 8 3 82.6259 8.45254 2 5 -3 -8 95.4486 8.02315 10 -5 8 3 89.2687 9.24444 6 3 -8 -5 95.8377 8.86458 7 3 -8 -5 96.3809 10.8878 3 5 -8 3 78.2089 7.53231 10 5 -3 -8 103.787 12.1911 3 -3 8 -5 92.1171 8.19527 2 3 -5 8 80.3986 7.67787 1 -3 8 -5 89.0766 9.24729 5 3 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6 -2 -8 41.1512 4.46329 6 2 -8 -6 40.6775 8.19675 3 6 -2 -8 51.9336 5.8133 10 -2 8 -6 38.5148 7.88047 6 6 -2 -8 34.7194 9.44907 3 -2 6 8 32.2434 6.29607 1 6 -8 2 30.6441 5.10178 7 6 -8 2 28.5113 5.42651 10 2 6 -8 28.3049 3.21741 7 6 -8 2 25.6136 3.23069 1 2 6 -8 25.897 8.2173 5 2 -8 -6 45.1463 7.57898 4 6 -8 2 29.4495 8.52582 4 -2 -8 6 39.2392 5.61298 2 2 6 -8 30.6148 6.65703 6 -2 8 -6 38.6583 5.78992 2 -6 8 2 33.4271 6.17089 8 -6 8 2 35.5916 6.19832 2 -2 6 8 35.5044 5.73627 6 -2 -8 6 45.5734 5.13886 4 -6 8 2 21.4277 5.96178 9 6 -2 -8 35.8925 7.76867 5 -2 6 -8 26.7611 4.50369 3 -6 2 8 29.676 7.42838 8 -2 -6 8 36.9845 4.66811 8 6 -8 -2 39.332 6.29015 10 2 -6 -8 39.549 5.82564 7 -6 8 -2 32.965 5.27309 8 -6 8 -2 26.472 6.96876 9 6 -8 -2 36.4726 5.97194 7 -2 -6 8 33.4615 3.65787 2 -6 8 -2 42.0896 5.93517 3 2 8 -6 32.6848 4.86014 1 2 -6 -8 43.2502 7.42909 4 6 -8 -2 26.5062 8.97678 3 -2 6 -8 38.2377 5.85435 1 2 -6 -8 51.1946 8.68001 3 -2 -6 8 36.1857 3.19026 4 -2 -6 8 32.291 3.73875 9 -2 6 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6.98416 4 -4 8 6 41.462 7.11712 2 -6 4 8 43.9231 5.98418 2 4 -6 -8 33.2589 6.50815 7 -4 8 6 31.7519 6.28905 1 -6 8 -4 55.1864 8.69392 9 6 -8 -4 39.338 10.4603 3 -6 8 -4 27.2124 5.7146 8 -4 8 6 37.9686 7.05298 6 6 -8 -4 30.9543 6.72518 10 6 -8 -4 42.7026 9.05986 4 -4 6 -8 33.4012 5.44951 3 -6 8 -4 26.2291 6.40397 3 4 -8 6 30.1623 3.43307 7 6 -8 -4 34.554 6.58739 7 4 -8 6 31.578 3.67812 1 6 -8 6 41.5722 5.07441 7 6 -8 -6 34.8914 10.0236 4 -6 6 8 36.2321 6.39515 9 -6 8 6 51.7388 7.1493 9 -8 6 6 49.8459 9.34912 8 8 -6 -6 47.365 7.22739 10 -6 6 8 37.768 8.72181 8 6 -8 6 38.3613 4.45928 1 -6 6 8 57.3002 7.67942 2 6 -6 -8 50.7249 7.59273 7 -6 8 -6 50.9924 10.7739 9 6 -6 -8 42.2231 7.60193 10 -6 8 6 41.8868 7.80221 1 8 -6 -6 13.8992 12.5746 3 6 -6 -8 24.5686 7.63553 5 6 -8 -6 42.8499 7.58108 10 -6 8 6 35.4619 7.7481 8 6 -8 -6 31.6599 12.4557 3 -6 8 6 45.0414 7.9112 2 -8 6 6 30.4191 7.26661 9 -6 6 8 46.7399 8.40949 1 8 -6 -6 36.9268 9.34282 4 6 -8 6 37.0631 5.28502 10 6 -6 -8 27.5108 9.60073 4 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3.72426 3.2555 7 -3 9 -2 3.35043 3.65184 3 -3 2 9 10.5089 5.53238 1 2 -9 3 9.32599 3.28981 7 3 -2 9 5.13025 5.67694 1 3 -9 -2 6.54086 4.50907 7 2 -3 -9 8.13197 5.5116 4 3 -9 -2 6.95588 4.5637 1 -3 2 9 9.36216 3.97299 2 -2 9 3 11.1927 3.71927 1 -2 9 3 2.32247 6.9603 6 3 -9 -2 11.623 6.94064 4 -2 9 3 6.43038 4.4784 8 -2 3 -9 3.50274 5.41211 3 3 -9 -2 7.01084 6.10803 3 -3 9 -2 10.826 5.2317 2 3 2 -9 7.78351 7.06666 5 3 2 -9 10.0928 6.93962 3 2 -9 3 9.82921 3.87665 3 3 2 -9 5.74768 3.07667 10 -2 3 -9 4.42845 4.53792 8 -2 -3 9 1.25037 4.38158 8 3 2 -9 7.2425 3.63314 7 -3 2 9 4.93827 5.33854 8 -4 9 1 34.9742 5.83683 9 4 -1 -9 30.9849 8.92085 3 -1 9 -4 38.8771 3.86049 7 1 -4 9 31.1245 3.52506 7 -1 -4 -9 34.5557 12.6659 3 -1 4 9 34.556 6.73771 1 -4 -1 9 39.6154 3.3979 2 1 4 -9 20.8507 8.12437 5 4 -1 -9 45.1538 5.15503 10 1 4 -9 28.8729 6.30092 3 4 -1 -9 43.4833 7.2299 5 -1 9 -4 31.2946 4.03642 10 -4 -1 9 37.7881 3.45367 9 -1 9 -4 39.8649 8.66062 6 4 -9 1 23.5663 8.13689 4 -1 4 9 31.4268 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43.5111 10.187 8 -5 8 -9 22.9731 8.51528 2 -5 9 8 36.1113 7.99486 6 -5 9 8 40.5239 8.6056 8 5 -9 8 26.0227 5.07187 1 5 -8 -9 22.4023 8.62398 7 -9 8 5 23.2949 8.8769 2 -8 5 9 34.1143 9.26032 1 -5 9 8 17.1331 9.45211 2 8 -9 -5 43.02 8.94901 10 -5 9 8 32.9838 7.87556 1 8 -9 -5 22.1389 13.8476 3 8 -9 -5 32.8577 7.74903 7 -5 8 -9 30.1434 8.26114 9 -9 8 5 17.4613 8.07647 9 -7 8 9 10.1295 7.43337 9 -9 7 8 9.5771 8.7797 2 8 -7 -9 28.9583 8.88815 7 -7 8 9 18.1527 8.93172 1 -8 9 7 11.8731 7.67036 1 -8 9 7 13.3136 8.29445 9 -9 7 8 25.4466 10.6586 8 -7 8 9 22.3305 8.83262 2 -9 7 8 25.6324 8.32114 9 9 -8 -7 13.2779 14.9327 3 -7 8 9 9.54306 8.97677 8 8 -7 -9 20.5299 8.8704 10 8 -7 -9 11.4516 11.511 4 9 -8 -7 17.225 8.48856 10 7 -9 -8 1.49668 11.5396 4 -7 9 -8 11.1815 14.8467 9 -8 9 7 25.5105 9.26547 8 9 -8 -7 17.2726 11.3775 4 7 -9 -8 21.7204 8.53539 10 7 -9 -8 2.1686 13.9977 3 -8 9 7 9.87172 9.36919 2 -7 9 8 18.8377 8.58568 1 -7 9 8 32.9324 7.78843 9 8 -9 -7 10.0437 11.6597 4 9 -7 -8 28.0787 8.83562 7 7 -8 -9 8.58189 8.41266 10 -7 9 8 4.93539 9.06179 2 7 -8 -9 16.999 8.73906 7 8 -9 -7 30.3145 8.72694 7 -8 7 9 16.5424 8.15374 9 -9 8 7 27.4449 8.15641 9 9 -7 -8 -0.9172 10.7518 4 8 -9 -7 14.5699 8.50666 10 -8 7 9 21.2036 8.56613 2 -8 7 9 8.81145 8.8612 1 9 -7 -8 18.3216 8.3971 10 8 -9 -7 10.1653 14.2935 3 -8 7 9 18.5863 10.4411 8 -9 8 7 22.9096 10.1404 8 7 -8 -9 11.3692 11.6589 4 9 -7 -8 3.13345 14.61 3 -9 8 7 20.6771 9.16443 2 7 -8 -9 -1.3024 14.1183 3 -7 9 8 23.4244 9.21358 8 0 9 -9 110.52 11.6857 6 0 9 -9 80.5131 13.0311 5 2 9 -9 36.2229 11.4575 5 2 -9 -9 57.2246 8.64655 7 -9 9 2 35.9956 9.5551 8 2 -9 -9 51.9467 11.8571 4 -2 9 9 59.4951 8.71607 1 -2 -9 9 62.1328 5.36012 8 -2 -9 9 54.8466 6.28483 4 -2 9 -9 43.4924 9.6704 6 -2 9 9 55.1084 8.99077 6 9 -9 -2 66.6486 8.52921 7 9 -9 -2 54.617 8.86122 10 2 9 -9 59.1273 10.1666 6 -9 9 2 50.5527 11.0369 9 4 -9 -9 4.04926 10.6751 4 -4 9 9 3.01126 7.89184 1 -4 9 -9 5.98747 8.05194 2 4 -9 9 5.05954 4.7999 1 -9 9 4 11.0449 8.3878 2 -9 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10.3569 8 -8 9 9 26.7938 10.7314 2 9 -9 -8 1.58292 15.7092 3 8 -9 -9 2.77843 14.8648 3 -8 9 9 30.2084 9.11064 9 8 -9 -9 10.887 13.2162 4 -9 9 8 34.5932 10.7056 2 9 -8 -9 28.1924 10.2518 10 8 -9 -9 34.6786 9.46204 10 -9 8 9 49.7834 11.6251 8 0 0 -10 111.647 7.43255 9 0 0 10 112.982 8.09508 10 0 -10 0 112.838 11.6572 4 0 0 -10 104.601 7.31273 2 0 0 10 120.369 9.08851 8 0 0 -10 125.582 8.60522 4 0 0 -10 124.333 12.2045 3 0 -10 0 116.229 10.4111 3 0 0 10 95.2349 10.288 1 0 0 -10 115.129 10.52 7 1 -10 -1 51.4218 7.73148 7 -1 1 10 60.8584 8.21795 1 1 -1 10 49.7738 5.72501 6 -1 -1 10 61.1506 6.85372 8 1 -1 -10 70.9424 9.73359 3 -1 1 -10 56.3038 5.69528 4 1 -10 1 60.0496 6.78139 3 1 1 -10 52.4124 6.15644 7 -1 -1 -10 59.8357 6.96429 4 -1 1 10 69.8111 7.26634 8 -1 -1 -10 49.779 9.63946 3 -1 10 -1 58.3757 4.60597 1 1 -1 -10 79.4432 6.78028 4 1 -1 10 56.2212 5.33719 10 1 -1 10 56.562 8.15477 1 1 1 -10 60.9817 6.56539 4 1 1 -10 62.1909 9.68475 3 -1 10 -1 58.4125 10.1793 6 1 -10 -1 89.8696 9.29864 4 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24.0638 6.54896 2 2 0 -10 24.5566 8.09022 3 0 2 -10 32.065 5.23112 7 2 0 -10 24.9661 5.721 4 2 0 10 20.6266 6.93363 1 2 -10 0 18.7059 4.95231 8 -2 10 -2 613.469 39.8562 6 2 -2 10 545.196 36.1362 10 2 2 -10 608.461 40.8556 7 -2 10 2 562.166 35.6372 1 -2 -2 10 640.735 35.1711 8 -2 -2 10 601.415 42.0491 7 -2 2 -10 593.46 44.8122 3 -2 2 10 582.413 35.5784 8 -2 10 -2 565.432 38.2205 2 2 -10 -2 603.357 45.4191 3 2 2 -10 607.467 45.9452 3 2 -2 -10 623.011 42.2666 7 -2 -2 10 567.061 38.2689 1 2 -2 10 563.532 37.6468 6 2 2 10 575.737 39.3682 1 -2 10 2 592.76 37.5682 6 2 -10 2 598.466 42.626 7 -2 10 -2 621.128 41.6795 7 2 -10 2 483.964 36.6402 8 2 -10 -2 591.028 42.7401 7 2 -10 -2 636.615 37.6119 4 -2 2 -10 542.293 42.706 4 2 -2 -10 647.74 35.7761 4 2 -10 2 571.245 37.3303 4 2 -10 2 508.879 42.7501 3 2 -2 10 596.753 36.8165 1 2 -2 -10 633.786 46.0852 3 2 -2 10 566.13 40.5729 7 -3 -1 10 115.084 8.52257 4 3 -10 1 118.213 9.78343 7 -1 10 -3 111.488 9.21455 7 3 -1 -10 119.107 9.15137 10 -1 3 10 103.383 10.6206 1 3 -1 -10 139.999 14.3205 3 1 -10 -3 113.948 11.4695 3 -1 3 10 90.0522 8.39738 6 -1 10 -3 120.35 12.8561 6 1 -3 10 104.666 10.37 1 1 -3 10 106.776 8.80186 7 -3 -1 10 138.398 9.61477 8 1 3 -10 104.802 12.1288 3 -1 3 10 113.257 9.89454 8 3 -1 -10 112.122 10.1674 7 1 -10 -3 110.05 11.7165 7 1 3 -10 99.1693 9.06904 7 -3 10 1 114.268 8.88929 8 -1 -3 -10 122.911 15.3095 3 3 -10 1 124.355 11.6756 3 3 -10 1 130.257 9.71944 8 -3 10 1 103.118 7.99683 1 -1 -3 -10 105.124 11.9069 4 -1 -10 3 123.43 10.8466 4 3 -10 1 102.633 12.4812 4 -3 -1 10 118.519 10.8859 1 -3 10 1 115.432 12.4035 6 1 -10 3 110.586 9.48229 3 -1 3 -10 139.498 12.013 3 3 -10 -1 126.792 12.0705 3 -1 3 -10 119.789 9.63493 8 -3 10 -1 133.695 12.1123 6 3 -1 10 118.69 11.0332 1 1 -3 -10 126.632 13.156 3 3 1 -10 121.084 13.5556 3 3 1 -10 104.45 9.60389 7 3 -10 -1 122.83 12.268 4 1 -3 -10 114.102 10.6761 7 1 -3 -10 122.488 10.2016 4 -1 -3 10 129.891 10.4801 1 3 -10 -1 123.093 10.3325 7 1 -10 3 106.194 11.1688 4 1 -3 -10 117.543 8.56828 9 3 1 -10 109.301 8.3918 10 1 -10 3 100.681 7.96533 8 -3 1 10 114.987 10.0243 8 -1 -3 10 110.574 8.99497 8 -3 1 10 115.777 9.05924 4 -1 10 3 100.115 8.90055 1 3 1 -10 104.744 11.9752 5 -3 10 -1 122.346 10.3824 3 -1 -3 10 117.589 9.36623 7 -3 10 -1 116.71 10.4827 2 1 -3 -10 113.433 8.37147 2 3 -10 3 35.8878 6.67556 3 3 3 -10 55.6733 5.30828 10 3 -3 10 48.8904 8.2843 1 -3 -3 10 61.5252 8.51604 1 -3 10 -3 72.152 6.28008 7 -3 -3 10 53.1983 4.68066 4 3 -3 -10 60.3499 8.56023 4 -3 10 3 57.5012 9.55932 6 -3 3 10 67.9754 7.76753 8 -3 10 3 58.1449 6.51734 8 -3 10 3 61.1357 6.30358 1 -3 10 3 60.3291 8.31147 2 3 3 -10 63.0295 5.87752 7 3 -3 -10 66.5561 7.76562 7 -3 3 10 68.9647 8.47394 1 3 -10 3 49.4381 9.73729 4 -3 3 -10 68.7761 11.2072 3 3 -3 10 50.0911 5.5875 7 3 -10 -3 61.089 9.65766 3 3 -3 -10 65.5909 10.5338 3 3 -10 3 60.683 6.0786 7 -3 -3 10 57.5217 7.43878 8 3 3 -10 58.4595 9.35927 3 3 3 -10 50.5008 5.07901 6 3 -10 -3 68.7133 7.60818 7 -3 10 -3 69.2694 7.53053 2 -3 10 -3 70.2564 10.2031 6 -4 0 10 15.1472 4.72341 4 0 4 -10 20.2964 7.07153 3 -4 10 0 26.457 5.08763 8 0 4 10 19.4183 6.86063 1 0 -4 -10 27.1484 9.72756 3 -4 0 10 14.2631 6.73069 1 0 -10 -4 15.2186 6.62603 3 4 0 -10 24.4446 5.20783 10 4 0 -10 26.6128 7.88337 5 0 10 -4 16.5684 3.42088 7 0 -4 10 17.8805 4.29793 3 4 -10 0 16.6338 8.09078 3 -4 10 0 20.0126 6.43291 2 4 0 -10 6.31104 8.6313 3 -4 0 10 22.8768 6.88324 8 0 -4 10 15.2841 6.25195 1 -4 0 10 9.21957 3.34364 2 4 -10 0 16.9127 5.13654 7 4 -10 0 11.7652 9.1273 4 0 -10 4 17.3477 3.37904 3 0 -4 -10 13.239 6.05021 7 0 -10 4 25.2741 6.46315 4 0 -4 10 13.3442 3.31885 7 0 -4 -10 18.4166 7.11261 4 0 10 -4 14.756 9.55573 6 0 -10 4 9.85143 2.76449 8 0 10 -4 18.834 4.25353 10 0 4 -10 18.5591 5.96903 8 4 0 -10 19.4992 4.75891 7 2 -10 -4 57.5397 7.38879 7 2 -4 10 49.2229 7.32503 6 -2 4 10 51.8806 7.65896 8 4 -2 -10 61.1744 11.7635 3 2 -4 10 40.0738 7.63525 1 -4 -2 10 57.1327 7.89815 8 4 -10 2 60.6394 6.35638 7 2 4 -10 47.3789 9.0478 3 4 -2 -10 80.839 9.02022 4 -4 -2 10 54.1479 8.30789 1 4 -10 2 62.7141 9.95042 4 2 -4 10 46.7103 4.76934 7 -2 10 -4 54.1199 5.34259 10 4 -2 -10 55.3866 6.26065 10 -2 10 -4 61.3341 5.28979 7 -4 10 2 31.1473 7.7264 2 -4 10 2 56.2819 6.80964 8 -2 4 10 50.8738 8.35439 1 2 -10 -4 54.6719 8.93354 3 2 4 -10 42.7661 5.12916 7 -2 10 -4 53.1086 7.86267 2 -4 -2 10 52.2692 4.05868 9 2 4 -10 43.7095 5.41393 6 4 -10 2 49.2164 8.25406 3 4 -2 -10 62.3572 8.74676 5 -4 -2 10 52.8328 5.55114 4 2 4 -10 41.5552 9.22108 5 -4 10 2 43.1186 8.84205 6 4 -2 -10 58.1575 7.39669 7 -4 10 2 47.1814 5.73332 1 -2 4 10 55.7015 4.96626 6 4 2 -10 51.1887 5.40783 10 -4 10 -2 54.5727 7.17237 9 4 2 -10 40.2177 9.55738 3 -4 2 10 42.6923 7.75451 8 4 -10 -2 57.7924 10.1691 4 -4 10 -2 78.0967 9.83278 6 -2 -4 10 58.906 8.06679 1 -2 4 -10 58.6576 7.92035 3 -2 4 -10 59.4801 6.57379 8 -2 -4 10 63.7807 6.39454 8 4 2 -10 36.2362 8.9426 5 -4 2 10 42.3448 7.90149 1 4 2 -10 56.4438 6.20206 7 2 -4 -10 60.2558 7.48208 7 4 -10 -2 71.3548 10.0189 3 -2 10 4 52.1407 6.25937 1 2 -4 -10 63.7128 8.21855 4 -2 4 -10 53.1492 4.75844 2 -2 4 -10 48.9579 4.41985 9 4 -10 -2 71.5699 6.38798 1 -4 10 -2 65.9054 7.25994 3 -2 10 4 44.8428 9.72188 6 -4 2 10 49.2429 5.89896 2 4 -10 -2 67.1326 7.35111 7 -4 10 -2 62.4637 5.80441 8 2 -4 -10 67.4741 10.5194 3 2 -10 4 45.5398 9.14473 4 -4 10 -2 58.284 8.47534 2 -4 10 4 119.31 9.92111 1 4 -10 4 136.145 10.0166 7 -4 -4 10 107.73 10.8402 1 -4 4 10 125.005 11.62 1 4 -4 10 124.592 11.5244 1 -4 10 -4 98.5052 10.3551 9 4 4 -10 120.388 10.0761 6 4 -4 -10 129.492 12.4314 4 4 -10 -4 114.341 11.4706 7 4 -4 -10 116.244 14.6576 3 -4 10 4 135.794 10.2874 8 4 -10 4 130.815 12.5036 4 -4 10 -4 95.5823 10.7091 5 -4 4 -10 115.232 17.6628 3 4 4 -10 132.181 10.0018 7 -4 -4 10 102.898 8.54649 4 4 -10 -4 118.375 13.3704 3 -4 10 4 122.3 11.4765 2 4 4 -10 124.218 8.73833 10 -4 4 10 124.944 10.1845 2 -4 10 4 123.115 12.4366 6 -4 10 -4 112.676 13.1202 6 -4 4 10 121.852 11.0334 8 -4 10 -4 97.9065 11.615 2 4 -4 -10 119.212 11.1727 7 -4 -4 10 132.131 10.3988 8 5 -1 -10 8.19529 5.31799 10 -5 -1 10 3.07741 3.08878 2 -1 -5 -10 14.0843 19.7001 3 5 -10 1 -2.7688 7.62443 3 1 5 -10 1.89947 4.19675 6 5 -10 1 1.05976 4.9395 7 5 -1 -10 2.57353 9.61408 3 -5 -1 10 3.15317 3.12617 9 -5 -1 10 12.8077 6.92226 8 5 -10 1 10.2506 9.27737 4 -1 5 10 5.57872 6.28995 8 1 -5 10 8.14772 6.37243 1 -5 10 1 5.83614 5.25962 8 -5 10 1 3.00174 6.10453 9 1 5 -10 1.53894 8.00294 5 -1 10 -5 0.90097 8.65688 6 -1 5 10 10.4377 7.02331 1 5 -1 -10 9.75657 5.31383 7 1 5 -10 12.2761 7.08056 3 -1 -10 5 3.43251 6.19681 4 5 -1 -10 4.35812 7.36115 5 -5 10 1 13.6684 7.37717 6 1 5 -10 1.84562 3.04656 7 -5 -1 10 15.5641 4.87209 4 -5 -1 10 5.9314 6.82101 1 -1 10 5 8.47959 4.77839 1 5 1 -10 -2.2227 8.29923 5 -5 10 -1 13.0896 6.35439 9 -5 10 -1 12.1934 4.7192 8 1 -5 -10 7.05559 9.34435 3 -1 -5 10 10.5215 6.18506 1 5 1 -10 1.54235 3.96275 10 -5 1 10 3.55693 3.55434 9 -1 -5 10 1.0777 4.44517 3 5 1 -10 4.65009 8.59148 3 -1 5 -10 13.6148 6.39349 3 -5 1 10 0.1207 3.94399 2 5 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10.0731 7 6 -5 -15 11.0972 9.75596 7 6 -5 -15 7.70369 11.0205 5 -6 15 5 5.46859 12.7149 6 6 -15 5 0.95943 13.6457 4 5 -6 -15 5.04265 9.26148 7 -6 15 -5 -38.84 15.0334 2 -5 15 6 -1.2809 12.6796 6 6 -15 -5 9.47186 10.2466 7 5 -6 -15 7.63015 11.2346 5 5 -15 6 -3.6089 13.2565 4 -6 5 15 4.06802 11.1122 8 6 -15 -5 -1.4284 16.5418 3 -7 0 15 22.4197 11.6484 8 7 0 -15 4.16042 14.468 5 0 -7 15 3.47735 11.608 1 0 7 -15 8.39423 19.3557 5 7 -15 0 9.28806 8.43079 7 -7 15 0 15.466 12.918 2 -7 0 15 6.83577 11.8258 1 7 -15 0 10.4352 17.5234 4 0 15 -7 0.40918 16.1398 6 2 -7 15 49.5821 11.3339 1 7 -15 2 38.1013 19.4095 4 7 -2 -15 56.3128 18.7601 3 7 -2 -15 29.7095 13.3027 5 -7 -2 15 20.7049 10.6231 1 2 -15 -7 27.8763 13.432 3 7 -2 -15 17.5918 9.86929 7 -7 -2 15 52.2927 11.989 8 -2 7 15 44.8776 12.5937 1 -2 15 -7 0.36562 15.2151 6 -2 -7 15 46.7301 11.9812 1 7 2 -15 33.2415 13.595 5 7 -15 -2 60.0761 17.2175 4 -2 15 7 18.8315 12.1258 6 -7 15 -2 30.5825 14.7185 2 2 -7 -15 25.548 11.7581 7 -7 2 15 33.6272 12.1725 8 -2 7 -15 19.779 23.4046 5 2 -7 -15 21.6825 21.9409 3 7 -15 -2 53.4788 10.158 7 4 -15 -7 42.3389 15.3914 3 7 -4 -15 14.9371 17.4706 3 -4 15 -7 -1.8717 14.4802 6 7 -4 -15 16.7295 11.9586 5 4 -15 -7 22.1202 11.3823 7 7 -15 4 20.7082 14.8956 4 7 -4 -15 33.2945 10.5607 7 -7 15 -4 16.3523 14.7641 2 -4 15 7 23.5959 12.8879 6 4 -7 -15 24.7483 10.3425 7 -7 4 15 23.9208 11.1223 8 7 -15 -4 43.9518 10.4904 7 7 -15 -4 48.4634 15.7843 3 -6 15 -7 34.2706 16.2971 2 6 -15 -7 16.852 18.63 3 -7 15 6 9.99701 10.3272 8 7 -15 -6 -6.7637 17.7532 3 -7 15 -6 27.7253 17.3008 2 -6 15 7 6.05192 12.7729 6 -1 15 -8 0.36611 15.4634 6 8 -15 1 22.3967 17.3075 4 8 -1 -15 27.9102 10.6722 7 8 -1 -15 8.2371 12.5612 5 8 -15 -1 32.5773 18.2661 4 8 -15 -1 20.1715 9.97643 7 -1 -8 15 36.8471 11.1314 1 -8 1 15 53.8285 11.8696 8 8 -15 3 16.7206 14.782 4 -3 15 -8 -0.3657 14.0355 6 8 -3 -15 12.3262 9.38579 10 8 -3 -15 27.4651 12.077 5 3 -15 -8 21.4876 14.4289 3 8 -3 -15 21.8088 10.3332 7 8 -15 -3 16.3639 17.2781 3 -8 15 -3 -1.1467 15.5034 2 8 -15 -3 5.14665 10.3795 7 -3 15 8 5.77984 11.0581 6 5 -15 -8 2.50436 17.1075 3 -8 15 -5 14.9323 17.615 2 8 -15 -5 13.4604 11.5625 7 -5 15 8 15.9734 12.3177 6 8 -15 -5 18.4534 18.1508 3 -8 15 7 11.5 12.5991 8 -7 15 -8 -6.6137 18.9619 2 -8 15 -7 20.823 19.0004 2 8 -15 -7 -7.3056 18.1476 3 0 15 -9 0.37176 14.8837 6 9 -15 0 10.5022 9.63403 7 -2 15 -9 0.72396 14.3397 6 9 -15 2 13.4882 15.8208 4 9 -15 -2 23.7027 10.8624 7 2 -9 -15 14.3434 26.8214 4 9 -4 -15 21.1292 10.0658 10 9 -15 -4 -5.023 17.5196 3 9 -15 -4 12.166 11.3638 7 -4 15 9 11.4518 11.7017 6 -1 15 -10 2.23631 15.278 6 10 -15 -1 19.3828 11.1615 7 1 15 -10 -0.3762 15.0287 6 3 -10 -15 -23.35 24.3992 4 10 -15 -3 15.1929 11.4145 7 -3 15 10 10.039 11.3471 6 0 0 -16 172.736 26.9856 3 0 0 16 175.647 19.0643 1 -1 16 -1 2.52285 20.4338 6 1 1 -16 21.7629 18.2998 3 -1 -1 16 17.2954 12.5533 1 -1 1 16 31.7294 13.2239 1 1 1 16 36.7405 13.6755 1 1 -1 16 27.1741 13.5416 1 1 -1 -16 58.4197 20.223 3 1 -16 1 46.3086 14.6952 4 -1 -1 -16 34.2523 27.6839 3 -2 0 -16 46.3282 32.7861 3 0 -2 16 34.7781 12.7827 1 -2 0 16 37.7898 13.1266 1 0 2 16 50.8142 13.0181 1 2 0 16 22.8461 13.7979 1 2 0 -16 60.6281 21.1363 3 0 -2 -16 41.0987 25.1058 3 2 -16 0 40.371 15.8106 4 2 -2 16 29.374 13.0444 1 2 -16 2 -0.8488 14.9808 4 2 2 -16 -0.5806 16.7051 5 -2 2 16 17.081 12.0594 1 -2 16 2 33.4219 17.2236 6 2 -2 -16 19.8911 20.5144 3 2 -16 -2 57.3665 16.3803 4 -2 16 -2 -0.4286 16.4547 6 2 -16 -2 25.4426 12.1372 3 -2 -2 16 16.2051 12.4729 1 2 -2 -16 36.1584 10.2559 7 -3 -1 16 31.2415 10.159 8 -3 16 1 39.6443 17.7219 6 -1 -3 -16 46.2713 46.1942 3 -1 16 -3 0.44267 18.7377 6 3 -1 -16 20.4938 20.029 3 3 -1 -16 21.3051 16.3155 5 -3 -1 16 38.1108 13.0286 1 -1 3 16 37.7508 12.5744 1 1 -3 16 48.7847 13.0908 1 3 -16 1 21.2987 14.9611 4 -3 1 16 51.9084 12.7616 1 -1 -3 16 37.4511 12.3531 1 1 -16 3 47.3199 15.5238 4 1 -3 -16 59.3708 22.9054 3 1 3 16 40.8263 12.6051 1 -3 1 16 25.168 10.4356 8 3 1 -16 29.4291 18.0939 3 3 -16 -1 57.2619 16.0648 4 3 1 -16 51.8323 17.0472 5 -3 -3 16 21.3825 13.1915 1 3 -3 16 43.8596 13.0807 1 -3 3 16 33.0913 11.4599 8 3 -16 3 48.5166 16.7455 4 -3 -3 16 20.1794 10.2183 8 3 -16 -3 0.92 15.4616 4 -3 16 -3 -0.3977 15.6339 6 3 -3 -16 -2.4908 20.9561 3 -3 16 3 11.8344 15.9974 6 3 3 -16 25.0222 16.3185 5 3 -16 -3 11.5185 13.8471 3 3 -3 -16 1.29994 8.88091 7 4 0 -16 93.1548 18.4914 5 0 -4 16 112.37 15.5634 1 0 -4 -16 165.902 36.8772 3 -4 0 16 86.6434 15.4688 1 4 -16 0 123.319 19.7665 4 0 4 -16 113.574 22.6838 5 -4 16 0 120.882 18.7284 6 4 0 -16 110.189 22.7201 3 -4 0 16 120.013 14.1722 8 4 -2 -16 15.0825 9.06734 7 4 -2 -16 2.48121 20.2527 3 -4 16 2 12.7836 15.2486 6 4 -2 -16 14.6537 13.7259 5 -4 -2 16 6.54516 12.9458 1 4 -16 2 38.9922 15.2964 4 2 -16 -4 18.733 14.0631 3 2 -4 16 13.7503 12.8791 1 -4 -2 16 23.5908 10.6845 8 -2 16 -4 0.80592 16.1768 6 2 -16 -4 12.7524 15.5287 4 2 -4 -16 -0.5845 10.461 7 2 -4 -16 16.8119 21.1119 3 4 2 -16 19.4623 15.3867 5 2 -16 4 31.846 15.3468 4 -2 16 4 20.4107 15.288 6 -2 -4 16 6.55304 11.9393 1 -4 2 16 4.23339 13.147 1 4 -16 -2 31.6095 15.8673 4 4 -16 -2 16.4775 11.5062 7 -4 2 16 14.176 11.784 8 4 -16 4 49.4816 17.6371 4 4 -4 -16 91.1573 16.1522 5 4 -4 -16 84.6562 12.2969 7 4 -4 -16 69.6396 23.6491 3 -4 -4 16 96.8662 14.5965 1 -4 4 16 49.7729 12.7626 8 4 -16 -4 79.7304 17.5004 3 4 -16 -4 87.2885 14.3728 7 -4 16 4 87.5577 16.4502 6 1 -5 16 43.1743 12.9021 1 5 -1 -16 -1.7311 13.1863 5 -5 16 1 -1.9382 14.9093 6 -5 -1 16 -14.208 12.9231 1 -5 -1 16 9.9704 10.3695 8 5 -16 1 5.06161 15.9317 4 -1 16 -5 -0.425 16.46 6 5 -1 -16 25.5842 18.9632 3 5 1 -16 18.846 15.2059 5 5 1 -16 13.5417 18.2454 3 -1 -5 16 11.3068 12.5322 1 1 -5 -16 -1.5776 25.8774 3 1 -16 5 3.35142 15.7021 4 -5 1 16 -0.3449 10.8749 8 5 -16 -1 21.6504 15.5357 4 5 -16 -1 7.22369 10.4309 7 3 -5 16 8.81395 11.5355 1 -5 -3 16 -6.567 12.2596 1 3 -16 -5 -6.8321 14.0074 3 5 -3 -16 -2.3571 8.87193 7 -5 -3 16 -0.3123 9.99219 8 -5 16 3 6.38697 14.7068 6 5 -3 -16 -17.22 13.2556 5 5 -3 -16 17.1419 19.66 3 5 -16 3 15.4877 14.667 4 3 -16 5 -2.0841 14.4312 4 3 -5 -16 15.272 20.4565 3 -5 3 16 7.15677 10.4955 8 5 -16 -3 25.5082 15.4758 3 -3 16 5 1.7349 13.7137 6 -3 -5 16 -9.3412 11.9125 1 3 -5 -16 12.5847 10.1866 7 5 -16 -3 7.17618 9.77815 7 5 -16 5 2.91645 15.3877 4 -5 16 5 11.3469 14.2022 6 5 -5 -16 11.843 11.8881 5 5 -16 -5 9.51159 17.8607 3 5 -16 -5 15.3908 10.7338 7 -5 -5 16 0.40341 9.5867 1 5 -5 -16 18.5979 10.2163 7 6 -16 0 11.2405 16.3958 4 6 0 -16 17.1293 14.3127 5 0 16 -6 0.43757 17.4645 6 0 -6 16 19.6772 12.082 1 -6 0 16 16.7425 10.5515 8 6 -16 0 10.3141 9.06374 7 6 0 -16 2.8299 19.07 3 2 -6 16 8.30315 12.3961 1 6 -2 -16 17.1339 13.5783 5 6 -16 2 14.6585 15.6814 4 6 -2 -16 29.0536 19.5034 3 6 -2 -16 16.6069 10.1477 7 -6 -2 16 19.4675 10.376 8 -6 2 16 20.5095 11.272 8 6 -16 -2 12.6159 9.34826 7 2 -6 -16 8.09739 11.5151 7 -6 16 -2 21.5429 14.1935 2 -2 -6 16 32.641 12.595 1 6 -4 -16 13.4021 10.4792 7 4 -16 -6 7.80961 11.1818 7 4 -16 -6 12.695 15.8449 3 4 -6 16 1.95263 11.1705 1 6 -4 -16 -1.9545 12.0872 5 6 -16 4 1.56265 15.2626 4 6 -16 -4 -12.687 10.7608 7 -6 16 -4 9.12339 14.5008 2 -4 -6 16 4.15037 10.5412 1 6 -16 -4 11.0895 16.7487 3 -4 16 6 21.3712 13.5689 6 4 -6 -16 17.7602 10.3974 7 4 -6 -16 15.8773 12.7733 5 6 -16 -6 -5.9114 18.9842 3 -6 16 -6 10.1258 15.8624 2 7 -1 -16 17.6741 13.9832 5 7 -1 -16 46.4422 19.8243 3 1 -7 16 27.2589 12.2896 1 7 -16 1 29.3553 18.0561 4 -7 -1 16 -7.4815 12.1405 8 -7 1 16 -7.3777 11.7369 8 7 -16 -1 17.5828 10.1434 7 7 1 -16 -4.8172 13.9768 5 -1 -7 16 13.3163 12.1756 1 7 -16 3 36.6229 16.4024 4 3 -16 -7 41.1963 14.6727 3 -7 -3 16 17.2459 12.3177 8 7 -3 -16 9.21401 12.6922 5 7 -3 -16 30.3241 11.3702 7 -3 16 7 3.58905 12.3817 6 -3 -7 16 16.0865 11.1577 1 7 -16 -3 19.4644 11.3903 7 7 -5 -16 28.0412 13.1667 5 7 -16 5 31.1938 14.7156 4 5 -16 -7 33.9474 18.5096 3 7 -16 -5 29.9389 17.2528 3 -5 16 7 5.28813 13.5592 6 8 0 -16 96.2747 16.9629 5 -8 0 16 97.848 14.511 8 8 -2 -16 12.6932 12.847 5 8 -2 -16 20.6103 10.8851 7 8 -16 2 7.19955 16.7796 4 8 -16 -2 3.74735 10.3086 7 8 -4 -16 71.6837 14.1815 5 8 -16 4 61.1605 17.5052 4 -4 16 8 58.5361 14.0673 6 9 -16 -1 9.40916 10.7555 7 0 -1 -17 17.6642 27.7957 3 0 -1 17 9.90428 14.1425 1 1 0 -17 25.7412 22.5016 3 -1 0 17 9.4 13.2989 1 1 0 17 6.56168 13.8979 1 -1 -2 -17 16.2391 44.8921 3 1 -2 17 2.10206 13.1926 1 2 -17 1 9.437 15.7093 4 2 -1 -17 37.7133 23.4938 3 -2 -1 17 17.7156 12.7278 1 1 -2 -17 2.94948 24.213 3 -1 -2 17 6.16123 13.326 1 1 -17 2 11.1883 15.2115 4 2 -1 17 28.535 13.7282 1 2 -17 -1 26.3297 16.5216 4 -3 0 17 10.3733 10.0966 8 3 0 -17 21.5265 22.9287 3 0 -3 17 2.0092 13.8146 1 3 -17 0 7.90993 15.7547 4 0 -3 -17 20.359 35.1709 3 3 -17 2 18.9936 17.0379 4 2 -3 17 31.1521 13.5809 1 3 -2 -17 -10.865 16.8534 5 -3 -2 17 4.23718 12.9029 1 3 -2 -17 10.6014 23.2587 3 -3 -2 17 4.37621 9.76827 8 2 -3 -17 -22.433 24.7761 3 -2 -3 17 7.5906 13.3628 1 -3 2 17 -4.9365 10.4693 8 2 -17 3 14.2209 15.3943 4 4 -1 -17 3.59219 16.1134 5 4 -17 1 14.617 15.371 4 -4 -1 17 24.4428 10.8984 8 4 -1 -17 -12.911 21.3113 3 1 -4 17 17.0674 13.032 1 -1 -4 17 -0.367 12.8827 1 1 -17 4 11.9577 16.7365 4 1 -4 -17 -13.126 29.4912 3 -4 1 17 -0.7431 11.3921 8 3 -17 -4 27.7682 16.3505 3 4 -3 -17 31.3879 22.6211 3 3 -4 17 25.2414 12.7123 1 4 -3 -17 16.2067 15.0385 5 4 -17 3 14.3414 16.3187 4 -3 -4 17 11.1891 13.7365 1 3 -17 4 14.0633 15.4229 4 -4 3 17 12.0159 11.0141 8 3 -4 -17 12.9242 10.9559 7 0 -5 17 18.2618 13.7618 1 5 0 -17 34.4313 21.3266 3 -5 0 17 20.3431 11.133 8 2 -5 17 7.60729 12.7888 1 5 -2 -17 14.1292 21.132 3 5 -2 -17 9.29305 13.5655 5 -5 -2 17 -6.0541 10.7968 8 5 -17 2 10.6864 17.6132 4 -2 -5 17 19.2991 14.0819 1 5 -17 -2 -10.644 11.113 7 -5 2 17 6.73355 11.3864 8 4 -17 -5 37.8887 17.4705 3 5 -17 4 38.8758 17.6017 4 5 -4 -17 7.63567 13.7852 5 5 -4 -17 18.4232 10.5669 7 5 -17 -4 -15.89 12.074 7 -4 -5 17 16.4038 13.4654 1 4 -5 -17 5.72439 14.5587 5 4 -5 -17 10.8681 10.5695 7 6 -1 -17 17.9046 20.962 3 1 -6 17 16.0056 13.5509 1 -6 -1 17 23.4456 11.9798 8 -6 1 17 14.22 11.807 8 -1 -6 17 35.9048 16.8446 1 6 -17 3 45.0222 18.3546 4 3 -17 -6 17.4719 15.8823 3 6 -3 -17 7.63551 14.7735 5 -3 -6 17 15.5424 12.6961 1 6 -17 -3 16.6499 11.5008 7 0 -2 -18 12.9956 40.6761 3 2 -2 -18 45.9963 29.1592 3 2 -18 2 94.3505 19.4787 4 3 -1 -18 37.5672 27.5413 3 -4 0 18 -2.1142 11.3147 8 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Co1 N1 110.5(3) 46 3_655 ? N1 Co1 N1 107.4(6) 3_655 . ? N1 Co1 N1 110.5(3) 46 . ? N1 Co1 N1 107.4(6) 46 48_554 ? N1 Co1 N1 110.5(3) 48_554 . ? N1 Co1 N1 110.5(3) 3_655 48_554 ? C2 N1 Co1 125.9(6) . . ? C2 N1 C1 105.6(9) . . ? C1 N1 Co1 128.0(8) . . ? N1 C2 N1 113.2(11) . 14_665 ? N1 C2 C3 123.3(6) . . ? N1 C2 C3 123.3(6) 14_665 . ? N1 C1 C1 107.8(7) . 14_665 ? N1 C1 H1 126.1 . . ? C1 C1 H1 126.1 14_665 . ? C2 C3 H3A 109.5 . . ? C2 C3 H3B 109.5 . . ? C2 C3 H3C 109.5 . . ? H3A C3 H3B 109.5 . . ? H3A C3 H3C 109.5 . . ? H3B C3 H3C 109.5 . . ? N3 N2 N3 180.0 . 3_655 ? N4 N5 N4 174(9) . 2_665 ? N2 N3 N3 0.000(2) . 3_655 ? N12 N11 N12 67(10) . 20 ? N12 N11 N12 67(10) . 21_654 ? N12 N11 N12 67(10) 14_665 20 ? N12 N11 N12 67(10) 14_665 6_665 ? N12 N11 N12 0(10) 6_665 21_654 ? N12 N11 N12 67(10) . 6_665 ? N12 N11 N12 67(10) 14_665 21_654 ? N12 N11 N12 67(10) 21_654 20 ? N12 N11 N12 0(10) 14_665 . ? N12 N11 N12 67(10) 6_665 20 ? N12 N11 N10 55(10) 14_665 12_654 ? N12 N11 N10 55(10) 12_654 6_665 ? N12 N11 N10 55(10) . 6_665 ? N12 N11 N10 55(10) . 12_654 ? N12 N11 N10 55(10) 20 14_665 ? N12 N11 N10 55(10) 6_665 12_654 ? N12 N11 N10 108(10) 21_654 6_665 ? N12 N11 N10 55(10) 21_654 12_654 ? N12 N11 N10 55(10) 21_654 14_665 ? N12 N11 N10 108(10) 20 12_654 ? N12 N11 N10 55(10) 12_654 14_665 ? N12 N11 N10 108(10) 12_654 12_654 ? N12 N11 N10 108(10) 6_665 6_665 ? N12 N11 N10 108(10) 14_665 14_665 ? N12 N11 N10 55(10) 20 6_665 ? N12 N11 N10 108(10) . 14_665 ? N12 N11 N10 55(10) 6_665 14_665 ? N12 N11 N10 55(10) 14_665 6_665 ? N10 N11 N10 0(10) . 14_665 ? N10 N11 N10 107(10) 12_654 14_665 ? N10 N11 N10 107(10) 14_665 6_665 ? N10 N11 N10 107(10) 12_654 . ? N10 N11 N10 107(10) 12_654 6_665 ? N10 N11 N10 107(10) . 6_665 ? N15 N13 N15 110(10) 6_665 . ? N15 N13 N15 110(10) 12_654 . ? N15 N13 N15 110(10) 6_665 12_654 ? N11 N10 N10 36(9) . 12_654 ? N13 N15 N15 35(8) . 12_654 ? N13 N15 N15 35(8) . 6_665 ? N15 N15 N15 60.00(2) 6_665 12_654 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Co1 N1 1.955(9) 46 ? Co1 N1 1.955(9) 48_554 ? Co1 N1 1.955(9) 3_655 ? Co1 N1 1.955(9) . ? N1 C2 1.336(9) . ? N1 C1 1.380(10) . ? C2 C3 1.52(2) . ? C1 C1 1.39(3) 14_665 ? C1 H1 1.0770 . ? C3 H3A 1.0830 . ? C3 H3B 1.0830 . ? C3 H3C 1.0830 . ? N2 N3 0.65(3) 3_655 ? N2 N3 0.65(3) . ? N5 N4 1.04(3) . ? N5 N4 1.04(3) 2_665 ? N8 N9 1.009(18) . ? N3 N3 1.31(6) 3_655 ? N6 N7 0.56(12) . ? N11 N12 0.79(10) 20 ? N11 N12 0.79(10) 6_665 ? N11 N12 0.79(10) 14_665 ? N11 N12 0.79(10) 12_654 ? N11 N12 0.79(10) . ? N11 N12 0.79(10) 21_654 ? N11 N10 0.80(18) 12_654 ? N11 N10 0.80(17) 6_665 ? N11 N10 0.80(17) 14_665 ? N11 N10 0.80(17) . ? N13 N15 0.70(13) 6_665 ? N13 N15 0.70(13) 12_654 ? N13 N15 0.70(13) . ? N10 N10 1.3(3) 12_654 ? N15 N15 1.1(2) 12_654 ? N15 N15 1.1(2) 6_665 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Co1 N1 C2 N1 173.5(5) . . . 14_665 ? Co1 N1 C2 C3 -2.9(18) . . . . ? Co1 N1 C1 C1 -172.7(6) . . . 14_665 ? C2 N1 C1 C1 -0.8(9) . . . 14_665 ? C1 N1 C2 N1 1.5(16) . . . 14_665 ? C1 N1 C2 C3 -175.0(12) . . . . ? N10 N11 N10 N10 115(40) 6_665 . . 12_654 ? N10 N11 N10 N10 0(100) 14_665 . . 12_654 ? N15 N13 N15 N15 -120(42) 12_654 . . 6_665 ? N15 N13 N15 N15 120(42) 6_665 . . 12_654 ?