#------------------------------------------------------------------------------ #$Date: 2023-11-23 01:39:40 +0200 (Thu, 23 Nov 2023) $ #$Revision: 287746 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/77/7247779.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7247779 loop_ _publ_author_name 'Jones, Isabelle M.' 'Turner, Gemma F.' 'Pitts, Kari' 'Powell, Rees' 'Riboldi-Tunnicliffe, Alan' 'Williamson, Rachel' 'Boer, Stephanie' 'Allen, Lauren' 'Moggach, Stephen A.' _publ_section_title ; High-pressure induced guest-mediated gate opening behaviour of the Co-based framework ZIF-67 ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D3CE00979C _journal_year 2023 _chemical_absolute_configuration ad _chemical_formula_moiety 'C8 H10 Co N4, 18.667(N0.5)' _chemical_formula_sum 'C8 H10 Co N13.33' _chemical_formula_weight 351.89 _space_group_crystal_system cubic _space_group_IT_number 217 _space_group_name_Hall 'I -4 2 3' _space_group_name_H-M_alt 'I -4 3 m' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2023-10-04 _audit_creation_method ; Olex2 1.5 (compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817) ; _audit_update_record ; 2023-10-04 deposited with the CCDC. 2023-11-21 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 12 _cell_length_a 16.5684(3) _cell_length_b 16.5684(3) _cell_length_c 16.5684(3) _cell_measurement_reflns_used 7907 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 20.7480 _cell_measurement_theta_min 3.4610 _cell_volume 4548.22(14) _computing_cell_refinement 'CrysAlisPro 1.171.42.58a (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.42.58a (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.58a (Rigaku OD, 2022)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _diffrn_ambient_temperature 293(2) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.986 _diffrn_measured_fraction_theta_max 0.986 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -84.00 -30.00 0.50 33.13 -- 13.12 -29.00 -95.00 108 2 \w 62.00 96.00 0.50 33.13 -- 13.12 29.00 65.00 68 3 \w -99.00 -30.00 0.50 33.13 -- -13.27 -29.00 -95.00 138 4 \w -16.00 43.00 0.50 33.13 -- 13.12 -38.00-180.00 118 5 \w -41.00 22.00 0.50 33.13 -- 13.12 53.00 162.00 126 6 \w -41.00 22.00 0.50 33.13 -- 13.12 53.00 -17.00 126 7 \w -22.00 57.00 0.50 33.13 -- 13.12 -53.00 17.00 158 8 \w 5.00 84.00 0.50 33.13 -- 13.12-114.00 45.00 158 9 \w -59.00 -5.00 0.50 33.13 -- 13.12 114.00 135.00 108 10 \w -10.00 68.00 0.50 33.13 -- 13.12 -82.00-151.00 156 11 \w -94.00 -68.00 0.50 33.13 -- 13.12 178.00 -90.00 52 12 \w -26.00 53.00 0.50 33.13 -- -13.27 -40.00-167.00 158 13 \w -53.00 26.00 0.50 33.13 -- -13.27 40.00 -12.00 158 14 \w -63.00 4.00 0.50 33.13 -- -13.27 57.00-180.00 134 15 \w -3.00 50.00 0.50 33.13 -- -13.27 -97.00 35.00 106 16 \w 54.00 96.00 0.50 33.13 -- 13.12-178.00 -90.00 84 17 \w -36.00 -16.00 0.50 33.13 -- 13.12 38.00 0.00 40 18 \w 68.00 96.00 0.50 33.13 -- 13.12-178.00 90.00 56 19 \w -27.00 -3.00 0.50 33.13 -- -13.27 19.00-150.00 48 20 \w -43.00 -18.00 0.50 33.13 -- -13.27 38.00-180.00 50 21 \w -68.00 10.00 0.50 33.13 -- -13.27 82.00 -29.00 156 22 \w -32.00 47.00 0.50 33.13 -- -13.27 -26.00 8.00 158 23 \w -38.00 -9.00 0.50 33.13 -- -13.27 77.00 150.00 58 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Single source at home/near, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0392875000 _diffrn_orient_matrix_UB_12 -0.0074377000 _diffrn_orient_matrix_UB_13 -0.0152804000 _diffrn_orient_matrix_UB_21 0.0063490000 _diffrn_orient_matrix_UB_22 -0.0421331000 _diffrn_orient_matrix_UB_23 0.0041757000 _diffrn_orient_matrix_UB_31 -0.0157705000 _diffrn_orient_matrix_UB_32 0.0015640000 _diffrn_orient_matrix_UB_33 0.0397717000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0666 _diffrn_reflns_av_unetI/netI 0.0186 _diffrn_reflns_Laue_measured_fraction_full 0.986 _diffrn_reflns_Laue_measured_fraction_max 0.986 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 16850 _diffrn_reflns_point_group_measured_fraction_full 0.989 _diffrn_reflns_point_group_measured_fraction_max 0.989 _diffrn_reflns_theta_full 18.983 _diffrn_reflns_theta_max 18.983 _diffrn_reflns_theta_min 3.478 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Mo) X-ray Source' _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 1.153 _exptl_absorpt_correction_T_max 0.7309 _exptl_absorpt_correction_T_min 0.6756 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0861 before and 0.0728 after correction. The Ratio of minimum to maximum transmission is 0.9243. The \l/2 correction factor is Not present. ; _exptl_crystal_colour 'clear bluish violet' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier bluish _exptl_crystal_colour_primary violet _exptl_crystal_density_diffrn 1.542 _exptl_crystal_description block _exptl_crystal_F_000 2140 _exptl_crystal_size_max 0.14 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.09 _refine_diff_density_max 0.747 _refine_diff_density_min -0.834 _refine_diff_density_rms 0.135 _refine_ls_abs_structure_details ; Flack x determined using 143 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.088(18) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.151 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 49 _refine_ls_number_reflns 373 _refine_ls_number_restraints 11 _refine_ls_restrained_S_all 1.172 _refine_ls_R_factor_all 0.0844 _refine_ls_R_factor_gt 0.0796 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1708P)^2^+9.6005P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2069 _refine_ls_wR_factor_ref 0.2121 _reflns_Friedel_coverage 0.759 _reflns_Friedel_fraction_full 0.994 _reflns_Friedel_fraction_max 0.994 _reflns_number_gt 346 _reflns_number_total 373 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL zif67_ln2_2900_a.res in I-43m zif67_ln2_2900.res created by SHELXL-2018/3 at 11:16:48 on 04-Oct-2023 REM Old TITL ZIF67_LN2_2900 in I-43m REM SHELXT solution in I-43m: R1 0.160, Rweak 0.056, Alpha 0.206 REM 0.000 for 0 systematic absences, Orientation as input REM Flack x = 0.355 ( 0.036 ) from 175 Parsons' quotients REM Formula found by SHELXT: C33 N19 Co3 CELL 0.71073 16.5684 16.5684 16.5684 90 90 90 ZERR 12 0.0003 0.0003 0.0003 0 0 0 LATT -2 SYMM -X,-Y,+Z SYMM -X,+Y,-Z SYMM +X,-Y,-Z SYMM +Z,+X,+Y SYMM +Z,-X,-Y SYMM -Z,-X,+Y SYMM -Z,+X,-Y SYMM +Y,+Z,+X SYMM -Y,+Z,-X SYMM +Y,-Z,-X SYMM -Y,-Z,+X SYMM +Y,+X,+Z SYMM -Y,-X,+Z SYMM +Y,-X,-Z SYMM -Y,+X,-Z SYMM +X,+Z,+Y SYMM -X,+Z,-Y SYMM -X,-Z,+Y SYMM +X,-Z,-Y SYMM +Z,+Y,+X SYMM +Z,-Y,-X SYMM -Z,+Y,-X SYMM -Z,-Y,+X SFAC C H Co N UNIT 96 120 12 160 DFIX 1.55 0.01 C3 C2 DFIX 1.337 0.01 N1 C2 DFIX 1.387 0.01 C1 N1 EADP C1 C2 N1 DFIX 2.175 0.01 C1 C2 FLAT C1 C2 N1 C3 RIGU C3 C2 EADP N15 N13 EADP N4 N5 DFIX 1.08 N9 N8 DFIX 1.08 N4 N5 EADP N3 N2 EADP N6 N7 EADP N9 N8 DFIX 1.09 N8 N9 L.S. 10 0 0 PLAN 5 SIZE 0.09 0.1 0.14 CONF BOND list 4 MORE -1 BOND $H fmap 2 53 acta REM REM REM WGHT 0.170800 9.600500 FVAR 0.14009 CO1 3 0.500000 0.250000 0.000000 10.25000 0.04165 0.04028 = 0.04165 0.00000 0.00000 0.00000 N1 4 0.585059 0.320093 0.042552 11.00000 0.03582 0.03622 = 0.04575 -0.00356 -0.01045 -0.00522 C2 1 0.632147 0.367853 -0.002230 10.50000 0.03582 0.03622 = 0.04575 -0.00356 -0.01045 -0.00522 C1 1 0.602525 0.339135 0.121696 11.00000 0.03582 0.03622 = 0.04575 -0.00356 -0.01045 -0.00522 AFIX 43 1.0770 H1 2 0.575005 0.312663 0.174301 11.00000 -1.20000 AFIX 0 C3 1 0.628959 0.371041 -0.095279 10.50000 0.04483 0.04483 = 0.05267 0.01179 -0.01179 -0.00851 PART -1 AFIX 33 1.0830 H3A 2 0.585750 0.327125 -0.117117 10.50000 -1.50000 H3B 2 0.610809 0.430847 -0.114421 10.50000 -1.50000 H3C 2 0.688080 0.357390 -0.119587 10.50000 -1.50000 AFIX 0 PART 0 N2 4 0.500000 0.500000 0.000000 10.08333 0.06609 N5 4 0.500000 0.500000 -0.231964 10.25000 0.11963 PART 1 N8 4 0.784838 0.215162 0.078425 10.50000 0.12645 PART 0 N3 4 0.500000 0.500000 -0.038831 10.16667 0.06609 PART 1 N9 4 0.762354 0.237646 0.025363 10.50000 0.12645 PART 0 N6 4 0.743117 0.256883 -0.256883 10.05555 0.06390 N4 4 0.544566 0.455434 -0.228174 10.25000 0.11963 N11 4 0.564616 0.435384 -0.435384 10.08333 0.08315 PART 1 N12 4 0.588501 0.411499 -0.465183 10.08333 0.09314 PART 0 N7 4 0.765173 0.234827 -0.234827 10.11112 0.06390 N13 4 0.875236 0.124764 -0.124764 10.08333 0.06873 PART 2 N10 4 0.575994 0.424006 -0.392379 10.08333 0.04260 PART 0 N15 4 0.839485 0.118205 -0.118205 10.08335 0.06873 HKLF 4 REM zif67_ln2_2900_a.res in I-43m REM wR2 = 0.2121, GooF = S = 1.151, Restrained GooF = 1.172 for all data REM R1 = 0.0796 for 346 Fo > 4sig(Fo) and 0.0844 for all 373 data REM 49 parameters refined using 11 restraints END WGHT 0.1708 9.6013 REM Highest difference peak 0.747, deepest hole -0.834, 1-sigma level 0.135 Q1 1 0.5000 0.5000 -0.2413 10.25000 0.05 0.75 Q2 1 0.7506 0.2494 -0.2215 10.50000 0.05 0.68 Q3 1 0.7540 0.2460 -0.2753 10.50000 0.05 0.65 Q4 1 0.8427 0.1363 -0.1193 11.00000 0.05 0.62 Q5 1 0.7792 0.2022 0.0449 11.00000 0.05 0.59 REM The information below was added by Olex2. REM REM R1 = 0.0796 for 346 Fo > 4sig(Fo) and 0.0844 for all 16850 data REM 49 parameters refined using n/a restraints REM Highest difference peak 0.75, deepest hole -0.83 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0844 REM R1_gt = 0.0796 REM wR_ref = 0.2121 REM GOOF = 1.151 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 16850 REM Reflections_gt = 346 REM Parameters = 49 REM Hole = -0.83 REM Peak = 0.75 REM Flack = 0.088(18) ; _cod_data_source_file d3ce00979c2.cif _cod_data_source_block zif67_ln2_2900 _cod_original_cell_volume 4548.2(2) _cod_database_code 7247779 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'Co C8 H10 N4' _chemical_oxdiff_usercomment 'ZIF67 @ 2.9 GPa in LN2' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.903 _shelx_estimated_absorpt_t_min 0.855 _diffrn_orient_matrix_axis[1] matrixX _diffrn_orient_matrix_axis[2] matrixY _diffrn_orient_matrix_axis[3] matrixZ _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances C3-C2 1.55 with sigma of 0.01 N1-C2 1.337 with sigma of 0.01 C1-N1 1.387 with sigma of 0.01 C1-C2 2.175 with sigma of 0.01 N9-N8 1.08 with sigma of 0.02 N4-N5 1.08 with sigma of 0.02 N8-N9 1.09 with sigma of 0.02 3. Restrained planarity C1, C2, N1, C3 with sigma of 0.1 4. Uiso/Uaniso restraints and constraints Uanis(C1) = Uanis(C2) = Uanis(N1) Uiso(N15) = Uiso(N13) Uiso(N4) = Uiso(N5) Uiso(N3) = Uiso(N2) Uiso(N6) = Uiso(N7) Uiso(N9) = Uiso(N8) 5. Rigid body (RIGU) restrains C3, C2 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 6. Others Fixed Sof: H3A(0.5) H3B(0.5) H3C(0.5) N2(0.083333) N3(0.166667) N6(0.05555) N4(0.25) N11(0.083333) N12(0.083333) N7(0.11112) N13(0.083333) N10(0.083333) N15(0.08335) 7.a Me refined with riding coordinates: C3(H3A,H3B,H3C) 7.b Aromatic/amide H refined with riding coordinates: C1(H1) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 15.828 _oxdiff_exptl_absorpt_empirical_full_min 0.726 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, z' '-y, -x, z' 'y, -x, -z' '-y, x, -z' 'x, z, y' '-x, z, -y' '-x, -z, y' 'x, -z, -y' 'z, y, x' 'z, -y, -x' '-z, y, -x' '-z, -y, x' 'x+1/2, y+1/2, z+1/2' '-x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' 'z+1/2, x+1/2, y+1/2' 'z+1/2, -x+1/2, -y+1/2' '-z+1/2, -x+1/2, y+1/2' '-z+1/2, x+1/2, -y+1/2' 'y+1/2, z+1/2, x+1/2' '-y+1/2, z+1/2, -x+1/2' 'y+1/2, -z+1/2, -x+1/2' '-y+1/2, -z+1/2, x+1/2' 'y+1/2, x+1/2, z+1/2' '-y+1/2, -x+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-y+1/2, x+1/2, -z+1/2' 'x+1/2, z+1/2, y+1/2' '-x+1/2, z+1/2, -y+1/2' '-x+1/2, -z+1/2, y+1/2' 'x+1/2, -z+1/2, -y+1/2' 'z+1/2, y+1/2, x+1/2' 'z+1/2, -y+1/2, -x+1/2' '-z+1/2, y+1/2, -x+1/2' '-z+1/2, -y+1/2, x+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co1 Co 0.500000 0.250000 0.000000 0.041(2) Uani 1 4 d S T P . . N1 N 0.5851(7) 0.3201(7) 0.0426(7) 0.039(3) Uani 1 1 d D . . . . C2 C 0.6321(7) 0.3679(7) -0.0022(9) 0.039(3) Uani 1 2 d DS T P . . C1 C 0.6025(10) 0.3391(11) 0.1217(7) 0.039(3) Uani 1 1 d D . . . . H1 H 0.575005 0.312663 0.174301 0.047 Uiso 1 1 calc R U . . . C3 C 0.6290(11) 0.3710(11) -0.0953(11) 0.047(7) Uani 1 2 d DS T P . . H3A H 0.585750 0.327125 -0.117117 0.071 Uiso 0.5 1 calc R U P A -1 H3B H 0.610809 0.430847 -0.114421 0.071 Uiso 0.5 1 calc R U P A -1 H3C H 0.688080 0.357390 -0.119587 0.071 Uiso 0.5 1 calc R U P A -1 N2 N 0.500000 0.500000 0.000000 0.066(10) Uiso 0.6666 8 d S . P . . N5 N 0.500000 0.500000 -0.232(3) 0.120(14) Uiso 1 4 d DS . P . . N8 N 0.7848(15) 0.2152(15) 0.078(2) 0.126(9) Uiso 1 2 d DS . P B 1 N3 N 0.500000 0.500000 -0.039(2) 0.066(10) Uiso 0.6667 4 d S . P . . N9 N 0.7624(15) 0.2376(15) 0.025(2) 0.126(9) Uiso 1 2 d DS . P B 1 N6 N 0.743(5) 0.257(5) -0.257(5) 0.064(14) Uiso 0.3333 6 d S . P . . N4 N 0.5446(12) 0.4554(12) -0.228(4) 0.120(14) Uiso 0.5 2 d DS . P . . N11 N 0.565(6) 0.435(6) -0.435(6) 0.08(4) Uiso 0.5 6 d S . P . . N12 N 0.589(9) 0.411(9) -0.465(12) 0.09(8) Uiso 0.1667 2 d S . P . 1 N7 N 0.765(2) 0.235(2) -0.235(2) 0.064(14) Uiso 0.6667 6 d S . P . . N13 N 0.875(5) 0.125(5) -0.125(5) 0.07(3) Uiso 0.5 6 d S . P . . N10 N 0.576(5) 0.424(5) -0.392(9) 0.04(6) Uiso 0.1667 2 d S . P . 2 N15 N 0.839(10) 0.118(7) -0.118(7) 0.07(3) Uiso 0.1667 2 d S . P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Co1 0.042(2) 0.040(3) 0.042(2) 0.000 0.000 0.000 N1 0.036(6) 0.036(7) 0.046(6) -0.004(5) -0.010(5) -0.005(5) C2 0.036(6) 0.036(7) 0.046(6) -0.004(5) -0.010(5) -0.005(5) C1 0.036(6) 0.036(7) 0.046(6) -0.004(5) -0.010(5) -0.005(5) C3 0.045(11) 0.045(11) 0.053(10) 0.012(8) -0.012(8) -0.009(16) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _axis.id _axis.type _axis.equipment _axis.parity _axis.depends_on _axis.zero _axis.vector[1] _axis.vector[2] _axis.vector[3] source . source . . . 1.00000000 0.00000000 0.00003403 omega rotation goniometer -1 . 0.12240000 0.00000000 0.00000000 1.00000000 kappa rotation goniometer -1 omega 0.28425000 -0.76560404 0.00000000 0.64331210 phi rotation goniometer -1 kappa . -0.00006266 0.00000000 1.00000000 theta rotation goniometer -1 . 0.19892000 0.00000000 0.00000000 1.00000000 matrixX general general . phi . 1.00000000 0.00000000 0.00000000 matrixY general general . phi . 0.00000000 1.00000000 0.00000000 matrixZ general general . phi . 0.00000000 0.00000000 1.00000000 dacX translation general . phi . 0.00000000 1.00000000 0.00000000 dacY translation general . phi . -1.00000000 0.00000000 0.00000000 dacZ translation general . phi . 0.00000000 0.00000000 1.00000000 loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u 0 2 2 121.79 8.1 -2 -2 0 131.49 7.8 0 -2 2 128.79 7.1 0 -2 2 120.89 7 0 2 2 126.69 7.7 0 2 -2 127.99 7.7 0 2 -2 126.09 7.1 0 -2 -2 127.99 7.1 0 -2 2 125.79 7.3 0 2 2 124.29 7.7 2 2 0 131.59 6.9 2 0 2 131.19 7.2 0 -2 -2 126.99 7.4 2 2 0 148.99 8 0 2 2 131.19 7.1 -2 -2 0 120.99 7.2 0 2 -2 126.99 7.3 0 2 -2 130.39 6.7 0 2 -2 119.79 7.3 0 2 -2 124.09 7.7 0 -2 -2 122.79 7.2 0 -2 -2 132.19 6.7 -2 -2 0 119.19 7 -2 -2 0 133.29 6.8 0 -2 -2 125.19 8.1 0 -2 2 125.69 7.7 0 -2 2 123.09 7.2 -2 0 -2 140.29 7.6 0 -2 2 126.39 6.8 0 2 -2 122.99 7.2 0 -2 -2 124.29 7.2 2 0 2 138.49 7.6 2 0 2 129.09 7.3 -2 0 -2 134.89 7.3 0 -2 -2 128.59 7.3 2 2 0 122.09 7 0 -2 2 133.59 7.2 0 -2 -2 124.99 7.6 0 -2 -2 126.39 7.4 0 2 -2 127.39 7.2 0 2 -2 125.39 7.6 -2 -2 0 122.99 7.9 0 -2 2 129.89 7.5 0 2 2 137.59 7.2 -2 -2 0 125.79 7.7 0 2 2 134.09 6.7 0 -2 2 119.19 7.2 0 2 -2 125.69 7.2 2 2 0 110.29 7.3 -2 -2 0 125.99 7.8 0 2 -2 116.29 7.5 0 -2 2 119.89 7.8 0 -2 2 125.79 7.4 0 2 2 130.49 7.2 0 -2 2 118.29 7.1 2 2 2 2471.65 120.69 -2 -2 2 2290.77 125.99 2 2 2 2287.07 130.29 2 2 2 2399.26 124.79 -2 -2 2 2381.16 129.09 2 2 2 2443.36 124.29 -2 -2 2 2138.29 120.49 2 2 2 2432.56 123.19 -2 -2 2 2286.47 122.69 2 2 2 2292.27 124.69 2 2 2 2364.46 124.29 -2 -2 -2 2459.35 118.99 -2 -2 -2 2678.13 124.29 -2 -2 -2 2461.55 120.29 2 2 -2 2536.85 128.39 -2 -2 -2 2443.96 119.89 2 2 -2 2420.96 123.09 -2 -2 -2 2504.55 127.59 2 2 -2 2327.57 122.89 -2 -2 -2 2408.66 117.79 -2 -2 -2 2396.96 120.99 -2 -2 -2 2377.36 120.79 0 -1 -3 366.66 19.7 -1 -3 0 394.66 20.8 0 -1 3 385.26 19.9 -1 -3 0 371.56 19 0 1 -3 362.86 19 0 1 -3 356.76 19.5 1 3 0 374.96 20.3 0 -1 3 354.56 19.1 -1 -3 0 363.06 18.8 1 3 0 379.56 20.3 1 3 0 388.26 18.9 -1 -3 0 361.66 19.7 0 1 3 383.66 20.8 0 1 -3 368.06 20.4 -1 -3 0 384.86 19.5 0 -1 3 356.16 19.5 -1 -3 0 371.56 20.2 0 -1 3 370.76 18.9 0 1 3 382.26 19.4 0 1 -3 367.26 20.8 1 3 0 390.36 18.9 -1 -3 0 407.76 20.4 0 1 -3 364.66 20 0 1 3 348.27 20 0 -1 -3 366.66 20.3 0 -1 -3 369.06 19.6 0 -1 3 369.26 19.4 0 -1 -3 368.16 19.4 1 3 0 366.56 20 -1 -3 0 365.26 20.1 0 -1 3 362.26 19.8 0 1 -3 375.96 19.5 0 -1 3 371.56 19.8 1 3 0 375.26 19.1 0 1 -3 382.36 20.9 0 1 -3 360.86 19.1 0 1 3 374.36 20.9 0 -1 3 368.96 19.8 1 3 0 374.46 20 1 3 0 390.96 19 0 1 3 389.86 21.2 0 -1 3 366.26 19.1 0 -1 3 354.56 20.8 1 3 0 379.66 20.2 -1 -3 0 366.56 18.9 0 1 -3 359.76 19.2 0 -1 -3 386.86 18.8 0 -1 3 372.56 19.3 1 3 0 363.06 20.4 1 3 0 384.56 19.9 0 1 -3 357.56 20 0 -1 3 375.26 20.8 -1 -3 0 379.36 19.9 0 1 3 371.96 19.4 -1 -3 0 378.46 20.3 -1 -3 0 382.86 19.8 0 -1 3 365.46 19.4 -1 -3 0 379.76 20.3 0 1 -3 371.56 19.3 0 -1 3 369.26 19.5 -1 -3 0 364.86 19 1 3 0 364.26 18.5 0 -1 -3 385.56 21 -1 -3 0 358.56 19.2 -1 -3 0 350.96 20.1 0 1 3 377.46 19.7 0 -1 -3 382.26 20 0 1 -3 376.26 18.8 0 1 -3 370.96 19.2 0 1 3 376.26 19.3 1 3 0 377.76 19.2 1 0 3 386.46 19.5 1 0 3 380.36 20 -1 0 3 377.26 20.8 0 -3 1 394.16 20.1 1 0 -3 371.46 18.9 0 -3 1 387.26 20.7 0 3 1 428.46 19.7 0 -3 1 383.66 21 -1 0 -3 381.16 20.1 1 0 -3 377.26 22 1 0 3 387.86 21.4 -1 0 -3 367.06 20.2 0 3 -1 379.76 20.1 0 3 -1 384.66 20.6 0 3 -1 396.16 19.7 0 -3 1 372.16 19.8 -1 0 -3 374.56 19.4 -1 0 -3 378.56 19.2 1 0 3 392.76 19.8 0 -3 1 365.96 20.7 1 0 -3 386.76 21.5 1 0 3 384.86 19.4 -1 0 -3 382.76 19.5 0 -3 -1 390.66 21.6 1 0 3 385.16 19.7 1 0 3 387.06 19.9 0 3 -1 385.06 19.8 0 3 -1 374.96 20.8 1 0 -3 369.46 20.4 1 0 3 388.76 20.8 0 -3 -1 389.06 20.8 -1 0 -3 387.16 20 1 0 3 362.76 20.3 0 3 1 402.96 19.7 0 3 -1 378.76 21.1 -1 0 -3 382.76 20.7 -1 0 3 431.16 20.4 0 -3 -1 378.96 20.2 0 -3 1 381.96 21.1 0 -3 1 356.26 19.4 0 3 -1 383.76 20.3 0 -3 -1 374.96 19.8 -1 0 -3 393.76 20.2 1 0 -3 392.16 21.1 -1 0 3 409.06 22.2 0 -3 -1 356.46 20.5 -1 0 -3 372.66 20.6 0 -3 1 378.76 20.8 0 3 1 387.26 20.9 1 0 3 367.96 19.3 -1 0 -3 381.36 20.2 1 0 3 372.46 20.3 0 -3 -1 410.26 19.8 1 0 3 348.37 19.6 1 2 3 75.49 5.3 1 2 3 78.89 5.2 1 2 3 84.99 6.4 1 2 3 81.89 4.9 2 3 1 79.19 5.2 -2 -3 1 83.09 5.8 -1 -2 3 79.39 5.5 -1 -2 3 73.89 5.6 1 -2 -3 77.99 5.8 -2 -3 1 83.79 5.6 -2 -3 1 76.69 6 2 3 1 79.09 5.7 -1 2 -3 80.19 5.6 -1 -2 3 77.29 4.9 2 3 1 82.59 5.3 2 3 1 79.19 4.7 -1 -2 3 76.09 5.4 -1 -2 3 76.49 5.4 -1 -2 3 86.39 6 -1 2 -3 75.69 5.4 1 2 3 82.19 5.2 -1 2 -3 81.89 5.5 2 3 1 81.39 5.3 -1 2 -3 79.19 5.4 2 3 1 83.79 5 -2 -3 1 79.59 5.2 -2 -3 1 79.69 5.8 1 2 3 79.99 5.3 -1 -2 3 81.29 5.4 -2 -3 1 80.19 5.7 -1 2 -3 84.59 5.5 -1 2 -3 82.09 5.3 -1 2 -3 84.09 5.4 -2 -3 1 77.49 5.6 -1 2 -3 75.19 5.1 -2 -3 1 81.49 5.3 -2 -3 1 87.09 5.3 -1 2 -3 80.89 6.1 -2 -3 1 79.19 5.4 2 3 1 75.69 5.7 -1 -2 3 80.99 5.4 1 2 3 84.59 4.9 2 3 1 81.19 5.7 -2 -3 1 80.69 4.8 -1 2 -3 81.89 5.1 1 2 3 81.69 5.2 3 1 2 85.09 5.7 -1 -2 3 73.69 5.4 -1 -2 3 78.09 5.3 -2 -3 1 77.59 5.7 -1 2 -3 83.99 6.2 -1 -2 3 70.49 5.5 2 3 1 81.09 5.6 -2 -3 1 91.19 5.5 1 2 3 81.19 5.7 1 2 3 78.09 5.3 -1 -2 3 83.99 5.7 -1 -2 -3 92.99 6.8 -2 -3 -1 87.19 5.9 -2 -3 -1 95.29 5.5 -2 -3 -1 91.99 6 1 2 -3 90.39 5.2 -2 -3 -1 92.19 4.9 -2 -3 -1 88.79 5.2 -3 -1 -2 75.69 6.2 2 3 -1 99.39 6 2 3 -1 91.09 5.5 -1 -2 -3 87.79 5.1 1 2 -3 90.59 5.1 -1 -2 -3 100.99 5.9 1 -2 3 95.29 5.5 2 3 -1 85.29 5.7 1 2 -3 92.39 5.7 2 3 -1 88.99 5.6 1 -2 3 90.39 5.2 -1 -2 -3 90.79 5.6 1 2 -3 95.79 6.4 2 3 -1 86.09 5.9 1 -2 3 97.69 5.8 2 3 -1 88.19 5 2 3 -1 92.79 6 1 2 -3 91.49 5.7 -1 -2 -3 93.59 5.4 1 -2 3 94.29 5.6 1 -2 3 91.19 5.3 1 -2 3 91.29 6.3 -2 -3 -1 89.19 5.7 2 3 -1 89.09 6.2 2 3 -1 95.59 6.2 1 -2 3 88.59 5.3 1 2 -3 86.39 5.1 -2 -3 -1 87.39 6 -1 -2 -3 89.39 5.5 -2 -3 -1 93.89 5.8 -1 -2 -3 96.79 5.6 1 2 -3 85.09 5.7 -3 -1 -2 69.99 6 -2 -3 -1 99.19 5.7 -1 -2 -3 92.19 5.9 -1 -2 -3 92.79 5.4 1 -2 3 92.39 5.2 -2 -3 -1 89.89 5.4 -2 -3 -1 90.99 5 -2 -3 -1 88.79 6.5 1 2 -3 88.39 5.7 1 2 -3 92.19 5.9 -1 -2 -3 93.89 5.6 -1 -2 -3 89.09 5.1 2 3 -1 98.59 5.3 -2 -3 -1 90.99 5.8 -3 -1 -2 88.69 5.8 -1 -2 -3 93.29 5.9 -1 -2 -3 94.39 5.3 2 3 -1 91.59 6 1 -2 3 92.09 5.5 1 2 -3 85.99 5.6 -2 -3 -1 91.39 5.5 -1 -2 -3 96.29 5.6 -1 -3 2 77.49 5.4 -2 1 -3 71.99 5.4 2 1 3 80.89 6 -1 3 -2 78.09 5.5 2 1 3 78.19 5.5 1 3 2 85.79 6.5 1 3 2 80.69 6.2 -1 3 -2 76.39 5.4 1 3 2 84.59 5.2 -1 3 -2 77.69 6 3 2 1 83.29 6 -2 1 -3 77.79 5.3 2 1 3 78.19 5.6 -1 -3 2 79.69 5.6 -1 3 -2 82.49 6.1 -1 -3 2 76.99 5.8 3 2 1 71.19 6 2 1 3 86.19 5.1 -2 1 -3 74.89 5.1 2 1 3 82.89 5.2 1 3 2 80.09 5.3 1 3 2 79.69 5.1 -1 3 -2 80.89 5.1 -2 1 -3 75.09 5.5 1 3 2 83.99 5.7 -1 3 -2 73.89 5.3 3 2 1 78.29 5.8 -1 -3 2 76.59 5.3 -1 -3 2 73.39 5.8 -1 -3 2 78.59 5.2 1 3 2 78.89 5.1 2 1 3 77.49 5 2 1 3 80.89 5.5 -1 -3 2 96.39 6.1 2 1 3 81.79 5.4 -1 -3 2 87.09 5.5 2 1 3 91.59 5.7 1 3 2 81.09 5.4 1 3 2 81.49 5.2 1 3 2 80.99 5.6 -1 3 -2 87.59 6.1 -1 -3 2 75.59 5 2 1 3 78.39 5.1 -1 3 -2 74.09 5 -1 -3 2 81.49 5.6 -1 -3 2 77.29 5.8 -1 -3 2 78.49 5.3 -1 -3 2 77.69 5.5 1 3 2 85.19 4.8 -2 -1 3 57.49 7.8 1 3 2 89.99 5.7 -2 1 -3 82.09 6.3 -3 -2 -1 91.59 6 -3 -2 -1 79.49 5.7 1 -3 2 89.19 5.6 -1 -3 -2 93.49 5.9 1 -3 2 95.59 5.3 1 -3 2 92.59 5.3 -1 -3 -2 97.39 5.8 -2 -1 -3 96.39 6.9 1 -3 2 90.19 6.1 1 -3 2 93.39 6.4 -1 -3 -2 88.79 5.2 -1 -3 -2 89.99 5.8 2 -1 3 97.69 5.8 2 -1 3 95.19 5.6 1 3 -2 89.89 6 -2 -1 -3 90.09 5.9 -2 -1 -3 88.89 5.8 -2 -1 -3 87.49 5.8 2 -1 3 96.79 5.4 2 -1 3 95.09 6.1 1 3 -2 90.39 6.2 1 3 -2 93.69 5.8 1 -3 2 90.89 5.5 2 -1 3 100.79 6 2 1 -3 94.39 6.7 -1 -3 -2 94.09 5.2 1 3 -2 92.69 6.2 -2 -1 -3 88.09 4.9 -1 -3 -2 91.49 5.9 1 3 -2 88.79 5.5 -2 -1 -3 96.09 5.9 -1 -3 -2 93.89 6.6 -1 -3 -2 92.49 5.4 -2 -1 -3 96.09 5.8 -1 -3 -2 91.09 5.5 1 -3 2 87.69 5.7 -3 -2 -1 102.69 6.7 -1 -3 -2 94.29 5.5 1 -3 2 89.19 6.3 -1 -3 -2 92.79 5.7 -1 -3 -2 94.09 5.6 2 -1 3 88.99 5.5 2 -1 3 93.79 5.6 1 3 -2 86.09 5.1 -2 -1 -3 93.09 6.3 -1 -3 -2 100.69 6 -2 -1 -3 91.49 5.8 1 3 -2 88.29 5.5 -1 -3 -2 99.59 5.7 1 3 -2 88.99 5.7 2 -1 3 91.29 5.5 -1 -3 -2 96.59 6.5 0 -3 -3 123.09 7.7 0 3 -3 131.89 6.9 -3 -3 0 127.99 8.2 3 0 3 130.09 7.7 3 3 0 127.19 8.2 -3 0 -3 126.29 7.4 0 3 -3 116.39 6.8 0 -3 -3 124.39 8.1 3 3 0 119.79 8.3 0 -3 3 121.49 7.6 0 3 -3 118.89 7 0 -3 3 132.89 8.4 0 -3 3 121.89 7.3 0 -3 3 115.89 7.5 0 -3 -3 123.39 8.9 0 -3 3 120.99 6.8 3 3 0 122.49 8.1 0 -3 3 133.19 7.7 -3 -3 0 125.99 7.2 0 -3 3 124.49 6.7 0 -3 3 120.59 7.8 3 0 3 126.09 7.8 0 3 3 126.59 9.2 0 3 3 126.09 6.9 0 3 -3 127.69 7.4 3 3 0 129.59 8 0 3 -3 124.49 8.2 -3 -3 0 124.89 8.5 0 3 3 128.79 7.4 0 -3 3 129.29 8 -3 -3 0 125.69 7.7 -3 -3 0 131.89 8.1 0 3 -3 118.19 8.3 3 3 0 122.19 7.9 3 3 0 125.49 7.5 0 3 -3 121.79 7.9 0 -3 -3 125.79 7.3 0 -3 3 119.89 6.8 0 -3 3 118.99 7.3 0 3 -3 121.99 7.4 0 3 3 127.69 7.5 0 -3 3 122.29 7.1 0 3 3 133.19 7.4 3 3 0 126.69 8.1 0 -3 3 121.39 6.8 0 -3 3 119.09 8.2 0 3 -3 128.49 7.8 0 3 -3 123.29 7.7 0 3 3 115.19 8.2 3 0 3 138.49 8.3 0 -3 -3 113.79 7.8 -3 -3 0 132.39 8.6 0 -3 3 125.09 7.6 0 -3 3 121.69 8.1 0 -3 -3 130.69 6.8 0 3 3 127.49 8.1 0 3 -3 119.29 7.7 0 -3 -3 122.69 7.8 2 3 3 461.85 22.8 3 3 2 458.95 23.1 2 3 3 441.66 22.3 -2 3 -3 424.16 23.5 2 3 3 462.15 24 3 2 3 466.15 23.5 3 2 3 479.75 22.8 -3 -3 2 458.75 22.7 3 2 3 443.56 22.6 -2 -3 3 431.36 24 2 3 3 459.05 22.8 3 3 2 458.25 24.1 3 3 2 466.55 22.9 -2 -3 3 429.46 23.1 3 3 2 469.35 23.3 3 3 2 477.75 22.5 3 2 3 458.25 21.9 3 2 3 446.36 23 -2 -3 3 426.56 22.6 -2 3 -3 482.25 22.6 3 2 3 471.35 23.6 2 3 3 464.95 24.2 3 3 2 461.25 22.7 -2 3 -3 485.85 23 -2 -3 3 451.35 23.3 3 3 2 462.35 23.4 3 3 2 451.75 22.7 2 3 3 456.25 23 -3 -3 2 442.66 24.2 2 3 3 442.16 23.2 -2 -3 3 439.76 23 -2 3 -3 444.36 22.5 -3 -3 2 430.36 24.7 2 3 3 435.66 22.5 -2 -3 3 457.15 23.2 3 2 3 473.95 22.8 2 3 3 451.25 22.5 -2 -3 3 420.16 22.9 -2 3 -3 461.05 22.9 3 2 3 471.75 24 -2 -3 3 442.36 22.9 2 3 3 445.26 22.5 -2 -3 3 448.06 22.6 -3 -3 2 442.26 23.7 2 3 3 442.26 22.6 2 3 3 457.85 22.6 -2 -3 -3 444.96 23.6 -3 -2 -3 470.25 26.3 -2 -3 -3 445.56 24.5 2 -3 3 414.86 24.2 -3 -3 -2 480.75 25 -3 -3 -2 475.15 24.4 -3 -3 -2 486.45 25.6 -2 -3 -3 447.16 24.9 -2 -3 -3 461.05 24.5 2 3 -3 457.65 25.9 -2 -3 -3 445.66 24.4 2 3 -3 450.15 24.1 2 3 -3 469.95 25.6 -3 -2 -3 459.95 24.3 -3 -2 -3 472.05 24.7 -2 -3 -3 438.66 24.9 -3 -3 -2 477.75 26.3 3 3 -2 500.05 26.7 -2 -3 -3 437.46 25 3 3 -2 434.26 25.4 2 3 -3 459.45 25.6 -2 -3 -3 463.55 24.8 3 3 -2 448.26 25.4 -3 -2 -3 496.35 25.1 -3 -3 -2 465.55 24.9 -3 -3 -2 482.05 25.2 -2 -3 -3 476.85 25 -2 -3 -3 447.46 24.2 -2 -3 -3 439.36 25.3 -2 -3 -3 475.05 24.4 -3 -3 -2 459.35 24.3 2 -3 3 435.86 24.5 3 2 -3 433.26 26.2 2 3 -3 443.16 25.4 2 -3 3 475.85 27.3 -3 -3 -2 463.35 26.4 -2 -3 -3 483.95 27 2 3 -3 450.95 24.9 -2 -3 -3 473.45 24.7 0 4 0 704.03 33.3 0 0 4 644.94 31.4 0 0 4 666.73 31.2 0 0 4 631.04 31.9 0 0 -4 669.63 31.3 0 -4 0 667.13 32.3 0 0 4 666.43 31.2 0 -4 0 633.74 33 0 4 0 666.03 31.2 0 0 4 667.83 34.1 0 -4 0 652.13 32.7 0 0 -4 636.84 31.6 0 0 -4 637.64 32.3 0 4 0 644.64 32.9 0 0 4 626.24 30.4 0 0 4 627.44 31.8 0 0 -4 640.24 31.2 0 -4 0 641.64 33 0 0 4 650.63 32.1 0 0 -4 632.14 30.8 0 0 -4 608.94 31.8 0 4 0 654.13 32.5 0 0 -4 649.04 31.5 0 0 4 672.93 32.3 0 0 -4 639.14 31.9 0 0 4 630.74 31.5 0 0 -4 619.24 30.5 0 0 4 612.24 32.3 0 -4 0 626.54 31 0 4 0 636.24 31.5 0 0 -4 630.94 32.9 0 4 0 627.74 32 0 -4 0 669.33 32.3 0 -4 0 629.24 32.4 0 0 -4 638.24 33.5 0 0 -4 650.73 33 0 0 4 618.04 31.6 0 0 4 648.44 31.6 0 0 4 641.74 31.9 0 -4 0 654.93 31.5 0 4 0 568.94 31.5 0 4 0 638.74 32.8 0 0 -4 620.34 32.1 0 -4 0 664.53 33.1 0 -2 4 17.1 2.4 2 4 0 16.8 2.6 0 -2 4 14.9 2.1 0 2 -4 17.8 3.2 -2 -4 0 18.5 3 2 4 0 15.7 2.2 2 4 0 16.4 2.9 -2 -4 0 13.7 2.3 0 -2 -4 16.6 3.6 0 2 4 21.1 3.6 0 2 4 16.2 3.9 0 2 -4 14.5 1.9 2 4 0 16 2.2 0 -2 4 17.6 2.2 0 2 -4 14.8 3.1 0 -2 4 16.9 2 0 2 -4 14.3 2.1 -2 -4 0 13 3.2 0 2 -4 17 2.5 0 -2 4 14.5 2.1 0 -2 4 16.9 2.6 0 -2 4 16.4 1.8 0 2 -4 17.7 2.8 0 2 -4 17.2 3 0 2 4 15.3 3 0 -2 -4 13.3 3 2 4 0 16.9 2.4 0 -2 -4 15.6 2.7 0 -2 -4 16.4 2.2 0 2 -4 15.3 2.5 0 -2 -4 16.8 2.7 2 4 0 14.8 2 -2 -4 0 19 2.2 0 2 -4 12.7 2.4 0 2 -4 11.9 2.5 0 2 -4 14.6 2.8 0 2 4 20.1 3.6 0 -2 4 17.3 2.9 0 2 4 17.1 2.7 -2 -4 0 16.2 2.7 -2 -4 0 18.7 2.2 0 -2 -4 13.6 2.6 2 4 0 18.4 2.2 0 -2 4 14.5 2.5 0 2 -4 14.3 2.2 2 4 0 17.7 3 -2 -4 0 15.8 2 0 2 4 17.4 2.7 0 2 -4 14.4 2.7 2 4 0 17.1 2.2 2 4 0 15.5 1.8 0 2 -4 15.8 2.8 2 4 0 17.5 3.6 0 -2 -4 14.5 2.3 -2 -4 0 15.5 2.9 0 2 -4 19.7 2.8 0 -2 4 11.9 2.2 0 -2 -4 22.4 3.7 0 -2 4 16.3 2.7 -2 -4 0 14.8 2.2 -2 -4 0 19.7 2.6 0 2 -4 16 2.7 0 -2 -4 18.6 2.4 0 -2 -4 12.8 2.7 0 2 4 17.3 2.5 -2 -4 0 13.3 2.9 0 -2 4 13.5 2.6 2 4 0 14.6 2.2 0 2 4 18.3 2.8 0 2 4 17.3 2.8 2 4 0 20.3 3.1 -2 -4 0 17.2 2 -2 -4 0 17 2.1 0 2 -4 13.9 2.1 -2 -4 0 17.6 2 0 -2 4 16 2.1 0 -2 4 16.4 2.2 -1 -4 1 139.29 9.3 -1 -4 1 139.49 9.1 -1 -4 1 134.89 9.2 1 1 4 145.19 8 -1 -4 1 136.59 8.9 -1 1 -4 133.09 8.2 1 1 4 142.09 8.4 1 4 1 140.69 9.1 -1 -1 4 136.69 9.4 -1 1 -4 132.39 7.7 1 1 4 143.29 8.6 1 1 4 135.99 9 -1 1 -4 137.79 9 -1 1 -4 129.39 8.8 -1 -4 1 138.69 8.4 1 4 1 143.79 8.3 1 -1 -4 128.89 8.9 -1 -4 1 141.19 9.1 1 -1 -4 151.58 8.5 1 1 4 143.19 8.6 1 -1 -4 148.79 9.7 1 1 4 141.19 9.9 -1 1 -4 134.29 8.1 1 4 1 140.69 8.1 1 1 4 134.79 8.7 -1 4 -1 135.39 7.8 -1 -4 1 135.99 7.9 1 1 4 137.29 8.2 1 1 4 131.29 8.6 1 4 1 140.69 8.4 -1 -1 4 133.89 8.6 1 1 4 140.39 8.7 -1 1 -4 148.19 9.4 -1 1 -4 142.59 8.2 1 4 1 142.89 7.9 -1 -4 1 139.09 8.6 1 1 4 138.59 7.9 -1 1 -4 134.59 8.5 -1 4 -1 137.39 7.9 -1 1 -4 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49 7.9 3 7 -4 48.2 7.2 3 7 -4 49.3 8.5 3 7 -4 58.99 7.7 3 7 -4 50.59 7.2 3 7 -4 47.6 8.2 -4 -3 -7 54.29 6.5 -4 -3 -7 49 4.2 -4 -3 -7 47 5.1 -3 -7 -4 47 6.9 3 7 -4 34.2 6 -4 -3 -7 53.49 7.6 -4 -3 -7 52.99 4.7 3 7 -4 44.6 5.6 -3 -7 -4 50.59 5.5 -3 -7 -4 53.69 6.7 -3 -7 -4 64.99 7.2 4 3 -7 44.8 8.1 -3 -7 -4 51.49 6.9 -4 -3 -7 46.2 4.9 4 -3 7 44.2 6.9 -3 -7 -4 42.5 7.3 4 -3 7 55.99 7.8 -3 -7 -4 46.7 5.6 4 5 7 86.39 6.7 -5 -7 4 72.19 8.9 5 7 4 74.79 5.6 -4 -5 7 77.29 11 4 5 7 76.39 9.3 -5 -7 4 56.99 10.1 7 4 5 99.59 11.1 -4 -5 7 75.59 9.4 -4 -5 7 81.19 12 5 7 4 81.59 8.4 7 4 5 73.89 10.4 -4 -5 7 58.49 11.2 4 5 7 78.59 7.8 5 7 4 74.59 10 -4 -5 7 78.59 12.2 -4 -5 7 64.19 10.5 4 5 7 79.19 11.8 7 4 5 111.99 11.3 4 5 7 77.59 9 7 4 5 85.59 9.9 5 7 4 78.59 9.7 4 5 7 68.49 9.4 -5 -7 4 74.39 9.6 4 5 7 80.19 11.1 5 7 -4 69.69 11.1 -5 -7 -4 90.79 8.9 5 7 -4 83.29 8.3 4 5 -7 69.99 6.5 5 7 -4 74.99 10.3 -4 -5 -7 75.59 10.1 5 7 -4 74.39 8.7 -5 -7 -4 80.39 9 -4 -5 -7 85.39 7.4 -4 -5 -7 76.99 7.1 4 -5 7 64.59 9 4 5 -7 74.29 11 5 7 -4 74.39 6.1 5 7 -4 80.39 9.7 -4 -5 -7 79.59 7.3 -4 -5 -7 87.79 9.2 -4 -5 -7 78.29 7.7 -5 -7 -4 85.49 8.9 4 5 -7 67.69 10 -5 -7 -4 69.99 9.2 -7 -4 -5 103.99 11 -4 -5 -7 76.09 8.8 4 -5 7 89.79 10.2 -5 -7 -4 85.09 7 -5 -7 -4 71.89 8 4 5 -7 82.79 8.1 -5 -7 -4 73.89 5.4 -7 -4 -5 87.19 9.3 -5 0 -7 196.08 12.5 0 -7 5 179.98 10.1 5 0 7 197.28 14.1 0 -7 5 174.08 11.6 0 -7 5 187.38 13 0 7 -5 189.58 13.4 0 7 -5 171.98 14.3 0 -7 -5 189.58 11.8 0 -7 5 193.48 12.9 0 -7 5 186.88 11.7 0 7 5 198.98 14.2 0 -7 -5 190.18 13.3 0 7 5 178.78 13.8 5 0 7 191.28 13.2 0 7 -5 207.08 14.2 0 -7 -5 192.68 10.9 0 7 -5 184.38 12.1 0 -7 5 187.68 13.7 0 -7 5 197.88 14.3 0 7 -5 185.18 13.6 0 7 -5 165.88 10.2 5 0 7 180.98 13.2 0 -7 -5 194.38 13.9 -5 0 -7 197.58 11.4 0 7 5 191.18 14.6 -5 0 -7 197.08 11.7 0 7 5 212.98 19 0 7 5 191.88 16.5 -5 0 -7 192.28 13.5 5 0 7 204.68 12.8 0 -7 5 193.58 13.2 0 -7 -5 195.78 12.7 0 -7 5 188.18 12 0 -7 5 173.98 10.9 -2 -7 5 38.3 5.7 5 2 7 42.7 4.9 5 2 7 42.9 6.8 5 2 7 57.99 7.9 5 2 7 49.4 8.2 -2 -7 5 38.2 6.6 -2 -7 5 42.5 7.9 -2 7 -5 55.09 8.8 2 7 5 49.4 8 -5 2 -7 32.6 6.1 5 2 7 50.79 6.2 2 7 5 52.29 10.1 2 7 5 41.1 4.8 5 2 7 48.3 5.3 -2 -7 5 46.9 6.9 5 2 7 50.59 7.4 -2 -7 5 41 4.9 -2 -7 5 38 6.1 2 7 5 37.4 7.7 2 7 5 46.9 6.9 -2 -7 5 41.7 7.3 -2 -7 5 46 7.5 2 7 5 33.1 6.9 -2 -7 5 40.1 7.7 2 7 5 48.5 9.9 -2 7 -5 38.6 7.9 -2 7 -5 48.7 8.2 -2 -7 5 42.8 6.4 -2 7 -5 34.3 8.1 2 7 -5 51.09 8.8 -2 -7 -5 47.2 6.8 -5 -2 -7 60.19 7.2 -5 -2 -7 55.09 4.7 2 -7 5 38.7 7.3 -5 -2 -7 44.7 5.8 2 7 -5 48.7 8.1 -2 -7 -5 44.2 5.1 2 7 -5 37.2 5.3 -5 -2 -7 47.8 5 -2 -7 -5 44.2 3.7 -2 -7 -5 49.3 5.8 2 7 -5 51.49 8.9 -2 -7 -5 45.8 6.3 2 -7 5 47.7 7.8 -5 -2 -7 49.8 8.4 2 -7 5 45.5 5.5 -5 -2 -7 46.6 8 -2 -7 -5 38.4 5.9 2 -7 5 39.3 5.8 -2 -7 -5 39.5 7.2 -2 -7 -5 51.39 6.3 2 7 -5 43.5 5 -2 -7 -5 49.1 7.7 2 7 -5 30.3 7.6 -2 -7 -5 47.8 6.8 5 4 7 78.59 7.5 5 4 7 76.59 9.6 4 7 5 90.39 10.6 7 5 4 84.09 9.8 -4 -7 5 71.59 10 -4 -7 5 77.09 9.9 4 7 5 82.39 12.3 4 7 5 75.99 5.1 5 4 7 71.89 7.1 7 5 4 71.69 10 7 5 4 85.09 8.9 5 4 7 94.49 7.8 4 7 5 72.79 5.7 4 7 5 74.99 8.5 4 7 5 80.49 10.9 5 4 7 80.79 8.9 7 5 4 97.29 10.7 -4 -7 5 69.59 8.9 4 7 5 77.99 9.2 -5 -4 7 -34.3 30.4 5 4 7 76.29 5.6 5 4 7 83.19 10.7 5 4 7 71.59 6.4 -4 -7 5 67.79 8.1 5 4 7 79.79 7 -4 -7 5 82.29 9.9 7 5 4 90.99 9.7 -4 -7 -5 70.59 9.4 -4 -7 -5 70.89 7.9 -5 -4 -7 81.99 9.4 4 7 -5 72.69 9.4 -7 -5 -4 74.99 5.2 -4 -7 -5 91.29 9.3 -5 -4 -7 75.59 6.1 -5 -4 -7 92.99 9.5 4 7 -5 70.69 7.5 -5 -4 -7 73.09 10.1 4 7 -5 80.29 9.4 5 4 -7 81.09 10.2 -7 -5 -4 73.79 9 4 7 -5 67.09 5 -4 -7 -5 76.99 8.7 -4 -7 -5 77.19 8.9 -7 -5 -4 89.79 10.2 -5 -4 -7 84.99 7.1 -5 -4 -7 79.59 5.3 -5 -4 -7 80.89 7.6 -4 -7 -5 81.99 7.4 4 7 -5 96.59 11 4 7 -5 74.69 11.2 5 6 7 45.5 8.4 6 7 5 44.1 9.7 7 5 6 45.8 6.4 7 5 6 44.2 9.2 5 6 7 46 5.8 5 6 7 53.99 12 5 6 7 45.1 5 -5 -6 7 31 14.4 7 5 6 43.5 6.7 5 6 7 54.79 7.9 -5 -6 7 53.09 11.4 6 7 5 53.59 9.5 -6 -7 5 42.2 14.5 6 7 5 43.4 3.9 -5 -6 7 47.3 14 5 6 7 46.1 11.2 7 5 6 37.8 10.1 -5 -6 7 18.7 24.2 -5 -6 7 45.2 12.5 7 5 6 41.2 8.1 6 7 5 48.9 8.9 6 7 5 53.79 11.3 -5 -6 7 43.8 9.7 -6 -7 5 33.2 15 7 5 6 51.79 9.1 7 5 6 32.5 10.8 6 7 5 35.2 3.9 6 7 5 44.1 10 5 6 7 50.99 9.7 6 7 -5 45.4 8 -5 -6 -7 41 8.7 6 7 -5 58.59 11.2 5 6 -7 50.99 8.5 -6 -7 -5 52.59 8.7 5 6 -7 25.3 10.6 -6 -7 -5 37.7 8.2 -7 -5 -6 54.99 9.6 -5 -6 -7 43.6 7.2 -5 -6 -7 39.9 8.8 -6 -7 -5 58.29 9.4 6 7 -5 56.39 10.5 -6 -7 -5 36.6 3.8 -5 -6 -7 44.6 10 -7 -5 -6 46.3 8.1 6 7 -5 44.7 11.9 -7 -5 -6 44 8 -6 -7 -5 35.8 5.9 5 6 -7 20.4 5.9 7 6 1 143.49 12.3 -1 -7 6 137.39 8.8 -1 7 -6 140.79 12.4 -1 7 -6 152.08 12.1 1 7 6 151.48 9.1 6 1 7 150.48 12.2 -1 7 -6 133.19 8.9 1 7 6 157.18 11.9 -1 -7 6 139.79 10.1 -1 -7 6 144.99 9.4 -1 -7 6 151.98 11.8 1 7 6 139.09 14.6 1 7 6 171.38 15.3 -1 7 -6 163.88 13.8 6 1 7 178.98 12.8 -1 -7 6 151.58 11.5 7 6 1 158.78 12.9 -1 7 -6 148.99 12.5 -1 7 -6 151.38 12.7 -1 7 -6 124.59 9.7 -1 -7 6 155.28 11.6 -1 -7 6 137.89 9.9 -1 -7 6 145.09 10.4 -1 -7 6 153.88 12.5 1 7 6 142.59 11.9 1 7 6 155.38 12.5 -1 -7 6 156.88 12.3 7 6 1 145.59 12.5 1 7 -6 134.49 9.6 -1 -7 -6 147.29 10.7 -6 -1 -7 159.48 9.5 1 7 -6 156.18 13.2 1 -7 6 150.68 10.2 1 -7 6 147.39 12.6 1 -7 6 146.29 9.1 1 -7 6 133.19 8.7 -1 -7 -6 141.69 10.5 -7 -6 -1 141.09 10.9 1 -7 6 151.78 12.8 -6 -1 -7 159.68 12 1 7 -6 158.88 12.9 -1 -7 -6 162.68 11.1 -1 -7 -6 135.79 11.7 1 7 -6 142.19 12.2 1 -7 6 128.09 10.7 -1 -7 -6 145.79 9.3 -1 -7 -6 134.99 9.6 1 -7 6 154.78 11.6 1 7 -6 126.09 8.9 -1 -7 -6 137.69 12.9 1 -7 6 143.39 8.2 1 -7 6 162.18 11.7 1 -7 6 148.19 10.9 1 -7 6 147.49 8.5 7 6 3 62.59 8.6 6 3 7 71.49 7.8 6 3 7 74.79 9.3 3 7 6 58.19 5 3 7 6 55.49 8.6 3 7 6 78.19 12 -3 -7 6 58.89 9 6 3 7 65.79 6.7 -3 -7 6 57.29 8 7 6 3 66.59 9.6 -3 -7 6 58.39 9.2 3 7 6 48.9 9.1 -3 7 -6 61.49 9.6 7 6 3 69.19 9.1 6 3 7 72.09 10 -3 -7 6 60.49 6.5 -3 -7 6 59.09 8.4 6 3 7 74.29 7 -3 7 -6 62.79 9.4 3 7 6 62.99 8.1 3 7 6 61.69 10.9 6 3 7 70.79 7.9 -3 -7 6 65.49 12 -7 -6 -3 73.09 9.1 3 -7 6 58.99 9.2 3 7 -6 60.19 8.2 -7 -6 -3 64.59 5.3 3 7 -6 53.89 4.6 -3 -7 -6 70.39 8 -3 -7 -6 59.29 8.8 -7 -6 -3 70.79 10.6 3 7 -6 56.79 10.3 3 -7 6 47.8 7.6 3 7 -6 51.59 5.7 3 7 -6 44.5 8.8 -3 -7 -6 69.19 9.4 -6 -3 -7 57.19 9.2 -3 -7 -6 64.79 7.9 -3 -7 -6 73.59 7.5 -3 -7 -6 71.39 6.9 -3 -7 -6 56.49 5.1 5 7 6 48.5 8.7 6 5 7 37.4 5.9 6 5 7 40.2 6 -5 -7 6 42.9 8.4 5 7 6 42.4 8.7 5 7 6 47.1 10 6 5 7 45.1 9.5 5 7 6 42.1 5.1 5 7 6 35.8 6.8 7 6 5 51.79 9.1 5 7 6 41.7 10.8 6 5 7 43.5 9.3 7 6 5 35.4 11 7 6 5 43.3 9.7 -5 -7 6 37.9 9 6 5 7 41.3 3.8 7 6 5 40 8.9 -5 -7 6 39.3 12.7 5 7 6 59.29 11.5 6 5 7 42.4 8.7 6 5 7 44.3 11.1 7 6 5 26.5 5.5 7 6 5 44.6 9.7 6 5 7 41.7 6 -5 -7 6 34.8 10.3 -5 -7 6 41.4 11.1 5 7 6 52.29 5.5 6 5 7 33.2 7.3 5 7 -6 38.6 9.2 -6 -5 -7 39.3 7 -6 -5 -7 53.59 8.7 -5 -7 -6 40.5 7.7 -6 -5 -7 36.2 3.3 -6 -5 -7 39.1 7 -5 -7 -6 44 7.9 -6 -5 -7 45.9 9.6 5 7 -6 62.29 12 -6 -5 -7 41.3 9.5 -5 -7 -6 38.6 5.2 5 7 -6 54.69 7 5 7 -6 54.99 11.6 -5 -7 -6 46.1 8.4 -7 -6 -5 48 8 -7 -6 -5 45.2 8.5 5 7 -6 46 8.8 -5 -7 -6 45.2 9.2 -5 -7 -6 39.9 9.6 -7 -6 -5 34.5 8.9 7 7 0 4.7 8.5 0 7 -7 -1.9 8.9 0 -7 7 0.5 6.1 0 -7 7 -0.7 7 0 7 7 -5.8 7.7 0 -7 -7 0.3 4 -7 -7 0 17.9 17.6 0 7 7 0.5 14.7 0 -7 7 4 7.1 0 7 7 6.2 8 0 -7 7 -2.7 6.2 -7 -7 0 13.3 7.9 0 -7 7 -2.8 4.4 -7 -7 0 6.2 11.7 0 7 7 -1.6 6.3 0 7 -7 4.6 8.1 0 7 -7 -2.1 7.7 0 7 -7 2.9 6 0 -7 -7 1.6 7.1 0 -7 7 2.1 7.3 0 7 -7 8 7.9 0 7 -7 0.3 5.5 7 7 0 16.1 9.4 -7 -7 0 1.1 9.1 0 7 -7 -1.9 4.6 -7 -7 0 4.5 7.9 7 7 0 -8.1 7.8 0 7 7 -1.5 12.6 0 -7 7 -2.4 3.3 0 -7 -7 3.4 7.8 7 7 0 3.2 4.8 0 7 7 3.5 7.3 0 -7 7 10.6 7 0 -7 -7 3.1 6.7 0 -7 -7 -5.4 6.3 7 7 0 -5.4 6.3 -2 -7 7 194.98 14.5 -2 7 -7 171.08 14.6 2 7 7 204.78 17.9 7 7 2 196.58 15.7 2 7 7 182.18 13.6 2 7 7 202.38 14.4 -2 -7 7 190.78 14.7 7 7 2 181.28 13.4 -2 7 -7 196.98 16.1 2 7 7 203.48 14.7 -2 7 -7 210.28 14.9 -2 -7 7 205.08 13 7 7 2 198.38 16.6 -2 -7 7 200.48 14.8 2 7 7 188.08 15.4 -2 -7 7 201.98 14.9 7 7 2 213.88 16.1 -7 -7 2 252.77 25.7 7 7 2 208.48 13.2 2 7 7 199.28 17.3 -2 7 -7 177.28 12.3 -2 7 -7 194.68 15 2 7 7 189.48 12 -2 -7 7 178.48 13.9 -2 -7 7 206.78 14.3 -2 -7 -7 197.28 13.4 2 7 -7 200.68 13.6 7 7 -2 199.08 15.4 2 7 -7 207.58 16.1 2 -7 7 211.78 11.9 2 -7 7 234.88 16 -2 -7 -7 219.18 14.5 7 7 -2 208.98 15.4 -7 -7 -2 262.07 17.7 -2 -7 -7 217.78 13.7 2 -7 7 219.58 16.6 2 -7 7 191.98 11.5 2 7 -7 223.38 15.8 -2 -7 -7 195.58 13 7 7 -2 223.28 17.1 2 -7 7 199.48 13.6 -7 -7 -2 218.28 12.4 2 -7 7 211.28 12.4 -2 -7 -7 213.38 14.6 -7 -7 -2 201.78 14.1 -7 -7 -2 208.78 12.2 -2 -7 -7 210.98 16.1 -2 -7 -7 198.28 14 -2 -7 -7 199.18 12.6 7 4 7 40.4 7.3 7 4 7 44.8 6.9 -7 -7 4 -1.5 37.1 -4 -7 7 26.7 6.6 -4 -7 7 38.5 10.6 7 4 7 37.4 8.6 4 7 7 35.3 11.2 7 7 4 34.2 5 4 7 7 41.6 8.1 4 7 7 35.8 8.9 7 4 7 28.3 5.2 7 7 4 36.1 9.8 -4 -7 7 51.19 10.2 7 4 7 32.5 9.2 -4 -7 7 31.4 8.1 4 7 7 27.8 8.4 7 7 4 30.4 8.2 7 4 7 38.4 9.3 -4 -7 7 17.2 8.4 7 4 7 29.4 9.5 7 7 4 35.9 9.8 4 7 7 40.2 12.4 -7 -7 4 11 43.6 -7 -7 -4 15.8 7.1 -7 -7 -4 21.6 5.6 -7 -4 -7 15.2 7.6 7 7 -4 30.5 10.5 -4 -7 -7 24 7.7 4 7 -7 19.5 5.3 -4 -7 -7 14 7 -7 -7 -4 25.9 8.6 -7 -7 -4 20.1 8.5 -4 -7 -7 32.6 9.9 -7 -4 -7 28.1 9.4 -4 -7 -7 34.1 5.9 -4 -7 -7 32.5 8.4 7 7 -4 4.6 8.8 4 7 -7 22.6 7.6 4 7 -7 26.1 10.1 4 7 -7 15.1 3.8 7 7 -4 12.3 8.4 6 7 7 12.8 11.8 -6 -7 7 25.1 17.9 6 7 7 26.6 10.6 7 6 7 39.9 11 -7 -7 6 -34.5 105.09 7 7 6 22.4 11.7 7 6 7 22.1 11.5 -7 -7 6 -51.09 71.29 7 6 7 30.9 5.5 -6 -7 7 3.5 14.8 7 7 6 33.4 9.4 7 6 7 23.6 3.1 7 7 6 28.9 4.7 7 7 6 24.3 10 7 6 7 26 9.4 6 7 7 27.2 8.7 7 6 7 25.1 6.9 6 7 7 31.1 9.6 7 6 7 30.4 8.4 -6 -7 7 23.3 19.7 7 7 6 27.1 9.3 7 6 7 31.5 9.8 7 7 6 36.9 11.2 6 7 7 31.8 4.5 7 7 6 20.3 3.2 6 7 -7 2 12.4 -7 -6 -7 28.4 9.3 -7 -7 -6 31.3 9.1 6 7 -7 0.2 7 -7 -7 -6 44.2 8.6 6 7 -7 30.5 9.9 -6 -7 -7 16.9 10.6 7 7 -6 -1.4 9.5 -7 -6 -7 22.3 8.1 -6 -7 -7 29.3 9.5 -7 -7 -6 31.2 10.1 -6 -7 -7 14 7.9 6 7 -7 1.7 11.9 -6 -7 -7 9.5 8.4 -7 -6 -7 33.5 10.8 0 -8 0 2011.7 95.09 0 -8 0 2030.6 94.79 0 0 8 1975.3 92.69 0 0 -8 1912.41 94.29 0 0 8 1880.51 94.29 0 0 -8 1835.42 93.09 0 0 8 1974.3 93.49 0 0 8 1895.61 92.89 0 8 0 2027.8 93.89 0 0 8 1963.3 93.19 0 0 8 1914.31 96.89 0 0 8 2003.2 98.69 0 0 -8 1813.42 93.19 0 -8 0 2000 91.89 0 0 -8 1940.21 90.79 0 -8 0 2060.19 95.49 0 0 8 1963 95.99 0 0 -8 1933.31 92.59 0 0 -8 1911.91 94.59 0 0 -8 1894.11 95.19 0 8 0 2036.2 95.89 0 8 0 1979.8 91.59 0 -8 0 2023.5 93.29 0 8 0 2050.89 95.49 0 0 -8 1838.22 93.19 0 8 0 1946.71 92.69 0 -8 0 1923.41 92.09 0 0 -8 1842.12 92.79 -2 -8 0 72.89 8.3 2 8 0 81.79 8 0 -2 -8 77.49 7.4 0 2 8 72.19 7.8 0 2 8 97.39 14.2 0 -2 -8 74.99 7.3 2 8 0 71.29 7.2 0 -2 8 75.99 5.5 2 8 0 77.69 7.5 0 -2 8 77.09 6.8 0 -2 8 87.59 9.2 0 -2 -8 72.99 8.8 0 2 8 68.69 7.5 -2 -8 0 83.89 6.6 0 2 -8 63.79 8.1 0 -2 8 68.29 8.4 0 2 -8 76.59 8.7 0 -2 8 77.59 6.9 0 -2 -8 85.19 8.2 0 2 8 78.59 9.2 2 8 0 81.29 10.3 0 2 -8 78.59 8 0 2 -8 76.39 7 0 2 8 80.19 5.7 2 8 0 87.69 7 0 -2 8 68.69 6.3 0 2 -8 73.19 5.6 2 8 0 74.99 6.8 0 -2 -8 78.29 8.7 2 8 0 80.39 7.9 -2 -8 0 80.99 7.2 2 8 0 75.59 5.7 0 2 -8 82.49 8.5 0 -2 8 84.99 6.2 0 -2 -8 77.39 9.2 2 8 0 79.29 6.3 0 2 -8 79.19 7.2 0 2 8 76.99 6.9 0 2 8 69.99 11.2 -2 -8 0 75.39 6 2 8 0 74.09 7 -2 -8 0 71.09 6.8 0 2 8 77.89 9 0 2 -8 78.49 8.7 0 2 8 76.99 8.8 -2 -8 0 79.39 8.7 -2 -8 0 70.99 5.8 0 -2 -8 80.19 5.1 0 2 -8 69.19 6 2 8 0 79.59 9.5 0 -2 8 71.39 5.7 2 8 0 85.49 8.3 0 -2 8 73.29 7.6 0 2 -8 66.29 6.6 -4 -8 0 541.65 30.2 0 -4 8 511.75 28.8 0 -4 8 526.35 30.2 4 8 0 559.54 28.1 0 4 -8 533.85 29.5 4 8 0 529.45 28.8 0 4 -8 537.75 31.9 -4 -8 0 553.24 28.9 0 -4 8 545.55 29.2 0 4 -8 517.75 29.6 0 4 -8 510.65 30.5 0 -4 -8 502.95 29.4 0 -4 8 518.85 30.2 0 -4 8 573.64 30.4 4 8 0 555.94 30.7 -4 -8 0 550.24 30.7 0 4 8 547.55 30.9 0 -4 -8 530.65 30.2 0 4 -8 509.65 31.8 -4 -8 0 555.84 31.6 0 4 -8 512.55 31 0 4 8 548.95 35.5 0 4 -8 499.65 27.9 4 8 0 488.65 30 4 8 0 541.45 28.8 0 4 -8 546.05 30.1 0 4 -8 529.75 29 0 4 8 551.84 30.9 4 8 0 545.95 30.3 0 -4 -8 562.14 29.7 -4 -8 0 552.34 28.8 -4 -8 0 501.15 28.7 0 -4 8 536.25 30 0 -4 -8 509.95 31.2 4 8 0 587.14 31.5 4 8 0 534.45 27.7 4 8 0 551.34 28.3 0 -4 8 529.05 29.2 0 -4 8 547.25 32.4 -4 -8 0 521.25 28.6 4 8 0 539.45 32 0 -4 -8 560.44 29.6 0 4 8 526.45 33.4 0 4 8 536.05 28.5 -4 -8 0 535.15 30.8 0 -4 8 513.95 29.5 0 4 8 563.54 31.1 0 -4 8 533.35 30.2 -4 -8 0 518.35 28.4 0 4 8 469.15 30.7 0 4 8 572.94 29.4 0 6 -8 231.98 16.5 0 -6 -8 240.58 16 -6 -8 0 263.97 18 0 -6 8 230.88 13.8 0 -6 -8 253.47 17 -6 -8 0 240.98 15 0 -6 8 242.98 15.5 0 -6 -8 252.27 15.8 0 6 8 249.88 16.6 0 6 -8 232.48 16.4 0 -6 -8 241.48 15.5 0 -6 8 250.67 18.2 0 -6 8 233.28 16.4 -6 -8 0 232.58 14.5 -6 -8 0 234.08 17.4 0 6 -8 232.38 16.6 0 6 -8 235.48 14 0 -6 8 227.38 15.2 0 6 -8 260.07 18.4 0 6 -8 230.58 16.4 0 -6 -8 240.08 18 6 8 0 250.07 17.6 6 8 0 253.87 18.1 0 6 -8 222.68 14.6 6 8 0 214.98 14.2 0 -6 8 234.18 13.8 0 -6 -8 237.38 16.3 6 8 0 248.18 18.3 6 8 0 236.98 18.5 -6 -8 0 235.48 16 0 6 8 231.48 17.3 0 6 -8 229.98 16.4 0 6 8 255.07 15 6 8 0 250.47 14.8 0 6 8 229.98 20.8 6 8 0 238.38 16.1 0 -6 8 231.18 16.1 1 1 8 119.79 11.9 1 1 8 123.99 8.3 -1 1 -8 108.19 9.9 -1 -1 8 114.59 8.9 -1 -8 1 111.09 8.8 1 -1 -8 123.69 9.9 1 8 1 122.79 8.8 1 -1 -8 97.99 9.9 1 8 1 103.39 8.5 -1 -8 1 113.99 10 1 1 8 113.49 8.6 -1 -8 1 111.39 8.4 -1 -1 8 112.99 11.1 -1 -8 1 102.99 7.1 -1 -1 8 115.29 9.1 1 -1 -8 100.19 7.4 -1 1 -8 111.49 9 1 -1 -8 103.69 8.7 -1 -8 1 115.29 10.2 -1 -1 8 112.79 9.6 -1 8 -1 120.09 11.7 -1 1 -8 111.89 9 -1 1 -8 108.19 9.6 -1 1 -8 98.69 8.9 1 8 1 103.49 10.1 1 1 8 120.89 10.3 -1 -1 8 112.09 10 -1 -8 1 110.09 7.6 1 1 8 103.29 9.5 -1 1 -8 115.39 8.2 1 1 8 125.99 9.1 1 8 1 124.59 8.4 1 1 8 109.09 8.5 1 8 1 116.29 11.1 1 8 1 118.49 9.6 1 8 1 124.89 11.8 -1 -8 1 107.89 10.5 1 1 8 110.49 9.4 -1 -1 8 107.19 9.3 -1 -1 8 105.09 11.4 1 -1 -8 106.49 10.3 1 -1 -8 113.79 9.6 -1 1 -8 119.79 9.8 1 8 1 116.19 9.9 1 8 -1 125.09 11.7 -1 1 8 126.49 12.6 1 8 -1 138.99 10.5 1 1 -8 111.39 10.4 1 8 -1 113.99 9.3 1 1 -8 119.79 7.7 1 8 -1 147.39 11.9 1 -1 8 135.59 11.5 1 1 -8 123.29 8.9 1 1 -8 111.39 8.1 1 -1 8 119.69 9.2 1 -1 8 121.69 9.4 -1 -8 -1 133.39 10.3 -1 -1 -8 116.19 10.4 1 -1 8 121.79 10.1 -1 -1 -8 120.19 8.9 1 -1 8 124.99 8.3 1 -1 8 129.19 8.8 1 8 -1 134.19 9.7 1 1 -8 127.49 9.2 -1 1 8 117.19 11.5 1 -1 8 116.79 7.8 -1 -1 -8 119.19 9.5 1 1 -8 119.19 8.2 1 8 -1 128.89 9.9 -1 -8 -1 128.89 8.2 -1 -1 -8 134.29 9.4 -1 -8 -1 136.39 8.9 1 1 -8 115.39 8.6 1 8 -1 123.49 8 1 8 -1 124.09 7.6 -1 -1 -8 119.39 10.3 -1 -1 -8 132.39 10.4 1 -1 8 122.09 8.9 -1 1 8 117.59 10.2 -1 -1 -8 111.69 7.4 1 8 -1 139.19 9.7 -1 -8 -1 131.19 10.7 -1 -8 -1 122.99 7.7 1 1 -8 124.29 10.2 -1 -8 -1 127.59 8.1 -1 1 8 129.89 14 1 -1 8 124.29 10.2 -1 -8 -1 122.69 8.7 -1 1 8 122.99 10.3 1 8 -1 126.19 11.6 -1 -1 -8 127.79 9.1 -1 3 -8 129.49 11.3 1 -3 -8 119.39 10.3 3 8 1 122.39 8.6 1 3 8 122.69 10.2 1 3 8 122.39 8.1 1 3 8 130.09 13.1 -1 -3 8 123.09 8.6 -3 -8 1 123.29 7.7 3 8 1 132.99 10.3 1 3 8 142.89 11.2 -1 3 -8 133.69 10.8 -1 -3 8 114.79 10.6 -3 -8 1 119.59 8.6 3 8 1 113.69 8.2 3 8 1 116.69 11.5 3 8 1 130.39 8.6 3 8 1 127.19 12.6 3 8 1 121.19 9.8 -1 3 -8 114.29 8.8 -1 3 -8 123.49 9.2 1 -3 -8 110.89 8.8 3 8 1 123.89 8.3 -3 -8 1 135.29 10.6 -1 -3 8 134.59 11.2 -1 -3 8 126.09 10 -3 -8 1 132.09 9.4 1 3 8 131.29 11 -1 -3 8 133.99 10.6 -1 -3 8 109.49 9 1 3 8 115.09 7.4 -3 -8 1 112.79 10.3 3 8 1 116.29 9.3 -1 3 -8 122.79 8.7 3 8 1 117.29 8.3 1 -3 -8 112.29 10.2 -1 -3 8 118.19 9.4 1 3 8 120.19 10.4 -1 3 -8 117.09 10 -1 -3 8 114.59 10.8 -1 3 -8 122.79 8.4 1 3 8 114.89 11.8 -1 3 -8 127.69 10 -3 -8 1 118.29 10.9 -3 -8 1 138.39 8.9 1 3 8 111.69 10 -1 -3 8 121.49 9.3 -1 3 -8 129.29 10.9 3 8 1 125.29 8.9 -1 -3 8 118.49 9.1 -3 -8 1 111.19 8 -1 3 -8 113.09 9.5 1 3 8 124.19 9.6 1 3 8 112.89 7.6 -3 -8 -1 115.19 8.8 -1 3 8 153.08 17.6 -3 -8 -1 121.59 9.1 1 3 -8 123.39 10 -1 -3 -8 128.29 10.3 1 3 -8 102.69 8.1 1 3 -8 105.69 10.3 3 8 -1 119.19 9 1 3 -8 124.19 10.9 1 -3 8 115.49 7.9 -3 -8 -1 119.49 10.5 -1 -3 -8 119.49 10.4 1 -3 8 109.99 7.1 3 8 -1 113.19 7.6 3 8 -1 123.09 7.6 1 -3 8 120.29 9.8 -1 -3 -8 103.09 8.6 1 3 -8 120.99 8.9 3 8 -1 118.39 10.3 -3 -8 -1 126.69 8.7 -3 -8 -1 124.79 8.5 3 8 -1 117.49 8.1 3 8 -1 126.09 9.6 1 3 -8 120.39 11 1 -3 8 118.59 8.1 1 -3 8 121.69 8.9 -3 -8 -1 115.79 7.6 3 8 -1 124.09 11.8 -3 -8 -1 132.59 9 1 -3 8 112.69 10.1 -3 -8 -1 118.59 10.7 1 -3 8 117.19 8.1 -3 -8 -1 120.39 10.7 -1 -3 -8 114.79 8.6 -1 3 8 126.09 10.9 -1 3 8 111.79 14 -1 -3 -8 117.39 7.5 -3 -8 -1 122.29 8.4 1 -3 8 114.89 8.9 -3 -8 -1 118.79 7.7 1 -3 8 111.29 8.2 1 3 -8 124.99 9.7 1 3 -8 102.99 9.4 -3 -8 -1 154.48 13.5 1 3 -8 105.09 9 3 8 -1 116.69 9 -1 -3 -8 107.09 7.5 3 8 -1 112.79 11.8 1 3 -8 120.39 8.6 3 8 -1 116.09 10 1 5 8 91.29 10 -1 -5 8 94.79 7.8 1 -5 -8 77.09 10.4 5 8 1 91.09 11.5 5 8 1 87.49 6.4 -1 -5 8 88.59 8.5 -1 5 -8 94.39 9.8 -5 -8 1 106.19 9.8 5 8 1 88.89 7.6 -1 5 -8 95.19 11.2 -1 5 -8 95.09 8.4 -5 -8 1 109.69 10.7 -1 5 -8 95.19 9 5 8 1 102.79 8.1 1 5 8 87.69 6.4 -1 -5 8 84.69 7.4 1 5 8 102.79 9.4 -1 -5 8 91.49 8.3 -1 -5 8 109.19 10 -1 -5 8 98.89 10 5 8 1 95.19 8.7 -1 -5 8 93.09 8.6 -5 -8 1 93.39 9 -1 5 -8 89.69 9.9 5 8 1 88.59 8.3 1 5 8 100.89 10 5 8 1 101.99 10.5 5 8 1 90.49 11.3 5 8 1 93.99 7.8 -1 -5 8 101.69 8.9 1 -5 -8 77.89 9.2 5 8 1 113.79 12 1 5 8 93.19 7.9 -1 5 -8 102.39 10.3 -1 -5 8 102.69 8.2 1 5 8 90.49 12.7 -1 5 -8 110.09 11.9 -1 5 -8 88.19 9.9 -1 5 -8 87.59 8 -1 5 -8 101.59 8.2 -5 -8 1 95.49 8.7 -5 -8 1 91.69 7.2 1 5 8 84.39 7.2 5 8 -1 89.79 10.8 -5 -8 -1 90.89 7.7 -1 -5 -8 90.79 6.8 5 8 -1 95.69 9.6 -1 -5 -8 87.29 6.7 1 -5 8 97.29 9.7 -5 -8 -1 99.69 8.3 1 -5 8 86.79 7.7 1 -5 8 93.19 7.6 1 -5 8 98.49 8.5 1 -5 8 94.69 8.2 1 -5 8 106.69 9.6 1 5 -8 93.79 10.8 -1 -5 -8 90.79 8.2 1 5 -8 73.59 6.4 -5 -8 -1 112.39 9.7 1 -5 8 93.79 10.3 1 5 -8 93.49 9.5 -5 -8 -1 101.29 8.5 5 8 -1 96.09 7.7 -1 -5 -8 93.69 7.8 1 5 -8 98.09 11.4 1 -5 8 89.29 8.2 5 8 -1 81.39 7.5 -1 -5 -8 85.89 10.8 1 -5 8 97.39 9.4 1 -5 8 81.69 6.7 1 5 -8 87.49 9.2 1 5 -8 90.29 10.3 1 5 -8 89.39 7.5 -1 5 8 86.19 12.5 -1 5 8 22.1 22.7 1 5 -8 95.59 10.2 -1 -5 -8 96.99 9.3 -5 -8 -1 104.79 8.3 5 8 -1 90.39 10 5 8 -1 78.49 11.1 1 -5 8 93.19 8.5 -5 -8 -1 88.39 7.5 5 8 -1 100.19 7.4 -5 -8 -1 99.89 9.5 -1 -5 -8 87.29 7.4 -1 -5 -8 86.29 9.3 -5 -8 -1 89.49 10.1 1 5 -8 96.79 8.3 5 8 -1 95.09 8.5 -7 -8 1 96.09 12.7 -7 -8 1 69.89 9.9 -1 -7 8 86.09 11.2 1 -7 -8 78.19 10.4 -1 -7 8 94.69 9.5 -1 -7 8 94.39 10.5 1 7 8 94.59 9.7 1 7 8 84.99 11.2 -1 7 -8 102.39 11.3 1 7 8 64.79 16.1 -7 -8 1 107.89 13.9 -7 -8 1 87.89 13.5 1 7 8 93.79 15.4 -1 7 -8 92.39 10.1 7 8 1 89.49 8.9 -1 -7 8 81.79 10 -1 7 -8 91.99 10.4 -7 -8 1 98.39 9.3 -1 -7 8 95.29 11.1 7 8 1 92.19 9.4 -7 -8 1 84.59 10.2 -1 7 -8 98.29 12.7 7 8 1 85.49 11.3 -1 7 -8 86.99 8.2 7 8 1 99.39 13 -1 7 -8 81.89 11 7 8 1 85.39 7.5 -1 -7 8 88.29 10.6 -1 7 -8 93.99 11.3 7 8 1 90.39 12.8 7 8 1 96.89 12.8 1 7 8 100.89 10.9 1 7 8 95.29 6.4 -1 -7 -8 92.39 9 1 -7 8 93.39 9.6 1 -7 8 90.29 11.1 -1 -7 -8 114.99 12.6 -1 -7 -8 92.89 9.8 -7 -8 -1 95.59 9.6 -7 -8 -1 88.79 13.4 7 8 -1 88.39 8.3 1 -7 8 112.99 11.6 1 7 -8 89.59 11.5 -1 -7 -8 92.59 10.8 7 8 -1 89.79 11.9 -1 -7 -8 92.79 10.4 -1 -7 -8 97.69 6.5 1 -7 8 91.09 7.5 1 -7 8 113.99 9.9 1 7 -8 83.49 7.5 -7 -8 -1 103.49 8.6 1 7 -8 101.29 12.5 -7 -8 -1 122.69 12.6 -7 -8 -1 84.99 9.7 1 -7 8 95.99 7.5 1 -7 8 89.19 6.4 -1 -7 -8 95.69 8.4 1 7 -8 100.89 13.5 7 8 -1 100.69 10.9 7 8 -1 102.89 8.8 -1 -7 -8 91.89 8.4 1 -7 8 93.49 9.9 1 7 -8 98.89 11.9 7 8 -1 83.49 11.2 -7 -8 -1 104.19 7.6 1 7 -8 86.69 8.8 0 8 2 61.39 6.4 0 8 -2 71.39 9 0 -8 -2 76.29 7.1 2 0 -8 90.09 8.9 0 8 2 88.89 8.9 2 0 8 88.79 6.8 0 -8 -2 79.39 6.8 -2 0 -8 88.49 9.3 2 0 8 91.19 8 0 -8 2 80.49 5.9 0 -8 2 84.69 7.8 0 8 2 83.69 7.6 2 0 8 92.19 8.5 2 0 -8 97.29 8 -2 0 -8 77.99 7.9 0 8 2 89.29 11 -2 0 -8 78.29 6.9 2 0 8 82.09 8.4 0 -8 2 69.39 5.3 -2 0 -8 79.49 7.8 0 8 -2 82.19 7.2 0 -8 -2 88.69 8.5 2 0 8 89.29 8.2 0 8 -2 82.89 8.7 -2 0 -8 71.29 8.6 0 8 2 78.59 9.7 0 8 -2 70.59 8.1 -2 0 -8 71.29 8.1 0 8 -2 77.39 9.1 -2 0 -8 82.09 6.7 -2 0 8 84.79 13.7 0 8 2 84.09 8.9 -2 0 8 99.09 12.1 0 -8 2 88.19 9.4 -2 0 8 83.59 11.5 0 8 2 79.79 9.9 -2 0 -8 73.89 8.1 2 0 8 82.49 7.1 0 -8 2 92.19 7.8 2 0 8 84.89 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15.7 2 4 -14 9.6 15.5 -4 -14 -2 37.4 13.7 -4 -14 -2 18.9 10.2 2 -4 14 22.1 12.4 2 -4 14 35.4 10 2 4 -14 24 10.3 2 -4 14 36.8 13.9 2 4 -14 19.5 11.1 -4 -14 -2 26 14.1 4 14 -2 36.4 13.1 4 14 -2 18.3 17.6 -4 -14 -2 26.8 13.6 4 14 -2 24.1 12.2 -2 -4 -14 39.8 14.8 -2 -4 -14 30.7 14.7 4 14 -2 25.1 12.4 2 -4 14 19.2 12.3 4 14 -2 34.9 11.1 -2 -4 -14 30.4 13.1 3 1 14 37.7 12.1 1 14 3 36 12.3 -3 -1 14 -21.1 29.7 -1 -14 3 0.5 14.6 -3 1 -14 43.7 14.2 -3 1 -14 45.1 11.6 -1 -14 3 36.5 14.8 -1 -14 3 53.39 11.8 -3 -1 14 14.8 14.3 3 1 14 38.9 9.4 1 14 3 23.2 13.6 3 1 14 34.1 11 -3 -1 14 50.29 40.8 1 14 3 46.5 19.7 -1 -14 3 0.6 14.7 1 14 3 4.3 15.8 -3 1 -14 38 11.5 1 14 3 33 16.1 1 14 -3 0.9 11.8 -3 -1 -14 39.6 14 -1 -14 -3 35.9 12.6 -1 -14 -3 48 14.7 3 -1 14 49.8 11.7 -1 -14 -3 52.69 14.7 3 -1 14 36.3 11 3 -1 14 63.29 14 1 14 -3 58.99 13.7 1 14 -3 7.9 14.7 1 -14 3 -1.2 14.6 1 14 -3 57.29 14.1 1 14 -3 40.8 15.4 -1 -14 -3 39.8 10.9 -3 -1 -14 39.1 14.9 3 1 -14 49.1 10.7 3 -1 14 42.5 10.1 -3 -1 -14 41.1 12.2 1 14 -3 6.3 16.7 3 1 -14 41.3 12.6 1 14 -3 69.49 12.6 3 1 -14 37 14 3 3 14 50.79 14.8 -3 -3 14 32.6 25.4 3 14 3 38.6 14.1 -3 -14 3 59.59 12.4 3 14 3 45.1 18.5 3 3 14 68.09 13.2 -3 3 -14 45.4 14.3 -3 -14 3 2.8 15.2 3 14 3 34.4 10.5 3 14 3 33.7 13.2 -3 -3 14 66.49 32.5 -3 3 -14 37 14.4 3 14 3 64.49 15.9 -3 3 -14 65.09 12.5 3 3 14 59.49 12.4 -3 3 -14 58.19 15.1 3 3 14 52.59 16.4 3 3 14 68.69 19.8 3 3 14 63.39 11.7 -3 3 -14 19.3 10 -3 3 -14 34.7 13.3 -3 -14 3 -0.9 14.5 -3 -3 -14 32.8 12.8 3 14 -3 51.69 14.5 -3 -14 -3 75.89 14.4 3 3 -14 32.2 16.4 3 14 -3 38.7 12.2 3 14 -3 3.6 18.7 3 -3 14 61.99 13.4 3 -3 14 51.09 12 3 14 -3 51.29 12.6 3 3 -14 52.89 11.9 3 -3 14 23.3 11.4 3 14 -3 43.1 13.9 3 3 -14 49.6 10.8 -3 -14 -3 37.8 13.4 3 -3 14 41 13.2 -3 -3 -14 44.3 15.4 3 14 -3 48 13.1 -3 -14 -3 51.29 11.5 -3 -3 -14 41.5 14.4 -3 -14 -3 46.2 14.8 5 14 3 16 14.3 -3 -5 14 33.1 32.8 5 14 3 16.1 11.9 -3 5 -14 10.4 14.3 5 14 3 0.6 17.9 -3 5 -14 16.8 13.3 5 14 3 14 12.7 -5 -14 3 2.2 11.3 -3 -5 14 -42.4 36.9 -3 5 -14 15.2 14.2 5 14 3 12.8 16.1 3 5 14 24.4 12 3 5 14 11.7 12.1 -5 -14 3 1 15.1 3 5 14 4.6 15.1 -3 -5 14 16.6 20.8 -3 5 -14 16.9 12.2 3 5 14 17.8 14.5 -5 -14 3 -1.7 13.1 3 5 14 16.6 20 3 5 14 25.9 16.7 -3 5 -14 25.2 15.7 -3 -5 14 19.4 16.3 3 5 -14 18.1 10.9 3 -5 14 22.1 10.5 5 14 -3 -2.6 18.3 -5 -14 -3 19.2 12 3 -5 14 11 12 -5 -14 -3 17.2 14.5 -5 -14 -3 28.8 13.8 -3 -5 -14 36.9 13.7 5 14 -3 36.3 12.3 -5 -14 -3 13.2 11.3 3 -5 14 24.3 13.6 -3 -5 -14 21.6 14.5 5 14 -3 9.7 13.7 3 -5 14 20.7 13.4 3 5 -14 26.8 15.3 5 14 -3 35.9 13.9 5 14 -3 12.9 12.2 -4 0 -14 38.4 14.3 4 0 14 36.2 12 0 14 -4 -1.9 17.5 0 14 -4 18.7 14.9 0 -14 4 3.5 11.3 -4 0 -14 39.9 15 0 -14 4 4.8 15.9 0 14 -4 32.5 14.1 0 14 -4 21.4 15.4 4 0 14 33.1 13.6 4 0 14 59.99 12.1 0 14 -4 29.5 18.2 0 14 -4 17.9 23.2 -4 0 -14 44.5 12.1 4 0 14 24.7 9.3 2 14 4 13.6 16 -4 2 -14 22.8 13.1 -2 -14 4 -1.7 14.2 -2 -14 4 32.1 12.4 -4 2 -14 18.9 14.4 -2 -14 4 12.8 14.6 2 14 4 24.4 16.2 -4 2 -14 6.7 14.5 4 2 14 15 12.2 -4 2 -14 41 12.6 -2 -14 4 4.8 14.3 2 14 4 34.5 19.8 4 2 14 30.8 10.4 -4 2 -14 40.1 13.5 2 14 4 30.6 12.6 2 14 4 19.1 10.6 -4 -2 14 -5.1 45.7 4 2 14 19.4 13.9 2 14 4 35.4 14 -4 2 -14 31.7 10.7 2 14 4 31.1 16 4 2 14 21.9 14.7 -2 -14 -4 29.9 13.3 -4 -2 -14 31.1 14.2 2 14 -4 13.8 14.7 -4 -2 -14 20.3 12.5 4 2 -14 9.6 11.6 2 14 -4 10.8 13.5 4 -2 14 41.5 11.8 4 -2 14 28.3 11 4 -2 14 49.3 14.4 -2 -14 -4 44.1 15.2 -2 -14 -4 17.6 13.2 -2 -14 -4 26.6 11.3 2 14 -4 21.1 12.7 -4 -2 -14 32.5 15.4 4 -2 14 19.4 12.8 2 14 -4 1.8 17 2 14 -4 37.7 14.1 2 14 -4 1 14.2 -4 4 -14 7.3 13.4 4 14 4 4.4 13.7 -4 4 -14 -2.1 12.9 4 4 14 6.9 12.4 4 4 14 23.2 10.7 -4 -14 4 -1.9 15.1 -4 -14 4 -6.9 15.2 -4 4 -14 24.8 13.8 4 4 14 3 14.8 -4 4 -14 -8.8 12.6 4 4 14 6.8 14.1 -4 4 -14 0.6 15 -4 -4 14 3.7 20.6 -4 -4 14 52.39 35 4 4 14 10.8 12.3 -4 -14 4 0.6 13.8 4 14 4 4.2 17.6 4 14 4 5 13.9 4 14 4 17.6 15.4 -4 -14 4 18 12 4 4 14 -16.8 18.3 4 14 -4 -7.1 12.8 -4 -14 -4 3.3 11.9 4 14 -4 -1.6 12 4 -4 14 0.4 10.9 4 -4 14 8.7 13.6 4 14 -4 4.6 13.7 -4 -14 -4 10.2 11 4 4 -14 -1.8 15.2 4 4 -14 8.6 10.7 -4 -4 -14 12.7 16.3 4 14 -4 2 10.8 -4 -14 -4 12.8 13.4 -4 -14 -4 -3 13.4 4 14 -4 15.5 12.1 4 14 -4 -4.4 17.5 -4 -4 -14 6 12.5 4 -4 14 -2.8 11.2 -4 -4 -14 -1.6 14.5 4 -4 14 11.2 13.7 -5 1 -14 -4.4 12.1 -5 1 -14 7.6 14 -1 -14 5 10.8 12.3 1 14 5 8.8 16.4 -5 1 -14 12.7 11.1 5 1 14 4.7 10.4 5 1 14 7 12.7 -1 14 -5 -4.4 14.1 -1 -14 5 8.6 13.5 -1 -14 5 -2 15.8 1 14 5 3 22 -1 14 -5 11.1 15.6 1 14 5 14.1 12.6 1 14 5 1.2 21.3 5 -1 14 25.2 13.1 5 -1 14 9.8 11.9 5 -1 14 16.9 11.9 1 -14 5 -2 10.7 1 -14 5 0.5 14.1 1 14 -5 3.6 15.7 1 14 -5 8.9 13.1 -1 -14 -5 9.4 13.9 1 -14 5 0.6 15 1 14 -5 9 13.7 -1 -14 -5 12.5 12.8 -5 -1 -14 0.6 15.1 -5 -1 -14 6.1 14.3 1 14 -5 -0.6 16.5 -1 -14 -5 10.5 11.6 1 14 -5 1.1 14.4 1 14 -5 1.6 13.8 -5 -1 -14 14.7 12.3 5 3 14 19.3 12.1 5 3 14 17.7 10 -5 3 -14 -16.9 14.3 3 14 5 34.8 16.3 5 3 14 23.6 12 -5 3 -14 23.6 14.5 -5 3 -14 9.2 14.2 5 3 14 32.5 14.6 -5 3 -14 25.7 15.4 -3 -14 5 14.2 14.5 -3 -14 5 15.7 13.2 3 14 5 14.4 13.2 3 14 5 23.3 18.9 3 14 5 27.8 16.2 -3 -14 5 -1.4 14.6 5 3 14 25.8 14.3 3 14 -5 16.7 12.8 5 -3 14 31.2 14.2 -3 -14 -5 18.7 12.1 -3 -14 -5 0.9 14 -5 -3 -14 10.1 12.9 3 14 -5 -1.8 17.8 5 -3 14 26.9 12.3 3 14 -5 -5.8 14.5 -5 -3 -14 30.5 16.5 5 -3 14 8.5 13.7 -5 -3 -14 15.2 14.4 -3 -14 -5 8.6 13.8 3 14 -5 -4.2 13.5 -3 -14 -5 25.6 12.5 0 -1 15 25.5 18.6 0 -1 15 8.3 12.4 -1 -15 0 8.5 16.3 0 -1 -15 12.3 14.4 1 15 0 5.7 18 0 1 -15 21.3 15.1 0 -1 -15 3.6 15.1 0 -1 15 -5.5 22 1 15 0 -20.8 13.1 0 -1 -15 49.6 13.5 0 1 -15 -2.4 13.3 0 1 15 18.6 24.7 0 1 15 -23.7 13.5 0 -1 15 12.2 11.8 0 1 15 11.5 13.3 0 1 -15 9.8 11.7 -1 -15 0 0.5 13.3 0 1 15 23.5 16.3 1 15 0 28.5 14 0 -1 15 16.3 13.5 1 15 0 22.7 16.7 0 -1 -15 30.9 13.7 1 0 -15 30.4 13.6 0 15 -1 5.7 16.3 -1 0 15 68.09 29.3 0 -15 1 5.2 13 1 0 -15 -5.6 13.4 1 0 15 15.2 15.6 -1 0 -15 0.6 15.2 -1 0 -15 -5.5 16 1 0 -15 16 13.8 0 15 -1 12 16.8 -1 0 -15 3.6 11.5 1 0 15 17.6 11.9 0 -15 1 2.3 14.5 -1 0 -15 2.5 12.3 -1 0 15 23.3 19.3 -1 0 15 -0.8 16 0 -15 1 0.6 14.5 0 15 -1 7.9 12.9 -1 0 15 -2.7 17.3 1 0 -15 24.2 14.2 -1 0 15 4.5 27.8 1 0 15 8.2 11.9 1 0 15 18.7 20.9 1 0 15 21.6 12.7 -2 -15 1 43.5 16.4 2 15 1 30.1 13.8 -1 2 -15 43.1 14.9 2 15 1 33.5 17.2 2 15 1 41.5 12.4 1 2 15 38.9 17 2 15 1 46.9 18.2 1 2 15 70.39 23.9 -1 -2 15 24.9 14.7 1 -2 -15 42.7 15.1 1 2 15 23.9 18.5 -1 2 -15 19.1 14.2 1 2 15 49.3 11.5 -1 2 -15 44.4 16 -2 -15 1 37 14.7 -1 -2 15 46.5 25.1 -1 -2 15 44 16.8 1 2 15 49.7 14.2 -1 -2 15 54.29 15.5 1 -2 -15 41.3 16 -1 2 -15 43.2 12.3 -1 -2 15 41 23.8 1 -2 -15 41.1 14.1 2 15 1 54.59 17.4 2 15 -1 17.2 16.5 -1 -2 -15 42.8 16 1 -2 15 28 15.6 -1 -2 -15 25.8 15.7 -2 -15 -1 19.2 16.1 1 -2 15 25.1 12.4 1 -2 15 10.1 12.7 2 15 -1 34 14.1 1 -2 15 48.1 12.3 2 15 -1 41.5 11.8 2 15 -1 37.8 13.3 1 2 -15 34.1 13.4 1 2 -15 19.7 14.6 1 2 -15 35.3 11.6 1 2 -15 49.5 13 -2 -15 -1 62.19 15.6 -1 2 15 26.7 35.4 -2 -15 -1 36.6 15.9 -1 2 15 30.2 18.8 2 15 -1 57.29 17.9 -1 -2 -15 48.5 14 1 15 2 14.7 13.2 2 1 15 41.4 19.9 -2 -1 15 39.4 19.3 -2 1 -15 53.69 12.4 1 15 2 0.4 14.6 2 -1 -15 68.69 14.7 1 15 2 33.2 16.9 -2 -1 15 45.6 34.2 2 -1 -15 56.39 14.8 -1 -15 2 51.19 16.4 -1 -15 2 -0.5 15.1 -2 1 -15 46.5 12.9 2 1 15 41.9 12.7 -2 1 -15 15.8 14.1 1 15 2 18.8 14.4 -2 -1 15 7.3 22.2 2 1 15 38.7 10.8 2 -1 -15 61.29 15.3 2 1 15 32.7 12.9 1 15 2 45.4 19.4 -2 1 15 10.3 43.7 1 15 -2 28.4 17.2 -1 -15 -2 28.9 15.8 1 15 -2 64.19 14.4 -1 -15 -2 41.4 13.4 -1 -15 -2 23 14.7 1 15 -2 -2.6 18.3 1 15 -2 47.9 14.7 2 -1 15 19.9 15.5 2 1 -15 24.5 14.8 2 1 -15 53.19 13.6 -2 -1 -15 44.6 15.7 1 15 -2 20.9 12.5 2 1 -15 41.3 12.6 -2 -1 -15 48 12.8 2 -1 15 41.1 12.4 2 -1 15 41.4 12.3 -2 1 15 27.2 28 2 -1 15 35 11.5 -2 -1 -15 43.9 16 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Co1 N1 110.6(4) . 46 ? N1 Co1 N1 107.2(7) 46 48_554 ? N1 Co1 N1 110.6(4) . 48_554 ? N1 Co1 N1 107.2(7) . 3_655 ? N1 Co1 N1 110.6(4) 46 3_655 ? N1 Co1 N1 110.6(4) 3_655 48_554 ? C2 N1 Co1 124.9(7) . . ? C2 N1 C1 105.7(11) . . ? C1 N1 Co1 129.0(10) . . ? N1 C2 N1 112.5(13) 14_665 . ? N1 C2 C3 123.7(7) 14_665 . ? N1 C2 C3 123.7(7) . . ? N1 C1 H1 126.0 . . ? C1 C1 N1 108.1(9) 14_665 . ? C1 C1 H1 126.0 14_665 . ? C2 C3 H3A 109.5 . . ? C2 C3 H3B 109.5 . . ? C2 C3 H3C 109.5 . . ? H3A C3 H3B 109.5 . . ? H3A C3 H3C 109.5 . . ? H3B C3 H3C 109.5 . . ? N3 N2 N3 180.0 . 3_655 ? N4 N5 N4 173(10) . 2_665 ? N2 N3 N3 0.000(3) . 3_655 ? N12 N11 N12 115(10) . 12_654 ? N12 N11 N12 115(10) . 6_665 ? N12 N11 N12 115(10) 12_654 6_665 ? N12 N11 N10 111(10) 12_654 12_654 ? N12 N11 N10 62(10) . 12_654 ? N12 N11 N10 62(10) 12_654 6_665 ? N12 N11 N10 62(10) 6_665 12_654 ? N12 N11 N10 62(10) . 6_665 ? N12 N11 N10 111(10) 6_665 6_665 ? N10 N11 N10 58(10) 6_665 12_654 ? N10 N11 N10 58(10) 6_665 . ? N10 N11 N10 58(10) 12_654 . ? N11 N12 N12 33(9) . 12_654 ? N11 N12 N12 33(9) . 6_665 ? N12 N12 N12 60.00(3) 12_654 6_665 ? N15 N13 N15 108(10) 6_665 12_654 ? N15 N13 N15 108(10) 6_665 . ? N15 N13 N15 108(10) 12_654 . ? N10 N10 N11 61(9) 12_654 . ? N10 N10 N11 61(9) 6_665 . ? N10 N10 N10 60.00(5) 12_654 6_665 ? N13 N15 N15 36(10) . 12_654 ? N13 N15 N15 36(10) . 6_665 ? N15 N15 N15 60.00(4) 6_665 12_654 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Co1 N1 1.958(11) . ? Co1 N1 1.958(11) 3_655 ? Co1 N1 1.958(11) 46 ? Co1 N1 1.958(11) 48_554 ? N1 C2 1.336(11) . ? N1 C1 1.379(12) . ? C2 C3 1.543(14) . ? C1 C1 1.37(4) 14_665 ? C1 H1 1.0770 . ? C3 H3A 1.0830 . ? C3 H3B 1.0830 . ? C3 H3C 1.0830 . ? N2 N3 0.64(4) . ? N2 N3 0.64(4) 3_655 ? N5 N4 1.05(3) . ? N5 N4 1.05(3) 2_665 ? N8 N9 1.02(2) . ? N3 N3 1.29(7) 3_655 ? N6 N7 0.63(13) . ? N11 N12 0.7(2) . ? N11 N12 0.7(2) 12_654 ? N11 N12 0.7(2) 6_665 ? N11 N10 0.76(17) 6_665 ? N11 N10 0.76(17) . ? N11 N10 0.76(17) 12_654 ? N12 N12 1.3(4) 6_665 ? N12 N12 1.3(4) 12_654 ? N13 N15 0.61(17) 6_665 ? N13 N15 0.61(17) . ? N13 N15 0.61(17) 12_654 ? N10 N10 0.7(2) 6_665 ? N10 N10 0.7(2) 12_654 ? N15 N15 1.0(3) 6_665 ? N15 N15 1.0(3) 12_654 ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Co1 N1 C2 N1 174.0(6) . . . 14_665 ? Co1 N1 C2 C3 -3(2) . . . . ? Co1 N1 C1 C1 -173.0(8) . . . 14_665 ? C2 N1 C1 C1 -0.8(11) . . . 14_665 ? C1 N1 C2 N1 1.4(19) . . . 14_665 ? C1 N1 C2 C3 -176.0(15) . . . . ? N12 N11 N12 N12 -136(69) 6_665 . . 12_654 ? N12 N11 N12 N12 136(69) 12_654 . . 6_665 ? N10 N11 N10 N10 -70(7) 6_665 . . 12_654 ? N10 N11 N10 N10 70(7) 12_654 . . 6_665 ? N15 N13 N15 N15 -117(63) 12_654 . . 6_665 ? N15 N13 N15 N15 117(63) 6_665 . . 12_654 ?