#------------------------------------------------------------------------------ #$Date: 2023-12-03 01:40:56 +0200 (Sun, 03 Dec 2023) $ #$Revision: 287949 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/78/7247803.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7247803 loop_ _publ_author_name 'Pradhan, Abinash' 'Sahoo, Sanand' 'Samal, Saroj L.' _publ_section_title ; (C2H5NH3)2BiCl5−xBrx Perovskites Containing 1D Chains: Effect of Br Substitution on Structural and Optical Properties ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D3CE01019H _journal_year 2023 _chemical_formula_moiety 'Bi Cl5, C4 H16 N2' _chemical_formula_sum 'C4 H16 Bi Cl5 N2' _chemical_formula_weight 478.42 _space_group_crystal_system orthorhombic _space_group_IT_number 64 _space_group_name_Hall '-C 2ac 2' _space_group_name_H-M_alt 'C m c e' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2023-06-01 _audit_creation_method ; Olex2 1.5-alpha (compiled 2021.06.29 svn.r12e2184c for OlexSys, GUI svn.r6374) ; _audit_update_record ; 2023-10-09 deposited with the CCDC. 2023-12-01 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 7.5640(2) _cell_length_b 21.9862(6) _cell_length_c 17.8275(4) _cell_measurement_reflns_used 3831 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 26.5670 _cell_measurement_theta_min 1.8440 _cell_volume 2964.78(13) _computing_cell_refinement 'CrysAlisPro 1.171.41.93a (Rigaku OD, 2020)' _computing_data_collection 'CrysAlisPro 1.171.41.93a (Rigaku OD, 2020)' _computing_data_reduction 'CrysAlisPro 1.171.41.93a (Rigaku OD, 2020)' _computing_molecular_graphics 'Olex2 1.5-alpha (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5-alpha (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 293(2) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.954 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -56.00 15.00 0.50 140.00 -- 10.00 -48.00-143.00 142 2 \w -70.00 -44.00 0.50 140.00 -- -10.20 -73.00 50.00 52 3 \w -15.00 97.00 0.50 140.00 -- 10.00 77.00 120.00 224 4 \w -7.00 45.00 0.50 140.00 -- 10.00 77.00 -60.00 104 5 \w -59.00 -34.00 0.50 140.00 -- 10.00 -77.00 150.00 50 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Pro II AFC12 (RINC): Kappa single' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0859065000 _diffrn_orient_matrix_UB_12 0.0110990000 _diffrn_orient_matrix_UB_13 0.0082748000 _diffrn_orient_matrix_UB_21 0.0375388000 _diffrn_orient_matrix_UB_22 -0.0236876000 _diffrn_orient_matrix_UB_23 -0.0217932000 _diffrn_orient_matrix_UB_31 -0.0033161000 _diffrn_orient_matrix_UB_32 0.0188709000 _diffrn_orient_matrix_UB_33 -0.0322328000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0299 _diffrn_reflns_av_unetI/netI 0.0277 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.954 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -27 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 7394 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.954 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.085 _diffrn_reflns_theta_min 1.852 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'Rigaku (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 12.759 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.21752 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.93a (Rigaku Oxford Diffraction, 2020) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_density_diffrn 2.144 _exptl_crystal_description crystalline _exptl_crystal_F_000 1776 _exptl_crystal_size_max 0.16 _exptl_crystal_size_mid 0.14 _exptl_crystal_size_min 0.09 _refine_diff_density_max 0.875 _refine_diff_density_min -0.543 _refine_diff_density_rms 0.113 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.020 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 75 _refine_ls_number_reflns 1680 _refine_ls_number_restraints 21 _refine_ls_restrained_S_all 1.015 _refine_ls_R_factor_all 0.0416 _refine_ls_R_factor_gt 0.0300 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0466P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0719 _refine_ls_wR_factor_ref 0.0751 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1365 _reflns_number_total 1680 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL ab251_final_111221_a.res in Cmca ab251_final_111221.res created by SHELXL-2018/3 at 16:28:26 on 01-Jun-2023 REM Old TITL AB251_Final_111221 in Cmce REM SHELXT solution in Cmca: R1 0.138, Rweak 0.007, Alpha 0.026 REM 0.568 for 97 systematic absences, Orientation as input REM Formula found by SHELXT: C C1 Cl5 Bi CELL 0.71073 7.564 21.9862 17.8275 90 90 90 ZERR 8 0.0002 0.0006 0.0004 0 0 0 LATT 7 SYMM -X,0.5-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM +X,-Y,-Z SFAC C H Bi Cl N UNIT 32 128 8 40 16 SIMU 0.02 0.04 2 C2 N1 C1 RIGU 0.01 0.01 C1 C2 N1 L.S. 15 0 0 PLAN 15 CONF list 4 MORE -1 BOND $H fmap 2 53 acta REM REM REM WGHT 0.046600 FVAR 0.11697 BI1 3 0.500000 0.364037 0.366301 10.50000 0.03825 0.06408 = 0.04213 0.00853 0.00000 0.00000 CL1 4 0.751530 0.379255 0.462004 11.00000 0.06997 0.12436 = 0.07369 0.00330 -0.02845 -0.01634 CL2 4 0.500000 0.245836 0.402541 10.50000 0.13319 0.05607 = 0.09230 0.01606 0.00000 0.00000 CL3 4 0.500000 0.483244 0.331108 10.50000 0.19265 0.05499 = 0.07637 0.00948 0.00000 0.00000 CL4 4 0.250000 0.344636 0.250000 10.50000 0.12648 0.14043 = 0.15470 0.00000 -0.10409 0.00000 N2 5 0.500000 0.467564 0.148978 10.50000 0.11623 0.06286 = 0.08335 0.01186 0.00000 0.00000 PART -1 AFIX 33 H2A 2 0.500000 0.438491 0.114240 10.50000 -1.20000 H2B 2 0.596071 0.463977 0.177459 10.50000 -1.20000 H2C 2 0.403929 0.463976 0.177459 10.50000 -1.20000 AFIX 0 PART 0 C3 1 0.500000 0.578524 0.148779 10.50000 0.49184 0.05272 = 0.11612 -0.01976 0.00000 0.00000 PART -1 AFIX 33 H3A 2 0.500000 0.611889 0.114043 10.50000 -1.50000 H3B 2 0.396373 0.580679 0.179755 10.50000 -1.50000 H3C 2 0.603627 0.580679 0.179755 10.50000 -1.50000 AFIX 0 PART 0 C4 1 0.500000 0.527731 0.112087 10.50000 0.25208 0.11507 = 0.09573 0.02911 0.00000 0.00000 AFIX 23 H4A 2 0.602766 0.528634 0.079559 10.50000 -1.20000 H4B 2 0.397234 0.528634 0.079559 10.50000 -1.20000 AFIX 6 PART -1 C1 1 0.453073 0.325999 0.686222 10.50000 0.07124 0.16486 = 0.13788 -0.05793 -0.01509 -0.00846 AFIX 33 H1A 2 0.517437 0.359917 0.706328 10.50000 -1.20000 H1B 2 0.340616 0.339688 0.667834 10.50000 -1.20000 H1C 2 0.435100 0.296234 0.724875 10.50000 -1.20000 AFIX 5 C2 1 0.558503 0.297529 0.621795 10.50000 0.09299 0.17240 = 0.16902 -0.06323 -0.01148 -0.00929 AFIX 23 H2D 2 0.578188 0.327741 0.583034 10.50000 -1.20000 H2E 2 0.672833 0.284213 0.640172 10.50000 -1.20000 AFIX 5 N1 5 0.459610 0.243648 0.588854 10.50000 0.05098 0.14749 = 0.13834 -0.06340 0.00547 0.00291 AFIX 33 H1D 2 0.522546 0.227661 0.551564 10.50000 -1.50000 H1E 2 0.442971 0.215715 0.624291 10.50000 -1.50000 H1F 2 0.355376 0.256000 0.571409 10.50000 -1.50000 AFIX 0 HKLF 4 REM ab251_final_111221_a.res in Cmca REM wR2 = 0.0751, GooF = S = 1.020, Restrained GooF = 1.015 for all data REM R1 = 0.0300 for 1365 Fo > 4sig(Fo) and 0.0416 for all 1680 data REM 75 parameters refined using 21 restraints END WGHT 0.0466 0.0000 REM Highest difference peak 0.875, deepest hole -0.543, 1-sigma level 0.113 Q1 1 0.6014 0.3614 0.3362 11.00000 0.05 0.88 Q2 1 0.3659 0.3611 0.3647 11.00000 0.05 0.87 Q3 1 0.5000 0.2998 0.6021 10.50000 0.05 0.79 Q4 1 0.2500 0.3660 0.2500 10.50000 0.05 0.71 Q5 1 0.5886 0.3606 0.4072 11.00000 0.05 0.70 Q6 1 0.5000 0.5200 0.0963 10.50000 0.05 0.66 Q7 1 0.5775 0.2415 0.3745 11.00000 0.05 0.50 Q8 1 0.5000 0.3430 0.6389 10.50000 0.05 0.47 Q9 1 0.5000 0.2653 0.6563 10.50000 0.05 0.45 Q10 1 0.3530 0.3381 0.2342 11.00000 0.05 0.42 Q11 1 0.1560 0.3591 0.2161 11.00000 0.05 0.42 Q12 1 0.5000 0.4793 0.3609 10.50000 0.05 0.41 Q13 1 0.5000 0.2625 0.5823 10.50000 0.05 0.36 Q14 1 0.5828 0.4802 0.3062 11.00000 0.05 0.33 Q15 1 0.5000 0.2800 0.6910 10.50000 0.05 0.32 REM The information below was added by Olex2. REM REM R1 = 0.0300 for 1365 Fo > 4sig(Fo) and 0.0416 for all 7680 data REM 75 parameters refined using n/a restraints REM Highest difference peak 0.88, deepest hole -0.54 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0416 REM R1_gt = 0.0300 REM wR_ref = 0.0751 REM GOOF = 1.020 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 7680 REM Reflections_gt = 1365 REM Parameters = 75 REM Hole = -0.54 REM Peak = 0.88 REM Flack = n/a ; _cod_data_source_file d3ce01019h2.cif _cod_data_source_block ab251_final_111221 _cod_original_sg_symbol_Hall '-C 2bc 2' _cod_database_code 7247803 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula (C2H5NH3)2BiCl5 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _reflns_odcompleteness_completeness 99.54 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 26.32 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H,H) groups, {H2A,H2B,H2C} of N2, {H1A,H1B,H1C} of C1 At 1.5 times of: {H1D,H1E,H1F} of N1, {H3A,H3B,H3C} of C3 2. Uiso/Uaniso restraints and constraints C2 \\sim N1 \\sim C1: within 2A with sigma of 0.02 and sigma for terminal atoms of 0.04 within 2A 3. Rigid body (RIGU) restrains C1, C2, N1 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01 4. Others Fixed Sof: H2B(0.5) H2C(0.5) H3B(0.5) H3C(0.5) H4A(0.5) H4B(0.5) C1(0.5) H1A(0.5) H1B(0.5) H1C(0.5) C2(0.5) H2D(0.5) H2E(0.5) N1(0.5) H1D(0.5) H1E(0.5) H1F(0.5) 5.a Free rotating group: C1(C2,N1) 5.b Secondary CH2 refined with riding coordinates: C4(H4A,H4B), C2(H2D,H2E) 5.c Me refined with riding coordinates: N2(H2A,H2B,H2C), C3(H3A,H3B,H3C), C1(H1A,H1B,H1C), N1(H1D,H1E,H1F) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.678 _oxdiff_exptl_absorpt_empirical_full_min 0.558 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1, z+1/2' '-x+1/2, y+1, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y-1/2, -z-1/2' 'x, -y-1/2, z-1/2' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y, -z-1/2' 'x+1/2, -y, z-1/2' '-x+1/2, y+1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Bi1 Bi 0.500000 0.36404(2) 0.36630(2) 0.04815(13) Uani 1 2 d S T P . . Cl1 Cl 0.7515(2) 0.37926(8) 0.46200(11) 0.0893(5) Uani 1 1 d . . . . . Cl2 Cl 0.500000 0.24584(10) 0.40254(16) 0.0939(8) Uani 1 2 d S T P . . Cl3 Cl 0.500000 0.48324(10) 0.33111(15) 0.1080(10) Uani 1 2 d S T P . . Cl4 Cl 0.250000 0.34464(16) 0.250000 0.1405(14) Uani 1 2 d S T P . . N2 N 0.500000 0.4676(3) 0.1490(4) 0.087(3) Uani 1 2 d S T P . . H2A H 0.500000 0.438491 0.114240 0.105 Uiso 0.5 1 calc R U P A -1 H2B H 0.596071 0.463977 0.177459 0.105 Uiso 0.5 1 calc R U P A -1 H2C H 0.403929 0.463976 0.177459 0.105 Uiso 0.5 1 calc R U P A -1 C3 C 0.500000 0.5785(6) 0.1488(7) 0.220(12) Uani 1 2 d S T P . . H3A H 0.500000 0.611889 0.114043 0.330 Uiso 0.5 1 calc R U P B -1 H3B H 0.396373 0.580679 0.179755 0.330 Uiso 0.5 1 calc R U P B -1 H3C H 0.603627 0.580679 0.179755 0.330 Uiso 0.5 1 calc R U P B -1 C4 C 0.500000 0.5277(7) 0.1121(7) 0.154(7) Uani 1 2 d S T P . . H4A H 0.602766 0.528634 0.079559 0.185 Uiso 0.5 1 calc R U P . . H4B H 0.397234 0.528634 0.079559 0.185 Uiso 0.5 1 calc R U P . . C1 C 0.4531(16) 0.3260(6) 0.6862(7) 0.125(6) Uani 0.5 1 d G U P C -1 H1A H 0.517437 0.359917 0.706328 0.150 Uiso 0.5 1 calc R U P C -1 H1B H 0.340616 0.339688 0.667834 0.150 Uiso 0.5 1 calc R U P C -1 H1C H 0.435100 0.296234 0.724875 0.150 Uiso 0.5 1 calc R U P C -1 C2 C 0.5585(15) 0.2975(7) 0.6218(7) 0.145(7) Uani 0.5 1 d G U P C -1 H2D H 0.578188 0.327741 0.583034 0.174 Uiso 0.5 1 calc R U P C -1 H2E H 0.672833 0.284213 0.640172 0.174 Uiso 0.5 1 calc R U P C -1 N1 N 0.4596(14) 0.2436(5) 0.5889(6) 0.112(5) Uani 0.5 1 d G U P C -1 H1D H 0.522546 0.227661 0.551564 0.168 Uiso 0.5 1 calc R U P C -1 H1E H 0.442971 0.215715 0.624291 0.168 Uiso 0.5 1 calc R U P C -1 H1F H 0.355376 0.256000 0.571409 0.168 Uiso 0.5 1 calc R U P C -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Bi1 0.03825(17) 0.0641(2) 0.04213(18) 0.00853(12) 0.000 0.000 Cl1 0.0700(10) 0.1244(14) 0.0737(11) 0.0033(9) -0.0285(8) -0.0163(10) Cl2 0.133(2) 0.0561(14) 0.0923(17) 0.0161(13) 0.000 0.000 Cl3 0.193(3) 0.0550(14) 0.0764(16) 0.0095(12) 0.000 0.000 Cl4 0.126(3) 0.140(3) 0.155(3) 0.000 -0.104(2) 0.000 N2 0.116(7) 0.063(5) 0.083(5) 0.012(4) 0.000 0.000 C3 0.49(4) 0.053(8) 0.116(11) -0.020(7) 0.000 0.000 C4 0.25(2) 0.115(12) 0.096(9) 0.029(9) 0.000 0.000 C1 0.071(13) 0.165(14) 0.138(12) -0.058(10) -0.015(8) -0.008(9) C2 0.093(14) 0.172(16) 0.169(15) -0.063(12) -0.011(10) -0.009(10) N1 0.051(11) 0.147(9) 0.138(9) -0.063(8) 0.005(6) 0.003(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Bi Bi -4.1077 10.2566 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u 0 0 -2 9.04 0.73 0 0 2 11.13 0.76 0 0 3 0.4 0.55 0 0 -3 6.67 0.86 0 0 4 5634.7 165.88 0 0 -4 5772.28 165.92 0 0 -5 0.35 1.01 0 0 5 2.73 1.01 0 0 6 297.61 10.35 0 0 -6 306.34 10.52 0 0 -7 2.24 1.65 0 0 7 0.92 1.19 0 0 8 2028.26 63.11 0 0 -8 2205.54 63.55 0 0 -9 -0.66 2 0 0 9 2.75 1.84 0 0 -10 1116.06 34.55 0 0 10 1057.59 34.04 0 0 11 -1.94 2.23 0 0 -11 -2.88 2.93 0 0 12 802 26.86 0 0 -12 839.62 27.61 0 0 13 3.11 2.52 0 0 -13 0.49 2.88 0 0 14 129.92 7.4 0 0 14 100.69 6.33 0 0 15 12.23 4.58 0 0 15 1.93 3.09 0 0 16 95.22 6.55 0 0 17 0.27 3.64 0 0 18 233.05 11.25 0 0 19 -0.6 4.18 0 0 20 34.75 5.55 0 0 21 2.31 4.9 0 0 22 116.14 8.65 0 2 0 228.23 7.48 0 2 1 4549.17 130.98 0 -2 -1 4771 131.79 0 -2 -1 4399.83 130.96 0 -2 1 4566.94 131.4 0 2 1 4526.82 131.67 0 2 2 52.89 2.05 0 2 2 50.11 2.4 0 -2 -2 52.74 2.05 0 -2 -2 49.4 2.38 0 -2 3 1647.29 49.17 0 2 3 1721.61 49.99 0 -2 -3 1735.74 49.94 0 -2 -3 1707.97 49.59 0 -2 -3 1669.28 49.11 0 2 3 1727.33 49.6 0 2 4 34.45 2.33 0 -2 4 33.36 2.11 0 2 4 35.7 1.92 0 -2 4 32.01 1.38 0 -2 -4 33.36 1.33 0 -2 -4 33.75 1.94 0 2 5 418.5 13.18 0 -2 5 401.86 12.14 0 -2 -5 404.58 12.08 0 -2 -5 431.09 13.24 0 -2 5 420.53 13.47 0 2 5 410.46 13.45 0 -2 -6 599.56 17.53 0 -2 -6 614.01 19 0 2 6 572.95 18.85 0 -2 6 563.22 19.08 0 -2 6 608.02 17.61 0 2 6 580.86 19.17 0 -2 7 80.27 2.58 0 -2 7 80.33 4.16 0 2 7 83.39 4.38 0 -2 -7 82.88 4.09 0 2 7 70.88 3.9 0 -2 -8 135.47 5.83 0 -2 8 122.16 5.79 0 2 8 131.83 5.98 0 2 8 125.42 5.64 0 2 9 3516.58 105.41 0 -2 -9 3735.32 105.49 0 2 9 3516.48 105.24 0 -2 9 3470.26 105.44 0 2 10 36.46 3.59 0 2 10 31.97 3.11 0 -2 10 32.29 3.18 0 -2 -10 33.95 3.27 0 -2 11 63.57 4.41 0 2 11 72.28 4.92 0 2 11 62.27 4.33 0 -2 -11 65.06 4.59 0 -2 12 12.12 2.94 0 2 12 19.44 3.94 0 2 12 12.21 2.81 0 -2 -12 17.63 3.37 0 2 13 880.79 29.29 0 2 13 837.1 28.78 0 -2 13 879.61 28.98 0 -2 -13 908.4 29.41 0 2 14 10.74 4.38 0 -2 14 5.32 3.03 0 2 14 4.67 2.82 0 2 15 4.82 4.73 0 -2 15 4.69 3.26 0 2 15 1.66 3.18 0 2 16 2.27 3.39 0 -2 16 -1.04 3.2 0 2 17 309.05 13.07 0 -2 17 296.23 13.22 0 -2 18 12.69 4.32 0 2 18 22.61 4.58 0 2 19 42.65 5.6 0 -2 19 42 5.72 0 -2 20 0.65 4.67 0 2 20 0.63 4.29 0 -2 21 175.93 10.6 0 2 21 180.48 10.52 0 2 22 11.29 5.02 0 -2 22 6.62 5.43 0 -4 0 3879.4 112.64 0 4 0 3984.5 113.97 0 4 0 3824.65 112.62 0 -4 0 4060.81 114.3 0 4 1 143.03 5.89 0 4 1 144.68 4.74 0 -4 -1 151.25 6.23 0 -4 -1 140.61 4.73 0 -4 1 147.55 5.73 0 4 -1 150.75 5.56 0 -4 2 25.72 1.67 0 -4 -2 37.41 2.63 0 -4 -2 27.21 1.64 0 4 2 28.14 2.24 0 -4 -2 29.07 1.5 0 4 2 28.56 1.49 0 -4 2 29.33 1.97 0 -4 -3 2.68 0.86 0 -4 3 3.07 1 0 -4 -3 1.27 1.31 0 -4 -3 2.8 0.84 0 4 3 2.73 0.8 0 4 3 2.89 1.25 0 -4 -4 295.87 9.54 0 -4 -4 309.53 9.96 0 -4 -4 309.44 10.77 0 -4 4 298.65 9.66 0 4 4 314.63 9.97 0 -4 5 21.83 1.47 0 -4 -5 23.67 2.37 0 -4 -5 21.45 1.34 0 4 5 17.45 2.4 0 4 5 19.53 1.7 0 -4 -5 21.07 1.83 0 -4 -6 256.26 8.13 0 4 6 252.49 9.84 0 -4 6 260.06 8.28 0 4 6 265.94 9.18 0 -4 -6 260.95 9.15 0 -4 6 259.42 9.71 0 -4 -6 260.83 9.66 0 4 7 231.91 8.43 0 -4 7 235.84 7.33 0 -4 -7 226.61 7.18 0 -4 7 223.84 8.89 0 -4 -7 211.24 8.39 0 4 7 224.23 9.04 0 -4 -8 1869.13 56.35 0 -4 8 1775.46 56.72 0 -4 8 1936.65 54.75 0 4 8 1782.41 56.19 0 4 8 1840.34 56.92 0 -4 -8 1868.55 54.58 0 4 9 197.74 9.04 0 -4 -9 210.31 8.52 0 4 9 198.99 8.36 0 -4 9 222.08 8.93 0 -4 -9 212.67 6.65 0 -4 9 221.02 6.8 0 4 10 1142.85 36.37 0 -4 -10 1206.39 36.53 0 4 10 1146.13 37.05 0 -4 10 1164.68 36.82 0 4 11 1.56 2.17 0 4 11 3.17 3.08 0 -4 -11 2.33 2.31 0 -4 11 2.75 2.16 0 -4 -12 1480.52 45.51 0 4 12 1421.29 45.15 0 -4 12 1413.18 45.63 0 4 12 1506.36 46.11 0 4 13 94.02 6.76 0 -4 13 86.73 5.94 0 -4 -13 92.96 5.99 0 4 13 86.95 5.69 0 4 14 226.17 10.24 0 -4 14 232.85 10.58 0 4 14 235.76 11.21 0 4 15 -1.46 4.72 0 4 15 2.37 3.09 0 -4 15 -2.34 3.32 0 4 16 176.96 9.25 0 -4 16 189.46 9.68 0 -4 17 33.27 4.82 0 4 17 37.4 4.87 0 4 18 295.13 12.85 0 -4 18 278.84 13.11 0 -4 19 10.44 4.81 0 4 19 4.76 4.31 0 4 20 34.72 5.57 0 -4 20 29.31 5.54 0 4 21 7.73 4.76 0 -4 21 13.25 5.25 0 -4 22 106.94 8.65 0 -6 0 743.79 25.18 0 -6 0 851.51 26.98 0 6 0 859.38 26.37 0 6 0 825.85 24.58 0 -6 0 861.33 24.64 0 -6 -1 2447.94 72.67 0 6 1 2570.99 72.2 0 -6 -1 2397.12 72.18 0 6 1 2547.47 74.24 0 6 -1 2535.19 73.68 0 -6 1 2479.7 72.75 0 -6 1 2409.04 72.05 0 -6 -1 2604.49 75.02 0 -6 1 2438.1 74.24 0 6 -2 798.85 24.8 0 -6 -2 866.13 26.36 0 6 2 734 25.32 0 -6 -2 776.22 23.6 0 -6 -2 778.58 23.95 0 -6 2 789.27 24.04 0 6 2 795.79 23.61 0 -6 2 763.16 25.11 0 -6 -3 2003.63 59.5 0 6 3 1960.74 61.11 0 -6 3 2142.73 60.85 0 -6 3 1954.78 59.58 0 -6 -3 2011.89 59.36 0 6 3 2049.3 59.35 0 6 4 114.09 5.77 0 -6 -4 110.35 4.51 0 -6 -4 112.76 4.43 0 -6 -4 121.66 5.85 0 -6 4 106.89 5.3 0 6 4 116.78 4.59 0 -6 4 115.45 4.63 0 -6 5 342.99 11.13 0 -6 -5 346.78 12.62 0 6 5 342.37 11.31 0 6 5 329.74 12.63 0 -6 -5 332.61 10.93 0 -6 -5 343.11 11.33 0 -6 -6 299.89 11.64 0 -6 -6 294.88 10.53 0 -6 6 330.07 10.22 0 6 6 296.37 10.54 0 -6 -6 303.76 9.92 0 -6 -7 191.93 7.67 0 -6 -7 193.06 6.78 0 -6 -7 203.08 8.67 0 6 7 201.18 7.71 0 -6 7 216.12 7.06 0 -6 -8 251.49 9.42 0 -6 -8 251.26 8.2 0 -6 -8 238.45 10.03 0 6 8 239.92 9.43 0 -6 8 271.62 8.52 0 -6 8 237.93 10.15 0 -6 9 2033.39 65.37 0 6 9 2161.03 65.77 0 -6 -9 2126.87 63.02 0 -6 -9 2118.48 64.67 0 6 9 2037.69 64.56 0 -6 9 2291.44 63.3 0 6 10 266.26 10.38 0 -6 10 249.29 10.89 0 -6 -10 293.56 10.65 0 6 10 259.39 11.3 0 6 11 189.54 8.24 0 -6 -11 194.96 8.39 0 6 11 183.11 9.11 0 -6 11 182.5 8.78 0 6 12 31.8 3.47 0 -6 -12 28.57 3.5 0 -6 12 38.31 4.03 0 6 12 31.34 4.56 0 -6 13 717.06 24.56 0 6 13 700.62 24.87 0 6 13 703.78 23.91 0 6 14 52.17 5.93 0 6 14 65.36 5.15 0 -6 14 68.14 5.62 0 -6 15 13.17 3.88 0 6 15 10.4 3.47 0 -6 16 48.67 5.15 0 6 16 46.17 4.92 0 6 17 236.32 11.05 0 -6 17 243.69 11.9 0 6 18 31.13 4.71 0 -6 18 21.56 4.9 0 -6 19 31.13 5.36 0 6 19 22.19 5.04 0 -6 20 4.75 4.96 0 6 20 8.22 4.8 0 -6 21 115.09 8.84 0 6 21 96.68 8.09 0 -6 22 26.02 6.44 0 8 0 6937.89 196.44 0 -8 0 6449.18 194.87 0 8 0 6587.73 194.13 0 -8 0 6982.1 197.7 0 -8 0 6803.2 194.19 0 -8 -1 1746.97 55.05 0 8 -1 1747.76 53.42 0 -8 1 1758.4 51.39 0 -8 -1 1720.06 52.12 0 8 1 1729.92 53.89 0 8 1 1744.92 51.46 0 -8 1 1678.96 54.34 0 -8 -1 1751.03 51.52 0 -8 1 1788.68 52.24 0 8 -2 197.53 8.1 0 -8 2 194.28 6.46 0 8 2 183.54 8.54 0 -8 2 191.16 8.69 0 -8 2 198.93 7.28 0 -8 -2 209.27 9.63 0 8 2 192.57 6.62 0 -8 -2 188.91 7.15 0 -8 -2 179.51 6.62 0 -8 -3 43.11 2.5 0 -8 3 41.5 3.62 0 8 3 41.67 3.77 0 -8 3 48.35 2.89 0 8 3 44.18 2.47 0 -8 -3 43.47 4.28 0 -8 -3 43.49 2.75 0 8 4 1744.92 56.46 0 -8 -4 1822.54 54.23 0 -8 -4 1803 54.25 0 -8 4 1906.32 54.55 0 -8 4 1810.21 56.12 0 8 4 1823.57 54.2 0 -8 -5 840.58 25.85 0 -8 -5 848.54 26.06 0 -8 5 920.2 26.25 0 8 5 812.05 27.96 0 -8 5 828.39 27.58 0 -8 -5 864.31 28 0 8 5 787.26 25.87 0 -8 -6 59.82 3.49 0 8 6 45.75 4.33 0 8 6 69.34 3.61 0 -8 6 67.61 4.49 0 -8 -6 65.57 4.85 0 -8 -6 69.24 3.35 0 -8 6 69.1 3.66 0 8 7 69.81 3.93 0 -8 -7 72.88 5.21 0 -8 -7 76.52 3.53 0 -8 7 73.14 4.77 0 -8 7 76.65 3.81 0 8 7 75.93 5.22 0 -8 -7 72.56 4.04 0 8 8 726.93 24.08 0 -8 -8 734.02 25.46 0 -8 -8 734.84 24.1 0 -8 8 815.83 23.62 0 -8 -8 755.48 23.15 0 8 8 732.17 25.88 0 -8 -9 464.36 16.68 0 8 9 460.07 16.64 0 -8 -9 489.29 15.53 0 -8 -9 492.03 17.98 0 -8 9 553.78 16.04 0 -8 9 475.47 17.86 0 -8 -10 263 11.41 0 -8 -10 277.43 10.7 0 -8 10 278.71 11.69 0 8 10 277.09 10.72 0 8 11 22.1 3.21 0 -8 -11 27.25 3.38 0 -8 11 19.57 3.6 0 -8 12 455.31 17.12 0 8 12 424.29 16 0 -8 -12 465.16 16.4 0 8 13 128.94 7.12 0 -8 13 143.15 7.99 0 -8 14 46.18 5.06 0 8 14 44.62 4.66 0 -8 15 9.52 3.84 0 8 15 1.87 3.42 0 8 16 48.48 5.28 0 -8 16 63.85 6.14 0 8 17 69.67 6.07 0 -8 17 72.01 6.53 0 8 18 107.46 7.62 0 -8 18 118.07 8.45 0 8 19 6.08 4.33 0 -8 19 0.34 4.86 0 8 20 18.47 5.12 0 -8 20 20.3 5.75 0 -8 21 17.27 6.04 0 8 21 10.01 5.1 0 10 0 1645.29 51.16 0 10 0 1607.27 48.51 0 -10 0 1642.01 49.39 0 -10 0 1664.17 48.66 0 -10 0 1701.6 52.91 0 10 -1 1504.19 47 0 10 1 1522.41 47.53 0 10 1 1477.49 44.64 0 -10 -1 1478.77 44.77 0 -10 1 1493.92 44.6 0 -10 -1 1546.01 49.3 0 -10 1 1492.9 48.58 0 -10 1 1562.95 45.5 0 -10 -1 1523.39 45.42 0 10 2 46.62 2.71 0 -10 -2 54.85 3.26 0 -10 2 45.39 2.52 0 -10 -2 62.69 5.42 0 -10 2 51.73 3.36 0 10 -2 56.03 4.06 0 -10 -2 51.93 2.82 0 10 2 52.06 4.62 0 -10 2 52.05 4.81 0 -10 -3 850.36 28.48 0 -10 -3 783.39 24.33 0 10 3 760.34 23.89 0 -10 3 749.27 26.83 0 10 3 784.67 26.68 0 -10 -3 754.43 23.9 0 -10 3 808.03 24.57 0 -10 -4 899.17 27.6 0 10 4 849.93 27.28 0 10 4 860.16 29.9 0 -10 4 812.08 29.72 0 -10 -4 937.45 27.51 0 -10 4 931.86 27.92 0 10 5 808.67 25.98 0 -10 5 921.15 26.64 0 10 5 792.87 28.48 0 -10 5 811.86 28.41 0 -10 -5 868.82 26.14 0 -10 -5 806.15 26.03 0 -10 -6 14.52 2.2 0 -10 -6 12.36 2.04 0 10 6 8.74 3.2 0 10 6 22.17 2.35 0 -10 -6 6.7 3.09 0 -10 6 14.91 2.9 0 -10 6 14.07 2.46 0 -10 -7 22.96 3.93 0 -10 -7 29.16 2.54 0 10 7 33.47 4.13 0 -10 7 38.71 3.94 0 -10 -7 34.04 2.95 0 10 7 31.35 2.83 0 -10 7 35.54 3.08 0 -10 -8 576.87 21.84 0 10 8 563.71 21.9 0 -10 -8 599.99 19.23 0 -10 8 592.42 21.73 0 -10 8 712.16 20 0 10 8 581.01 19.86 0 -10 -8 593.32 20.01 0 -10 -9 849.46 30.24 0 -10 -9 908.11 27.6 0 10 9 825.74 28.45 0 -10 9 841.67 30.23 0 -10 -9 884.15 28.65 0 10 9 820.59 30.57 0 -10 10 66.98 5.51 0 -10 10 72.51 5.57 0 10 10 63.63 4.36 0 -10 -10 67.29 5.75 0 -10 -10 75.21 4.76 0 10 10 69.36 5.94 0 10 11 14.81 2.9 0 -10 -11 28.8 4.34 0 -10 11 17.1 3.78 0 10 11 13.52 3.97 0 -10 11 20.72 3.66 0 -10 -11 20.15 3.33 0 -10 12 84.21 6.26 0 10 12 75.03 5.25 0 -10 13 283.52 12.58 0 10 13 260.38 11.22 0 10 14 121.83 7.13 0 -10 14 127.98 8.06 0 10 15 6.07 3.58 0 -10 15 13.82 4.38 0 10 16 29.37 4.46 0 -10 16 37.72 5.32 0 10 17 100.74 7.19 0 -10 17 126.29 8.63 0 10 18 69.34 6.53 0 -10 18 87.25 7.76 0 -10 19 9.11 5.58 0 10 19 2.57 4.47 0 10 20 6.55 4.91 0 -12 0 595.99 19.41 0 -12 0 582.5 18.64 0 12 0 635.59 21.47 0 -12 0 590.45 23.23 0 -12 1 312.19 14.79 0 -12 1 321.54 10.87 0 -12 -1 325.35 11.59 0 -12 -1 329.96 11.02 0 12 -1 347.96 13.3 0 -12 1 336.7 11.76 0 12 1 342.53 13.54 0 12 1 314.28 10.81 0 -12 -1 339.74 15.52 0 -12 -2 40.56 5.19 0 -12 2 39.06 4.88 0 12 2 39.93 2.57 0 -12 -2 43.07 3.26 0 -12 -2 43.64 2.82 0 12 -2 37.76 4.01 0 -12 2 44.61 2.67 0 12 2 44.31 4.36 0 -12 2 45 3.37 0 -12 3 125.02 8.26 0 12 3 134.92 7.81 0 12 3 129.23 5.48 0 -12 -3 135.53 9.2 0 -12 -3 129.87 5.56 0 -12 -3 141.6 6 0 -12 3 131.7 5.2 0 -12 3 141.93 6.33 0 -12 4 301.78 14.26 0 12 4 313.06 11.25 0 -12 -4 327.44 11.38 0 -12 -4 335.95 11.74 0 12 4 317.02 13.96 0 -12 4 358.92 12.11 0 -12 5 327.46 11.24 0 12 5 288.32 13.06 0 12 5 303.02 10.56 0 -12 5 292.43 13.3 0 -12 -5 294.09 10.64 0 -12 -5 271.38 10.5 0 -12 6 143.55 8.48 0 -12 6 164.57 6.93 0 -12 -6 139.08 6.23 0 12 6 129.88 8.18 0 -12 -6 140.48 6.17 0 -12 -6 139.54 8.79 0 12 6 142.72 6.25 0 -12 7 311.28 10.65 0 -12 -7 263.26 10.12 0 -12 7 268.98 12.45 0 12 7 251.12 9.91 0 12 7 255.64 12.25 0 -12 -7 250.58 12.4 0 -12 -7 268.4 9.77 0 -12 -8 318.42 11.31 0 12 8 302.01 11.66 0 12 8 295.59 13.97 0 -12 -8 290.9 13.94 0 -12 8 392.74 12.39 0 -12 8 311.58 14.02 0 -12 -8 319.95 11.84 0 -12 9 381.37 15.73 0 -12 -9 363.71 15.81 0 -12 -9 380.02 13.57 0 12 9 355.55 13.26 0 12 9 371.48 15.89 0 12 10 149.82 9.18 0 -12 -10 161.89 7.55 0 -12 -10 150.49 9.4 0 12 10 152.71 7.28 0 -12 10 173.95 9.4 0 12 11 9.37 2.99 0 -12 11 5.16 3.95 0 -12 -11 17.96 4.7 0 -12 11 13.58 3.98 0 -12 12 382.96 16.68 0 12 12 387.24 14.68 0 -12 12 402.67 16.55 0 -12 -12 398.09 16.44 0 12 13 271.16 11.53 0 -12 13 282.38 13.17 0 -12 13 288.42 13.71 0 12 14 31.1 4.31 0 -12 14 34.27 5.46 0 12 15 5.12 3.79 0 -12 15 4.02 4.4 0 -12 16 66.95 6.85 0 12 16 66.09 5.79 0 12 17 109.42 7.47 0 12 18 45.66 5.74 0 12 19 12.97 4.61 0 -14 0 400.7 18.5 0 14 0 427.45 16.13 0 -14 0 398.7 13.32 0 -14 0 395.31 14.13 0 -14 -1 98.17 8.05 0 -14 1 90.73 5.15 0 -14 1 86.32 4.23 0 14 1 87.87 4.14 0 -14 -1 94.7 4.45 0 14 1 89.38 6.29 0 14 -1 99.8 6.31 0 -14 1 82.43 7.57 0 -14 -1 87.86 5.05 0 -14 -2 83.5 7.66 0 -14 -2 74.25 4.06 0 14 2 80.77 4 0 -14 2 84.34 4.88 0 -14 2 74.16 6.99 0 14 -2 79.46 5.73 0 14 2 77.26 5.99 0 -14 -2 73.52 4.5 0 -14 2 72.36 3.8 0 -14 -3 390.73 13.71 0 14 3 393.9 16.23 0 14 3 380.95 13.15 0 -14 -3 383.86 13.3 0 -14 3 379.31 17.59 0 -14 3 381.6 12.81 0 -14 -3 424.05 18.68 0 -14 3 431.78 14.26 0 -14 4 398.52 18.47 0 14 4 422.41 14.55 0 -14 -4 455.03 15.06 0 14 4 432.6 17.73 0 -14 4 425.1 14.09 0 -14 -4 427.52 14.69 0 -14 4 484.38 15.63 0 -14 5 60.8 3.35 0 -14 5 70.83 6.7 0 14 5 57.68 3.69 0 -14 5 67.88 4.56 0 -14 -5 62.69 4 0 14 5 70.92 6.12 0 -14 -5 57.76 3.99 0 14 6 129.2 6.13 0 -14 -6 137.74 6.27 0 14 6 130.71 8.49 0 -14 -6 136.07 6.31 0 -14 6 160.74 7.14 0 -14 6 120.77 8.83 0 -14 7 41.39 5.5 0 14 7 46.72 3.77 0 -14 -7 49.51 6.34 0 -14 -7 49.02 3.6 0 -14 7 61.17 4.51 0 -14 -7 55.44 4.03 0 14 7 46.97 5.54 0 14 8 375.19 16.67 0 -14 8 353.55 16.74 0 -14 -8 403.7 13.74 0 -14 -8 383.26 16.98 0 14 8 371.76 13.96 0 -14 8 485.84 15.09 0 -14 -8 378.04 14.13 0 14 9 221.38 9.11 0 14 9 210.5 11.49 0 -14 -9 214.58 11.63 0 -14 -9 213.38 9.16 0 -14 9 200.38 11.39 0 -14 -10 171.06 10.66 0 14 10 186.93 8.34 0 14 10 185.54 10.78 0 -14 10 175.29 10.46 0 14 11 72.62 5.11 0 -14 -11 83.44 7.43 0 -14 11 66.81 6.77 0 -14 12 123.48 8.64 0 -14 12 121.75 8.92 0 14 12 119 6.81 0 -14 -12 123.8 8.98 0 14 13 115.57 6.91 0 -14 -13 123.62 8.86 0 -14 13 131 9.27 0 14 14 132.08 7.52 0 14 15 7.96 3.63 0 14 16 50.64 5.38 0 14 17 41.41 5.49 0 14 18 60.5 6.17 0 14 19 5.59 4.48 0 -16 0 284.62 15.67 0 16 0 289.51 12.97 0 -16 0 286.66 10.26 0 -16 0 288.26 10.97 0 16 -1 537.96 19.5 0 16 1 516.85 19.45 0 -16 -1 502.34 22.65 0 -16 1 481.21 17.02 0 -16 1 488.33 22.13 0 -16 -1 508.06 16.4 0 -16 -1 466.26 16.81 0 16 2 55.35 3.56 0 -16 2 47.88 6.64 0 -16 2 55.92 4.35 0 -16 -2 54.82 3.7 0 -16 -2 56.05 7.27 0 -16 -2 58.71 4.17 0 16 -2 65.59 5.49 0 16 2 48.59 5.31 0 -16 -3 157.49 6.94 0 -16 3 164.08 7.51 0 16 3 154.74 8.99 0 -16 -3 157.1 6.78 0 -16 3 130.24 10.3 0 16 3 148.98 6.57 0 -16 -3 188.59 12.07 0 -16 4 143.24 10.26 0 16 4 155.19 9.28 0 16 4 152.56 6.55 0 -16 4 160.45 7.46 0 -16 -4 142.84 6.65 0 -16 -4 154.2 6.94 0 16 5 546.05 18.57 0 -16 -5 569.42 18.75 0 -16 -5 534.79 18.67 0 16 5 543.69 21.85 0 -16 5 643.05 19.73 0 -16 5 512.27 23.25 0 -16 -6 2.49 2.43 0 -16 6 -1.45 4.33 0 -16 -6 0.14 2.41 0 16 6 1.69 2.19 0 16 6 -0.72 4.16 0 -16 6 2.88 3.24 0 16 7 36.34 3.62 0 -16 -7 38.68 3.66 0 -16 -7 40.42 3.91 0 16 7 38.92 5.57 0 -16 7 34.13 6.09 0 -16 -7 29.73 6.02 0 -16 7 43.06 4.65 0 -16 -8 68.52 4.87 0 -16 8 95.94 6.02 0 -16 -8 46.3 6.85 0 -16 8 56.13 7.06 0 16 8 60.72 4.6 0 -16 -9 201.96 12.52 0 16 9 235.33 9.53 0 -16 9 218.1 12.91 0 -16 10 1.4 4.39 0 16 10 -0.55 3.1 0 -16 -10 6.37 5.12 0 16 11 2.35 3.41 0 -16 -11 2.37 5.06 0 -16 11 -4.21 4.63 0 -16 -12 70.94 7.65 0 16 12 63.57 5.4 0 -16 12 58.25 7.31 0 -16 13 120.3 9.72 0 -16 -13 109.43 8.73 0 16 13 112.45 6.78 0 16 14 2.98 3.59 0 -16 -14 12.04 5.62 0 16 15 3.63 4.07 0 16 16 18.14 4.53 0 16 17 68.38 6.34 0 16 18 13.35 5.11 0 -18 0 710.17 30.01 0 -18 1 31.87 6.6 0 -18 -1 30.9 6.42 0 -18 -2 9.92 5.52 0 18 2 9.25 2.42 0 -18 2 7.83 5.36 0 18 3 32.99 3.27 0 -18 3 28.02 6.06 0 -18 -3 41.47 7.68 0 18 4 540.13 18.14 0 -18 4 554.44 24.57 0 -18 5 33.39 6.73 0 18 5 28.8 3.43 0 -18 6 28.19 5.98 0 18 6 22.67 3.34 0 -18 -7 -1.78 6.15 0 -18 7 7.91 5.19 0 18 7 3.37 2.87 0 18 8 174.29 8.04 0 -18 -8 171.25 11.79 0 -18 8 186.73 12.69 0 -18 9 40.44 7.09 0 18 9 23.68 3.73 0 -18 -9 26.73 6.45 0 -18 -10 49.68 7.19 0 -18 10 32.78 6.94 0 18 10 31.13 4.23 0 -18 11 3.4 5.58 0 -18 -11 3.92 5.56 0 18 11 6.97 3.7 0 -18 -12 59.64 7.79 0 -18 12 51.11 8.33 0 18 12 51.21 5.22 0 18 13 5.07 4.13 0 -18 -13 13.95 5.98 0 18 14 39.59 5.28 0 -18 -14 57.24 7.68 0 18 15 6.35 4.64 0 18 16 21.32 5.17 0 18 17 7.11 4.79 0 -20 0 32.07 6.95 0 -20 -1 77.88 9.33 0 -20 1 79.87 9.75 0 -20 2 2.05 5.57 0 -20 -2 -2.07 5.77 0 -20 -3 61.1 8.84 0 -20 3 69.3 8.88 0 -20 4 2.65 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1 10 715.24 23.98 1 1 10 700.87 23.64 -1 -1 -10 710.59 23.67 -1 -1 10 707.37 24.08 -1 1 10 769.91 24.01 -1 1 -10 730.22 23.93 1 -1 10 692.37 23.62 -1 1 -11 415.23 14.76 1 -1 11 397.56 14.39 1 1 11 378.34 14.31 -1 -1 11 406.35 14.86 -1 1 11 410.99 14.59 -1 -1 -11 419.52 14.57 -1 1 11 385.82 14.61 -1 1 -12 173.87 8.27 -1 1 12 191.07 8.48 -1 -1 12 197.62 8.12 -1 -1 12 167.86 8.21 -1 -1 -12 168.27 8.01 1 -1 12 161.13 7.82 -1 1 12 164.67 8.09 1 1 12 161.22 7.81 -1 -1 -13 5.71 3.01 -1 1 13 -1.52 2.74 1 -1 13 4.89 2.69 1 1 13 6.85 2.74 -1 1 -13 4.44 3.08 -1 -1 13 4.14 2.63 -1 1 13 7.36 3.76 -1 1 -14 186.2 9.23 1 -1 14 176.99 8.66 -1 -1 14 193.88 9.12 -1 1 14 160.29 8.75 1 1 14 181.55 8.66 -1 1 15 190.2 9.97 -1 -1 15 228.97 10.37 1 -1 15 217.53 10.03 1 1 15 221.09 9.99 -1 -1 16 168.48 9.19 1 1 16 180.01 9.11 1 -1 16 181.32 9.16 -1 1 16 171.14 9.11 -1 -1 17 -1.69 3.74 -1 1 17 6.87 3.75 1 -1 17 -2.68 3.62 1 1 17 2.44 3.76 1 1 18 42.9 5.13 -1 1 18 38.72 5.22 -1 -1 18 37.48 5.01 1 -1 18 35.03 5.05 1 1 19 115.24 8.02 -1 1 19 117.41 8.21 -1 -1 19 114.68 7.97 1 -1 19 119.02 8.08 -1 1 20 97.26 7.35 1 -1 20 91.73 7.67 1 1 20 95.77 7.6 -1 -1 20 81.18 7.42 -1 -1 21 2.02 4.88 1 -1 21 3.37 4.83 -1 1 21 -0.33 4.74 1 1 21 4.91 4.83 1 -1 22 15.03 5.46 1 1 22 6.14 5.07 1 -3 0 0.05 0.33 1 3 0 0.15 0.51 1 3 0 1.03 0.37 -1 -3 0 0.22 0.6 1 -3 0 0.21 0.5 -1 3 0 -0.03 0.39 -1 -3 0 -0.4 0.84 -1 -3 1 1721.43 51.12 -1 3 -1 1762.27 51.27 -1 3 1 1808.3 51.29 -1 3 1 1729.14 51.12 1 3 1 1860.96 51.89 -1 -3 -1 1705.95 51.36 1 -3 1 1734.78 51.26 1 -3 -1 1733.48 51.13 -1 -3 1 1724.45 52.44 1 -3 -1 1813.83 51.29 -1 -3 -1 1749.18 51.81 1 -3 -1 1771.27 51.8 -1 3 1 1785.05 51.06 1 3 1 1726.91 51.37 1 3 -1 1684.88 52.2 -1 -3 2 1595.99 46.82 1 -3 2 1543.87 45.59 -1 -3 -2 1550.7 45.82 1 3 2 1553.21 45.8 -1 3 2 1504.47 46 1 3 -2 1563.65 46.46 1 -3 2 1525.56 45.4 -1 3 2 1591.48 45.67 1 -3 -2 1568.65 45.6 -1 3 -2 1553.4 45.59 -1 3 2 1568.43 45.6 1 -3 -2 1532.94 45.76 -1 -3 -2 1604.81 46.37 1 -3 -2 1571.83 46.28 1 3 2 1628.28 46.45 1 3 3 1917.15 55.81 -1 3 3 1848.45 55.44 1 -3 -3 1893.64 54.79 1 -3 3 1874.18 54.8 -1 3 3 1884.39 54.78 -1 -3 3 1769.83 55.69 1 3 -3 1876.38 55.26 1 3 3 1876.82 55.19 1 -3 -3 1941.16 55.67 -1 3 -3 1897.06 54.79 -1 3 3 1898.75 55.14 1 -3 3 1846.01 54.89 -1 3 -3 1845.2 55.03 1 -3 -3 1872.88 55.26 -1 -3 -3 1875.81 55.14 -1 -3 4 180.11 6.87 -1 3 -4 201.41 6.81 -1 3 -4 201.18 6.29 -1 -3 -4 193.26 6.82 -1 3 4 186.95 7.04 1 -3 -4 200.11 6.28 1 -3 4 202.68 6.67 1 -3 -4 185.5 7.23 1 -3 -4 199.34 7.04 1 3 4 202.27 7.53 1 3 4 201.25 6.85 1 -3 4 191.73 6.28 -1 3 4 194.5 6.86 -1 3 4 194.4 6.27 1 -3 5 858.77 26.9 -1 -3 5 863.3 26.96 -1 3 5 884.31 26.27 1 -3 -5 854.14 27.44 1 -3 5 894.23 26.26 1 3 5 907.87 27.07 -1 3 -5 913.13 27.15 1 3 5 910.15 27.83 1 -3 -5 934.32 27.45 -1 -3 -5 911.13 27.07 -1 3 -5 872.07 26.26 -1 3 5 916.96 27.19 1 -3 -5 873.48 26.24 -1 3 5 890.12 27.25 -1 3 -6 736.18 22.11 1 -3 6 703.39 20.87 -1 3 6 703.95 20.89 1 -3 6 694.08 21.81 1 -3 -6 708.45 20.83 1 3 6 683.28 21.9 -1 3 6 706.39 22.03 1 -3 -6 722.61 22.36 1 3 6 675.83 22.44 1 -3 -6 670.27 22.04 -1 -3 -6 684.88 21.83 -1 3 -6 702.03 20.91 -1 3 -7 1778.06 51.37 1 -3 -7 1773.89 51.65 -1 3 -7 1686.98 49.76 -1 3 7 1737.58 49.79 1 3 7 1716.42 51.12 1 -3 -7 1644.37 49.69 1 -3 7 1631.57 50.95 1 -3 -7 1665.3 51.03 -1 -3 -7 1704.03 51.01 1 3 7 1815.63 51.82 1 -3 7 1698.84 49.72 -1 3 7 1782.07 51.6 -1 3 7 1679.33 51.16 -1 3 -8 288.3 10.52 -1 -3 8 259.81 10.93 -1 -3 -8 282.55 10.13 1 -3 8 278.54 8.65 -1 3 8 292.07 8.75 -1 3 -8 277.11 8.7 1 -3 -8 270.94 8.61 1 -3 -8 298.65 10.79 -1 3 8 281.68 10.28 -1 3 8 287.29 10.57 1 3 8 287.28 10.71 1 3 8 275.4 10.13 1 -3 8 268.14 10.04 1 -3 -9 223.44 9.17 -1 3 9 203.28 8.53 -1 3 9 232.31 7.06 -1 3 -9 227.2 8.99 -1 3 9 200 8.9 -1 -3 9 208.8 9.27 1 3 9 207.41 9.07 1 -3 9 200.81 8.43 -1 3 -9 219.78 6.97 1 3 9 206.95 8.45 -1 -3 -9 215.81 8.5 1 3 10 360.86 13.01 -1 3 -10 371.8 13.46 1 -3 -10 365.87 13.68 -1 -3 -10 370.22 13.07 1 3 10 360.99 13.62 -1 3 10 349.2 13.43 -1 3 10 353.33 13.05 1 -3 10 357.76 12.96 -1 -3 10 352.35 13.72 -1 3 -11 1150.75 35.22 -1 3 11 1136.51 35.27 -1 3 11 1066.61 34.68 1 -3 -11 1135.61 35.49 -1 -3 11 1071 35.36 1 -3 11 1030.17 34.48 1 3 11 1071.72 34.59 1 3 11 1082.47 35.2 -1 -3 -11 1145.33 34.71 1 -3 -12 170.04 8.35 1 3 12 155.42 8.23 -1 3 12 162.95 8.23 -1 -3 12 145.12 7.69 1 -3 12 147.18 7.25 -1 3 12 133.3 7.16 1 3 12 156.37 7.42 -1 -3 -12 152.36 7.26 1 -3 13 8.62 2.81 1 -3 -13 4.11 3.32 -1 -3 -13 11.17 3.08 -1 3 13 1.22 3.92 1 3 13 7.32 2.86 -1 -3 13 8.83 2.79 1 3 13 13.97 4.21 -1 3 13 5.03 2.65 1 -3 14 146.39 7.7 -1 3 14 142.6 7.84 1 3 14 167.95 8.85 -1 -3 14 129.61 7.78 1 3 14 155.95 7.79 1 -3 15 540.66 20.04 1 3 15 559.48 20.08 -1 3 15 565.6 20.12 -1 -3 15 553.18 20.53 -1 -3 16 93.23 6.66 1 -3 16 96.58 6.59 -1 3 16 84.89 6.35 1 3 16 81.48 6.19 -1 3 17 26.4 4.37 -1 -3 17 23.83 4.64 1 3 17 29.27 4.51 1 -3 17 21.66 4.5 -1 3 18 43.49 5.09 -1 -3 18 51.09 5.69 1 3 18 47.76 5.56 1 -3 18 48.9 5.6 1 3 19 144.99 9.05 -1 3 19 147.34 8.94 1 -3 19 165.19 9.43 -1 -3 19 146.15 9.3 -1 3 20 42.94 5.47 1 3 20 27.87 5.34 1 -3 20 41.32 5.95 -1 -3 20 35.92 5.7 -1 -3 21 21.84 5.65 1 -3 21 19.67 5.59 -1 3 21 16.53 5.18 1 3 21 16.09 5.57 1 -3 22 12.12 5.5 1 -5 0 -0.25 0.79 -1 5 0 -0.31 0.69 1 -5 0 0.28 0.36 1 5 0 0.16 0.37 1 -5 0 0.2 0.4 1 -5 0 0.11 1.02 -1 5 0 0.02 0.35 1 5 0 0.29 1.44 1 5 0 0.15 0.71 -1 -5 0 -0.74 0.85 -1 -5 -1 187.98 6.16 1 -5 1 183.66 6.07 1 5 1 198.13 7.64 1 5 1 186.85 6.13 -1 5 1 165.73 5.59 -1 -5 1 198.04 8.06 1 5 -1 180.4 7.38 1 -5 -1 181.95 6.05 1 -5 -1 184.99 5.74 1 -5 1 183.2 5.45 -1 5 1 168.36 6.7 -1 5 1 181.35 5.65 -1 5 1 168.78 6.05 -1 -5 1 185.28 6.09 -1 -5 1 174.58 5.63 -1 5 -1 175.85 6.05 1 -5 -1 181.53 7.01 -1 5 2 1663.09 48.31 1 -5 -2 1616.07 49.63 -1 -5 -2 1672.26 49.49 -1 -5 2 1670.43 50.36 1 5 -2 1693.13 49.64 -1 -5 -2 1652.78 48.41 1 -5 -2 1599.92 48.2 -1 5 2 1689.21 48.07 1 5 2 1632.56 48.4 -1 5 2 1599.6 49.12 1 -5 2 1639.33 48.25 -1 5 -2 1565.97 48.22 1 -5 -2 1654.01 48.13 -1 5 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282.56 9.87 -2 -10 8 226.51 11.83 2 10 8 259.89 10.34 2 -10 8 273.75 9.52 -2 10 8 265.29 9.87 -2 -10 -8 271.81 10.27 2 -10 -8 264.03 9.3 2 -10 8 257.9 9.8 2 -10 -9 353.88 12.85 -2 10 -9 335.37 11.66 2 10 9 318.35 12.52 2 -10 9 345.28 11.5 -2 10 9 322.75 12.03 -2 -10 -9 338.19 12.37 -2 -10 9 297.56 14 -2 10 9 350.74 11.92 2 -10 -9 306.82 13.59 2 -10 -10 52.98 4.54 -2 10 -10 54.06 3.66 2 -10 -10 43.89 5.08 2 10 10 58.17 4.42 -2 10 10 50.77 3.96 -2 -10 -10 50.74 4.12 2 10 11 2.9 2.78 2 -10 -11 3.1 2.89 -2 10 11 1.22 2.4 2 -10 -11 7.31 3.83 2 -10 -12 175.04 8.6 2 -10 -12 166.86 8.93 2 10 12 153.28 7.93 -2 10 12 152.15 7.57 2 -10 -13 252.59 11.54 2 10 13 247.19 10.94 -2 10 13 239.71 10.42 -2 -10 14 85.6 7.61 2 10 14 83.29 6.3 -2 10 14 91.99 6.03 2 10 15 7.07 3.74 -2 10 15 0.23 3.35 -2 -10 15 -0.36 4.62 2 10 16 19.18 4.43 -2 10 16 16.73 4.16 -2 -10 16 14.03 4.64 -2 -10 17 131.99 9.63 2 10 17 153.06 8.76 -2 10 17 159.13 8.71 -2 -10 18 85.48 7.85 2 10 18 74.37 6.71 -2 10 18 78.95 6.73 2 10 19 2.04 4.58 -2 10 19 -2 4.72 -2 -10 19 3.75 4.86 -2 -10 20 6.52 5.28 -2 10 20 5.34 4.79 -2 12 0 154.29 6.63 2 12 0 163.03 8.79 2 -12 0 141.86 8.34 2 -12 0 144.9 6.39 -2 -12 0 166.75 6.56 -2 12 -1 169.21 7.19 2 -12 -1 153.43 9.05 -2 12 1 173.21 7.24 2 -12 1 160.7 8.89 2 12 -1 162.91 8.94 2 12 1 181.62 6.97 2 -12 1 160.28 6.82 2 12 1 163.28 9.32 -2 12 1 174.07 5.77 2 -12 -1 157.77 6.77 -2 -12 1 180.68 6.95 -2 -12 -1 180.54 7.05 -2 -12 -2 162.54 8.65 -2 12 2 145.67 6.32 -2 12 -2 143 6.21 -2 -12 2 152.25 9.87 2 12 2 131.08 8.04 2 -12 -2 129.8 8.05 2 -12 2 138.17 7.95 2 12 2 144.82 6.15 2 -12 2 136.78 6.02 2 -12 -2 130.41 5.9 -2 -12 2 142.11 5.96 -2 12 2 131.12 4.99 -2 -12 -2 143.27 6.15 2 12 -2 137.14 7.9 -2 12 3 311.4 11.43 -2 -12 -3 320.97 13.9 -2 12 -3 307.25 11.35 2 12 3 299.25 13.68 2 -12 -3 291.35 13.6 2 -12 3 315.03 13.49 2 12 3 328.69 11.39 2 -12 3 299.11 11.13 2 -12 -3 298.25 11.01 -2 12 3 306.41 10.27 -2 -12 -3 335.87 11.45 -2 -12 3 313.67 15.54 -2 -12 3 335.37 11.17 -2 -12 3 329.38 10.14 -2 12 3 313.01 10.08 2 -12 -3 316.99 10.65 2 12 -3 317.14 13.18 -2 -12 4 394.04 18.5 2 -12 -4 375.95 16.83 2 12 -4 463.75 16.47 2 -12 4 432.41 17.04 -2 12 4 437.76 16.12 -2 -12 -4 463.92 17.61 -2 -12 4 442.55 14.45 2 -12 4 425.75 14.51 2 12 4 425.17 14.69 2 -12 -4 405.09 14.32 -2 12 4 422.85 13.79 -2 -12 -4 438.23 14.72 -2 -12 4 467.9 13.61 -2 12 4 430.58 13.47 2 12 4 387.8 17.34 2 -12 -4 425.3 14.18 -2 12 4 409.98 14.67 -2 12 -4 416.99 14.66 -2 -12 -5 274.24 12.64 -2 12 -5 272.8 10.39 2 12 5 278.56 13.12 2 -12 -5 263.27 12.61 -2 -12 5 253.74 13.66 2 12 -5 281.63 11.64 -2 12 5 280.78 11.69 2 -12 5 312.11 12.91 2 12 5 286.23 10.59 2 -12 5 282.86 10.36 2 -12 -5 279.36 10.16 -2 12 5 282.15 10.52 -2 12 5 286.12 9.76 -2 -12 -5 298.09 10.63 2 -12 -5 288.15 10.23 -2 -12 -6 31.53 4.91 -2 -12 -6 30.32 3.3 2 12 -6 42.29 3.93 2 12 6 37.75 4.98 2 -12 -6 31.87 4.48 -2 -12 6 34.74 5.26 2 -12 -6 32.07 2.97 -2 12 6 45.53 4.21 -2 12 -6 31.44 3.17 -2 12 6 33.44 3.22 2 -12 6 32.9 3.17 2 12 6 35.32 3.51 -2 12 6 40.26 2.83 2 -12 -6 41.29 3.26 -2 -12 -7 62.01 6.04 -2 12 7 53.91 4.02 2 12 7 54.79 5.79 -2 12 7 50.97 3.38 -2 -12 7 32.17 5.04 -2 12 7 51.21 4.6 2 12 7 45.23 3.82 2 -12 7 52.68 3.74 2 -12 -7 53.32 3.44 -2 -12 -7 56.57 4.05 -2 12 -7 52.1 3.87 2 -12 -7 57.87 3.9 -2 12 8 490.42 15.85 -2 12 -8 461.55 15.55 2 12 8 465.08 18.94 -2 -12 8 385.44 18.26 2 12 8 413.14 15.75 2 -12 8 466.89 15.27 2 -12 -8 455.64 14.93 -2 12 8 437.52 15.22 -2 -12 -8 439.91 15.78 -2 -12 -8 421.72 17.61 2 -12 -8 477.24 15.96 2 -12 -9 327.19 14.13 -2 -12 9 296.52 14.64 -2 -12 -9 316.97 14.13 2 12 9 329.36 12.6 -2 12 9 341.07 11.98 2 12 10 47.23 4.54 2 -12 -10 39.22 5.27 -2 12 10 46.61 3.9 2 12 11 25.21 3.8 -2 12 11 24.9 3.47 2 -12 -11 19.34 4.6 2 -12 -12 129.84 8.22 2 12 12 116.11 7.02 -2 12 12 120.86 6.54 2 -12 -13 258.33 12.34 2 12 13 253.34 11.09 -2 12 13 245.39 10.69 -2 -12 14 84.84 7.83 2 12 14 102.52 6.6 -2 12 14 84.08 6.01 2 -12 -14 101.6 7.45 2 12 15 5.78 4.03 -2 12 15 -1.59 3.77 -2 -12 15 4.33 5.06 -2 -12 16 112.16 8.79 2 12 16 104.02 7.35 -2 12 16 96.62 6.9 -2 12 17 70.59 6.3 2 12 17 88.17 6.79 -2 -12 17 73.53 7.89 2 12 18 33.88 5.52 -2 12 18 19.23 5.01 -2 -12 18 27.17 6.26 -2 12 19 8.65 4.85 2 12 19 16.39 5.24 -2 -12 19 19.44 6.14 2 14 0 388.15 16.4 2 -14 0 379.56 16.98 2 -14 0 357.61 13.49 -2 -14 0 426.33 13.64 -2 14 0 391.23 14.08 -2 14 -1 119.08 6.04 -2 14 1 112.93 6 2 14 1 108.06 7.57 2 14 -1 112.85 7.66 2 -14 1 112.88 7.92 -2 -14 -1 124.6 5.79 2 -14 1 102.53 5.48 2 -14 -1 113.35 5.56 2 -14 -1 109.81 7.97 -2 -14 1 121.46 5.57 2 14 2 2.55 1.96 -2 -14 2 3.25 2.24 -2 -14 2 8.55 4.54 2 -14 2 1.62 2.26 2 14 2 -1.37 3.07 2 -14 -2 2.31 2.94 2 -14 2 4.93 3.34 -2 14 -2 2.65 2.46 -2 14 2 0.5 2.34 2 14 -2 2.99 3.05 2 -14 -2 4.18 2.29 -2 -14 -2 5.57 2.43 2 14 -3 58.25 5.35 2 14 3 50.97 3.77 -2 14 -3 46.82 3.91 -2 -14 -3 47.03 6.02 -2 -14 3 51.97 6.62 2 -14 -3 45.7 5.36 2 -14 3 48.76 5.34 2 -14 3 47.97 3.8 2 -14 -3 45.24 3.73 2 14 3 51.39 5.68 -2 -14 3 47.81 3.64 -2 -14 -3 54.6 3.91 -2 14 3 51.77 4.11 -2 14 4 378.27 13.31 -2 -14 4 331.97 17.01 2 14 4 318.79 15.58 2 -14 4 361.76 15.57 -2 14 4 347.99 14.25 -2 14 -4 350.34 13.08 2 14 -4 377.15 14.66 -2 -14 4 360.59 12.42 2 -14 4 332.92 12.54 2 -14 -4 355.29 12.52 2 14 4 353.31 12.72 -2 -14 -4 370.28 12.8 2 -14 -4 311.97 15.43 -2 -14 -4 363.35 16.19 -2 14 -5 162.75 7.5 -2 -14 -5 175.48 10.2 -2 -14 5 156.83 10.67 2 14 5 155.58 9.59 2 -14 5 150.3 9.21 2 14 -5 178.97 8.7 -2 14 5 162.97 8.48 -2 -14 5 162.98 6.95 2 -14 5 162.16 7.16 2 -14 -5 158.11 6.94 -2 14 5 170.88 7.72 2 14 5 161.25 7.24 -2 -14 -5 166.91 7.34 2 -14 -5 148.25 9.35 2 -14 6 152.61 6.87 -2 14 6 162.47 7.38 -2 -14 -6 147.77 9.53 2 14 6 125.7 9 -2 14 6 156.79 8.27 2 -14 6 140.61 8.93 2 14 -6 162.5 8.09 2 -14 -6 146.61 6.55 2 14 6 152.08 7.01 -2 -14 -6 141.34 6.79 -2 -14 6 135.64 10.12 2 -14 -6 130.81 8.86 2 -14 7 249.74 12.44 -2 -14 7 218.56 13.17 2 14 7 248.47 10.14 2 -14 7 271.28 9.97 2 -14 -7 246.54 9.44 -2 -14 -7 233.73 12.25 -2 -14 -8 255.06 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5.74 -2 -18 6 14.9 6.27 2 -18 6 20.33 5.5 2 18 7 10.9 3.36 -2 -18 -7 11.39 6.26 -2 -18 7 4.93 5.35 2 -18 7 16.1 5.46 -2 -18 8 165.71 12.42 2 18 8 145.42 7.8 2 -18 8 175.13 11.44 -2 -18 -8 183.62 11.7 2 18 9 12.23 3.76 -2 -18 9 7.85 5.74 2 -18 9 10.94 5.2 -2 -18 -9 12.78 6.33 2 18 10 41.42 4.88 2 -18 -10 23.41 5.99 2 -18 10 35.33 6.58 -2 -18 -10 61.41 7.87 -2 -18 -11 5.98 5.81 2 18 11 2.44 3.52 2 -18 -11 -4.72 5.41 2 -18 11 -0.52 4.85 2 -18 12 65.37 8.2 2 18 12 53.4 5.59 2 -18 -12 62.2 7.72 2 18 13 14.49 4.56 2 -18 13 16.21 6.66 2 -18 -13 7.9 5.44 2 -18 -14 41.26 7.07 2 18 14 33.25 5.48 2 -18 14 49.48 8.34 2 -18 15 3.44 6.38 2 18 15 4.79 4.84 2 18 16 12.26 5.26 2 -18 16 14.31 7.28 2 -20 0 1.17 5.32 2 -20 -1 88.76 9.19 2 -20 1 74.31 8.95 -2 -20 2 19.1 7.18 2 -20 -2 11.11 5.8 2 -20 2 13.56 5.7 -2 -20 3 73.78 9.81 2 -20 -3 59.85 7.97 2 -20 3 64.03 8.1 -2 -20 -3 58.73 8.94 -2 -20 -4 0.52 6.85 2 20 4 12.05 3.24 -2 -20 4 13.09 6.52 2 -20 -4 3.88 5.24 2 -20 4 5.86 5.26 -2 -20 -5 94.18 10.24 2 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7.86 -7 -3 14 41 5.54 -7 3 14 34.72 5.43 -7 -3 15 75.95 9.66 -7 5 0 3.82 2.95 -7 5 -1 38.64 4.25 -7 5 1 44.18 4.26 -7 5 -2 406.02 14.53 -7 5 2 374.45 14.42 -7 5 -3 54.98 4.69 -7 5 3 63.67 4.84 -7 5 -4 17.99 3.48 -7 5 4 20.37 3.46 -7 5 -5 38.06 4.16 -7 5 5 30.95 4.08 -7 5 -6 227.93 9.79 -7 -5 6 245.6 10.61 -7 5 6 238.32 10.5 -7 5 6 226.33 9.84 -7 -5 7 46.26 4.85 -7 5 7 37.46 4.74 -7 5 -7 40.96 4.22 -7 5 7 43.48 4.42 -7 5 -8 42.25 4.27 -7 -5 8 48 5.13 -7 5 8 40.84 5.03 -7 5 8 44.45 4.5 -7 -5 9 0.96 3.61 -7 5 9 4.73 3.83 -7 -5 10 175.63 9.02 -7 5 10 167.24 8.89 -7 -5 11 36.39 5.12 -7 5 11 47.47 5.31 -7 -5 12 90.92 6.72 -7 5 12 94.6 6.93 -7 -5 13 1.53 4.13 -7 5 13 3.53 4.24 -7 -5 14 58.89 9.47 -7 -5 14 52.61 5.99 -7 5 14 53.77 6.14 -7 7 0 1.47 3.08 -7 7 -1 197.1 8.65 -7 7 1 184.39 8.69 -7 7 -2 43.14 4.42 -7 7 2 46.26 4.3 -7 7 -3 241.1 10.07 -7 7 3 234.73 10.06 -7 7 -4 -1.82 3.07 -7 7 4 0.73 3.16 -7 7 -5 74.54 5.36 -7 7 5 69.52 5.26 -7 -7 6 33.65 4.53 -7 7 6 37.02 4.52 -7 7 -6 37.21 4.19 -7 7 6 27.62 3.99 -7 7 -7 200.71 8.9 -7 7 7 196.29 8.89 -7 -7 7 202.46 9.57 -7 7 7 200.79 9.58 -7 -7 8 -0.23 3.75 -7 7 8 2.01 3.55 -7 7 -8 1.41 3.28 -7 7 8 0.36 3.1 -7 -7 9 14.96 4.21 -7 7 9 17.75 4.24 -7 -7 10 12.26 4.1 -7 7 10 11.97 4.22 -7 -7 11 222.46 10.52 -7 7 11 208.41 10.3 -7 -7 12 7.4 4.24 -7 7 12 5.3 4.26 -7 -7 13 4.54 4.2 -7 7 13 0.5 4.22 -7 -7 14 19.08 4.94 -7 7 14 18.64 5.1 -7 9 0 -1.31 3.21 -7 9 -1 6.54 3.15 -7 9 1 5.23 3.13 -7 9 -2 350.02 13.4 -7 9 2 349.88 13.39 -7 9 -3 6.09 3.28 -7 9 3 4.09 3.03 -7 9 -4 4.21 3.36 -7 9 4 10.18 3.46 -7 9 -5 6.77 3.35 -7 9 5 9.02 3.38 -7 9 -6 199.49 9.07 -7 9 6 210.05 9.35 -7 -9 7 8.59 3.88 -7 9 7 5.14 3.54 -7 9 -7 0.54 3.06 -7 9 7 5.39 3.29 -7 -9 8 41.51 4.85 -7 9 8 35.09 4.63 7 9 8 40.66 4.81 -7 9 -8 29.41 4.09 -7 9 8 32.07 4.2 -7 -9 9 0.7 3.73 -7 9 9 2.24 3.81 7 9 9 0.23 4.04 7 9 10 121.32 7.72 -7 -9 10 131.7 7.93 -7 9 10 131.71 7.66 -7 -9 11 2.18 3.9 -7 9 11 3.04 3.93 -7 9 12 57.78 5.7 -7 -9 12 60.76 6.04 -7 -9 13 6.23 4.38 -7 9 13 0.72 4.09 -7 11 0 0.96 3.37 -7 11 -1 127.39 6.96 -7 11 1 124.57 6.92 -7 11 -2 2.86 3.22 -7 11 2 -2.11 3.2 -7 11 -3 153.08 7.56 -7 11 3 144.83 7.67 -7 11 -4 2.27 3.07 -7 11 4 3.44 3.42 -7 11 5 49.18 4.86 -7 11 -5 58.18 4.88 -7 11 -6 5.99 3.53 -7 11 6 2.1 3.36 -7 11 -7 147.25 7.65 -7 11 7 141.58 7.63 7 11 8 6.9 4.16 -7 11 -8 2.79 3.48 -7 11 8 0.19 3.58 7 11 9 9.77 4.58 7 11 10 3.64 4.52 7 11 11 129.91 8.08 7 11 12 1.83 4.69 7 11 13 0.27 4.76 -7 13 0 3.24 3.44 -7 13 -1 3.04 3.65 -7 13 1 2.64 3.37 -7 13 -2 185.83 8.81 -7 13 2 176.31 8.81 -7 13 -3 5.03 3.64 -7 13 3 2.84 3.4 -7 13 -4 7.43 3.7 -7 13 4 9.12 3.7 -7 13 -5 4 3.7 -7 13 5 1.22 3.61 -7 13 -6 116.74 6.87 -7 13 6 128.66 7.25 -7 13 -7 5.16 3.75 -7 13 7 -0.41 3.45 -7 13 -8 30.9 4.49 -7 13 8 25.41 4.39 7 13 9 2.71 4.29 7 13 10 72.06 6.56 7 13 11 4.92 4.62 -7 15 0 -1.49 3.67 -7 15 1 64.31 5.55 -7 15 -1 75.58 5.77 -7 15 -2 6.6 3.86 -7 15 2 11.99 4.16 -7 15 -3 74.82 5.96 -7 15 3 77.48 5.9 -7 15 -4 0.64 3.79 -7 15 4 1.07 3.89 -7 15 -5 35.9 4.92 -7 15 5 31.67 4.9 -7 15 -6 12.19 4.19 -7 15 6 11.11 4.48 -7 15 -7 72.05 6.14 -7 15 7 76.79 6.19 -7 15 -8 2.51 4.07 -7 15 8 4.31 4.3 -7 17 0 -0.45 4 -7 17 -1 5.63 4.24 -7 17 1 4.96 4.09 -7 17 -2 90.83 6.54 -7 17 2 93.3 6.62 -7 17 -3 11.75 4.49 -7 17 3 12.96 4.44 -7 17 -4 3.1 4.04 -7 17 4 -0.22 3.95 7 -17 5 7.96 4.47 -7 17 -5 1.54 3.99 -7 17 5 1.79 4.09 7 -17 6 42.33 6.22 -7 17 -6 56.56 5.53 -7 17 6 51.39 5.66 7 -17 7 12.97 5.23 -7 17 -7 11.65 4.34 -7 17 7 12.85 4.35 -8 0 0 437.31 16.2 -8 0 -1 -2.44 3.53 -8 0 1 -0.2 3.41 -8 0 -2 4.69 3.44 -8 0 2 2.85 3.52 -8 0 -3 2.64 3.54 -8 0 3 1.63 3.4 -8 0 -4 204.43 9.5 -8 0 4 201.77 9.41 -8 0 -5 -2.42 3.55 -8 0 5 3.48 3.54 -8 0 -6 21.62 4.12 -8 0 6 20.06 4.34 -8 0 -7 -2.79 3.6 -8 0 7 0.41 3.61 -8 0 -8 184.81 8.82 -8 0 8 175.12 8.88 -8 0 8 175.85 9.55 -8 0 9 2.41 4.45 -8 0 10 87.54 7.16 -8 0 11 -0.83 4.54 -8 2 0 3.24 3.59 -8 -2 0 4.62 3.81 -8 2 -1 203.04 9.27 -8 2 1 198.57 9.12 -8 -2 -1 185.09 9.23 -8 -2 1 192.07 9.36 -8 -2 -2 -1.88 3.46 -8 -2 2 -2.54 3.52 -8 2 -2 0.81 3.48 -8 2 2 -0.81 3.54 -8 2 -3 128.02 7.23 -8 2 3 122.65 7.02 -8 -2 -3 119.16 7.03 -8 -2 3 121.62 7.28 -8 2 -4 3.86 3.63 -8 -2 -4 2.92 3.68 -8 2 4 4.87 3.63 -8 -2 4 -0.85 3.96 -8 2 -5 128.48 7.32 -8 2 5 129.69 7.18 -8 -2 -5 115.64 7.24 -8 -2 5 120.1 7.29 -8 -2 -6 -0.62 3.54 -8 -2 6 1.09 3.96 -8 2 -6 1.01 3.8 -8 2 6 -2.05 3.75 -8 -2 -7 15.68 4.16 -8 -2 7 15.27 4.39 -8 2 -7 20.1 4.18 -8 2 7 18.52 4.08 -8 -2 8 5.01 4.41 -8 2 8 3.93 4.43 -8 2 -8 -1.8 3.85 -8 2 8 5.38 3.98 -8 -2 -8 4.81 3.76 -8 -2 8 3.07 4.22 -8 -2 9 236.78 11.71 -8 2 9 258.22 11.86 -8 -2 10 3.26 4.17 -8 2 10 5.93 4.32 -8 -2 11 8.04 4.86 -8 2 11 7.71 4.79 -8 4 0 407.47 15.47 -8 4 -1 11.74 3.9 -8 4 1 13.35 4.04 -8 4 -2 -1.86 3.54 -8 4 2 0.41 3.57 -8 4 -3 5.56 3.81 -8 4 3 1.02 3.5 -8 4 -4 192.75 9.2 -8 4 4 191.34 9.11 -8 4 -5 13.7 3.77 -8 4 5 16.13 4.01 -8 4 -6 21.96 4.23 -8 4 6 22.98 4.43 -8 -4 -6 18.81 4.24 -8 -4 7 0.23 4.08 -8 4 -7 3.42 3.66 -8 4 7 5.53 3.75 -8 -4 -7 -0.83 3.9 -8 -4 -8 158.28 8.34 -8 -4 8 156.31 8.72 -8 4 -8 157.4 8.17 -8 -4 8 158.88 9.02 -8 4 8 167.33 9.07 -8 4 8 138.61 8 -8 -4 9 18.13 4.9 -8 4 9 21.83 5 -8 -4 10 74.81 6.53 -8 4 10 71.34 6.42 -8 -4 11 4.41 4.6 -8 4 11 0.27 4.48 -8 6 0 34.48 4.78 -8 6 -1 141.64 7.8 -8 6 1 154.79 8.09 -8 6 -2 3.3 3.61 -8 6 2 1.85 3.55 -8 6 -3 92.22 6.19 -8 6 3 98.66 6.44 -8 6 -4 30.86 4.35 -8 6 4 33.97 4.55 -8 6 -5 88.61 6.21 -8 6 5 92.13 6.38 -8 6 -6 2.23 3.63 -8 6 6 4.5 3.69 -8 6 -7 8 3.78 -8 6 7 9.19 4.07 -8 -6 8 35.68 5.23 -8 6 8 25.29 4.94 -8 6 -8 29.78 4.55 -8 6 8 36.77 4.76 -8 -6 9 169.72 9.48 -8 6 9 177.66 9.55 -8 -6 10 15.31 4.89 -8 6 10 5.25 4.51 -8 8 0 212.02 9.73 -8 8 -1 40 4.71 -8 8 1 40.12 4.61 -8 8 -2 1.24 3.65 -8 8 2 0.83 3.61 -8 8 -3 21.5 4.23 -8 8 3 13.81 3.98 -8 8 -4 110.73 6.72 -8 8 4 108.32 6.87 -8 8 -5 44.66 5.01 -8 8 5 43.35 5.02 -8 8 -6 12.65 3.94 -8 8 6 15.27 4.23 -8 8 -7 11.02 4.03 -8 8 7 6.77 4.11 -8 8 -8 83.59 6.12 -8 8 8 84.08 6.21 -8 -8 9 43.99 5.7 -8 8 9 43.34 5.65 -8 -8 10 34.83 5.69 -8 8 10 28 5.25 -8 10 0 63.86 5.68 -8 10 -1 68.31 5.5 -8 10 1 73.5 5.64 -8 10 -2 -0.42 3.81 -8 10 2 4.01 3.65 -8 10 -3 52.66 5.11 -8 10 3 52.03 5.29 -8 10 4 62.27 5.58 -8 10 -4 65.65 5.42 -8 10 -5 41.09 4.95 -8 10 5 48.76 5.18 -8 10 -6 4.33 3.92 -8 10 6 8.39 4.01 -8 10 -7 5.92 3.91 -8 10 7 9.18 4.25 -8 10 -8 36.98 4.86 -8 10 8 53.9 5.47 -8 -10 10 15.99 5.2 -8 12 0 89.89 6.48 -8 12 -1 42.54 4.95 -8 12 1 42.1 5.02 -8 12 -2 -1.93 3.81 -8 12 2 4.94 3.77 -8 12 -3 18.01 4.18 -8 12 3 17.83 4.27 -8 12 -4 47.49 5.22 -8 12 4 46.65 5.14 -8 12 -5 51.14 5.21 -8 12 5 55.3 5.56 -8 12 -6 6.19 4.23 -8 12 6 7.33 4.15 -8 12 -7 10.2 4.19 -8 12 7 14.28 4.51 -8 14 0 57.63 5.71 -8 14 -1 23.76 4.74 -8 14 1 18.79 4.61 -9 1 0 1.36 3.99 -9 -1 0 0.46 4.01 -9 1 1 32.54 4.99 -9 -1 -1 35.31 4.93 -9 -1 1 27.01 4.88 -9 1 -1 30.5 4.83 -9 1 -2 92.42 6.55 -9 1 2 83.91 6.59 -9 -1 -2 93.28 6.77 -9 -1 2 97.88 6.78 -9 -1 -3 35.95 4.95 -9 -1 3 41.63 5.33 -9 1 -3 41.32 5.36 -9 1 3 45.98 5.35 -9 -1 -4 1.12 4.05 -9 -1 4 7.38 4.27 -9 1 -4 5.18 4.09 -9 1 4 3.64 4.05 -9 -1 -5 13.38 4.16 -9 -1 5 14.36 4.68 -9 1 -5 20.25 4.63 -9 1 5 16.67 4.39 -9 1 -6 86.03 6.56 -9 1 6 84.38 6.66 -9 -1 -6 78.37 6.45 -9 -1 6 86.08 6.85 -9 -1 -7 50.84 5.55 -9 -1 7 59.83 5.96 -9 1 -7 63.93 5.95 -9 1 7 67.06 6.19 -9 3 0 -5.91 4.3 -9 -3 0 -0.48 4.14 -9 3 -1 47.33 5.43 -9 3 1 49.93 5.43 -9 -3 -1 53.43 5.72 -9 -3 1 39.24 5.38 -9 3 -2 48.97 5.27 -9 3 2 50.58 5.56 -9 -3 -2 37.18 5.24 -9 -3 2 39.54 5.49 -9 -3 3 79.12 6.55 -9 -3 -3 68.6 6.4 -9 3 -3 84.27 6.53 -9 3 3 80.72 6.34 -9 -3 -4 4.65 4.41 -9 -3 4 6.39 4.36 -9 3 -4 5.45 4.15 -9 3 4 4.77 4.08 -9 -3 -5 19.09 4.77 -9 -3 5 19.11 5.17 -9 3 -5 25.49 4.83 -9 3 5 27.94 4.69 -9 -3 6 45.05 5.91 -9 3 -6 42.55 5.42 -9 3 6 38.44 5.41 -9 -3 -6 40.58 5.19 -9 -3 -7 83.88 6.84 -9 -3 7 91.96 7.43 -9 3 -7 92.61 6.71 -9 3 7 103.39 7.12 -9 5 0 7.49 4.35 -9 5 -1 14.55 4.36 -9 5 1 14.72 4.5 -9 -5 -2 99.38 7.09 -9 5 -2 109.5 7.28 -9 5 2 120.48 7.3 -9 -5 -3 14.92 4.74 -9 5 -3 18.89 4.55 -9 5 3 24.18 4.83 -9 -5 3 16.42 5.01 -9 -5 -4 8.95 4.46 -9 5 -4 7.71 4.39 -9 5 4 8.12 4.41 -9 -5 4 4.37 4.62 -9 5 -5 8.12 4.38 -9 5 5 4.5 4.35 -9 -5 -5 3.05 4.29 -9 -5 5 7.6 4.83 -9 -5 -6 113.23 7.52 -9 -5 6 117.03 8.3 -9 5 -6 116.59 7.48 -9 5 6 119.26 7.61 -9 5 7 25.77 4.87 -9 -5 7 24.05 5.85 -9 7 0 1.13 4.04 -9 7 -1 51.77 5.39 -9 7 1 40.04 5.08 -9 7 -2 9.05 4.51 -9 7 2 15.52 4.48 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cl1 Bi1 Cl1 95.16(9) 12_655 . ? Cl1 Bi1 Cl2 88.07(5) . . ? Cl1 Bi1 Cl2 88.07(6) 12_655 . ? Cl1 Bi1 Cl3 91.60(5) . . ? Cl1 Bi1 Cl3 91.60(5) 12_655 . ? Cl1 Bi1 Cl4 90.65(4) . 14_556 ? Cl1 Bi1 Cl4 174.19(5) . . ? Cl1 Bi1 Cl4 90.64(4) 12_655 . ? Cl1 Bi1 Cl4 174.18(5) 12_655 14_556 ? Cl2 Bi1 Cl3 179.50(8) . . ? Cl2 Bi1 Cl4 91.74(8) . 14_556 ? Cl2 Bi1 Cl4 91.74(8) . . ? Cl3 Bi1 Cl4 88.63(8) . 14_556 ? Cl3 Bi1 Cl4 88.63(8) . . ? Cl4 Bi1 Cl4 83.55(2) 14_556 . ? Bi1 Cl4 Bi1 162.72(14) . 14_456 ? H2A N2 H2B 109.5 . . ? H2A N2 H2C 109.5 . . ? H2B N2 H2C 109.5 . . ? C4 N2 H2A 109.5 . . ? C4 N2 H2B 109.5 . . ? C4 N2 H2C 109.5 . . ? H3A C3 H3B 109.5 . . ? H3A C3 H3C 109.5 . . ? H3B C3 H3C 109.5 . . ? C4 C3 H3A 109.5 . . ? C4 C3 H3B 109.5 . . ? C4 C3 H3C 109.5 . . ? N2 C4 H4A 106.5 . . ? N2 C4 H4B 106.5 . . ? C3 C4 N2 123.2(12) . . ? C3 C4 H4A 106.5 . . ? C3 C4 H4B 106.5 . . ? H4A C4 H4B 106.5 . . ? H1A C1 H1B 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? C2 C1 H1A 109.5 . . ? C2 C1 H1B 109.5 . . ? C2 C1 H1C 109.5 . . ? C1 C2 H2D 109.5 . . ? C1 C2 H2E 109.5 . . ? H2D C2 H2E 108.1 . . ? N1 C2 C1 110.6 . . ? N1 C2 H2D 109.5 . . ? N1 C2 H2E 109.5 . . ? C2 N1 H1D 109.5 . . ? C2 N1 H1E 109.5 . . ? C2 N1 H1F 109.5 . . ? H1D N1 H1E 109.5 . . ? H1D N1 H1F 109.5 . . ? H1E N1 H1F 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Bi1 Cl1 2.5773(16) 12_655 ? Bi1 Cl1 2.5773(16) . ? Bi1 Cl2 2.678(2) . ? Bi1 Cl3 2.695(2) . ? Bi1 Cl4 2.8384(6) 14_556 ? Bi1 Cl4 2.8384(6) . ? N2 H2A 0.8900 . ? N2 H2B 0.8900 . ? N2 H2C 0.8900 . ? N2 C4 1.477(15) . ? C3 H3A 0.9600 . ? C3 H3B 0.9600 . ? C3 H3C 0.9600 . ? C3 C4 1.294(18) . ? C4 H4A 0.9700 . ? C4 H4B 0.9700 . ? C1 H1A 0.9600 . ? C1 H1B 0.9600 . ? C1 H1C 0.9600 . ? C1 C2 1.5320 . ? C2 H2D 0.9700 . ? C2 H2E 0.9700 . ? C2 N1 1.5191 . ? N1 H1D 0.8900 . ? N1 H1E 0.8900 . ? N1 H1F 0.8900 . ?