#------------------------------------------------------------------------------ #$Date: 2024-02-04 13:40:19 +0200 (Sun, 04 Feb 2024) $ #$Revision: 289452 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/78/7247804.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7247804 loop_ _publ_author_name 'Pradhan, Abinash' 'Sahoo, Sanand' 'Samal, Saroj L.' _publ_section_title ; (C2H5NH3)2BiCl5−xBrx perovskites containing 1D chains: effect of Br substitution on their structural and optical properties ; _journal_issue 3 _journal_name_full CrystEngComm _journal_page_first 312 _journal_page_last 323 _journal_paper_doi 10.1039/D3CE01019H _journal_volume 26 _journal_year 2024 _chemical_formula_moiety 'Bi Br2.259 Cl2.741, C4 H16 N2' _chemical_formula_sum 'C4 H16 Bi Br2.27 Cl2.73 N2' _chemical_formula_weight 579.23 _space_group_crystal_system orthorhombic _space_group_IT_number 64 _space_group_name_Hall '-C 2ac 2' _space_group_name_H-M_alt 'C m c e' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2023-06-01 _audit_creation_method ; Olex2 1.5-alpha (compiled 2021.06.29 svn.r12e2184c for OlexSys, GUI svn.r6374) ; _audit_update_record ; 2023-10-09 deposited with the CCDC. 2023-12-01 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 7.6954(2) _cell_length_b 22.2151(8) _cell_length_c 17.9473(5) _cell_measurement_reflns_used 3515 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 24.8430 _cell_measurement_theta_min 1.8230 _cell_volume 3068.16(16) _computing_cell_refinement 'CrysAlisPro 1.171.41.93a (Rigaku OD, 2020)' _computing_data_collection 'CrysAlisPro 1.171.41.93a (Rigaku OD, 2020)' _computing_data_reduction 'CrysAlisPro 1.171.41.93a (Rigaku OD, 2020)' _computing_molecular_graphics 'Olex2 1.5-alpha (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5-alpha (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 293(2) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.954 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -77.00 -51.00 0.50 171.53 -- 10.00 -80.00 126.00 52 2 \w 11.00 37.00 0.50 171.53 -- 10.00 46.00 52.00 52 3 \w -21.00 16.00 0.50 171.53 -- 10.00 -80.00 126.00 74 4 \w -17.00 28.00 0.50 171.53 -- 10.00 -77.00-180.00 90 5 \w -13.00 99.00 0.50 171.53 -- 10.00 77.00 60.00 224 6 \w -70.00 -33.00 0.50 171.53 -- 10.00 -77.00-180.00 74 7 \w -38.00 6.00 0.50 171.53 -- -10.20 -77.00 90.00 88 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Pro II AFC12 (RINC): Kappa single' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0780942000 _diffrn_orient_matrix_UB_12 -0.0003674000 _diffrn_orient_matrix_UB_13 0.0209859000 _diffrn_orient_matrix_UB_21 0.0117863000 _diffrn_orient_matrix_UB_22 -0.0308669000 _diffrn_orient_matrix_UB_23 -0.0088542000 _diffrn_orient_matrix_UB_31 0.0475395000 _diffrn_orient_matrix_UB_32 0.0082163000 _diffrn_orient_matrix_UB_33 -0.0322703000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0465 _diffrn_reflns_av_unetI/netI 0.0535 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.954 _diffrn_reflns_limit_h_max 6 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 27 _diffrn_reflns_limit_k_min -27 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 8465 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.954 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.075 _diffrn_reflns_theta_min 1.833 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'Rigaku (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 17.841 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.38775 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.93a (Rigaku Oxford Diffraction, 2020) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_density_diffrn 2.508 _exptl_crystal_description crystalline _exptl_crystal_F_000 2103 _exptl_crystal_size_max 0.18 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.12 _refine_diff_density_max 1.111 _refine_diff_density_min -0.662 _refine_diff_density_rms 0.145 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.032 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 79 _refine_ls_number_reflns 1737 _refine_ls_number_restraints 57 _refine_ls_restrained_S_all 1.021 _refine_ls_R_factor_all 0.0796 _refine_ls_R_factor_gt 0.0438 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0462P)^2^+1.2022P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0848 _refine_ls_wR_factor_ref 0.0924 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1193 _reflns_number_total 1737 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL ab256f_311221_rint0.2_a.res in Cmca ab256f_311221_rint0.2.res created by SHELXL-2018/3 at 16:33:49 on 01-Jun-2023 REM Old TITL AB256F_311221_rint0 in Cmce REM SHELXT solution in Cmca: R1 0.188, Rweak 0.023, Alpha 0.046 REM 0.542 for 99 systematic absences, Orientation as input REM Formula found by SHELXT: C1 Cl5 Bi CELL 0.71073 7.6954 22.2151 17.9473 90 90 90 ZERR 8 0.0002 0.0008 0.0005 0 0 0 LATT 7 SYMM -X,0.5-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM +X,-Y,-Z SFAC C H Bi Br Cl N UNIT 32 128 8 18.14 21.86 16 EADP Cl1 Br1 EADP Cl3 Br3 EADP Cl4 Br4 EADP Cl2 Br2 SIMU 0.02 0.04 2 RIGU 0.01 0.01 N1 C1 C2 EXYZ Cl1 Br1 EXYZ Cl3 Br3 EXYZ Cl4 Br4 EXYZ Cl2 Br2 L.S. 30 PLAN 3 CONF list 4 MORE -1 BOND $H fmap 2 53 acta REM REM REM WGHT 0.046200 1.202200 FVAR 0.09165 0.50319 0.49858 0.71804 0.51832 BI1 3 0.500000 0.365654 0.632074 10.50000 0.04224 0.06334 = 0.04700 -0.00873 0.00000 0.00000 PART 3 CL1 5 0.246870 0.379409 0.531928 21.00000 0.07225 0.12968 = 0.08099 -0.00568 -0.02771 0.01681 PART 5 CL3 5 0.500000 0.488910 0.662637 30.50000 0.16696 0.05755 = 0.08192 -0.01154 0.00000 0.00000 PART 9 CL2 5 0.500000 0.244111 0.601122 50.50000 0.12647 0.06170 = 0.10953 -0.01743 0.00000 0.00000 PART 7 CL4 5 0.750000 0.348947 0.750000 40.50000 0.10648 0.14785 = 0.12679 0.00000 -0.07447 0.00000 PART 6 BR3 4 0.500000 0.488910 0.662637 -30.50000 0.16696 0.05755 = 0.08192 -0.01154 0.00000 0.00000 PART 4 BR1 4 0.246870 0.379409 0.531928 -21.00000 0.07225 0.12968 = 0.08099 -0.00568 -0.02771 0.01681 PART 8 BR4 4 0.750000 0.348947 0.750000 -40.50000 0.10648 0.14785 = 0.12679 0.00000 -0.07447 0.00000 PART 10 BR2 4 0.500000 0.244111 0.601122 -50.50000 0.12647 0.06170 = 0.10953 -0.01743 0.00000 0.00000 PART 0 N2 6 0.500000 0.467634 0.848956 10.50000 0.12939 0.06977 = 0.06901 -0.00007 0.00000 0.00000 PART -1 AFIX 33 H2A 2 0.500000 0.437534 0.881681 10.50000 -1.20000 H2B 2 0.405569 0.465205 0.820483 10.50000 -1.20000 H2C 2 0.594431 0.465205 0.820484 10.50000 -1.20000 AFIX 0 PART 0 C4 1 0.500000 0.524200 0.888142 10.50000 0.23142 0.09609 = 0.09152 -0.02538 0.00000 0.00000 AFIX 23 H4A 2 0.398660 0.524770 0.920274 10.50000 -1.20000 H4B 2 0.601340 0.524770 0.920274 10.50000 -1.20000 AFIX 0 C3 1 0.500000 0.576179 0.848322 10.50000 0.31784 0.06969 = 0.09630 0.01524 0.00000 0.00000 PART -1 AFIX 33 H3A 2 0.500000 0.609868 0.881822 10.50000 -1.50000 H3B 2 0.601858 0.577707 0.817498 10.50000 -1.50000 H3C 2 0.398142 0.577706 0.817498 10.50000 -1.50000 AFIX 6 C1 1 0.551000 0.325721 0.315319 10.50000 0.05584 0.16270 = 0.15022 0.05050 -0.02758 0.03380 AFIX 33 H1A 2 0.484033 0.357575 0.293364 10.50000 -1.20000 H1B 2 0.653623 0.342210 0.337866 10.50000 -1.20000 H1C 2 0.583660 0.297380 0.277445 10.50000 -1.20000 AFIX 5 C2 1 0.442015 0.293810 0.374797 10.50000 0.07113 0.17473 = 0.19946 0.06543 -0.01325 -0.00726 AFIX 23 H2D 2 0.407549 0.322545 0.412712 10.50000 -1.20000 H2E 2 0.337469 0.277640 0.352190 10.50000 -1.20000 AFIX 5 N1 6 0.544839 0.243083 0.410572 10.50000 0.04371 0.14039 = 0.18859 0.06722 0.00582 -0.02259 AFIX 33 H1D 2 0.479698 0.225052 0.444936 10.50000 -1.50000 H1E 2 0.575095 0.216460 0.375861 10.50000 -1.50000 H1F 2 0.639957 0.258021 0.431876 10.50000 -1.50000 AFIX 0 HKLF 4 REM ab256f_311221_rint0.2_a.res in Cmca REM wR2 = 0.0924, GooF = S = 1.032, Restrained GooF = 1.021 for all data REM R1 = 0.0438 for 1193 Fo > 4sig(Fo) and 0.0796 for all 1737 data REM 79 parameters refined using 57 restraints END WGHT 0.0462 1.2022 REM Highest difference peak 1.111, deepest hole -0.662, 1-sigma level 0.145 Q1 1 0.5525 0.3615 0.5828 11.00000 0.05 1.11 Q2 1 0.5000 0.3988 0.6375 10.50000 0.05 0.99 Q3 1 0.5595 0.3627 0.6798 11.00000 0.05 0.98 REM The information below was added by Olex2. REM REM R1 = 0.0438 for 1193 Fo > 4sig(Fo) and 0.0796 for all 8804 data REM 79 parameters refined using n/a restraints REM Highest difference peak 1.11, deepest hole -0.66 REM Mean Shift 0, Max Shift -0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0796 REM R1_gt = 0.0438 REM wR_ref = 0.0924 REM GOOF = 1.032 REM Shift_max = -0.001 REM Shift_mean = 0 REM Reflections_all = 8804 REM Reflections_gt = 1193 REM Parameters = 79 REM Hole = -0.66 REM Peak = 1.11 REM Flack = n/a ; _cod_data_source_file d3ce01019h2.cif _cod_data_source_block ab256f _cod_depositor_comments 'Adding full bibliography for 7247803--7247812.cif.' _cod_original_sg_symbol_Hall '-C 2bc 2' _cod_database_code 7247804 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula (C2H5NH3)2BiCl3Br2 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _reflns_odcompleteness_completeness 99.67 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 26.32 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H,H) groups, {H2A,H2B,H2C} of N2, {H1A,H1B,H1C} of C1 At 1.5 times of: {H1D,H1E,H1F} of N1, {H3A,H3B,H3C} of C3 2. Shared sites {Cl1, Br1} {Cl3, Br3} {Cl4, Br4} {Cl2, Br2} 3. Uiso/Uaniso restraints and constraints All non-hydrogen atoms have similar U: within 2A with sigma of 0.02 and sigma for terminal atoms of 0.04 within 2A Uanis(Cl1) = Uanis(Br1) Uanis(Cl3) = Uanis(Br3) Uanis(Cl4) = Uanis(Br4) Uanis(Cl2) = Uanis(Br2) 4. Rigid body (RIGU) restrains N1, C1, C2 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01 5. Others Sof(Br1)=1-FVAR(1) Sof(Cl1)=FVAR(1) Sof(Br3)=0.5*(1-FVAR(3)) Sof(Cl3)=0.5*FVAR(3) Sof(Br4)=0.5*(1-FVAR(4)) Sof(Cl4)=0.5*FVAR(4) Sof(Br2)=0.5*(1-FVAR(5)) Sof(Cl2)=0.5*FVAR(5) Fixed Sof: H2B(0.5) H2C(0.5) H4A(0.5) H4B(0.5) H3B(0.5) H3C(0.5) C1(0.5) H1A(0.5) H1B(0.5) H1C(0.5) C2(0.5) H2D(0.5) H2E(0.5) N1(0.5) H1D(0.5) H1E(0.5) H1F(0.5) 6.a Free rotating group: C1(C2,N1) 6.b Secondary CH2 refined with riding coordinates: C4(H4A,H4B), C2(H2D,H2E) 6.c Me refined with riding coordinates: N2(H2A,H2B,H2C), C3(H3A,H3B,H3C), C1(H1A,H1B,H1C), N1(H1D,H1E,H1F) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.793 _oxdiff_exptl_absorpt_empirical_full_min 0.476 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1, z+1/2' '-x+1/2, y+1, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y-1/2, -z-1/2' 'x, -y-1/2, z-1/2' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y, -z-1/2' 'x+1/2, -y, z-1/2' '-x+1/2, y+1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Bi1 Bi 0.500000 0.36565(2) 0.63207(2) 0.0509(2) Uani 1 2 d S T P . . Cl1 Cl 0.24687(18) 0.37941(7) 0.53193(8) 0.0943(7) Uani 0.503(6) 1 d . U P A 3 Cl3 Cl 0.500000 0.48891(9) 0.66264(12) 0.1021(11) Uani 0.499(9) 2 d S TU P A 5 Cl2 Cl 0.500000 0.24411(9) 0.60112(14) 0.0992(12) Uani 0.518(10) 2 d S TU P A 9 Cl4 Cl 0.750000 0.34895(15) 0.750000 0.1270(17) Uani 0.718(9) 2 d S TU P A 7 Br3 Br 0.500000 0.48891(9) 0.66264(12) 0.1021(11) Uani 0.501(9) 2 d S TU P A 6 Br1 Br 0.24687(18) 0.37941(7) 0.53193(8) 0.0943(7) Uani 0.497(6) 1 d . U P A 4 Br4 Br 0.750000 0.34895(15) 0.750000 0.1270(17) Uani 0.282(9) 2 d S TU P A 8 Br2 Br 0.500000 0.24411(9) 0.60112(14) 0.0992(12) Uani 0.482(10) 2 d S TU P A 10 N2 N 0.500000 0.4676(5) 0.8490(5) 0.089(4) Uani 1 2 d S TU P . . H2A H 0.500000 0.437534 0.881681 0.107 Uiso 0.5 1 calc R U P B -1 H2B H 0.405569 0.465205 0.820483 0.107 Uiso 0.5 1 calc R U P B -1 H2C H 0.594431 0.465205 0.820484 0.107 Uiso 0.5 1 calc R U P B -1 C4 C 0.500000 0.5242(8) 0.8881(9) 0.140(7) Uani 1 2 d S TU P . . H4A H 0.398660 0.524770 0.920274 0.168 Uiso 0.5 1 calc R U P . . H4B H 0.601340 0.524770 0.920274 0.168 Uiso 0.5 1 calc R U P . . C3 C 0.500000 0.5762(7) 0.8483(8) 0.161(8) Uani 1 2 d S TU P . . H3A H 0.500000 0.609868 0.881822 0.242 Uiso 0.5 1 calc R U P C -1 H3B H 0.601858 0.577707 0.817498 0.242 Uiso 0.5 1 calc R U P C -1 H3C H 0.398142 0.577706 0.817498 0.242 Uiso 0.5 1 calc R U P C -1 C1 C 0.5510(19) 0.3257(8) 0.3153(9) 0.123(8) Uani 0.5 1 d G U P D -1 H1A H 0.484033 0.357575 0.293364 0.148 Uiso 0.5 1 calc R U P D -1 H1B H 0.653623 0.342210 0.337866 0.148 Uiso 0.5 1 calc R U P D -1 H1C H 0.583660 0.297380 0.277445 0.148 Uiso 0.5 1 calc R U P D -1 C2 C 0.4420(16) 0.2938(9) 0.3748(11) 0.148(9) Uani 0.5 1 d G U P D -1 H2D H 0.407549 0.322545 0.412712 0.178 Uiso 0.5 1 calc R U P D -1 H2E H 0.337469 0.277640 0.352190 0.178 Uiso 0.5 1 calc R U P D -1 N1 N 0.5448(17) 0.2431(8) 0.4106(9) 0.124(7) Uani 0.5 1 d G U P D -1 H1D H 0.479698 0.225052 0.444936 0.186 Uiso 0.5 1 calc R U P D -1 H1E H 0.575095 0.216460 0.375861 0.186 Uiso 0.5 1 calc R U P D -1 H1F H 0.639957 0.258021 0.431876 0.186 Uiso 0.5 1 calc R U P D -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Bi1 0.0422(3) 0.0633(3) 0.0470(3) -0.0087(2) 0.000 0.000 Cl1 0.0723(9) 0.1297(15) 0.0810(11) -0.0057(8) -0.0277(7) 0.0168(9) Cl3 0.167(2) 0.0576(14) 0.0819(15) -0.0115(11) 0.000 0.000 Cl2 0.126(2) 0.0617(16) 0.1095(18) -0.0174(12) 0.000 0.000 Cl4 0.106(2) 0.148(3) 0.127(3) 0.000 -0.074(2) 0.000 Br3 0.167(2) 0.0576(14) 0.0819(15) -0.0115(11) 0.000 0.000 Br1 0.0723(9) 0.1297(15) 0.0810(11) -0.0057(8) -0.0277(7) 0.0168(9) Br4 0.106(2) 0.148(3) 0.127(3) 0.000 -0.074(2) 0.000 Br2 0.126(2) 0.0617(16) 0.1095(18) -0.0174(12) 0.000 0.000 N2 0.129(10) 0.070(8) 0.069(7) 0.000(6) 0.000 0.000 C4 0.231(18) 0.096(13) 0.092(11) -0.025(10) 0.000 0.000 C3 0.32(2) 0.070(11) 0.096(12) 0.015(10) 0.000 0.000 C1 0.056(16) 0.16(2) 0.150(18) 0.051(13) -0.028(10) 0.034(12) C2 0.071(16) 0.17(2) 0.20(2) 0.065(15) -0.013(12) -0.007(13) N1 0.044(14) 0.140(14) 0.189(14) 0.067(11) 0.006(9) -0.023(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Bi Bi -4.1077 10.2566 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u 0 0 -2 32.36 1.64 0 0 2 31.24 1.67 0 0 2 30.18 1.63 0 0 -2 32.7 1.67 0 0 -3 0.75 0.84 0 0 3 -0.55 1.11 0 0 3 0.22 0.89 0 0 -3 -0.53 1.1 0 0 -3 -0.66 0.89 0 0 3 -0.5 0.96 0 0 -4 3195.58 116.77 0 0 4 3279.84 116.63 0 0 4 3234.12 116.71 0 0 5 0.67 1.42 0 0 5 -0.45 1.62 0 0 -5 0.1 1.7 0 0 6 352.1 13.69 0 0 -6 337.48 13.69 0 0 6 342.35 13.54 0 0 7 -0.74 2.27 0 0 -7 -0.07 2.37 0 0 7 3.02 2.07 0 0 8 1849.83 70.72 0 0 -8 1931.39 70.91 0 0 8 2016.29 70.78 0 0 9 -0.54 2.98 0 0 -9 0.42 3.17 0 0 9 0.99 2.83 0 0 10 722.97 26.64 0 0 10 653.95 26.71 0 0 -10 672.57 26.7 0 0 11 -1.59 3.97 0 0 -11 -3.27 3.94 0 0 11 -1.57 3.55 0 0 12 505.12 20.16 0 0 -12 472.94 20.31 0 0 -13 5 4.83 0 0 13 -5.92 4.45 0 0 -14 -1.41 5.35 0 0 -15 -5.59 6.21 0 0 -16 19.73 6.6 0 0 -17 1.32 6.54 0 0 -18 148.02 10.85 0 0 -19 9.58 7.53 0 0 -20 59.16 9.17 0 0 21 9.26 8.58 0 0 22 25.88 9.35 0 -2 0 90.69 4.03 0 2 -1 3383.12 114.79 0 -2 -1 2925.68 114.49 0 -2 -1 3527.88 115.27 0 2 1 3033.14 114.5 0 -2 1 3577.92 114.89 0 2 1 3693.75 115.38 0 2 -2 68.16 2.89 0 -2 -2 64.63 2.74 0 -2 -2 68.94 3.66 0 2 2 70.77 3.7 0 2 2 65.47 2.77 0 -2 -2 63.64 2.8 0 2 2 67.53 2.86 0 -2 2 65.09 2.87 0 -2 -3 1351.29 48.25 0 2 3 1336.29 47.53 0 -2 -3 1237.9 47.52 0 2 -3 1326.07 47.69 0 2 3 1287.44 47.57 0 2 3 1368.27 48.57 0 -2 3 1259.94 47.63 0 -2 -3 1391.75 47.58 0 2 -4 13.93 1.76 0 2 4 17.25 1.7 0 -2 4 13.3 1.79 0 -2 -4 12.78 2.09 0 2 4 12.04 2.52 0 2 4 15.44 1.78 0 -2 -4 11.19 1.43 0 2 5 37.46 2.75 0 -2 -5 37.38 2.57 0 2 5 38.29 2.92 0 -2 5 41.89 2.9 0 -2 -5 43.27 2.96 0 2 -5 39.42 2.89 0 2 5 39.16 3.76 0 2 6 742.87 28.94 0 -2 -6 743.87 27.97 0 -2 -6 718.51 27.81 0 2 6 765.01 27.94 0 -2 6 752.98 28.06 0 2 -6 746.26 28.17 0 -2 -7 12.05 2.38 0 -2 -7 17.72 2.68 0 2 7 9.93 3.43 0 -2 -7 15.71 2.46 0 2 -7 12.17 2.8 0 2 7 14.6 2.65 0 -2 7 16.15 2.95 0 -2 8 101.05 5.91 0 -2 -8 118.16 5.62 0 2 -8 103.75 6.01 0 -2 -8 97.3 5.52 0 -2 8 102.32 5.23 0 2 8 105.74 5.75 0 -2 8 102.16 5.66 0 -2 -8 107.36 5.69 0 2 8 100.01 6.7 0 2 9 3040.92 113.78 0 -2 -9 3143.4 112.7 0 -2 -9 3115.26 112.63 0 2 -9 2961.37 112.93 0 2 9 3217.08 112.69 0 -2 9 2957.32 112.2 0 -2 -9 3187.04 112.41 0 -2 9 3148.54 112.76 0 -2 9 3106.69 112.58 0 -2 10 95.41 5.39 0 2 10 98.53 7.24 0 -2 -10 83.06 5.74 0 2 -10 84.79 6.36 0 2 10 101.21 6.13 0 -2 10 92.26 5.82 0 -2 -10 101.82 5.57 0 -2 -10 99.51 6.03 0 2 11 194.52 10.94 0 -2 11 197.42 9.42 0 2 11 193.33 9.55 0 -2 11 186.69 8.91 0 -2 -11 196.02 9.63 0 2 -11 202.55 10.16 0 2 -12 24.22 5.26 0 -2 -12 34.03 4.82 0 2 12 23.46 4.5 0 2 12 23.07 5.53 0 -2 12 24.19 4.38 0 2 13 290.26 12.91 0 2 13 263.98 13.35 0 -2 -13 281.11 12.99 0 2 -13 264.24 13.24 0 -2 13 269.38 12.52 0 2 14 5.11 5.76 0 2 -14 2.15 5.45 0 -2 -14 1.87 5.08 0 2 -15 5.9 6.01 0 -2 -15 2.97 5.52 0 2 15 9.57 6.45 0 2 -16 11.53 6.52 0 -2 -16 13.84 6.16 0 2 17 243.89 13.25 0 -2 -17 214.49 12.45 0 2 -17 222.94 12.91 0 2 18 17.39 7.48 0 -2 -18 13.87 7.11 0 2 -18 16.64 7.4 0 2 -19 16.58 7.85 0 2 19 25.73 8.16 0 -2 -19 2.39 7.31 0 2 20 6.47 8.17 0 2 -20 1.47 8.21 0 2 -21 111.34 11.1 0 2 21 118.46 11.61 0 2 22 9.22 9.45 0 2 -22 5.74 9.01 0 4 0 2718.87 98.49 0 -4 0 2728.54 98.61 0 -4 0 2702.68 97.82 0 4 1 54.09 2.77 0 -4 1 59.16 3.76 0 4 -1 52.68 3.32 0 -4 -1 61.53 4.05 0 -4 -1 56.02 2.76 0 4 1 59.89 4.12 0 -4 2 225.66 8.8 0 -4 2 191.11 7.85 0 4 -2 224.96 8.48 0 -4 -2 231 9.34 0 4 2 215.03 9.66 0 -4 -2 191.9 7.83 0 4 2 201.03 7.86 0 -4 3 8.03 1.45 0 4 3 7.77 1.17 0 -4 3 7.08 2.43 0 -4 -3 8.16 1.1 0 -4 -3 7.37 2.54 0 -4 -3 9.52 1.36 0 4 3 5.44 3.24 0 -4 -4 73.3 3.55 0 4 4 71.74 3.57 0 -4 -4 75.5 3.62 0 -4 4 73.09 3.83 0 -4 -4 77.03 5.08 0 4 4 77.28 3.74 0 4 4 85.24 5.69 0 4 -4 77.77 3.83 0 -4 -5 1.62 1.54 0 -4 -5 3.19 1.44 0 4 5 2.61 1.77 0 4 -5 2.79 1.97 0 4 5 3.67 3.34 0 -4 -5 1.68 2.64 0 -4 5 2.04 1.91 0 4 5 1.89 1.68 0 -4 6 120.54 6.02 0 -4 -6 129.52 6.93 0 -4 -6 113.25 5.68 0 4 6 132.72 5.88 0 4 6 130.59 7.96 0 4 6 125.08 5.96 0 4 -6 134.84 6.24 0 4 -7 178.59 8 0 4 7 174.92 9.8 0 -4 7 140.26 7.53 0 4 7 165.92 7.64 0 -4 -7 169.85 7.49 0 4 7 179.64 7.64 0 -4 -7 168.26 8.34 0 -4 -8 1366.47 50.7 0 4 8 1384.65 50.8 0 -4 8 1425.58 50.89 0 4 -8 1371.1 51.15 0 -4 -8 1354.62 51.19 0 4 8 1324.84 52.85 0 4 8 1360.99 50.96 0 4 9 84.46 5.44 0 4 9 75.35 7.3 0 4 9 84.77 5.24 0 -4 -9 90.63 5.57 0 -4 9 83.13 5.54 0 -4 -9 78.22 5.11 0 4 9 72.57 5.37 0 4 -9 86.27 5.71 0 4 10 539.7 22.01 0 -4 -10 529.42 21.62 0 4 -10 561.9 22.32 0 -4 10 574.54 21.99 0 -4 -10 522.23 21.67 0 4 10 575.69 21.79 0 4 10 544.37 24 0 -4 -10 555.83 21.71 0 4 10 540.33 21.86 0 4 11 2.68 3.6 0 4 11 -0.65 4.16 0 4 11 7.05 6.08 0 4 11 3.87 4.19 0 -4 11 1.23 4.24 0 4 -11 2.15 4.08 0 -4 11 1.59 3.38 0 -4 -11 2.65 3.64 0 -4 11 6.56 3.11 0 -4 -11 0.73 3.26 0 -4 -12 1071.19 41.66 0 4 12 1153.01 41.86 0 -4 12 1131.63 41.87 0 4 12 1033.34 41.79 0 4 12 1071.41 42.13 0 4 -12 1091.87 42.25 0 -4 -12 1108.69 41.68 0 -4 12 1124.1 41.57 0 -4 13 33.43 4.82 0 4 13 38.7 5.95 0 4 13 41.8 5.46 0 -4 -13 33.88 4.96 0 -4 -13 46.88 5.41 0 4 -13 39.75 6 0 4 13 41.3 5.97 0 -4 -14 46 5.68 0 4 14 40.86 6.35 0 4 14 42.35 6.61 0 4 -14 44.76 6.55 0 4 15 -0.25 5.89 0 4 15 -1.18 5.87 0 -4 -15 0.58 5.18 0 4 -15 0.86 5.95 0 -4 -16 142.04 9.26 0 4 -16 138.09 10.13 0 4 16 141.42 10.14 0 4 17 18.14 7.32 0 -4 -17 28.9 6.77 0 4 -17 22.39 7.54 0 4 18 208.99 13.24 0 4 -18 229.65 13.28 0 4 -19 11.12 8.23 0 4 19 5.91 8.22 0 4 -20 84.64 10.08 0 4 20 73.91 10.23 0 4 -21 0.17 8.72 0 4 21 10.28 9.39 0 4 22 33.15 10.12 0 4 -22 37.32 9.69 0 6 0 441.86 17.93 0 -6 0 446.11 18.31 0 -6 0 437.57 16.92 0 6 1 1903.29 71.39 0 -6 -1 1938.92 72.78 0 6 1 2061.71 72.85 0 -6 -1 1952.27 71.31 0 -6 1 2041.76 72.65 0 6 -1 1982.87 72.13 0 6 2 691.99 27.28 0 -6 -2 794.92 29.15 0 6 2 803.37 29.43 0 -6 -2 719.94 27.01 0 -6 2 797.41 28.64 0 6 -2 725.18 27.93 0 6 3 1472 54.79 0 -6 -3 1603.59 56.63 0 -6 3 1655.03 56.03 0 -6 3 1484.51 54.6 0 -6 -3 1452.34 54.52 0 6 3 1677.49 57.33 0 6 3 1478.29 54.57 0 -6 -4 43.13 2.89 0 -6 -4 45.53 4.97 0 -6 4 44.16 4.84 0 -6 4 39.86 2.83 0 -6 -4 41.08 2.48 0 6 4 32.72 5.8 0 6 4 35.26 2.63 0 -6 5 51.11 4.58 0 -6 5 43.65 3.21 0 -6 -5 40.31 4.89 0 6 5 40.44 2.97 0 -6 -5 42.56 2.71 0 -6 -5 38.79 2.91 0 6 5 33.68 6.21 0 -6 6 286.14 11.68 0 -6 -6 243.99 10.41 0 -6 6 262.41 10.74 0 -6 -6 246.87 10.35 0 -6 -6 254.85 12.27 0 6 -6 264.97 10.79 0 6 6 258.03 10.36 0 6 6 247.09 13.66 0 -6 -6 254.31 10.32 0 6 6 246.27 10.57 0 6 7 97.55 5.1 0 -6 -7 94.04 5.07 0 -6 -7 88.98 6.76 0 -6 7 98.5 6.12 0 6 7 95.01 5.28 0 -6 -7 90.81 5 0 -6 7 99.47 5.46 0 6 -7 95.45 5.52 0 6 7 103.78 8.52 0 -6 -8 85.15 5 0 -6 8 90.73 5.44 0 6 8 92.07 5.3 0 -6 8 91.68 6.06 0 -6 -8 78.69 6.47 0 6 8 98.37 8.42 0 6 8 95.85 5.73 0 6 -8 92.16 5.63 0 -6 9 1762.12 62.16 0 6 9 1688.68 62.3 0 6 9 1667.98 65.06 0 -6 -9 1623.52 62.97 0 6 9 1691.12 62.01 0 -6 -9 1645.05 62.04 0 6 -9 1684.07 62.55 0 6 -10 288.09 12.91 0 -6 -10 263.54 12.87 0 6 10 281.7 12.72 0 -6 10 287.88 12.5 0 6 10 318.52 15.99 0 6 10 294.93 12.42 0 -6 -10 267.97 12.19 0 -6 -11 327.3 14.54 0 6 -11 329 15.26 0 6 11 365.12 15.29 0 6 11 334.52 14.82 0 6 11 357.59 18.11 0 -6 11 366.13 15 0 6 -12 1.86 4.86 0 -6 -12 4.69 3.88 0 6 12 0.36 4.62 0 -6 -12 2.54 3.74 0 -6 12 -3.61 4.74 0 6 12 2.99 4.41 0 6 13 229.6 12.03 0 6 -13 210.67 12.06 0 -6 13 241.79 11.86 0 -6 -13 247.65 11.4 0 6 13 237.68 11.72 0 -6 -13 233.95 11.23 0 6 14 37.7 6.51 0 6 -14 33.62 6.46 0 -6 -14 28.99 5.29 0 -6 -14 30.06 5.11 0 6 15 6.5 6.33 0 -6 -15 15.58 5.19 0 -6 -15 9.7 5.02 0 6 -15 14.93 6.4 0 -6 -16 20.93 5.91 0 6 -16 20.72 7.21 0 6 16 23.04 7.08 0 -6 -16 18.25 5.52 0 6 -17 165.8 11.8 0 6 17 192.26 12.02 0 6 -18 3.64 7.46 0 6 18 5.24 7.8 0 6 19 5.89 8.41 0 6 -19 8.75 8.37 0 6 20 0.95 8.97 0 6 -20 18.2 8.83 0 6 -21 69.06 10.57 0 6 21 80.11 11.07 0 6 -22 2.74 9.53 0 -8 0 7839.82 278.76 0 8 0 7774.71 278.3 0 -8 0 7600.44 277.01 0 8 -1 1197.31 43.97 0 -8 -1 1131.08 44.69 0 -8 1 1146.63 44.69 0 -8 -1 1126.35 42.82 0 8 1 1216.71 44.64 0 8 -2 269.62 11.9 0 -8 2 275.37 12.97 0 -8 -2 267.3 13.01 0 -8 -2 259.19 10.37 0 -8 -2 263.09 10.8 0 8 2 282.59 13.4 0 8 2 246.09 10.85 0 -8 3 19.75 5.25 0 -8 -3 22.96 4.7 0 8 3 11.29 2.26 0 8 -3 11.76 3.22 0 -8 -3 11.03 2.13 0 8 3 13.75 5.46 0 -8 -4 1211.26 42.55 0 -8 4 1092.71 42.58 0 -8 -4 1134.62 42.55 0 8 4 1153.46 42.92 0 8 4 1112.12 42.59 0 -8 4 1351.21 44.89 0 -8 -4 1200.17 45.23 0 8 4 1282.1 46.28 0 8 5 414.69 16.55 0 -8 -5 442.65 16.62 0 8 5 430.95 20.43 0 -8 5 452.18 18.45 0 -8 -5 418.59 16.35 0 -8 -5 408.87 18.94 0 -8 5 424.4 16.56 0 8 6 92.73 5.11 0 -8 -6 83.41 7.16 0 -8 6 118.11 7.41 0 -8 -6 91.5 5 0 -8 6 99.07 5.35 0 -8 -6 95.81 4.88 0 -8 -7 91.71 5.18 0 -8 7 96.35 5.59 0 -8 7 110.79 7.56 0 8 7 99 5.45 0 -8 -7 90.75 7.38 0 -8 -7 93.06 5.01 0 8 7 87.36 9.49 0 -8 -8 699.83 27.92 0 -8 8 745.31 28.16 0 -8 8 770.71 29.37 0 -8 -8 747.06 30.03 0 -8 -8 733.52 27.85 0 8 8 712.26 31.96 0 8 8 742.17 28.17 0 -8 9 227.05 10.15 0 -8 -9 207.3 9.78 0 -8 9 234.22 11.64 0 8 9 194.78 14.27 0 8 9 217.82 10.22 0 8 9 222.9 9.84 0 -8 -9 209.96 11.68 0 8 10 151.3 8.28 0 -8 10 158.74 8.12 0 8 -10 161.13 8.68 0 8 10 120.58 12.45 0 -8 -10 138.16 9.18 0 8 10 148.78 7.77 0 -8 -10 148.27 7.82 0 -8 -11 25.49 4.25 0 8 11 26.8 4.99 0 8 -11 28.79 5.21 0 8 11 24.21 4.5 0 8 11 27.73 9.57 0 -8 11 28.79 4.86 0 8 12 280.11 13.53 0 8 -12 285.37 13.72 0 8 12 254.93 17.52 0 -8 12 302.37 13.24 0 8 12 287.53 12.94 0 -8 -12 272.08 12.73 0 8 -13 46.08 6.71 0 8 13 50.66 6.54 0 -8 -13 48.09 5.26 0 -8 -14 2.59 4.74 0 -8 -14 3.18 4.5 0 8 14 4.88 6.11 0 8 -14 -1.02 6.1 0 8 15 -1.11 6.6 0 8 -15 4.63 6.69 0 -8 -15 6.13 4.88 0 8 16 12.86 7.34 0 -8 -16 12.87 5.58 0 8 -16 13.56 7.2 0 -8 -17 19.17 6.01 0 8 17 25.95 8.38 0 8 -17 19.98 7.88 0 8 18 81.01 10.14 0 8 -18 53.61 9.31 0 -8 -18 57.2 7.35 0 8 19 0.98 9.17 0 8 -19 -3.61 8.65 0 8 20 35.63 10.28 0 8 21 1.86 10.13 0 -10 0 697.32 28.92 0 -10 0 670.6 26.36 0 10 0 699.07 28.04 0 -10 1 1159.84 42.68 0 10 1 1092.5 42.05 0 -10 -1 1057.92 42.48 0 -10 -1 1064.56 39.97 0 -10 1 1020.79 40.18 0 10 -1 1072.67 41.3 0 -10 -2 33.23 3.04 0 -10 2 37.86 6.89 0 10 2 34.67 6.75 0 -10 -2 42.1 3.72 0 -10 -2 43.39 6.2 0 10 -2 33.3 4.66 0 10 2 39.1 3.87 0 -10 3 619.75 24.44 0 10 3 547.78 21.63 0 -10 -3 579.99 24.2 0 10 3 555.19 24.45 0 10 -3 545.39 22.49 0 -10 -3 539.82 21.05 0 -10 -4 364.19 14.73 0 -10 -4 382.74 17.82 0 -10 4 366.5 14.76 0 10 4 380.3 15.3 0 10 4 366.72 18.52 0 -10 4 438.01 18.26 0 -10 5 388.94 15.37 0 -10 -5 386.82 15.29 0 -10 -5 384.6 15.22 0 10 5 388.59 19.67 0 10 5 380.6 15.67 0 -10 5 420.23 18.37 0 -10 -5 379.28 18.3 0 10 6 143.07 11.69 0 -10 6 156.03 10.14 0 10 6 140.26 7.06 0 -10 -6 129.64 9.57 0 10 6 136.52 6.8 0 -10 6 145.85 6.93 0 -10 -6 136.66 6.58 0 -10 -6 130.84 6.66 0 -10 -7 55.99 7.1 0 -10 -7 64.87 4.41 0 -10 7 59.74 7.7 0 10 7 64.65 9.44 0 -10 7 58.46 4.72 0 -10 -7 56.75 4.01 0 10 7 55.21 4.47 0 -10 8 368.85 15.01 0 -10 8 385.55 17.54 0 10 8 319.29 19.52 0 -10 -8 325.64 17.09 0 10 8 359.67 14.93 0 -10 -8 362.28 14.62 0 -10 -8 355.05 14.46 0 -10 -9 813.87 31.82 0 -10 -9 822.27 31.58 0 10 9 746.39 36.31 0 -10 9 864.34 32.04 0 10 9 875.32 32.17 0 -10 9 879.62 34.26 0 -10 -9 784.65 34.03 0 -10 -10 5.62 3.6 0 10 10 3.78 4.18 0 -10 -10 5.4 5.76 0 -10 10 6.77 4.28 0 10 10 7.27 9.87 0 -10 -11 38 4.71 0 10 11 40.4 5.39 0 10 11 36.13 11.18 0 -10 11 45.7 5.29 0 10 12 56.85 11.99 0 10 12 54.39 6.36 0 -10 -12 41.4 5.32 0 10 13 99.95 8.13 0 -10 -13 98.94 7.25 0 10 14 30.04 6.99 0 -10 -14 23.23 5.38 0 10 15 -4.26 6.64 0 -10 -15 -3.44 5.02 0 -10 -16 29.84 6.04 0 10 16 33.77 7.83 0 -10 -17 73.4 7.4 0 10 17 72.38 9.28 0 -10 -18 32.79 6.78 0 10 18 15.67 8.6 0 10 19 4.52 9.07 0 -10 -19 -8.3 6.81 0 -10 -20 -0.78 6.89 0 10 20 -3.72 9.35 0 10 21 44.92 10.82 0 -12 0 354.03 18.24 0 12 0 354.51 17.1 0 -12 0 362.82 15.2 0 -12 -1 96.88 5.94 0 -12 1 90.31 6.16 0 12 1 111.92 8.83 0 12 -1 102.72 7.71 0 -12 1 96.51 9.88 0 -12 -1 80.55 9.19 0 -12 -2 113.96 5.82 0 12 -2 121.97 8.09 0 -12 -2 106.42 6.28 0 -12 2 116.58 10.42 0 12 2 121.69 9.61 0 -12 -2 134.14 9.92 0 -12 -3 23.02 6.35 0 -12 -3 14.32 2.97 0 12 3 18.2 7.06 0 12 3 5.3 3.19 0 -12 3 11.12 7.66 0 12 -3 12.74 4.5 0 12 4 57.83 8.79 0 -12 4 74.09 9.32 0 -12 -4 64.28 7.68 0 12 4 63.27 4.93 0 -12 4 54.31 4.15 0 -12 -4 57.46 4.24 0 -12 5 66.22 9.54 0 -12 -5 65.13 4.37 0 -12 -5 63.03 4.53 0 -12 5 68.66 4.68 0 -12 -5 54.33 7.72 0 12 5 70.99 9.16 0 12 5 69.94 5.05 0 -12 -6 70.95 8.35 0 12 6 74.43 10.85 0 12 6 90.88 5.7 0 -12 6 79.18 5.33 0 -12 6 84.73 10.47 0 -12 -6 91.46 5.48 0 -12 -6 85.43 5.11 0 -12 -7 206.83 9.18 0 -12 7 212.15 13.89 0 -12 -7 158.47 12 0 12 7 180.38 9.37 0 12 7 189.37 14.73 0 12 7 203.43 9.21 0 -12 7 203.17 9.28 0 -12 -7 193.74 8.9 0 -12 -8 261.88 11.39 0 -12 8 290.02 16.26 0 12 8 275.78 11.94 0 12 8 236.1 17.5 0 -12 -8 254.62 14.74 0 -12 -8 261.17 11.62 0 -12 8 270.72 11.94 0 12 8 269.66 12.12 0 -12 -9 154.95 7.82 0 -12 9 149.86 8.22 0 -12 -9 140.66 7.55 0 12 9 121.91 14.22 0 -12 -9 141.13 10.48 0 12 9 151.51 8.26 0 -12 -10 61.54 5.29 0 -12 10 76.49 6.21 0 12 10 74.82 6.27 0 -12 -10 67.76 5.6 0 12 10 58.06 11.94 0 -12 -10 64.63 8.32 0 12 11 8.41 11.6 0 12 11 0.34 4.96 0 -12 -11 2.01 4.21 0 12 12 368.82 16.26 0 12 12 326.33 21.58 0 -12 -12 350.44 15.64 0 12 13 153.74 9.77 0 -12 -13 143.24 8.88 0 -12 -14 9.61 5.16 0 12 14 8.16 6.52 0 12 15 1.53 6.88 0 -12 -15 5.37 5.26 0 -12 -16 52.11 6.78 0 12 16 50.11 8.5 0 12 17 65.34 9.3 0 -12 -17 68.85 7.77 0 12 18 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4 1 21.1 3.86 -2 4 1 18.57 1.28 -2 4 1 18.16 1.74 -2 4 -1 18.9 1.93 2 -4 1 20.3 3.3 -2 4 2 334.87 15.88 2 -4 2 342.41 14.88 2 -4 -2 354.84 15.37 -2 4 2 355.49 13.48 2 4 2 359.17 13.47 -2 4 -2 377.77 15.32 2 4 2 352.33 13.07 -2 4 -2 346.87 13.85 2 -4 -2 381.41 13.76 2 -4 -3 156.95 6.53 -2 4 -3 153.71 6.85 -2 4 -3 152.62 7.78 -2 4 3 145.69 9.04 2 -4 3 142.8 7.52 2 -4 -3 147.82 8.38 -2 -4 -3 141.8 6.68 2 4 3 154.81 6.05 -2 -4 -4 1995.95 71.22 2 -4 -4 1962.95 70.71 2 -4 -4 2018.25 70.92 -2 -4 -4 1894.42 70.65 -2 4 -4 1959.13 71.32 -2 4 -4 1974.93 71.82 2 -4 4 1892.13 71.58 -2 4 4 1911.33 73.61 2 -4 -4 2074.84 72.8 -2 4 4 1906.92 70.92 -2 -4 -5 44.26 2.94 -2 -4 -5 50.97 3.57 2 4 5 51.81 3.74 2 -4 -5 52.09 3.1 -2 -4 -5 53.55 3.73 -2 4 -5 54.78 3.65 -2 4 -5 49.45 4 2 -4 5 45.99 4.13 2 -4 -5 47.43 4.21 2 -4 5 49.76 3.68 2 -4 -5 55.26 5.27 -2 4 5 44.17 3.32 2 -4 -5 48.22 3.35 -2 4 5 49.8 5.72 -2 4 6 60.88 4.01 2 -4 -6 74.89 3.36 2 4 6 70.95 4.52 -2 -4 6 69.14 3.8 -2 -4 -6 62.39 4.29 -2 -4 -6 68.8 4.24 -2 4 -6 62.26 3.95 -2 4 -6 67.85 4.68 2 -4 6 67.13 4.82 2 -4 -6 71.67 4.72 2 -4 6 59.33 3.83 2 -4 -6 67.29 5.93 2 -4 -6 63.73 4.05 -2 4 6 50.8 6.09 -2 -4 -6 60.21 3.78 2 -4 -6 59.62 3.84 2 -4 7 2.14 1.93 -2 4 7 1.53 2.6 2 -4 -7 1.16 3.91 -2 -4 -7 -0.24 2.63 -2 -4 7 3.24 2.3 -2 -4 -7 -1.04 2.32 2 4 7 0.79 3.02 2 -4 -7 -0.12 2.25 -2 4 -7 0.71 2.97 -2 4 -7 5.19 1.78 2 -4 -7 1.59 2.02 -2 -4 -7 -2.18 2.93 2 -4 -7 3.66 2.92 2 -4 7 2.98 3.03 -2 4 7 0.2 4.57 2 -4 -7 -0.94 2.5 -2 4 8 703.42 25.9 -2 -4 -8 676.34 26.08 2 4 8 694.29 26.1 -2 -4 8 692.98 25.34 2 -4 -8 691.99 25.24 2 -4 -8 709.29 25.66 -2 -4 -8 642.82 25.52 -2 4 -8 684.24 26.31 -2 -4 -8 689.48 25.52 -2 4 8 659.3 28.73 2 -4 8 692.41 25.86 2 -4 -8 733.14 25.87 2 -4 8 580.71 24.48 2 -4 -8 720.1 27.35 -2 4 9 34.35 4.24 2 -4 9 32.18 3.82 2 -4 -9 43.91 5.41 2 4 9 36.28 4.54 -2 4 -9 39.39 4.62 -2 -4 9 33.19 3.67 2 -4 -9 33.22 3.76 -2 -4 -9 25.09 3.57 -2 4 9 27.95 6.4 -2 -4 -9 33.68 3.55 2 -4 -9 38.24 3.68 2 -4 -9 32.63 3.82 2 -4 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4 15 -0.62 6.25 -2 -4 -15 2.43 5.57 -2 4 -16 334.74 16.74 -2 -4 -16 343.61 15.97 -2 4 16 323.91 16.65 -2 4 -17 7.18 7.55 -2 4 17 14.91 7.84 -2 -4 -17 8.58 6.39 -2 4 -18 40.41 8.7 -2 -4 -18 43.18 7.5 -2 4 18 42.25 8.75 2 4 18 44.42 8.34 -2 4 -19 -0.35 8.14 -2 -4 -19 2.33 7.05 -2 4 19 -0.76 8.6 2 4 19 2.75 8.17 -2 4 20 30.34 10.54 2 4 20 32.52 9.24 -2 -4 -20 23.85 7.76 -2 4 -20 29.62 9.17 -2 4 -21 10.58 9.16 -2 4 21 3.52 10.68 -2 -4 -21 6.44 7.89 -2 -4 21 16.07 8.82 2 4 21 14.5 9.35 2 4 22 61.09 10.82 -2 -4 -22 60.06 9.4 -2 6 0 102.6 4.31 2 -6 0 107.81 4.97 -2 -6 0 108.9 5.01 -2 6 0 99.8 7.3 2 -6 0 102.12 7.45 -2 6 -1 342.11 15.69 -2 6 -1 335.18 12.97 -2 6 1 329.58 16.09 2 -6 1 309.71 13.21 2 -6 1 340.66 15.81 2 -6 -1 351.41 15.79 2 -6 -1 358.4 13.22 -2 -6 -1 362.92 13.26 -2 -6 -1 340.09 12.5 2 -6 -2 2.03 2 2 -6 -2 2.24 3.87 -2 6 2 0.38 1.68 -2 6 -2 0.09 1.93 2 6 2 -0.09 1.67 2 -6 2 0.3 3.98 -2 6 -2 -0.14 3.56 2 -6 2 -2.58 2.44 -2 6 2 1.68 3.83 -2 6 -3 355.12 15.31 2 -6 3 335.57 14.09 -2 6 3 344.02 17.08 2 -6 3 365.06 16.1 -2 -6 -3 372.61 14.51 2 -6 -3 374.46 16.27 -2 6 3 345.43 13.6 2 6 3 350.47 13.59 2 -6 -3 363.42 13.8 2 6 3 337.93 13.06 -2 6 -3 352.23 13.9 -2 -6 -4 193.93 8.67 2 6 4 194.87 7.91 -2 -6 -4 213.29 9.19 -2 6 -4 191.5 8.78 -2 6 -4 203.79 9.58 -2 6 4 185.61 11.81 2 -6 4 195.65 10.51 2 -6 -4 204.22 10.86 2 -6 -4 202.36 8.46 -2 -6 -5 2007.96 72.62 -2 -6 -5 1952.96 72.36 -2 6 5 1876.23 72.09 -2 6 -5 1970.12 72.54 -2 6 -5 1960.17 72.77 2 -6 5 1984.84 73.84 -2 6 5 1869.96 75.85 2 -6 -5 1998.22 74.26 2 -6 -5 2043.61 72.11 2 6 5 2033.24 71.75 -2 -6 -6 566.81 22.55 -2 -6 -6 602.03 23.12 -2 6 6 581.95 21.83 2 -6 -6 583.69 22.04 2 6 6 631.21 22.62 -2 6 -6 607.26 23.44 -2 -6 -6 590.28 23.38 -2 6 -6 585.19 22.97 2 -6 6 624.77 24.38 -2 6 6 581.45 26.74 2 -6 -6 596.04 24.81 2 -6 -6 654.25 22.89 2 -6 -6 586.51 22.64 -2 6 6 606.96 22.94 2 -6 -7 961.44 35.85 2 6 7 1010.51 35.89 -2 6 -7 971.55 35.59 -2 -6 -7 940.12 35.74 -2 6 7 944.65 35.09 2 6 7 985.14 36.26 2 -6 -7 924.58 35.3 -2 -6 7 978.85 35.71 -2 6 -7 952.98 36.6 -2 -6 -7 917.73 36.5 2 -6 -7 958.23 35.88 -2 6 7 890.26 39.86 2 -6 7 992.29 37.09 2 -6 -7 1031.85 38.1 -2 -6 -7 987.7 36.28 -2 6 7 956.24 36.08 2 -6 -8 6.55 3.15 -2 6 8 3.92 3.16 -2 -6 -8 8.77 3.27 -2 6 8 6.53 2.31 2 -6 8 2.39 3.85 2 6 8 5.92 3.55 -2 -6 -8 3.09 2.6 2 -6 -8 6.33 2.74 2 6 8 4.62 3 2 -6 -8 3.06 2.68 -2 -6 8 6.06 2.97 -2 -6 -8 -1.9 4.16 -2 6 8 4.66 6.22 2 -6 -8 10.98 4.92 -2 6 -8 7.06 3.9 -2 -6 9 110.01 5.99 -2 -6 -9 101.95 6.43 2 6 9 102.72 6.59 -2 -6 -9 96.21 5.83 2 -6 -9 97.42 5.74 -2 6 -9 105.18 7.1 -2 -6 -9 89.64 6.4 -2 6 9 94.04 10.03 2 -6 -9 118.63 8.1 2 6 9 106.07 6.25 -2 6 9 104.51 6.43 2 -6 -9 99.01 5.92 2 6 10 112.39 6.74 -2 6 10 104.75 6.79 -2 -6 10 110.49 6.22 2 -6 -10 94.38 6.17 -2 6 -10 98.86 7.31 -2 6 10 96.21 10.53 2 -6 -10 108.23 6.29 2 -6 -10 106.86 7.99 2 6 10 99.49 6.87 -2 -6 -10 98.19 6.02 -2 6 11 23.19 5.03 2 6 11 30.29 5.35 2 6 11 29.43 4.95 -2 -6 -11 17.83 3.83 -2 -6 11 27.61 4.25 -2 6 -11 18.25 5.38 2 -6 -11 18.77 3.97 2 -6 -11 21.52 5.79 -2 6 11 14.18 7.63 -2 -6 -12 35.7 4.61 2 -6 -12 37.64 4.86 2 6 12 43.89 6 -2 -6 12 48.45 4.92 2 6 12 40.89 5.9 -2 6 -12 34.37 6.37 2 -6 -12 40.33 6.34 -2 6 12 32.67 5.78 -2 6 12 32.19 9 2 6 13 555.09 23.52 -2 6 -13 589.93 24.25 -2 -6 13 558.59 22.6 -2 6 13 552.07 27.48 2 6 13 574.08 23.76 -2 -6 -13 542.69 22.76 2 -6 -13 568.52 23 -2 6 13 587.08 23.85 -2 -6 -14 24.1 4.96 2 -6 -14 23.35 5.21 -2 6 -14 25.03 6.94 -2 6 14 21.18 6.46 2 6 14 32.77 6.58 -2 6 15 3.17 6.52 -2 -6 -15 9.11 5.05 -2 6 -15 8.02 7.18 2 -6 -15 5.48 5.18 2 6 15 15.31 6.58 -2 6 -16 -0.5 7.1 2 6 16 3.2 6.73 -2 -6 -16 0.52 5.64 -2 6 16 -6.75 7.12 2 6 17 150.28 11.24 -2 6 -17 173.31 11.79 -2 6 17 151.25 11.76 -2 -6 -17 155.02 10.33 -2 6 18 0.75 8.39 -2 6 -18 10.79 8.1 -2 -6 -18 -0.56 6.68 2 6 18 14.27 8.06 2 6 19 5.6 8.63 -2 6 19 -0.2 8.78 -2 6 -19 3.01 8.37 -2 -6 -19 1.73 7.27 -2 6 20 5.57 9.23 2 6 20 3.26 9.04 -2 6 -20 8.5 9.16 -2 -6 -20 -0.73 7.36 2 6 21 40.58 10 -2 6 -21 41.11 9.98 -2 6 21 33.88 10.71 2 -8 0 1097.91 42.33 -2 -8 0 1170.61 42.44 2 -8 0 1151.06 41.87 -2 8 0 1094.51 45.19 2 -8 0 1257.26 46.03 -2 -8 -1 244.69 11.07 2 -8 -1 244.81 9.13 2 -8 1 215.35 9.91 2 -8 1 238.35 9.6 -2 8 -1 227.53 12.15 -2 8 1 204.91 12.54 2 -8 1 253.06 13.37 2 -8 -1 240.83 13.15 2 -8 -1 232.33 9.73 -2 -8 -1 229.09 9.69 -2 -8 -1 224.9 8.83 -2 8 -2 261.92 10.46 -2 8 2 250.49 10.96 -2 -8 -2 267.85 12.05 2 -8 2 258.09 10.94 -2 8 -2 266.04 13.06 2 -8 2 277.9 14.38 -2 -8 -2 256.09 10.02 2 -8 -2 277.22 14.33 2 8 2 255.23 10.91 2 -8 -2 266.3 10.82 2 -8 -2 272.43 9.98 -2 8 2 254.37 14.44 -2 -8 -3 366.64 14.8 2 -8 3 440.09 19.26 2 -8 3 393.91 15.87 -2 8 3 377.16 19.51 2 -8 -3 417.72 14.46 2 -8 -3 403.96 18.82 -2 8 -3 386 15.43 -2 8 -3 392.79 17.63 -2 -8 -3 399.89 16.64 2 -8 -3 390.16 15.61 -2 8 3 370.69 15.56 2 8 3 385.01 15.58 -2 8 -4 3046.44 108.44 -2 -8 -4 2968.82 109.3 -2 8 -4 3010.22 109.9 2 -8 4 3098.01 108.83 -2 8 4 2740.81 112.5 -2 -8 -4 2943.62 108.6 2 -8 4 3187.23 111.83 -2 8 4 3018.76 108.43 2 8 4 2931.55 108.34 2 -8 -4 3062.16 111.43 2 -8 -4 3056.45 108.39 2 8 4 2913.08 107.75 2 -8 -5 515.88 19.65 2 8 5 499.12 19.03 -2 -8 -5 493.99 19.83 -2 8 -5 514.95 20.68 -2 8 -5 489.21 19.81 -2 -8 -5 517.63 20.66 2 -8 5 543.23 20.32 -2 8 5 456.31 23.7 2 -8 5 535.33 22.89 2 -8 -5 504.15 22.36 -2 8 5 489.65 19.52 2 8 5 495.25 19.54 2 -8 -6 7.77 5.09 2 8 6 3.65 2.39 -2 8 6 6.76 2.82 2 -8 -6 5.92 3.21 -2 -8 -6 3.44 2.96 -2 8 -6 14.24 3.57 -2 8 -6 3.68 3.24 -2 -8 -6 7.89 4.35 2 -8 -6 5.67 1.84 2 -8 6 1.37 3.85 -2 8 6 5 6.15 2 -8 6 3.53 5.54 2 -8 -7 16.88 3.49 2 8 7 14.53 3.02 -2 -8 7 18.13 3.2 -2 -8 -7 11.68 3.33 -2 8 -7 19.51 3.48 2 -8 -7 18.3 2.93 -2 8 -7 16.16 4.01 -2 -8 -7 13.36 4.82 2 -8 -7 16.57 2.42 -2 8 7 12.04 3.23 2 -8 7 14.17 4.59 -2 8 7 14.47 6.98 2 -8 7 7.84 5.69 -2 -8 -7 16.52 2.93 2 -8 -7 23.33 5.56 -2 8 8 486.08 26.11 -2 -8 -8 531.23 21.15 2 -8 -8 535.51 21.24 -2 -8 -8 551.69 21.7 -2 8 8 568.58 21.68 -2 -8 8 562.1 21.12 -2 8 -8 532.22 22.01 -2 8 -8 495.04 20.8 -2 -8 -8 453.4 22.24 2 -8 8 595.36 22.43 2 -8 -8 563.35 23.59 2 8 8 608.85 21.45 2 -8 -8 559.08 21.37 -2 -8 -9 138.27 7.26 2 -8 -9 135.85 7.32 -2 -8 -9 139.91 7.95 2 -8 -9 149.61 9.5 -2 -8 9 151.24 7.4 -2 8 9 145.93 7.97 -2 8 -9 130.47 8.35 -2 8 9 134.16 12.23 2 -8 -9 144.54 7.58 2 8 9 154.36 7.79 -2 8 10 5.44 4.09 -2 -8 10 8.68 3.85 -2 -8 -10 2.52 3.41 -2 8 -10 4.73 4.91 2 -8 -10 4.13 3.63 -2 8 10 -0.64 7.94 2 -8 -10 5.82 5.66 -2 -8 -10 9.49 4.34 2 8 10 7.15 4.14 2 8 11 8.01 4.77 2 -8 -11 8.05 5.65 2 8 11 14 4.78 -2 -8 -11 8.03 3.78 -2 -8 11 5.95 4.05 -2 8 11 7.65 4.74 -2 8 -11 5.19 5.41 -2 8 11 9.49 8.64 2 -8 -11 5.56 3.76 2 -8 -12 65.35 5.7 -2 8 12 52.36 6.33 2 -8 -12 66.35 7.53 2 8 12 58.35 6.51 -2 -8 12 65.23 5.87 -2 -8 -12 53.37 5.33 -2 8 -12 60.09 7.18 -2 8 12 58.83 10.79 2 8 12 59.2 6.24 2 8 13 61.87 6.79 -2 -8 -13 50.46 5.6 -2 8 13 49.81 11.13 -2 8 -13 59.71 7.75 -2 8 13 53.52 6.79 2 -8 -13 53.86 5.64 -2 8 -14 132.11 10.04 -2 8 14 139.88 9.64 -2 -8 -14 107.3 7.79 2 -8 -14 132.72 8.26 2 8 14 131.28 9.19 2 8 15 1 6.36 2 -8 -15 7.98 5.29 -2 8 15 3.6 6.73 -2 -8 -15 0.36 4.86 -2 8 -15 3.56 7.23 -2 8 -16 110.73 10.2 2 8 16 100.59 9.22 -2 -8 -16 97.55 7.82 2 -8 -16 93.56 7.88 -2 8 16 88.95 9.57 2 8 17 10.45 7.73 -2 -8 -17 13.45 5.85 2 -8 -17 11.73 6 -2 8 17 5.83 7.91 -2 8 -17 22.79 8.15 -2 -8 -17 12.78 6.58 2 8 18 1.88 8.11 -2 8 18 2.6 8.53 -2 8 -18 17.16 8.39 -2 -8 -18 7.5 6.79 -2 8 19 -3.88 9.34 2 8 19 -2.14 8.65 -2 8 -19 2.71 8.73 -2 -8 -19 3 7.23 2 8 20 12.76 9.49 -2 8 20 2.62 9.63 -2 8 -20 20.72 9.54 2 -10 0 393.54 16.68 -2 -10 0 418.31 16.86 2 -10 0 418.99 16.1 -2 -10 0 432.97 18.26 -2 10 0 407.74 19.74 2 -10 0 466 21.18 2 -10 1 526.07 21.55 -2 -10 1 550.69 21.7 -2 -10 1 585.91 22.99 -2 -10 -1 565.37 22.81 2 -10 1 593.24 21.1 -2 10 1 495.13 24.49 2 -10 1 576.04 25.73 2 -10 -1 581.26 20.59 2 -10 -1 599.14 25.86 2 -10 -1 539.55 21.31 -2 10 -1 476.34 23.83 -2 -10 -1 549.25 21.4 -2 -10 -1 513.18 20.34 -2 -10 -2 118.11 5.64 2 -10 2 146.37 6.71 -2 10 -2 120.67 9.44 2 -10 -2 137.33 5.63 -2 -10 2 148.54 8.73 -2 -10 -2 145.4 8.49 -2 10 2 137.5 10.58 2 -10 -2 134.21 10.83 2 -10 2 136.48 11.04 -2 -10 -3 48.55 5.83 2 -10 -3 42.03 7.67 2 -10 3 51.5 4.25 -2 10 -3 38.7 6.03 -2 10 3 35.64 7.46 2 10 3 44.09 3.93 2 -10 3 42.64 8.22 -2 10 3 43.35 4 2 -10 -3 40.91 3.87 -2 -10 -3 43.9 3.1 2 -10 -4 447.11 16.74 -2 10 4 452.29 18.11 2 -10 -4 474.56 18.04 -2 -10 -4 458.46 19.5 -2 10 -4 449.16 19.81 2 -10 4 503.22 18.4 -2 10 4 379.13 22.06 2 -10 4 520.83 23.07 2 -10 -4 499.06 22.09 -2 -10 -4 430.35 17.17 2 10 4 459.19 18.16 -2 10 -5 1231.12 45.29 -2 10 -5 1258.78 46.56 -2 -10 -5 1234.71 45.51 2 10 5 1251.34 44.59 -2 -10 -5 1163.68 46.63 2 -10 5 1335.71 45.73 2 -10 5 1305.5 49.87 2 -10 -5 1239.9 48.82 2 -10 -5 1159.12 43.99 -2 10 5 1179.12 45.23 2 10 5 1218.74 45.31 -2 -10 -5 1241.6 44.56 -2 10 5 1108.94 50.02 2 -10 -5 1232.51 45.21 2 -10 -6 0.15 3.35 2 10 6 2.63 2.75 2 -10 -6 -2.29 5.91 -2 10 -6 5.12 3.4 -2 -10 -6 -0.09 3.24 -2 10 -6 7.61 4.34 -2 10 6 3.91 2.83 2 10 6 2.75 2.79 -2 -10 -6 -2.68 5.38 2 -10 6 -0.56 4.1 -2 10 6 -1.89 6.98 2 -10 6 -11.7 7.67 -2 -10 -7 192.52 9.58 -2 10 -7 177.21 9.54 -2 -10 -7 163.88 11.03 -2 10 7 173.81 14.58 2 -10 7 213.43 10.27 2 -10 7 194.26 13.58 -2 10 -7 197 9.59 2 -10 -7 201.6 12.33 2 10 7 206.11 9.37 2 -10 -7 222.83 9.7 2 10 7 200.79 8.85 -2 10 7 198.37 9.35 2 10 8 148.8 7.33 2 -10 -8 156.35 7.76 -2 -10 -8 137.63 7.76 -2 10 -8 139.5 8.2 2 -10 -8 137.31 7.21 -2 10 -8 130.5 7.41 -2 -10 -8 103.58 9.23 -2 10 8 114.26 12.31 2 -10 8 154.24 8.84 2 -10 -8 146.99 10.25 -2 -10 -8 139.44 7.16 -2 -10 8 150.14 7.36 -2 10 8 141.27 7.71 2 -10 -9 129.14 7.38 -2 -10 -9 128.43 7.03 2 -10 -9 125.44 7.08 2 10 9 127.81 7.19 -2 10 -9 125.97 8.13 -2 -10 9 125.4 7.1 2 -10 9 151.3 8.75 2 -10 -9 118.97 9.56 -2 10 9 105.67 12.45 -2 -10 -9 120.25 7.58 -2 10 9 136.26 7.71 -2 10 10 10.18 4.84 -2 -10 -10 -0.53 4.45 2 -10 -10 8.2 6.43 -2 -10 -10 2.49 3.6 2 -10 -10 1.01 3.66 -2 10 -10 0.99 5.05 -2 -10 10 3.34 4.03 -2 10 10 -1.79 9.55 2 -10 10 -0.72 5.57 2 10 10 -2.44 4.57 2 -10 -10 1.74 4.26 2 -10 -11 20.09 6.44 -2 -10 -11 12.17 5.04 -2 10 11 14.01 5.25 -2 -10 -11 8.72 4.15 2 -10 -11 12.65 4.25 -2 10 -11 3.86 5.57 -2 10 11 -0.73 10.22 2 10 11 8.23 4.8 -2 -10 -12 124.53 7.59 -2 -10 -12 117.87 8.29 2 -10 -12 126.78 7.73 -2 10 -12 120.08 9.01 2 -10 -12 124.2 9.81 -2 10 12 115.91 13.65 2 10 12 123.06 8.35 -2 10 12 116.82 8.54 -2 -10 -13 222.87 11.32 2 10 13 254.96 12.4 -2 10 -13 238.04 12.99 -2 10 13 235.37 18.04 2 -10 -13 225.81 11.44 -2 10 13 221.85 12.38 2 10 14 31.88 6.77 -2 -10 -14 21.32 5.24 -2 10 -14 22.87 7.32 2 -10 -14 14.75 5.28 -2 10 14 24.89 6.96 -2 -10 -15 2.88 5.11 2 -10 -15 4.21 5.1 -2 10 -15 13.06 7.63 2 10 15 3.98 6.83 -2 10 15 5.58 7.17 -2 -10 -16 -0.76 5.37 2 -10 -16 5.48 5.44 -2 10 -16 10.46 7.88 2 10 16 8.2 7.43 -2 10 16 3.9 7.44 2 10 17 70.6 9.49 -2 -10 -17 69.53 7.36 2 -10 -17 67.97 7.48 -2 10 17 72.43 9.6 -2 10 -17 74.08 9.73 -2 10 18 26.12 9.07 -2 -10 -18 26.97 6.75 2 -10 -18 27 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9.43 -7 -5 1 33.64 9.52 -7 5 -1 34.9 10.12 -7 5 1 29.49 10.52 -7 -5 -2 212.14 11.21 -7 5 -2 198.77 15.22 -7 5 2 207.26 16.6 -7 -5 -2 219.67 14.99 -7 -5 2 198.35 14.98 -7 -5 2 193.86 14.97 -7 -5 -2 197.37 14.28 -7 5 3 35.37 11.27 -7 -5 3 34.48 9.9 -7 -5 -3 30.44 8.97 -7 -5 -3 29.65 6.06 -7 -5 -3 29.75 9.54 -7 -5 3 32.3 9.62 -7 5 4 20.58 10.9 -7 -5 4 15.25 9.48 -7 -5 -4 5.34 5.61 -7 -5 -4 7.1 8.89 -7 -5 4 11.48 9.11 -7 5 5 15.48 11.55 -7 -5 5 35.4 9.79 -7 -5 -5 27.88 6.36 -7 -5 -5 34.73 9.22 -7 -5 5 25.91 9.19 -7 5 6 98.81 14.2 -7 -5 -6 99.9 8.36 -7 -5 6 94.07 11.97 -7 -5 -6 89.46 10.89 -7 -5 6 82.31 11.25 -7 -5 7 21.58 10.27 -7 -5 -7 12.36 6.73 -7 -5 -7 29.12 8.92 -7 -5 7 22.76 9.23 -7 5 7 23.64 12.39 -7 -5 8 32.45 10.44 -7 -5 -8 23.36 7.17 -7 -5 -8 17.02 8.74 -7 -5 8 26.28 9.04 -7 5 8 18.3 12.75 -7 -5 9 6.62 9.77 -7 -5 -9 3.41 7.25 -7 -5 -9 11.79 8.56 -7 5 9 -7.75 11.92 -7 -5 10 116.17 13.2 -7 5 10 111.57 15.78 -7 -5 11 36.74 11.45 -7 5 11 20.76 13.82 -7 -5 12 52.86 11.97 -7 5 12 37.09 14.84 -7 -5 13 2.79 11.08 -7 5 13 6.45 14.41 -7 -5 14 38.66 12.26 -7 5 -14 34.37 9.38 -7 5 14 36.99 15.99 -7 -5 15 21.21 12.48 -7 5 -15 22.9 9.36 -7 5 15 8.54 15.45 -7 -7 0 -2.08 5.27 -7 -7 0 -10.55 9.39 -7 7 0 -5.24 11.06 -7 -7 -1 122.03 8.79 -7 -7 1 130.98 8.57 -7 -7 -1 120.91 12.83 -7 -7 1 113.84 13.05 -7 7 -1 125.79 14.42 -7 7 1 136.71 14.9 -7 -7 -2 44.71 6.72 -7 -7 -2 42.77 10.55 -7 -7 2 39.82 10.81 -7 7 -2 26.78 10.9 -7 7 2 47.1 12.48 -7 -7 -3 128.8 9.04 -7 -7 3 108.88 12.74 -7 -7 -3 122.35 12.89 -7 7 3 114.89 14.9 -7 -7 4 6.52 9.18 -7 -7 -4 -4.47 6.01 -7 -7 -4 -4.01 9.56 -7 -7 4 -3.48 9.11 -7 7 4 2.58 11.93 -7 -7 5 49.28 10.47 -7 -7 -5 35.79 6.8 -7 -7 -5 43.83 10.28 -7 -7 5 46.23 10.53 -7 7 5 44.39 13.14 -7 -7 6 41.01 10.41 -7 -7 -6 28.04 6.85 -7 -7 -6 24.84 9.72 -7 -7 6 21.98 10.07 -7 7 6 26.89 12.67 -7 -7 -7 103.13 8.86 -7 -7 7 91.32 11.96 -7 -7 -7 84.57 11.07 -7 -7 7 81.85 11.51 -7 7 7 84.37 15.51 -7 -7 8 4.49 9.91 -7 -7 -8 9.2 7.2 -7 -7 -8 11.43 9.15 -7 -7 8 5.81 8.92 -7 7 8 18.4 14.06 -7 -7 9 9.76 10 -7 -7 -9 3.89 7.41 -7 -7 -9 10.3 8.78 -7 7 9 18.15 14.2 -7 -7 10 5.6 10.25 -7 -7 -10 19.31 8.29 -7 7 10 4.54 14.52 -7 -7 -11 126.19 11.23 -7 -7 11 120.59 13.43 -7 7 11 106.05 18.87 -7 -7 12 1.77 10.42 -7 7 12 -2.57 15.22 -7 -7 13 7.05 10.92 -7 7 13 9.86 16.78 -7 -7 14 7.5 10.99 -7 7 14 -8.33 16.96 -7 -7 15 34.25 12.34 -7 -9 0 -2.48 5.64 -7 9 0 -1.63 11.67 -7 -9 -1 8.29 5.93 -7 9 -1 -3.49 11.31 -7 9 1 -8.92 12.37 -7 -9 -2 221.77 12.23 -7 9 2 233.47 19.74 -7 -9 -3 4.5 6.31 -7 9 3 -2.76 12.49 -7 -9 -4 -0.29 6.2 -7 9 4 7.66 13.25 -7 -9 -5 8.96 6.44 -7 9 5 -1.98 13.05 -7 -9 -6 99.05 9.05 -7 9 6 98.74 16.9 -7 -9 -7 2.48 6.98 -7 9 7 2.61 14.29 -7 -9 8 24.99 10.35 -7 -9 -8 8.19 7.44 -7 -9 -8 9.07 9.79 -7 -9 8 3.24 9.51 -7 9 8 14.88 15.41 -7 -9 9 5.02 10.32 -7 -9 -9 8.01 7.73 -7 9 9 -11.87 16.07 -7 -9 10 98.26 12.66 -7 -9 -10 84.68 10.1 -7 9 10 74.41 17.76 -7 -9 11 16.09 10.4 -7 -9 -11 8.51 8.64 -7 9 11 -1.11 16.88 -7 -9 12 39.37 11.26 -7 -9 -12 8.94 9.11 -7 9 12 11.8 17.04 -7 -9 13 8.97 10.84 -7 9 13 3.41 17.4 -7 -9 14 27.91 11.71 -7 11 0 -2.57 12.47 -7 -11 -1 86.45 8.17 -7 11 -1 69.67 14.19 -7 11 1 50.81 14.05 -7 -11 -2 3.35 6.35 -7 11 2 15.11 14 -7 -11 -3 80.87 8.47 -7 11 3 71.06 15.61 -7 -11 -4 -2.44 6.87 -7 11 4 -6.16 14.14 -7 -11 -5 30.2 7.5 -7 11 5 5.32 14.82 -7 -11 -6 1.59 7.11 -7 11 6 -7.66 15.66 -7 -11 -7 69.93 8.92 -7 11 7 59.56 17.48 -7 -11 -8 7.99 7.68 -7 11 8 0.57 16.32 -7 -11 -9 10.97 8.2 -7 11 9 1.17 17.1 -7 -11 -10 1.6 8.38 -7 11 10 10.6 17.44 -7 -11 11 86.5 12.99 -7 -11 -11 84.52 10.48 -7 11 11 98.51 20.41 -7 -11 12 17.95 11.15 -7 -11 -12 -4.03 9.39 -7 11 12 14.88 18.53 -7 13 0 -13.67 13.97 -7 -13 -1 -1.21 6.81 -7 13 -1 6.89 13.13 -7 13 1 -13.88 14.66 -7 -13 -2 94.04 9.32 -7 13 2 95.48 16.66 -7 -13 -3 -1.58 7.24 -7 13 3 8.33 14.79 -7 -13 -4 3.88 7.33 -7 13 4 -5.96 15.12 -7 -13 -5 4.09 7.51 -7 13 5 14.54 15.88 -7 -13 -6 74.45 9.32 -7 13 6 58.86 18.06 -7 -13 -7 4.09 8.08 -7 13 7 -11.25 17.08 -7 -13 -8 21.24 8.49 -7 13 8 4.24 17.52 -7 -13 -9 8.73 8.49 -7 13 9 8.61 18.5 -7 -13 -10 63.93 9.84 -7 13 10 42.3 18.84 -7 15 0 -6.08 14.47 -7 15 1 24.75 15.1 -7 -15 -2 7.03 7.63 -7 15 2 4.15 15.17 -7 -15 -3 37.43 8.36 -7 15 3 44.66 17.02 -7 -15 -4 4.92 7.76 -7 15 4 -6.8 16.3 -7 -15 -5 14.48 8.38 -7 15 5 28.84 17.56 -7 -15 -6 -5.26 8.28 -7 15 6 10.33 17.44 -7 -15 -7 53.6 9.6 -7 15 7 43.05 18.97 -7 -15 -8 4.01 8.79 -7 15 8 7.02 18.74 -7 17 0 12.33 14.35 -7 17 1 16.55 15.03 -7 -17 -2 66.64 9.62 -7 17 2 85.66 17.77 -7 -17 -3 3.5 8.16 -7 17 3 3.85 16.3 -7 -17 -4 -9.61 8.53 -7 17 4 6.94 17.48 -7 -17 -5 0.18 8.52 -7 17 5 0.6 18.23 -7 -17 -6 36.62 9.37 -7 17 6 25.51 19.26 -7 19 1 65.68 17.57 -7 19 2 53.69 17.71 -7 19 3 36.87 17.77 -8 0 0 341.84 21.08 -8 0 0 362.14 21 -8 0 -1 0.3 9.75 -8 0 1 2.58 10.41 -8 0 -1 0.3 9.77 -8 0 1 10.64 10.23 -8 0 2 -2 10.76 -8 0 -2 11.09 10.05 -8 0 2 6.66 9.66 -8 0 3 4.13 10.97 -8 0 -3 -7.69 9.87 -8 0 3 -0.6 9.92 -8 0 4 82.36 13.61 -8 0 -4 102.52 12.58 -8 0 4 96.97 12.51 -8 0 5 -2.15 11.08 -8 0 -5 -4.82 9.76 -8 0 5 -2.6 9.87 -8 0 6 4.05 11.85 -8 0 -6 7.45 9.65 -8 0 6 8.18 10.09 -8 0 7 -2.97 12.08 -8 0 8 115.43 15.74 -8 0 9 -17 13.42 -8 0 10 54.87 13.84 -8 0 11 17.12 12.96 -8 0 12 79.26 14.74 -8 2 0 23.57 10.7 -8 -2 0 1.22 10.23 -8 -2 0 1.25 10.16 -8 -2 -1 115.3 13.25 -8 -2 1 108.17 13.23 -8 2 -1 160.94 14.03 -8 2 1 144.85 14.24 -8 -2 -1 133.22 13.89 -8 -2 1 142.34 14.42 -8 2 2 3.55 10.11 -8 -2 -2 7.82 9.8 -8 -2 2 2.73 9.83 -8 -2 2 -0.66 10.41 -8 2 3 91.56 13 -8 -2 -3 75.92 11.63 -8 -2 3 62.47 11.72 -8 -2 3 83.65 13.05 -8 2 4 19.19 11.1 -8 -2 -4 2.04 9.69 -8 -2 4 1.18 9.86 -8 -2 4 -5.56 11.1 -8 -2 -5 38.47 10.59 -8 -2 5 35.16 10.88 -8 2 5 53.07 12.53 -8 -2 5 32.08 12.38 -8 -2 -6 5.83 9.81 -8 -2 6 5.67 9.83 -8 2 6 26.59 12.38 -8 -2 6 -5.36 11.59 -8 -2 -7 5.94 9.65 -8 -2 7 21.24 10.14 -8 2 7 34.87 12.82 -8 -2 7 -5.8 11.87 -8 -2 8 -2.18 12.24 -8 -2 -8 -4.73 9.76 -8 -2 8 -7.25 9.83 -8 2 9 187.07 18.03 -8 -2 9 169.28 17.22 -8 2 10 20.75 13.89 -8 -2 10 -6.14 12.71 -8 2 11 27.29 13.79 -8 -2 11 9.02 12.62 -8 2 12 28.39 14.85 -8 -2 12 -1.45 13.59 -8 4 0 267.15 18.69 -8 -4 0 226.43 17.11 -8 -4 0 241.8 17.27 -8 4 1 6.75 11.02 -8 -4 1 6.32 10.1 -8 -4 -1 8.03 10.19 -8 -4 -1 11.92 10 -8 -4 1 11.98 10.32 -8 4 2 7.74 11.27 -8 -4 2 7.12 10.63 -8 -4 -2 12.12 10.04 -8 -4 2 7.94 10.19 -8 4 3 12.84 11.53 -8 -4 3 11.21 10.7 -8 -4 -3 9.53 9.97 -8 -4 3 4.22 10.02 -8 4 4 95.56 14.52 -8 -4 4 62.45 12.14 -8 -4 -4 58.53 11.57 -8 -4 4 68.88 11.83 -8 4 5 4.67 12.13 -8 -4 5 -1.36 11.03 -8 -4 -5 12.81 9.92 -8 -4 5 8.69 9.99 -8 4 6 30.31 13.31 -8 -4 6 11.84 11.52 -8 -4 -6 -1.39 9.56 -8 -4 6 4.24 9.65 -8 -4 -6 8.11 7.31 -8 4 7 20.01 13.28 -8 -4 7 6.63 11.55 -8 -4 -7 5.41 9.91 -8 -4 7 -0.55 9.68 -8 -4 -7 0.16 7.38 -8 4 8 109.31 16.14 -8 -4 -8 111.86 12.62 -8 -4 8 94.63 12.39 -8 -4 -8 101.11 10.3 -8 -4 8 97.34 14.36 -8 4 9 14.67 14.06 -8 -4 9 4.57 11.87 -8 -4 10 42.66 13.27 -8 4 10 42.39 15.44 -8 -4 11 -1.41 12.23 -8 4 11 9.32 14.18 -8 -6 0 15.47 10.71 -8 -6 0 22.66 10.91 -8 6 0 17.43 12.15 -8 -6 1 82.32 12.43 -8 -6 -1 84.81 12.52 -8 -6 -1 82.65 12.53 -8 -6 1 80.51 12.44 -8 6 1 88.12 14.51 -8 -6 2 13.07 10.76 -8 -6 -2 -1.24 10.16 -8 -6 2 9.68 10.37 -8 6 2 20.47 12.94 -8 -6 3 66.47 12.45 -8 -6 -3 53.75 11.55 -8 -6 3 61.75 11.85 -8 6 3 58.17 13.97 -8 -6 4 10.66 11.09 -8 -6 -4 12.9 6.99 -8 -6 -4 9.93 10.28 -8 -6 4 10.37 10.34 -8 6 4 6.74 13.04 -8 -6 5 25.61 11.56 -8 -6 -5 42.52 7.82 -8 -6 -5 47.05 11.27 -8 -6 5 46.58 11.29 -8 6 5 45.72 14.35 -8 -6 6 6.41 11.29 -8 -6 -6 3.83 7.16 -8 -6 -6 -1.44 10.2 -8 -6 6 -0.88 10.11 -8 6 6 -7.56 13.34 -8 -6 7 14.82 11.19 -8 -6 -7 6.71 7.44 -8 -6 -7 1.12 9.91 -8 -6 7 14.23 10.53 -8 6 7 17.72 14.41 -8 -6 8 14.14 11.92 -8 -6 -8 9.98 8.08 -8 -6 -8 18.45 10.3 -8 -6 8 22.81 10.4 -8 6 8 32.45 15.9 -8 -6 -9 119.68 11.05 -8 -6 9 124.91 14.87 -8 6 9 121 18.89 -8 -6 10 6.05 11.89 -8 6 10 -1.04 16 -8 -6 11 13.29 12.53 -8 6 11 15.88 16.85 -8 -8 0 135.13 15.46 -8 -8 0 162.72 15.33 -8 8 0 173.32 18.02 -8 -8 1 27.65 11.59 -8 -8 -1 23.46 11.26 -8 -8 -1 17.31 11.42 -8 -8 1 17.38 11.72 -8 8 1 18.97 13.94 -8 -8 2 8.74 11.02 -8 -8 -2 -2.46 6.9 -8 -8 -2 9.75 11.28 -8 -8 2 -0.34 11.15 -8 8 2 6.1 13.82 -8 -8 3 21.3 11.56 -8 -8 -3 9.32 6.93 -8 -8 -3 15.21 11.26 -8 -8 3 -2 10.76 -8 8 3 9.77 14.52 -8 -8 4 81.82 13.27 -8 -8 -4 62.85 8.49 -8 -8 -4 49.06 12.25 -8 -8 4 56.14 12.32 -8 8 4 68.64 16.52 -8 -8 5 28.7 11.58 -8 -8 -5 24.41 7.67 -8 -8 -5 19.99 11.3 -8 -8 5 20.28 11.13 -8 8 5 20.67 15.69 -8 -8 6 20.31 11.49 -8 -8 -6 4.13 7.53 -8 -8 -6 14.67 10.81 -8 -8 6 12.46 10.84 -8 8 6 17.51 15.42 -8 -8 7 17.79 11.93 -8 -8 -7 3.12 7.79 -8 -8 -7 9.47 10.75 -8 -8 7 9.9 10.43 -8 8 7 -4.87 15.91 -8 -8 8 67.01 13.51 -8 -8 -8 61.33 9.36 -8 -8 -8 71.82 11.78 -8 -8 8 66.45 12.03 -8 8 8 56.19 18.14 -8 -8 9 20.29 12.25 -8 -8 -9 19.49 8.72 -8 8 9 -1.13 17.02 -8 -8 10 28.02 12.42 -8 -8 -10 14.75 9.09 -8 8 10 -13.6 17.93 -8 -10 0 32.92 7.77 -8 -10 -1 47.9 8.24 -8 -10 -1 35.3 12.92 -8 10 1 32.31 15.79 -8 -10 -2 6.63 7.44 -8 -10 -2 -1.8 12.05 -8 -10 2 5.43 12.07 -8 10 2 1.01 14.86 -8 -10 -3 38.55 8.25 -8 -10 -3 45.62 12.87 -8 -10 3 27.86 12.82 -8 10 3 12.07 16.3 -8 -10 -4 31.36 8.13 -8 -10 -4 33.22 12.78 -8 -10 4 23.44 12.28 -8 10 4 3.27 16.01 -8 -10 5 32.1 12.05 -8 -10 -5 24.96 8.15 -8 -10 -5 21.16 12 -8 -10 5 12.25 11.72 -8 10 5 29.48 16.6 -8 -10 6 16.78 11.88 -8 -10 -6 6.42 7.73 -8 -10 -6 9.37 11.77 -8 -10 6 0.33 11.3 -8 10 6 -8.58 16.91 -8 -10 7 5.76 11.65 -8 -10 -7 1.36 8.04 -8 -10 -7 1.87 11.14 -8 -10 7 7.89 11.52 -8 10 7 3.51 17.14 -8 -10 8 43.31 12.67 -8 -10 -8 21.1 8.55 -8 -10 -8 26.79 11.87 -8 -10 8 19.22 11.72 -8 10 8 11.91 18.24 -8 -10 -9 53.88 9.76 -8 -12 0 70.68 9.04 -8 -12 -1 13.12 7.99 -8 -12 1 14.78 7.74 -8 12 1 23.49 15.86 -8 -12 -2 6.36 7.83 -8 12 2 -31.99 16.87 -8 -12 -3 11.38 8.17 -8 12 3 -10.86 16.53 -8 -12 -4 28.66 8.39 -8 12 4 12.98 17 -8 -12 -5 30.2 8.66 -8 12 5 26.77 17.32 -8 -12 -6 13.18 8.35 -8 12 6 -2.4 17.17 -8 -12 -7 9.29 8.3 -8 12 7 -0.61 18.15 -8 -12 -8 32.37 12.73 -8 -14 0 28.31 8.62 -8 -14 -1 14.38 8.39 -8 14 1 35.03 17.38 -8 -14 -2 1.03 8.21 -8 14 2 -13.72 17.31 -8 -14 -3 18.22 8.59 -8 14 3 -15.42 18.73 -8 -14 -4 24.01 8.95 -8 14 4 8.86 17.94 -8 -14 -5 19.23 8.84 -8 14 5 -7.95 19.16 -8 16 2 -5.59 17.76 -9 -1 0 15.22 11.42 -9 1 1 40.83 12.71 -9 -1 1 27.15 12.65 -9 -1 -1 23.91 11.69 -9 -1 1 21.97 11.92 -9 1 2 75.26 14.13 -9 -1 2 50.87 13.38 -9 -1 -2 46.83 12.8 -9 -1 2 46.91 12.53 -9 1 3 53.95 13.92 -9 -1 3 17.39 12.71 -9 -1 -3 31.11 11.88 -9 -1 3 26.87 11.73 -9 1 4 21.7 12.97 -9 -1 4 1.93 12.9 -9 -1 -4 11.58 11.41 -9 -1 4 15.02 11.52 -9 1 5 46.75 13.56 -9 -1 5 21.41 13.89 -9 -1 -5 23.8 11.29 -9 -1 5 22.97 11.86 -9 1 6 57.79 14.8 -9 -1 6 56.45 15.16 -9 1 7 47.55 14.86 -9 -1 7 32.46 14.68 -9 -3 0 10.23 11.5 -9 3 1 24.67 13.01 -9 -3 -1 24.46 11.91 -9 -3 1 22.84 12.02 -9 -3 1 35.89 12.85 -9 3 2 21.03 13.52 -9 -3 -2 18.17 12 -9 -3 2 20.01 11.87 -9 -3 2 17.12 12.69 -9 3 3 48.24 14.2 -9 -3 -3 55.96 12.9 -9 -3 3 36.87 12.36 -9 -3 3 29.25 13.71 -9 3 4 21.91 13.83 -9 -3 -4 10.4 11.43 -9 -3 4 8.57 11.52 -9 -3 4 -3.86 13.06 -9 -3 -5 26.34 11.97 -9 -3 5 14.84 11.68 -9 3 5 37.05 14.91 -9 -3 5 9.82 13.09 -9 3 6 42.82 15.57 -9 -3 6 37.95 14.17 -9 -3 -6 28.43 12.1 -9 -3 6 36.78 12.03 -9 3 7 68.81 16.5 -9 -3 7 59.99 15.27 -9 -3 -7 43.67 12.6 -9 -3 7 45.98 12.32 -9 -3 -8 -6.38 11.18 -9 -5 0 12.7 11.66 -9 -5 1 21.44 12.55 -9 -5 -1 31.42 12.22 -9 -5 1 11.66 11.68 -9 -5 2 36.85 13.48 -9 -5 -2 61.2 12.86 -9 -5 2 48.03 12.76 -9 5 2 63.04 15.94 -9 -5 3 30.94 13.49 -9 -5 -3 3.01 11.27 -9 -5 3 15.2 11.72 -9 5 3 18.34 14.67 -9 -5 4 14.5 13.32 -9 -5 -4 24.24 12.03 -9 -5 4 19.91 11.91 -9 5 4 12.29 14.37 -9 -5 5 12.69 13.35 -9 -5 -5 2.57 11.65 -9 -5 5 13.38 11.79 -9 5 5 10.67 14.93 -9 -5 -6 56.28 12.96 -9 -5 6 59.37 12.94 -9 -5 6 58.98 14.63 -9 5 6 79.7 17.45 -9 -5 -7 20.98 12.03 -9 -5 7 16.37 11.7 -9 -5 -8 6.46 11.26 -9 -7 0 10.04 12.04 -9 -7 1 26.55 13.16 -9 -7 -1 22.84 12.47 -9 -7 1 21.86 12.5 -9 -7 2 21.79 12.9 -9 -7 -2 11.34 12.08 -9 -7 2 21.4 12.31 -9 7 2 16.37 15.34 -9 -7 3 44.78 14.01 -9 -7 -3 47.45 13.33 -9 -7 3 29.93 12.45 -9 7 3 33.67 16.45 -9 -7 4 7.5 13.07 -9 -7 -4 6.83 12.24 -9 -7 4 7.26 11.95 -9 7 4 -3.69 15.53 -9 -7 5 30.85 13.57 -9 -7 -5 19.41 12.19 -9 -7 5 22 12.1 -9 7 5 13.02 16.4 -9 -7 -6 12.42 11.85 -9 -7 6 16.19 12.04 -9 -7 7 50.94 12.88 -9 -9 0 8.94 12.94 -9 -9 1 17.28 13.18 -9 -9 2 64.14 14.97 -9 9 2 52.71 17.71 -9 -9 3 9.53 13.5 -9 9 3 0.54 16.31 -9 9 4 1.69 17.45 -9 -11 1 23.86 14.29 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cl4 Bi1 Cl4 83.678(19) 14_457 . ? Bi1 Cl4 Bi1 165.21(14) 14_557 . ? Bi1 Br4 Bi1 165.21(14) 14_557 . ? H2A N2 H2B 109.5 . . ? H2A N2 H2C 109.5 . . ? H2B N2 H2C 109.5 . . ? C4 N2 H2A 109.5 . . ? C4 N2 H2B 109.5 . . ? C4 N2 H2C 109.5 . . ? N2 C4 H4A 107.6 . . ? N2 C4 H4B 107.6 . . ? H4A C4 H4B 107.0 . . ? C3 C4 N2 119.0(15) . . ? C3 C4 H4A 107.6 . . ? C3 C4 H4B 107.6 . . ? C4 C3 H3A 109.5 . . ? C4 C3 H3B 109.5 . . ? C4 C3 H3C 109.5 . . ? H3A C3 H3B 109.5 . . ? H3A C3 H3C 109.5 . . ? H3B C3 H3C 109.5 . . ? H1A C1 H1B 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? C2 C1 H1A 109.5 . . ? C2 C1 H1B 109.5 . . ? C2 C1 H1C 109.5 . . ? C1 C2 H2D 109.5 . . ? C1 C2 H2E 109.5 . . ? H2D C2 H2E 108.1 . . ? N1 C2 C1 110.7 . . ? N1 C2 H2D 109.5 . . ? N1 C2 H2E 109.5 . . ? C2 N1 H1D 109.5 . . ? C2 N1 H1E 109.5 . . ? C2 N1 H1F 109.5 . . ? H1D N1 H1E 109.5 . . ? H1D N1 H1F 109.5 . . ? H1E N1 H1F 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Bi1 Cl1 2.6680(13) . ? Bi1 Cl1 2.6680(13) 12_655 ? Bi1 Cl3 2.7925(19) . ? Bi1 Cl2 2.757(2) . ? Bi1 Cl4 2.8842(5) . ? Bi1 Cl4 2.8841(5) 14_457 ? Bi1 Br3 2.7925(19) . ? Bi1 Br1 2.6680(13) . ? Bi1 Br4 2.8842(5) . ? Bi1 Br2 2.757(2) . ? N2 H2A 0.8900 . ? N2 H2B 0.8900 . ? N2 H2C 0.8900 . ? N2 C4 1.440(17) . ? C4 H4A 0.9700 . ? C4 H4B 0.9700 . ? C4 C3 1.36(2) . ? C3 H3A 0.9600 . ? C3 H3B 0.9600 . ? C3 H3C 0.9600 . ? C1 H1A 0.9600 . ? C1 H1B 0.9600 . ? C1 H1C 0.9600 . ? C1 C2 1.5315 . ? C2 H2D 0.9700 . ? C2 H2E 0.9700 . ? C2 N1 1.5193 . ? N1 H1D 0.8900 . ? N1 H1E 0.8900 . ? N1 H1F 0.8900 . ?