#------------------------------------------------------------------------------ #$Date: 2024-02-04 13:40:19 +0200 (Sun, 04 Feb 2024) $ #$Revision: 289452 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/78/7247805.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7247805 loop_ _publ_author_name 'Pradhan, Abinash' 'Sahoo, Sanand' 'Samal, Saroj L.' _publ_section_title ; (C2H5NH3)2BiCl5−xBrx perovskites containing 1D chains: effect of Br substitution on their structural and optical properties ; _journal_issue 3 _journal_name_full CrystEngComm _journal_page_first 312 _journal_page_last 323 _journal_paper_doi 10.1039/D3CE01019H _journal_volume 26 _journal_year 2024 _chemical_formula_moiety 'Bi Br3.126 Cl1.874, C4 H16 N2' _chemical_formula_sum 'C4 H16 Bi Br3.13 Cl1.87 N2' _chemical_formula_weight 617.41 _space_group_crystal_system orthorhombic _space_group_IT_number 64 _space_group_name_Hall '-C 2ac 2' _space_group_name_H-M_alt 'C m c e' _atom_sites_solution_hydrogens geom _audit_creation_date 2023-06-01 _audit_creation_method ; Olex2 1.5-alpha (compiled 2021.06.29 svn.r12e2184c for OlexSys, GUI svn.r6374) ; _audit_update_record ; 2023-10-09 deposited with the CCDC. 2023-12-01 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 7.7670(3) _cell_length_b 22.3242(8) _cell_length_c 18.0376(6) _cell_measurement_reflns_used 3415 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 24.1230 _cell_measurement_theta_min 1.824 _cell_volume 3127.58(19) _computing_molecular_graphics 'Olex2 1.5-alpha (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5-alpha (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.948 _diffrn_measurement_device_type 'XtaLAB Pro II AFC12 (RINC): Kappa single' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0268 _diffrn_reflns_av_unetI/netI 0.0296 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.948 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -27 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 8850 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.948 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.123 _diffrn_reflns_theta_min 1.824 _exptl_crystal_density_diffrn 2.622 _exptl_crystal_description crystalline _exptl_crystal_F_000 2226 _exptl_crystal_size_max 0.16 _exptl_crystal_size_mid 0.15 _exptl_crystal_size_min 0.09 _refine_diff_density_max 0.788 _refine_diff_density_min -0.687 _refine_diff_density_rms 0.119 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.026 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 79 _refine_ls_number_reflns 1760 _refine_ls_number_restraints 57 _refine_ls_restrained_S_all 1.013 _refine_ls_R_factor_all 0.0506 _refine_ls_R_factor_gt 0.0339 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0236P)^2^+19.4857P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0622 _refine_ls_wR_factor_ref 0.0660 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1389 _reflns_number_total 1760 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL ab257_new_121221_a.res in Cmca ab257_new_121221.res created by SHELXL-2018/3 at 16:36:08 on 01-Jun-2023 REM Old TITL AB257_NEW_121221 in Cmce REM SHELXT solution in Cmca: R1 0.204, Rweak 0.019, Alpha 0.042 REM 0.487 for 99 systematic absences, Orientation as input REM Formula found by SHELXT: C2 Cl5 Bi CELL 0.71073 7.767 22.3242 18.0376 90 90 90 ZERR 8 0.0003 0.0008 0.0006 0 0 0 LATT 7 SYMM -X,0.5-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM +X,-Y,-Z SFAC C H Bi Br Cl N UNIT 32 128 8 25.01 14.99 16 EADP Cl3 Br3 EADP Cl1 Br1 EADP Cl4 Br4 EADP Cl2 Br2 SIMU 0.02 0.04 2 RIGU 0.01 0.01 N2 C4 C3 EXYZ Cl2 Br2 EXYZ Cl1 Br1 EXYZ Cl3 Br3 EXYZ Cl4 Br4 L.S. 20 0 0 PLAN 6 CONF list 4 MORE -1 BOND $H fmap 2 53 acta REM REM REM WGHT 0.023600 19.485699 FVAR 0.08686 0.32681 0.33591 0.30761 0.56753 BI1 3 0.500000 0.366602 0.630946 10.50000 0.03818 0.05880 = 0.04242 -0.00906 0.00000 0.00000 PART 5 CL1 5 0.245736 0.379676 0.530736 31.00000 0.06338 0.12129 = 0.07090 -0.00535 -0.02506 0.01335 PART 7 CL3 5 0.500000 0.490119 0.661517 40.50000 0.16411 0.05514 = 0.07482 -0.00998 0.00000 0.00000 PART 3 CL2 5 0.500000 0.244162 0.601465 20.50000 0.12186 0.05519 = 0.10382 -0.01678 0.00000 0.00000 PART 9 CL4 5 0.750000 0.349569 0.750000 50.50000 0.08927 0.13473 = 0.10494 0.00000 -0.06169 0.00000 PART 0 C1 1 0.000000 0.575616 0.651182 10.50000 0.28571 0.05777 = 0.09621 0.00350 0.00000 0.00000 PART -1 AFIX 33 H1A 2 0.000000 0.608819 0.617360 10.50000 -1.50000 H1B 2 -0.100919 0.577431 0.681828 10.50000 -1.50000 H1C 2 0.100919 0.577431 0.681828 10.50000 -1.50000 AFIX 0 PART 0 N1 6 0.000000 0.468118 0.651896 10.50000 0.13961 0.06723 = 0.06980 0.00364 0.00000 0.00000 PART -1 AFIX 33 H1D 2 0.000000 0.437733 0.619954 10.50000 -1.20000 H1E 2 0.093560 0.466080 0.680272 10.50000 -1.20000 H1F 2 -0.093560 0.466080 0.680272 10.50000 -1.20000 AFIX 0 PART 0 C2 1 0.000000 0.523305 0.612169 10.50000 0.21625 0.07367 = 0.10265 0.02227 0.00000 0.00000 AFIX 23 H2A 2 0.100427 0.523505 0.580204 10.50000 -1.20000 H2B 2 -0.100427 0.523505 0.580203 10.50000 -1.20000 AFIX 0 PART 6 BR1 4 0.245736 0.379676 0.530736 -31.00000 0.06338 0.12129 = 0.07090 -0.00535 -0.02506 0.01335 PART 8 BR3 4 0.500000 0.490119 0.661517 -40.50000 0.16411 0.05514 = 0.07482 -0.00998 0.00000 0.00000 PART 10 BR4 4 0.750000 0.349569 0.750000 -50.50000 0.08927 0.13473 = 0.10494 0.00000 -0.06169 0.00000 PART 4 BR2 4 0.500000 0.244162 0.601465 -20.50000 0.12186 0.05519 = 0.10382 -0.01678 0.00000 0.00000 PART -1 AFIX 6 N2 6 0.954783 0.744649 0.410853 10.50000 0.05422 0.15963 = 0.17753 0.08255 -0.01401 0.01548 AFIX 33 H2C 2 1.021293 0.725811 0.443576 10.50000 -1.20000 H2D 2 0.867246 0.762009 0.434350 10.50000 -1.20000 H2E 2 0.914307 0.718351 0.378119 10.50000 -1.20000 AFIX 5 C4 1 1.060629 0.792449 0.370431 10.50000 0.08926 0.20226 = 0.19682 0.07384 0.00730 0.00504 AFIX 23 H4A 2 1.106168 0.820805 0.406149 10.50000 -1.20000 H4B 2 1.157016 0.773634 0.345391 10.50000 -1.20000 AFIX 5 C3 1 0.950098 0.825386 0.314109 10.50000 0.08565 0.14845 = 0.14886 0.06009 0.01734 -0.02542 AFIX 33 H3A 2 1.018408 0.855120 0.289348 10.50000 -1.50000 H3B 2 0.906414 0.797376 0.278374 10.50000 -1.50000 H3C 2 0.855652 0.844467 0.339028 10.50000 -1.50000 AFIX 0 HKLF 4 REM ab257_new_121221_a.res in Cmca REM wR2 = 0.0660, GooF = S = 1.026, Restrained GooF = 1.013 for all data REM R1 = 0.0339 for 1389 Fo > 4sig(Fo) and 0.0506 for all 1760 data REM 79 parameters refined using 57 restraints END WGHT 0.0236 19.4862 REM Highest difference peak 0.788, deepest hole -0.687, 1-sigma level 0.119 Q1 1 1.0000 0.7968 0.3911 10.50000 0.05 0.79 Q2 1 1.0000 0.7633 0.3426 10.50000 0.05 0.75 Q3 1 0.5886 0.4979 0.6797 11.00000 0.05 0.61 Q4 1 0.2772 0.4226 0.5437 11.00000 0.05 0.51 Q5 1 0.9184 0.3192 0.7387 11.00000 0.05 0.51 Q6 1 0.8122 0.3341 0.7214 11.00000 0.05 0.46 REM The information below was added by Olex2. REM REM R1 = 0.0339 for 1389 Fo > 4sig(Fo) and 0.0506 for all 9213 data REM 79 parameters refined using n/a restraints REM Highest difference peak 0.79, deepest hole -0.69 REM Mean Shift 0, Max Shift -0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0506 REM R1_gt = 0.0339 REM wR_ref = 0.0660 REM GOOF = 1.026 REM Shift_max = -0.001 REM Shift_mean = 0 REM Reflections_all = 9213 REM Reflections_gt = 1389 REM Parameters = 79 REM Hole = -0.69 REM Peak = 0.79 REM Flack = n/a ; _cod_data_source_file d3ce01019h2.cif _cod_data_source_block ab257_new_121221 _cod_depositor_comments 'Adding full bibliography for 7247803--7247812.cif.' _cod_original_sg_symbol_Hall '-C 2bc 2' _cod_database_code 7247805 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 24.1450 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H,H) groups, All N(H,H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Shared sites {Cl2, Br2} {Cl1, Br1} {Cl3, Br3} {Cl4, Br4} 3. Uiso/Uaniso restraints and constraints All non-hydrogen atoms have similar U: within 2A with sigma of 0.02 and sigma for terminal atoms of 0.04 within 2A Uanis(Cl3) = Uanis(Br3) Uanis(Cl1) = Uanis(Br1) Uanis(Cl4) = Uanis(Br4) Uanis(Cl2) = Uanis(Br2) 4. Rigid body (RIGU) restrains N2, C4, C3 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01 5. Others Sof(Br2)=0.5*(1-FVAR(2)) Sof(Cl2)=0.5*FVAR(2) Sof(Br1)=1-FVAR(2) Sof(Cl1)=FVAR(2) Sof(Br3)=0.5*(1-FVAR(4)) Sof(Cl3)=0.5*FVAR(4) Sof(Br4)=0.5*(1-FVAR(5)) Sof(Cl4)=0.5*FVAR(5) Fixed Sof: H1B(0.5) H1C(0.5) H1E(0.5) H1F(0.5) H2A(0.5) H2B(0.5) N2(0.5) H2C(0.5) H2D(0.5) H2E(0.5) C4(0.5) H4A(0.5) H4B(0.5) C3(0.5) H3A(0.5) H3B(0.5) H3C(0.5) 6.a Free rotating group: N2(C4,C3) 6.b Secondary CH2 refined with riding coordinates: C2(H2A,H2B), C4(H4A,H4B) 6.c Me refined with riding coordinates: C1(H1A,H1B,H1C), N1(H1D,H1E,H1F), N2(H2C,H2D,H2E), C3(H3A,H3B,H3C) ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y, -z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1, z+1/2' '-x+1/2, y+1, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x, y-1/2, -z-1/2' 'x, -y-1/2, z-1/2' '-x, y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, y, -z-1/2' 'x+1/2, -y, z-1/2' '-x+1/2, y+1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Bi1 Bi 0.500000 0.36660(2) 0.63095(2) 0.04647(13) Uani 1 2 d S T P . . Cl1 Cl 0.24574(13) 0.37968(5) 0.53074(6) 0.0852(5) Uani 0.336(5) 1 d . U P A 5 Cl3 Cl 0.500000 0.49012(6) 0.66152(9) 0.0980(8) Uani 0.308(8) 2 d S TU P A 7 Cl2 Cl 0.500000 0.24416(6) 0.60147(10) 0.0936(8) Uani 0.327(8) 2 d S TU P A 3 Cl4 Cl 0.750000 0.34957(10) 0.750000 0.1096(11) Uani 0.568(8) 2 d S TU P A 9 C1 C 0.000000 0.5756(6) 0.6512(7) 0.147(7) Uani 1 2 d S TU P . . H1A H 0.000000 0.608819 0.617360 0.220 Uiso 0.5 1 calc R U P B -1 H1B H -0.100919 0.577431 0.681828 0.220 Uiso 0.5 1 calc R U P B -1 H1C H 0.100919 0.577431 0.681828 0.220 Uiso 0.5 1 calc R U P B -1 N1 N 0.000000 0.4681(4) 0.6519(5) 0.092(3) Uani 1 2 d S TU P . . H1D H 0.000000 0.437733 0.619954 0.111 Uiso 0.5 1 calc R U P C -1 H1E H 0.093560 0.466080 0.680272 0.111 Uiso 0.5 1 calc R U P C -1 H1F H -0.093560 0.466080 0.680272 0.111 Uiso 0.5 1 calc R U P C -1 C2 C 0.000000 0.5233(6) 0.6122(8) 0.131(6) Uani 1 2 d S TU P . . H2A H 0.100427 0.523505 0.580204 0.157 Uiso 0.5 1 calc R U P . . H2B H -0.100427 0.523505 0.580203 0.157 Uiso 0.5 1 calc R U P . . Br1 Br 0.24574(13) 0.37968(5) 0.53074(6) 0.0852(5) Uani 0.664(5) 1 d . U P A 6 Br3 Br 0.500000 0.49012(6) 0.66152(9) 0.0980(8) Uani 0.692(8) 2 d S TU P A 8 Br4 Br 0.750000 0.34957(10) 0.750000 0.1096(11) Uani 0.432(8) 2 d S TU P A 10 Br2 Br 0.500000 0.24416(6) 0.60147(10) 0.0936(8) Uani 0.673(8) 2 d S TU P A 4 N2 N 0.9548(16) 0.7446(7) 0.4109(8) 0.130(7) Uani 0.5 1 d G U P D -1 H2C H 1.021293 0.725811 0.443576 0.157 Uiso 0.5 1 calc R U P D -1 H2D H 0.867246 0.762009 0.434350 0.157 Uiso 0.5 1 calc R U P D -1 H2E H 0.914307 0.718351 0.378119 0.157 Uiso 0.5 1 calc R U P D -1 C4 C 1.0606(15) 0.7924(9) 0.3704(10) 0.163(9) Uani 0.5 1 d G U P D -1 H4A H 1.106168 0.820805 0.406149 0.195 Uiso 0.5 1 calc R U P D -1 H4B H 1.157016 0.773634 0.345391 0.195 Uiso 0.5 1 calc R U P D -1 C3 C 0.950(2) 0.8254(8) 0.3141(9) 0.128(8) Uani 0.5 1 d G U P D -1 H3A H 1.018408 0.855120 0.289348 0.191 Uiso 0.5 1 calc R U P D -1 H3B H 0.906414 0.797376 0.278374 0.191 Uiso 0.5 1 calc R U P D -1 H3C H 0.855652 0.844467 0.339028 0.191 Uiso 0.5 1 calc R U P D -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Bi1 0.03818(19) 0.0588(2) 0.04242(19) -0.00906(16) 0.000 0.000 Cl1 0.0634(7) 0.1213(9) 0.0709(7) -0.0054(6) -0.0251(5) 0.0133(6) Cl3 0.1641(18) 0.0551(9) 0.0748(11) -0.0100(7) 0.000 0.000 Cl2 0.1219(15) 0.0552(10) 0.1038(13) -0.0168(8) 0.000 0.000 Cl4 0.0893(15) 0.1347(19) 0.1049(17) 0.000 -0.0617(13) 0.000 C1 0.29(2) 0.058(8) 0.096(10) 0.003(7) 0.000 0.000 N1 0.140(9) 0.067(6) 0.070(6) 0.004(5) 0.000 0.000 C2 0.216(16) 0.074(9) 0.103(10) 0.022(8) 0.000 0.000 Br1 0.0634(7) 0.1213(9) 0.0709(7) -0.0054(6) -0.0251(5) 0.0133(6) Br3 0.1641(18) 0.0551(9) 0.0748(11) -0.0100(7) 0.000 0.000 Br4 0.0893(15) 0.1347(19) 0.1049(17) 0.000 -0.0617(13) 0.000 Br2 0.1219(15) 0.0552(10) 0.1038(13) -0.0168(8) 0.000 0.000 N2 0.054(14) 0.160(13) 0.178(14) 0.083(11) -0.014(9) 0.015(8) C4 0.089(16) 0.20(2) 0.20(2) 0.074(14) 0.007(12) 0.005(13) C3 0.086(19) 0.148(15) 0.149(16) 0.060(12) 0.017(11) -0.025(11) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Bi Bi -4.1077 10.2566 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u 0 0 2 63.78 1.83 0 0 -2 63.61 1.86 0 0 -2 64.29 1.92 0 0 -3 -0.26 0.5 0 0 -3 2.39 0.67 0 0 3 0.65 0.56 0 0 4 2613.97 58.33 0 0 -4 2650.4 58.48 0 0 -4 2621.53 58.61 0 0 -5 -0.92 0.89 0 0 -5 -0.77 1.07 0 0 5 0.94 0.94 0 0 -6 301.08 8.17 0 0 6 302.34 7.86 0 0 -6 292.64 8.06 0 0 -7 -1.34 1.48 0 0 -7 0.6 1.1 0 0 7 0.8 1.24 0 0 -8 2314.41 52.11 0 0 -8 2244.38 51.9 0 0 -9 1.73 1.91 0 0 -9 2.22 1.65 0 0 -10 626.16 16.56 0 0 -10 630.58 16.36 0 0 -11 1.99 2.39 0 0 -11 -0.81 1.92 0 0 -12 459.21 13.54 0 0 -12 480.42 13.43 0 0 -13 2.06 2.92 0 0 -13 1.11 2.37 0 0 -14 17.11 3.11 0 0 -15 2.6 2.74 0 0 -16 17.89 3.69 0 0 -17 -1.28 3.43 0 0 -18 153.93 7.92 0 0 -19 2.88 4.01 0 0 -20 77.99 6.45 0 0 -21 8.44 4.71 0 0 -22 21.17 5.37 0 2 0 67.29 1.8 0 -2 0 70.38 1.83 0 -2 0 67.93 1.86 0 2 0 67.86 1.85 0 -2 -1 2988.53 65.85 0 2 1 3000.35 65.87 0 2 -1 2999.16 65.87 0 2 2 65.41 1.97 0 -2 -2 63.95 1.95 0 -2 3 1203.67 26.69 0 -2 -3 1156.6 26.76 0 2 3 1195.12 26.76 0 2 4 10.63 1.02 0 2 -4 8.44 0.99 0 -2 -4 14.92 1.28 0 -2 4 11.45 1.03 0 -2 -4 12.65 1.02 0 -2 5 14.93 1.39 0 2 -5 15.12 1.4 0 -2 5 15.15 1.21 0 -2 -5 16.11 1.49 0 2 5 15.92 1.32 0 -2 -5 17.15 1.25 0 -2 5 16.62 1.17 0 -2 -5 14.61 1.24 0 -2 -5 15.24 1.1 0 -2 -6 953.54 20.88 0 -2 -6 935.15 21.78 0 2 6 931.97 21.88 0 -2 6 920.05 20.89 0 -2 -6 929.65 21.85 0 -2 -6 921.47 20.93 0 -2 6 915.05 20.89 0 -2 6 893.85 21.54 0 2 -6 906.79 21.71 0 -2 7 15.27 1.67 0 2 7 12.6 1.6 0 -2 -7 15.99 0.88 0 -2 -7 16.32 1.62 0 -2 -7 13.6 1.79 0 2 -7 13.33 1.73 0 2 -8 111.67 4.35 0 -2 8 115.76 4.05 0 -2 -8 117.07 4.42 0 -2 -8 122.19 4.58 0 -2 -9 3299.87 74.52 0 2 -9 3335.84 74.32 0 -2 -9 3327 74.52 0 -2 9 3210.14 73.85 0 2 -9 3322 74.91 0 -2 -10 134.43 5.4 0 2 -10 146.18 5.52 0 -2 10 140.39 5.07 0 2 -10 139.87 5.76 0 -2 -10 153.73 5.86 0 2 -11 287.61 9.61 0 -2 -11 303.62 9.6 0 2 -11 300.28 9.2 0 -2 -11 295.36 9.27 0 -2 -12 28.9 2.95 0 2 -12 29.95 3.23 0 2 -12 31.81 3.29 0 -2 -12 27.69 3.74 0 -2 -13 187.32 7.18 0 -2 -13 184 7.58 0 2 -13 177.33 7.3 0 -2 -14 5.05 3.5 0 -2 -14 1.68 2.54 0 2 -14 0.37 2.57 0 2 -15 13.54 3.4 0 -2 -15 19.22 3.36 0 -2 -16 19.39 3.47 0 2 -16 15.37 3.71 0 -2 -17 277.38 10.15 0 2 -17 255.9 10.3 0 2 -18 9.62 4.05 0 -2 -18 15.58 3.95 0 -2 -19 3.95 3.93 0 2 -19 -1.48 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13.43 3.39 0 -20 6 26.37 5.84 0 -20 -7 36.7 4.07 0 -20 -7 47.44 6.87 0 -20 -7 33.88 4.43 0 -20 7 51.7 6.88 0 20 -8 19.2 3.96 0 -20 -8 11.7 3.87 0 -20 -8 23.8 3.66 0 -20 -8 30.69 6.17 0 -20 8 23.36 5.94 0 -20 9 70.52 7.42 0 -20 -9 50.62 5.18 0 20 -9 48.1 4.92 0 -20 -9 55.65 4.54 0 -20 -9 65.94 7.51 0 20 -10 -0.36 3.82 0 -20 -10 6.17 3.47 0 20 -11 5.41 3.88 0 -20 -11 7.72 3.58 0 -20 -12 61.97 5.08 0 20 -12 43.39 5.27 0 20 -13 86.93 6.33 0 -20 -13 76.41 5.45 0 20 -14 -0.81 4.57 0 -20 -14 0.85 3.93 0 20 -15 0.62 4.53 0 -20 -15 5.1 4.25 0 -20 -16 16.71 4.71 0 -22 0 36.08 6.57 0 -22 1 17.32 6.07 0 -22 -1 13.63 5.83 0 -22 -2 11.68 3.75 0 -22 2 7.34 5.62 0 -22 -2 11 6.05 0 -22 -3 40.92 4.77 0 -22 -3 64.72 7.48 0 -22 3 53.01 7.2 0 -22 -4 84.79 8.22 0 -22 -4 65.44 5.34 0 -22 4 78.44 7.92 0 -22 -5 2 3.8 0 -22 -5 3.62 5.9 0 -22 5 5.04 5.85 0 -22 6 27.42 6.03 0 -22 -6 24.12 6.19 0 -22 -6 11.28 4.02 0 -22 7 32.89 6.68 0 -22 -7 32.41 6.56 0 -22 -7 20.69 4.52 0 -22 -8 39.41 4.97 0 -22 -8 70.14 7.65 0 -22 8 48.62 7.1 0 -22 -9 3.2 4.24 0 -22 -9 6.2 6.41 0 22 -10 22.97 4.65 0 -22 -10 20.21 5.11 0 -22 -11 31.81 5.44 0 22 -11 49.86 5.36 0 22 -12 32.09 5.23 0 -22 -12 26.92 5.28 0 22 -13 0.62 4.58 0 -24 0 27.66 6.9 0 -24 1 77.03 8.44 0 -24 -1 93.07 8.71 0 -24 -2 9.84 6.43 0 -24 2 8.68 6.01 0 -24 -3 41.8 5.18 0 -24 -3 54.05 7.63 0 -24 3 56.05 7.81 0 -24 -4 18.27 6.47 0 -24 4 23.75 6.69 0 -24 -4 12.68 4.33 0 -24 -5 93.71 8.89 0 -24 5 97.4 9.05 0 -24 -5 79.36 6.1 0 -24 6 1.16 6.03 0 -24 -6 4.66 6.18 0 -24 -6 1.19 4.44 0 -24 7 14.18 6.84 0 -24 -7 13.54 4.66 0 -24 -7 22.54 7.02 0 -24 -8 -0.41 4.68 0 -24 8 13.32 6.72 0 -24 -8 15.98 6.96 0 -24 -9 22.72 5.31 0 -24 -10 0.22 4.81 0 -24 -11 -2.9 5.16 0 -26 0 50.24 8.45 0 -26 -1 1.68 6.51 0 -26 1 8.44 6.67 0 -26 2 -1.27 6.6 0 -26 -2 -2.53 6.63 0 -26 3 10.94 7.05 0 -26 -3 0.42 6.51 0 -26 4 53.58 8.36 0 -26 -4 53.76 8 0 -26 -5 12.45 7.17 0 -26 5 8.31 7.15 0 -26 -6 6.47 5 0 -26 6 5.79 6.96 0 -26 -6 3.74 7.11 0 -26 7 5.3 7.09 0 -26 -7 7.42 6.84 0 -26 -7 3.42 4.87 0 -26 -8 18.03 7.52 0 -26 -8 18.81 5.44 0 -26 8 10.8 7.25 0 -26 -9 4.45 5.11 1 1 0 0.3 0.36 -1 -1 0 0.2 0.35 1 1 0 -0.04 0.42 -1 -1 0 -0.04 0.46 1 1 -1 654.18 15.17 -1 -1 -1 627.5 15.21 1 1 1 648.06 15.19 -1 -1 -1 629.51 15.07 1 1 1 663.95 14.68 1 1 1 653.59 14.61 -1 -1 1 635.01 15.08 1 1 1 638.35 15.16 -1 -1 -1 655.5 14.63 -1 -1 -1 644.98 14.71 -1 -1 -2 2007.18 44.98 -1 -1 -2 1990.11 45.36 -1 -1 2 2014.09 44.95 1 -1 2 2011.19 44.51 -1 -1 -2 2059.21 44.67 1 1 2 1987 45.1 1 1 -2 2040.29 45.07 -1 1 -2 2003.9 44.52 1 1 2 1994.09 45.31 1 1 2 2019.01 44.66 -1 -1 -3 1247.73 27.61 -1 1 -3 1233.97 27.52 1 1 3 1225.31 27.59 1 -1 3 1204.7 28.38 -1 -1 -3 1219.58 28.29 1 1 -3 1224.84 27.78 -1 -1 3 1242.31 27.65 -1 -1 -3 1227.18 27.67 1 -1 3 1206.64 27.5 1 1 3 1177.73 27.8 1 1 3 1250.93 28.26 -1 -1 -4 4.96 0.7 1 1 4 3.23 1.35 1 -1 4 3.34 0.82 1 1 4 3.99 0.75 1 -1 4 5.44 1.26 1 1 -4 3.08 0.66 1 1 4 5.34 0.83 -1 -1 4 4.64 0.65 -1 -1 -4 3.78 0.77 -1 -1 -4 7.88 1.57 -1 1 -4 4.21 0.77 -1 -1 -5 78.42 2.53 1 1 -5 75.87 2.66 -1 -1 -5 82.73 3.55 1 1 5 78.45 2.67 -1 1 -5 81.86 3.59 1 1 5 81.67 2.88 -1 1 -5 84.13 2.94 1 1 5 82.74 3.47 -1 -1 -5 85.58 3 1 -1 5 80.49 3.48 1 1 -5 84.78 2.66 1 1 5 85.3 2.72 1 -1 6 1581.73 37.5 1 1 6 1595.24 36.3 -1 1 -6 1634.72 37.62 1 1 6 1633.01 37.43 1 1 -6 1634.68 36.22 -1 -1 -6 1594.12 37.6 1 1 6 1581.24 36.32 1 1 -6 1626.23 36.23 1 1 6 1679.8 36.91 -1 -1 -6 1610.05 36.94 1 1 -6 1596.33 36.29 -1 1 -6 1629.5 36.91 1 1 -7 873.52 19.59 1 -1 7 823.08 20.8 -1 1 -7 866.41 20.31 1 1 7 839.68 20.19 1 1 -7 839.56 19.32 1 -1 7 864.37 19.27 -1 1 -7 838.89 20.94 1 1 -7 841.25 19.25 1 -1 -7 821.59 20.51 -1 -1 -7 846.94 20.94 1 1 7 832.29 19.33 -1 -1 -7 841.53 20.3 1 1 7 819.87 20.6 1 1 7 824.76 19.35 1 1 -8 5 1.41 1 -1 8 3.99 0.71 -1 1 -8 2.26 1.92 1 1 8 5.87 0.87 1 1 -8 6.48 0.86 -1 -1 -8 8.02 2.24 1 1 8 6.24 0.92 1 -1 -8 4.1 1.47 -1 -1 -8 7.58 1.54 1 1 -8 5.23 0.84 -1 1 -8 5.74 1.45 1 -1 -8 8.35 1.66 1 -1 -8 3.8 0.71 1 1 8 4.34 1.45 1 -1 8 2.02 1.77 1 1 8 3.54 1.76 1 -1 9 3.51 2.17 -1 -1 -9 2.35 2.15 1 -1 -9 2.66 0.67 1 1 9 4.78 0.95 1 1 -9 4.96 0.89 1 1 9 3.94 0.95 1 1 -9 3.99 0.87 -1 1 -9 2.9 1.54 1 1 -9 3.64 1.69 -1 1 -9 4.41 2.42 1 -1 -9 6.65 1.83 1 -1 -9 2.69 1.67 1 -1 9 3.14 0.68 -1 -1 -9 5.88 1.64 1 1 9 3.97 1.97 1 -1 -10 474.7 11.52 -1 -1 -10 502.99 14.09 -1 -1 -10 499.94 13.5 -1 1 -10 489.92 14.04 1 -1 10 491.91 13.64 1 1 -10 522.12 13.04 1 1 10 507.3 13.61 1 -1 -10 536.93 13.08 -1 1 -10 515.99 13.58 1 -1 -10 519.89 13.92 1 1 -11 221.25 7.09 -1 -1 -11 217.17 7.4 1 1 -11 214.91 7.84 1 -1 11 208.54 7.4 -1 -1 -11 201.55 7.86 -1 1 -11 209.45 7.93 1 -1 -11 215.79 7.07 -1 1 -11 213.91 7.44 1 -1 -11 218.07 7.66 1 1 11 232.43 7.48 1 1 -12 8.54 2.54 -1 -1 -12 13.34 3.12 -1 -1 -12 15.21 2.63 1 -1 -12 10.09 2.51 1 -1 -12 13.84 2.77 1 -1 12 17.57 3.02 1 1 12 18.2 2.68 -1 1 -12 9.23 3.23 -1 1 -12 12.24 2.5 -1 -1 -13 1.21 2.29 -1 1 -13 1.21 3.3 1 -1 -13 1 2.42 1 -1 13 3.63 2.68 -1 1 -13 4.46 2.47 1 1 -13 2.5 2.54 -1 -1 -13 0.89 3.26 1 1 -14 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13.42 -1 -3 -7 552.01 13.48 1 3 -7 572.66 13.67 1 3 7 565.32 13.82 1 3 -7 567.3 13.19 1 3 -8 202.93 6.03 1 3 8 215.98 6.16 -1 3 -8 216.15 6.76 1 3 8 214.05 6.47 1 3 -8 215.18 5.93 1 3 8 215.78 6.54 1 -3 -8 216.59 6.68 1 3 -8 208.51 6.25 -1 -3 -8 216.16 7.35 1 3 8 212.3 6.87 -1 -3 8 210.59 5.74 -1 -3 -8 210.2 5.86 -1 -3 -8 208.36 6.65 1 -3 8 212.95 7.07 -1 -3 -9 336.27 8.54 1 -3 9 337.46 10.1 1 -3 -9 343.54 9.73 -1 -3 -9 345.35 9.77 1 3 9 325.46 9.8 -1 -3 -9 350.05 10.5 1 3 9 332.45 9.58 -1 3 -9 349.17 9.86 -1 -3 9 335.03 8.35 1 3 -9 334.44 8.93 -1 -3 -10 222.53 6.07 -1 -3 -10 237.52 7.65 1 -3 -10 236.29 7.61 1 3 -10 231.12 6.86 -1 3 -10 234.7 7.72 1 -3 10 232.55 7.95 -1 -3 -10 239.74 8.29 1 3 10 230.36 7.46 1 -3 -10 238.91 7.29 1 3 11 469.29 13.12 1 -3 -11 463.47 13.24 -1 3 -11 484.23 13.44 -1 -3 -11 472.53 13.96 1 -3 -11 473.81 12.81 1 -3 11 461.27 13.43 -1 -3 -11 496.9 13.35 1 -3 -12 110.26 4.93 -1 3 -12 104.18 5.02 -1 -3 -12 100.61 4.93 -1 -3 -12 96.9 5.6 1 -3 -12 101.91 4.94 1 -3 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579.01 13.55 4 2 -3 583.09 13.2 -4 2 -3 580.28 13.2 4 2 3 587.3 16.38 4 2 -3 587.64 16.4 4 2 3 587.52 16.41 4 2 4 12.42 2.89 -4 -2 -4 12.58 1.64 -4 2 -4 13.34 1.36 4 2 4 12.26 1.55 4 2 4 8.11 2.33 4 -2 4 11.53 1.27 4 2 -4 12.33 2.37 -4 -2 -5 45.71 2.71 -4 -2 -5 52.05 2.64 -4 2 -5 49 2.19 4 2 5 50.55 2.66 4 -2 5 46.39 2.19 4 2 5 45.06 3.62 4 2 -5 40.17 3.44 4 2 5 46.73 4.1 -4 2 -6 115.5 3.61 -4 -2 -6 111.03 4.39 -4 -2 -6 115.04 4.26 -4 2 -6 119.97 3.91 4 2 6 116.65 4.33 4 -2 6 116.8 3.95 4 2 6 111.77 5.52 4 2 -6 107.49 5.49 4 2 6 121.2 6.19 4 -2 6 119.44 5.2 4 -2 -6 116.94 5.26 4 -2 6 100.68 6.16 4 2 7 21.25 3.54 4 -2 7 19.42 3.75 -4 -2 -7 16.48 2.13 4 -2 -7 17.75 2.46 4 -2 7 16.85 2.46 4 2 7 15.3 2.78 4 2 -7 13.12 2.44 -4 -2 -7 20.02 2.09 -4 2 -7 16.52 1.76 4 2 7 16.59 2.03 4 -2 7 19.25 1.88 4 2 8 39.15 4.22 -4 -2 -8 34.91 2.63 -4 -2 -8 34.87 2.61 -4 2 -8 35.83 2.4 4 2 8 28.95 3.21 4 2 8 34.59 2.71 4 2 -8 36.96 3.33 4 -2 8 32.25 2.41 4 -2 8 39.1 3.2 4 -2 -8 32.69 3.09 4 -2 8 33.89 4.34 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5 9 92.75 5.64 5 5 -9 84.99 5.69 5 5 9 87.04 4.58 5 5 9 85.27 6.31 -5 -5 -10 167.64 6.34 5 5 10 145.44 7.24 5 5 10 157.31 8.19 5 -5 10 157.5 8.95 5 -5 11 27.3 5.54 -5 -5 -11 33.48 3.52 5 5 11 34.57 5.28 5 -5 12 36.19 5.72 -5 -5 -12 26.39 3.53 5 5 12 33.64 5.21 5 -5 13 6.39 4.84 -5 -5 -13 9.02 3.29 5 5 13 7.79 4.65 -5 -5 -14 124.72 6.2 5 5 14 125.72 7.68 5 -5 14 124.07 8.51 -5 -5 -15 45.61 4.64 5 5 15 66.58 6.48 5 -5 15 44.81 6.6 -5 -5 -16 70.17 5.44 5 5 16 84.98 7.05 5 -5 16 81.33 7.73 5 5 17 8.05 5.43 5 -5 17 -2.54 6.67 5 5 18 56.31 6.74 5 7 0 -1.94 2.32 -5 -7 0 2.92 2.54 5 7 0 -2.54 3.13 5 7 0 -1.76 2.16 5 7 0 -0.46 2.82 5 7 0 3.07 2.74 5 7 -1 241.33 7.8 5 7 1 238.66 7.84 5 7 1 247.01 9.4 5 7 -1 230.95 9.34 -5 -7 -1 226.37 7.86 5 7 -1 230.63 7.63 5 7 1 229.73 7.41 5 7 1 242.9 9.62 5 7 -1 240.21 9.62 -5 -7 -1 242 9.1 -5 -7 1 244.51 9.14 5 7 1 227.49 8.71 5 7 -1 255.78 8.32 5 7 -2 140.61 5.69 5 7 2 142.29 5.67 5 7 2 145.22 7.07 5 7 -2 152.7 7.2 -5 -7 -2 147.56 5.88 5 7 -2 142.88 5.7 5 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5 7 7 403.28 13.66 5 7 -7 423.08 13.78 5 7 7 434.41 12.04 5 7 7 409.01 13.71 -5 -7 -7 413.93 13.15 -5 -7 7 450.63 13.2 -5 -7 -8 7.11 3.18 -5 -7 8 7.77 2.76 5 7 8 7.06 3.18 5 7 -8 10.33 3.57 -5 -7 -8 8.04 2.59 -5 -7 -8 5.08 2.72 5 7 8 8.92 3.24 5 7 -8 10.44 3.61 5 7 8 6.09 2.62 5 7 8 11.86 3.98 5 -7 9 28.81 5.59 -5 -7 -9 32.32 3.84 5 7 9 42.53 4.29 5 7 -9 37.22 4.36 -5 -7 -9 38.32 3.77 5 7 9 37.95 4.76 5 -7 10 53.39 6.38 -5 -7 -10 63.4 4.28 5 7 10 70.49 5.61 -5 -7 -11 112.59 5.54 5 7 11 124.74 7 5 -7 11 99.6 7.89 5 -7 12 3.8 5.08 -5 -7 -12 2.78 3.17 5 7 12 2.92 4.16 5 -7 13 4.13 5.13 -5 -7 -13 6.55 3.34 5 7 13 6.5 4.54 5 -7 14 6.98 5.33 -5 -7 -14 9.46 3.49 5 7 14 11.72 4.88 -5 -7 -15 129.09 6.59 5 7 15 135.45 7.97 5 -7 15 120.51 8.72 -5 -7 -16 15.51 4.34 5 7 16 13.53 5.3 5 -7 16 10.97 5.64 -5 -7 -17 2.55 4.02 -5 -7 -18 16.98 4.52 5 9 0 -0.25 2.53 5 9 0 5.11 3.18 -5 -9 0 1.96 2.63 5 9 0 -0.24 3.18 5 9 0 -1.47 2.42 5 9 0 3.62 2.6 5 9 -1 17 2.93 5 9 1 18.24 2.96 5 9 1 21.05 3.58 5 9 -1 27.8 3.83 -5 -9 -1 22.88 3.52 -5 -9 1 15.91 3.41 -5 -9 -1 18.79 3.18 5 9 1 25.1 3.96 5 9 -1 22.21 3.81 5 9 -1 16.85 2.82 5 9 1 18.94 2.69 5 9 1 20.03 3.11 5 9 -2 542.83 14.95 5 9 2 557.65 16.6 5 9 -2 554.23 16.59 5 9 2 553.57 15.13 -5 -9 -2 554.34 15.37 5 9 -2 563.79 15.02 5 9 2 548.35 17.11 5 9 -2 539.56 17 5 9 2 553.35 14.63 -5 -9 -2 575.64 16.89 -5 -9 2 558.06 16.77 5 9 2 554.56 15.42 5 9 -3 57.79 3.83 5 9 3 56.87 4.67 -5 -9 -3 53.93 4.17 5 9 -3 52.82 3.86 5 9 -3 52.73 4.9 5 9 3 45.14 3.43 5 9 -3 45.4 4.38 5 9 3 49.26 4.85 -5 -9 -3 50.14 4.49 -5 -9 3 54.92 4.68 5 9 3 52.42 4.19 5 9 4 13.26 3.38 5 9 -4 13.49 3.34 5 9 -4 11.26 3.4 5 9 4 10.64 3.45 -5 -9 -4 8.96 3.03 5 9 -4 8.75 2.84 -5 -9 -4 10.85 3.22 -5 -9 4 12.12 3.12 5 9 4 8.74 2.51 5 9 4 9.7 3.47 5 9 5 6.2 3.25 5 9 -5 1.61 3.06 5 9 -5 0.71 2.93 5 9 5 3.8 2.97 5 9 -5 2.66 2.69 -5 -9 -5 0.15 2.88 -5 -9 -5 0.42 2.64 5 9 5 -0.59 2.59 -5 -9 5 5.65 3.02 5 9 5 4.75 3.16 -5 -9 -6 497.36 14.62 5 9 6 487.39 15.26 5 9 -6 496.74 15.4 5 9 -6 491.16 15.88 5 9 6 499.55 16 -5 -9 -6 495.75 14.3 5 9 6 496.34 13.85 -5 -9 -6 525.4 15.58 -5 -9 6 528.09 15.64 5 9 6 508.85 15.01 5 9 -7 49.94 4.45 -5 -9 -7 40.09 4.31 -5 -9 7 46.64 4.23 5 9 7 44.84 4.41 5 9 -7 37.7 4.53 5 9 7 45.34 4.91 -5 -9 -7 37.94 3.87 5 9 7 44.39 4.44 -5 -9 -8 10.01 3.56 5 9 -8 16.11 3.86 5 9 8 13.78 3.8 -5 -9 -8 11.02 3.11 5 9 8 12.52 3.88 -5 -9 -9 16.25 3.62 5 9 -9 16.78 4.25 5 9 9 10.74 3.6 -5 -9 -9 18.1 3.45 5 9 9 15.66 4.01 -5 -9 -10 115.88 6.17 -5 -9 -10 125.83 6.08 5 9 10 144.49 7.42 5 -9 10 111.87 8.22 5 -9 11 12.71 5.69 -5 -9 -11 17.33 3.65 5 9 11 15.65 4.31 5 -9 12 6.97 5.6 -5 -9 -12 15.94 3.53 5 9 12 20.89 4.62 5 -9 13 0.67 5.76 -5 -9 -13 2.12 3.47 5 9 13 10.71 4.75 5 -9 14 70.3 7.64 -5 -9 -14 81.17 5.45 5 -9 15 7.62 6.02 -5 -9 -15 15.36 4.12 -5 -9 -16 34.29 4.78 -5 -9 -17 5.58 4.09 -5 -9 -18 23.87 4.78 5 11 0 -0.81 2.81 5 11 0 6.46 3.57 5 11 1 90.21 4.99 5 11 -1 83.35 6.17 5 11 1 98.18 6.45 -5 -11 -1 86.62 5.18 5 11 1 100.41 4.88 5 11 -2 6.19 3.51 5 11 2 4.42 3.82 -5 -11 -2 8.34 3.15 5 11 2 8.39 3.06 5 11 -3 173.1 8.77 5 11 3 167.47 8.66 -5 -11 -3 169.01 7.24 5 11 3 191.17 7.23 -5 -11 -4 9.97 4.46 5 11 -4 15.73 4.23 5 11 4 12 4.26 -5 -11 -4 13.17 3.35 5 11 4 23.5 3.42 5 11 -5 95.23 6.59 5 11 5 103.26 6.73 -5 -11 -5 98.23 5.46 5 11 5 105.15 5.7 -5 -11 -5 90.96 7.12 -5 -11 -6 5.06 3.58 5 11 -6 5.45 4.06 5 11 6 6.3 4.08 -5 -11 -6 6.23 3.2 5 11 6 9.07 3.56 -5 -11 -7 194.46 8.19 5 11 -7 214.91 9.45 5 11 7 199.19 9.39 -5 -11 -7 187.35 7.72 5 11 7 195.33 8.22 -5 -11 -8 0.9 3.53 5 11 -8 -0.26 3.93 5 11 8 2.39 3.65 -5 -11 -8 1.78 3.23 5 11 8 7.84 4.07 -5 -11 -9 53.4 4.88 5 11 -9 44.71 5.5 5 11 9 45.31 5.4 -5 -11 -9 43.89 4.35 5 11 9 44.54 4.87 -5 -11 -10 15.13 3.9 -5 -11 -10 9.6 3.56 5 -11 11 86.88 8.19 -5 -11 -11 102.9 6.2 -5 -11 -11 117.3 6.13 5 -11 12 -3.56 6 -5 -11 -12 -1.5 4.12 -5 -11 -12 3.93 3.71 5 -11 13 1.76 6.14 -5 -11 -13 9.3 3.92 5 -11 14 1.05 5.9 -5 -11 -14 10.04 4.18 -5 -11 -15 111.64 6.57 -5 -11 -16 1.33 4.27 -5 -11 -17 4.11 4.35 5 13 0 0.29 4.12 5 13 -1 1.16 4 5 13 1 3.48 4.17 -5 -13 -1 5.36 3.36 5 13 -2 149.38 8.65 5 13 2 161.77 8.82 -5 -13 -2 158.05 7.12 5 13 -3 0.87 4.07 5 13 3 7.02 4.47 -5 -13 -3 4.35 3.28 5 13 -4 15.4 4.56 5 13 4 17.36 4.72 -5 -13 -4 26.53 3.91 5 13 -5 4.09 4.28 5 13 5 3.85 4.23 -5 -13 -5 0.17 3.41 -5 -13 -6 214.95 8.83 5 13 -6 215.19 10.51 5 13 6 231.16 10.56 -5 -13 -6 201.27 8.38 -5 -13 -7 -1.34 3.7 5 13 -7 4.43 4.57 5 13 7 -1.19 4.21 -5 -13 -7 2.62 3.57 5 13 -8 15.89 5.12 -5 -13 -8 17.08 4.35 5 13 8 15.96 4.97 -5 -13 -8 15.05 3.78 5 13 -9 33.02 5.99 5 13 9 34.75 5.67 -5 -13 -9 30.45 4.87 -5 -13 -9 36.63 4.47 -5 -13 -10 127.66 7.16 -5 -13 -10 121.61 6.67 -5 -13 -11 -0.4 4.34 -5 -13 -11 -1.27 3.79 5 -13 12 18.94 6.85 -5 -13 -12 22.67 4.74 -5 -13 -12 26.85 4.67 -5 -13 -13 1.24 4.57 -5 -13 -13 0.57 4.13 -5 -13 -14 65.72 5.69 -5 -13 -15 0.39 4.43 -5 -13 -16 31.15 5.37 5 15 0 4.6 4.72 5 15 -1 115.61 8.13 5 15 1 99.15 7.76 -5 -15 -1 105.07 6.22 5 15 -2 -0.65 4.5 5 15 2 1.98 4.74 -5 -15 -2 3.07 3.75 5 15 -3 196.51 10.24 5 15 3 208.85 10.66 -5 -15 -3 180.63 8.06 5 15 -4 9.53 4.91 5 15 4 9.35 5.1 -5 -15 -4 4.74 3.52 5 15 -5 81.88 7.45 5 15 5 82.02 7.31 -5 -15 -5 72.88 5.44 5 15 -6 0.67 4.97 5 15 6 0.34 4.94 -5 -15 -6 0.19 3.72 5 15 -7 127.07 9.03 5 15 7 135.07 9.19 -5 -15 -7 127.73 7.25 -5 -15 -7 129.57 7.09 5 15 -8 23.37 5.79 5 15 8 19.02 6.16 -5 -15 -8 30.14 5.05 -5 -15 -8 23.16 4.44 5 15 9 42.41 6.68 -5 -15 -9 30.14 5.06 -5 -15 -9 27.68 4.53 -5 -15 -10 6.41 4.45 -5 -15 -10 6.35 4.19 -5 -15 -11 60.82 6.2 -5 -15 -11 68.13 5.76 -5 -15 -12 1.31 4.75 -5 -15 -12 0.59 4.22 -5 -15 -13 3.1 4.89 -5 -15 -13 6.46 4.44 -5 -15 -14 2.92 4.96 -5 -15 -14 -0.82 4.49 5 17 0 -0.75 5.23 5 17 -1 7.87 5.56 5 17 1 5.65 5.08 5 17 -2 214.81 11.56 5 17 2 219.38 11.42 -5 -17 -2 200.07 8.84 5 17 -3 9 5.41 5 17 3 3.05 5.64 -5 -17 -3 2.12 4.04 5 17 -4 6.41 5.52 5 17 4 8.06 5.81 -5 -17 -4 3.09 3.91 -5 -17 -5 4.29 4.14 5 17 -5 3.8 5.56 5 17 5 3.48 5.99 5 17 -6 133.21 9.75 5 17 6 145.84 9.93 -5 -17 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5.77 -5 -19 -12 3.94 5.47 -5 -21 0 -6.59 7.95 -5 -21 -1 0.55 7.42 -5 -21 1 0.55 7.48 -5 -21 -2 24.6 8.09 -5 -21 2 29.52 8.05 -5 -21 -3 9.21 7.73 -5 -21 3 7.59 7.7 -5 -21 -3 6.01 4.75 -5 -21 -4 1.61 7.34 -5 -21 4 -4.3 7.53 -5 -21 -4 2.6 4.74 -5 -21 -5 2.11 7.16 -5 -21 5 -7.99 7.9 -5 -21 -5 -1.95 4.77 -5 -21 -6 27.49 7.78 -5 -21 6 37.51 8.6 -5 -21 -6 38.69 5.6 -5 -21 -7 7.95 5.01 -5 -21 -8 0.9 5.04 -5 -21 -9 7.9 5.66 -5 -23 0 2.92 8.07 -5 -23 -1 15.73 8.55 -5 -23 1 24.97 8.54 -5 -23 -2 4.07 7.83 -5 -23 2 1.73 8.04 -5 -23 -3 19.7 8.6 -5 -23 3 17.78 8.21 -5 -23 -4 2.87 7.96 -5 -23 4 0.57 8.13 -5 -23 -4 2.48 5.01 -5 -23 -5 11.88 8.41 -5 -23 5 14.67 7.81 -5 -23 -6 3.89 7.9 -5 -23 6 -6.13 8.34 6 0 0 207.73 9.13 6 0 1 -0.25 3 6 0 -1 1.01 2.99 6 0 2 69.26 5.35 6 0 -2 74.06 5.5 6 0 3 -4.21 4.43 6 0 3 -3 3.17 6 0 -3 -2.53 3.05 6 0 4 1302.93 34.12 6 0 -4 1324.88 34.32 6 0 4 1277.31 34.55 6 0 5 1.65 4.42 6 0 5 -0.25 3.09 6 0 -5 -0.25 3.23 6 0 6 15.82 4.74 6 0 6 11.86 3.56 6 0 -6 12.01 3.47 6 0 7 -1.73 4.56 6 0 7 -1.27 3.2 6 0 -7 -1.79 3.38 6 0 8 230.26 9.87 6 0 -8 228.11 9.78 6 0 8 225.26 10.58 6 0 9 3.57 4.77 6 0 9 1.29 3.06 6 0 -9 1.03 3.2 6 0 10 13.89 5.14 6 0 11 5.24 5.08 6 0 12 112.72 8.26 6 0 13 -3.2 5.64 6 0 14 120.33 9.18 6 0 15 -4.83 6 6 0 16 63.68 7.56 6 0 17 2.8 6.49 6 -2 0 7.44 3.1 6 2 0 6.89 3.88 6 2 0 7.08 3.51 6 2 1 142.72 7.72 6 2 -1 127.2 7.45 6 -2 1 127.4 7.21 6 -2 -1 128.68 7.11 6 2 1 132.91 7.33 6 2 2 7.83 3.91 6 2 2 9.21 3.47 6 2 -2 8.49 3.49 6 -2 2 5.29 3.16 6 -2 -2 7.96 3.17 6 2 3 134.3 7.53 6 2 -3 140.59 7.6 6 -2 3 135.88 7.14 6 -2 -3 124.4 6.99 6 2 3 131.54 7.59 6 2 4 9.85 4.37 6 -2 4 15.53 3.6 6 -2 -4 10.24 3.62 6 2 4 10.31 3.62 6 2 -4 8.24 3.58 6 2 5 814.82 23.61 6 2 -5 847.39 23.77 6 -2 5 824.92 22.98 6 -2 -5 779.55 23.01 6 2 5 780.13 23.2 6 -2 5 814.23 24.07 6 2 6 6.36 4.41 6 -2 6 -2.99 4.74 6 -2 6 2.37 2.89 6 -2 -6 3.39 3.05 6 2 6 0.27 3.24 6 2 -6 2.47 3.42 6 2 7 201.1 9.48 6 2 -7 230.53 9.98 6 -2 7 235.51 9.5 6 -2 -7 216.5 9.37 6 2 7 217.09 10.19 6 -2 7 208.33 10.3 6 2 8 3.89 4.33 6 -2 8 1.54 4.48 6 2 8 -0.27 3.53 6 2 -8 0.27 3.46 6 -2 8 1.2 3 6 -2 -8 2.67 3.21 6 2 9 31.96 5.65 6 -2 9 35.35 5.87 6 2 9 37.1 4.98 6 2 -9 35.39 4.65 6 -2 9 34.68 4.24 6 -2 -9 30.88 4.47 6 -2 10 6.92 5.12 6 2 10 14.95 5 6 -2 11 9.87 5.35 6 2 11 1.2 5.4 6 -2 12 9.99 5.33 6 2 12 -0.3 5.46 6 2 13 285.4 12.66 6 -2 13 289.42 12.89 6 2 14 -1.22 5.79 6 -2 14 8.31 5.76 6 2 15 8.73 5.85 6 -2 15 -1.34 6.26 6 2 16 4.48 5.55 6 -2 16 -7.66 6.88 6 2 17 54.31 7.03 6 -2 17 50.95 7.67 6 4 0 26.38 4.18 6 4 0 18.28 4.24 6 4 1 0.63 3.48 6 4 -1 3.1 3.25 6 4 1 -2.8 3.58 6 4 -1 -2.82 3.98 -6 -4 -2 65.93 4.05 6 4 2 70.58 5.8 6 4 -2 75.93 6.11 6 4 2 68.56 5.43 6 4 -2 65.67 5.02 6 4 3 29.17 4.59 6 4 3 28.27 4.64 6 4 -3 20.65 4.21 -6 -4 -3 23.42 3.19 -6 -4 -4 689.07 18.21 6 4 4 707.56 21.22 6 4 -4 718.65 21.3 6 4 4 690.17 20.52 6 -4 4 712.33 20.42 6 4 5 16.73 4.34 6 -4 -5 15.21 3.4 6 4 5 15 3.97 6 4 -5 12.71 3.89 -6 -4 -5 13.56 3.03 6 -4 5 16.06 3.57 6 4 6 15.53 4.6 6 -4 6 13.21 3.37 6 4 6 8.18 3.71 6 4 -6 9.82 3.71 6 -4 -6 8.92 3.28 6 -4 7 -5.1 4.97 6 4 7 -2.07 3.32 6 4 -7 0.52 3.6 6 -4 7 7.88 3.22 6 -4 -7 -1.84 2.66 6 4 7 8.26 4.31 6 4 8 170.29 8.52 6 4 -8 201.47 8.91 6 -4 8 166.65 8.43 6 -4 -8 168.78 8.43 6 4 8 202.99 9.61 6 -4 8 179.13 9.9 6 -4 9 2.6 4.9 6 4 9 7.55 3.66 6 4 -9 3.53 3.65 6 -4 9 8.51 3.3 6 -4 -9 9.09 3.34 6 4 9 1.37 4.98 6 -4 10 1.32 5.07 6 4 10 1.13 5.09 6 -4 11 5.32 5.14 6 4 11 4.54 5.06 6 4 12 121.5 8.36 6 -4 12 109.72 8.48 6 -4 13 15.11 5.98 6 4 13 12.53 5.72 6 4 14 114.02 8.38 6 -4 14 111.6 8.64 6 4 15 4.26 5.54 6 -4 15 6.45 6.03 6 4 16 113.17 8.46 6 -4 16 107.68 9.07 6 4 17 5.61 5.55 6 -4 17 -0.34 6.64 6 6 0 30.73 4 6 6 0 23.91 4.15 6 6 -1 121.57 5.31 6 6 1 115.98 7.13 6 6 -1 124.48 7.29 6 6 1 130.14 6.7 6 6 2 4.87 3.42 6 6 2 0.54 3.46 6 6 -2 1.9 3.31 6 6 -2 6.27 2.73 -6 -6 -2 3.64 2.81 6 6 -2 2.02 2.59 -6 -6 -3 92.92 5.09 6 6 -3 94.8 4.98 6 6 3 95.44 6.43 6 6 -3 92.7 6.5 6 6 3 101.75 6.16 6 6 4 33.75 4.66 6 6 -4 44.69 5.08 -6 -6 -4 41.73 3.82 6 6 -4 39.91 3.85 6 6 4 41.24 4.87 6 6 -5 521.58 14.3 -6 -6 -5 492.28 14.33 6 6 5 512.74 16.54 6 6 -5 502.4 16.58 6 6 5 495.93 16.29 -6 -6 -6 47.75 4.14 6 6 6 40.73 4.88 6 6 -6 47.19 5.19 6 6 6 41.51 5.5 -6 -6 -7 216.56 8.06 6 6 7 218.96 9.54 6 6 -7 210.79 9.59 6 6 7 201.81 9.76 6 -6 8 -5.07 5.09 -6 -6 -8 4.82 3.23 6 6 8 5.63 3.69 6 6 -8 1.54 3.33 6 6 8 5.77 4.75 6 -6 9 26.12 6.17 -6 -6 -9 32.77 3.88 6 -6 9 32.12 4.4 6 6 9 27.34 4.48 6 6 -9 40.13 4.97 6 6 9 35.3 5.9 6 -6 10 6.2 5.29 6 6 10 9.28 4.88 6 -6 11 7.28 5.63 6 6 11 5.98 4.7 6 -6 12 33.82 6.7 6 6 12 40.8 5.72 6 6 13 192.69 9.69 6 -6 13 174.4 10.55 6 -6 14 16.43 6.17 6 6 14 27.05 5.81 6 -6 15 21.34 6.58 6 6 15 11.77 5.52 6 6 16 7.94 5.56 6 -6 16 4.9 6.05 6 -6 17 51.36 7.86 6 8 0 161.13 6.46 6 8 0 152.94 6.1 6 8 0 155.63 8.3 6 8 -1 36.59 3.7 6 8 -1 29.62 3.33 6 8 1 28.16 3.08 6 8 1 33.17 4.58 6 8 -1 33.49 4.76 6 8 1 23.59 4.33 6 8 -2 48.26 3.86 6 8 2 41.21 3.31 -6 -8 -2 46.6 4.29 6 8 -2 42.8 3.78 6 8 2 33.7 4.71 6 8 -2 45.67 5.16 6 8 2 39.76 4.85 -6 -8 -3 64.66 4.71 6 8 3 68.27 5.65 6 8 -3 65.18 5.76 6 8 3 59.07 3.77 6 8 3 64.77 5.48 -6 -8 -4 595.34 16.63 6 8 4 571.23 18.5 6 8 -4 595.63 18.67 6 8 4 608.15 17.76 -6 -8 -5 54.41 4.61 6 8 5 58.63 5.49 6 8 -5 57.59 5.51 6 8 5 58.22 5.68 -6 -8 -6 -2.24 3.31 6 8 6 3.16 3.46 6 8 -6 7.6 3.81 6 8 6 -0.65 4.24 -6 -8 -7 3.52 3.45 6 8 7 4.97 3.61 6 8 -7 4.19 3.65 6 8 7 -1.76 4.13 -6 -8 -8 154.1 6.94 6 8 8 167.01 8.39 6 8 -8 154.57 8.27 6 8 8 150.04 8.18 6 8 9 32.75 4.76 6 8 -9 30.63 4.84 -6 -8 -9 29.01 4.09 6 8 9 37.69 5.38 6 -8 10 1.09 5.92 -6 -8 -10 5.99 3.32 6 8 10 5.4 4.64 6 -8 11 2.55 5.93 -6 -8 -11 8.73 3.81 6 8 11 21.35 5.15 6 -8 12 53.06 7.45 -6 -8 -12 41.34 4.59 6 8 12 57.98 6.2 6 -8 13 20.09 6.89 -6 -8 -13 21.78 4.27 6 8 13 27.59 5.5 6 -8 14 50.64 7.69 6 8 14 53.27 6.57 6 -8 15 14.86 6.7 6 8 15 6.85 5.61 6 -8 16 65.09 8.16 6 8 16 64.81 7 6 10 0 102.48 6.78 6 10 1 108.9 7.07 6 10 -1 101.56 6.95 -6 -10 -2 11.67 3.73 6 10 2 14.62 4.27 6 10 -2 13.76 4.25 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7.52 6 18 4 47.12 7.77 -6 -18 -4 60.16 6.12 6 18 -5 27.14 7.06 6 18 5 18.28 6.8 -6 -18 -5 24.43 5.27 6 18 6 -2.51 6.33 -6 -18 -6 4.14 4.94 6 18 -6 5.41 6.52 -6 -18 -7 16.38 4.98 6 18 -7 13.46 6.72 6 18 7 10.56 7.1 -6 -18 -8 28.62 5.65 6 18 -8 33.79 7.53 6 18 8 30.72 7.56 -6 -18 -9 2.96 5.09 -6 -18 -11 5.74 5.6 6 20 0 2.31 6.98 6 20 -1 21.66 7.45 6 20 1 19.44 7.59 6 20 -2 -0.92 6.94 6 20 2 4.64 7.03 6 20 -3 14.28 7.5 6 20 3 9.32 7.05 -6 -20 -4 17.08 5.39 6 20 -4 12.42 7.24 6 20 4 11.19 7.35 -6 -20 -5 29.72 5.72 6 20 -5 22.56 8.01 6 20 5 19.12 7.84 -6 -20 -6 9.57 5.31 7 1 0 -4.77 4.71 7 -1 0 -3.84 3.59 7 1 0 -0.94 3.67 7 1 1 103.46 7.13 7 1 -1 97.9 7.16 7 -1 1 84.97 6.63 7 -1 -1 95.45 6.77 7 1 1 88.87 7.05 7 1 2 258.41 11.35 7 1 -2 259.02 11.33 7 -1 2 250.55 10.95 7 -1 -2 259.23 11.14 7 1 2 250.99 11.18 7 -1 3 85.22 7.22 7 1 3 92.86 6.8 7 1 -3 104.5 7.22 7 -1 3 81.92 6.5 7 -1 -3 81.87 6.52 7 1 3 81.06 6.89 7 1 4 0.88 4.52 7 -1 4 -6.27 5.16 7 -1 4 7.33 3.8 7 -1 -4 0.3 3.58 7 1 4 -2.48 3.89 7 1 -4 0.95 3.78 7 1 5 38.36 5.74 7 -1 5 39.73 6.11 7 -1 5 34.3 4.8 7 -1 -5 29.6 4.68 7 1 5 35.37 4.94 7 1 -5 38.29 5.27 7 1 6 99.02 7.21 7 1 -6 101.73 7.42 7 -1 6 97.8 6.96 7 -1 -6 104.42 7.2 7 1 6 89.6 7.52 7 -1 6 109 8.38 7 1 7 58.18 6.48 7 -1 7 54.93 6.79 7 -1 7 45.31 5.32 7 -1 -7 48.05 5.51 7 1 7 48.48 5.62 7 1 -7 50.98 5.87 7 1 8 5.44 5.14 7 -1 8 6.39 5.48 7 -1 8 3.84 3.98 7 -1 -8 3.31 3.99 7 1 8 6.58 4.1 7 1 -8 7.6 4.21 7 1 9 9.1 5.54 7 -1 9 1.69 5.16 7 1 9 8.65 4.32 7 1 -9 9.39 4.56 7 -1 9 10.12 4.05 7 -1 -9 13.28 4.53 7 1 10 104.15 8.35 7 -1 10 102.96 8.42 7 1 11 120.26 8.75 7 -1 11 113.67 8.97 7 -1 12 33.35 7.02 7 1 12 32.28 6.89 7 1 13 -10.69 7 7 -1 13 13.49 6.08 7 1 14 15.64 6.89 7 -1 14 30.69 7.14 7 1 15 11.01 6.67 7 -1 15 12.91 7.36 7 3 0 -1.95 4.42 7 3 0 1.98 4.21 7 -3 0 0.58 3.63 7 3 1 122.89 8.13 7 3 -1 119.29 7.87 7 -3 1 125.37 7.69 7 -3 -1 132.28 7.96 7 3 1 120.75 7.58 7 3 2 103.27 7.66 7 3 -2 104.78 7.52 7 -3 2 121.29 7.33 7 -3 -2 117.95 7.47 7 3 2 106.88 7.44 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44.63 5.59 7 -5 1 36.3 4.94 7 -5 -1 56.98 5.48 7 5 2 217.94 10.33 7 5 -2 216.41 10.45 7 5 2 219.57 9.59 7 -5 2 206.12 9.85 7 -5 -2 170.54 9.61 7 5 3 33.24 5.12 7 5 3 28.72 5.11 7 5 -3 27.18 5.1 7 -5 3 20.11 4.63 7 -5 -3 35.3 4.72 7 5 4 11.39 4.74 7 -5 4 2.27 3.51 7 5 4 6.17 4.26 7 5 -4 3.13 3.97 7 -5 -4 5.28 3.71 7 5 5 23.21 4.7 7 5 -5 34.64 5.39 7 -5 5 39.34 5.13 7 -5 -5 22.48 4.56 7 5 5 32.09 5.33 7 5 6 85.4 6.87 7 5 -6 112.39 7.41 7 -5 6 86.54 6.69 7 -5 -6 79.35 6.67 7 5 6 99.85 7.26 7 5 7 17.71 4.74 7 5 -7 29.56 4.94 7 -5 7 10.86 5.61 7 -5 7 17.17 4.47 7 -5 -7 18.15 4.46 7 5 7 28.98 5.69 7 5 -8 20.8 4.81 7 -5 8 13.61 5.89 7 -5 8 27.53 4.83 7 -5 -8 19.13 4.39 7 5 8 16.3 4.63 7 5 8 11.74 5.6 7 -5 9 -4.05 6.07 7 -5 9 1.97 3.8 7 -5 -9 5.72 4.15 7 5 9 -0.29 4.09 7 5 9 -8.09 5.8 7 5 10 128.77 8.94 7 -5 10 138.99 10.12 7 -5 11 41.28 7.37 7 5 11 32.47 6.77 7 -5 12 38.36 7.11 7 5 12 32.43 6.55 7 -5 13 19.17 7.03 7 5 13 9.68 6.21 7 -5 14 41.3 7.54 7 5 14 41.5 6.87 7 -5 15 19.64 6.81 7 7 0 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4.74 7 9 7 8.3 4.98 7 9 8 7.29 4.58 7 9 -8 14.93 5.01 7 9 8 11.16 5.23 7 -9 9 -4.49 6.99 7 9 9 2.42 4.38 7 9 9 -0.25 5.01 7 -9 10 84.06 8.97 7 9 10 113.04 7.6 7 -9 11 3.7 6.81 7 9 11 26.7 5.79 7 -9 12 13.52 6.93 7 9 12 31.6 6.23 7 -9 13 11.09 7.27 7 9 13 19.29 5.92 7 -9 14 43.7 8.23 7 11 0 3.95 4.63 7 11 -1 87.41 7.19 7 11 1 99.78 7.43 7 11 -2 3.29 4.3 7 11 2 8.55 4.64 -7 -11 -3 75.97 5.83 7 11 3 83.4 6.97 7 11 -3 78.04 7.06 7 11 -4 1.31 4.29 -7 -11 -4 2.87 4.18 7 11 4 5.54 4.57 7 11 -5 36.26 5.67 7 11 5 34.95 5.52 -7 -11 -5 37.47 5.11 7 11 -6 6.78 4.63 7 11 6 6.45 4.87 -7 -11 -6 10.27 4.32 7 11 6 9.23 4.59 -7 -11 -7 79.97 6.15 7 11 -7 75.38 7.22 7 11 7 71.32 6.69 7 11 7 89.21 6.7 7 11 -8 2.58 5.02 7 11 8 4.16 4.9 -7 -11 -8 6.37 4.57 7 11 8 13.79 4.92 7 11 9 10.25 5.52 7 11 9 21.04 5.54 7 -11 10 -2.17 7.09 7 11 10 17.82 5.56 7 -11 11 76.85 9.2 7 11 11 83.39 7.22 7 -11 12 -3.04 7.44 7 11 12 8.72 5.37 7 -11 13 3.44 7.67 7 13 0 -3.13 5.02 7 13 -1 1.74 4.88 7 13 1 5.91 5.06 7 13 -2 127.91 8.87 7 13 2 103.68 8.44 7 13 -3 -0.35 4.79 7 13 3 -0.35 4.88 7 13 -4 2.41 4.95 7 13 4 2.07 5.22 -7 -13 -4 8.52 4.57 7 13 -5 0.34 5.21 7 13 5 5.86 4.97 -7 -13 -5 11.21 4.8 -7 -13 -6 72.74 6.19 7 13 -6 75.03 7.65 7 13 6 69.87 7.43 7 13 -7 -0.34 5.4 7 13 7 3.78 5.3 -7 -13 -7 -0.21 4.44 7 13 -8 8.65 5.99 7 13 8 14.43 5.78 -7 -13 -8 17.23 5.16 7 13 8 28.85 5.51 -7 -13 -9 -1.5 4.76 -7 -13 -10 76.8 6.62 7 -13 11 -11.55 8.06 -7 -13 -11 0.65 4.87 7 15 0 0.37 5.55 7 15 -1 56.71 7.19 7 15 1 54.12 7.34 7 15 -2 2.61 5.55 7 15 2 4.11 5.51 7 15 -3 53.3 7.25 7 15 3 50.41 7.24 7 15 -4 9.7 5.87 7 15 4 7.1 5.87 -7 -15 -4 4.06 4.67 7 15 -5 22.03 6.3 7 15 5 30.67 6.55 -7 -15 -5 29.77 5.4 7 15 -6 -3.73 6.02 7 15 6 1.49 5.6 -7 -15 -6 3.67 4.76 7 15 -7 56.74 7.63 7 15 7 61.97 7.61 -7 -15 -7 57.51 6.24 7 15 -8 10.15 6.1 7 15 8 3.36 5.98 -7 -15 -8 -2.87 4.79 -7 -15 -9 9.62 5.21 -7 -15 -10 1.82 5.16 7 17 0 2.43 5.96 7 17 -1 13.37 6.59 7 17 1 -0.81 6.07 7 17 -2 85.85 8.6 7 17 2 85.61 8.71 7 17 -3 2.43 6.32 7 17 3 7.71 6.59 7 17 -4 5.26 6.37 7 17 4 1.22 6.04 -7 -17 -4 8.07 5.19 7 17 -5 -0.41 6.46 7 17 5 0.81 6.1 -7 -17 -5 5.67 5.23 7 17 -6 46 7.75 7 17 6 39.92 7.75 -7 -17 -6 44.73 6.08 7 17 -7 8.19 7.01 7 17 7 5.3 6.69 -7 -17 -7 6.39 5.39 7 17 8 1.23 6.51 -7 -17 -8 4.87 5.25 8 0 0 479.36 17.4 8 0 0 456.1 16.74 8 0 -1 -2.86 4.69 8 0 1 -0.31 5.63 8 0 1 0.36 4.56 8 0 2 8.35 5.18 8 0 2 6.4 4.48 8 0 -2 5.38 4.57 8 0 3 1.95 5.5 8 0 3 3.19 4.48 8 0 -3 -2.52 4.66 8 0 4 74.31 7.59 8 0 4 76.05 6.81 8 0 -4 70.76 6.84 8 0 5 2.04 5.86 8 0 5 -5.3 4.72 8 0 -5 -4.34 4.91 8 0 6 10.38 5.84 8 0 6 8.83 4.78 8 0 -6 19.86 5.32 8 0 7 3.86 6.02 8 0 7 2.12 4.59 8 0 -7 -2.53 4.92 8 0 8 158.41 9.69 8 0 -8 167.88 10.08 8 0 8 178.02 10.66 8 0 9 2.9 5.69 8 0 10 38.74 7.14 8 0 11 5.55 6.5 8 0 12 93.36 9.12 8 -2 0 4.17 4.33 8 2 0 0.38 4.64 8 2 1 153.69 9.51 8 2 -1 145.3 9.45 8 -2 1 165.61 9.38 8 -2 -1 159.12 9.42 8 2 2 -0.3 5.19 8 -2 2 -3.8 4.38 8 -2 -2 -1.39 4.23 8 2 2 -0.74 4.61 8 2 -2 1.13 4.66 8 -2 3 86.31 8.21 8 2 3 86.37 7.64 8 2 -3 91.77 7.74 8 -2 3 99.21 7.48 8 -2 -3 88.6 7.4 8 2 3 104.01 8.12 8 2 4 1.57 5.59 8 -2 4 -6.72 5.88 8 -2 4 0.34 4.04 8 -2 -4 0.35 4.34 8 2 4 -5.11 4.59 8 2 -4 -2.99 4.83 8 2 5 34.16 6.3 8 -2 5 20.38 6.27 8 -2 5 42.86 5.78 8 -2 -5 36.13 5.82 8 2 5 33.07 5.52 8 2 -5 29.61 5.6 8 2 6 10.49 5.76 8 -2 6 -7.94 6.18 8 -2 6 1.37 4.29 8 -2 -6 5.22 4.5 8 2 6 -2.84 5.02 8 2 -6 4.73 4.83 8 2 7 8.35 5.96 8 -2 7 3.68 6.08 8 -2 7 8.85 5.03 8 -2 -7 5.91 4.68 8 2 7 2.8 5.12 8 2 -7 5.39 5.24 8 2 8 7.49 5.74 8 -2 8 13.43 6.67 8 -2 8 1.7 4.63 8 -2 -8 2.78 4.73 8 2 8 -1.03 4.96 8 2 -8 -2.46 5.29 8 2 9 213.81 11.52 8 -2 9 218.41 12.17 8 -2 10 4.92 6.5 8 2 10 15.26 6.73 8 -2 11 39.39 7.55 8 2 11 32.99 7.32 8 -2 12 7.29 6.85 8 2 12 -10.55 7.59 8 4 0 366.73 14.86 8 -4 0 344.49 14.46 8 -4 1 6.57 4.39 8 -4 -1 4.82 4.58 8 4 1 6.14 4.86 8 4 -1 4.38 4.73 8 -4 2 4.83 4.12 8 -4 -2 11.66 4.75 8 4 2 2.51 4.87 8 4 -2 6.18 4.94 8 4 3 0.29 4.73 8 -4 3 -3.1 4.24 8 -4 -3 -1.36 4.27 8 4 3 1.07 4.62 8 4 -3 -2.54 4.93 8 4 4 63.34 6.67 8 -4 4 56.19 6.46 8 -4 -4 61.92 6.5 8 4 4 64.93 6.82 8 4 -4 59.28 6.73 8 4 5 13.91 5.72 8 -4 5 3.39 6.46 8 4 5 2.77 4.9 8 4 -5 3.55 4.89 8 -4 5 7.5 4.42 8 -4 -5 0.34 4.32 8 -4 6 7.26 6.35 8 4 6 9.93 4.69 8 4 -6 8.72 5.03 8 -4 6 25.09 5.5 8 -4 -6 4.38 4.37 8 4 6 18.99 6.08 8 -4 7 0.38 6.05 8 4 7 1.01 4.88 8 4 -7 -4.12 5.07 8 -4 7 3.38 4.52 8 -4 -7 1.69 4.46 8 4 7 11.49 5.86 8 4 8 133.98 8.91 8 4 -8 153.41 9.46 8 -4 8 140.41 8.83 8 -4 -8 126.66 8.7 8 4 8 147.87 9.71 8 -4 8 129.17 9.94 8 -4 9 11.38 6.85 8 4 9 2.01 7.18 8 -4 10 30.07 7.37 8 4 10 26.23 7.27 8 -4 11 2.38 6.88 8 4 11 -8.59 7.03 8 4 12 77.88 8.85 8 6 0 11.12 5.1 8 -6 0 10.03 4.82 8 6 1 107.1 8.28 8 6 -1 107 8.21 8 -6 1 118.86 8.22 8 -6 -1 99.34 8.32 8 6 2 0.71 4.48 8 6 -2 -1.43 4.83 8 -6 2 6.71 4.79 8 -6 -2 7.51 4.63 8 6 3 78.87 7.53 8 6 -3 75.3 7.48 8 -6 3 85.92 7.41 8 -6 -3 80.42 7.37 8 -6 4 18.17 5.24 8 -6 -4 7.08 4.72 8 6 4 6.63 4.79 8 6 -4 7.44 5.27 8 -6 5 32.39 5.85 8 -6 -5 22.79 5.5 8 6 5 31.07 5.96 8 6 -5 31.55 5.9 8 6 5 28.55 6.33 8 -6 6 -0.4 6.58 8 -6 6 -0.35 4.57 8 -6 -6 1.34 4.4 8 6 6 6.84 4.71 8 6 -6 3.12 4.92 8 6 6 -6.53 6.45 8 -6 7 2.43 6.53 8 -6 7 14.66 5.36 8 -6 -7 8.38 4.96 8 6 7 8.49 5.04 8 6 -7 7.2 5.09 8 6 7 -0.3 6.41 8 -6 8 0.41 6.5 8 -6 8 13.67 5.21 8 -6 -8 10.59 5 8 6 8 20.53 5.55 8 6 -8 11.51 5.34 8 6 8 7.43 6.14 8 6 9 140.24 9.7 8 -6 9 129.61 10.52 8 -6 10 7.4 6.98 8 6 10 0.63 6.59 8 -6 11 24.39 7.53 8 6 11 25.94 6.9 8 8 0 239.38 11.9 8 8 1 20.08 5.59 8 8 -1 24.49 5.82 8 8 2 9.26 5.02 8 8 -2 6.1 4.96 8 8 3 1.41 4.71 8 8 -3 8.53 5.28 8 -8 4 66.66 7.33 8 8 4 53.44 6.73 8 8 -4 67.34 7.01 8 -8 -5 9.53 4.61 8 -8 5 20.96 5.53 8 8 5 25.73 5.68 8 8 -5 18.37 5.51 8 -8 6 2.88 4.72 8 8 6 13.26 5.25 8 8 -6 4.1 5.04 8 8 6 6.01 5.64 8 -8 -6 11.32 4.63 8 -8 -7 3.78 4.68 8 8 7 10.44 5.27 8 -8 7 13.21 5.49 8 8 -7 17.61 5.67 8 8 7 8.23 5.54 8 -8 8 82.64 9.32 8 8 8 85.22 7.44 8 8 -8 98.67 7.89 8 -8 8 77.29 7.96 8 -8 -8 72.25 7.12 8 8 8 84.66 7.78 8 -8 9 7.77 7.03 8 8 9 18.88 6.18 8 -8 10 3.44 7.01 8 8 10 16.24 6.2 8 8 11 12.08 6.49 8 10 0 31.84 5.99 8 10 1 64.24 7.05 8 10 -1 60.46 6.96 8 10 2 6.1 5.04 8 10 -2 14.79 5.41 8 10 3 50.5 6.4 8 10 -3 52.31 6.87 8 10 4 33.8 6.27 8 10 -4 29.73 6.17 8 10 5 28.95 5.98 8 10 -5 18.12 5.97 8 10 6 3.15 5.19 8 10 -6 1.41 5.15 8 10 -7 13.29 5.8 8 10 7 5.23 5.17 8 10 -8 28.54 6.17 8 10 8 25.36 6.04 8 10 8 28.46 6.01 8 -10 9 75.04 9.8 8 10 9 98.46 7.72 8 10 10 20.69 6.01 8 12 0 85.21 8.19 8 12 -1 19.51 5.85 8 12 1 24.72 5.93 8 12 -2 9.36 5.41 8 12 2 10.07 5.46 8 12 -3 7.09 5.42 8 12 3 4.46 5.15 8 12 -4 43.49 7.26 8 12 4 35.87 6.8 8 12 -5 15.52 5.86 8 12 5 23.91 6.57 8 12 -6 9.18 5.89 8 12 6 9.15 5.67 8 12 -7 12.07 6.38 8 12 7 9.84 5.85 8 12 8 39.5 6.69 8 14 0 31.5 6.68 8 14 -1 26.38 6.62 8 14 1 38.52 6.98 8 14 -2 4.72 5.97 8 14 2 -1.96 5.9 8 14 -3 20 6.67 8 14 3 24.61 6.64 8 14 -4 23.84 6.44 8 14 4 27.26 6.7 8 14 -5 14.03 6.2 8 14 5 11.65 6.54 8 14 -6 -4.26 6.29 8 14 6 9.28 6.3 8 14 -7 5.41 6.71 8 14 7 7.7 6.49 9 1 0 -3.36 5.5 9 -1 0 -2.46 5.03 9 1 1 19.26 5.74 9 1 -1 13.07 5.54 9 -1 1 13.89 5.75 9 -1 -1 10.25 5.48 9 -1 2 41.97 7.45 9 1 2 52.77 7.27 9 1 -2 47.95 6.98 9 -1 2 71.87 7.62 9 -1 -2 52.57 7.05 9 -1 3 22.03 6.85 9 1 3 34.26 6.38 9 1 -3 29.42 6.31 9 -1 3 34.21 6.7 9 -1 -3 33.26 6.39 9 1 4 12.17 6.26 9 -1 4 -2.2 6.63 9 1 4 8.16 5.53 9 1 -4 -1.25 5.43 9 -1 4 4.46 5.34 9 -1 -4 -1.23 5.43 9 1 5 16.56 6.45 9 -1 5 16.81 6.93 9 1 5 12.9 5.67 9 1 -5 15.3 6.2 9 -1 5 18.12 5.73 9 -1 -5 7.78 5.66 9 1 6 77.05 8.26 9 -1 6 62.55 8.17 9 1 6 77.17 7.98 9 1 -6 74.45 7.81 9 -1 6 61.82 7.54 9 -1 -6 67.53 7.8 9 1 7 52.79 7.95 9 -1 7 43.52 7.93 9 1 7 33.15 6.31 9 1 -7 40.96 7.07 9 -1 7 35.1 6.51 9 -1 -7 38.41 6.9 9 1 8 9.59 7.12 9 -1 8 7.32 6.74 9 1 8 -2.29 5.72 9 -1 8 6.35 5.59 9 3 0 -3.23 5.55 9 -3 0 2.84 5.16 9 -3 1 31.69 6.01 9 -3 -1 25.48 6.14 9 3 1 12.47 5.81 9 3 -1 13.78 6.01 9 -3 2 27.03 7.43 9 -3 2 19.5 5.77 9 -3 -2 33.87 6.18 9 3 2 24.7 6.15 9 3 -2 25.04 6.25 9 -3 3 34.69 7.55 9 -3 3 43.79 6.75 9 -3 -3 49.02 6.98 9 3 3 45.44 6.93 9 3 -3 37.92 6.91 9 -3 4 2.75 6.73 9 -3 4 4.85 5.66 9 -3 -4 3.6 5.43 9 3 4 -4.29 5.6 9 3 -4 2.8 5.71 9 3 5 34.64 6.95 9 -3 5 12.94 6.97 9 -3 5 17.65 5.97 9 -3 -5 30.31 6.37 9 3 5 21.2 6.24 9 3 -5 16.62 6.14 9 3 6 46.3 7.56 9 -3 6 37.99 7.98 9 -3 6 38.58 6.81 9 -3 -6 40.85 6.89 9 3 6 38.28 6.85 9 3 -6 36.72 6.73 9 -3 7 39.67 8 9 -3 7 54.89 7.45 9 -3 -7 64.09 7.49 9 3 7 47.84 6.91 9 3 -7 56.75 7.58 9 3 7 66.05 8.19 9 3 8 0.37 5.8 9 -3 8 9.02 5.64 9 3 8 13.17 6.79 9 5 0 -1.58 5.55 9 -5 0 4.47 5.36 9 5 1 5.89 5.7 9 5 -1 11.86 5.67 9 -5 1 17.59 6.04 9 -5 -1 13.3 5.65 9 5 2 65.09 7.53 9 5 -2 56.9 7.49 9 -5 2 65.36 7.61 9 -5 -2 64.65 7.57 9 5 3 11.23 5.82 9 5 -3 14.56 5.95 9 -5 3 8.24 5.57 9 -5 -3 24.51 6.2 9 5 4 4.6 5.57 9 5 -4 6.65 5.53 9 -5 4 -5 7 9 -5 4 4.94 5.54 9 -5 -4 1.57 5.11 9 5 5 -2.28 5.47 9 5 -5 5.43 5.58 9 -5 5 0.42 7.26 9 -5 5 3.28 5.55 9 -5 -5 9.73 5.54 9 -5 6 84.26 9.59 9 -5 6 84.21 8.3 9 -5 -6 93.09 8.38 9 5 6 88.59 8.21 9 5 -6 94.02 8.6 9 -5 7 7.11 7.08 9 -5 7 15.66 6.27 9 -5 -7 10.03 5.68 9 5 7 15.95 5.98 9 5 -7 23.44 6.51 9 5 7 -1 7.01 9 -5 8 -3.17 5.57 9 5 8 4.42 5.42 9 5 8 -0.34 7.3 9 -7 0 13.46 5.85 9 7 0 -3.17 5.5 9 -7 1 27.75 6.49 9 -7 -1 29.78 6.61 9 7 1 22.92 6.28 9 7 -1 30.21 6.48 9 -7 2 23.31 6.76 9 -7 -2 15.02 5.79 9 7 2 12.95 5.79 9 7 -2 17.05 5.98 9 -7 3 57.38 7.75 9 -7 -3 54.26 7.17 9 7 3 58.89 7.51 9 7 -3 52.23 7.35 9 -7 4 -0.43 5.53 9 -7 -4 2.73 5.15 9 7 4 5.01 5.88 9 7 -4 0.78 5.63 9 -7 5 18.48 6.39 9 -7 -5 24.14 6.15 9 7 5 17.14 6.17 9 7 -5 22.87 6.48 9 -7 6 15.64 6.47 9 -7 -6 26.47 6.24 9 7 6 19.84 6.28 9 7 -6 15.21 6.22 9 -7 7 79.44 8.32 9 -7 -7 59.24 7.29 9 7 7 50.39 7.17 9 7 -7 61.81 7.59 9 -7 8 -0.41 5.48 9 -9 0 12.73 5.8 9 9 0 1.18 5.65 9 -9 -1 4 5.31 9 9 1 6.65 5.47 9 9 -1 6.29 5.55 9 -9 1 9.71 5.81 9 9 2 54.05 7.47 9 9 -2 57.62 7.41 9 -9 2 60.87 8.26 9 -9 -2 62.41 7.23 9 -9 3 8.84 6.1 9 9 3 8.13 5.73 9 9 -3 5.09 5.91 9 -9 -3 5.7 5.25 9 -9 4 12.95 6.38 9 -9 -4 10.86 5.55 9 9 -4 3.5 5.71 9 -9 -5 3.7 5.24 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cl1 Bi1 Cl1 94.33(5) 12_655 . ? Cl4 Bi1 Cl4 83.361(14) 14_457 . ? Bi1 Cl4 Bi1 165.03(9) 14_557 . ? H1A C1 H1B 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? C2 C1 H1A 109.5 . . ? C2 C1 H1B 109.5 . . ? C2 C1 H1C 109.5 . . ? H1D N1 H1E 109.5 . . ? H1D N1 H1F 109.5 . . ? H1E N1 H1F 109.5 . . ? C2 N1 H1D 109.5 . . ? C2 N1 H1E 109.5 . . ? C2 N1 H1F 109.5 . . ? C1 C2 N1 118.7(12) . . ? C1 C2 H2A 107.6 . . ? C1 C2 H2B 107.6 . . ? N1 C2 H2A 107.6 . . ? N1 C2 H2B 107.6 . . ? H2A C2 H2B 107.1 . . ? Bi1 Br4 Bi1 165.03(9) 14_557 . ? H2C N2 H2D 109.5 . . ? H2C N2 H2E 109.5 . . ? H2D N2 H2E 109.5 . . ? C4 N2 H2C 109.5 . . ? C4 N2 H2D 109.5 . . ? C4 N2 H2E 109.5 . . ? N2 C4 H4A 109.5 . . ? N2 C4 H4B 109.5 . . ? H4A C4 H4B 108.1 . . ? C3 C4 N2 110.6 . . ? C3 C4 H4A 109.5 . . ? C3 C4 H4B 109.5 . . ? C4 C3 H3A 109.5 . . ? C4 C3 H3B 109.5 . . ? C4 C3 H3C 109.5 . . ? H3A C3 H3B 109.5 . . ? H3A C3 H3C 109.5 . . ? H3B C3 H3C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Bi1 Cl1 2.6930(10) 12_655 ? Bi1 Cl1 2.6930(10) . ? Bi1 Cl3 2.8120(14) . ? Bi1 Cl2 2.7846(14) . ? Bi1 Cl4 2.9200(4) 14_457 ? Bi1 Cl4 2.9200(4) . ? Bi1 Br1 2.6930(10) . ? Bi1 Br3 2.8120(14) . ? Bi1 Br4 2.9200(4) . ? Bi1 Br2 2.7846(14) . ? C1 H1A 0.9600 . ? C1 H1B 0.9600 . ? C1 H1C 0.9600 . ? C1 C2 1.363(17) . ? N1 H1D 0.8900 . ? N1 H1E 0.8900 . ? N1 H1F 0.8900 . ? N1 C2 1.425(14) . ? C2 H2A 0.9700 . ? C2 H2B 0.9700 . ? N2 H2C 0.8900 . ? N2 H2D 0.8900 . ? N2 H2E 0.8900 . ? N2 C4 1.5317 . ? C4 H4A 0.9700 . ? C4 H4B 0.9700 . ? C4 C3 1.5198 . ? C3 H3A 0.9600 . ? C3 H3B 0.9600 . ? C3 H3C 0.9600 . ?