#------------------------------------------------------------------------------ #$Date: 2024-02-04 13:40:19 +0200 (Sun, 04 Feb 2024) $ #$Revision: 289452 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/78/7247809.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7247809 loop_ _publ_author_name 'Pradhan, Abinash' 'Sahoo, Sanand' 'Samal, Saroj L.' _publ_section_title ; (C2H5NH3)2BiCl5−xBrx perovskites containing 1D chains: effect of Br substitution on their structural and optical properties ; _journal_issue 3 _journal_name_full CrystEngComm _journal_page_first 312 _journal_page_last 323 _journal_paper_doi 10.1039/D3CE01019H _journal_volume 26 _journal_year 2024 _chemical_formula_moiety 'Bi2 Cl10, 4(C2 N), [+ solvents]' _chemical_formula_sum 'C4 H16 Bi Cl5 N2' _chemical_formula_weight 478.42 _space_group_crystal_system orthorhombic _space_group_IT_number 41 _space_group_name_Hall 'A 2 -2ab' _space_group_name_H-M_alt 'A e a 2' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2023-06-01 _audit_creation_method ; Olex2 1.5-alpha (compiled 2021.06.29 svn.r12e2184c for OlexSys, GUI svn.r6374) ; _audit_update_record ; 2023-10-09 deposited with the CCDC. 2023-12-01 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 17.5689(7) _cell_length_b 21.6639(9) _cell_length_c 7.4870(3) _cell_measurement_reflns_used 5943 _cell_measurement_temperature 90(2) _cell_measurement_theta_max 26.9960 _cell_measurement_theta_min 1.8420 _cell_volume 2849.6(2) _computing_cell_refinement 'CrysAlisPro 1.171.41.93a (Rigaku OD, 2020)' _computing_data_collection 'CrysAlisPro 1.171.41.93a (Rigaku OD, 2020)' _computing_data_reduction 'CrysAlisPro 1.171.41.93a (Rigaku OD, 2020)' _computing_molecular_graphics 'Olex2 1.5-alpha (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5-alpha (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 90(2) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.974 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 47.00 93.00 0.50 34.50 -- 10.00 5.00 8.00 92 2 \w -32.00 -7.00 0.50 34.50 -- -10.20 -5.00-169.00 50 3 \w 65.00 91.00 0.50 34.50 -- 10.00 77.00 -90.00 52 4 \w -12.00 29.00 0.50 34.50 -- 10.00 77.00 60.00 82 5 \w -13.00 16.00 0.50 34.50 -- -10.20 -82.00 30.00 58 6 \w -99.00 8.00 0.50 34.50 -- -10.20 -82.00 90.00 214 7 \w -82.00 13.00 0.50 34.50 -- -10.20 -57.00 120.00 190 8 \w -81.00 -55.00 0.50 34.50 -- -10.20 -82.00 30.00 52 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Pro II AFC12 (RINC): Kappa single' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0007890000 _diffrn_orient_matrix_UB_12 -0.0316279000 _diffrn_orient_matrix_UB_13 -0.0103393000 _diffrn_orient_matrix_UB_21 0.0059838000 _diffrn_orient_matrix_UB_22 0.0083617000 _diffrn_orient_matrix_UB_23 -0.0389741000 _diffrn_orient_matrix_UB_31 0.0945467000 _diffrn_orient_matrix_UB_32 -0.0007837000 _diffrn_orient_matrix_UB_33 0.0023876000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0369 _diffrn_reflns_av_unetI/netI 0.0345 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.974 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_h_min -21 _diffrn_reflns_limit_k_max 25 _diffrn_reflns_limit_k_min -26 _diffrn_reflns_limit_l_max 5 _diffrn_reflns_limit_l_min -9 _diffrn_reflns_number 9149 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.974 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.863 _diffrn_reflns_theta_min 1.880 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'Rigaku (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 13.275 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.28963 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.93a (Rigaku Oxford Diffraction, 2020) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_density_diffrn 2.230 _exptl_crystal_description crystalline _exptl_crystal_F_000 1776 _exptl_crystal_size_max 0.15 _exptl_crystal_size_mid 0.13 _exptl_crystal_size_min 0.10 _refine_diff_density_max 1.539 _refine_diff_density_min -1.195 _refine_diff_density_rms 0.173 _refine_ls_abs_structure_details ; Refined as a perfect inversion twin. ; _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.021 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 106 _refine_ls_number_reflns 2295 _refine_ls_number_restraints 22 _refine_ls_restrained_S_all 1.026 _refine_ls_R_factor_all 0.0342 _refine_ls_R_factor_gt 0.0272 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0280P)^2^+27.0003P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0598 _refine_ls_wR_factor_ref 0.0621 _reflns_Friedel_coverage 0.852 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.975 _reflns_number_gt 2065 _reflns_number_total 2295 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL ab313_lt_040322_a.res in Aba2 ab313_lt_040322.res created by SHELXL-2018/3 at 15:00:09 on 01-Jun-2023 REM Old TITL AB313_LT_040322 in Cmce REM SHELXT solution in Aba2: R1 0.082, Rweak 0.008, Alpha 0.044 REM 0.696 for 94 systematic absences, Orientation a'=c, b'=-b, c'=a REM Formula found by SHELXT: C1 C2 Cl5 Bi CELL 0.71073 17.5689 21.6639 7.487 90 90 90 ZERR 8 0.0007 0.0009 0.0003 0 0 0 LATT -5 SYMM -X,-Y,+Z SYMM 0.5+X,0.5-Y,+Z SYMM 0.5-X,0.5+Y,+Z SFAC C H Bi Cl N UNIT 32 128 8 40 16 SIMU 0.02 0.04 2 N2 C3 C4 RIGU 0.01 0.01 N2 C3 C4 L.S. 100 PLAN 10 CONF LIST 6 MORE -1 BOND $H fmap 2 acta TWIN -1 0 0 0 -1 0 0 0 -1 2 OMIT 0 4 -2 REM REM REM WGHT 0.028000 27.000299 FVAR 0.11105 BI1 3 0.633217 0.637023 0.635070 11.00000 0.00948 0.02451 = 0.01186 -0.00584 0.00041 0.00082 CL1 4 0.526623 0.621594 0.859450 11.00000 0.01405 0.03562 = 0.01606 -0.00247 0.00261 0.00223 CL2 4 0.549351 0.613952 0.357967 11.00000 0.02272 0.06939 = 0.01054 -0.00938 -0.00158 -0.01787 CL3 4 0.592238 0.755524 0.592486 11.00000 0.01716 0.03068 = 0.01663 -0.00027 -0.00182 0.00547 CL4 4 0.726535 0.662539 0.936204 11.00000 0.02232 0.03802 = 0.01826 -0.00177 -0.01202 -0.00226 CL5 4 0.671159 0.515984 0.665492 11.00000 0.02274 0.02240 = 0.07617 -0.01431 0.01788 0.00061 N1 5 0.594089 0.742472 0.155283 11.00000 0.02056 0.05073 = 0.01510 -0.00085 0.00377 -0.01640 AFIX 33 H1A 2 0.550787 0.729725 0.105833 11.00000 -1.20000 H1B 2 0.630330 0.714547 0.136055 11.00000 -1.20000 H1C 2 0.587417 0.747300 0.272289 11.00000 -1.20000 AFIX 0 C2 1 0.691302 0.824071 0.159651 11.00000 0.02725 0.04087 = 0.03196 -0.00207 0.00143 -0.00477 AFIX 33 H2A 2 0.705617 0.862720 0.106684 11.00000 -1.50000 H2B 2 0.684348 0.829488 0.285861 11.00000 -1.50000 H2C 2 0.730636 0.794158 0.138912 11.00000 -1.50000 AFIX 0 C1 1 0.616689 0.801454 0.075759 11.00000 0.02778 0.03734 = 0.02457 -0.00266 0.00061 0.00880 AFIX 23 H1D 2 0.576996 0.831839 0.095240 11.00000 -1.20000 H1E 2 0.623383 0.796435 -0.052021 11.00000 -1.20000 AFIX 6 PART -1 C4 1 0.646221 0.416767 0.196647 11.00000 0.03494 0.06301 = 0.24307 0.01665 0.02873 -0.01648 AFIX 33 H4A 2 0.613979 0.384598 0.241954 11.00000 -1.50000 H4B 2 0.668510 0.403772 0.085782 11.00000 -1.50000 H4C 2 0.685802 0.425301 0.281525 11.00000 -1.50000 AFIX 5 C3 1 0.598935 0.475223 0.165817 11.00000 0.09537 0.08535 = 0.15418 0.06788 -0.04977 -0.07444 AFIX 23 H3A 2 0.558477 0.466482 0.081365 11.00000 -1.20000 H3B 2 0.575798 0.488049 0.277442 11.00000 -1.20000 AFIX 5 N2 5 0.648602 0.526993 0.093984 11.00000 0.01797 0.02970 = 0.03476 0.00650 -0.00559 -0.00471 AFIX 33 H2D 2 0.620312 0.560553 0.076840 11.00000 -1.20000 H2E 2 0.685309 0.535355 0.172252 11.00000 -1.20000 H2F 2 0.669278 0.515395 -0.009218 11.00000 -1.20000 AFIX 0 HKLF 4 REM ab313_lt_040322_a.res in Aba2 REM wR2 = 0.0621, GooF = S = 1.021, Restrained GooF = 1.026 for all data REM R1 = 0.0272 for 2065 Fo > 4sig(Fo) and 0.0342 for all 2295 data REM 106 parameters refined using 22 restraints END WGHT 0.0280 26.9576 REM Highest difference peak 1.539, deepest hole -1.195, 1-sigma level 0.173 Q1 1 0.6368 0.4197 0.1366 11.00000 0.05 1.54 Q2 1 0.6357 0.4319 0.2921 11.00000 0.05 1.31 Q3 1 0.6268 0.6912 0.6353 11.00000 0.05 1.25 Q4 1 0.6304 0.4535 0.0746 11.00000 0.05 1.24 Q5 1 0.6332 0.4312 -0.0164 11.00000 0.05 1.20 Q6 1 0.6245 0.5800 0.6360 11.00000 0.05 0.94 Q7 1 0.6361 0.4555 0.2056 11.00000 0.05 0.91 Q8 1 0.6494 0.5911 0.6381 11.00000 0.05 0.88 Q9 1 0.6372 0.6901 0.4961 11.00000 0.05 0.79 Q10 1 0.6388 0.6889 0.7756 11.00000 0.05 0.73 REM The information below was added by Olex2. REM REM R1 = 0.0272 for 2065 Fo > 4sig(Fo) and 0.0342 for all 9510 data REM 106 parameters refined using n/a restraints REM Highest difference peak 1.54, deepest hole -1.20 REM Mean Shift 0, Max Shift 0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0342 REM R1_gt = 0.0272 REM wR_ref = 0.0621 REM GOOF = 1.021 REM Shift_max = 0.001 REM Shift_mean = 0 REM Reflections_all = 9510 REM Reflections_gt = 2065 REM Parameters = 106 REM Hole = -1.20 REM Peak = 1.54 ; _cod_data_source_file d3ce01019h2.cif _cod_data_source_block ab313_lt_040322 _cod_depositor_comments 'Adding full bibliography for 7247803--7247812.cif.' _cod_original_sg_symbol_Hall 'A 2 -2ac' _cod_database_code 7247809 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula (C2H5NH3)2BiCl5 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _reflns_odcompleteness_completeness 99.64 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 26.32 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H,H) groups, All N(H,H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Uiso/Uaniso restraints and constraints N2 \\sim C3 \\sim C4: within 2A with sigma of 0.02 and sigma for terminal atoms of 0.04 within 2A 3. Rigid body (RIGU) restrains N2, C3, C4 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.01 4.a Free rotating group: C4(C3,N2) 4.b Secondary CH2 refined with riding coordinates: C1(H1D,H1E), C3(H3A,H3B) 4.c Me refined with riding coordinates: N1(H1A,H1B,H1C), C2(H2A,H2B,H2C), C4(H4A,H4B,H4C), N2(H2D,H2E,H2F) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.151 _oxdiff_exptl_absorpt_empirical_full_min 0.524 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' 'x+1/2, -y+1, z+1/2' '-x+1/2, y+1, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Bi1 Bi 0.63322(2) 0.63702(2) 0.63507(6) 0.01528(11) Uani 1 1 d . . . . . Cl1 Cl 0.52662(15) 0.62159(15) 0.8595(4) 0.0219(7) Uani 1 1 d . . . . . Cl2 Cl 0.54935(16) 0.6140(2) 0.3580(4) 0.0342(8) Uani 1 1 d . . . . . Cl3 Cl 0.59224(13) 0.75552(12) 0.5925(3) 0.0215(6) Uani 1 1 d . . . . . Cl4 Cl 0.72653(14) 0.66254(13) 0.9362(4) 0.0262(6) Uani 1 1 d . . . . . Cl5 Cl 0.67116(15) 0.51598(11) 0.6655(6) 0.0404(11) Uani 1 1 d . . . . . N1 N 0.5941(4) 0.7425(4) 0.1553(15) 0.029(2) Uani 1 1 d . . . . . H1A H 0.550787 0.729725 0.105833 0.035 Uiso 1 1 calc R U . . . H1B H 0.630330 0.714547 0.136055 0.035 Uiso 1 1 calc R U . . . H1C H 0.587417 0.747300 0.272289 0.035 Uiso 1 1 calc R U . . . C2 C 0.6913(5) 0.8241(5) 0.160(2) 0.033(3) Uani 1 1 d . . . . . H2A H 0.705617 0.862720 0.106684 0.050 Uiso 1 1 calc R U . . . H2B H 0.684348 0.829488 0.285861 0.050 Uiso 1 1 calc R U . . . H2C H 0.730636 0.794158 0.138912 0.050 Uiso 1 1 calc R U . . . C1 C 0.6167(6) 0.8015(5) 0.0758(16) 0.030(3) Uani 1 1 d . . . . . H1D H 0.576996 0.831839 0.095240 0.036 Uiso 1 1 calc R U . . . H1E H 0.623383 0.796435 -0.052021 0.036 Uiso 1 1 calc R U . . . C4 C 0.6462(7) 0.4168(5) 0.197(4) 0.114(11) Uani 1 1 d G U . A -1 H4A H 0.613979 0.384598 0.241954 0.171 Uiso 1 1 calc R U . A -1 H4B H 0.668510 0.403772 0.085782 0.171 Uiso 1 1 calc R U . A -1 H4C H 0.685802 0.425301 0.281525 0.171 Uiso 1 1 calc R U . A -1 C3 C 0.5989(5) 0.4752(5) 0.166(3) 0.112(8) Uani 1 1 d G U . A -1 H3A H 0.558477 0.466482 0.081365 0.134 Uiso 1 1 calc R U . A -1 H3B H 0.575798 0.488049 0.277442 0.134 Uiso 1 1 calc R U . A -1 N2 N 0.6486(4) 0.5270(3) 0.0940(13) 0.027(3) Uani 1 1 d G U . A -1 H2D H 0.620312 0.560553 0.076840 0.033 Uiso 1 1 calc R U . A -1 H2E H 0.685309 0.535355 0.172252 0.033 Uiso 1 1 calc R U . A -1 H2F H 0.669278 0.515395 -0.009218 0.033 Uiso 1 1 calc R U . A -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Bi1 0.00948(16) 0.02451(18) 0.01186(17) -0.0058(3) 0.0004(3) 0.00082(13) Cl1 0.0141(13) 0.0356(18) 0.0161(13) -0.0025(14) 0.0026(11) 0.0022(12) Cl2 0.0227(15) 0.069(2) 0.0105(13) -0.0094(16) -0.0016(12) -0.0179(17) Cl3 0.0172(11) 0.0307(13) 0.0166(15) -0.0003(10) -0.0018(9) 0.0055(10) Cl4 0.0223(14) 0.0380(15) 0.0183(14) -0.0018(13) -0.0120(10) -0.0023(12) Cl5 0.0227(12) 0.0224(12) 0.076(3) -0.0143(18) 0.0179(18) 0.0006(10) N1 0.021(4) 0.051(5) 0.015(5) -0.001(6) 0.004(5) -0.016(4) C2 0.027(5) 0.041(6) 0.032(8) -0.002(7) 0.001(7) -0.005(5) C1 0.028(6) 0.037(7) 0.025(6) -0.003(5) 0.001(5) 0.009(5) C4 0.035(8) 0.063(10) 0.24(3) 0.017(15) 0.029(13) -0.016(7) C3 0.095(11) 0.085(10) 0.15(2) 0.068(15) -0.050(15) -0.074(9) N2 0.018(4) 0.030(5) 0.035(7) 0.007(4) -0.006(4) -0.005(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Bi Bi -4.1077 10.2566 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u 2 0 0 6.18 0.75 -2 0 0 4.04 0.66 2 0 0 4.52 0.69 -2 0 0 5.24 0.76 3 0 0 0.67 0.85 -3 0 0 0.37 0.38 -3 0 0 0.89 0.94 3 0 0 0.02 0.81 -3 0 0 0.4 0.72 3 0 0 0.66 0.38 -4 0 0 5636.32 196.87 -4 0 0 5406.58 197.49 4 0 0 5477.46 197.46 -4 0 0 5776.68 197.46 4 0 0 5770.41 197.59 5 0 0 1.26 1.51 -5 0 0 1.11 1.13 -5 0 0 1.19 1.68 5 0 0 2.45 1.56 -5 0 0 2.88 0.73 -6 0 0 222.37 8.48 6 0 0 229.53 9.47 -6 0 0 225.53 9.46 -6 0 0 229.37 9.43 6 0 0 239.99 9.63 7 0 0 0.11 2.19 -7 0 0 -0.2 2.62 7 0 0 -0.52 2.09 8 0 0 2099.87 75.9 8 0 0 2187.38 76.14 -8 0 0 2065.67 75.74 9 0 0 0.35 3.15 -9 0 0 1.64 3.57 9 0 0 -1.01 3.3 10 0 0 748.39 28.71 -10 0 0 725.81 28.23 -10 0 0 730.52 28.16 10 0 0 752.07 28.4 -11 0 0 3.93 4.47 11 0 0 -3.03 4.09 -11 0 0 0.68 4.51 11 0 0 -4.57 4.71 12 0 0 1308.45 48.46 -12 0 0 1242.58 47.68 -12 0 0 1304.42 47.64 13 0 0 -3.15 6.18 -13 0 0 1.04 5.59 -13 0 0 5.73 5.66 14 0 0 330.04 16.26 15 0 0 11.72 7.22 16 0 0 182.43 12.39 17 0 0 24.58 9 18 0 0 662.13 29.41 19 0 0 31.58 11.14 20 0 0 342.9 20.35 21 0 0 15.21 12.88 22 0 0 872.93 39.22 0 2 0 188.79 8.02 0 -2 0 203.78 8.02 0 2 0 200.93 7.62 0 2 0 220.23 8.04 0 -2 0 209.18 7.67 -1 2 0 3573.76 125.79 -1 -2 0 3591.23 125.62 -1 -2 0 3588.08 125.92 1 2 0 3535.62 125.65 1 2 0 3583.23 125.88 1 -2 0 3615.79 125.81 2 2 0 39.59 1.98 -2 -2 0 40.56 2.04 2 2 0 38.56 1.81 -2 -2 0 40.04 1.79 2 -2 0 45.92 2.22 -2 2 0 35.58 2.02 -2 2 0 41.27 2.32 3 2 0 1716.83 61.45 -3 -2 0 1752.11 61.61 -3 2 0 1824.33 61.9 3 2 0 1721.98 61.62 -3 -2 0 1688 61.38 3 -2 0 1800.4 61.86 4 -2 0 34.83 2.52 -4 -2 0 31.24 2.37 -4 -2 0 36.64 2.2 -4 2 0 35.28 2.74 4 2 0 39.63 2.24 -5 -2 0 535.03 19.75 -5 2 0 547.78 20.34 -5 -2 0 534.8 19.99 5 2 0 543.03 19.9 -5 -2 0 511.54 20.01 5 -2 0 550.03 20.3 -6 -2 0 760.97 29.82 6 -2 0 828.97 30.21 -6 -2 0 807.8 29.54 -6 2 0 815.03 30.13 -6 -2 0 792.57 29.82 6 2 0 814.22 28.85 6 2 0 859.25 29.87 7 2 0 69.12 4.24 -7 2 0 64.08 3.22 -7 -2 0 65.23 4.41 -7 -2 0 64.43 4.12 7 -2 0 66.67 4.29 7 -2 0 61.89 4.4 -7 -2 0 59.24 3.95 7 2 0 65.8 2.88 -7 2 0 59.49 4.61 8 2 0 183.08 8.43 -8 -2 0 174.14 8.4 -8 2 0 177.35 7.22 -8 2 0 172.06 8.66 8 -2 0 176.58 8.78 8 -2 0 171.47 8.35 8 2 0 186.49 6.94 -8 -2 0 173.28 8.24 -8 -2 0 177.03 8.13 -9 2 0 3844.15 139.09 9 2 0 3988.12 140.52 9 -2 0 3926.73 140.29 -9 -2 0 3916.85 140.2 9 -2 0 3995.61 140.84 9 2 0 4054.81 138.85 -9 -2 0 3938.37 139.92 -9 -2 0 3884.16 140.33 -9 2 0 3924.34 140.39 -10 -2 0 151.74 7.97 -10 -2 0 147.77 7.92 -10 2 0 151.65 6.43 10 -2 0 142.34 8.01 -10 2 0 146.24 8.41 10 -2 0 146.51 8.5 10 2 0 162.07 8.37 -10 -2 0 154.74 8.16 -11 -2 0 148.32 8.18 -11 -2 0 151.13 8.47 -11 2 0 145.34 6.48 -11 -2 0 154.15 8.35 11 2 0 150.19 8.82 11 -2 0 143.82 8.25 -11 2 0 148.61 8.93 11 -2 0 158.72 9.02 12 -2 0 43.01 5.92 12 2 0 29.57 6.13 -12 -2 0 39.18 5.51 -12 2 0 34.72 6.09 12 -2 0 29.25 5.21 -12 -2 0 32.01 5.62 -12 -2 0 36.52 4.89 13 2 0 1815.23 64.47 -13 -2 0 1685.77 63.42 13 -2 0 1714.93 63.65 13 -2 0 1707.85 64.36 -13 -2 0 1777.59 63.29 -13 2 0 1697.36 63.78 -14 2 0 21.77 6.77 14 -2 0 34.91 6.82 -14 -2 0 25.86 6.46 14 2 0 14.68 7.23 15 2 0 -7.93 8.1 15 -2 0 11.06 7.01 16 2 0 7.46 8.16 16 -2 0 22.8 8.19 17 -2 0 752.97 33.3 17 2 0 830.67 33.46 18 2 0 86.38 11.45 18 -2 0 79.88 11.23 19 2 0 46.26 11.36 19 -2 0 21.04 10.97 20 2 0 25.91 12.26 20 -2 0 15.7 11.81 21 2 0 972.6 40.04 21 -2 0 863.68 39.49 22 2 0 83.62 15.55 0 4 0 3243.23 114.81 0 4 0 3253.31 115.5 0 -4 0 3415.7 115.62 0 4 0 3019.64 115.02 0 4 0 3175.12 115.76 0 -4 0 3480.82 114.98 0 -4 0 3196.23 115.7 -1 -4 0 180.51 7.13 -1 4 0 180.01 7.22 1 4 0 177.77 7.12 -1 -4 0 178.37 7.49 1 -4 0 176.27 8.07 1 -4 0 196.78 8.08 -1 4 0 167.76 7.4 1 4 0 171.5 7.57 -1 -4 0 167.15 7.52 1 4 0 218.96 8.12 -1 4 0 181.32 7.99 -2 -4 0 42.45 2.03 2 -4 0 50.97 2.99 -2 4 0 42.15 2.86 2 -4 0 41.71 2.58 -2 -4 0 40.24 2.82 2 -4 0 42.68 2.75 2 4 0 43.28 2.01 -2 4 0 46.47 3.05 2 4 0 42.73 2.39 -2 -4 0 41.95 2.48 -2 4 0 41.27 2.42 3 -4 0 3.25 1.42 3 4 0 2.29 1.19 -3 -4 0 2.88 1.37 3 4 0 4.81 0.97 -3 -4 0 3.49 1.14 -3 -4 0 3.89 1.44 -3 4 0 3.07 1.95 -3 4 0 3.01 1.46 4 4 0 352.06 13.75 4 -4 0 362.79 14.14 -4 -4 0 367.1 13.35 -4 -4 0 360.56 13.77 -4 4 0 352.59 13.86 -4 4 0 362.39 14.39 4 4 0 360.63 13.39 -5 4 0 64.84 4.14 5 -4 0 70.47 4.24 -5 -4 0 71.31 3.59 -5 -4 0 68.27 4.03 5 4 0 75.66 3.71 5 4 0 70.34 3.85 -5 4 0 62.52 4.6 6 4 0 422.06 16.63 6 4 0 443.24 16.36 -6 -4 0 434.13 16.14 6 -4 0 434.81 17.03 -6 4 0 420.44 17.22 -6 -4 0 412.37 16.58 -7 -4 0 314.01 12.72 -7 -4 0 312.68 12.23 -7 4 0 282.87 13.25 7 -4 0 307.98 13.1 7 4 0 321.02 12.57 -8 -4 0 2174.48 80.43 -8 4 0 2188.8 80.77 8 -4 0 2138.69 80.72 -8 -4 0 2293 80.25 8 4 0 2303.53 80.21 -8 -4 0 2277.32 79.75 -9 4 0 312.62 14.3 9 -4 0 322.71 14.23 -9 -4 0 319.22 13.74 -9 -4 0 315.97 13.88 9 4 0 346.72 13.95 -9 -4 0 331.18 13.29 -10 4 0 1372.16 48.96 10 4 0 1455.1 50.36 10 4 0 1345.44 48.37 -10 -4 0 1380.02 49.52 -10 -4 0 1327.66 50.21 -10 -4 0 1366.93 50.02 10 -4 0 1363.81 50.07 10 -4 0 1331.47 50.55 -10 4 0 1328.69 50.53 -11 -4 0 10.95 3.84 -11 -4 0 20.13 4.58 -11 4 0 14.12 2.74 -11 -4 0 13.02 5.07 11 4 0 16.3 4.89 11 -4 0 13.58 4.32 11 -4 0 21.52 4.97 -11 4 0 19.43 5.62 -12 -4 0 2840.83 104.19 -12 -4 0 2887.42 104.72 -12 -4 0 2980.83 103.79 12 -4 0 2874.85 105.18 12 4 0 3148.78 104.99 -12 4 0 2774.34 104.74 12 -4 0 2817.18 104.26 -13 -4 0 248.43 12.53 13 -4 0 252.25 13.4 -13 -4 0 250.76 12.68 13 -4 0 243.78 12.31 13 4 0 271.99 13.5 -13 4 0 222.2 13.38 -13 -4 0 266.79 12.22 -14 -4 0 739.58 28.3 -14 -4 0 710.97 29.22 14 4 0 770.82 29.87 14 -4 0 666.71 29.65 15 4 0 25.56 8.19 -15 -4 0 31.4 6.73 15 -4 0 42.7 7.97 16 4 0 639.64 27.5 16 -4 0 601.78 27.16 17 4 0 69.84 10.76 17 -4 0 81.85 10.8 18 -4 0 589.18 29.1 18 4 0 741.63 29.74 19 4 0 29.34 11.39 19 -4 0 17.52 10.97 -19 -4 0 36.37 12.42 20 4 0 371.22 20.44 20 -4 0 289.97 19.77 21 -4 0 107.91 14.8 21 4 0 147.58 15.91 0 6 0 963.64 35.79 0 -6 0 939.55 36.25 0 6 0 872.13 35.07 0 6 0 954.92 36.23 0 6 0 959.01 34.82 0 -6 0 998.66 35.1 0 -6 0 1030.33 35.94 1 6 0 1897.38 70.51 -1 6 0 1959.64 70.13 1 -6 0 1980.05 70.33 -1 6 0 1913.58 70.32 1 6 0 1961.66 70.04 -1 -6 0 1971.74 70 1 -6 0 2140.88 71.32 -1 6 0 1933.53 71.15 -1 -6 0 1923.64 70.82 1 6 0 2058.56 71.43 -1 -6 0 2126.24 71.14 1 -6 0 1749.61 71.44 -2 6 0 908.38 37.79 2 -6 0 1026.24 37.66 2 -6 0 1107 38.87 2 6 0 1197.12 38.71 -2 6 0 1048.35 38.51 2 6 0 1008.29 36.82 2 6 0 1055.58 38.22 -2 6 0 1077.98 37.54 -2 -6 0 1032.26 37.46 -2 -6 0 1011.97 38.19 2 6 0 1058.06 37.51 3 -6 0 2409.85 81.05 -3 -6 0 2104.41 80.61 -3 6 0 2074.67 80.42 -3 -6 0 2252.74 79.89 -3 6 0 2283.82 80.79 3 -6 0 2255.78 80.21 3 6 0 2284.1 79.99 -3 6 0 2234.28 79.77 3 -6 0 2228.59 80.41 3 6 0 2512.45 80.55 3 6 0 2208.64 79.27 -4 6 0 148.62 6.79 -4 -6 0 148.74 6.79 4 6 0 154.54 6.81 4 6 0 150.36 6.15 4 -6 0 163.36 7.53 -4 -6 0 157.76 6.16 -4 -6 0 146.91 7.51 -4 6 0 132.79 7.64 4 -6 0 144.03 7.2 -5 6 0 387.98 17.62 -5 -6 0 450.73 16.78 5 6 0 448.38 16.82 -5 -6 0 399.74 17.46 -5 -6 0 446.54 16.07 5 6 0 436.74 16.19 5 -6 0 434.52 17.24 -5 6 0 419.91 16.7 6 6 0 472.92 18.42 -6 -6 0 481.25 18.29 -6 -6 0 490.37 17.66 6 -6 0 462.13 18.84 -6 -6 0 455.61 19.15 6 6 0 485.81 17.85 -6 6 0 476.37 18.4 -6 6 0 410.78 19.12 7 -6 0 225.92 10.9 7 6 0 233.59 10.44 -7 6 0 218.57 11.31 -7 6 0 244.32 10.72 -7 -6 0 248.39 10.49 -7 -6 0 226.72 11.19 7 6 0 247.36 10.05 -7 -6 0 243.66 9.75 -8 -6 0 379.04 15.52 8 6 0 373.04 15.65 -8 -6 0 395.98 14.86 8 6 0 388.33 15.25 8 -6 0 374.26 16.11 -8 6 0 369.67 15.86 -8 6 0 358.01 16.46 -9 -6 0 2489.19 90.88 -9 -6 0 2596.63 90.26 9 6 0 2638.44 90.93 9 -6 0 2423.4 91.59 -9 6 0 2419.53 91.86 -9 6 0 2564.25 91.28 -10 -6 0 216.38 11.19 10 -6 0 228.5 11.76 -10 6 0 234.21 11.7 10 6 0 258.62 11.35 -10 -6 0 238.98 11.16 -10 6 0 215.57 12.04 -10 -6 0 237.32 10.44 11 6 0 422.6 16.74 -11 6 0 340.24 17.18 -11 -6 0 387.98 16.41 -11 -6 0 365.58 16.64 11 -6 0 367.42 17.13 -11 6 0 389.52 17.1 -11 -6 0 383.59 15.61 -12 -6 0 236.51 11 -12 -6 0 233.5 11.88 12 6 0 268.12 12.36 12 -6 0 212.89 11.42 -12 -6 0 230.03 11.86 -12 6 0 213.44 12.81 -12 6 0 256.41 12.94 12 -6 0 221.88 12.42 13 -6 0 1256.04 52.67 -13 -6 0 1326.87 52.25 -13 6 0 1452.14 52.81 -13 -6 0 1423.69 51.13 13 6 0 1479.45 52.42 -14 6 0 146.73 11.41 14 -6 0 119.97 10.42 -14 -6 0 142.69 8.98 -14 -6 0 134.95 9.49 14 6 0 147.99 10.76 15 6 0 5.76 8.18 15 -6 0 5.22 7.56 -15 -6 0 1.83 5.97 -16 -6 0 156.25 13.36 -16 -6 0 148.47 10.83 16 6 0 150.59 12.55 16 -6 0 139.76 11.93 -17 -6 0 852.24 33.77 -17 -6 0 755.28 35.31 17 6 0 893.12 34.87 17 -6 0 743.14 34.06 -18 -6 0 29.38 12.09 -18 -6 0 14.52 8.39 18 -6 0 12.14 10.23 18 6 0 20.82 10.88 -19 -6 0 65.34 13.87 19 -6 0 50.23 12.33 -20 -6 0 222.87 19.47 20 -6 0 187.43 16.8 21 -6 0 479.8 25.93 0 8 0 5319.73 194.2 0 8 0 5476.86 195.47 0 -8 0 5833.46 195.11 0 -8 0 5060.09 195.72 0 -8 0 5771.2 194.15 0 8 0 5518.28 194.93 0 8 0 5390.82 193.72 1 8 0 1782.64 63.89 1 8 0 1619.59 64.34 -1 -8 0 1797.82 65.11 -1 -8 0 1689.47 65.15 -1 8 0 1742.42 65.21 -1 8 0 1762.79 63.94 1 -8 0 1859.11 64.41 -1 -8 0 1781.3 63.93 1 -8 0 1676.03 66.08 1 -8 0 1811.59 65.22 -1 8 0 1905.84 64.4 1 8 0 1882.41 65.95 -2 8 0 284.31 13.34 2 -8 0 334.99 14.39 -2 8 0 324.87 14.51 2 -8 0 312.7 13.13 -2 -8 0 342.21 13.05 -2 -8 0 302.7 13.83 2 8 0 323.23 13.9 2 8 0 330.57 12.96 -2 -8 0 318 13.91 2 8 0 355.91 14.76 -2 8 0 334.77 13.11 2 -8 0 285.37 14.74 3 -8 0 42.57 4.49 -3 8 0 46.69 3.39 3 -8 0 50.64 4.07 -3 -8 0 50.59 3.81 -3 -8 0 40.62 4.32 -3 8 0 33.66 4.25 3 8 0 57.26 5.07 -3 8 0 44.61 4.96 3 8 0 49.25 3.61 3 8 0 44.53 2.62 -4 8 0 1917.42 65.44 -4 -8 0 1868.36 64.21 4 8 0 1840.75 64.33 -4 -8 0 1688.11 65.11 4 8 0 1776.86 63.33 -4 8 0 1597.38 64.87 4 -8 0 1885.3 65.75 -4 8 0 1747.96 63.9 4 -8 0 1711.95 64.58 4 8 0 1865.98 64.78 5 -8 0 1199.69 46.01 5 8 0 1202.37 45.4 -5 -8 0 1205.22 46.51 -5 -8 0 1293.44 44.54 -5 8 0 1264.79 45.28 5 8 0 1236.81 44.6 5 8 0 1275.74 45.58 5 -8 0 1308.1 46.7 -5 8 0 1132.68 46.31 -5 -8 0 1260.54 45.35 -6 -8 0 117.74 6.5 -6 -8 0 123.12 5.61 6 -8 0 137.48 7.51 6 -8 0 102.92 6.92 6 8 0 120.71 6.55 6 8 0 118 5.7 -6 8 0 130.13 6.64 -6 8 0 98.33 7.78 -6 -8 0 111.81 7.35 -7 -8 0 210.42 8.7 7 8 0 202.25 8.91 -7 -8 0 207.37 10.83 -7 8 0 183.72 10.81 -7 8 0 214.91 9.73 7 -8 0 193.91 10.19 7 8 0 197.86 9.62 -7 -8 0 210.18 9.68 7 -8 0 223.42 10.44 -8 -8 0 763.98 27.21 8 -8 0 750.58 28.81 8 -8 0 708.06 28.75 8 8 0 746.41 27.6 -8 -8 0 680.07 29.38 -8 -8 0 745.74 28.11 -8 8 0 680.83 29.26 -8 8 0 764.62 28.28 8 8 0 714.44 28.22 -9 8 0 767.45 28.61 -9 8 0 680.15 29.5 9 -8 0 745.4 28.94 9 8 0 787.01 28.03 9 8 0 730.17 28.6 -9 -8 0 741.65 28.32 -9 -8 0 760.86 27.44 -9 -8 0 689.35 29.72 9 -8 0 655.39 28.88 -10 -8 0 324.58 13.07 10 8 0 343.7 13.86 -10 8 0 289.78 15.44 -10 -8 0 316.93 14.04 -10 -8 0 289.93 15.28 -10 8 0 325.81 14.59 10 -8 0 266.16 14.38 11 -8 0 0.69 5.3 -11 -8 0 9.05 5.61 -11 8 0 3.46 6.64 -11 -8 0 5.48 4.63 11 8 0 7.62 5.24 -11 -8 0 13.74 6.26 -11 8 0 1.47 6.3 12 -8 0 478.42 19.98 -12 -8 0 458.85 20.21 -12 -8 0 439.9 21.35 12 -8 0 407.51 20.39 -12 8 0 502.22 20.59 -12 -8 0 489.99 19.83 -12 8 0 400.78 21.01 12 8 0 501.02 19.96 13 -8 0 300.49 16.77 -13 -8 0 332.81 17.95 -13 -8 0 350.92 16.47 13 8 0 384.96 16.88 -14 -8 0 89.11 8.7 -14 -8 0 100.62 11.15 14 -8 0 81.77 9.46 14 8 0 106.96 9.64 15 -8 0 23.3 8.38 -15 -8 0 23.42 7.05 -15 -8 0 42.73 10.18 -16 -8 0 86.7 11.96 16 -8 0 60.97 10.08 -16 -8 0 71.13 9 -17 -8 0 204.01 16.6 -17 -8 0 194.27 12.86 17 -8 0 155.09 13.89 -18 -8 0 547.94 23.77 -18 -8 0 495.87 26.76 -19 -8 0 3.61 9.27 -19 -8 0 19.95 14.15 19 -8 0 -4.31 11.59 20 -8 0 86.1 14.85 -20 -8 0 137.02 13.11 -20 -8 0 108.56 17.19 -21 -8 0 329.95 24.38 0 -10 0 1636.37 57.07 0 -10 0 1606.1 57.99 0 10 0 1582.54 58.52 0 10 0 1490.9 56.87 0 -10 0 1518.77 59.12 0 10 0 1499.09 56.4 0 10 0 1573.82 57.89 1 -10 0 1399.87 55.55 -1 10 0 1485.2 54.26 -1 -10 0 1466.8 52.93 -1 10 0 1589.24 53.31 -1 -10 0 1377.92 54.53 1 -10 0 1459.35 54.12 1 10 0 1473.64 54.77 1 10 0 1314.3 53.17 -1 10 0 1447.69 52.97 -1 10 0 1413.35 52.64 1 10 0 1389.42 52.61 1 -10 0 1541.77 53.41 -2 10 0 56.27 4.54 2 -10 0 64.74 5.88 2 -10 0 56.6 4.91 -2 10 0 55.25 5.45 -2 -10 0 52.12 5.64 2 10 0 74.65 7.31 2 -10 0 56.33 7.03 2 10 0 60.61 4.46 2 10 0 55.71 5.92 -2 10 0 49.22 6.37 -2 -10 0 56.7 4.76 3 10 0 1051.44 37.64 3 10 0 1038.77 38.62 3 10 0 1093.25 39.39 -3 10 0 1017.98 39.06 3 10 0 973.33 36.37 -3 -10 0 1055.68 37.59 -3 -10 0 979.82 38.77 -3 10 0 961.61 38.3 3 -10 0 1093.4 39.43 3 -10 0 974.14 37.85 -3 10 0 1017.07 37.54 -3 -10 0 1007.64 38.81 -4 10 0 1017.29 43.89 4 10 0 1217.32 44.42 4 -10 0 1131.54 43.67 -4 -10 0 1190.49 44.62 -4 10 0 1199.66 43.12 -4 10 0 1174.18 44.56 4 10 0 1236.08 43.45 4 -10 0 1213.73 45.04 4 10 0 1167.47 42.09 -4 -10 0 1208.9 43.22 5 10 0 1129.49 43.33 5 10 0 1173.23 41.72 -5 10 0 1030.11 43.86 -5 -10 0 1163.06 44.23 5 -10 0 1207.66 44.66 5 10 0 1238.62 43.08 5 -10 0 1046.39 43.1 -5 10 0 1222.67 44.22 -5 -10 0 1215.78 42.88 -6 10 0 33.24 6.12 -6 10 0 21.19 4.19 -6 -10 0 24.37 4.42 6 -10 0 15.16 4.59 6 10 0 26.32 4.14 -6 -10 0 23.57 5.08 6 -10 0 24.2 5.52 6 10 0 27.72 3.12 6 10 0 22.02 4.26 -6 10 0 15.32 5.7 -7 -10 0 107.38 5.51 -7 -10 0 99.9 7.94 7 -10 0 86.39 7.42 7 10 0 95.41 6.26 7 10 0 107.47 5.76 -7 10 0 109.84 6.83 -7 10 0 85.69 8.32 7 -10 0 109.68 8.11 7 10 0 111.96 6.94 -7 -10 0 107.02 6.88 8 -10 0 993.09 39.6 -8 -10 0 1126.45 37.78 8 -10 0 1062.37 40.23 -8 10 0 1152.92 39.03 -8 -10 0 1024.29 40.71 8 10 0 815.39 37.83 8 10 0 1104.1 38.2 -8 -10 0 1102.57 38.85 -8 10 0 937.35 40.18 8 10 0 1073.29 39.24 -9 10 0 1543.92 52.9 9 10 0 1421.04 53.11 -9 -10 0 1364.96 54.56 9 10 0 1532.89 52.25 -9 10 0 1231.98 53.96 9 -10 0 1443.19 54.03 9 -10 0 1297.77 53.55 -9 -10 0 1470.33 52.73 10 10 0 37.02 5.28 -10 -10 0 30.98 6.03 -10 -10 0 29.23 7.08 10 -10 0 20.26 6.33 10 10 0 28.9 5.83 -10 10 0 23.81 8.24 10 -10 0 28.08 6.61 11 10 0 47.66 6.1 11 -10 0 35.21 7.14 -11 10 0 22.45 8.32 -11 -10 0 43.89 6.75 -11 -10 0 36.23 7.99 11 -10 0 42.16 7.39 12 -10 0 240.7 14.48 -12 -10 0 264.5 15.71 12 -10 0 287.83 14.55 -13 -10 0 460.42 20.75 13 -10 0 472.66 21 -13 -10 0 460.35 22.58 13 -10 0 409.16 20.9 -14 -10 0 362.63 19.93 14 -10 0 320.28 18.44 -14 -10 0 393.75 18.19 -15 -10 0 15.64 7.64 -15 -10 0 18.54 10.26 15 -10 0 0.8 8.77 -16 -10 0 50.95 9.04 -16 -10 0 70.32 12.61 16 -10 0 41.76 10.64 -17 -10 0 507.47 26.47 -17 -10 0 526.23 23.71 18 -10 0 300.41 20.05 -18 -10 0 365.94 19.2 -18 -10 0 345.07 22.43 -19 -10 0 33.69 14.73 19 -10 0 5.39 12.53 -19 -10 0 30.96 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2 -20 -6 20.73 19.96 3 20 -6 223.81 18.58 3 -20 -6 242.7 25.18 -3 20 -6 221.54 17.93 4 -20 -6 38.57 21.18 5 -20 -6 326.93 28.47 6 -20 -6 -3.17 21.27 0 1 -7 -1.24 4.75 0 -1 -7 0.38 5.04 0 -1 -7 -5.13 10.54 0 1 -7 -6 7.56 0 -1 -7 -0.73 6.93 -1 1 -7 237.46 11.92 1 1 -7 240.05 12.11 -1 -1 -7 252.01 12.16 1 -1 -7 257.6 12.31 -1 -1 -7 240.45 13.26 1 1 -7 243.58 13.48 1 -1 -7 245.32 13.3 1 -1 -7 227.84 17.01 -1 -1 -7 216.86 16.83 -2 1 -7 715.27 28.07 2 1 -7 686.78 28.33 -2 -1 -7 765.98 28.35 2 -1 -7 742.12 28.55 2 1 -7 715.76 29.24 2 -1 -7 730.17 28.96 2 -1 -7 696.6 32.46 3 1 -7 393.36 17.92 3 -1 -7 424.44 18.15 3 1 -7 413.82 18.97 3 -1 -7 427.51 18.67 3 1 -7 404.89 21.33 3 -1 -7 385.34 21.85 4 1 -7 72 7.12 4 -1 -7 73.97 7.16 4 1 -7 87.92 9.03 4 1 -7 84.67 11.82 4 -1 -7 80.44 12.26 4 -1 -7 77.61 8.75 5 1 -7 127.24 9.12 5 -1 -7 144.35 9.4 5 1 -7 152.28 10.67 5 1 -7 138.89 13.52 5 -1 -7 149.09 10.5 5 -1 -7 146.12 14.34 6 1 -7 498.81 21.38 6 -1 -7 500.13 21.47 6 1 -7 466.72 24.69 6 -1 -7 485.55 25.6 6 1 -7 508.69 22.13 6 -1 -7 527.02 21.89 7 1 -7 217.43 12.24 7 -1 -7 228.77 12.45 7 1 -7 218.5 15.99 7 -1 -7 222.22 17.24 7 1 -7 236.93 13.56 7 -1 -7 244.11 13.27 8 1 -7 70.63 7.68 8 -1 -7 76.44 7.68 8 1 -7 89.41 9.57 8 -1 -7 75.69 12.54 8 -1 -7 74.79 9.24 9 1 -7 18.41 6.67 9 -1 -7 20.13 6.48 9 1 -7 15.5 8.56 9 -1 -7 11.93 8.44 10 1 -7 460.78 21.08 10 -1 -7 476.16 21.19 10 1 -7 490.14 22.16 10 -1 -7 499.39 22 11 1 -7 490.86 22.36 11 -1 -7 512.5 22.55 11 1 -7 523.86 23.37 11 -1 -7 527.23 23.28 12 1 -7 451.2 20.83 12 -1 -7 443.15 20.72 12 1 -7 477.9 22.02 12 -1 -7 488.79 22 13 1 -7 7.46 7.34 13 -1 -7 2.33 7.12 13 1 -7 16.21 10.43 13 -1 -7 7.97 9.95 14 1 -7 353.07 17.68 14 -1 -7 345.13 17.44 14 1 -7 353.1 19.18 14 -1 -7 372.84 19.36 0 -3 -7 -0.1 4.91 0 -3 -7 -6.11 11.82 -1 -3 -7 400.8 16.91 1 -3 -7 410.39 17.07 1 3 -7 345.9 17.93 1 -3 -7 360.42 22.19 -1 -3 -7 319.75 21.57 2 -3 -7 585.34 22.84 2 3 -7 562.04 24.04 2 -3 -7 555.9 22.84 2 -3 -7 526.72 27.8 3 3 -7 598.58 26.26 3 -3 -7 696.5 26.74 3 3 -7 657.87 27.63 3 -3 -7 687.62 26.78 3 -3 -7 649.52 31.25 4 3 -7 13.4 5.54 4 -3 -7 14.57 5.59 4 -3 -7 25.62 11.42 4 3 -7 14.65 7.89 4 -3 -7 15.7 6.99 5 3 -7 164.98 10.27 5 -3 -7 169.59 10.35 5 3 -7 184.91 12.05 5 -3 -7 195.73 11.23 5 -3 -7 152.31 15.83 6 3 -7 258.71 13.62 6 -3 -7 280.06 13.89 6 3 -7 290.5 15.13 6 -3 -7 268.2 18.9 6 -3 -7 290.97 14.21 -6 3 -7 227.91 15.66 7 3 -7 363.76 17.42 7 -3 -7 407.03 17.69 7 -3 -7 361.08 22.38 7 3 -7 413.21 18.81 7 -3 -7 404.49 18.02 -7 3 -7 329.57 19.45 8 3 -7 37.99 6.85 8 -3 -7 46.58 6.93 8 -3 -7 54.97 13.48 8 3 -7 53.87 9.11 8 -3 -7 37.48 8.65 9 3 -7 76.45 8.26 9 -3 -7 86.55 8.28 9 3 -7 113.31 10.72 9 -3 -7 87.2 13.58 9 -3 -7 84.55 9.77 10 3 -7 104.81 9.22 10 -3 -7 116.81 9.19 10 3 -7 113.76 11.32 10 -3 -7 121.04 11.02 11 3 -7 756.88 31.76 11 -3 -7 768.99 31.68 11 3 -7 810.48 32.83 11 -3 -7 820.03 32.34 12 3 -7 144.27 10.82 12 -3 -7 148.04 10.63 12 3 -7 161.24 13.15 12 -3 -7 154.39 12.38 13 3 -7 7.35 7.37 13 3 -7 -1.12 10.6 13 -3 -7 10.27 10.09 14 3 -7 160.39 11.72 14 3 -7 180.85 14.55 14 -3 -7 183.65 14.07 0 -5 -7 6.62 5.04 0 -5 -7 -5.89 12.5 -1 5 -7 72.7 11.94 1 -5 -7 92.69 7.37 -1 -5 -7 97.16 7.54 1 -5 -7 70.52 13.71 1 5 -7 83.57 9.82 -1 -5 -7 57.9 13.57 2 5 -7 1100.72 43.92 2 -5 -7 1080.49 48.18 -2 5 -7 1017.7 45.83 -3 5 -7 100.77 12.31 3 -5 -7 105.54 7.97 3 5 -7 101.77 10.42 3 -5 -7 117.14 14.95 -4 5 -7 30.75 10.51 4 -5 -7 37.59 6.27 4 -5 -7 45.76 13.27 4 5 -7 31.43 8.67 5 -5 -7 125.46 8.79 5 5 -7 117.92 10.9 5 -5 -7 140.48 15.79 -5 5 -7 115.14 12.61 6 -5 -7 732.04 28.89 6 5 -7 752.55 30.16 6 -5 -7 735.11 34.92 -6 5 -7 633.93 31.01 -7 5 -7 68.75 10.93 7 -5 -7 73.1 7.52 7 5 -7 56.91 7.43 7 -5 -7 61.04 14.31 7 5 -7 79.62 10.05 8 5 -7 94.82 8.77 -8 5 -7 90.66 11.91 8 -5 -7 101.01 8.65 8 5 -7 129.09 11.14 8 -5 -7 102.91 15.52 9 5 -7 -3.27 6.54 9 -5 -7 -2.16 12.95 9 5 -7 15.12 9.04 10 5 -7 543.55 24.49 10 5 -7 618.56 25.89 11 5 -7 145.31 11.01 11 5 -7 158.42 13.25 11 -5 -7 164.59 12.18 12 5 -7 332.94 17.04 12 5 -7 357.22 18.96 12 -5 -7 354.17 18.14 13 5 -7 10.22 7.64 13 5 -7 20.14 11.32 13 -5 -7 27.2 10.32 14 5 -7 298.05 16.21 14 -5 -7 329.24 18.12 0 7 -7 1.92 10.74 0 -7 -7 -7.55 13.2 1 -7 -7 352.6 24.19 -1 -7 -7 319.61 22.89 -1 7 -7 429.52 22 1 7 -7 453.54 21.82 -2 7 -7 48.28 12.28 2 7 -7 77.64 11.2 2 -7 -7 57.72 14.73 2 7 -7 54.07 9.77 3 7 -7 803.37 32.69 3 -7 -7 745.92 37.57 -3 7 -7 753.92 34.57 -4 7 -7 0.81 10.52 4 -7 -7 2.11 13.5 4 7 -7 -1.3 8.97 5 7 -7 262.54 15.49 5 -7 -7 263.52 20.53 -5 7 -7 236.31 17.13 -6 7 -7 44.35 11.11 6 -7 -7 41.33 14.71 6 7 -7 46.41 9.67 7 7 -7 651.95 26.98 7 -7 -7 597.27 32.17 -8 7 -7 61.13 11.92 8 -7 -7 74.42 15.76 8 7 -7 79.3 10.7 -9 7 -7 79.77 12.74 9 7 -7 104.24 11.47 9 -7 -7 84.72 16.16 -10 7 -7 21.85 11.67 10 7 -7 -1.5 7 10 -7 -7 18.86 14.03 10 7 -7 18.56 10.18 11 7 -7 764.16 32.72 11 7 -7 873.87 34.36 12 7 -7 49.24 8.49 12 7 -7 73.35 12.15 13 7 -7 -0.13 7.66 13 7 -7 9.04 11.57 0 9 -7 2.59 11.18 0 -9 -7 -4.3 13.78 -1 9 -7 6.13 11.22 1 9 -7 18.95 10.79 1 -9 -7 -0.63 13.63 -1 -9 -7 4.64 12.8 2 9 -7 763.45 32.68 2 -9 -7 683.89 37.44 -2 9 -7 790.93 34.98 2 9 -7 806.23 33.94 -3 9 -7 8.7 11.77 3 9 -7 16.32 10.45 3 -9 -7 -5.01 14.74 3 9 -7 4.53 9.61 -4 9 -7 116.72 14.08 4 9 -7 100.55 12.82 4 -9 -7 119.13 17.68 4 9 -7 105.77 11.73 -5 9 -7 50.44 12.25 5 9 -7 39.59 11.29 5 -9 -7 63.92 16.61 5 9 -7 54.25 10.82 6 9 -7 702.36 29.34 6 -9 -7 628.27 34.92 -6 9 -7 628.94 30.77 -7 9 -7 18.25 12 7 -9 -7 -1.32 15.09 7 9 -7 19.94 10.1 8 9 -7 152.25 13.19 8 -9 -7 136.9 18.58 -8 9 -7 150.09 14.99 -9 9 -7 45.68 12.72 9 -9 -7 45.97 16.57 9 9 -7 41.38 11 10 -9 -7 418.16 28.2 -10 9 -7 431.48 24.76 -11 9 -7 14.46 13.35 11 -9 -7 7.72 14.69 11 9 -7 25.31 11.01 12 9 -7 285.33 15.96 12 9 -7 343.97 18.83 -12 9 -7 293.1 20.88 13 9 -7 4.23 8.03 0 11 -7 1.03 11.39 0 -11 -7 -8.67 14.41 1 -11 -7 284.32 23.2 -1 -11 -7 248.46 21.39 -1 11 -7 315.68 19.89 1 11 -7 357.74 20.08 -2 11 -7 72.11 13.41 2 11 -7 79.68 12.82 2 -11 -7 71.31 17.28 2 11 -7 55.74 11.3 3 11 -7 586.87 27.26 3 -11 -7 544.74 33.33 -3 11 -7 573.41 28.99 3 11 -7 633.75 28.34 -4 11 -7 13.66 12.53 4 11 -7 4.85 12.04 4 -11 -7 14.76 16.63 4 11 -7 15.69 10.66 5 11 -7 274.69 17.78 5 11 -7 264 16.76 5 -11 -7 243.69 23.12 -5 11 -7 242.21 18.37 -6 11 -7 52.2 13.3 6 11 -7 39.96 11.76 6 -11 -7 50.33 17.76 6 11 -7 50.56 11.24 7 11 -7 665.52 28.67 7 11 -7 622.8 28.08 7 -11 -7 553.49 34.37 -7 11 -7 575.12 29.8 -8 11 -7 4.53 12.54 8 11 -7 15.68 11.46 8 -11 -7 2.48 16.59 8 11 -7 1.91 10.58 -9 11 -7 56.58 13.98 9 -11 -7 65.09 18.26 9 11 -7 77.59 12.13 -10 11 -7 52.7 14.22 10 -11 -7 50.99 18.48 10 11 -7 70.79 12.48 11 -11 -7 410.24 30.21 -11 11 -7 470.35 27.41 0 13 -7 -0.42 11.93 0 -13 -7 5.62 15.38 -1 13 -7 9.2 12.67 1 13 -7 26.36 12.49 1 -13 -7 22.75 16.76 -1 -13 -7 14.29 14.74 2 13 -7 654.09 30.54 2 -13 -7 647.48 36.65 -2 13 -7 688.82 31.96 2 13 -7 712.71 31.84 -3 13 -7 14.45 12.77 3 13 -7 27.64 12.08 3 -13 -7 27.7 17.76 3 13 -7 17.09 11.13 -4 13 -7 16.15 13.11 4 13 -7 14.03 12.8 4 -13 -7 38.38 18.55 4 13 -7 13.18 11.31 -5 13 -7 -1.77 13.24 5 13 -7 -4.39 12.68 5 -13 -7 -4.87 17.98 5 13 -7 0.17 11.31 6 13 -7 722.2 31.8 6 13 -7 717.36 31.31 -6 13 -7 669.96 32.76 -7 13 -7 40.97 13.78 7 13 -7 62 13 7 -13 -7 49.87 19.4 7 13 -7 56.47 12.5 -8 13 -7 65.13 14.76 8 13 -7 72.43 13.46 8 -13 -7 71.75 19.71 8 13 -7 81.41 13.02 -9 13 -7 59.35 14.92 9 13 -7 68.07 13.59 9 -13 -7 44.23 18.79 9 13 -7 60.33 12.76 10 13 -7 356.17 21.11 0 15 -7 -0.21 13.04 0 -15 -7 -15.77 17.54 1 -15 -7 155.34 21.55 -1 -15 -7 148.29 19.6 -1 15 -7 176.35 16.89 1 15 -7 201.05 17.1 -2 15 -7 106.38 14.86 2 15 -7 117.64 14.82 2 -15 -7 88.84 19.79 2 15 -7 75.81 13.34 3 15 -7 276.86 18.92 3 -15 -7 340.62 27.51 -3 15 -7 308.06 20.47 3 15 -7 304.5 20.52 -4 15 -7 8.26 13.15 4 15 -7 -7.77 13.83 4 -15 -7 5.4 19.62 4 15 -7 4.48 12.46 5 15 -7 179.21 16.69 -5 15 -7 149.5 16.97 5 15 -7 161.76 15.58 5 -15 -7 177.92 23.88 -6 15 -7 48.68 14.89 6 15 -7 69.87 14.26 6 -15 -7 47.39 20.54 6 15 -7 67.34 13.5 7 15 -7 480.98 25.04 7 15 -7 472.63 24.39 7 -15 -7 457.88 32.32 -7 15 -7 444.95 26.28 8 15 -7 34.82 13.71 8 15 -7 28.95 12.88 0 17 -7 10.89 13.61 0 -17 -7 19.81 18.74 -1 17 -7 72.04 14.85 1 17 -7 78.38 14.79 1 -17 -7 58.5 19.79 -1 -17 -7 54.12 18.39 2 17 -7 332.92 21.77 2 -17 -7 390.98 29.31 -2 17 -7 380.69 22.92 2 17 -7 398.12 22.97 -3 17 -7 79.07 15.02 3 17 -7 85.34 15.42 3 -17 -7 76.76 21.74 3 17 -7 59.85 13.75 4 17 -7 28.86 14.59 4 -17 -7 34.23 21.13 4 17 -7 20.51 13.09 5 17 -7 15.41 12.83 0 0 -8 842.89 33.37 0 0 -8 855.95 34.33 1 0 -8 1.1 6.04 1 0 -8 -1.34 8.81 2 0 -8 142.17 9.83 2 0 -8 142.83 11.75 3 0 -8 4.16 6.26 3 0 -8 -2.93 8.87 4 0 -8 847.81 34.19 4 0 -8 878.27 34.87 5 0 -8 0.61 6.57 5 0 -8 4.31 8.93 6 0 -8 166.48 11.25 6 0 -8 190.54 12.99 7 0 -8 2.41 7 7 0 -8 9.71 9.3 8 0 -8 576.5 25.36 8 0 -8 610.69 26.07 9 0 -8 -2.23 7.45 9 0 -8 -1.16 10.18 10 0 -8 293.31 15.91 10 0 -8 304.62 17.32 11 0 -8 0.13 10.8 0 2 -8 3.77 5.7 0 -2 -8 4.4 6.16 0 2 -8 -4.72 9.07 -1 2 -8 376.12 17.58 1 2 -8 390.92 17.87 1 -2 -8 445.56 18.48 -1 2 -8 385.1 19.49 1 2 -8 394.54 19.64 2 2 -8 -0.67 5.96 2 -2 -8 0.92 6.15 2 2 -8 -0.79 9.41 3 2 -8 537.35 23.6 3 -2 -8 604.3 24.13 3 2 -8 552.81 25.01 3 -2 -8 541.91 29.22 4 2 -8 22.88 6.75 4 -2 -8 40.84 7.44 4 -2 -8 34.33 14.14 4 2 -8 27.78 9.6 5 2 -8 626.08 27.18 5 -2 -8 683.94 27.62 5 2 -8 681.39 28.62 5 -2 -8 659.37 32.62 6 2 -8 14.47 6.93 6 -2 -8 15.82 7.27 6 -2 -8 30.79 14.15 6 2 -8 31.86 9.81 7 2 -8 159.06 11.16 7 -2 -8 171.94 11.58 7 -2 -8 164.38 17.98 7 2 -8 183.27 13.25 7 -2 -8 183.11 12.81 8 2 -8 5.79 7.23 8 -2 -8 13.93 7.5 8 -2 -8 9.89 13.48 8 2 -8 29.96 10.26 8 -2 -8 -0.48 9.8 9 2 -8 728.75 31.38 9 -2 -8 763.06 31.49 9 2 -8 773.6 32.24 9 -2 -8 801.95 31.98 10 2 -8 17.2 7.96 10 -2 -8 13.57 7.66 10 2 -8 4.98 10.87 10 -2 -8 19.11 10.28 11 2 -8 49.28 11.62 11 -2 -8 60.1 11.59 12 -2 -8 27.78 11.38 0 4 -8 935.39 37.07 0 -4 -8 854.05 41.12 1 -4 -8 33.45 6.92 1 -4 -8 21.96 14.54 -1 -4 -8 13.28 13.4 1 4 -8 16.12 9.63 2 -4 -8 69.06 7.86 2 4 -8 46.78 6.88 2 -4 -8 71.07 15.37 2 4 -8 50.39 10.44 -2 -4 -8 31.27 13.77 3 -4 -8 68.79 7.98 3 4 -8 58.04 7.35 3 -4 -8 74.05 15.89 3 4 -8 65.37 10.79 -3 -4 -8 33.39 13.17 4 4 -8 773.03 33.53 4 -4 -8 908.67 34.21 4 4 -8 900.22 35.41 4 -4 -8 844.3 39.78 5 4 -8 106.14 9.29 5 -4 -8 123.3 9.85 5 4 -8 134.84 12.33 5 -4 -8 110.93 17.23 6 4 -8 79.27 8.74 6 -4 -8 90.86 9.13 6 4 -8 102.51 11.91 6 -4 -8 97.54 16.71 7 4 -8 12.62 7.23 7 -4 -8 21.35 7.42 7 -4 -8 28.77 15.53 7 4 -8 23.96 10.36 8 4 -8 508.06 23.57 8 -4 -8 558.11 23.91 8 -4 -8 523.97 30.02 8 4 -8 591.25 25.44 9 4 -8 52.2 8.57 9 -4 -8 65 8.68 9 -4 -8 63.82 15.91 9 4 -8 82.2 11.56 10 4 -8 143.68 11.4 10 -4 -8 161.14 11.43 10 4 -8 174.95 14.14 0 -6 -8 98 16.61 0 6 -8 96.63 11.92 1 6 -8 303.75 16.99 1 -6 -8 293.36 22.51 2 -6 -8 5.93 15.54 2 6 -8 -10.79 10.87 -2 -6 -8 -9.52 14.05 3 6 -8 275.52 15.88 3 -6 -8 269.64 21.77 4 6 -8 222.55 15.46 4 -6 -8 231.79 21.37 5 6 -8 453.85 22.32 5 -6 -8 423.66 27.6 6 6 -8 28.2 7.28 6 -6 -8 30.32 16.66 6 6 -8 40.84 11.22 7 6 -8 64.41 8.42 7 -6 -8 94.7 17.7 7 6 -8 89.91 11.84 8 6 -8 82.15 9.52 8 6 -8 130.53 12.94 8 -6 -8 102.88 18.39 9 6 -8 515.07 23.76 9 -6 -8 505.08 30.85 10 -6 -8 33.49 15.92 0 -8 -8 462.87 28.12 1 -8 -8 47.25 16.01 1 8 -8 57.38 11.35 -1 -8 -8 36.07 15.22 2 -8 -8 42.17 17.12 2 8 -8 36.03 11.1 -2 -8 -8 4.01 14.2 3 -8 -8 103.92 18.69 3 8 -8 100.11 12.68 4 8 -8 396.08 20.94 4 -8 -8 350.45 26.61 5 8 -8 300.13 18.1 5 -8 -8 275.52 24.13 6 -8 -8 56.91 18.57 6 8 -8 56.03 12.15 -7 8 -8 25.16 13.1 7 -8 -8 26.5 17.14 7 8 -8 40.36 12.2 8 -8 -8 381.08 27.65 -8 8 -8 339.09 22.44 9 -8 -8 185.83 21.86 -9 8 -8 156.05 16.25 -10 8 -8 110.1 15.38 0 -10 -8 137.62 19.19 1 -10 -8 209.96 22.46 -1 -10 -8 200.26 20.87 -2 10 -8 3.69 13.2 2 -10 -8 -2.16 16.97 2 10 -8 -0.52 11.24 -2 -10 -8 -13.67 14.87 -3 10 -8 120.96 15.95 3 -10 -8 98.29 19.76 3 10 -8 110.11 13.74 4 10 -8 384.21 20.93 4 -10 -8 330.99 27.06 -4 10 -8 341.53 22.66 5 10 -8 265.57 17.61 5 -10 -8 218 23.82 -5 10 -8 224.11 19.26 -6 10 -8 47.94 14.36 6 -10 -8 64.05 19.31 6 10 -8 45.4 12.31 -7 10 -8 64.56 14.93 7 -10 -8 68.68 19.84 7 10 -8 88.95 13.83 -8 10 -8 204.42 18.5 0 -12 -8 304.25 25.91 0 12 -8 394.29 22.94 1 -12 -8 145.26 20.89 1 12 -8 143.34 15.23 -1 -12 -8 130.51 19.77 -1 12 -8 183.59 17.55 -2 12 -8 13.52 13.85 2 12 -8 26.45 13.81 2 -12 -8 13.47 18.63 2 12 -8 -4.5 12.48 -2 -12 -8 10.14 15.07 -3 12 -8 116.48 16.48 3 -12 -8 130.85 21.72 3 12 -8 127.41 14.81 4 12 -8 194.1 16.72 4 -12 -8 186.82 23.57 -4 12 -8 193.22 18.62 5 -12 -8 260.77 25.89 -5 12 -8 272.34 20.79 -6 12 -8 3.94 15.07 0 14 -8 419.07 24.96 -1 14 -8 132.23 17.54 1 14 -8 150.43 17.16 -2 14 -8 8.06 14.48 2 14 -8 38.92 14.96 -3 14 -8 20.19 15.26 3 14 -8 10.52 15.48 4 14 -8 430.43 25.35 1 1 -9 123.1 9.89 2 1 -9 288.32 15.24 2 -1 -9 312.8 15.72 3 1 -9 163.07 11.44 3 -1 -9 180.16 11.75 4 1 -9 36.91 8.1 4 -1 -9 44.87 8.45 5 1 -9 39.98 8.36 5 -1 -9 52.65 8.63 5 1 -9 57.99 11.41 6 1 -9 379.82 20.05 7 1 -9 357.63 19.51 0 3 -9 -14.04 11.43 1 3 -9 192.1 11.77 -1 3 -9 186.47 14.47 1 3 -9 211.7 15.06 2 3 -9 215.03 13.12 2 -3 -9 271.2 14.24 2 3 -9 241.15 16.24 3 3 -9 249.19 14.2 3 -3 -9 283.92 14.86 3 3 -9 260.86 16.88 4 3 -9 6.69 7.19 4 -3 -9 18.16 8.1 4 3 -9 10.01 10.97 5 -3 -9 78.56 9.51 5 3 -9 69.5 9.04 5 3 -9 93.68 12.67 6 3 -9 212.66 15.54 0 5 -9 -6.76 11.38 1 5 -9 31.17 7.2 -1 5 -9 21.66 11.17 1 5 -9 27.65 11.86 2 5 -9 528.15 23.62 2 5 -9 603.42 26.66 3 -5 -9 75.58 9.34 3 5 -9 45.14 7.96 3 -5 -9 79 18.45 3 5 -9 51.04 12.22 4 5 -9 18.65 7.56 4 -5 -9 28.25 17.69 4 5 -9 40.41 12.2 5 -5 -9 13.84 17.7 6 -5 -9 510.81 31.17 0 -7 -9 9.22 16.29 0 7 -9 -5.23 11.94 -1 7 -9 228.52 16.36 1 7 -9 254.2 17.49 1 -7 -9 229.73 22.67 -1 -7 -9 187.29 20.73 2 -7 -9 20.07 17.64 -2 -7 -9 -4.62 15.37 2 7 -9 -8.61 12.63 3 -7 -9 293.09 25.17 4 -7 -9 49.82 18.75 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cl1 Bi1 Cl2 94.87(10) . . ? Cl1 Bi1 Cl3 90.38(9) . . ? Cl1 Bi1 Cl4 168.89(9) . 8_644 ? Cl1 Bi1 Cl4 85.77(9) . . ? Cl1 Bi1 Cl5 89.91(11) . . ? Cl2 Bi1 Cl3 86.38(11) . . ? Cl2 Bi1 Cl4 179.36(9) . . ? Cl2 Bi1 Cl4 96.18(8) . 8_644 ? Cl2 Bi1 Cl5 91.17(13) . . ? Cl3 Bi1 Cl4 89.13(8) . 8_644 ? Cl3 Bi1 Cl4 93.61(8) . . ? Cl3 Bi1 Cl5 177.56(10) . . ? Cl4 Bi1 Cl4 83.19(3) . 8_644 ? Cl5 Bi1 Cl4 88.83(11) . . ? Cl5 Bi1 Cl4 91.05(9) . 8_644 ? Bi1 Cl4 Bi1 148.34(11) . 8_645 ? H1A N1 H1B 109.5 . . ? H1A N1 H1C 109.5 . . ? H1B N1 H1C 109.5 . . ? C1 N1 H1A 109.5 . . ? C1 N1 H1B 109.5 . . ? C1 N1 H1C 109.5 . . ? H2A C2 H2B 109.5 . . ? H2A C2 H2C 109.5 . . ? H2B C2 H2C 109.5 . . ? C1 C2 H2A 109.5 . . ? C1 C2 H2B 109.5 . . ? C1 C2 H2C 109.5 . . ? N1 C1 C2 110.1(9) . . ? N1 C1 H1D 109.6 . . ? N1 C1 H1E 109.6 . . ? C2 C1 H1D 109.6 . . ? C2 C1 H1E 109.6 . . ? H1D C1 H1E 108.2 . . ? H4A C4 H4B 109.5 . . ? H4A C4 H4C 109.5 . . ? H4B C4 H4C 109.5 . . ? C3 C4 H4A 109.5 . . ? C3 C4 H4B 109.5 . . ? C3 C4 H4C 109.5 . . ? C4 C3 H3A 109.5 . . ? C4 C3 H3B 109.5 . . ? H3A C3 H3B 108.1 . . ? N2 C3 C4 110.6 . . ? N2 C3 H3A 109.5 . . ? N2 C3 H3B 109.5 . . ? C3 N2 H2D 109.5 . . ? C3 N2 H2E 109.5 . . ? C3 N2 H2F 109.5 . . ? H2D N2 H2E 109.5 . . ? H2D N2 H2F 109.5 . . ? H2E N2 H2F 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Bi1 Cl1 2.538(3) . ? Bi1 Cl2 2.593(3) . ? Bi1 Cl3 2.685(3) . ? Bi1 Cl4 2.842(3) . ? Bi1 Cl4 2.931(3) 8_644 ? Bi1 Cl5 2.715(3) . ? N1 H1A 0.8900 . ? N1 H1B 0.8900 . ? N1 H1C 0.8900 . ? N1 C1 1.465(13) . ? C2 H2A 0.9600 . ? C2 H2B 0.9600 . ? C2 H2C 0.9600 . ? C2 C1 1.534(15) . ? C1 H1D 0.9700 . ? C1 H1E 0.9700 . ? C4 H4A 0.9600 . ? C4 H4B 0.9600 . ? C4 H4C 0.9600 . ? C4 C3 1.5320 . ? C3 H3A 0.9700 . ? C3 H3B 0.9700 . ? C3 N2 1.5194 . ? N2 H2D 0.8900 . ? N2 H2E 0.8900 . ? N2 H2F 0.8900 . ?