#------------------------------------------------------------------------------ #$Date: 2023-12-04 20:10:40 +0200 (Mon, 04 Dec 2023) $ #$Revision: 288015 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/78/7247816.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7247816 loop_ _publ_author_name 'Li, Wen-Ze' 'Sheng, Yu-Shu' 'Zhang, Xiao-Sa' 'Liu, Yu' 'Li, Jing' 'Luan, Jian' _publ_section_title ; Fabrication of 5-R-isophthalic acid-modulated cadmium--organic coordination polymers and selectivity for the efficient detection of multiple analytes ; _journal_issue 43 _journal_name_full CrystEngComm _journal_page_first 6067 _journal_page_last 6079 _journal_paper_doi 10.1039/D3CE00899A _journal_volume 25 _journal_year 2023 _chemical_formula_moiety 'C23 H20 Cd N4 O7, 1.5(H2 O)' _chemical_formula_sum 'C23 H23 Cd N4 O8.5' _chemical_formula_weight 603.872 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _symmetry_Int_Tables_number 15 _audit_creation_date 2023-10-02 _audit_creation_method ; Olex2 1.5-dev (compiled 2023.09.29 svn.re1ec1418 for OlexSys, GUI svn.r6697) ; _audit_update_record ; 2023-10-02 deposited with the CCDC. 2023-10-05 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 105.530(1) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 27.3243(2) _cell_length_b 10.2895(1) _cell_length_c 17.8117(2) _cell_measurement_reflns_used 13484 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 68.15 _cell_measurement_theta_min 3.36 _cell_volume 4824.99(8) _computing_cell_refinement 'SAINT V8.38A (Bruker AXS Inc., 2017)' _computing_data_collection 'Bruker Instrument Service vV6.2.9' _computing_data_reduction 'SAINT V8.38A (Bruker AXS Inc., 2017)' _computing_molecular_graphics 'Olex2 1.5-dev (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5-dev (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine 1.5-dev (Bourhis et al., 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 0.9828 _diffrn_measured_fraction_theta_max 0.9785 _diffrn_measurement_device_type 'multiwire proportional' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0160 _diffrn_reflns_av_unetI/netI 0.0158 _diffrn_reflns_Laue_measured_fraction_full 0.9828 _diffrn_reflns_Laue_measured_fraction_max 0.9785 _diffrn_reflns_limit_h_max 32 _diffrn_reflns_limit_h_min -32 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 13484 _diffrn_reflns_point_group_measured_fraction_full 0.9828 _diffrn_reflns_point_group_measured_fraction_max 0.9785 _diffrn_reflns_theta_full 67.6786 _diffrn_reflns_theta_max 68.15 _diffrn_reflns_theta_min 3.36 _exptl_absorpt_coefficient_mu 7.768 _exptl_absorpt_correction_T_max 0.459 _exptl_absorpt_correction_T_min 0.417 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS _exptl_crystal_colour COLOURLESS _exptl_crystal_density_diffrn 1.663 _exptl_crystal_density_method 'not measured' _exptl_crystal_description BLOCK _exptl_crystal_F_000 2451.256 _exptl_crystal_size_max 0.13 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.1 _refine_diff_density_max 1.0890 _refine_diff_density_min -1.3558 _refine_diff_density_rms 0.1743 _refine_ls_d_res_high 0.8305 _refine_ls_d_res_low 13.1634 _refine_ls_extinction_coef 0.000083(7) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_goodness_of_fit_ref 0.9176 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_constraints 72 _refine_ls_number_parameters 531 _refine_ls_number_reflns 4324 _refine_ls_number_restraints 428 _refine_ls_restrained_S_all 0.8698 _refine_ls_R_factor_all 0.0579 _refine_ls_R_factor_gt 0.0576 _refine_ls_shift/su_max 0.0008 _refine_ls_shift/su_mean 0.0001 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0000P)^2^+235.3824P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1448 _refine_ls_wR_factor_ref 0.1449 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 31 _reflns_limit_h_min -32 _reflns_limit_k_max 12 _reflns_limit_k_min 0 _reflns_limit_l_max 21 _reflns_limit_l_min 0 _reflns_number_gt 4274 _reflns_number_total 4324 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL luan in C2/c CELL 1.54178 27.3243 10.2895 17.8117 90 105.53 90 ZERR 8 0.0002 0.0001 0.0002 0 0.001 0 LATT 7 SYMM -X,+Y,0.5-Z SFAC C H Cd N O UNIT 184 184 8 32 68 SADI N1 C1 N1A C1A SADI N2 C11 N2A C11A SADI N2 C15 N2A C15A SADI N1 C5 N1A C5A SADI C1 C2 C1A C2A SADI 0.04 N2 C12 N2A C12A SADI 0.04 N2 C14 N2A C14A RIGU C5 N1 C1 C2 C4 C3 C6 N3 O6 C7 C8 C9 N4 C10 O7 C14 C13 C15 C12 N2 C11 SADI C2 C3 C2A C3A RIGU C4A C10A N4A O7A C14A C9A C13A C15A C8A C12A N2A C7A C11A N3A C6A O6A = C5A C3A N1A C2A C1A SADI N3 C6 N3A C6A ISOR 0.005 0.01 N1 N1A N2 N2A SADI N3 C7 N3A C7A SADI C3 C4 C3A C4A SADI N4 C9 N4A C9A SADI N4 C10 N4A C10A SADI C4 C5 C4A C5A SADI C4 C6 C4A C6A SADI O6 C6 O6A C6A SADI C7 C8 C7A C8A SADI O7 C10 O7A C10A SADI C8 C9 C8A C9A SADI C10 C14 C10A C14A SADI C11 C12 C11A C12A SADI C12 C13 C12A C13A SADI C13 C14 C13A C14A SADI C14 C15 C14A C15A SADI 0.04 N1 C2 N1A C2A SADI 0.04 N1 C4 N1A C4A SADI 0.04 C1 C3 C1A C3A SADI 0.04 C1 C5 C1A C5A SADI 0.04 C2 C4 C2A C4A SADI 0.04 N3 C4 N3A C4A SADI 0.04 N3 O6 N3A O6A SADI 0.04 N3 C8 N3A C8A SADI 0.04 C3 C5 C3A C5A SADI 0.04 C3 C6 C3A C6A SADI 0.04 N4 O7 N4A O7A SADI 0.04 N4 C8 N4A C8A SADI 0.04 N4 C14 N4A C14A SADI 0.04 C4 O6 C4A O6A SADI 0.04 C5 C6 C5A C6A SADI 0.04 C6 C7 C6A C7A SADI 0.04 C7 C9 C7A C9A SADI 0.04 O7 C14 O7A C14A SADI 0.04 C9 C10 C9A C10A SADI 0.04 C10 C13 C10A C13A SADI 0.04 C10 C15 C10A C15A SADI 0.04 C11 C13 C11A C13A SADI 0.04 C11 C15 C11A C15A SADI 0.04 C12 C14 C12A C14A SADI 0.04 C13 C15 C13A C15A ISOR 0.05 0.01 N1 N1A L.S. 15 PLAN 5 TEMP 20(2) CONF CONN 8 $Cd BOND $H fmap 2 acta EXTI 0.000083 WGHT 0 235.382354 FVAR 0.039665 REM REM REM > REM REM > REM > REM REM Cd1 3 0.02004 0.86750 0.07930 11.00000 0.03496 0.01526 0.02614 = -0.00075 0.00167 -0.00242 O1 5 0.01953 0.63875 0.07312 11.00000 0.08891 0.02079 0.03137 = 0.00532 0.00692 0.01442 PART 1 N1 4 0.10322 0.90750 0.06619 10.50000 0.03628 0.03196 0.03823 = 0.00043 0.00794 -0.00014 C1 1 0.12321 0.85656 0.01008 10.50000 0.05187 0.08993 0.07588 = -0.04579 0.02875 -0.02793 AFIX 43 H1 2 0.10327 0.80305 -0.02815 10.50000 -1.20000 AFIX 0 PART 0 AFIX 6 O1W 5 0.42746 1.00426 0.51873 10.60000 0.05026 0.04204 0.03774 = 0.00102 0.01042 -0.00056 H1Wa 2 0.44360 1.02944 0.48665 10.60000 -1.50000 H1Wb 2 0.44914 0.96110 0.55272 10.60000 -1.50000 AFIX 0 O2 5 0.05311 0.72525 0.18607 11.00000 0.15082 0.01863 0.04026 = 0.00459 -0.03239 -0.01791 PART 1 N2 4 0.43509 0.64995 0.59223 10.50000 0.03238 0.02552 0.02818 = 0.00227 0.00862 0.00165 C2 1 0.17186 0.88289 0.00924 10.50000 0.04474 0.04689 0.06436 = -0.02005 0.01987 -0.01221 AFIX 43 H2 2 0.18387 0.85651 -0.03251 10.50000 -1.20000 AFIX 0 PART 0 AFIX 6 O2W 5 0.30072 0.79964 0.15170 10.90000 0.08069 0.08814 0.12595 = -0.00589 -0.01148 0.01896 H2Wa 2 0.30331 0.78544 0.19962 10.90000 -1.50000 H2Wb 2 0.32633 0.76177 0.14313 10.90000 -1.50000 AFIX 0 O3 5 0.03299 0.03526 0.16462 11.00000 0.05230 0.01257 0.03730 = -0.00182 0.00516 -0.00377 PART 1 N3 4 0.26543 1.07254 0.21233 10.50000 0.04351 0.04106 0.05125 = -0.00143 0.00934 -0.00775 AFIX 43 H3 2 0.27878 1.03166 0.18061 10.50000 -1.20000 AFIX 0 C3 1 0.20373 0.95033 0.07210 10.50000 0.04631 0.05350 0.06616 = -0.02292 0.01834 -0.01440 AFIX 43 H3a 2 0.23799 0.96068 0.07496 10.50000 -1.20000 AFIX 0 PART 0 O4 5 0.01041 0.14438 0.05475 11.00000 0.06054 0.03746 0.02249 = -0.00814 0.00065 -0.00331 PART 1 N4 4 0.32899 0.88760 0.43636 10.50000 0.03696 0.05973 0.05013 = 0.01594 -0.00616 -0.00654 AFIX 43 H4 2 0.36078 0.90607 0.44624 10.50000 -1.20000 AFIX 0 C4 1 0.18388 1.00194 0.13043 10.50000 0.03979 0.04919 0.05489 = -0.01245 0.00902 -0.00292 PART 0 O5 5 0.10389 0.34821 0.37220 11.00000 0.13044 0.02540 0.02117 = 0.00294 -0.01579 -0.00001 AFIX 147 H5 2 0.09434 0.40412 0.39789 11.00000 -1.50000 AFIX 0 PART 1 C5 1 0.13338 0.98054 0.12078 10.50000 0.03930 0.02631 0.04205 = 0.00165 0.00497 0.00171 AFIX 43 H5a 2 0.11858 1.02112 0.15591 10.50000 -1.20000 AFIX 0 O6 5 0.19401 1.12876 0.24235 10.50000 0.04972 0.13253 0.08693 = -0.06541 0.01699 -0.01571 C6 1 0.21529 1.07219 0.19970 10.50000 0.04328 0.05191 0.05116 = -0.01019 0.01017 -0.00865 C7 1 0.29877 1.14115 0.27928 10.50000 0.04121 0.03762 0.05638 = -0.00330 0.00707 -0.00262 AFIX 23 H7a 2 0.27868 1.20268 0.29967 10.50000 -1.20000 H7b 2 0.32404 1.18988 0.26177 10.50000 -1.20000 AFIX 0 O7 5 0.26842 0.76581 0.45645 10.50000 0.03889 0.10864 0.09814 = 0.05810 -0.01151 -0.01442 C8 1 0.32528 1.05017 0.34351 10.50000 0.04558 0.03261 0.05430 = -0.00490 0.00378 -0.00244 AFIX 23 H8a 2 0.34876 0.99675 0.32470 10.50000 -1.20000 H8b 2 0.34512 1.10141 0.38673 10.50000 -1.20000 AFIX 0 C9 1 0.28936 0.95916 0.37430 10.50000 0.04413 0.04614 0.04383 = 0.00355 -0.01034 -0.00906 AFIX 23 H9a 2 0.26608 1.00779 0.39624 10.50000 -1.20000 H9b 2 0.27037 0.90094 0.33415 10.50000 -1.20000 AFIX 0 C10 1 0.31230 0.79661 0.47392 10.50000 0.03738 0.04647 0.04397 = 0.00564 0.00242 0.00091 C11 1 0.41977 0.60666 0.65286 10.50000 0.04508 0.00875 0.03094 = -0.00476 0.01342 -0.00431 AFIX 43 H11 2 0.44300 0.56261 0.69239 10.50000 -1.20000 AFIX 0 C12 1 0.37177 0.62398 0.65951 10.50000 0.04605 0.09347 0.04615 = 0.02590 0.02195 0.01568 AFIX 43 H12 2 0.36263 0.59642 0.70361 10.50000 -1.20000 AFIX 0 C13 1 0.33744 0.68325 0.59919 10.50000 0.04597 0.07033 0.04747 = 0.01664 0.01414 0.00691 AFIX 43 H13 2 0.30407 0.69335 0.60160 10.50000 -1.20000 AFIX 0 C14 1 0.35089 0.72755 0.53608 10.50000 0.03435 0.03403 0.03386 = -0.00221 0.00566 0.00117 C15 1 0.40521 0.73460 0.54267 10.50000 0.03713 0.03313 0.03769 = 0.00838 0.00765 0.00340 AFIX 43 H15 2 0.41851 0.79428 0.51421 10.50000 -1.20000 AFIX 0 PART 0 C16 1 0.03981 0.62719 0.14617 11.00000 0.03623 0.02179 0.03461 = -0.00317 0.00246 0.00181 C17 1 0.04762 0.49611 0.17998 11.00000 0.04291 0.02477 0.02895 = -0.00272 0.00122 -0.00770 C18 1 0.03384 0.38286 0.13691 11.00000 0.03762 0.02256 0.02477 = 0.00523 0.00181 -0.00298 AFIX 43 H18 2 0.01822 0.38846 0.08377 11.00000 -1.20000 AFIX 0 C19 1 0.06597 0.25394 0.25022 11.00000 0.05717 0.02446 0.02492 = 0.00817 0.00134 -0.00522 AFIX 43 H19 2 0.07248 0.17279 0.27378 11.00000 -1.20000 AFIX 0 C20 1 0.07935 0.36502 0.29387 11.00000 0.08328 0.02525 0.02823 = -0.00439 -0.00508 -0.00267 C21 1 0.04291 0.26320 0.17153 11.00000 0.02975 0.01871 0.03181 = -0.00299 0.00548 -0.00885 C22 1 0.02728 0.13804 0.12697 11.00000 0.02972 0.02594 0.02988 = 0.00138 0.00783 -0.00149 C23 1 0.06991 0.48574 0.26089 11.00000 0.06818 0.01816 0.02511 = -0.00374 -0.01108 -0.00597 AFIX 43 H23 2 0.07809 0.56000 0.29145 11.00000 -1.20000 AFIX 0 PART 2 C10A 1 0.32948 0.88296 0.51394 10.50000 0.03047 0.03727 0.03812 = -0.00463 0.00120 0.00028 N1A 4 0.09932 0.90677 0.06523 10.50000 0.03628 0.03224 0.04030 = 0.00020 0.00815 0.00017 C1A 1 0.11501 0.84948 0.00718 10.50000 0.03499 0.02266 0.04394 = 0.00208 0.00655 0.00188 AFIX 43 H1A 2 0.09125 0.80058 -0.02894 10.50000 -1.20000 AFIX 0 C5A 1 0.13560 0.96753 0.11804 10.50000 0.03697 0.04618 0.05273 = -0.01127 0.00909 -0.00278 AFIX 43 H5Aa 2 0.12718 0.99838 0.16206 10.50000 -1.20000 AFIX 0 C2A 1 0.16249 0.85751 -0.00264 10.50000 0.04270 0.12580 0.07759 = -0.05527 0.02243 -0.02607 AFIX 43 H2A 2 0.17113 0.81503 -0.04337 10.50000 -1.20000 AFIX 0 C4A 1 0.18398 0.98907 0.11398 10.50000 0.03281 0.04013 0.04046 = 0.00174 0.00298 0.00148 C3A 1 0.19810 0.93320 0.05174 10.50000 0.03238 0.07557 0.05396 = -0.02004 0.00903 -0.00788 AFIX 43 H3Aa 2 0.23064 0.94566 0.04610 10.50000 -1.20000 AFIX 0 C6A 1 0.21728 1.07529 0.17212 10.50000 0.03636 0.03910 0.04056 = 0.00535 0.00141 -0.00037 N3A 4 0.26498 1.03436 0.20086 10.50000 0.03402 0.03827 0.04128 = 0.00816 0.00057 -0.00223 AFIX 43 H3Ab 2 0.27377 0.96255 0.18345 10.50000 -1.20000 AFIX 0 O6A 5 0.19872 1.17701 0.19078 10.50000 0.04201 0.05222 0.06770 = -0.01248 -0.00884 0.00778 C7A 1 0.30362 1.10541 0.26095 10.50000 0.03187 0.04540 0.05182 = -0.00004 -0.00291 0.00099 AFIX 23 H7Aa 2 0.32928 1.14014 0.23796 10.50000 -1.20000 H7Ab 2 0.28767 1.17777 0.28013 10.50000 -1.20000 AFIX 0 C8A 1 0.32880 1.01583 0.32890 10.50000 0.03558 0.05024 0.04998 = 0.00207 -0.00918 0.00037 AFIX 23 H8Aa 2 0.33793 0.93500 0.30809 10.50000 -1.20000 H8Ab 2 0.35992 1.05632 0.35909 10.50000 -1.20000 AFIX 0 C9A 1 0.29481 0.98442 0.38415 10.50000 0.04038 0.04929 0.04777 = 0.00051 -0.00816 -0.00239 AFIX 23 H9Aa 2 0.29268 1.06075 0.41508 10.50000 -1.20000 H9Ab 2 0.26076 0.96388 0.35306 10.50000 -1.20000 AFIX 0 N4A 4 0.31498 0.87222 0.43784 10.50000 0.04970 0.04649 0.03755 = -0.00475 -0.00089 0.00796 AFIX 43 H4A 2 0.31709 0.79729 0.41754 10.50000 -1.20000 AFIX 0 O7A 5 0.32072 0.97782 0.54968 10.50000 0.05772 0.04689 0.04703 = -0.01011 0.00208 0.01204 C14A 1 0.36018 0.77335 0.55869 10.50000 0.02954 0.03619 0.02795 = -0.00778 0.00101 -0.00100 C13A 1 0.34813 0.71341 0.61966 10.50000 0.04207 0.06583 0.04380 = 0.01201 0.01325 0.00938 AFIX 43 H13A 2 0.31786 0.73229 0.63183 10.50000 -1.20000 AFIX 0 C15A 1 0.40024 0.70856 0.53225 10.50000 0.03607 0.02919 0.03100 = 0.00375 0.00793 0.00106 AFIX 43 H15A 2 0.39944 0.71020 0.47973 10.50000 -1.20000 AFIX 0 C12A 1 0.38221 0.62307 0.66345 10.50000 0.04285 0.06553 0.03956 = 0.01327 0.01531 0.00933 AFIX 43 H12A 2 0.37437 0.58049 0.70480 10.50000 -1.20000 AFIX 0 N2A 4 0.43851 0.64616 0.58391 10.50000 0.03600 0.02957 0.03004 = 0.00422 0.00928 0.00178 C11A 1 0.42733 0.59644 0.64596 10.50000 0.04129 0.04075 0.03350 = 0.01062 0.01176 0.00330 AFIX 43 H11A 2 0.45070 0.54182 0.67874 10.50000 -1.20000 AFIX 0 HKLF 4 END Q1 1 0.020833 0.333333 0.083333 11 0.05 1.09 Q2 1 0.020833 0.972222 0.033333 11 0.05 0.78 Q4 1 0.041667 0.805556 0.15 11 0.05 0.71 Q3 1 0.052083 0.083333 0.266667 11 0.05 0.72 Q5 1 0.395833 0.638889 0.6 11 0.05 0.68 REM The information below was added by Olex2. REM REM R1 = 0.0576 for 4274 Fo > 4sig(Fo) and 0.0579 for all 4324 data REM 531 parameters refined using 428 restraints REM Highest difference peak 1.0890, deepest hole -1.3558 REM Mean Shift 0.0001, Max Shift 0.0008. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0579 REM R1_gt = 0.0576 REM wR_ref = 0.1449 REM GOOF = 0.9176 REM Shift_max = 0.0008 REM Shift_mean = 0.0001 REM Reflections_all = 4324 REM Reflections_gt = 4274 REM Parameters = 531 REM Hole = -1.3558 REM Peak = 1.0890 REM Flack = n/a ; _cod_data_source_file d3ce00899a2.cif _cod_data_source_block Cd_CP_4 _cod_database_code 7247816 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All N(H) groups At 1.5 times of: All O(H) groups, All O(H,H) groups 2. Restrained distances N1-C1 \\sim N1A-C1A with sigma of 0.02 N2-C11 \\sim N2A-C11A with sigma of 0.02 N2-C15 \\sim N2A-C15A with sigma of 0.02 N1-C5 \\sim N1A-C5A with sigma of 0.02 C1-C2 \\sim C1A-C2A with sigma of 0.02 N2-C12 \\sim N2A-C12A with sigma of 0.04 N2-C14 \\sim N2A-C14A with sigma of 0.04 C2-C3 \\sim C2A-C3A with sigma of 0.02 N3-C6 \\sim N3A-C6A with sigma of 0.02 N3-C7 \\sim N3A-C7A with sigma of 0.02 C3-C4 \\sim C3A-C4A with sigma of 0.02 N4-C9 \\sim N4A-C9A with sigma of 0.02 N4-C10 \\sim N4A-C10A with sigma of 0.02 C4-C5 \\sim C4A-C5A with sigma of 0.02 C4-C6 \\sim C4A-C6A with sigma of 0.02 O6-C6 \\sim O6A-C6A with sigma of 0.02 C7-C8 \\sim C7A-C8A with sigma of 0.02 O7-C10 \\sim O7A-C10A with sigma of 0.02 C8-C9 \\sim C8A-C9A with sigma of 0.02 C10-C14 \\sim C10A-C14A with sigma of 0.02 C11-C12 \\sim C11A-C12A with sigma of 0.02 C12-C13 \\sim C12A-C13A with sigma of 0.02 C13-C14 \\sim C13A-C14A with sigma of 0.02 C14-C15 \\sim C14A-C15A with sigma of 0.02 N1-C2 \\sim N1A-C2A with sigma of 0.04 N1-C4 \\sim N1A-C4A with sigma of 0.04 C1-C3 \\sim C1A-C3A with sigma of 0.04 C1-C5 \\sim C1A-C5A with sigma of 0.04 C2-C4 \\sim C2A-C4A with sigma of 0.04 N3-C4 \\sim N3A-C4A with sigma of 0.04 N3-O6 \\sim N3A-O6A with sigma of 0.04 N3-C8 \\sim N3A-C8A with sigma of 0.04 C3-C5 \\sim C3A-C5A with sigma of 0.04 C3-C6 \\sim C3A-C6A with sigma of 0.04 N4-O7 \\sim N4A-O7A with sigma of 0.04 N4-C8 \\sim N4A-C8A with sigma of 0.04 N4-C14 \\sim N4A-C14A with sigma of 0.04 C4-O6 \\sim C4A-O6A with sigma of 0.04 C5-C6 \\sim C5A-C6A with sigma of 0.04 C6-C7 \\sim C6A-C7A with sigma of 0.04 C7-C9 \\sim C7A-C9A with sigma of 0.04 O7-C14 \\sim O7A-C14A with sigma of 0.04 C9-C10 \\sim C9A-C10A with sigma of 0.04 C10-C13 \\sim C10A-C13A with sigma of 0.04 C10-C15 \\sim C10A-C15A with sigma of 0.04 C11-C13 \\sim C11A-C13A with sigma of 0.04 C11-C15 \\sim C11A-C15A with sigma of 0.04 C12-C14 \\sim C12A-C14A with sigma of 0.04 C13-C15 \\sim C13A-C15A with sigma of 0.04 3. Uiso/Uaniso restraints and constraints Uanis(N1) \\sim Ueq, Uanis(N1A) \\sim Ueq, Uanis(N2) \\sim Ueq, Uanis(N2A) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.01 Uanis(N1) \\sim Ueq, Uanis(N1A) \\sim Ueq: with sigma of 0.05 and sigma for terminal atoms of 0.01 4. Rigid body (RIGU) restrains C5, N1, C1, C2, C4, C3, C6, N3, O6, C7, C8, C9, N4, C10, O7, C14, C13, C15, C12, N2, C11 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C4A, C10A, N4A, O7A, C14A, C9A, C13A, C15A, C8A, C12A, N2A, C7A, C11A, N3A, C6A, O6A, C5A, C3A, N1A, C2A, C1A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 5. Others Fixed Sof: N1(0.5) C1(0.5) H1(0.5) O1W(0.6) H1Wa(0.6) H1Wb(0.6) N2(0.5) C2(0.5) H2(0.5) O2W(0.9) H2Wa(0.9) H2Wb(0.9) N3(0.5) H3(0.5) C3(0.5) H3a(0.5) N4(0.5) H4(0.5) C4(0.5) C5(0.5) H5a(0.5) O6(0.5) C6(0.5) C7(0.5) H7a(0.5) H7b(0.5) O7(0.5) C8(0.5) H8a(0.5) H8b(0.5) C9(0.5) H9a(0.5) H9b(0.5) C10(0.5) C11(0.5) H11(0.5) C12(0.5) H12(0.5) C13(0.5) H13(0.5) C14(0.5) C15(0.5) H15(0.5) C10A(0.5) N1A(0.5) C1A(0.5) H1A(0.5) C5A(0.5) H5Aa(0.5) C2A(0.5) H2A(0.5) C4A(0.5) C3A(0.5) H3Aa(0.5) C6A(0.5) N3A(0.5) H3Ab(0.5) O6A(0.5) C7A(0.5) H7Aa(0.5) H7Ab(0.5) C8A(0.5) H8Aa(0.5) H8Ab(0.5) C9A(0.5) H9Aa(0.5) H9Ab(0.5) N4A(0.5) H4A(0.5) O7A(0.5) C14A(0.5) C13A(0.5) H13A(0.5) C15A(0.5) H15A(0.5) C12A(0.5) H12A(0.5) N2A(0.5) C11A(0.5) H11A(0.5) 6.a Free rotating group: O1W(H1Wa,H1Wb), O2W(H2Wa,H2Wb) 6.b Secondary CH2 refined with riding coordinates: C7(H7a,H7b), C8(H8a,H8b), C9(H9a,H9b), C7A(H7Aa,H7Ab), C8A(H8Aa,H8Ab), C9A(H9Aa,H9Ab) 6.c Aromatic/amide H refined with riding coordinates: C1(H1), C2(H2), N3(H3), C3(H3a), N4(H4), C5(H5a), C11(H11), C12(H12), C13(H13), C15(H15), C18(H18), C19(H19), C23(H23), C1A(H1A), C5A(H5Aa), C2A(H2A), C3A(H3Aa), N3A(H3Ab), N4A(H4A), C13A(H13A), C15A(H15A), C12A(H12A), C11A(H11A) 6.d Idealised tetrahedral OH refined as rotating group: O5(H5) ; _iucr_refine_fcf_details ; data_Cd_CP_4_CCDC1 _computing_structure_refinement 'olex2.refine 1.5-dev (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,y,-z+1/2 3 -x,-y,-z 4 x,-y,z-1/2 5 x+1/2,y+1/2,z 6 -x+1/2,y+1/2,-z+1/2 7 -x+1/2,-y+1/2,-z 8 x+1/2,-y+1/2,z-1/2 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_H-M_alt 'C 1 2/c 1' _space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _symmetry_space_group_name_Hall '-C 2yc' _symmetry_Int_Tables_number 15 _cell_length_a 27.3243(2) _cell_length_b 10.2895(1) _cell_length_c 17.8117(2) _cell_angle_alpha 90 _cell_angle_beta 105.530(1) _cell_angle_gamma 90 _cell_volume 4824.99(8) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -32 0 2 3051.550 3227.660 94.931 14.204 o -32 0 4 1775.110 1512.140 69.597 30.137 o -32 0 6 1208.030 1152.660 66.425 39.245 o -32 0 8 7216.770 6046.570 266.024 6.834 o -32 0 10 447.331 497.351 44.278 90.855 o -32 2 3 1204.840 1114.200 88.569 39.069 o -32 2 4 46.026 60.876 9.487 765.464 o -32 2 5 2698.770 2419.830 57.657 19.272 o -32 2 6 7.503 9.487 13.417 4027.590 o -32 2 7 1076.410 1141.430 101.219 37.306 o -32 2 8 164.807 103.565 15.180 444.654 o -31 1 1 89.296 77.633 11.853 597.047 o -31 1 2 2307.330 2425.750 52.058 19.294 o -31 1 3 557.545 543.686 56.928 81.092 o -31 1 4 71.227 107.247 19.755 423.153 o -31 1 5 1541.240 1702.490 67.258 26.968 o -31 1 6 2178.770 2129.240 64.758 21.742 o -31 1 7 523.030 398.128 53.765 108.967 o -31 1 8 848.401 1068.060 33.625 43.861 o -31 1 9 44.333 210.831 16.755 221.803 o -31 1 10 286.187 354.307 20.848 131.922 o -31 1 11 2698.800 2314.220 53.790 20.179 o -31 1 12 163.249 162.837 17.890 284.224 o -31 3 1 7.981 63.248 13.417 725.713 o -31 3 2 2367.530 2156.920 136.049 19.829 o -31 3 3 340.965 468.536 41.114 96.883 o -31 3 4 114.119 127.763 17.890 359.948 o -31 3 5 551.547 569.921 31.309 81.472 o -31 3 6 397.563 557.524 47.439 80.999 o -31 3 7 276.518 250.457 41.113 174.353 o -31 3 8 2753.520 2138.050 107.580 20.750 o -31 3 9 865.296 676.869 44.281 67.547 o -30 0 2 3439.980 3385.750 113.913 13.366 o -30 0 4 370.229 383.116 33.321 119.434 o -30 0 6 1076.360 1521.700 53.677 30.474 o -30 0 8 6616.450 7281.710 183.626 6.161 o -30 0 10 59.310 784.276 50.599 58.233 o -30 0 12 1205.950 1284.220 63.262 35.544 o -30 2 1 4.006 51.306 13.489 887.083 o -30 2 2 93.706 69.255 11.099 669.117 o -30 2 3 1159.880 1151.860 88.564 37.901 o -30 2 4 21.950 191.270 37.949 226.858 o -30 2 5 3259.080 3275.640 87.172 14.075 o -30 2 6 27.856 211.442 34.786 209.626 o -30 2 7 261.068 337.703 19.637 138.570 o -30 2 8 91.070 37.949 11.574 1191.280 o -30 2 9 814.816 859.030 31.145 54.459 o -30 2 10 10.419 18.399 11.853 2352.330 o -30 2 11 2385.630 2540.240 88.587 17.979 o -30 2 12 3.668 12.649 10.525 3380.080 o -30 4 1 4.387 6.325 13.417 5505.600 o -30 4 2 4688.490 4121.170 265.890 9.451 o -30 4 3 47.738 62.357 15.180 727.052 o -30 4 4 102.194 135.908 28.462 324.631 o -30 4 5 238.406 269.420 24.295 171.367 o -30 4 6 3075.870 2333.330 158.212 17.879 o -30 4 7 106.267 151.797 31.624 288.542 o -29 1 1 4.113 100.236 13.969 463.181 o -29 1 2 2942.550 2705.670 136.048 16.130 o -29 1 3 1938.240 2211.520 94.901 20.406 o -29 1 4 3.070 0.000 17.889 11583.700 o -29 1 5 1178.530 1360.850 38.678 34.401 o -29 1 6 1511.200 1711.350 49.825 27.235 o -29 1 7 8.189 18.974 17.889 2060.330 o -29 1 8 650.956 847.606 40.255 54.683 o -29 1 9 472.596 1239.880 49.199 37.407 o -29 1 10 227.754 652.026 35.779 71.126 o -29 1 11 2591.800 2155.330 62.640 21.508 o -29 1 12 350.242 528.320 31.308 87.816 o -29 1 13 269.427 387.506 24.295 120.213 o -29 1 14 1126.970 1050.190 35.786 44.483 o -29 3 1 43.899 94.436 17.889 482.317 o -29 3 2 2828.150 2911.820 240.458 13.006 o -29 3 3 816.396 861.335 60.093 52.297 o -29 3 4 49.217 22.137 17.889 1803.400 o -29 3 5 1529.990 1326.650 53.681 34.789 o -29 3 6 2641.060 2709.320 281.577 12.756 o -29 3 7 454.493 371.635 63.252 112.173 o -29 3 8 1916.880 2009.840 60.271 23.084 o -29 3 9 524.043 661.738 35.781 70.016 o -29 3 10 57.681 56.923 25.299 728.792 o -29 3 11 947.696 826.276 104.377 49.134 o -29 3 12 1149.970 886.260 107.545 45.861 o -29 3 13 120.409 88.549 25.300 490.016 o -29 5 1 75.579 56.924 18.974 770.446 o -29 5 2 1036.980 942.584 56.935 48.211 o -29 5 3 2048.010 1847.570 75.928 24.697 o -29 5 4 219.301 227.700 31.625 197.320 o -29 5 5 2109.640 1790.630 75.928 25.446 o -29 5 7 549.627 461.756 37.953 98.763 o -29 5 8 689.882 531.352 44.279 85.205 o -29 5 9 1903.830 1524.870 69.600 29.890 o -29 5 10 3.825 25.299 18.974 1590.490 o -28 0 2 6006.230 5779.380 212.080 7.474 o -28 0 4 352.832 1122.780 53.670 41.001 o -28 0 6 11734.700 11906.100 272.465 3.698 o -28 0 8 8242.160 7257.630 196.323 6.128 o -28 0 10 440.452 683.121 56.927 65.556 o -28 0 12 1878.570 1695.570 82.248 26.624 o -28 0 14 1846.310 1676.640 69.596 27.291 o -28 2 1 31.302 316.766 63.248 129.289 o -28 2 2 18.879 31.624 17.889 1330.030 o -28 2 3 6732.720 6406.590 303.914 6.261 o -28 2 4 300.233 302.984 53.763 139.592 o -28 2 5 3108.360 2984.030 59.155 15.670 o -28 2 6 2.320 211.348 22.948 218.207 o -28 2 7 276.320 589.331 30.293 79.065 o -28 2 8 148.485 163.289 19.266 282.431 o -28 2 9 2832.750 2905.420 62.106 16.066 o -28 2 10 9.256 35.840 14.606 1232.870 o -28 2 11 3556.320 3572.440 65.768 13.086 o -28 2 12 86.540 55.116 15.571 813.633 o -28 2 13 68.984 79.253 14.117 580.233 o -28 2 14 1.959 98.093 12.685 475.146 o -28 2 15 1118.390 784.456 50.610 57.998 o -28 4 1 215.872 281.781 26.835 163.167 o -28 4 2 5141.070 4596.450 246.882 8.833 o -28 4 3 169.633 114.200 22.362 392.883 o -28 4 4 0.860 59.734 19.755 735.165 o -28 4 5 331.864 285.733 28.814 160.029 o -28 4 6 4929.070 4337.690 100.635 10.625 o -28 4 7 195.534 127.132 18.259 360.512 o -28 4 8 3021.490 3410.600 177.185 12.458 o -28 4 9 3.709 65.194 25.299 648.352 o -28 4 10 136.882 210.047 24.295 218.277 o -28 4 11 29.307 50.598 15.180 887.212 o -28 4 12 3317.240 3008.340 249.990 12.471 o -28 4 13 56.215 54.260 13.417 838.735 o -28 6 1 7.529 31.624 18.974 1312.540 o -28 6 2 150.885 132.824 25.300 336.356 o -28 6 3 3312.050 2791.100 94.935 16.327 o -28 6 5 1377.180 1309.580 63.265 34.871 o -28 6 6 181.201 126.499 25.300 351.847 o -28 6 7 57.791 56.923 18.974 771.141 o -28 6 8 614.303 499.719 37.953 91.517 o -28 6 9 1388.070 1233.700 56.940 37.205 o -27 1 1 976.167 724.682 50.606 62.585 o -27 1 2 5589.130 5698.580 231.053 7.443 o -27 1 3 5421.220 5766.670 183.571 7.664 o -27 1 4 126.513 196.887 26.834 230.462 o -27 1 5 3853.940 3838.090 107.585 11.910 o -27 1 6 5239.570 5299.480 123.432 8.643 o -27 1 7 37.966 49.625 16.755 892.229 o -27 1 8 1265.760 1460.010 47.480 31.886 o -27 1 9 2230.980 2515.620 60.806 18.525 o -27 1 10 13.712 374.876 31.306 122.824 o -27 1 11 3204.840 2964.840 80.542 15.571 o -27 1 12 1901.510 1742.000 77.038 26.101 o -27 1 13 16.385 33.732 14.606 1303.290 o -27 1 14 2229.100 2136.470 60.275 21.740 o -27 1 15 2384.110 2338.770 58.166 19.925 o -27 1 16 1.221 12.649 10.955 3353.740 o -27 3 1 1027.160 936.387 49.203 49.040 o -27 3 2 2101.400 2039.910 79.086 22.387 o -27 3 3 2021.530 1794.800 69.234 25.560 o -27 3 4 1366.110 1217.280 58.152 37.633 o -27 3 5 2529.850 2423.300 62.845 19.184 o -27 3 6 4100.640 4173.030 84.903 11.131 o -27 3 7 30.301 82.797 24.294 526.152 o -27 3 8 2942.060 3046.200 99.042 14.968 o -27 3 9 1967.300 1811.580 64.753 25.438 o -27 3 10 77.941 174.363 24.294 261.253 o -27 3 11 999.923 928.044 44.281 49.775 o -27 3 12 1782.340 1991.180 129.697 21.520 o -27 3 13 76.472 246.423 31.624 183.417 o -27 3 14 1785.060 1189.460 69.596 37.872 o -27 3 15 804.756 536.122 117.027 66.663 o -27 5 1 297.703 390.046 63.251 107.625 o -27 5 2 669.620 619.896 56.929 71.735 o -27 5 3 3785.870 3221.370 126.577 13.850 o -27 5 4 854.515 904.569 69.582 49.108 o -27 5 5 3981.810 3946.290 96.141 11.681 o -27 5 6 1437.220 1426.800 53.123 32.439 o -27 5 7 52.333 164.688 22.361 277.895 o -27 5 8 693.709 734.955 39.515 62.865 o -27 5 9 1705.440 1793.900 57.643 25.847 o -27 5 10 6.069 128.680 19.755 355.959 o -27 5 11 1612.480 1722.120 151.840 23.539 o -27 5 12 498.560 543.710 50.603 82.336 o -27 5 13 31.222 34.786 13.417 1279.690 o -27 7 5 721.193 670.527 44.280 68.203 o -27 7 6 4328.290 3722.460 107.622 12.264 o -26 0 2 10539.800 9831.810 259.732 4.444 o -26 0 4 3132.630 2974.050 126.555 14.931 o -26 0 6 25748.600 24515.600 469.867 1.743 o -26 0 8 7425.480 6984.130 202.622 6.325 o -26 0 10 997.784 955.184 69.583 46.651 o -26 0 12 4526.360 4892.550 151.903 9.155 o -26 0 14 2955.850 2794.330 351.199 10.865 o -26 0 16 546.974 1474.270 306.782 17.751 o -26 2 1 1919.730 1626.330 67.104 28.169 o -26 2 2 24.468 28.461 22.361 1361.980 o -26 2 3 10112.700 9806.600 127.055 4.745 o -26 2 4 592.770 493.699 35.781 92.968 o -26 2 5 7462.100 7189.500 114.509 6.455 o -26 2 6 216.962 330.815 25.562 140.034 o -26 2 7 442.813 700.259 35.169 66.334 o -26 2 8 175.169 110.654 19.266 410.432 o -26 2 9 5618.600 5599.970 86.050 8.339 o -26 2 10 0.026 10.985 13.260 3595.220 o -26 2 11 3424.750 3556.060 73.072 13.099 o -26 2 12 100.045 176.185 19.171 262.638 o -26 2 13 4.397 470.996 37.968 97.229 o -26 2 14 160.256 100.546 15.571 456.943 o -26 2 15 3491.590 3260.820 71.602 14.269 o -26 2 16 18.773 84.416 15.881 542.624 o -26 4 1 93.889 251.793 31.306 179.835 o -26 4 2 8370.890 8362.560 196.327 5.365 o -26 4 3 570.953 491.695 37.821 92.995 o -26 4 4 658.497 688.216 35.171 67.405 o -26 4 5 6.775 80.156 15.327 572.098 o -26 4 6 8249.820 7352.710 104.134 6.339 o -26 4 7 53.483 56.551 19.266 774.189 o -26 4 8 4678.610 4276.500 319.638 8.507 o -26 4 9 44.675 63.248 22.361 681.898 o -26 4 10 587.207 802.272 63.254 55.644 o -26 4 11 362.934 347.166 63.251 119.121 o -26 4 12 6274.280 5446.180 101.249 8.512 o -26 4 13 15.147 27.197 13.016 1617.980 o -26 4 14 2199.710 2218.560 55.793 21.017 o -26 4 15 287.938 200.135 22.138 229.574 o -26 6 1 637.443 664.174 50.604 68.095 o -26 6 2 110.336 88.548 19.756 506.876 o -26 6 3 8457.230 8023.190 291.367 5.217 o -26 6 4 236.125 379.500 44.275 117.413 o -26 6 5 2967.710 2967.830 113.904 15.149 o -26 6 6 1510.890 1347.520 75.917 33.381 o -26 6 7 111.819 974.346 44.274 47.601 o -26 6 8 170.585 207.194 25.300 220.410 o -26 6 9 3015.060 2599.190 85.431 17.623 o -26 6 10 0.216 6.325 13.417 5513.930 o -26 6 11 3085.230 2791.320 95.559 16.320 o -26 6 12 192.716 89.523 11.854 517.729 o -25 1 1 3096.020 2811.150 91.643 16.259 o -25 1 2 1977.710 2295.150 63.245 20.235 o -25 1 3 8429.120 8254.920 161.208 5.532 o -25 1 4 4767.010 4302.240 87.702 10.786 o -25 1 5 3095.160 2679.920 68.128 17.320 o -25 1 6 5766.290 5571.790 101.071 8.327 o -25 1 7 25.090 605.820 33.957 76.677 o -25 1 8 1049.290 1082.990 43.826 42.848 o -25 1 9 5291.360 4990.940 93.752 9.303 o -25 1 10 779.459 780.123 33.711 59.711 o -25 1 11 3871.190 3862.600 82.612 12.019 o -25 1 12 1678.860 1695.190 54.545 27.381 o -25 1 13 79.930 82.635 18.258 546.054 o -25 1 14 1976.780 2087.920 67.106 22.124 o -25 1 15 2401.060 2553.980 113.892 17.455 o -25 1 16 69.346 100.042 15.571 460.426 o -25 1 17 1015.840 1110.010 88.564 39.221 o -25 3 1 149.124 291.507 44.274 150.094 o -25 3 2 641.525 596.178 42.315 76.629 o -25 3 3 2123.640 2222.280 62.840 20.885 o -25 3 4 1269.690 1213.490 47.199 38.202 o -25 3 5 1952.440 1920.990 72.904 23.860 o -25 3 6 10368.300 9427.430 176.552 4.835 o -25 3 7 1392.700 1421.680 62.147 32.261 o -25 3 8 6066.530 6511.060 140.529 7.023 o -25 3 9 3465.940 3493.040 100.011 13.111 o -25 3 10 13.815 185.844 34.786 236.317 o -25 3 11 1035.430 1102.050 63.258 41.156 o 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261.030 o -24 2 11 4218.740 4987.500 83.171 9.357 o -24 2 12 203.392 348.759 23.079 133.605 o -24 2 13 1276.410 1303.020 55.202 35.363 o -24 2 14 46.748 99.704 19.266 454.963 o -24 2 15 4974.800 5274.670 105.115 8.769 o -24 2 16 19.601 11.500 11.853 3562.080 o -24 2 17 2605.550 2562.940 60.282 18.190 o -24 4 1 101.605 120.172 24.294 371.665 o -24 4 2 2776.830 3180.850 95.494 14.400 o -24 4 3 70.008 57.410 16.755 777.325 o -24 4 4 11223.500 10322.800 148.143 4.481 o -24 4 5 576.161 601.248 30.519 77.393 o -24 4 6 21391.600 20948.700 248.448 2.190 o -24 4 7 404.589 631.549 47.438 71.933 o -24 4 8 7692.890 8295.570 162.284 5.504 o -24 4 9 20.299 28.461 22.361 1362.490 o -24 4 10 5769.010 5930.660 130.634 7.724 o -24 4 11 8.366 215.437 28.813 210.490 o -24 4 12 11898.700 10579.700 294.667 4.066 o -24 4 13 15.096 60.085 22.361 715.256 o -24 4 14 2032.840 1869.330 132.867 22.652 o -24 4 15 419.552 385.839 30.361 119.297 o -24 4 16 12.760 21.685 15.179 1928.630 o -24 6 1 2866.050 3019.630 180.339 13.821 o -24 6 2 203.530 457.210 47.437 97.792 o -24 6 3 9912.370 9603.700 174.696 4.755 o -24 6 4 1458.960 1069.130 75.915 41.483 o -24 6 5 2949.050 2853.810 126.555 15.519 o -24 6 6 413.419 506.013 56.926 86.722 o -24 6 7 3097.980 3320.360 86.481 13.899 o -24 6 8 192.826 165.747 19.266 278.148 o -24 6 9 9083.510 8158.780 129.929 5.672 o -24 6 10 36.689 55.950 17.660 792.402 o -24 6 11 2955.000 2702.080 89.493 16.922 o -24 6 12 427.052 247.933 20.578 186.870 o -24 6 13 420.678 364.882 34.758 124.701 o -24 6 14 402.604 463.912 31.627 99.575 o -24 8 1 356.499 461.740 37.951 98.886 o -24 8 2 1531.220 1467.790 69.594 31.021 o -24 8 3 147.751 227.697 31.625 197.503 o -24 8 4 1951.920 2100.620 88.580 21.570 o -24 8 5 56.627 132.821 31.624 326.399 o -24 8 6 13957.000 13496.500 272.721 3.293 o -24 8 7 50.330 56.923 25.299 729.049 o -24 8 8 1571.040 1369.830 44.737 33.996 o -23 1 1 1799.930 1971.310 55.468 23.609 o -23 1 2 383.272 622.467 30.590 74.874 o -23 1 3 4709.500 4597.170 68.986 10.192 o -23 1 4 5717.770 5854.540 78.907 8.003 o -23 1 5 632.139 424.826 22.709 109.816 o -23 1 6 3697.680 5023.630 95.178 9.244 o -23 1 7 613.874 1040.930 35.407 44.948 o -23 1 8 1889.230 2244.110 62.095 20.703 o -23 1 9 13225.600 12208.400 164.571 3.786 o -23 1 10 119.850 1216.290 60.084 37.684 o -23 1 11 1191.540 1317.450 60.262 34.803 o -23 1 12 8851.460 8755.390 163.413 5.223 o -23 1 13 1181.800 1692.890 67.096 27.134 o -23 1 14 3050.160 3524.860 93.963 13.054 o -23 1 15 4142.190 3923.420 96.140 11.745 o -23 1 16 153.718 124.065 22.362 363.433 o -23 1 17 676.713 829.792 37.822 55.981 o -23 1 18 1404.420 1420.480 44.735 32.819 o -23 3 1 7644.130 7248.090 158.525 6.275 o -23 3 2 880.550 1031.940 44.619 44.895 o -23 3 3 3216.500 3197.050 95.501 14.325 o -23 3 4 3215.820 3290.480 132.885 13.501 o -23 3 5 2454.840 2469.770 84.652 18.530 o -23 3 6 12343.900 12236.700 213.815 3.708 o -23 3 7 616.583 1684.420 71.145 27.179 o -23 3 8 1249.030 1415.580 66.651 32.241 o -23 3 9 11116.300 10648.100 195.742 4.267 o -23 3 10 5959.710 5497.510 130.635 8.307 o -23 3 11 3240.790 3326.110 98.825 13.756 o -23 3 12 7549.660 7118.120 150.465 6.412 o -23 3 13 116.291 250.801 30.359 180.978 o -23 3 14 701.988 818.868 44.061 56.265 o -23 3 15 1832.030 1442.490 94.900 30.447 o -23 3 16 141.777 113.848 37.949 358.543 o -23 3 17 906.997 613.608 56.933 72.344 o -23 5 1 2915.200 3065.490 76.544 15.117 o -23 5 2 342.436 300.474 35.780 149.692 o -23 5 3 10295.700 10100.400 304.067 4.213 o -23 5 4 1046.790 1320.040 49.260 35.144 o -23 5 5 2931.010 2712.980 84.659 16.920 o -23 5 6 6688.800 6624.620 142.422 6.899 o -23 5 7 5698.430 5474.420 126.106 8.363 o -23 5 8 1233.070 1251.560 48.087 37.042 o -23 5 9 9501.650 8921.380 209.709 5.010 o -23 5 10 413.405 526.847 31.143 88.045 o -23 5 11 3971.540 3924.090 82.159 11.837 o -23 5 12 2467.740 2687.610 66.524 17.300 o -23 5 13 594.329 376.209 26.625 122.939 o -23 5 14 279.868 352.079 24.354 132.001 o -23 5 15 4033.760 3400.740 73.748 13.674 o -23 5 16 319.149 357.033 31.626 128.340 o -23 7 1 1835.060 2116.490 69.233 21.801 o -23 7 2 230.000 196.075 37.950 221.114 o -23 7 3 2343.290 2575.170 113.890 17.322 o -23 7 4 3651.150 4037.620 145.557 11.022 o -23 7 5 104.017 271.969 44.274 160.026 o -23 7 6 5685.700 5855.930 183.591 7.555 o -23 7 7 440.435 572.349 66.415 75.520 o -23 7 8 2345.490 2149.770 69.240 21.460 o -23 7 9 2164.260 2314.960 71.165 19.949 o -23 7 10 1272.750 1057.480 59.880 42.986 o -23 7 11 521.976 532.767 27.989 87.422 o -23 7 12 4918.930 4218.500 262.735 9.309 o -23 7 13 491.092 436.454 37.953 104.277 o -22 0 2 3156.170 2771.130 86.668 16.549 o -22 0 4 14997.800 15501.300 175.937 2.992 o -22 0 6 41471.600 43009.100 398.994 1.060 o -22 0 8 206.502 2130.130 78.946 21.529 o -22 0 10 10389.800 12067.700 291.399 3.615 o -22 0 12 21609.600 20781.600 418.804 2.068 o -22 0 14 3273.470 2986.790 126.559 14.870 o -22 0 16 1004.580 1151.290 75.909 38.754 o -22 0 18 7267.580 5725.320 152.000 7.885 o -22 2 1 8888.140 8923.430 110.304 5.233 o -22 2 2 452.407 500.106 31.116 92.610 o -22 2 3 10595.600 10200.900 113.259 4.584 o -22 2 4 30.835 238.466 19.375 195.550 o -22 2 5 1007.670 1242.770 35.865 37.705 o -22 2 6 356.252 450.672 21.017 104.042 o -22 2 7 7070.950 7381.150 84.572 6.357 o -22 2 8 233.609 145.664 15.828 318.124 o -22 2 9 21341.300 21584.600 218.361 2.145 o -22 2 10 1198.750 1405.930 48.608 33.057 o -22 2 11 3109.970 2688.670 68.129 17.265 o -22 2 12 16.394 199.992 24.149 229.340 o -22 2 13 3776.170 4180.210 102.922 11.003 o -22 2 14 0.867 24.596 19.755 1607.930 o -22 2 15 8485.500 8140.420 119.410 5.708 o -22 2 16 72.087 148.701 22.362 306.388 o -22 2 17 584.151 547.604 31.309 84.692 o -22 2 18 14.556 57.473 16.528 779.960 o -22 4 1 576.045 675.774 50.602 67.000 o -22 4 2 569.609 1090.610 39.057 42.804 o -22 4 3 2970.030 2847.480 64.253 16.364 o -22 4 4 11128.700 10440.200 158.813 4.415 o -22 4 5 254.568 329.567 32.641 138.347 o -22 4 6 18237.200 19762.100 244.652 2.318 o -22 4 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5087.670 4831.890 142.456 9.328 o -22 8 1 494.253 670.482 50.602 67.528 o -22 8 2 253.701 297.276 37.950 150.365 o -22 8 3 539.473 562.955 50.603 79.666 o -22 8 4 1511.340 1625.890 88.570 27.499 o -22 8 5 1562.230 1824.420 60.268 25.378 o -22 8 6 13279.300 14146.200 212.375 3.231 o -22 8 7 23.571 313.940 28.813 146.593 o -22 8 8 47.855 108.544 41.111 365.128 o -22 8 9 1248.980 1253.390 49.207 36.949 o -22 8 10 3068.660 3012.410 101.257 15.102 o -22 8 11 220.390 265.652 31.625 170.492 o -21 1 1 10068.300 10685.800 115.371 4.378 o -21 1 2 53.751 89.518 12.928 518.270 o -21 1 3 8917.140 9689.970 125.435 4.805 o -21 1 4 10320.100 11246.600 103.286 4.176 o -21 1 5 179.587 330.518 21.351 141.257 o -21 1 6 3568.010 4193.720 76.142 11.128 o -21 1 7 3190.520 3900.090 64.867 12.012 o -21 1 8 3148.550 3712.680 63.762 12.614 o -21 1 9 14654.600 13307.700 141.882 3.504 o -21 1 10 8445.870 8169.580 140.580 5.640 o -21 1 11 1772.040 1834.800 120.203 23.504 o -21 1 12 14008.300 14368.900 228.571 3.163 o -21 1 13 8784.670 8369.960 130.380 5.532 o -21 1 14 1030.620 1096.760 43.826 42.325 o -21 1 15 8881.490 8147.500 125.510 5.689 o -21 1 16 2381.710 2440.710 107.562 18.337 o -21 1 17 1048.650 1268.720 53.677 36.366 o -21 1 18 1789.690 1781.000 58.158 26.016 o -21 1 19 359.905 234.204 22.363 196.886 o -21 3 1 4995.900 4862.820 123.336 9.388 o -21 3 2 61.388 267.587 29.479 170.633 o -21 3 3 6430.000 6173.540 134.996 7.412 o -21 3 4 7765.010 8372.800 125.889 5.541 o -21 3 5 578.840 390.399 30.184 117.845 o -21 3 6 6295.790 6436.650 117.532 7.182 o -21 3 7 5564.070 5828.500 112.064 7.930 o -21 3 8 96.806 250.798 33.778 179.108 o -21 3 9 3622.710 3814.700 107.929 11.979 o -21 3 10 3694.100 4303.620 117.007 10.604 o -21 3 11 1729.200 2183.650 81.946 20.924 o -21 3 12 10109.700 9037.510 179.383 5.028 o -21 3 13 3419.020 3296.920 126.561 13.555 o -21 3 14 2363.840 2049.990 77.434 22.308 o -21 3 15 3915.400 3799.020 224.670 10.684 o -21 3 16 732.234 623.214 123.348 58.020 o -21 3 17 335.248 313.626 63.251 130.068 o -21 5 1 10033.500 9647.320 187.962 4.705 o -21 5 2 1649.890 1978.700 78.189 23.084 o -21 5 3 12218.200 11519.600 212.792 3.929 o -21 5 4 5427.910 5899.920 112.421 7.836 o -21 5 5 1539.000 2039.370 77.424 22.444 o -21 5 6 1083.860 1535.470 62.622 29.954 o -21 5 7 1831.370 1832.340 59.157 25.282 o -21 5 8 28.940 188.535 25.561 241.586 o -21 5 9 4342.610 4126.520 112.482 11.070 o -21 5 10 1029.370 1585.940 68.362 28.865 o -21 5 11 1617.960 1480.460 66.655 30.862 o -21 5 12 3089.920 3438.800 100.006 13.313 o -21 5 13 2229.570 1726.030 94.905 25.757 o -21 5 14 745.461 986.026 107.534 41.882 o -21 5 15 5627.440 5659.950 111.649 8.161 o -21 5 16 1050.420 1249.460 44.732 37.235 o -21 5 17 1032.770 1151.360 56.935 39.797 o -21 7 1 3752.960 3749.660 102.923 12.219 o -21 7 2 1110.960 1208.240 82.236 36.662 o -21 7 3 863.298 993.119 75.907 44.500 o -21 7 4 6730.510 6983.570 215.269 6.271 o -21 7 5 689.362 880.841 51.291 51.922 o -21 7 6 7133.310 6976.350 155.131 6.521 o 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170.910 8.486 o -20 0 18 4960.650 4431.140 139.264 10.146 o -20 2 1 15888.000 15237.800 150.197 3.063 o -20 2 2 66.452 84.390 12.557 549.443 o -20 2 3 10815.000 10573.400 107.577 4.433 o -20 2 4 163.173 266.244 17.025 175.963 o -20 2 5 793.855 1876.780 38.440 25.075 o -20 2 6 1399.300 1002.050 28.607 46.810 o -20 2 7 5810.590 5947.730 80.697 7.874 o -20 2 8 439.425 823.765 29.828 56.894 o -20 2 9 9698.790 9861.760 132.958 4.711 o -20 2 10 87.411 62.571 15.095 723.684 o -20 2 11 496.900 569.411 32.867 81.386 o -20 2 12 848.206 819.107 38.836 56.590 o -20 2 13 10308.400 10229.800 148.701 4.520 o -20 2 14 372.758 519.984 31.501 89.150 o -20 2 15 11417.700 11700.100 158.489 3.954 o -20 2 16 284.876 559.406 46.876 80.880 o -20 2 17 340.570 354.883 25.563 130.637 o -20 2 18 288.353 145.752 22.363 310.947 o -20 2 19 2635.850 2566.140 62.645 18.142 o -20 4 1 200.010 158.579 21.284 288.426 o -20 4 2 21.759 155.126 17.171 299.371 o -20 4 3 217.533 604.730 31.777 76.968 o -20 4 4 20378.000 19639.300 215.347 2.352 o -20 4 5 1018.230 1153.710 49.356 40.063 o -20 4 6 10162.600 10209.800 145.164 4.535 o -20 4 7 33.111 242.487 26.575 189.127 o -20 4 8 677.933 1457.320 79.602 30.895 o -20 4 9 1065.460 1372.140 101.212 31.592 o -20 4 10 12089.600 11601.900 497.404 3.221 o -20 4 11 511.130 898.183 54.710 50.734 o -20 4 12 8103.840 7940.430 224.807 5.533 o -20 4 13 19.921 64.829 25.733 648.619 o -20 4 14 695.662 619.278 94.882 64.603 o -20 4 15 886.553 837.008 43.715 55.074 o -20 4 16 1557.720 2214.650 158.160 18.743 o -20 4 17 4.215 18.974 18.974 2016.680 o -20 4 18 5843.820 5547.070 139.310 8.196 o -20 6 1 22892.200 22352.800 327.521 2.007 o -20 6 2 2161.610 2049.970 80.527 22.248 o -20 6 3 10996.100 10833.400 291.425 3.988 o -20 6 4 325.491 303.603 50.600 141.053 o -20 6 5 404.857 1759.720 71.142 26.067 o -20 6 6 2689.130 2589.770 89.147 17.634 o -20 6 7 3473.030 3300.940 79.712 14.033 o -20 6 8 654.128 591.800 36.154 77.951 o -20 6 9 4627.890 4637.590 95.369 9.987 o -20 6 10 494.313 332.352 27.830 138.429 o -20 6 11 913.229 826.515 39.841 56.017 o -20 6 12 923.770 729.816 45.286 62.714 o -20 6 13 3701.090 3781.180 93.656 12.194 o -20 6 14 72.318 610.493 35.779 75.889 o -20 6 15 6717.770 6226.390 114.119 7.429 o -20 6 16 46.256 139.433 17.889 331.238 o -20 8 1 556.401 759.038 63.253 58.613 o -20 8 2 1077.150 1606.770 88.562 27.826 o -20 8 3 497.225 477.430 37.952 95.680 o -20 8 4 11241.900 10349.200 181.417 4.413 o -20 8 5 2439.290 2178.210 98.073 20.619 o -20 8 6 10885.700 10090.800 179.043 4.526 o -20 8 7 80.947 158.121 26.834 283.964 o -20 8 8 197.138 252.998 28.814 180.105 o -20 8 9 1797.850 1784.130 88.574 25.185 o -20 8 10 5164.800 5564.580 158.265 8.072 o -20 8 11 33.902 101.197 25.299 434.621 o -20 8 12 4345.450 4095.660 120.274 11.092 o -19 1 1 11858.000 12412.900 120.804 3.773 o -19 1 2 973.064 1078.010 29.913 43.568 o -19 1 3 8918.670 8322.330 86.083 5.644 o -19 1 4 26393.700 26603.600 187.622 1.762 o -19 1 5 16.877 41.928 11.128 1092.360 o -19 1 6 5772.130 5704.010 77.823 8.214 o -19 1 7 5705.540 6286.120 86.258 7.444 o -19 1 8 2004.110 2260.590 50.393 20.704 o -19 1 9 8986.470 9721.600 114.685 4.805 o -19 1 10 753.067 858.661 37.937 54.121 o -19 1 11 302.586 473.130 24.766 98.754 o -19 1 12 3639.680 3370.560 62.417 13.875 o -19 1 13 3317.870 3628.280 81.540 12.787 o -19 1 14 73.967 111.187 20.461 407.527 o -19 1 15 5181.750 4532.910 98.282 10.193 o -19 1 16 2475.030 3230.150 75.435 14.380 o -19 1 17 321.562 378.201 26.624 122.573 o -19 1 18 2498.660 2354.900 71.587 19.607 o -19 1 19 1887.100 1591.390 53.686 29.132 o -19 1 20 216.950 151.801 17.890 303.955 o -19 3 1 4474.690 4962.330 141.678 9.100 o -19 3 2 1457.650 1438.670 47.347 32.340 o -19 3 3 5061.770 5803.620 95.436 8.024 o -19 3 4 8572.620 8632.020 116.483 5.396 o -19 3 5 411.175 454.741 26.599 102.333 o -19 3 6 8252.360 8679.200 126.838 5.348 o -19 3 7 1749.400 2414.030 63.919 19.259 o -19 3 8 664.169 641.450 39.962 71.682 o -19 3 9 1131.900 940.403 58.421 48.194 o 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68.141 12.865 o -19 5 17 158.285 89.203 22.137 495.879 o -19 7 1 2242.570 1866.440 107.558 23.549 o -19 7 2 436.014 512.338 56.926 85.723 o -19 7 3 1130.380 1303.400 62.623 35.073 o -19 7 4 14531.100 14375.100 326.449 3.022 o -19 7 5 1122.040 1506.090 66.649 30.386 o -19 7 6 7867.740 8119.330 167.510 5.604 o -19 7 7 1689.960 2144.650 142.344 19.757 o -19 7 8 16.932 25.299 19.755 1568.040 o -19 7 9 991.435 998.192 43.521 46.412 o -19 7 10 4265.100 4054.520 132.910 11.091 o -19 7 11 236.888 610.771 40.252 75.273 o -19 7 12 4932.630 4363.450 81.567 10.670 o -19 7 13 1802.040 1815.420 48.615 25.715 o -19 7 14 93.716 152.979 16.755 303.387 o -19 7 15 2472.360 2283.170 66.444 20.284 o -19 9 1 8378.450 7689.570 202.690 5.783 o -19 9 2 2286.070 2170.250 101.236 20.623 o -19 9 3 8194.230 7575.160 202.680 5.865 o -19 9 4 1408.720 1895.690 75.915 24.116 o -19 9 5 145.193 123.169 22.362 366.013 o -19 9 6 428.401 695.774 56.927 64.437 o -19 9 7 5192.730 5039.210 151.936 8.902 o -19 9 8 139.303 847.537 56.924 53.506 o -19 9 9 7373.140 6419.930 126.674 7.169 o -19 9 10 874.637 650.268 34.792 71.202 o -18 0 2 2310.520 2645.150 66.820 17.571 o -18 0 4 102910.000 105215.000 917.765 0.417 o -18 0 6 17271.600 16529.600 208.017 2.785 o -18 0 8 2533.690 2428.860 77.532 18.940 o -18 0 10 3420.270 3127.350 73.456 14.847 o -18 0 12 3705.340 4793.030 156.039 9.307 o -18 0 14 1850.020 2461.280 91.735 18.488 o -18 0 16 5062.590 4517.040 111.894 10.149 o -18 0 18 7173.060 7003.510 189.969 6.364 o -18 0 20 330.655 524.989 44.276 86.357 o -18 2 1 22039.400 22703.000 180.938 2.060 o -18 2 2 2348.030 2246.740 41.159 20.920 o -18 2 3 13814.700 12982.800 170.659 3.560 o -18 2 4 1204.200 1262.930 28.697 37.268 o -18 2 5 289.865 532.553 21.226 88.261 o -18 2 6 3592.080 2890.310 65.435 16.107 o -18 2 7 9386.010 9395.220 115.661 4.967 o -18 2 8 2896.070 3474.010 66.018 13.454 o -18 2 9 5322.830 6070.440 97.438 7.672 o -18 2 10 73.957 205.454 22.327 224.413 o -18 2 11 331.129 479.309 27.065 97.183 o 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12.864 o -18 4 17 41.403 50.598 17.889 868.028 o -18 4 18 12117.700 11646.200 814.576 2.366 o -18 4 19 319.108 297.283 31.626 152.990 o -18 6 1 8234.510 8193.690 281.804 5.160 o -18 6 2 1401.680 2024.350 113.870 21.688 o -18 6 3 7192.200 6654.720 149.535 6.842 o -18 6 4 1040.490 1519.100 69.223 30.055 o -18 6 5 1392.100 1336.690 66.652 34.051 o -18 6 6 290.927 836.726 51.288 54.621 o -18 6 7 7151.290 6716.530 121.703 6.876 o -18 6 8 0.897 37.204 19.265 1134.170 o -18 6 9 6415.280 6637.770 122.080 6.956 o -18 6 10 1699.780 1592.060 56.656 29.053 o -18 6 11 77.097 118.474 22.948 379.334 o -18 6 12 1115.000 1104.090 53.677 41.590 o -18 6 13 9358.000 9423.540 370.551 4.252 o -18 6 14 142.374 253.154 26.834 181.080 o -18 6 15 6360.150 5625.350 91.391 8.283 o -18 6 16 248.261 161.376 16.755 287.140 o -18 6 17 36.220 269.734 22.361 172.275 o -18 8 1 390.991 686.439 66.414 63.957 o -18 8 2 1169.880 1206.720 75.911 37.066 o -18 8 3 139.472 168.146 26.834 267.662 o -18 8 4 22988.800 23479.600 533.187 1.757 o -18 8 5 607.635 828.422 69.579 53.339 o -18 8 6 9465.560 9144.880 316.709 4.558 o -18 8 7 1108.130 1066.420 51.294 43.132 o -18 8 8 2605.040 2075.870 71.586 22.148 o -18 8 9 1603.690 1692.540 64.749 27.183 o -18 8 10 7073.580 7265.600 136.511 6.331 o -18 8 11 3.348 16.264 15.179 2475.430 o -18 8 12 3395.770 3373.240 104.423 13.515 o -18 8 13 778.101 617.276 25.565 75.783 o -18 8 14 836.811 891.950 50.607 51.328 o -18 10 1 9212.880 8325.000 332.665 4.881 o -18 10 2 62.310 196.069 31.624 227.630 o -18 10 5 603.548 600.923 44.279 75.800 o -18 10 6 1971.020 1607.130 69.600 28.418 o -17 1 1 10695.700 11212.300 105.137 4.187 o -17 1 2 10443.200 10634.400 90.786 4.426 o -17 1 3 9327.980 8593.690 102.523 5.443 o -17 1 4 10319.800 11265.400 110.162 4.163 o -17 1 5 2097.070 3869.990 102.280 11.871 o -17 1 6 3303.530 3577.840 62.554 13.088 o -17 1 7 16398.000 15887.200 149.019 2.942 o -17 1 8 741.400 2081.490 64.534 22.271 o -17 1 9 4040.800 4105.070 60.870 11.434 o -17 1 10 1830.540 2494.850 48.093 18.815 o -17 1 11 153.097 230.015 17.841 202.889 o -17 1 12 2398.560 2844.120 52.911 16.488 o -17 1 13 3427.580 3373.600 59.463 13.884 o -17 1 14 30.236 7.906 12.649 4735.400 o -17 1 15 714.850 1292.490 53.179 35.761 o -17 1 16 2138.630 2609.380 69.403 17.779 o -17 1 17 147.445 141.519 21.910 321.286 o -17 1 18 2597.800 2513.560 62.104 18.518 o -17 1 19 3850.470 3864.630 89.506 11.968 o -17 1 20 2.694 32.527 15.812 1331.660 o -17 3 1 1852.180 2177.950 73.546 21.130 o -17 3 2 1416.870 1098.120 37.311 42.487 o -17 3 3 3499.400 3902.750 70.400 11.973 o -17 3 4 17554.000 16683.300 203.485 2.764 o -17 3 5 471.865 1575.370 42.151 29.754 o -17 3 6 14424.800 15485.600 204.509 2.969 o -17 3 7 15474.600 15893.700 320.554 2.765 o -17 3 8 3293.940 3162.190 164.531 13.531 o -17 3 9 4095.310 4280.420 156.631 10.336 o -17 3 10 15189.200 15694.800 329.470 2.785 o -17 3 11 39.507 423.336 34.099 108.568 o -17 3 12 2956.750 3083.260 104.189 14.734 o -17 3 13 2413.120 2872.490 120.214 15.533 o -17 3 14 193.569 189.748 37.950 227.933 o -17 3 15 3246.550 3429.720 132.886 12.988 o -17 3 16 2733.480 3030.850 126.549 14.675 o -17 3 17 1.186 221.366 37.949 198.449 o -17 3 18 1688.880 1979.290 67.104 23.310 o -17 3 19 1756.730 1400.860 145.518 28.380 o -17 5 1 11434.300 10701.400 162.845 4.304 o -17 5 2 927.871 1765.430 125.085 24.177 o -17 5 3 8134.050 8048.630 151.999 5.693 o -17 5 4 9286.290 9776.370 152.304 4.718 o -17 5 5 5093.380 4818.180 81.344 9.683 o -17 5 6 3073.570 3521.560 107.904 12.938 o -17 5 7 14954.200 14782.700 220.685 3.087 o -17 5 8 1226.290 1196.450 66.642 37.863 o -17 5 9 8198.570 8444.000 183.455 5.354 o -17 5 10 4629.160 5645.650 215.193 7.616 o -17 5 11 184.670 128.705 25.734 345.460 o -17 5 12 2274.630 2359.200 89.141 19.289 o -17 5 13 6976.930 6445.870 136.128 7.106 o -17 5 14 74.800 117.095 22.362 384.629 o -17 5 15 6817.070 7056.950 138.576 6.505 o -17 5 16 2154.460 2282.660 284.716 14.308 o -17 5 17 1069.010 994.157 42.318 46.647 o -17 5 18 156.337 240.514 22.362 192.363 o -17 7 1 5253.340 5639.370 134.052 8.092 o -17 7 2 5504.640 5122.260 127.507 8.907 o -17 7 3 2340.190 2747.690 91.632 16.631 o -17 7 4 12147.800 11198.500 208.019 4.044 o -17 7 5 31.321 1025.850 104.359 40.835 o -17 7 6 5892.820 6002.100 115.256 7.695 o -17 7 7 2575.380 3203.060 81.357 14.445 o -17 7 8 804.428 862.591 42.499 53.585 o -17 7 9 1239.880 1179.590 47.199 39.274 o -17 7 10 5942.610 5841.070 129.777 7.841 o -17 7 11 11.702 127.760 22.361 354.624 o -17 7 12 5110.880 4307.660 107.423 10.652 o -17 7 13 1233.200 1306.520 53.678 35.331 o -17 7 14 77.221 133.123 22.362 340.501 o -17 7 15 408.094 303.611 26.836 151.521 o -17 7 16 3107.940 2690.740 62.653 17.313 o -17 9 1 11049.800 10245.700 253.450 4.295 o -17 9 2 634.759 936.159 69.579 47.589 o -17 9 3 2058.740 2207.020 59.590 21.075 o -17 9 4 106.080 335.539 25.562 138.251 o -17 9 5 136.665 509.543 37.818 90.087 o -17 9 6 1036.400 1198.520 53.770 38.424 o -17 9 7 10955.800 10261.500 281.971 4.215 o -17 9 8 8.276 1460.120 55.769 31.728 o -17 9 9 5134.260 4647.530 100.643 9.938 o -17 9 10 1073.490 882.488 40.258 52.504 o -17 9 11 103.020 127.762 17.889 360.042 o -17 9 12 172.096 259.324 31.625 174.541 o -16 0 2 5601.660 7040.010 110.682 6.604 o -16 0 4 114108.000 111918.000 843.647 0.401 o -16 0 6 3324.830 7024.010 219.228 6.225 o -16 0 8 17354.500 18245.600 198.888 2.538 o -16 0 10 16391.300 19038.800 235.210 2.410 o -16 0 12 4563.810 4102.810 110.762 11.143 o -16 0 14 420.689 1790.040 71.561 25.630 o -16 0 16 9593.410 7904.990 161.518 5.764 o -16 0 18 4995.560 4538.500 151.916 9.821 o -16 0 20 89.571 208.720 31.624 214.561 o -16 2 1 12191.200 10878.300 96.043 4.322 o -16 2 2 3523.460 3715.870 50.124 12.668 o -16 2 3 3809.080 3865.530 48.316 12.188 o -16 2 4 85.044 537.185 18.733 87.816 o -16 2 5 9345.460 10718.400 111.620 4.371 o -16 2 6 241.064 438.265 26.116 106.292 o -16 2 7 23481.300 24051.000 290.562 1.896 o -16 2 8 469.129 1250.910 39.106 37.418 o -16 2 9 9072.420 8750.950 128.426 5.302 o -16 2 10 365.739 652.816 26.979 71.755 o -16 2 11 3303.470 3539.130 63.956 13.220 o -16 2 12 976.200 1308.730 39.807 35.732 o -16 2 13 6755.520 7496.350 129.128 6.162 o -16 2 14 1085.110 1707.870 56.637 27.163 o -16 2 15 1267.120 1159.780 46.163 39.965 o -16 2 16 186.273 91.316 20.461 489.323 o -16 2 17 496.608 402.707 29.215 114.632 o -16 2 18 91.664 104.613 18.258 435.942 o -16 2 19 6980.720 6400.710 97.450 7.281 o -16 2 20 3.387 22.137 13.417 1946.230 o -16 4 1 1932.090 3404.630 80.095 13.630 o -16 4 2 19179.300 19652.600 193.623 2.365 o -16 4 3 157.989 314.079 27.020 146.923 o -16 4 4 37111.900 37304.200 391.983 1.216 o -16 4 5 959.748 1044.140 40.704 44.553 o -16 4 6 19519.400 21607.900 266.597 2.115 o -16 4 7 442.317 544.433 40.505 83.966 o -16 4 8 10236.100 10975.800 179.488 4.174 o -16 4 9 126.178 159.527 39.511 264.521 o -16 4 10 23864.000 22548.600 584.029 1.771 o -16 4 11 66.232 211.695 34.947 209.151 o -16 4 12 2683.560 2719.820 98.074 16.697 o -16 4 13 1006.860 1097.270 55.778 41.743 o -16 4 14 620.068 689.520 44.727 66.374 o -16 4 15 53.576 213.744 28.813 211.946 o -16 4 16 1593.790 4144.690 253.054 9.579 o -16 4 17 697.259 595.671 40.255 76.941 o -16 4 18 11638.900 10920.500 703.500 2.759 o -16 4 19 118.402 115.254 17.890 397.516 o -16 6 1 12712.300 11465.000 162.341 4.027 o -16 6 2 6144.630 5909.780 108.142 7.837 o -16 6 3 1123.780 1417.350 55.441 32.597 o -16 6 4 4262.560 4644.720 101.834 9.940 o -16 6 5 3908.550 4277.050 98.501 10.790 o -16 6 6 782.989 1182.590 54.084 38.934 o -16 6 7 16254.400 15876.600 184.355 2.916 o -16 6 8 446.564 582.321 37.623 79.080 o -16 6 9 5481.490 5127.850 109.290 8.991 o -16 6 10 1689.030 1853.710 76.048 24.626 o -16 6 11 1058.690 1616.240 71.568 28.246 o -16 6 12 2473.830 2093.150 78.199 21.847 o -16 6 13 7663.790 7370.660 152.239 6.195 o -16 6 14 189.839 206.091 22.948 222.987 o -16 6 15 2012.890 1866.720 85.413 24.210 o -16 6 16 156.567 112.808 19.756 402.312 o -16 6 17 496.813 403.329 28.815 114.545 o -16 8 1 858.161 1021.340 55.777 44.740 o -16 8 2 1234.740 1960.820 70.130 23.475 o -16 8 3 304.877 1046.210 64.989 43.217 o -16 8 4 28280.400 28258.200 406.682 1.569 o -16 8 5 770.034 1839.190 60.792 25.198 o -16 8 6 1024.250 1955.960 76.041 23.410 o -16 8 7 384.843 612.937 42.313 74.707 o -16 8 8 3224.080 3011.030 91.646 15.219 o -16 8 9 1179.260 1212.730 55.780 37.890 o -16 8 10 8062.830 7227.420 145.486 6.334 o -16 8 11 173.151 287.819 31.307 158.159 o -16 8 12 2416.540 2438.880 58.450 19.119 o -16 8 13 766.247 767.962 44.279 59.836 o -16 8 14 26.496 153.057 19.755 300.946 o -16 10 1 6605.260 6337.730 120.647 7.280 o -16 10 2 2681.510 2562.750 101.245 17.619 o -16 10 3 1193.450 1113.390 63.261 40.741 o -16 10 4 4344.860 4013.020 126.594 11.255 o -16 10 5 2114.680 2568.830 101.235 17.590 o -16 10 6 267.134 759.007 50.600 60.044 o -16 10 7 5268.150 5157.610 145.615 8.748 o -16 10 8 363.476 404.813 28.815 114.249 o -16 10 9 2764.460 3163.010 79.105 14.644 o -15 1 1 19082.000 17277.700 186.740 2.686 o -15 1 2 9186.010 10865.200 182.841 4.211 o -15 1 3 316.587 305.487 25.992 151.029 o -15 1 4 2273.760 1887.300 82.683 24.023 o -15 1 5 1389.220 1768.510 84.996 25.520 o -15 1 6 10249.100 13389.700 125.714 3.500 o -15 1 7 30273.100 29077.100 321.715 1.569 o -15 1 8 5102.980 4893.130 70.042 9.581 o -15 1 9 4802.280 5167.360 63.536 9.100 o -15 1 10 21900.000 21806.200 164.436 2.150 o -15 1 11 6151.200 6445.040 70.833 7.297 o -15 1 12 5098.100 5459.160 67.883 8.607 o -15 1 13 17208.600 16385.700 137.905 2.860 o -15 1 14 2647.270 2461.020 47.866 19.054 o -15 1 15 1694.210 1962.580 46.338 23.857 o -15 1 16 4034.820 4176.450 90.078 11.093 o -15 1 17 605.526 399.138 30.294 115.302 o -15 1 18 1202.250 1193.120 43.828 38.969 o -15 1 19 5849.990 5869.210 97.426 7.928 o -15 1 20 4.905 47.436 17.889 923.202 o -15 3 1 9827.160 9818.860 249.810 4.478 o -15 3 2 15878.800 16081.200 147.794 2.908 o -15 3 3 4540.400 4237.830 72.538 11.027 o -15 3 4 29894.300 28375.200 219.012 1.645 o -15 3 5 2209.060 1985.630 79.453 22.962 o -15 3 6 3572.840 3976.420 111.898 11.481 o -15 3 7 15940.600 15174.500 240.206 2.990 o -15 3 8 3703.500 3584.750 136.434 12.419 o -15 3 9 7660.290 8031.860 212.664 5.519 o -15 3 10 20151.600 19062.000 212.017 2.424 o -15 3 11 1809.350 2068.960 58.184 22.476 o -15 3 12 2908.290 2359.290 64.690 19.659 o -15 3 13 3498.010 3997.010 87.406 11.597 o -15 3 14 166.499 180.315 26.834 250.406 o -15 3 15 2566.440 2667.100 82.679 17.233 o -15 3 16 4136.070 3984.700 102.928 11.521 o -15 3 17 386.348 366.858 44.276 121.050 o -15 3 18 820.772 1467.540 82.233 30.576 o -15 3 19 1147.740 1404.380 69.587 32.382 o -15 3 20 53.819 124.064 17.889 370.848 o -15 5 1 20378.700 19742.000 214.426 2.341 o -15 5 2 6054.940 6781.260 96.248 6.885 o -15 5 3 3347.610 3770.020 86.194 12.286 o -15 5 4 9506.230 9117.880 132.668 5.085 o -15 5 5 7957.860 6900.360 168.390 6.538 o -15 5 6 1638.980 1655.030 81.269 27.284 o -15 5 7 15614.600 13852.100 153.679 3.359 o 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3642.100 100.609 12.588 o -15 7 13 3236.200 2917.230 126.561 15.201 o -15 7 14 471.533 457.116 47.439 97.647 o -15 7 15 352.609 330.723 60.089 125.886 o -15 7 16 5143.090 4567.470 243.748 8.915 o -15 9 1 11382.900 10639.300 278.790 4.086 o -15 9 2 628.481 990.252 67.758 45.285 o -15 9 3 78.420 322.816 60.086 128.869 o -15 9 4 64.983 466.573 37.818 98.107 o -15 9 5 1281.900 1644.990 67.098 27.891 o -15 9 6 2908.380 3994.370 105.076 11.487 o -15 9 7 16532.900 15239.500 235.390 2.983 o -15 9 8 284.849 1266.340 55.772 36.412 o -15 9 9 3084.800 3338.900 89.492 13.797 o -15 9 10 3135.680 2857.180 80.545 16.141 o -15 9 11 2010.130 1664.020 82.252 27.097 o -15 9 12 42.036 75.897 25.299 565.036 o -15 9 13 8352.120 7438.490 171.073 6.082 o -15 11 2 7407.160 6480.680 158.374 6.985 o -15 11 3 462.586 745.608 33.322 62.521 o -14 0 2 12554.100 17009.500 277.575 2.646 o -14 0 4 146697.000 144050.000 1522.300 0.283 o -14 0 6 3461.110 9892.320 291.137 4.334 o -14 0 8 9571.690 11208.000 150.772 4.135 o 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31.308 132.477 o -14 2 19 4781.720 4361.510 80.401 10.681 o -14 2 20 195.306 285.280 21.910 162.966 o -14 4 1 3816.130 3650.770 72.580 12.767 o -14 4 2 34072.700 32736.300 266.899 1.419 o -14 4 3 256.305 780.931 33.181 59.803 o -14 4 4 43286.300 42216.000 407.183 1.079 o -14 4 5 1712.730 1474.660 46.785 31.567 o -14 4 6 7711.760 9497.250 140.358 4.876 o -14 4 7 104.121 162.709 23.429 279.843 o -14 4 8 33031.900 33587.700 264.457 1.384 o -14 4 9 34.770 477.597 29.343 97.376 o -14 4 10 29535.500 29710.700 295.685 1.546 o -14 4 11 373.676 731.448 39.922 63.203 o -14 4 12 2007.190 2649.890 74.130 17.460 o -14 4 13 1236.940 1403.210 60.263 32.746 o -14 4 14 308.080 1752.060 67.087 26.285 o -14 4 15 5.382 6.325 17.889 4558.320 o -14 4 16 3196.650 4336.950 105.079 10.609 o -14 4 17 160.094 254.117 28.813 179.422 o -14 4 18 7040.790 6174.880 408.440 5.719 o -14 4 19 133.500 103.035 22.137 433.723 o -14 6 1 36109.200 36386.600 334.804 1.262 o -14 6 2 2391.310 2214.250 61.554 20.971 o -14 6 3 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23892.400 263.753 1.924 o -13 1 8 9090.140 8995.110 77.422 5.239 o -13 1 9 3074.480 3304.330 45.487 14.255 o -13 1 10 19242.900 18186.400 169.693 2.565 o -13 1 11 10522.100 11493.200 149.338 4.036 o -13 1 12 2291.270 2544.290 38.123 18.524 o -13 1 13 16825.900 16067.200 116.761 2.928 o -13 1 14 2342.280 3071.050 44.792 15.337 o -13 1 15 2306.910 2333.250 50.325 20.063 o -13 1 16 5405.860 5465.060 91.553 8.522 o -13 1 17 1919.990 1891.200 49.763 24.680 o -13 1 18 587.570 508.775 27.564 91.469 o -13 1 19 5210.280 5233.970 92.540 8.887 o -13 1 20 268.774 277.273 37.950 160.484 o -13 1 21 436.212 376.596 26.836 122.926 o -13 3 1 19826.100 19630.900 233.187 2.343 o -13 3 2 26535.200 27870.500 263.155 1.659 o -13 3 3 405.563 1108.380 41.817 42.043 o -13 3 4 11842.400 11856.400 166.945 3.894 o -13 3 5 4889.520 5795.380 91.357 8.050 o -13 3 6 282.276 424.643 25.249 109.740 o -13 3 7 7122.910 6639.550 94.672 7.032 o -13 3 8 9310.440 8537.170 155.643 5.370 o -13 3 9 3049.560 3713.280 62.230 12.622 o -13 3 10 21943.800 21340.100 281.273 2.131 o -13 3 11 6877.410 6526.380 100.041 7.137 o -13 3 12 2172.410 1909.280 52.486 24.397 o -13 3 13 8652.720 8411.410 144.127 5.475 o -13 3 14 5454.040 5200.330 132.930 8.750 o -13 3 15 466.862 427.161 35.781 106.949 o -13 3 16 6283.840 6188.390 134.297 7.398 o -13 3 17 3174.920 2944.100 87.167 15.605 o -13 3 18 1381.500 1410.760 58.153 32.640 o -13 3 19 1666.600 1676.550 82.246 26.920 o -13 3 20 518.170 442.777 37.952 102.833 o -13 5 1 34192.300 34958.300 275.519 1.328 o -13 5 2 6331.750 6851.180 94.337 6.821 o -13 5 3 114.138 102.304 15.269 450.477 o -13 5 4 12827.300 11726.100 117.772 3.993 o -13 5 5 25646.300 26051.700 224.987 1.785 o -13 5 6 2017.690 2200.540 45.853 21.312 o -13 5 7 12282.800 12394.300 131.857 3.768 o -13 5 8 849.252 1179.770 36.554 39.680 o -13 5 9 2129.230 2170.860 56.868 21.455 o -13 5 10 6015.470 6038.530 85.151 7.745 o -13 5 11 9754.370 8551.830 111.914 5.452 o -13 5 12 773.307 2738.150 72.528 16.951 o -13 5 13 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31.626 85.058 o -13 9 1 14776.200 14550.300 211.734 3.144 o -13 9 2 619.831 879.223 51.290 52.025 o -13 9 3 56.733 687.854 79.060 61.961 o -13 9 4 172.928 613.582 44.724 74.393 o -13 9 5 6054.290 6050.640 140.956 7.533 o -13 9 6 1708.930 2098.980 64.458 22.064 o -13 9 7 13924.600 13312.000 182.907 3.460 o -13 9 8 1556.040 1560.160 54.595 29.692 o -13 9 9 305.205 442.754 35.780 103.440 o -13 9 10 3338.020 3347.660 126.566 13.364 o -13 9 11 7342.570 6649.460 183.652 6.708 o -13 9 12 30.080 56.923 25.299 729.758 o -13 9 13 8022.920 6803.590 171.040 6.618 o -13 11 1 24.536 195.515 23.983 234.487 o -13 11 2 9715.020 9875.360 159.019 4.661 o -13 11 3 11.853 705.695 50.598 64.441 o -13 11 4 6251.510 5757.380 120.319 7.992 o -13 11 5 263.068 295.522 24.295 156.606 o -13 11 6 61.232 141.199 53.761 266.755 o -13 11 7 1323.930 1113.480 56.939 41.069 o -12 0 2 264105.000 268475.000 2612.440 0.144 o -12 0 4 200508.000 200116.000 2119.440 0.195 o -12 0 6 459.694 847.599 75.904 51.576 o -12 0 8 50389.300 48576.400 807.937 0.843 o -12 0 10 34049.700 33436.600 250.655 1.394 o -12 0 12 15367.500 16685.800 159.019 2.797 o -12 0 14 15872.800 15894.500 171.992 2.923 o -12 0 16 18172.100 17731.700 215.977 2.596 o -12 0 18 2431.870 2453.360 78.199 18.749 o -12 0 20 184.803 1340.890 75.899 33.628 o -12 2 1 30302.400 30938.700 225.437 1.512 o -12 2 2 17.141 566.479 24.867 82.846 o -12 2 3 9137.820 9477.510 133.679 4.899 o -12 2 4 1281.990 1420.780 48.018 32.733 o -12 2 5 40551.400 40979.500 372.258 1.120 o -12 2 6 1873.240 2390.230 52.357 19.583 o -12 2 7 39693.400 38388.700 678.929 1.081 o -12 2 8 939.300 781.322 22.801 60.182 o -12 2 9 633.309 1004.930 22.138 46.977 o -12 2 10 699.717 793.752 21.125 59.373 o -12 2 11 27202.200 26650.100 194.355 1.756 o -12 2 12 104.129 264.462 15.740 177.607 o -12 2 13 26070.700 26268.300 181.595 1.785 o -12 2 14 315.224 369.601 19.857 126.699 o -12 2 15 890.210 1358.190 43.421 34.363 o -12 2 16 139.265 378.846 26.741 122.520 o -12 2 17 6479.960 6680.830 109.657 6.949 o -12 2 18 39.019 99.108 16.453 463.411 o -12 2 19 5274.530 4908.040 75.134 9.533 o -12 2 20 25.293 56.923 15.180 793.802 o -12 4 1 34.498 273.650 20.785 170.399 o -12 4 2 76429.900 74970.000 499.945 0.616 o -12 4 3 961.016 1535.060 43.997 30.457 o -12 4 4 54064.500 55637.300 428.688 0.827 o -12 4 5 623.005 946.819 27.205 49.670 o -12 4 6 5167.610 7424.060 84.075 6.325 o -12 4 7 23.732 59.730 10.759 776.524 o -12 4 8 54177.800 54571.400 466.249 0.835 o -12 4 9 1134.080 1546.770 60.440 29.804 o -12 4 10 28749.700 28741.400 410.359 1.543 o -12 4 11 408.773 327.575 29.503 139.981 o -12 4 12 3324.350 3118.910 73.070 14.891 o -12 4 13 1563.800 2080.710 56.022 22.393 o -12 4 14 4332.920 3708.170 82.769 12.501 o -12 4 15 44.926 21.785 19.755 1767.570 o -12 4 16 16821.200 17134.700 253.311 2.650 o -12 4 17 807.815 814.641 46.805 56.313 o -12 4 18 3697.300 3539.520 148.724 12.420 o -12 4 19 48.769 67.043 17.889 667.531 o -12 4 20 2701.840 1936.490 82.269 23.439 o -12 6 1 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182.952 o -12 8 7 2861.160 3312.200 84.023 13.956 o -12 8 8 13730.600 13219.000 187.744 3.478 o -12 8 9 77.222 262.274 35.082 171.020 o -12 8 10 9471.540 9109.350 143.714 5.069 o -12 8 11 2058.280 1711.110 55.932 27.086 o -12 8 12 1791.060 2237.540 79.082 20.491 o -12 8 13 851.520 862.693 42.316 53.583 o -12 8 14 4628.750 4248.650 93.676 10.886 o -12 8 15 401.326 1485.520 51.289 31.303 o -12 10 1 6821.610 6686.340 196.285 6.617 o -12 10 2 2106.120 2201.760 107.557 20.203 o -12 10 3 164.876 234.022 44.274 183.298 o -12 10 4 3239.600 3195.690 126.562 13.960 o -12 10 5 7875.590 7859.210 152.254 5.825 o -12 10 6 66.827 110.232 22.362 407.299 o -12 10 7 9271.010 8520.230 156.776 5.378 o -12 10 8 2852.540 2581.780 107.574 17.385 o -12 10 9 77.639 145.471 31.624 300.218 o -12 10 10 3656.090 3316.480 113.925 13.630 o -12 10 11 4379.210 4266.710 126.609 10.619 o -11 1 1 68332.900 67710.400 602.415 0.668 o -11 1 2 60454.900 60618.200 788.242 0.704 o -11 1 3 321.048 879.086 33.910 53.189 o -11 1 4 24253.500 25380.700 251.628 1.823 o -11 1 5 54786.400 52682.200 512.501 0.858 o -11 1 6 1700.110 1870.260 78.198 24.366 o -11 1 7 32343.800 33354.300 932.867 1.076 o -11 1 8 9849.710 9115.120 140.924 5.073 o -11 1 9 103.917 1287.620 25.461 36.715 o -11 1 10 33286.100 32060.300 183.284 1.469 o -11 1 11 17714.000 18387.600 133.599 2.557 o -11 1 12 1520.410 1801.630 31.156 26.172 o -11 1 13 13542.200 12680.700 105.378 3.707 o -11 1 14 5116.370 4690.550 64.209 10.007 o -11 1 15 549.841 688.417 26.039 68.107 o -11 1 16 5941.200 5397.740 89.300 8.632 o -11 1 17 4443.840 4215.300 77.482 11.060 o -11 1 18 25.334 190.252 35.658 230.334 o -11 1 19 5485.300 5423.270 96.054 8.570 o -11 1 20 705.252 883.723 69.581 50.211 o -11 1 21 97.599 104.456 17.889 437.181 o -11 3 1 15532.500 15074.200 185.348 3.068 o -11 3 2 63612.000 63176.200 472.882 0.729 o -11 3 3 237.050 2156.930 54.652 21.673 o -11 3 4 46976.900 46016.200 362.512 1.005 o -11 3 5 12628.000 12875.500 150.660 3.613 o -11 3 6 29.022 1144.860 52.258 40.334 o -11 3 7 36384.900 36702.200 339.223 1.252 o -11 3 8 31634.400 32245.300 271.845 1.438 o -11 3 9 175.647 190.343 16.679 244.746 o -11 3 10 18008.900 18058.000 165.279 2.585 o -11 3 11 11189.500 10248.200 114.606 4.562 o -11 3 12 81.706 67.833 13.793 674.811 o -11 3 13 10409.000 10623.700 123.495 4.393 o -11 3 14 4214.600 4749.290 88.830 9.792 o -11 3 15 464.798 1344.470 58.144 34.260 o -11 3 16 6052.230 5853.010 129.816 7.825 o -11 3 17 4303.130 3927.870 102.931 11.681 o -11 3 18 1752.340 1765.470 62.630 26.139 o -11 3 19 3836.490 3490.750 85.029 13.246 o -11 5 1 49197.300 48440.700 442.728 0.940 o -11 5 2 10273.200 10336.900 103.843 4.538 o -11 5 3 6.190 1145.490 31.285 41.096 o -11 5 4 15795.300 16757.700 159.688 2.785 o -11 5 5 30661.400 31143.600 250.318 1.493 o -11 5 6 75.215 619.297 27.894 75.602 o -11 5 7 6435.460 9249.010 184.390 4.909 o -11 5 8 2616.650 2893.820 78.876 15.968 o -11 5 9 37.755 171.587 16.864 271.410 o -11 5 10 9413.700 9667.260 126.973 4.813 o -11 5 11 9756.200 9352.440 143.614 4.941 o -11 5 12 227.824 365.047 25.659 127.187 o -11 5 13 20215.600 19976.100 240.393 2.298 o -11 5 14 5355.640 5497.300 127.505 8.324 o -11 5 15 44.607 43.370 15.570 1020.940 o -11 5 16 1979.710 2003.260 59.159 23.174 o -11 5 17 7288.270 7432.910 160.004 6.122 o -11 5 18 345.172 356.561 24.151 130.354 o -11 5 19 5702.700 4537.220 205.789 9.348 o -11 7 1 3711.020 4484.430 82.804 10.388 o -11 7 2 15224.300 15720.400 167.515 2.958 o -11 7 3 681.575 1689.040 45.298 27.713 o -11 7 4 16826.600 16127.000 237.247 2.824 o -11 7 5 3681.830 4095.830 85.295 11.336 o -11 7 6 238.773 1325.920 47.213 35.118 o -11 7 7 2594.180 2276.920 64.919 20.355 o -11 7 8 12158.800 12089.700 163.447 3.824 o -11 7 9 872.594 901.533 37.755 51.595 o -11 7 10 11730.800 11894.100 175.284 3.869 o -11 7 11 844.120 1215.220 49.819 38.088 o -11 7 12 21.025 161.343 26.834 278.911 o -11 7 13 4176.080 4112.650 87.086 11.277 o -11 7 14 4164.180 4020.800 83.884 11.548 o -11 7 15 2.639 18.974 17.889 2061.880 o -11 7 16 5812.600 4995.930 170.948 8.842 o -11 7 17 1070.470 915.353 63.261 49.076 o -11 9 1 11919.000 11920.000 212.784 3.803 o -11 9 2 259.387 612.581 46.801 74.196 o -11 9 3 343.225 946.706 48.713 48.655 o -11 9 4 98.180 156.818 22.948 290.423 o -11 9 5 11499.400 11489.700 171.928 4.005 o -11 9 6 452.746 1980.160 104.271 22.441 o -11 9 7 17248.500 16588.500 214.718 2.769 o -11 9 8 2305.460 2279.240 82.676 20.054 o -11 9 9 26.413 40.760 19.755 1038.180 o -11 9 10 3605.300 3635.990 167.704 11.883 o -11 9 11 12009.300 11550.900 437.291 3.398 o -11 9 12 56.427 145.471 31.624 300.344 o -11 9 13 5394.150 5546.140 151.949 8.132 o -11 9 14 92.680 421.769 26.834 110.350 o -11 11 1 27.111 264.284 22.948 175.539 o -11 11 2 10935.700 10523.000 172.482 4.360 o -11 11 3 117.623 517.825 35.779 89.025 o -11 11 4 10868.500 10752.200 172.484 4.270 o -11 11 5 751.943 961.527 101.210 43.466 o -11 11 6 35.428 82.222 25.299 525.690 o -11 11 7 709.199 822.334 50.605 55.517 o -11 11 8 6104.830 5718.660 145.658 7.930 o -10 0 2 341295.000 328357.000 2632.190 0.126 o -10 0 4 91942.400 89105.000 1353.810 0.434 o -10 0 6 21002.800 20368.100 305.627 2.212 o -10 0 8 37834.300 39923.500 428.062 1.132 o -10 0 10 38705.200 38996.000 279.120 1.195 o -10 0 12 3970.950 4052.020 68.663 11.545 o -10 0 14 29720.200 28203.200 300.820 1.623 o -10 0 16 22570.100 21881.600 261.573 2.092 o -10 0 18 1455.880 1562.570 94.893 28.293 o -10 0 20 5470.190 5222.940 158.271 8.567 o -10 2 1 17313.700 15764.900 130.964 2.980 o -10 2 2 186.973 2289.820 54.358 20.442 o -10 2 3 25059.100 24729.800 240.092 1.875 o -10 2 4 1678.440 2176.700 54.378 21.448 o -10 2 5 30980.600 31511.800 391.746 1.428 o -10 2 6 4528.170 4672.100 89.395 9.948 o -10 2 7 44721.600 43698.300 321.301 1.064 o -10 2 8 2480.150 2948.190 59.719 15.863 o -10 2 9 2963.240 2870.710 38.110 16.428 o -10 2 10 618.803 386.973 13.549 121.648 o -10 2 11 28129.600 26927.900 164.342 1.748 o -10 2 12 29.354 90.515 13.334 512.371 o -10 2 13 23681.500 22984.600 177.562 2.036 o -10 2 14 3.792 518.546 23.016 90.590 o -10 2 15 156.546 71.155 15.812 635.852 o -10 2 16 6.143 329.766 24.902 140.915 o -10 2 17 16479.000 16373.700 175.934 2.836 o -10 2 18 253.006 649.180 29.919 71.954 o -10 2 19 9373.040 8755.570 126.750 5.302 o -10 2 20 121.731 293.538 21.910 158.604 o -10 4 1 1749.350 2819.220 83.512 16.338 o -10 4 2 53130.200 54103.700 554.681 0.827 o -10 4 3 710.449 835.401 47.477 54.931 o -10 4 4 47449.600 48497.800 513.126 0.924 o -10 4 5 658.754 2069.720 76.519 22.172 o -10 4 6 5690.280 6275.440 79.384 7.475 o -10 4 7 1492.470 1737.030 43.609 26.955 o -10 4 8 73707.400 75786.800 690.367 0.588 o -10 4 9 2546.370 2537.690 69.040 18.265 o -10 4 10 28476.600 26156.000 300.740 1.745 o -10 4 11 2222.590 2450.500 57.921 19.040 o -10 4 12 36.774 74.832 14.287 613.589 o -10 4 13 370.862 1421.620 41.447 32.942 o -10 4 14 5187.580 6158.720 108.374 7.530 o -10 4 15 174.974 133.675 22.948 337.610 o -10 4 16 33495.700 32670.000 411.300 1.369 o -10 4 17 513.734 534.032 40.254 85.541 o -10 4 18 736.408 617.958 37.822 74.535 o -10 4 19 8.911 133.021 18.258 346.574 o -10 4 20 5866.440 4705.020 132.982 9.627 o -10 6 1 14201.100 13124.600 125.423 3.568 o -10 6 2 2974.870 3108.300 75.936 14.919 o -10 6 3 2405.430 2469.330 62.724 18.839 o -10 6 4 6802.570 6741.800 100.557 6.913 o -10 6 5 16402.200 16019.200 173.484 2.900 o -10 6 6 1725.130 1557.700 46.995 29.914 o -10 6 7 13209.500 12981.800 137.356 3.596 o -10 6 8 2156.100 2236.010 64.271 20.738 o -10 6 9 29.868 164.618 34.171 264.885 o -10 6 10 1057.230 1476.570 45.146 31.607 o -10 6 11 15239.300 15767.200 209.445 2.913 o -10 6 12 655.111 699.555 39.839 65.928 o -10 6 13 11677.500 11200.600 144.458 4.144 o -10 6 14 1223.890 981.474 43.523 47.149 o -10 6 15 16.820 49.139 17.545 895.680 o -10 6 16 1288.250 1415.530 59.287 32.502 o -10 6 17 9555.770 8449.430 1346.270 1.506 o -10 6 18 159.791 336.296 26.834 137.543 o -10 8 1 979.344 1666.890 65.201 27.603 o -10 8 2 39424.400 39355.500 373.238 1.161 o -10 8 3 623.488 3092.230 76.487 15.018 o -10 8 4 15347.600 15883.100 197.514 2.903 o -10 8 5 82.943 110.233 21.910 408.018 o -10 8 6 2353.810 2261.290 69.405 20.430 o -10 8 7 1466.460 1836.450 63.240 25.156 o -10 8 8 12454.500 12770.300 185.194 3.599 o -10 8 9 281.553 341.572 30.293 134.365 o -10 8 10 5767.500 5572.570 109.523 8.292 o -10 8 11 2674.090 2424.380 69.217 19.089 o -10 8 12 615.491 689.465 44.727 66.380 o -10 8 13 538.713 644.580 32.867 72.103 o -10 8 14 8371.060 7735.360 175.783 5.843 o -10 8 15 16.442 148.699 22.361 306.732 o -10 8 16 7806.240 6962.400 158.380 6.523 o -10 10 1 3989.950 4101.030 151.890 10.801 o -10 10 2 6536.220 7002.410 208.933 6.284 o -10 10 3 1346.270 2011.700 107.544 21.997 o -10 10 4 3810.570 3924.550 107.400 11.660 o -10 10 5 6657.530 6778.150 118.157 6.828 o -10 10 6 11.938 163.347 21.910 280.718 o -10 10 7 10982.400 10454.200 228.104 4.275 o -10 10 8 3165.530 2958.240 87.170 15.533 o -10 10 9 806.796 848.925 47.442 54.071 o -10 10 10 2628.850 2700.770 88.589 16.948 o -10 10 11 5065.250 5571.280 151.944 8.098 o -9 1 1 14197.800 13480.100 129.177 3.479 o -9 1 2 43744.400 40731.600 298.413 1.148 o -9 1 3 8878.570 7983.100 119.447 5.824 o -9 1 4 26954.700 27520.300 224.407 1.697 o -9 1 5 72226.900 75011.300 673.089 0.599 o -9 1 6 2741.630 2598.640 53.688 18.011 o -9 1 7 23612.900 22559.000 241.373 2.047 o -9 1 8 53223.300 52205.700 404.362 0.884 o -9 1 9 1514.790 2231.210 57.033 20.901 o -9 1 10 27552.700 27654.300 189.239 1.696 o -9 1 11 46967.900 48495.400 273.641 0.968 o -9 1 12 1938.440 2274.490 37.132 20.714 o -9 1 13 10673.400 11138.800 102.004 4.217 o -9 1 14 7667.150 8493.640 101.963 5.508 o -9 1 15 272.526 204.027 18.357 227.504 o -9 1 16 4916.740 4765.870 82.947 9.781 o -9 1 17 9767.120 9073.390 140.056 5.095 o -9 1 18 4.866 31.624 15.570 1369.750 o -9 1 19 6643.200 6309.400 170.888 7.107 o -9 1 20 1306.990 1263.200 41.291 36.926 o -9 1 21 15.240 67.043 17.889 668.516 o -9 3 1 8353.530 7872.140 114.772 5.911 o -9 3 2 22389.300 21975.100 200.491 2.121 o -9 3 3 5545.270 5340.630 78.997 8.763 o -9 3 4 68556.300 69547.100 649.998 0.644 o -9 3 5 51210.800 51901.400 637.607 0.841 o -9 3 6 1583.640 1669.210 78.195 27.166 o -9 3 7 7592.630 7325.670 174.684 6.158 o -9 3 8 37615.600 37354.900 331.051 1.233 o -9 3 9 3642.850 3837.070 62.549 12.215 o -9 3 10 12193.200 13007.800 171.649 3.553 o -9 3 11 12998.900 12687.700 148.930 3.665 o -9 3 12 7.668 176.316 18.968 263.008 o -9 3 13 11916.800 12229.000 152.804 3.795 o -9 3 14 13116.300 13831.000 169.072 3.349 o -9 3 15 98.476 189.745 26.834 238.822 o -9 3 16 5854.190 5507.460 125.335 8.318 o -9 3 17 3495.050 3667.180 98.443 12.524 o -9 3 18 460.214 554.695 37.820 82.851 o -9 3 19 3497.330 3398.420 120.242 13.248 o -9 3 20 2629.570 2271.720 88.591 20.003 o -9 5 1 31471.500 30313.900 233.197 1.539 o -9 5 2 20037.400 20223.800 158.011 2.318 o -9 5 3 2155.000 2225.730 42.721 21.105 o -9 5 4 103.015 592.063 25.037 79.265 o 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16725.600 16043.600 217.822 2.857 o -9 7 11 7400.750 7267.020 142.244 6.311 o -9 7 12 155.340 233.746 30.360 193.434 o -9 7 13 4583.510 3983.520 111.618 11.456 o -9 7 14 6871.240 6451.290 131.170 7.118 o -9 7 15 8.747 25.299 14.606 1696.100 o -9 7 16 3605.510 4020.200 262.645 9.690 o -9 7 17 1675.920 1545.180 173.988 24.564 o -9 9 1 5393.620 5476.630 134.278 8.321 o -9 9 2 289.994 1114.100 58.142 41.088 o -9 9 3 406.753 700.863 40.170 65.846 o -9 9 4 2257.840 2378.410 70.560 19.438 o -9 9 5 24876.500 24046.500 283.444 1.899 o -9 9 6 22.044 1527.630 57.129 30.322 o -9 9 7 12309.600 11764.400 215.075 3.847 o -9 9 8 4992.500 4958.020 127.500 9.192 o -9 9 9 877.018 1075.500 58.148 42.439 o -9 9 10 1656.230 1712.870 54.545 27.107 o -9 9 11 13085.100 12520.000 219.998 3.619 o -9 9 12 150.651 374.823 25.733 124.010 o -9 9 13 4165.490 4205.950 124.590 10.781 o -9 9 14 245.303 619.856 44.275 73.704 o -9 11 1 159.453 398.871 31.307 115.536 o -9 11 2 14436.400 14948.400 224.175 3.051 o -9 11 3 358.279 528.168 35.780 87.218 o -9 11 4 6175.370 5837.780 170.955 7.646 o -9 11 5 1460.710 1575.270 82.243 28.566 o -9 11 6 303.561 359.032 28.814 128.417 o -9 11 7 200.107 423.774 44.275 105.878 o -9 11 8 8315.660 7583.360 177.389 5.950 o -8 0 2 529003.000 527933.000 5099.410 0.068 o -8 0 4 3320.540 7156.570 978.176 2.454 o -8 0 6 34823.500 35377.500 439.973 1.266 o -8 0 8 34203.000 37510.000 482.118 1.182 o -8 0 10 19731.500 20112.400 215.613 2.300 o -8 0 12 1738.360 3034.940 67.365 15.364 o -8 0 14 35935.100 32737.600 359.269 1.387 o -8 0 16 14929.700 13687.300 269.412 3.253 o -8 0 18 574.534 796.989 69.578 55.292 o -8 0 20 8958.980 8912.890 215.379 4.999 o -8 2 1 13794.800 12926.600 125.516 3.628 o -8 2 2 17120.500 19244.700 213.787 2.406 o -8 2 3 1779.340 1929.600 41.834 24.323 o -8 2 4 9143.360 8185.130 126.865 5.666 o -8 2 5 18707.500 16582.500 199.211 2.789 o -8 2 6 118.420 832.405 30.806 56.327 o -8 2 7 9955.240 9335.840 107.997 5.012 o -8 2 8 472.437 1697.600 47.989 27.535 o -8 2 9 4486.040 4418.350 84.229 10.531 o -8 2 10 3311.490 5248.660 53.945 8.991 o -8 2 11 28118.400 27812.200 184.758 1.688 o -8 2 12 605.161 986.815 28.267 47.646 o -8 2 13 5405.830 5180.400 70.421 9.054 o -8 2 14 27.152 699.342 28.414 67.052 o -8 2 15 534.500 710.876 28.766 65.816 o -8 2 16 392.539 378.245 25.002 122.829 o -8 2 17 14138.600 13363.400 178.070 3.453 o -8 2 18 243.525 243.389 24.150 189.144 o -8 2 19 8493.160 8382.120 123.073 5.540 o -8 2 20 308.267 332.023 22.949 140.091 o -8 4 1 1884.110 3689.720 89.755 12.533 o -8 4 2 99195.700 93453.000 851.533 0.473 o -8 4 3 27.965 1806.170 56.080 25.773 o -8 4 4 52909.100 53579.300 543.723 0.837 o -8 4 5 106.401 1250.760 48.634 37.141 o -8 4 6 15499.600 14125.700 355.262 3.024 o -8 4 7 1670.280 3125.520 64.358 14.953 o -8 4 8 52196.100 49582.200 425.990 0.923 o -8 4 9 199.148 396.641 26.022 117.241 o -8 4 10 11265.000 9712.150 137.556 4.773 o -8 4 11 31.210 1354.690 41.423 34.567 o -8 4 12 84.996 243.744 21.793 190.295 o -8 4 13 1208.390 1748.170 65.741 26.337 o -8 4 14 3098.730 6424.390 111.995 7.220 o -8 4 15 15.796 101.406 19.265 448.087 o -8 4 16 24582.700 24508.900 273.615 1.870 o -8 4 17 646.060 930.865 40.172 49.914 o -8 4 18 46.918 273.504 28.813 167.407 o -8 4 19 102.477 411.116 44.274 109.020 o -8 4 20 7852.550 6332.010 706.354 3.743 o -8 6 1 12291.100 12302.000 149.455 3.777 o -8 6 2 10250.500 9861.480 177.153 4.631 o -8 6 3 7558.390 7677.630 116.593 6.051 o -8 6 4 3718.970 4123.810 64.789 11.368 o -8 6 5 22739.900 21433.500 191.186 2.174 o -8 6 6 15.491 43.802 10.374 1052.210 o -8 6 7 4579.680 4259.390 64.993 11.005 o -8 6 8 1061.350 1138.720 35.630 41.094 o -8 6 9 1522.930 1699.060 44.866 27.522 o -8 6 10 3627.360 3659.620 75.751 12.717 o -8 6 11 21081.900 21320.000 221.674 2.169 o -8 6 12 102.882 376.998 36.682 120.621 o -8 6 13 5528.120 5910.820 114.246 7.815 o -8 6 14 349.079 382.286 26.586 121.278 o -8 6 15 894.430 943.284 36.898 49.400 o -8 6 16 1961.790 1909.980 55.932 24.336 o -8 6 17 9027.390 8068.460 718.987 3.241 o -8 6 18 435.100 308.357 37.952 145.033 o -8 8 1 291.338 556.995 40.455 82.217 o -8 8 2 71350.500 69977.500 585.600 0.645 o -8 8 3 18.616 1319.870 48.231 35.260 o -8 8 4 2100.240 2111.970 56.098 22.052 o -8 8 5 1522.700 1349.540 52.269 34.264 o -8 8 6 4528.270 5154.900 107.016 8.959 o -8 8 7 3653.770 3823.960 114.040 11.899 o -8 8 8 22925.900 22368.600 334.321 2.001 o -8 8 9 446.851 468.572 33.512 98.263 o -8 8 10 9268.070 9105.110 147.366 5.064 o -8 8 11 1445.720 1476.010 53.483 31.375 o -8 8 12 146.057 177.323 26.834 254.499 o -8 8 13 384.627 566.118 40.253 80.932 o -8 8 14 8925.470 8239.200 145.519 5.583 o -8 8 15 6.053 114.197 22.361 394.551 o -8 8 16 4984.960 4723.140 126.626 9.636 o -8 10 1 4235.870 4322.650 164.552 10.170 o -8 10 2 10558.100 10066.600 266.077 4.332 o -8 10 3 1399.480 1910.490 107.544 23.074 o -8 10 4 1791.240 1989.820 76.050 23.003 o -8 10 5 9988.550 9827.150 183.653 4.632 o -8 10 6 20.215 262.516 31.306 172.975 o -8 10 7 7268.390 7198.310 149.948 6.346 o -8 10 8 2692.710 2567.510 101.241 17.587 o -8 10 9 1514.700 1586.140 120.201 26.805 o -8 10 10 2373.390 2715.410 79.093 16.986 o -8 10 11 5870.450 6287.450 170.958 7.133 o -8 10 12 10.588 150.659 19.755 305.676 o -7 1 1 4365.330 5015.000 120.363 9.142 o -7 1 2 5364.430 11266.000 165.615 4.099 o -7 1 3 7564.990 7900.240 108.454 5.910 o -7 1 4 23301.900 23261.900 241.549 1.991 o -7 1 5 21670.600 21070.300 230.255 2.196 o -7 1 6 5535.640 5132.070 73.584 9.133 o -7 1 7 12127.600 12922.300 125.880 3.626 o -7 1 8 1465.030 1596.730 42.965 29.297 o -7 1 9 179.429 3587.480 103.161 12.779 o -7 1 10 2209.100 1986.140 39.112 23.656 o -7 1 11 23494.700 21725.800 162.754 2.159 o -7 1 12 446.995 661.129 32.980 70.358 o -7 1 13 5426.050 5350.070 78.264 8.747 o -7 1 14 10119.400 10947.200 118.227 4.272 o -7 1 15 1902.250 1947.210 51.383 23.958 o -7 1 16 1963.710 2199.490 63.245 21.093 o -7 1 17 15214.300 15272.200 196.263 3.017 o -7 1 18 404.267 550.724 32.866 84.114 o 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244.377 1.883 o 8 8 5 3737.320 4488.400 83.806 10.374 o 8 8 6 7244.040 6665.130 105.165 6.976 o 8 8 7 5378.220 5087.500 90.160 9.145 o 8 8 8 94.832 395.882 31.500 116.393 o 8 8 9 758.601 966.391 53.674 47.329 o 8 8 10 15329.500 14399.100 323.362 3.023 o 8 8 11 68.169 746.328 63.248 59.655 o 8 8 12 5916.930 5476.770 158.288 8.192 o 8 8 13 197.761 387.763 28.814 119.275 o 8 10 0 3109.820 3382.540 100.600 13.520 o 8 10 1 13886.300 13494.700 228.582 3.357 o 8 10 2 1916.850 2227.630 80.525 20.549 o 8 10 3 8804.170 8718.770 141.270 5.294 o 8 10 4 4123.980 4028.900 77.287 11.564 o 8 10 5 3259.780 2985.920 65.501 15.607 o 8 10 6 232.456 564.502 29.163 82.609 o 8 10 7 11728.500 11998.700 252.726 3.711 o 8 10 8 1060.510 1564.960 47.199 29.809 o 8 10 9 3053.480 2816.180 73.736 16.447 o 9 1 0 41823.200 40598.700 275.593 1.155 o 9 1 1 21095.100 20171.200 184.180 2.316 o 9 1 2 3244.700 4136.670 76.235 11.284 o 9 1 3 12639.600 11791.100 169.353 3.914 o 9 1 4 8923.550 8941.070 216.362 4.984 o 9 1 5 1427.820 1275.450 71.578 35.380 o 9 1 6 460.905 1778.090 61.611 26.035 o 9 1 7 34662.600 32535.700 260.152 1.429 o 9 1 8 130.399 264.118 16.896 177.461 o 9 1 9 6319.500 7124.310 91.280 6.571 o 9 1 10 5489.280 5354.030 75.385 8.750 o 9 1 11 2184.690 2395.820 50.831 19.545 o 9 1 12 8169.520 7626.460 98.391 6.128 o 9 1 13 15040.700 15407.800 193.977 2.993 o 9 1 14 992.966 1154.830 38.676 40.437 o 9 1 15 4823.560 5078.800 83.042 9.191 o 9 1 16 1816.180 1637.310 43.428 28.555 o 9 1 17 1035.270 924.691 29.924 50.670 o 9 1 18 948.112 977.622 40.258 47.536 o 9 3 0 4479.930 4321.690 82.019 10.774 o 9 3 1 26079.100 25356.800 320.029 1.790 o 9 3 2 1647.200 2187.900 59.982 21.262 o 9 3 3 11173.900 12336.700 329.654 3.467 o 9 3 4 74396.600 71301.200 839.528 0.600 o 9 3 5 4165.050 5453.180 151.459 8.269 o 9 3 6 13395.800 13445.700 148.274 3.465 o 9 3 7 7102.500 6911.170 110.008 6.722 o 9 3 8 1678.800 1628.390 66.196 28.172 o 9 3 9 15282.000 14597.100 227.579 3.117 o 9 3 10 11269.800 10676.100 265.784 4.105 o 9 3 11 1872.210 1554.520 215.103 22.113 o 9 3 12 3895.150 4138.830 151.884 10.710 o 9 3 13 4061.030 4740.170 164.545 9.338 o 9 3 14 470.531 594.569 56.927 74.652 o 9 3 15 2599.600 2366.450 107.566 18.873 o 9 3 16 3741.850 3999.820 132.906 11.238 o 9 3 17 3.461 -6.325 18.974 10296.500 o 9 5 0 3046.690 3217.190 54.581 14.585 o 9 5 1 39316.000 36427.500 247.079 1.284 o 9 5 2 1100.740 725.825 24.078 64.613 o 9 5 3 6011.050 6121.240 100.990 7.598 o 9 5 4 18106.700 17336.200 173.559 2.685 o 9 5 5 7392.250 7017.870 98.962 6.649 o 9 5 6 7450.120 8052.350 128.389 5.750 o 9 5 7 22343.700 23448.300 223.228 1.977 o 9 5 8 1951.240 2151.990 55.582 21.662 o 9 5 9 21016.000 20823.900 245.278 2.204 o 9 5 10 4190.510 3908.080 167.713 11.123 o 9 5 11 6804.810 7178.040 147.738 6.370 o 9 5 12 1091.940 1246.180 82.236 35.622 o 9 5 13 20357.700 19771.100 399.737 2.183 o 9 5 14 29.913 170.769 37.949 251.396 o 9 5 15 2789.490 2689.350 107.574 16.729 o 9 5 16 1277.260 1232.080 46.811 37.657 o 9 7 0 3909.930 4294.770 75.131 10.874 o 9 7 1 9503.160 8988.090 115.183 5.188 o 9 7 2 6918.540 6311.330 99.269 7.376 o 9 7 3 3023.110 3265.410 68.977 14.274 o 9 7 4 19663.600 19485.200 215.419 2.370 o 9 7 5 85.150 354.792 23.183 131.489 o 9 7 6 2891.920 3210.960 81.535 14.405 o 9 7 7 5103.600 4998.510 104.717 9.239 o 9 7 8 4271.210 4425.810 96.176 10.449 o 9 7 9 3720.460 3584.540 84.034 12.917 o 9 7 10 12545.600 12243.300 297.844 3.554 o 9 7 11 6.968 75.897 31.624 536.370 o 9 7 12 3952.160 4075.830 139.237 10.982 o 9 7 13 3296.310 3404.730 113.913 13.297 o 9 7 14 249.452 227.702 37.950 192.741 o 9 9 0 5852.830 6640.560 215.233 6.569 o 9 9 1 24482.700 25152.000 501.516 1.680 o 9 9 2 393.865 1214.720 62.615 37.589 o 9 9 3 3271.390 3475.610 83.870 13.315 o 9 9 4 5284.220 4576.220 97.409 10.103 o 9 9 5 10201.300 10046.800 166.411 4.569 o 9 9 6 798.983 1592.130 42.319 29.425 o 9 9 7 17734.500 16799.500 183.269 2.761 o 9 9 8 213.836 592.975 42.312 77.189 o 9 9 9 4780.490 4665.610 111.632 9.841 o 9 9 10 1943.330 2078.020 110.723 21.244 o 9 9 11 1063.350 1024.830 56.935 44.501 o 9 11 0 2481.050 2579.750 63.253 18.043 o 9 11 1 1678.700 1585.270 48.614 29.372 o 9 11 2 5746.250 5576.450 96.213 8.339 o 9 11 3 1522.910 2292.850 57.145 20.349 o 9 11 4 14228.300 13864.400 145.763 3.365 o 9 11 5 244.563 714.787 40.252 64.638 o 9 11 6 1861.530 2252.520 88.582 20.184 o 10 0 0 20605.400 19302.500 267.330 2.360 o 10 0 2 78145.400 70667.000 636.183 0.638 o 10 0 4 75187.600 69235.100 899.337 0.607 o 10 0 6 32633.200 31458.600 347.199 1.447 o 10 0 8 7169.550 7111.500 167.195 6.360 o 10 0 10 13847.200 13302.800 211.870 3.426 o 10 0 12 3205.930 3372.740 132.885 13.194 o 10 0 14 867.021 1088.000 53.674 42.211 o 10 0 16 11193.100 11667.900 185.908 3.926 o 10 2 0 80.569 81.763 11.010 569.502 o 10 2 1 43072.700 37956.700 414.807 1.194 o 10 2 2 677.339 2019.880 80.513 22.612 o 10 2 3 11452.400 11250.800 217.125 4.013 o 10 2 4 163.141 854.069 38.672 54.470 o 10 2 5 32593.000 30179.400 636.427 1.351 o 10 2 6 1901.300 2552.290 48.089 18.396 o 10 2 7 34303.300 33027.200 252.380 1.410 o 10 2 8 1523.430 1852.130 45.961 25.268 o 10 2 9 618.976 747.396 27.528 62.705 o 10 2 10 673.450 890.726 32.396 52.518 o 10 2 11 6838.230 7628.160 114.771 6.094 o 10 2 12 3.579 85.888 16.755 531.772 o 10 2 13 12595.000 12469.500 168.216 3.705 o 10 2 14 150.328 144.360 15.650 321.638 o 10 2 15 5084.380 5204.850 72.429 9.007 o 10 2 16 1063.390 944.359 27.649 49.714 o 10 2 17 1952.530 1711.970 36.278 27.441 o 10 4 0 42091.100 43106.600 403.128 1.059 o 10 4 1 1015.910 1768.540 69.202 25.968 o 10 4 2 61962.000 64759.800 788.963 0.661 o 10 4 3 167.740 587.291 31.818 79.217 o 10 4 4 33084.500 31255.700 260.062 1.486 o 10 4 5 1733.070 1941.090 46.482 24.114 o 10 4 6 4850.200 4777.430 77.168 9.783 o 10 4 7 1491.380 1962.270 52.204 23.779 o 10 4 8 2870.140 2540.280 73.747 18.180 o 10 4 9 12.139 343.169 33.319 133.149 o 10 4 10 20406.000 19915.200 406.045 2.162 o 10 4 11 2735.090 2360.110 113.893 18.783 o 10 4 12 10382.300 9989.940 259.726 4.379 o 10 4 13 622.371 961.454 69.579 46.416 o 10 4 14 2388.280 2258.800 107.562 19.719 o 10 4 15 33.794 69.573 25.299 611.113 o 10 4 16 9604.270 9510.920 209.101 4.721 o 10 6 0 1668.910 2896.460 70.966 16.049 o 10 6 1 15544.100 15580.800 140.978 3.004 o 10 6 2 4801.680 4870.290 69.819 9.626 o 10 6 3 3744.770 4160.590 67.636 11.255 o 10 6 4 8136.560 7985.730 112.296 5.831 o 10 6 5 11293.300 11025.300 138.935 4.216 o 10 6 6 349.832 554.264 30.257 83.927 o 10 6 7 27658.000 26604.900 358.701 1.687 o 10 6 8 3532.640 3312.160 100.606 13.791 o 10 6 9 3643.010 3916.270 132.893 11.464 o 10 6 10 782.999 825.309 56.929 54.755 o 10 6 11 5798.670 5286.170 123.037 8.664 o 10 6 12 25.909 268.917 41.111 163.743 o 10 6 13 11709.600 10716.300 247.154 4.134 o 10 6 14 425.581 499.694 44.277 90.461 o 10 6 15 3064.580 2776.490 66.681 16.750 o 10 8 0 175.184 494.762 41.585 91.973 o 10 8 1 1979.940 2212.580 66.901 20.915 o 10 8 2 12078.400 11937.900 210.583 3.801 o 10 8 3 449.843 1149.610 60.256 39.744 o 10 8 4 19440.700 19699.000 210.076 2.349 o 10 8 5 4055.780 3859.720 76.699 12.063 o 10 8 6 10769.100 11079.700 163.346 4.162 o 10 8 7 5667.120 5482.330 105.989 8.440 o 10 8 8 4103.390 3746.560 85.208 12.362 o 10 8 9 1683.440 1231.840 63.265 36.949 o 10 8 10 9981.610 9509.430 234.410 4.654 o 10 8 11 1831.710 1948.660 88.576 23.168 o 10 8 12 2882.220 2702.210 94.925 16.846 o 10 10 0 170.671 193.444 28.813 232.597 o 10 10 1 12917.800 12791.500 217.318 3.549 o 10 10 2 3216.490 3634.320 129.725 12.336 o 10 10 3 903.089 1163.450 55.778 39.464 o 10 10 4 4879.930 4919.530 82.197 9.486 o 10 10 5 4396.300 4036.940 70.377 11.576 o 10 10 6 522.254 824.430 41.997 56.083 o 10 10 7 8083.930 7661.730 145.105 5.991 o 10 10 8 1598.260 1630.020 139.190 25.281 o 11 1 0 708.046 1595.750 38.185 29.443 o 11 1 1 40199.400 39765.900 284.878 1.174 o 11 1 2 44632.000 40992.100 273.643 1.142 o 11 1 3 3984.980 4423.770 102.966 10.418 o 11 1 4 24615.200 23598.700 259.303 1.949 o 11 1 5 34388.700 34128.000 354.041 1.337 o 11 1 6 1286.130 3048.260 52.334 15.418 o 11 1 7 26141.100 25437.400 208.592 1.833 o 11 1 8 1815.810 1609.600 50.849 28.880 o 11 1 9 564.447 699.961 30.174 66.717 o 11 1 10 25589.400 24313.400 203.787 1.917 o 11 1 11 2493.420 2461.750 53.547 18.996 o 11 1 12 1210.750 1719.290 54.784 27.022 o 11 1 13 22092.100 21368.700 300.652 2.114 o 11 1 14 466.541 1142.070 37.951 40.960 o 11 1 15 2795.340 3052.250 60.112 15.323 o 11 1 16 2806.270 2668.780 52.133 17.555 o 11 1 17 2088.200 1964.930 39.451 23.908 o 11 3 0 3022.220 4523.020 91.532 10.264 o 11 3 1 25201.900 22464.400 284.688 2.029 o 11 3 2 29369.300 28438.100 464.395 1.530 o 11 3 3 7631.890 7398.100 259.694 5.753 o 11 3 4 36430.100 36352.900 326.887 1.267 o 11 3 5 12219.400 12128.600 188.994 3.778 o 11 3 6 271.083 282.149 24.703 163.655 o 11 3 7 21760.800 21895.600 339.124 2.038 o 11 3 8 8390.550 8255.990 183.889 5.468 o 11 3 9 2837.790 2974.110 96.904 15.343 o 11 3 10 2568.520 2723.900 127.504 16.193 o 11 3 11 2795.560 3290.260 132.876 13.506 o 11 3 12 2129.300 3081.150 132.863 14.366 o 11 3 13 8916.850 8911.200 234.339 4.943 o 11 3 14 1364.480 1258.900 75.913 35.604 o 11 3 15 1940.680 1784.170 88.576 25.179 o 11 3 16 6724.250 6218.760 164.651 7.235 o 11 5 0 170.452 719.843 24.691 65.358 o 11 5 1 21401.700 20117.600 180.232 2.319 o 11 5 2 1164.830 873.751 41.675 52.910 o 11 5 3 123.820 171.193 20.099 269.253 o 11 5 4 26880.800 27609.900 288.079 1.663 o 11 5 5 15266.100 14941.900 192.727 3.085 o 11 5 6 2861.900 3167.760 70.473 14.694 o 11 5 7 27336.000 26772.800 330.037 1.692 o 11 5 8 7087.240 8422.210 136.341 5.487 o 11 5 9 2832.680 3071.290 76.543 15.090 o 11 5 10 1617.320 1224.600 136.015 32.459 o 11 5 11 14640.500 13977.400 316.948 3.116 o 11 5 12 1616.020 1632.200 88.569 27.394 o 11 5 13 15774.100 15592.700 329.735 2.802 o 11 5 14 54.882 335.215 37.949 134.503 o 11 5 15 1279.810 1290.570 63.263 35.371 o 11 7 0 23.012 160.082 19.013 288.808 o 11 7 1 9136.700 9397.500 120.752 4.958 o 11 7 2 11930.200 11611.500 130.830 4.018 o 11 7 3 628.360 819.030 36.239 56.809 o 11 7 4 28792.400 27342.800 262.365 1.688 o 11 7 5 596.859 927.781 42.497 49.954 o 11 7 6 115.679 237.240 25.562 193.485 o 11 7 7 5819.510 6171.250 115.697 7.489 o 11 7 8 8618.820 8338.070 170.171 5.455 o 11 7 9 1032.910 1176.900 58.149 38.906 o 11 7 10 8547.380 8303.090 228.003 5.298 o 11 7 11 847.040 885.589 63.256 50.663 o 11 7 12 1943.870 2100.540 88.577 21.570 o 11 9 0 3103.070 2929.750 132.883 15.041 o 11 9 1 14360.800 14059.400 233.070 3.223 o 11 9 2 1005.080 1414.540 53.479 32.729 o 11 9 3 2002.430 2136.600 64.461 21.678 o 11 9 4 5417.370 5321.510 115.879 8.644 o 11 9 5 9530.720 9598.210 124.227 4.851 o 11 9 6 152.095 258.227 21.201 179.959 o 11 9 7 13096.200 13243.200 554.630 2.770 o 11 9 8 414.092 491.885 63.252 87.422 o 11 9 9 989.046 1315.400 66.422 34.618 o 11 9 10 1747.740 1849.030 142.358 22.521 o 11 11 0 192.280 173.880 19.266 265.529 o 11 11 1 453.126 652.435 31.502 71.403 o 11 11 2 6432.050 6426.410 99.890 7.248 o 11 11 3 584.857 1021.830 36.520 45.733 o 11 11 4 9658.200 9796.460 190.857 4.633 o 12 0 0 4120.240 4182.530 111.913 10.937 o 12 0 2 41784.300 42233.000 615.768 1.018 o 12 0 4 29115.600 28017.800 431.686 1.570 o 12 0 6 30671.400 29426.900 341.943 1.543 o 12 0 8 28296.300 28748.300 355.159 1.570 o 12 0 10 29007.500 27525.000 352.664 1.637 o 12 0 12 6244.840 6090.180 183.592 7.283 o 12 0 14 4948.690 4597.430 155.077 9.679 o 12 0 16 15989.600 15598.900 219.779 2.934 o 12 2 0 6.488 725.239 27.351 64.764 o 12 2 1 72641.500 71750.800 548.879 0.637 o 12 2 2 1910.570 2260.830 91.635 20.052 o 12 2 3 2146.760 2155.520 93.638 20.932 o 12 2 4 7629.130 7547.650 142.509 6.086 o 12 2 5 29217.000 28345.500 254.756 1.635 o 12 2 6 258.348 467.817 22.080 100.223 o 12 2 7 42176.200 40712.600 383.553 1.122 o 12 2 8 2276.860 2299.890 58.478 20.252 o 12 2 9 4993.470 5345.240 85.626 8.732 o 12 2 10 418.203 614.322 27.027 76.152 o 12 2 11 15901.800 15930.100 208.275 2.885 o 12 2 12 317.889 437.296 30.293 105.752 o 12 2 13 17930.800 17003.400 206.256 2.711 o 12 2 14 81.467 151.915 14.596 307.243 o 12 2 15 2214.690 2335.990 43.511 20.112 o 12 2 16 79.505 297.982 17.179 157.582 o 12 4 0 1855.590 1838.830 47.814 25.405 o 12 4 1 97.212 188.885 19.619 245.168 o 12 4 2 51409.900 50910.500 387.676 0.907 o 12 4 3 0.377 1229.670 39.811 38.074 o 12 4 4 65352.800 64571.500 477.461 0.711 o 12 4 5 42.167 161.813 17.996 286.534 o 12 4 6 4221.620 4250.610 107.128 10.797 o 12 4 7 1597.820 1670.830 64.749 27.524 o 12 4 8 5177.960 5166.800 123.025 8.858 o 12 4 9 8.639 847.517 69.572 52.324 o 12 4 10 39088.800 37308.100 661.672 1.113 o 12 4 11 6026.000 5532.910 183.586 7.962 o 12 4 12 5044.090 5272.640 170.902 8.412 o 12 4 13 58.850 158.120 31.624 278.127 o 12 4 14 3003.620 2923.530 113.904 15.365 o 12 4 15 183.118 202.399 31.625 220.559 o 12 6 0 18.857 1188.880 39.016 39.382 o 12 6 1 36339.300 33981.800 252.163 1.371 o 12 6 2 3338.690 3678.500 79.251 12.632 o 12 6 3 292.913 418.340 31.703 110.136 o 12 6 4 1142.840 1423.710 53.451 32.516 o 12 6 5 15201.600 14940.200 201.060 3.077 o 12 6 6 625.613 989.974 48.365 46.576 o 12 6 7 22095.800 22881.300 332.059 1.960 o 12 6 8 830.686 915.365 53.674 49.847 o 12 6 9 2164.850 2387.930 91.818 19.023 o 12 6 10 1247.370 1518.230 62.624 30.273 o 12 6 11 7833.160 7398.460 143.083 6.201 o 12 6 12 14.767 581.878 50.598 77.420 o 12 6 13 8473.380 8253.870 196.370 5.433 o 12 6 14 1422.410 1594.300 69.593 28.664 o 12 8 0 98.107 351.336 30.292 130.964 o 12 8 1 425.762 430.672 32.666 106.791 o 12 8 2 13228.600 12762.900 586.215 2.773 o 12 8 3 486.471 1086.120 46.157 42.688 o 12 8 4 12933.300 13411.400 160.789 3.460 o 12 8 5 3187.480 3236.310 80.374 14.303 o 12 8 6 1887.500 1708.280 55.930 27.137 o 12 8 7 3546.610 3791.070 84.034 12.233 o 12 8 8 5581.300 5381.960 123.038 8.517 o 12 8 9 30.152 158.119 31.624 278.273 o 12 8 10 9175.670 9078.350 215.397 4.914 o 12 8 11 778.445 1050.070 56.931 43.508 o 12 10 0 381.223 1054.700 51.289 43.681 o 12 10 1 9886.500 9804.340 174.531 4.662 o 12 10 2 4082.810 4688.730 111.883 9.796 o 12 10 3 76.301 376.134 26.623 123.470 o 12 10 4 2361.560 2288.650 51.357 20.435 o 12 10 5 3313.930 3272.900 117.079 13.768 o 12 10 6 792.090 948.672 49.159 48.466 o 12 10 7 8350.150 7539.560 196.409 5.916 o 13 1 0 3547.660 4183.590 69.215 11.191 o 13 1 1 33329.400 31773.000 277.308 1.458 o 13 1 2 21628.700 19723.400 314.309 2.270 o 13 1 3 574.082 1187.800 98.044 36.258 o 13 1 4 32982.900 32571.900 522.405 1.324 o 13 1 5 47697.500 46922.600 360.334 0.985 o 13 1 6 54.839 190.239 16.997 245.176 o 13 1 7 20621.500 21373.400 189.989 2.181 o 13 1 8 9064.400 9671.770 115.156 4.829 o 13 1 9 45.476 1185.670 38.046 39.516 o 13 1 10 4021.920 3425.970 62.913 13.648 o 13 1 11 12131.700 12182.600 165.817 3.792 o 13 1 12 127.764 860.600 49.196 53.354 o 13 1 13 11565.000 11149.300 188.174 4.097 o 13 1 14 973.841 1081.650 34.792 43.264 o 13 1 15 922.670 896.909 30.740 52.197 o 13 1 16 3763.950 3140.560 52.953 14.938 o 13 3 0 8187.200 8025.120 157.017 5.697 o 13 3 1 17606.900 16537.200 183.978 2.805 o 13 3 2 24670.200 24529.400 352.007 1.826 o 13 3 3 1222.990 1332.780 46.770 34.883 o 13 3 4 29139.000 27537.400 306.206 1.659 o 13 3 5 9553.650 9382.110 171.041 4.871 o 13 3 6 2.200 135.877 33.517 316.697 o 13 3 7 15080.800 15453.200 240.003 2.938 o 13 3 8 18177.100 16456.000 570.832 2.308 o 13 3 9 283.759 383.437 56.925 111.766 o 13 3 10 3440.570 3315.900 139.217 13.320 o 13 3 11 7006.390 6920.330 208.940 6.352 o 13 3 12 745.417 778.033 63.255 57.234 o 13 3 13 3484.520 3758.990 139.222 11.851 o 13 3 14 3230.140 3069.180 113.908 14.672 o 13 3 15 332.158 449.084 44.276 100.149 o 13 5 0 278.937 676.125 38.016 68.429 o 13 5 1 19942.900 20030.100 212.231 2.310 o 13 5 2 8760.970 9164.070 140.423 5.047 o 13 5 3 223.946 229.386 26.475 199.078 o 13 5 4 10983.400 10953.600 160.312 4.213 o 13 5 5 12509.300 12469.800 149.588 3.727 o 13 5 6 82.191 341.653 40.168 131.259 o 13 5 7 31511.700 30533.200 375.260 1.475 o 13 5 8 6362.440 6258.070 138.558 7.302 o 13 5 9 11.523 31.624 17.889 1330.890 o 13 5 10 748.332 915.355 49.201 50.170 o 13 5 11 9053.160 9057.270 234.349 4.869 o 13 5 12 929.375 936.204 63.257 48.062 o 13 5 13 8065.330 8195.730 202.676 5.449 o 13 5 14 1455.850 1107.140 63.265 40.934 o 13 7 0 606.148 562.569 29.489 82.688 o 13 7 1 2479.710 2486.120 59.682 18.747 o 13 7 2 21525.500 21025.100 194.372 2.213 o 13 7 3 846.578 1461.200 67.093 31.283 o 13 7 4 18995.500 19304.900 296.021 2.330 o 13 7 5 1897.480 2234.910 145.511 18.951 o 13 7 6 625.301 592.249 44.727 76.788 o 13 7 7 4892.190 5038.290 125.318 9.064 o 13 7 8 3758.520 4340.380 111.873 10.553 o 13 7 9 64.441 170.770 37.949 251.252 o 13 7 10 4566.880 4424.390 145.581 10.112 o 13 7 11 955.998 1372.700 69.584 33.108 o 13 9 0 633.852 597.431 42.315 76.478 o 13 9 1 9183.970 9249.810 332.524 4.457 o 13 9 2 3128.690 3457.040 80.208 13.415 o 13 9 3 180.713 513.004 37.431 89.541 o 13 9 4 1527.350 1345.240 58.154 34.165 o 13 9 5 15164.100 15122.200 187.894 3.054 o 13 9 6 255.407 348.336 31.307 131.585 o 13 9 7 8862.470 8488.570 209.047 5.252 o 13 9 8 299.363 278.305 37.951 159.877 o 13 9 9 311.963 414.245 28.814 111.761 o 13 11 0 14.773 167.647 20.135 275.274 o 13 11 1 279.882 425.801 24.150 109.625 o 13 11 2 7978.310 7665.280 113.333 6.069 o 14 0 0 11586.400 11237.700 507.170 3.276 o 14 0 2 53870.800 50223.300 640.821 0.865 o 14 0 4 35701.900 37111.900 601.248 1.145 o 14 0 6 1319.940 1595.920 63.665 28.815 o 14 0 8 18599.300 21198.300 294.603 2.134 o 14 0 10 39268.200 38817.500 668.060 1.073 o 14 0 12 3636.770 3917.210 145.550 11.338 o 14 0 14 12615.200 12464.500 197.192 3.668 o 14 0 16 9013.410 8475.670 129.940 5.468 o 14 2 0 86.673 317.644 21.420 146.982 o 14 2 1 26433.900 24146.500 375.117 1.838 o 14 2 2 2571.760 3068.830 59.872 15.247 o 14 2 3 5986.910 5947.360 98.758 7.822 o 14 2 4 2112.070 2929.660 74.920 15.826 o 14 2 5 28436.000 27309.800 461.370 1.588 o 14 2 6 273.702 309.419 20.797 150.699 o 14 2 7 28053.500 27144.800 245.079 1.707 o 14 2 8 50.876 147.168 16.764 315.327 o 14 2 9 142.973 467.574 27.743 99.590 o 14 2 10 413.494 490.140 30.293 94.585 o 14 2 11 16331.000 16014.100 197.609 2.880 o 14 2 12 446.171 464.383 29.215 99.838 o 14 2 13 19050.300 18353.700 211.197 2.515 o 14 2 14 12.718 65.958 9.881 707.688 o 14 2 15 713.223 689.783 24.386 68.032 o 14 4 0 6817.350 6868.150 112.970 6.756 o 14 4 1 117.003 526.018 27.093 88.826 o 14 4 2 74951.600 74729.500 596.936 0.606 o 14 4 3 2678.480 2354.320 54.394 19.833 o 14 4 4 33818.000 31971.500 280.553 1.447 o 14 4 5 195.395 610.373 40.252 75.336 o 14 4 6 1086.380 1247.280 57.635 36.807 o 14 4 7 724.703 741.644 51.061 61.232 o 14 4 8 2892.470 3187.570 93.959 14.386 o 14 4 9 1234.450 1094.390 75.911 40.613 o 14 4 10 27681.800 26581.000 508.120 1.595 o 14 4 11 1251.940 1132.350 75.912 39.337 o 14 4 12 99.153 189.745 37.949 228.256 o 14 4 13 277.774 360.527 44.275 123.137 o 14 4 14 5576.120 5641.220 151.952 8.001 o 14 4 15 0.277 158.119 25.299 286.145 o 14 6 0 595.593 506.715 28.759 91.675 o 14 6 1 14160.200 14065.400 191.522 3.272 o 14 6 2 966.674 1513.240 56.544 30.566 o 14 6 3 720.181 708.555 41.244 64.969 o 14 6 4 557.806 536.781 36.798 85.622 o 14 6 5 19810.300 19862.800 300.545 2.265 o 14 6 6 277.587 206.001 31.307 216.900 o 14 6 7 9032.490 8817.810 174.659 5.160 o 14 6 8 333.766 418.135 34.129 109.637 o 14 6 9 197.031 249.368 60.087 160.662 o 14 6 10 1980.000 1827.680 64.753 25.221 o 14 6 11 9443.350 9280.600 221.721 4.796 o 14 6 12 129.886 177.097 25.300 256.282 o 14 6 13 10197.600 9659.240 202.819 4.668 o 14 8 0 1991.440 2057.340 64.460 22.489 o 14 8 1 2332.390 3140.080 129.703 14.157 o 14 8 2 14969.000 14957.500 285.265 2.973 o 14 8 3 157.328 709.045 46.800 64.524 o 14 8 4 9440.030 8435.670 167.911 5.400 o 14 8 5 1618.310 1572.870 67.101 29.104 o 14 8 6 866.234 1075.950 53.675 42.667 o 14 8 7 631.241 779.310 44.727 58.986 o 14 8 8 11148.500 10037.600 240.802 4.409 o 14 8 9 1.121 354.186 44.273 125.472 o 14 8 10 7919.860 7874.180 183.710 5.722 o 14 10 0 251.556 349.716 31.307 131.089 o 14 10 1 8419.500 7776.860 116.907 5.974 o 14 10 2 2734.530 2668.600 62.107 17.463 o 14 10 3 153.716 309.055 21.910 150.759 o 14 10 4 1319.550 1340.350 41.292 34.840 o 14 10 5 7254.370 6562.030 171.018 6.849 o 14 10 6 112.776 373.169 44.274 119.390 o 15 1 0 35.794 129.889 18.974 353.541 o 15 1 1 5694.300 5803.900 62.870 8.113 o 15 1 2 24907.700 23549.400 301.568 1.929 o 15 1 3 26.811 1271.930 47.277 36.590 o 15 1 4 9713.780 8643.840 126.516 5.369 o 15 1 5 27215.800 26544.700 221.680 1.754 o 15 1 6 149.296 251.757 19.591 185.082 o 15 1 7 17591.500 17529.200 171.286 2.657 o 15 1 8 4606.370 4383.190 75.350 10.654 o 15 1 9 33.793 490.278 30.292 94.777 o 15 1 10 10738.000 10027.400 145.052 4.615 o 15 1 11 10751.300 10426.700 181.383 4.381 o 15 1 12 380.735 404.808 35.780 112.675 o 15 1 13 6234.620 7011.870 134.304 6.560 o 15 1 14 2516.780 2251.050 47.456 20.811 o 15 1 15 8.517 54.017 9.487 862.212 o 15 3 0 377.600 462.504 28.812 100.342 o 15 3 1 13351.800 12685.900 176.423 3.634 o 15 3 2 31005.000 30862.700 337.510 1.476 o 15 3 3 131.699 915.757 42.478 50.669 o 15 3 4 17688.500 17461.300 257.868 2.599 o 15 3 5 16673.200 15519.000 235.892 2.931 o 15 3 6 531.081 978.401 43.863 47.372 o 15 3 7 18789.800 17503.700 267.830 2.583 o 15 3 8 14506.400 14984.800 335.953 2.895 o 15 3 9 1220.150 1341.090 88.563 32.933 o 15 3 10 4072.500 4518.680 158.217 9.815 o 15 3 11 3676.850 3872.950 145.552 11.459 o 15 3 12 705.565 632.546 56.929 70.382 o 15 3 13 2884.720 2847.530 107.573 15.847 o 15 3 14 1684.070 1765.150 75.921 25.813 o 15 5 0 341.644 590.548 38.344 77.965 o 15 5 1 14169.000 14542.800 194.013 3.166 o 15 5 2 9633.580 8770.590 141.661 5.262 o 15 5 3 3956.070 4230.850 94.718 10.927 o 15 5 4 6845.820 6449.020 102.297 7.214 o 15 5 5 14752.800 14347.900 178.046 3.223 o 15 5 6 1495.320 1407.880 62.148 32.559 o 15 5 7 26780.700 26233.400 359.152 1.709 o 15 5 8 9354.320 9145.160 174.495 4.983 o 15 5 9 631.246 880.759 60.091 51.234 o 15 5 10 271.232 240.351 44.275 178.715 o 15 5 11 11954.300 11654.100 266.163 3.785 o 15 5 12 319.839 278.304 37.951 159.843 o 15 5 13 4615.060 4311.010 126.608 10.514 o 15 7 0 269.528 662.930 79.062 63.983 o 15 7 1 3191.880 3314.210 102.912 13.762 o 15 7 2 11633.600 12068.700 217.254 3.751 o 15 7 3 347.595 322.703 35.780 139.903 o 15 7 4 14006.000 13857.500 233.055 3.268 o 15 7 5 4843.370 4905.840 125.317 9.298 o 15 7 6 192.586 393.944 37.819 115.273 o 15 7 7 1368.250 1198.990 98.055 35.888 o 15 7 8 6940.550 6813.560 332.425 5.776 o 15 7 9 0.181 37.949 25.299 1031.290 o 15 7 10 4088.010 3664.750 120.260 12.330 o 15 7 11 2155.910 2220.950 82.257 20.573 o 15 9 0 473.211 510.466 37.820 89.756 o 15 9 1 7743.020 7628.200 127.754 6.061 o 15 9 2 2673.850 2503.830 79.483 18.361 o 15 9 3 297.979 499.679 50.600 89.225 o 15 9 4 1846.680 2246.430 71.579 20.539 o 15 9 5 13318.000 12640.000 194.960 3.623 o 15 9 6 244.259 301.271 26.835 152.905 o 15 9 7 9106.860 8249.660 190.084 5.455 o 15 9 8 1132.310 1113.430 56.937 41.090 o 16 0 0 6200.570 6457.730 89.141 7.242 o 16 0 2 33675.800 31225.600 296.497 1.475 o 16 0 4 11599.300 11399.700 189.835 4.008 o 16 0 6 128.368 233.783 28.753 194.432 o 16 0 8 42414.300 43530.000 2011.570 0.503 o 16 0 10 5012.530 5139.610 170.898 8.614 o 16 0 12 46.703 88.547 31.624 468.868 o 16 0 14 6244.540 6096.410 202.621 7.174 o 16 2 0 452.091 3267.860 49.078 14.422 o 16 2 1 3966.110 3451.970 54.098 13.600 o 16 2 2 927.497 1632.120 56.123 28.411 o 16 2 3 3833.090 3608.650 86.330 12.815 o 16 2 4 9.675 92.569 14.969 498.494 o 16 2 5 53891.000 52766.700 519.925 0.852 o 16 2 6 663.945 726.855 31.149 64.201 o 16 2 7 4054.700 4202.060 79.813 11.084 o 16 2 8 91.391 148.787 21.652 306.887 o 16 2 9 588.519 1069.300 43.823 43.437 o 16 2 10 254.871 676.652 35.168 68.648 o 16 2 11 11857.500 11773.700 158.500 3.930 o 16 2 12 614.747 542.185 29.216 85.751 o 16 2 13 7446.210 7142.510 82.073 6.571 o 16 2 14 631.496 609.531 22.139 77.044 o 16 4 0 8667.480 10491.200 130.577 4.439 o 16 4 1 512.715 745.486 34.974 62.398 o 16 4 2 34634.600 32970.400 331.384 1.388 o 16 4 3 75.429 661.251 35.719 70.212 o 16 4 4 6071.180 5617.200 117.495 8.195 o 16 4 5 58.049 77.162 24.151 561.122 o 16 4 6 324.405 473.837 50.600 93.753 o 16 4 7 2465.530 2355.230 82.677 19.428 o 16 4 8 5992.120 5830.400 189.915 7.548 o 16 4 9 247.397 493.349 56.925 88.854 o 16 4 10 12479.900 11831.400 278.833 3.707 o 16 4 11 184.413 278.297 37.950 160.071 o 16 4 12 77.250 284.617 37.949 156.910 o 16 4 13 74.425 151.796 25.299 297.026 o 16 6 0 429.793 303.900 29.160 150.550 o 16 6 1 1736.410 1857.850 64.000 24.849 o 16 6 2 2814.550 3265.150 104.403 13.948 o 16 6 3 1578.280 1666.980 71.573 27.397 o 16 6 4 1525.090 1938.990 76.046 23.591 o 16 6 5 15306.200 15115.000 248.759 2.990 o 16 6 6 454.110 634.795 44.726 71.912 o 16 6 7 4766.630 4411.810 116.318 10.354 o 16 6 8 222.096 377.829 33.320 121.180 o 16 6 9 258.979 323.952 56.925 129.941 o 16 6 10 827.894 806.545 50.605 56.534 o 16 6 11 10056.200 8750.840 196.435 5.140 o 16 6 12 4.669 139.144 25.299 322.964 o 16 8 0 1467.220 1643.970 69.228 27.838 o 16 8 1 3476.600 3372.900 145.547 13.028 o 16 8 2 10728.400 10442.300 190.349 4.358 o 16 8 3 576.194 507.338 47.440 88.473 o 16 8 4 6983.940 6650.170 148.798 6.850 o 16 8 5 3908.860 3866.140 100.616 11.882 o 16 8 6 570.302 760.164 47.440 60.188 o 16 8 7 68.997 47.436 17.889 919.622 o 16 8 8 10589.700 9658.220 221.810 4.621 o 16 8 9 75.368 183.420 25.299 248.061 o 16 10 0 931.141 1373.050 42.501 34.021 o 16 10 1 3243.220 3511.450 82.697 13.194 o 16 10 2 3441.030 3404.990 113.921 13.296 o 16 10 3 1532.080 1650.790 66.430 27.806 o 16 10 4 580.968 518.695 37.953 88.312 o 17 1 0 10630.300 10117.200 97.449 4.642 o 17 1 1 6683.990 6493.130 79.195 7.225 o 17 1 2 16927.900 16465.800 233.502 2.772 o 17 1 3 8125.620 8181.010 127.759 5.663 o 17 1 4 5358.090 6402.340 124.693 7.197 o 17 1 5 31599.800 31627.500 259.836 1.468 o 17 1 6 746.467 688.367 31.283 67.682 o 17 1 7 4643.010 4742.320 112.199 9.684 o 17 1 8 15174.500 15453.900 246.879 2.930 o 17 1 9 536.907 545.002 32.867 84.912 o 17 1 10 2042.950 2699.640 82.672 17.041 o 17 1 11 12086.300 12402.700 199.357 3.682 o 17 1 12 1089.080 1088.200 49.204 42.401 o 17 1 13 3747.150 3794.980 120.249 11.930 o 17 1 14 1533.190 1651.180 35.513 28.470 o 17 3 0 443.170 541.402 31.041 85.736 o 17 3 1 4363.970 4834.290 104.022 9.551 o 17 3 2 17029.500 16902.900 227.353 2.709 o 17 3 3 1677.860 1521.300 64.750 30.124 o 17 3 4 2052.810 2498.680 76.181 18.456 o 17 3 5 6761.010 6362.330 117.887 7.261 o 17 3 6 2485.380 2723.990 94.754 16.724 o 17 3 7 4211.920 4689.640 164.549 9.431 o 17 3 8 5339.140 5488.010 183.567 8.024 o 17 3 9 4969.580 4721.860 164.569 9.368 o 17 3 10 3912.840 4100.940 151.887 10.802 o 17 3 11 7455.130 8061.130 215.301 5.491 o 17 3 12 152.434 132.823 31.625 325.729 o 17 3 13 1372.980 1252.620 63.264 36.389 o 17 5 0 305.253 433.979 32.999 106.026 o 17 5 1 441.874 545.540 48.827 82.420 o 17 5 2 1487.260 1922.060 80.865 23.677 o 17 5 3 745.123 686.026 35.768 67.537 o 17 5 4 1273.530 1592.710 65.267 28.827 o 17 5 5 9874.490 9955.650 185.514 4.571 o 17 5 6 3346.850 3720.470 126.559 12.097 o 17 5 7 9837.940 9943.860 193.196 4.560 o 17 5 8 4047.590 3575.780 98.452 12.827 o 17 5 9 3222.550 3113.380 120.232 14.392 o 17 5 10 975.469 1069.060 69.584 41.970 o 17 5 11 11720.700 11192.900 240.844 3.984 o 17 5 12 4.228 44.273 18.974 973.275 o 17 7 0 681.593 732.240 49.200 62.186 o 17 7 1 67.059 166.634 31.306 265.285 o 17 7 2 14730.800 15311.800 251.011 2.951 o 17 7 3 289.974 1363.400 62.614 33.646 o 17 7 4 1603.030 1679.400 104.384 26.099 o 17 7 5 2004.620 2272.430 80.526 20.157 o 17 7 6 1485.930 1400.420 58.153 32.866 o 17 7 7 2498.560 2602.870 78.201 17.706 o 17 7 8 7470.170 6997.980 189.990 6.368 o 17 7 9 96.273 132.822 31.624 326.121 o 17 7 10 3478.680 2867.200 94.940 15.910 o 17 9 0 375.166 632.514 56.926 70.489 o 17 9 1 3889.170 3645.440 132.907 12.262 o 17 9 2 5198.750 4697.160 151.930 9.510 o 17 9 3 1722.620 1720.850 82.247 26.260 o 17 9 4 774.675 1442.270 53.675 32.126 o 17 9 5 11912.300 11586.500 172.538 3.974 o 17 9 6 338.156 417.463 37.951 108.919 o 18 0 0 22699.400 21743.000 275.964 2.097 o 18 0 2 10450.900 10977.200 214.469 4.110 o 18 0 4 15617.200 14378.700 262.678 3.116 o 18 0 6 9463.820 11585.500 253.358 3.832 o 18 0 8 9732.300 9526.480 247.030 4.611 o 18 0 10 5512.790 5836.410 177.245 7.614 o 18 0 12 246.007 253.000 37.950 174.835 o 18 0 14 6690.950 6191.840 103.009 7.507 o 18 2 0 12.817 39.877 11.220 1145.960 o 18 2 1 5289.960 4955.910 67.519 9.468 o 18 2 2 2317.950 2727.440 78.204 16.924 o 18 2 3 7808.260 7579.680 144.880 6.053 o 18 2 4 1569.900 1797.250 46.973 26.006 o 18 2 5 10433.900 11791.600 141.650 3.946 o 18 2 6 1844.520 3008.800 99.038 15.160 o 18 2 7 5855.870 6177.280 108.268 7.506 o 18 2 8 324.809 444.700 33.257 103.490 o 18 2 9 5190.800 5987.420 104.598 7.752 o 18 2 10 207.752 162.976 22.015 280.230 o 18 2 11 9947.300 9454.390 130.417 4.913 o 18 2 12 0.975 378.955 21.910 123.579 o 18 2 13 2907.350 2972.100 48.968 15.810 o 18 4 0 11450.400 11080.700 139.553 4.195 o 18 4 1 1750.180 1933.790 57.030 24.031 o 18 4 2 6602.270 6064.310 125.125 7.580 o 18 4 3 61.808 67.923 18.402 656.850 o 18 4 4 3822.990 3951.850 107.118 11.584 o 18 4 5 1176.030 1526.170 85.399 29.324 o 18 4 6 1642.670 1531.620 67.101 29.856 o 18 4 7 5.419 91.709 22.361 484.977 o 18 4 8 16666.900 16340.900 348.759 2.659 o 18 4 9 241.517 252.999 37.950 174.844 o 18 4 10 8128.960 7504.890 196.330 5.939 o 18 4 11 192.386 309.923 37.950 144.671 o 18 4 12 1436.780 1379.180 69.592 32.928 o 18 6 0 1458.240 1491.490 69.227 30.564 o 18 6 1 1541.150 1711.440 73.708 26.655 o 18 6 2 1967.410 2080.040 80.525 21.946 o 18 6 3 3888.640 3837.000 272.125 9.927 o 18 6 4 64.985 328.890 35.779 137.751 o 18 6 5 13020.000 12971.100 266.174 3.426 o 18 6 6 995.905 1252.020 55.778 36.756 o 18 6 7 3165.860 2856.470 82.689 16.119 o 18 6 8 935.382 1046.760 46.807 44.165 o 18 6 9 3243.940 3472.860 82.694 13.336 o 18 6 10 106.728 120.173 25.299 369.776 o 18 8 0 5704.430 5570.790 183.583 7.913 o 18 8 1 478.261 702.100 63.252 63.053 o 18 8 2 8037.960 7566.530 149.966 6.048 o 18 8 3 1660.310 1775.030 67.102 25.901 o 18 8 4 3550.780 3648.630 93.974 12.622 o 18 8 5 3577.050 3494.600 89.502 13.197 o 18 8 6 2518.430 2497.370 69.244 18.551 o 18 8 7 44.560 88.547 25.299 491.217 o 18 10 0 1044.660 1480.310 69.587 30.798 o 18 10 1 1801.910 1828.560 75.926 24.952 o 19 1 0 5413.350 5295.690 73.741 8.850 o 19 1 1 1405.990 1454.300 50.221 31.926 o 19 1 2 4405.130 4739.350 95.906 9.777 o 19 1 3 3022.440 3468.180 427.123 8.191 o 19 1 4 1176.620 1125.270 41.677 41.348 o 19 1 5 3749.040 3648.180 80.700 12.721 o 19 1 6 565.351 630.067 32.867 73.714 o 19 1 7 527.602 1414.040 58.144 32.622 o 19 1 8 1784.540 1903.380 55.929 24.424 o 19 1 9 3310.370 3740.710 98.440 12.287 o 19 1 10 49.769 31.624 17.889 1326.450 o 19 1 11 9633.600 10020.000 163.454 4.587 o 19 1 12 852.052 1082.030 44.730 42.869 o 19 1 13 587.998 592.838 22.139 79.201 o 19 3 0 3320.750 3482.680 85.591 13.275 o 19 3 1 579.260 685.690 41.142 67.113 o 19 3 2 8278.810 7990.160 148.440 5.743 o 19 3 3 2870.430 2905.560 83.915 15.846 o 19 3 4 3225.470 3394.760 95.902 13.517 o 19 3 5 6784.870 6838.060 147.737 6.674 o 19 3 6 4450.780 4303.740 158.226 10.268 o 19 3 7 405.302 354.208 50.601 122.579 o 19 3 8 3409.730 3499.430 139.218 12.670 o 19 3 9 2435.790 2467.600 107.562 18.148 o 19 3 10 1119.140 1151.320 69.585 39.118 o 19 3 11 2253.990 2277.810 94.909 19.836 o 19 3 12 1021.770 1088.070 56.934 42.021 o 19 5 0 1165.680 1211.810 62.623 37.608 o 19 5 1 1096.550 1104.870 47.197 41.870 o 19 5 2 8523.150 9185.290 144.816 5.027 o 19 5 3 4110.140 3833.630 170.875 11.284 o 19 5 4 517.377 458.972 37.820 99.381 o 19 5 5 13078.100 12274.300 210.475 3.702 o 19 5 6 2436.760 2895.970 87.156 15.865 o 19 5 7 2522.530 2807.180 85.007 16.374 o 19 5 8 1741.140 1812.580 75.919 25.163 o 19 5 9 4709.290 4601.810 139.257 9.791 o 19 5 10 1188.740 1473.990 69.588 30.916 o 19 5 11 9912.240 9170.760 196.471 4.919 o 19 7 0 12030.400 11752.800 208.310 3.862 o 19 7 1 541.122 755.989 49.199 60.347 o 19 7 2 11182.100 10722.700 194.845 4.240 o 19 7 3 77.068 149.239 26.834 299.878 o 19 7 4 276.524 321.464 33.321 141.414 o 19 7 5 2909.590 3152.050 218.309 12.625 o 19 7 6 2711.920 2657.640 107.571 16.919 o 19 7 7 956.328 974.180 63.258 46.284 o 19 7 8 4097.290 3848.570 113.938 11.826 o 19 9 0 752.036 740.095 56.930 60.714 o 19 9 1 1036.130 948.892 63.259 47.440 o 19 9 2 1679.900 1524.750 75.921 29.683 o 19 9 3 7938.890 7512.990 177.372 6.003 o 19 9 4 16.896 252.991 31.624 179.013 o 20 0 0 22930.800 22944.500 358.310 1.937 o 20 0 2 12623.400 13312.300 250.872 3.368 o 20 0 4 1566.930 1582.400 76.503 28.637 o 20 0 6 1107.500 4352.160 151.819 10.235 o 20 0 8 10989.100 12639.200 291.431 3.465 o 20 0 10 2775.270 2752.510 107.569 16.365 o 20 0 12 4107.650 4006.700 120.264 11.327 o 20 2 0 1864.840 2313.690 50.797 20.235 o 20 2 1 137.890 247.332 26.221 185.493 o 20 2 2 391.815 377.995 31.302 121.484 o 20 2 3 5117.800 4664.200 107.828 9.863 o 20 2 4 174.454 327.335 25.562 141.538 o 20 2 5 12512.600 12826.300 170.401 3.602 o 20 2 6 2573.920 2532.230 65.551 18.345 o 20 2 7 45.175 273.473 30.171 166.827 o 20 2 8 31.041 131.086 21.279 347.423 o 20 2 9 6931.830 7509.930 114.505 6.188 o 20 2 10 158.050 327.141 21.910 142.584 o 20 2 11 10351.600 10247.300 184.003 4.451 o 20 2 12 3.194 182.868 12.649 257.349 o 20 4 0 19127.800 18146.000 250.039 2.512 o 20 4 1 687.628 450.074 34.361 101.842 o 20 4 2 19889.900 19149.000 291.163 2.352 o 20 4 3 600.585 626.782 44.727 72.744 o 20 4 4 20.919 566.896 66.410 76.335 o 20 4 5 144.420 149.240 26.834 299.480 o 20 4 6 1492.350 1617.390 67.100 28.339 o 20 4 7 612.953 392.172 44.278 113.539 o 20 4 8 13558.700 13463.300 297.916 3.258 o 20 4 9 2595.040 2568.980 101.240 17.580 o 20 4 10 857.468 790.716 50.606 57.611 o 20 4 11 286.949 246.679 31.626 182.780 o 20 6 0 2539.850 2575.280 91.744 17.692 o 20 6 1 63.627 198.054 28.813 227.834 o 20 6 2 903.649 879.990 49.202 52.086 o 20 6 3 7931.590 8006.240 246.969 5.408 o 20 6 4 80.570 354.190 50.599 122.901 o 20 6 5 5661.900 5444.240 177.254 8.123 o 20 6 6 959.128 1120.380 88.561 38.893 o 20 6 7 1701.440 1698.640 55.786 27.299 o 20 6 8 237.950 215.712 28.463 209.816 o 20 6 9 3975.950 3721.980 107.608 12.267 o 20 8 0 10226.000 9743.980 240.749 4.533 o 20 8 1 21.117 622.150 40.251 74.018 o 20 8 2 7557.980 7140.580 134.343 6.444 o 20 8 3 1826.840 1791.050 58.158 25.872 o 20 8 4 1680.760 1644.950 53.684 28.217 o 20 8 5 1254.740 1417.550 49.207 32.773 o 20 8 6 3139.530 2443.030 82.278 18.753 o 21 1 0 9185.110 8949.530 125.414 5.192 o 21 1 1 260.698 516.748 34.212 89.367 o 21 1 2 3052.590 3020.250 96.531 15.120 o 21 1 3 10852.700 10955.600 230.836 4.084 o 21 1 4 63.881 387.153 27.828 119.796 o 21 1 5 5035.880 5417.330 100.934 8.561 o 21 1 6 957.622 1505.720 76.091 30.071 o 21 1 7 122.089 473.400 29.213 98.185 o 21 1 8 3853.310 3645.360 93.975 12.630 o 21 1 9 3114.910 2939.370 80.542 15.703 o 21 1 10 487.401 509.676 31.308 90.872 o 21 1 11 3951.290 4073.000 85.036 11.399 o 21 1 12 513.084 397.234 16.454 118.308 o 21 3 0 18491.500 17885.700 315.286 2.484 o 21 3 1 1501.470 1418.430 59.558 32.414 o 21 3 2 21088.200 20337.400 302.623 2.213 o 21 3 3 3879.700 4151.990 111.604 11.014 o 21 3 4 397.364 679.117 46.802 67.183 o 21 3 5 6695.800 6432.520 196.268 6.858 o 21 3 6 7302.710 7465.290 215.284 5.896 o 21 3 7 244.335 404.799 50.600 108.571 o 21 3 8 449.711 499.691 50.602 89.146 o 21 3 9 1211.230 1220.930 69.587 36.994 o 21 3 10 196.168 309.923 37.950 144.666 o 21 3 11 2360.850 2562.760 88.589 17.829 o 21 5 0 5209.380 5687.420 108.123 8.137 o 21 5 1 1739.150 1675.990 56.930 27.629 o 21 5 2 6865.190 6735.500 145.037 6.781 o 21 5 3 8997.090 9407.250 176.517 4.846 o 21 5 4 565.634 519.878 47.440 86.462 o 21 5 5 15847.700 15322.500 235.352 2.967 o 21 5 6 2954.690 2497.210 76.065 18.451 o 21 5 7 139.868 293.616 50.599 145.610 o 21 5 8 281.156 531.305 44.275 85.401 o 21 5 9 7349.900 6935.550 164.680 6.524 o 21 7 0 7079.620 7068.800 145.461 6.472 o 21 7 1 556.324 745.468 63.253 59.609 o 21 7 2 7268.960 6891.040 138.806 6.654 o 21 7 3 1607.480 1789.690 66.428 25.715 o 21 7 4 66.721 93.891 19.755 480.242 o 21 7 5 1569.230 1663.880 82.245 27.119 o 21 7 6 3807.220 3652.090 113.930 12.435 o 21 7 7 149.350 88.549 18.975 508.312 o 21 9 0 408.366 404.817 37.952 112.109 o 21 9 1 0.644 259.314 31.624 174.886 o 22 0 0 19605.400 19797.600 352.084 2.226 o 22 0 2 5178.470 5665.120 183.563 7.792 o 22 0 4 1155.030 1473.920 88.562 30.165 o 22 0 6 7823.180 9042.610 234.297 4.877 o 22 0 8 5387.130 6798.680 183.577 6.573 o 22 0 10 70.160 139.146 31.624 312.742 o 22 2 0 431.760 385.041 32.365 119.042 o 22 2 1 1073.970 1144.970 60.095 39.846 o 22 2 2 38.424 733.892 49.195 62.210 o 22 2 3 23279.200 23620.700 229.803 1.960 o 22 2 4 2885.020 3476.730 76.543 13.371 o 22 2 5 7367.560 7536.700 119.275 6.154 o 22 2 6 115.201 348.098 25.562 133.374 o 22 2 7 10.135 75.410 16.755 602.129 o 22 2 8 6.701 50.598 14.606 892.025 o 22 2 9 4207.990 4260.430 91.666 10.871 o 22 2 10 8.164 203.314 18.258 229.233 o 22 4 0 25853.800 24033.200 631.782 1.636 o 22 4 1 941.919 810.474 49.202 56.367 o 22 4 2 13354.300 13080.300 256.674 3.415 o 22 4 3 19.304 63.248 22.361 682.675 o 22 4 4 658.866 1318.780 60.258 34.809 o 22 4 5 768.300 746.892 44.728 61.421 o 22 4 6 2903.270 3037.300 120.227 14.734 o 22 4 7 401.475 1100.580 69.577 40.894 o 22 4 8 9692.650 9623.800 221.747 4.636 o 22 4 9 1268.570 1024.860 56.937 44.474 o 22 4 10 70.492 164.446 25.299 275.312 o 22 6 0 2168.180 2063.050 76.054 22.206 o 22 6 1 309.097 337.334 34.788 134.519 o 22 6 2 785.680 784.571 44.728 58.570 o 22 6 3 9624.870 8463.120 228.048 5.205 o 22 6 4 71.584 50.599 25.299 806.355 o 22 6 5 5702.930 5364.280 107.162 8.616 o 22 6 6 100.038 107.523 17.889 425.174 o 22 6 7 27.806 77.489 15.180 590.994 o 22 8 0 5758.280 6021.130 164.615 7.460 o 22 8 1 143.900 206.776 22.362 222.777 o 22 8 2 5054.060 4784.820 94.010 9.695 o 22 8 3 1912.850 1751.640 51.306 26.578 o 23 1 0 9371.150 9324.670 183.461 4.871 o 23 1 1 1958.330 2529.050 155.002 16.746 o 23 1 2 10038.800 10065.300 259.710 4.349 o 23 1 3 18092.900 19091.200 282.219 2.367 o 23 1 4 382.711 483.774 29.214 95.974 o 23 1 5 8236.860 9027.110 132.810 5.136 o 23 1 6 6838.160 7477.990 116.977 6.208 o 23 1 7 411.034 357.400 31.308 128.203 o 23 1 8 5219.740 5153.790 129.772 8.844 o 23 1 9 8376.380 8011.040 132.074 5.770 o 23 1 10 16.098 31.624 13.417 1400.570 o 23 3 0 13677.300 13566.800 259.853 3.295 o 23 3 1 13.752 284.417 33.319 159.338 o 23 3 2 3902.510 4031.430 126.570 11.208 o 23 3 3 4578.230 4560.550 116.361 10.030 o 23 3 4 947.033 1083.230 136.002 35.975 o 23 3 5 9006.490 9335.930 240.682 4.716 o 23 3 6 6429.630 6470.630 183.609 6.882 o 23 3 7 552.171 841.269 56.928 53.810 o 23 3 8 1510.480 1505.700 75.917 30.049 o 23 3 9 2403.500 2733.570 94.916 16.669 o 23 5 0 3340.530 3336.670 96.126 13.740 o 23 5 1 356.958 413.898 33.321 110.880 o 23 5 2 4639.210 4453.910 145.576 10.048 o 23 5 3 7598.820 7578.650 174.143 5.963 o 23 5 4 198.499 706.948 40.252 65.345 o 23 5 5 8096.880 8205.110 145.497 5.606 o 23 5 6 1800.000 2031.850 60.271 22.844 o 23 5 7 584.372 468.084 37.953 97.461 o 23 5 8 62.320 69.573 18.974 639.847 o 23 7 0 8855.750 8759.080 154.478 5.242 o 23 7 1 114.225 251.812 37.949 175.866 o 23 7 2 3454.110 3215.170 80.551 14.391 o 23 7 3 1378.440 1796.690 82.243 25.219 o 23 7 4 362.926 417.463 37.951 108.900 o 23 7 5 610.496 657.861 44.279 69.497 o 24 0 0 15669.500 15703.700 348.689 2.756 o 24 0 2 13548.300 13087.500 304.214 3.332 o 24 0 4 762.699 1056.360 69.580 42.468 o 24 0 6 21405.700 21172.100 399.834 2.051 o 24 0 8 5764.920 5812.060 151.949 7.777 o 24 2 0 930.967 973.254 55.777 46.847 o 24 2 1 1093.760 1239.890 88.561 35.422 o 24 2 2 27.690 40.925 14.805 1086.080 o 24 2 3 18225.600 17732.300 209.799 2.601 o 24 2 4 9.406 48.791 15.570 916.522 o 24 2 5 7123.790 7042.980 109.550 6.600 o 24 2 6 381.153 409.830 25.563 113.483 o 24 2 7 340.228 492.680 25.563 94.786 o 24 2 8 1.113 169.994 15.570 274.928 o 24 2 9 7239.550 6422.450 136.182 7.132 o 24 4 0 9475.430 9008.950 174.501 5.055 o 24 4 1 182.135 297.271 33.320 152.509 o 24 4 2 2569.920 2714.410 84.655 16.918 o 24 4 3 1555.040 1666.960 64.748 27.588 o 24 4 4 604.438 859.060 44.727 53.685 o 24 4 5 142.863 224.935 26.834 202.860 o 24 4 6 5846.970 5926.100 158.283 7.604 o 24 4 7 24.106 56.923 25.299 729.968 o 24 4 8 5914.060 5433.420 132.986 8.392 o 24 6 0 871.514 798.418 60.094 56.169 o 24 6 1 1320.040 1360.120 82.240 32.809 o 24 6 2 163.340 246.672 37.950 179.168 o 24 6 3 8399.630 8126.860 202.696 5.492 o 24 6 4 228.109 246.676 31.625 182.909 o 24 6 5 2226.190 1986.870 75.931 23.027 o 24 8 0 5075.370 5001.990 126.633 9.122 o 25 1 0 8937.590 8794.680 285.001 4.832 o 25 1 1 1121.580 1303.120 88.562 33.828 o 25 1 2 88.146 227.694 26.834 200.645 o 25 1 3 9162.000 9407.160 135.203 4.929 o 25 1 4 382.680 576.354 35.599 80.153 o 25 1 5 2724.470 3391.130 69.411 13.755 o 25 1 6 4655.270 5263.970 105.110 8.788 o 25 1 7 250.933 313.121 22.362 148.584 o 25 1 8 989.525 1028.210 40.258 45.244 o 25 3 0 6926.190 6352.780 140.974 7.187 o 25 3 1 232.158 308.939 33.320 146.942 o 25 3 2 3767.210 3823.700 100.611 12.010 o 25 3 3 6788.050 6688.990 246.933 6.361 o 25 3 4 1461.620 1746.050 88.568 25.716 o 25 3 5 2246.690 2132.250 94.907 21.116 o 25 3 6 3694.160 3753.060 120.250 12.057 o 25 3 7 2065.750 2119.630 82.254 21.516 o 25 3 8 1211.650 1157.730 56.938 39.569 o 25 5 0 2791.510 2869.020 82.684 16.057 o 25 5 1 1604.490 1485.770 57.641 31.046 o 25 5 2 1286.310 1224.500 51.297 37.712 o 25 5 3 5318.220 5140.100 193.084 8.455 o 25 5 4 915.983 1476.380 51.294 31.461 o 25 5 5 4034.710 3864.740 80.564 12.026 o 25 5 6 2584.250 2271.850 75.939 20.230 o 25 7 0 6623.560 6250.350 136.157 7.322 o 25 7 1 68.055 132.821 25.299 336.973 o 25 7 2 646.459 449.119 37.954 101.359 o 26 0 0 8202.820 8542.850 227.978 5.161 o 26 0 2 4475.820 4145.620 139.242 10.805 o 26 0 4 2131.560 2650.990 107.558 16.968 o 26 0 6 7282.120 7428.570 177.323 6.068 o 26 0 8 3269.220 2772.190 82.280 16.599 o 26 2 0 9.257 18.974 22.361 1873.090 o 26 2 1 3373.110 3206.240 62.329 14.577 o 26 2 2 93.667 33.733 14.607 1294.710 o 26 2 3 8356.240 8475.920 120.555 5.485 o 26 2 4 10.751 76.068 14.606 603.684 o 26 2 5 3042.050 2894.330 65.065 16.097 o 26 2 6 184.601 190.018 16.755 245.080 o 26 2 7 3455.770 3301.530 67.131 14.132 o 26 4 0 8093.200 7823.190 240.654 5.548 o 26 4 1 94.547 190.589 26.834 237.831 o 26 4 2 1763.620 1853.630 107.553 23.716 o 26 4 3 16.399 24.395 15.179 1737.020 o 26 4 4 918.838 948.764 53.769 48.145 o 26 4 5 228.762 126.500 25.300 351.461 o 26 4 6 7881.680 7330.070 164.721 6.190 o 26 6 0 512.799 543.979 50.603 82.291 o 26 6 1 2567.000 2315.990 94.918 19.519 o 26 6 2 40.935 170.769 25.299 265.731 o 26 6 3 4640.900 4235.490 120.290 10.741 o 27 1 0 3617.390 3596.100 98.446 12.761 o 27 1 1 2733.620 2799.560 75.401 16.527 o 27 1 2 509.266 650.914 31.502 71.548 o 27 1 3 3886.940 3688.320 70.582 12.651 o 27 1 4 583.667 618.894 27.830 75.472 o 27 1 5 1431.230 1418.510 46.812 32.806 o 27 1 6 3207.420 2838.440 62.651 16.428 o 27 3 0 7462.360 6755.180 136.514 6.790 o 27 3 1 1329.160 1541.870 58.152 29.950 o 27 3 2 344.275 243.558 26.835 187.481 o 27 3 3 3522.840 3151.670 113.916 14.306 o 27 3 4 3358.000 3550.380 113.916 12.777 o 27 3 5 409.217 360.540 37.952 125.161 o 27 5 0 2009.360 2256.160 64.756 20.555 o 27 5 1 1163.170 1159.520 44.065 40.067 o 27 5 2 157.238 98.138 17.890 463.276 o 27 5 3 6555.040 5823.140 167.834 7.681 o 28 0 0 4824.220 5899.260 164.572 7.607 o 28 0 2 77.254 63.248 25.299 663.870 o 28 0 4 1447.800 1467.730 69.591 31.027 o 28 2 0 596.664 679.110 26.744 68.965 o 28 2 1 4269.450 4318.150 95.010 10.709 o 28 2 2 411.194 611.339 26.624 76.554 o 28 2 3 6795.370 6674.590 93.656 6.999 o 28 2 4 32.183 18.974 10.955 2308.880 o 28 2 5 176.276 164.693 17.890 281.042 o 28 4 0 7151.230 6404.410 237.481 6.666 o 28 4 1 30.236 41.563 15.180 1066.860 o 28 4 2 31.552 370.243 26.834 125.384 o 28 4 3 277.828 278.448 22.363 166.572 o 29 1 0 3491.730 3685.310 69.229 12.673 o 29 1 1 2677.510 2645.080 55.940 17.677 o 29 1 2 55.286 124.011 15.493 373.972 o 29 1 3 2082.290 2018.720 53.689 23.088 o 29 1 4 896.900 974.849 35.785 47.884 o 29 3 0 3242.690 2967.680 132.898 14.863 o 29 3 1 1281.790 1442.330 94.894 30.482 o 29 3 2 9.067 37.949 18.974 1117.470 o 29 3 3 3192.190 2892.380 88.607 15.859 o 29 5 0 1146.210 873.035 50.611 52.344 o 30 0 0 647.791 980.450 56.929 46.482 o 30 0 2 135.081 132.823 25.300 336.473 o 30 2 0 59.993 93.074 13.694 497.489 o 30 2 1 3780.150 3702.850 148.742 11.913 o 30 2 2 13.828 46.573 10.525 990.749 o 31 1 0 218.493 426.083 19.266 110.291 o 31 1 1 2502.300 2040.950 49.221 22.895 o ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,y,-z+1/2 3 -x,-y,-z 4 x,-y,z-1/2 5 x+1/2,y+1/2,z 6 -x+1/2,y+1/2,-z+1/2 7 -x+1/2,-y+1/2,-z 8 x+1/2,-y+1/2,z-1/2 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_group Cd1 Cd 0.020038(19) 0.86750(5) 0.07930(3) 0.02671(17) Uani 1.000000 . . . . O1 O 0.0195(3) 0.6388(5) 0.0731(3) 0.0488(15) Uani 1.000000 . . . . N1 N 0.1032(13) 0.907(5) 0.066(2) 0.036(6) Uani 0.500000 D U P 1 C1 C 0.1232(12) 0.857(4) 0.010(2) 0.070(12) Uani 0.500000 D U P 1 H1 H 0.1033(12) 0.803(4) -0.028(2) 0.084(14) Uiso 0.500000 R . P 1 O1W O 0.4275(4) 1.0043(10) 0.5187(6) 0.044(2) Uani 0.600000 . . P . H1Wa H 0.444(4) 1.029(16) 0.487(7) 0.065(3) Uiso 0.600000 G . P . H1Wb H 0.449(4) 0.961(15) 0.553(7) 0.065(3) Uiso 0.600000 G . P . O2 O 0.0531(4) 0.7252(6) 0.1861(4) 0.081(3) Uani 1.000000 . . . . N2 N 0.4351(9) 0.650(3) 0.5922(15) 0.029(5) Uani 0.500000 D U P 1 C2 C 0.1719(9) 0.883(3) 0.0092(16) 0.051(6) Uani 0.500000 D U P 1 H2 H 0.1839(9) 0.857(3) -0.0325(16) 0.061(7) Uiso 0.500000 R . P 1 O2W O 0.3007(4) 0.7996(12) 0.1517(8) 0.106(4) Uani 0.900000 . . P . H2Wa H 0.303(7) 0.79(2) 0.200(4) 0.159(6) Uiso 0.900000 G . P . H2Wb H 0.326(5) 0.762(19) 0.143(10) 0.159(6) Uiso 0.900000 G . P . O3 O 0.0330(2) 0.0353(5) 0.1646(3) 0.0354(12) Uani 1.000000 . . . . N3 N 0.2654(7) 1.073(2) 0.2123(14) 0.046(5) Uani 0.500000 D U P 1 H3 H 0.2788(7) 1.032(2) 0.1806(14) 0.055(6) Uiso 0.500000 R . P 1 C3 C 0.2037(10) 0.950(3) 0.0721(16) 0.055(7) Uani 0.500000 D U P 1 H3a H 0.2380(10) 0.961(3) 0.0750(16) 0.066(9) Uiso 0.500000 R . P 1 O4 O 0.0104(2) 0.1444(6) 0.0547(3) 0.0422(14) Uani 1.000000 . . . . N4 N 0.3290(9) 0.888(2) 0.4364(11) 0.052(6) Uani 0.500000 D U P 1 H4 H 0.3608(9) 0.906(2) 0.4462(11) 0.063(7) Uiso 0.500000 R . P 1 C4 C 0.1839(9) 1.002(3) 0.1304(17) 0.049(7) Uani 0.500000 D U P 1 O5 O 0.1039(3) 0.3482(6) 0.3722(3) 0.066(2) Uani 1.000000 . . . . H5 H 0.094(4) 0.404(8) 0.3979(8) 0.099(3) Uiso 1.000000 GR . . . C5 C 0.1334(12) 0.981(6) 0.121(2) 0.037(8) Uani 0.500000 D U P 1 H5a H 0.1186(12) 1.021(6) 0.156(2) 0.044(9) Uiso 0.500000 R . P 1 O6 O 0.1940(6) 1.129(2) 0.2423(11) 0.090(6) Uani 0.500000 D U P 1 C6 C 0.2153(7) 1.072(2) 0.1997(13) 0.049(6) Uani 0.500000 D U P 1 C7 C 0.2988(8) 1.141(2) 0.2793(13) 0.046(5) Uani 0.500000 D U P 1 H7a H 0.2787(8) 1.203(2) 0.2997(13) 0.055(6) Uiso 0.500000 R . P 1 H7b H 0.3240(8) 1.190(2) 0.2618(13) 0.055(6) Uiso 0.500000 R . P 1 O7 O 0.2684(5) 0.7658(18) 0.4565(10) 0.088(6) Uani 0.500000 D U P 1 C8 C 0.3253(9) 1.050(2) 0.3435(14) 0.046(6) Uani 0.500000 D U P 1 H8a H 0.3488(9) 0.997(2) 0.3247(14) 0.055(7) Uiso 0.500000 R . P 1 H8b H 0.3451(9) 1.101(2) 0.3867(14) 0.055(7) Uiso 0.500000 R . P 1 C9 C 0.2894(10) 0.959(3) 0.3743(17) 0.049(7) Uani 0.500000 D U P 1 H9a H 0.2661(10) 1.008(3) 0.3962(17) 0.059(9) Uiso 0.500000 R . P 1 H9b H 0.2704(10) 0.901(3) 0.3341(17) 0.059(9) Uiso 0.500000 R . P 1 C10 C 0.3123(6) 0.7966(17) 0.4739(10) 0.044(4) Uani 0.500000 D U P 1 C11 C 0.4198(11) 0.607(2) 0.6529(15) 0.028(5) Uani 0.500000 D U P 1 H11 H 0.4430(11) 0.563(2) 0.6924(15) 0.033(6) Uiso 0.500000 R . P 1 C12 C 0.3718(11) 0.624(4) 0.6595(18) 0.060(11) Uani 0.500000 D U P 1 H12 H 0.3626(11) 0.596(4) 0.7036(18) 0.072(13) Uiso 0.500000 R . P 1 C13 C 0.3374(9) 0.683(3) 0.5992(13) 0.054(7) Uani 0.500000 D U P 1 H13 H 0.3041(9) 0.693(3) 0.6016(13) 0.065(8) Uiso 0.500000 R . P 1 C14 C 0.3509(6) 0.7275(17) 0.5361(9) 0.035(4) Uani 0.500000 D U P 1 C15 C 0.4052(8) 0.735(3) 0.5427(14) 0.036(6) Uani 0.500000 D U P 1 H15 H 0.4185(8) 0.794(3) 0.5142(14) 0.044(7) Uiso 0.500000 R . P 1 C16 C 0.0398(3) 0.6272(7) 0.1462(4) 0.0322(16) Uani 1.000000 . . . . C17 C 0.0476(3) 0.4961(7) 0.1800(4) 0.0338(17) Uani 1.000000 . . . . C18 C 0.0338(3) 0.3829(7) 0.1369(4) 0.0296(16) Uani 1.000000 . . . . H18 H 0.0182(3) 0.3885(7) 0.0838(4) 0.0355(19) Uiso 1.000000 R . . . C19 C 0.0660(3) 0.2539(8) 0.2502(4) 0.0374(19) Uani 1.000000 . . . . H19 H 0.0725(3) 0.1728(8) 0.2738(4) 0.045(2) Uiso 1.000000 R . . . C20 C 0.0793(4) 0.3650(8) 0.2939(5) 0.049(2) Uani 1.000000 . . . . C21 C 0.0429(3) 0.2632(7) 0.1715(4) 0.0273(15) Uani 1.000000 . . . . C22 C 0.0273(3) 0.1380(7) 0.1270(4) 0.0285(15) Uani 1.000000 . . . . C23 C 0.0699(3) 0.4857(7) 0.2609(4) 0.042(2) Uani 1.000000 . . . . H23 H 0.0781(3) 0.5600(7) 0.2914(4) 0.050(3) Uiso 1.000000 R . . . C10A C 0.3295(6) 0.8830(15) 0.5139(8) 0.037(3) Uani 0.500000 D U P 2 N1A N 0.0993(13) 0.907(5) 0.065(2) 0.037(6) Uani 0.500000 D U P 2 C1A C 0.1150(9) 0.849(2) 0.0072(15) 0.035(5) Uani 0.500000 D U P 2 H1A H 0.0912(9) 0.801(2) -0.0289(15) 0.042(6) Uiso 0.500000 R . P 2 C5A C 0.1356(12) 0.968(6) 0.118(3) 0.046(13) Uani 0.500000 D U P 2 H5Aa H 0.1272(12) 0.998(6) 0.162(3) 0.055(15) Uiso 0.500000 R . P 2 C2A C 0.1625(10) 0.858(4) -0.0026(19) 0.081(12) Uani 0.500000 D U P 2 H2A H 0.1711(10) 0.815(4) -0.0434(19) 0.097(14) Uiso 0.500000 R . P 2 C4A C 0.1840(8) 0.989(3) 0.1140(15) 0.039(5) Uani 0.500000 D U P 2 C3A C 0.1981(9) 0.933(3) 0.0517(16) 0.054(8) Uani 0.500000 D U P 2 H3Aa H 0.2306(9) 0.946(3) 0.0461(16) 0.065(9) Uiso 0.500000 R . P 2 C6A C 0.2173(6) 1.075(2) 0.1721(12) 0.040(4) Uani 0.500000 D U P 2 N3A N 0.2650(6) 1.034(2) 0.2009(13) 0.040(4) Uani 0.500000 D U P 2 H3Ab H 0.2738(6) 0.963(2) 0.1835(13) 0.048(5) Uiso 0.500000 R . P 2 O6A O 0.1987(5) 1.1770(14) 0.1908(9) 0.059(4) Uani 0.500000 D U P 2 C7A C 0.3036(8) 1.105(2) 0.2610(12) 0.046(5) Uani 0.500000 D U P 2 H7Aa H 0.3293(8) 1.140(2) 0.2380(12) 0.055(6) Uiso 0.500000 R . P 2 H7Ab H 0.2877(8) 1.178(2) 0.2801(12) 0.055(6) Uiso 0.500000 R . P 2 C8A C 0.3288(8) 1.016(3) 0.3289(13) 0.049(6) Uani 0.500000 D U P 2 H8Aa H 0.3379(8) 0.935(3) 0.3081(13) 0.059(7) Uiso 0.500000 R . P 2 H8Ab H 0.3599(8) 1.056(3) 0.3591(13) 0.059(7) Uiso 0.500000 R . P 2 C9A C 0.2948(10) 0.984(3) 0.3842(17) 0.050(7) Uani 0.500000 D U P 2 H9Aa H 0.2927(10) 1.061(3) 0.4151(17) 0.060(8) Uiso 0.500000 R . P 2 H9Ab H 0.2608(10) 0.964(3) 0.3531(17) 0.060(8) Uiso 0.500000 R . P 2 N4A N 0.3150(8) 0.872(2) 0.4378(10) 0.047(5) Uani 0.500000 D U P 2 H4A H 0.3171(8) 0.797(2) 0.4175(10) 0.056(6) Uiso 0.500000 R . P 2 O7A O 0.3207(5) 0.9778(12) 0.5497(7) 0.053(3) Uani 0.500000 D U P 2 C14A C 0.3602(6) 0.7733(16) 0.5587(9) 0.033(3) Uani 0.500000 D U P 2 C13A C 0.3481(8) 0.713(3) 0.6197(12) 0.050(6) Uani 0.500000 D U P 2 H13A H 0.3179(8) 0.732(3) 0.6318(12) 0.060(8) Uiso 0.500000 R . P 2 C15A C 0.4002(7) 0.709(3) 0.5323(14) 0.032(5) Uani 0.500000 D U P 2 H15A H 0.3994(7) 0.710(3) 0.4797(14) 0.039(6) Uiso 0.500000 R . P 2 C12A C 0.3822(11) 0.623(3) 0.6634(16) 0.048(9) Uani 0.500000 D U P 2 H12A H 0.3744(11) 0.580(3) 0.7048(16) 0.058(10) Uiso 0.500000 R . P 2 N2A N 0.4385(10) 0.646(3) 0.5839(15) 0.032(5) Uani 0.500000 D U P 2 C11A C 0.4273(11) 0.596(3) 0.6460(16) 0.038(7) Uani 0.500000 D U P 2 H11A H 0.4507(11) 0.542(3) 0.6787(16) 0.046(9) Uiso 0.500000 R . P 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cd1 0.0350(3) 0.0153(3) 0.0261(3) -0.0024(2) 0.00167(19) -0.0007(2) O1 0.089(5) 0.021(3) 0.031(3) 0.014(3) 0.007(3) 0.005(2) N1 0.036(7) 0.032(7) 0.038(7) -0.000(2) 0.008(2) 0.000(2) C1 0.052(9) 0.09(2) 0.076(13) -0.028(6) 0.029(5) -0.046(9) O1W 0.050(6) 0.042(6) 0.038(5) -0.001(5) 0.010(4) 0.001(4) O2 0.151(8) 0.019(3) 0.040(4) -0.018(4) -0.032(4) 0.005(3) N2 0.032(6) 0.026(6) 0.028(6) 0.002(2) 0.009(2) 0.002(2) C2 0.045(8) 0.047(12) 0.064(10) -0.012(5) 0.020(4) -0.020(6) O2W 0.081(7) 0.088(8) 0.126(9) 0.019(6) -0.011(7) -0.006(8) O3 0.052(3) 0.013(2) 0.037(3) -0.004(2) 0.005(2) -0.002(2) N3 0.044(6) 0.041(12) 0.051(8) -0.008(4) 0.009(3) -0.001(5) C3 0.046(8) 0.054(14) 0.066(11) -0.014(5) 0.018(4) -0.023(7) O4 0.061(4) 0.037(3) 0.022(3) -0.003(3) 0.001(2) -0.008(2) N4 0.037(8) 0.060(9) 0.050(9) -0.007(4) -0.006(4) 0.016(5) C4 0.040(7) 0.049(14) 0.055(10) -0.003(4) 0.009(3) -0.012(6) O5 0.130(7) 0.025(3) 0.021(3) -0.000(4) -0.016(3) 0.003(2) C5 0.039(7) 0.026(14) 0.042(10) 0.002(4) 0.005(3) 0.002(6) O6 0.050(7) 0.133(15) 0.087(10) -0.016(6) 0.017(5) -0.065(8) C6 0.043(6) 0.052(12) 0.051(10) -0.009(4) 0.010(3) -0.010(6) C7 0.041(8) 0.038(9) 0.056(8) -0.003(4) 0.007(4) -0.003(4) O7 0.039(5) 0.109(12) 0.098(11) -0.014(4) -0.012(4) 0.058(8) C8 0.046(9) 0.033(10) 0.054(9) -0.002(5) 0.004(4) -0.005(5) C9 0.044(9) 0.046(13) 0.044(11) -0.009(5) -0.010(4) 0.004(6) C10 0.037(5) 0.046(8) 0.044(7) 0.001(3) 0.002(3) 0.006(4) C11 0.045(9) 0.009(9) 0.031(7) -0.004(4) 0.013(3) -0.005(4) C12 0.046(9) 0.09(2) 0.046(10) 0.016(6) 0.022(4) 0.026(8) C13 0.046(8) 0.070(16) 0.047(8) 0.007(5) 0.014(4) 0.017(6) C14 0.034(5) 0.034(8) 0.034(6) 0.001(3) 0.006(3) -0.002(4) C15 0.037(6) 0.033(11) 0.038(9) 0.003(4) 0.008(3) 0.008(5) C16 0.036(4) 0.022(4) 0.035(4) 0.002(3) 0.002(3) -0.003(3) C17 0.043(4) 0.025(4) 0.029(4) -0.008(3) 0.001(3) -0.003(3) C18 0.038(4) 0.023(4) 0.025(3) -0.003(3) 0.002(3) 0.005(3) C19 0.057(5) 0.024(4) 0.025(4) -0.005(4) 0.001(3) 0.008(3) C20 0.083(7) 0.025(4) 0.028(4) -0.003(4) -0.005(4) -0.004(3) C21 0.030(4) 0.019(4) 0.032(4) -0.009(3) 0.005(3) -0.003(3) C22 0.030(4) 0.026(4) 0.030(4) -0.001(3) 0.008(3) 0.001(3) C23 0.068(6) 0.018(4) 0.025(4) -0.006(4) -0.011(4) -0.004(3) C10A 0.030(6) 0.037(6) 0.038(5) 0.000(3) 0.001(3) -0.005(3) N1A 0.036(7) 0.032(7) 0.040(7) 0.000(2) 0.008(2) 0.000(2) C1A 0.035(8) 0.023(10) 0.044(8) 0.002(4) 0.007(3) 0.002(4) C5A 0.037(7) 0.05(3) 0.053(12) -0.003(6) 0.009(4) -0.011(9) C2A 0.043(8) 0.13(2) 0.078(13) -0.026(6) 0.022(4) -0.055(9) C4A 0.033(6) 0.040(10) 0.040(8) 0.001(3) 0.003(3) 0.002(5) C3A 0.032(7) 0.076(16) 0.054(10) -0.008(5) 0.009(4) -0.020(6) C6A 0.036(6) 0.039(7) 0.041(9) -0.000(3) 0.001(3) 0.005(4) N3A 0.034(5) 0.038(10) 0.041(8) -0.002(4) 0.001(3) 0.008(5) O6A 0.042(6) 0.052(7) 0.068(9) 0.008(4) -0.009(5) -0.012(5) C7A 0.032(7) 0.045(10) 0.052(8) 0.001(5) -0.003(4) -0.000(4) C8A 0.036(8) 0.050(13) 0.050(8) 0.000(5) -0.009(4) 0.002(6) C9A 0.040(10) 0.049(12) 0.048(9) -0.002(6) -0.008(5) 0.001(5) N4A 0.050(12) 0.046(8) 0.038(5) 0.008(5) -0.001(3) -0.005(3) O7A 0.058(7) 0.047(6) 0.047(6) 0.012(4) 0.002(5) -0.010(4) C14A 0.030(6) 0.036(6) 0.028(6) -0.001(3) 0.001(3) -0.008(3) C13A 0.042(8) 0.066(12) 0.044(8) 0.009(5) 0.013(4) 0.012(6) C15A 0.036(7) 0.029(10) 0.031(7) 0.001(4) 0.008(3) 0.004(4) C12A 0.043(9) 0.066(16) 0.040(10) 0.009(6) 0.015(5) 0.013(6) N2A 0.036(6) 0.030(6) 0.030(6) 0.002(2) 0.009(2) 0.004(2) C11A 0.041(9) 0.041(14) 0.034(8) 0.003(5) 0.012(4) 0.011(5) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source C 0.01788 0.00908 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.21560 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' Cd 0.13958 4.66053 19.22140 17.64440 4.46100 1.60290 0.59460 6.90890 24.70080 87.48250 5.06940 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.00304 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' N 0.03110 0.01806 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750 0.58260 -11.52900 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' O 0.04960 0.03233 3.04850 2.28680 1.54630 0.86700 13.27710 5.70110 0.32390 32.90890 0.25080 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u 0 0 -1 0.04 0.01 0 0 1 0.03 0.01 0 0 -1 0.02 0 0 0 -2 54.74 0.79 0 0 2 53.92 0.77 0 0 -2 54.68 0.79 0 0 -2 54.84 0.78 0 0 -3 0.03 0.02 0 0 -3 0.03 0.01 0 0 3 0.04 0.02 0 0 -4 120.87 1.75 0 0 4 119.59 1.7 0 0 -4 121.4 1.71 0 0 -5 0.03 0.02 0 0 -5 0.04 0.02 0 0 -6 61.04 1.02 0 0 -7 0 0.03 0 0 7 0.08 0.03 0 0 -8 83.21 1.41 0 0 8 83.06 1.38 0 0 -9 0.02 0.03 0 0 9 0.08 0.04 0 0 -10 4.34 0.24 0 0 10 4.55 0.24 0 0 10 4.4 0.15 0 0 -11 0.01 0.05 0 0 11 0.01 0.03 0 0 -11 0.01 0.03 0 0 12 56.38 0.94 0 0 -12 56.03 0.94 0 0 -12 57.07 1.19 0 0 -13 0.03 0.04 0 0 13 0.03 0.04 0 0 -13 0.06 0.06 0 0 -14 28.46 0.58 0 0 14 27.75 0.58 0 0 -14 28.57 0.82 0 0 15 0.02 0.05 0 0 -15 0.03 0.04 0 0 16 4.67 0.2 0 0 -16 4.87 0.2 0 0 17 0 0.05 0 0 -17 -0.02 0.04 0 0 18 16.22 0.4 0 0 19 0.02 0.04 0 0 20 11.54 0.28 0 -2 0 1.15 0.06 0 -2 0 1.24 0.07 0 -2 -1 56.02 0.83 0 -2 1 56.42 0.87 0 -2 -1 55.08 0.88 0 -2 1 57.16 0.88 0 -2 -1 56.33 0.79 0 -2 -1 56.13 0.86 0 2 -1 57.02 0.79 0 -2 1 57.68 0.86 0 -2 -2 13.69 0.23 0 -2 -2 13.11 0.23 0 -2 -2 13.73 0.3 0 2 -2 13.22 0.25 0 -2 2 13.77 0.23 0 2 2 13.62 0.23 0 -2 -2 13.58 0.27 0 -2 2 13.99 0.29 0 -2 -3 413.38 5.76 0 -2 3 423 5.74 0 2 3 410.33 5.67 0 -2 3 423.12 5.67 0 -2 3 404.74 5.73 0 -2 4 9.88 0.26 0 -2 -4 9.52 0.27 0 -2 4 9.7 0.22 0 2 4 9.49 0.22 0 -2 5 19.02 0.43 0 2 -5 20.15 0.41 0 2 5 19.51 0.4 0 -2 5 19.22 0.39 0 -2 5 19.48 0.43 0 2 -5 19.96 0.42 0 -2 -6 4.38 0.2 0 -2 6 4.22 0.18 0 2 -6 4.25 0.17 0 2 6 3.91 0.16 0 -2 6 3.96 0.16 0 2 -6 4.21 0.17 0 -2 7 25 0.55 0 -2 -7 24.73 0.58 0 2 7 23.74 0.52 0 -2 7 24.38 0.52 0 2 -7 24.02 0.53 0 -2 -8 2.51 0.17 0 -2 8 2.71 0.15 0 2 8 2.55 0.15 0 2 -8 2.55 0.15 0 -2 9 63.83 1.19 0 -2 -9 63.32 1.23 0 2 9 64.32 1.16 0 -2 9 61.69 1.15 0 2 -9 63.01 1.15 0 -2 -10 0.66 0.06 0 -2 -10 0.46 0.09 0 -2 10 0.46 0.09 0 2 10 0.52 0.05 0 -2 -10 0.51 0.05 0 2 -10 0.49 0.05 0 -2 10 0.54 0.05 0 -2 -11 24.51 0.71 0 -2 -11 23.71 0.48 0 -2 11 24.08 0.47 0 2 -11 24.11 0.48 0 2 11 24.52 0.48 0 -2 -11 25.12 0.49 0 2 -11 25.11 0.66 0 -2 -11 24.34 0.66 0 -2 -12 0.78 0.13 0 2 -12 1 0.08 0 2 12 0.87 0.08 0 -2 -12 0.8 0.07 0 -2 12 1.17 0.09 0 -2 -12 0.78 0.08 0 2 -12 1.1 0.14 0 -2 -12 0.71 0.11 0 -2 -13 1.37 0.18 0 -2 13 1.38 0.1 0 -2 -13 1.47 0.1 0 2 13 1.47 0.1 0 2 -13 1.32 0.1 0 -2 -13 1.24 0.1 0 2 -13 1.44 0.16 0 -2 -13 1.4 0.16 0 -2 -14 0.02 0.06 0 2 -14 0.15 0.07 0 -2 -14 0.1 0.06 0 -2 -14 0.11 0.05 0 2 -14 0.14 0.05 0 -2 14 0.12 0.05 0 -2 -14 0.11 0.04 0 2 14 0.17 0.05 0 2 -15 35.67 0.7 0 2 15 36.53 0.71 0 -2 15 36.41 0.71 0 -2 -15 37.07 0.71 0 -2 -15 35.24 0.71 0 -2 -16 0.59 0.08 0 -2 16 0.54 0.08 0 -2 -16 0.56 0.08 0 2 16 0.64 0.08 0 2 -16 0.56 0.08 0 -2 17 18.75 0.44 0 2 17 18.37 0.44 0 -2 -17 17.83 0.43 0 -2 18 1.04 0.09 0 2 18 1.18 0.1 0 -2 -18 1.15 0.09 0 2 19 0.48 0.06 0 -2 19 0.52 0.07 0 -2 -19 0.47 0.06 0 -2 20 0.39 0.05 0 2 20 0.41 0.05 0 -4 0 194.63 2.8 0 -4 0 192.42 2.82 0 -4 0 189.57 2.77 0 -4 0 196.32 2.83 0 -4 1 8.46 0.26 0 -4 1 8.38 0.24 0 -4 -1 8.43 0.27 0 -4 1 8.26 0.27 0 -4 -1 8.35 0.26 0 -4 2 106.48 1.65 0 -4 -2 102.58 1.61 0 -4 2 103.11 1.62 0 -4 -2 106.44 1.67 0 -4 3 1.94 0.13 0 -4 3 1.76 0.12 0 -4 4 41.76 0.82 0 -4 -4 42.91 0.85 0 -4 4 41.11 0.81 0 -4 5 8.57 0.31 0 -4 -5 9.09 0.33 0 -4 5 8.27 0.3 0 4 -5 7.96 0.28 0 -4 6 168.31 2.62 0 -4 6 165.84 2.61 0 4 -6 168.4 2.57 0 -4 -6 169.69 2.67 0 -4 7 0.12 0.05 0 4 -7 0.1 0.05 0 4 -8 28.16 0.68 0 -4 8 28.74 0.54 0 -4 8 28.34 0.55 0 -4 -8 27.58 0.52 0 -4 -8 28.99 0.55 0 -4 -8 28.72 0.54 0 -4 8 28.64 0.72 0 -4 8 28.43 0.72 0 -4 9 0.17 0.07 0 4 -9 0.16 0.06 0 -4 -9 0.31 0.05 0 -4 9 0.14 0.06 0 -4 9 0.16 0.05 0 -4 -9 0.3 0.05 0 4 -10 3.69 0.24 0 -4 10 4.07 0.18 0 -4 -10 4.06 0.16 0 -4 -10 3.96 0.17 0 -4 10 4.27 0.27 0 4 -11 0.07 0.05 0 -4 -11 0.08 0.04 0 -4 -11 0.04 0.04 0 -4 11 0.1 0.06 0 -4 -12 37.39 0.71 0 -4 -12 35.11 1.01 0 -4 12 36.59 0.98 0 -4 -13 5.54 0.22 0 -4 -13 5.25 0.36 0 -4 13 4.96 0.33 0 -4 -14 90.34 1.47 0 -4 15 4.17 0.2 0 -4 -15 4.37 0.19 0 -4 16 0.32 0.07 0 -4 -16 0.28 0.06 0 -4 17 0.13 0.05 0 -4 -17 0.18 0.05 0 -4 -18 14.48 0.35 0 -4 -19 0.24 0.05 0 -6 0 28.15 0.68 0 -6 2 10.08 0.26 0 -6 2 9.98 0.37 0 -6 3 51.65 0.86 0 -6 3 53.03 1.07 0 6 -3 51.45 0.99 0 -6 3 50.83 1.02 0 -6 4 8.94 0.25 0 -6 4 9.07 0.25 0 -6 4 8.45 0.36 0 -6 4 9.17 0.35 0 6 -4 8.69 0.33 0 -6 5 6.03 0.3 0 6 -5 5.86 0.28 0 -6 5 5.99 0.21 0 -6 5 6.34 0.21 0 -6 5 6.94 0.31 0 -6 5 6.61 0.33 0 -6 -5 6.06 0.2 0 -6 -5 6.31 0.2 0 -6 -6 6.65 0.35 0 6 -6 6.4 0.3 0 -6 6 6.61 0.22 0 -6 6 6.9 0.23 0 -6 6 7 0.35 0 -6 6 7.13 0.34 0 -6 -6 6.52 0.22 0 -6 -6 7.41 0.23 0 -6 7 1.13 0.15 0 -6 -7 1.33 0.16 0 6 -7 1.21 0.14 0 -6 7 0.98 0.09 0 -6 7 0.98 0.09 0 -6 7 0.96 0.09 0 -6 7 0.89 0.13 0 -6 -7 1.2 0.1 0 -6 -7 1.24 0.09 0 -6 8 2.45 0.14 0 -6 8 2.28 0.13 0 -6 8 2.45 0.14 0 -6 8 2.45 0.21 0 -6 8 2.29 0.22 0 6 -8 2.48 0.2 0 -6 -8 2.73 0.24 0 -6 -8 2.52 0.14 0 -6 9 86.13 1.42 0 -6 9 86.16 1.42 0 -6 9 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19.62 0.46 1 -1 -15 19.41 0.45 1 1 -14 6.59 0.23 -1 1 14 6.06 0.22 -1 -1 14 6.01 0.22 1 -1 -14 6.4 0.23 1 -1 -14 6.05 0.35 1 1 -14 6.02 0.34 1 -1 -14 6.27 0.22 1 -1 -13 1.24 0.09 -1 -1 13 1.2 0.09 -1 1 13 1.11 0.09 1 1 -13 1.2 0.09 1 -1 -13 1.12 0.09 1 1 -13 1.07 0.14 1 -1 -13 1.09 0.14 1 -1 -12 31.53 0.84 1 -1 -12 31.52 0.6 1 1 -12 31.64 0.6 -1 -1 12 32.73 0.6 -1 1 12 32.23 0.6 1 -1 -12 32.08 0.61 1 -1 -12 33.72 0.83 1 1 -12 32.79 0.82 1 -1 -11 28.83 0.75 1 1 -11 28.53 0.53 -1 -1 11 28.68 0.53 -1 1 11 28.82 0.53 1 -1 -11 28.91 0.54 1 -1 -11 28.04 0.54 1 -1 -11 28.94 0.72 1 1 -11 28.47 0.71 1 -1 -10 4.72 0.25 -1 -1 10 4.51 0.15 1 -1 -10 4.38 0.15 1 1 -10 4.51 0.15 -1 1 10 4.66 0.15 1 -1 -10 4.54 0.15 1 1 -10 4.7 0.23 1 -1 -10 4.48 0.23 1 -1 -9 129.1 2.09 -1 -1 9 129.01 2.04 -1 1 9 128.9 2.04 -1 -1 9 126.25 2.04 1 -1 -8 44.61 0.89 1 1 -8 44.93 0.85 -1 -1 8 46.56 0.86 -1 -1 8 46.28 0.86 -1 1 8 45.94 0.86 1 1 -7 5.04 0.19 1 -1 -7 5.24 0.22 -1 -1 7 5.06 0.2 1 1 -7 4.86 0.19 -1 -1 7 5.02 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61.65 0.93 2 2 -2 59.72 0.91 -2 -2 1 30.73 0.52 -2 -2 1 30.44 0.5 2 -2 -1 31.03 0.5 2 -2 -1 30.1 0.54 2 -2 -1 30.47 0.53 -2 -2 1 29.99 0.47 -2 -2 1 30.54 0.5 2 -2 -1 30.59 0.47 2 2 -1 30.85 0.49 -2 -2 0 25.36 0.43 -2 -2 0 24.99 0.41 2 -2 0 26.07 0.38 2 2 0 25.16 0.38 -2 -2 0 25.61 0.43 2 2 0 25.15 0.4 -2 -2 0 25.35 0.4 2 -2 0 25.27 0.44 2 -2 0 24.94 0.46 2 -2 0 24.91 0.45 -2 -2 0 24.58 0.42 -2 -2 -1 119.74 1.72 -2 2 -1 117.09 1.72 -2 -2 -1 121.68 1.68 2 -2 1 122.47 1.73 -2 -2 -1 117.74 1.65 2 2 1 119.14 1.64 -2 -2 -1 119.99 1.68 -2 2 -2 44.58 0.72 -2 -2 -2 45.08 0.73 2 -2 2 43.54 0.73 -2 -2 -2 43.56 0.66 -2 -2 -3 255.48 3.64 2 -2 3 259.48 3.63 -2 -2 -4 0.26 0.05 2 -2 4 0.17 0.04 2 -2 4 0.18 0.04 -2 2 -5 18.98 0.41 2 -2 5 19.76 0.43 -2 -2 -5 19.25 0.46 2 2 5 19.33 0.41 2 -2 5 18.71 0.4 2 -2 5 19.33 0.44 -2 2 -6 42.64 0.81 -2 -2 -6 43.17 0.85 2 -2 6 43.34 0.8 2 2 6 44.33 0.78 2 -2 6 42.86 0.77 2 -2 6 44.47 0.82 2 -2 7 76.29 1.27 -2 2 -7 73 1.28 -2 -2 -7 75.01 1.33 2 -2 7 75.64 1.25 2 2 7 75.45 1.25 -2 2 -7 76.13 1.25 -2 -2 -8 0.25 0.07 -2 2 -8 0.24 0.06 2 2 8 0.27 0.06 2 -2 8 0.29 0.06 -2 -2 -9 94.3 1.42 -2 -2 -9 93.54 1.69 2 -2 9 94.18 1.59 2 2 9 93.42 1.6 -2 -2 -10 2.99 0.13 2 -2 10 2.78 0.2 -2 -2 -10 2.92 0.22 2 -2 10 2.64 0.18 2 -2 10 2.81 0.12 2 2 10 2.86 0.19 2 2 10 2.81 0.12 -2 -2 -11 5.47 0.19 -2 -2 -11 5.28 0.31 -2 -2 -11 5.41 0.18 -2 2 -11 5.51 0.18 2 -2 11 4.81 0.17 2 2 11 5.09 0.18 2 -2 11 5.09 0.28 2 2 11 4.49 0.26 -2 -2 -12 0.88 0.14 -2 2 -12 1.13 0.09 2 2 12 1.13 0.09 2 -2 12 1.1 0.09 -2 -2 -12 1.11 0.09 -2 -2 -12 1.06 0.09 -2 2 -12 1.07 0.14 -2 -2 -12 1.18 0.14 -2 -2 -13 16.79 0.65 2 -2 13 16.27 0.39 2 2 13 16.19 0.39 -2 -2 -13 16.75 0.4 -2 2 -13 16.39 0.4 -2 -2 -13 16.92 0.41 -2 -2 -13 16.59 0.59 -2 2 -13 16.81 0.59 -2 -2 -14 2.46 0.25 -2 -2 -14 2.91 0.15 -2 2 -14 2.59 0.23 -2 -2 -14 2.78 0.24 2 2 14 2.93 0.15 2 -2 14 2.79 0.15 -2 -2 -14 2.85 0.15 -2 2 -14 2.78 0.15 -2 2 -15 50.22 0.91 -2 -2 -15 50.67 0.91 2 -2 15 50.99 0.91 2 2 15 50.93 0.91 -2 -2 -15 49.48 0.91 -2 -2 -16 0.29 0.06 2 2 16 0.31 0.06 2 -2 16 0.28 0.06 -2 2 -16 0.28 0.06 -2 -2 -16 0.34 0.06 -2 -2 -17 15.88 0.39 2 -2 17 15.87 0.39 -2 2 -17 15.78 0.39 2 2 17 15.49 0.39 -2 -2 -17 15.19 0.39 -2 -2 -18 0.41 0.06 2 -2 18 0.43 0.06 2 2 18 0.44 0.06 2 2 19 2.23 0.11 2 -2 19 2.21 0.11 -2 -2 -19 2.27 0.11 2 -4 -19 0.02 0.03 2 -4 -18 9.4 0.27 -2 -4 17 0.45 0.07 2 -4 -17 0.39 0.06 2 -4 -16 0.91 0.09 -2 -4 16 0.98 0.1 2 -4 -15 3.25 0.17 -2 -4 15 3.27 0.18 2 -4 -14 56.29 0.99 -2 -4 14 55.7 1.01 2 -4 -13 2.03 0.13 2 -4 -13 1.92 0.22 -2 -4 13 2.08 0.22 2 -4 -12 5.01 0.2 2 -4 -12 5.26 0.2 2 -4 -11 4.43 0.3 2 -4 -11 4.52 0.18 2 -4 -11 4.87 0.19 -2 -4 11 4.72 0.3 -2 -4 10 0.11 0.06 2 -4 -10 0.12 0.04 2 4 -10 0.09 0.05 2 -4 -10 0.1 0.06 2 -4 -10 0.13 0.04 2 4 -9 0.96 0.12 2 -4 -9 1.12 0.14 -2 -4 9 1.05 0.09 -2 -4 9 1.02 0.13 2 -4 -9 1.11 0.08 2 -4 -9 1.07 0.08 -2 -4 8 48.83 0.84 -2 -4 8 50.46 0.84 -2 -4 8 49.09 1.03 2 -4 -8 51.07 0.83 2 -4 -8 49.74 1.08 2 4 -8 48.69 1 -2 -4 7 10.04 0.37 -2 -4 7 10.44 0.37 2 4 -7 10.5 0.35 2 -4 -7 10.78 0.4 -2 -4 6 70.18 1.28 -2 -4 6 72.39 1.31 2 -4 -6 74.39 1.35 2 4 -6 72.23 1.26 -2 -4 5 2.15 0.15 -2 -4 5 2.23 0.15 2 -4 -5 2.45 0.17 2 4 -5 2.28 0.14 -2 -4 4 9.02 0.29 -2 -4 4 9.14 0.31 2 -4 -4 9.39 0.32 2 -4 -4 8.7 0.29 2 4 -4 9.38 0.28 -2 -4 4 8.87 0.29 -2 -4 3 1.24 0.1 -2 -4 3 1.24 0.1 2 4 -3 1.06 0.08 -2 -4 3 1.18 0.09 2 -4 -3 1.17 0.11 2 -4 -3 1.18 0.1 -2 -4 2 109.2 1.67 -2 -4 2 108.35 1.7 2 -4 -2 108.86 1.74 2 -4 -2 108.75 1.71 2 4 -2 108.9 1.64 -2 -4 2 108.86 1.67 -2 -4 1 5.3 0.2 2 -4 -1 5.36 0.19 2 -4 -1 5.16 0.21 2 -4 -1 5.7 0.22 2 -4 0 196.17 2.86 -2 -4 0 193.56 2.84 2 -4 0 199.88 2.9 2 -4 0 195.02 2.9 -2 -4 0 197.63 2.86 2 -4 1 22.37 0.49 -2 -4 -1 21.4 0.46 2 -4 1 22.2 0.51 2 -4 1 22.38 0.48 2 -4 2 140.18 2.14 2 -4 2 139.7 2.16 2 -4 2 139.97 2.12 -2 -4 -2 138.99 2.14 2 -4 3 12.57 0.36 -2 -4 -3 12.17 0.36 2 -4 3 12.23 0.35 2 -4 4 337.35 4.99 2 -4 4 355.88 4.97 2 -4 5 5.37 0.25 2 -4 5 5.86 0.25 2 -4 6 246.56 3.7 -2 -4 -6 246.87 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0.96 0.07 27 -1 4 1 0.08 27 1 5 2.21 0.1 27 -1 5 2.28 0.11 27 1 6 4.48 0.14 27 -1 6 4.49 0.14 27 -3 -15 0.99 0.07 -27 -3 15 0.62 0.07 -27 -3 14 1.88 0.11 -27 -3 13 0.35 0.05 -27 -3 13 0.45 0.07 -27 -3 12 3.31 0.13 -27 -3 12 2.9 0.15 -27 -3 11 1.52 0.09 -27 -3 11 1.38 0.11 -27 -3 10 0.3 0.05 -27 -3 10 0.23 0.06 -27 -3 9 2.94 0.14 -27 -3 9 2.77 0.15 -27 -3 8 5.11 0.19 -27 -3 8 4.75 0.2 -27 -3 8 4.51 0.2 -27 -3 7 0.14 0.05 -27 -3 7 0.12 0.06 -27 -3 6 6.57 0.22 -27 -3 6 6.52 0.25 -27 -3 6 6.68 0.23 -27 -3 5 3.81 0.16 -27 -3 5 3.82 0.19 -27 -3 5 3.86 0.17 -27 -3 4 1.83 0.13 -27 -3 4 2.01 0.13 -27 -3 3 2.81 0.16 -27 -3 3 2.86 0.15 -27 -3 2 3.36 0.17 -27 -3 2 3.11 0.15 -27 -3 1 1.46 0.11 -27 -3 1 1.5 0.11 -27 -3 0 10.5 0.31 -27 -3 0 10.82 0.3 -27 -3 -1 2.36 0.13 -27 -3 -1 2.51 0.13 -27 -3 -2 0.38 0.06 -27 -3 -2 0.39 0.06 -27 -3 -3 4.98 0.18 -27 -3 -4 5.61 0.18 -27 -3 -5 0.57 0.06 -27 -5 13 0.05 0.03 -27 -5 13 0.06 0.03 -27 -5 12 0.92 0.06 -27 -5 12 0.76 0.07 -27 -5 11 2.92 0.11 -27 -5 11 2.44 0.12 -27 -5 10 0.22 0.04 -27 -5 10 0.17 0.05 -27 -5 9 2.77 0.12 -27 -5 9 2.92 0.14 -27 -5 8 1.15 0.08 -27 -5 8 1.18 0.1 -27 -5 7 0.27 0.05 -27 -5 7 0.25 0.05 -27 -5 6 2.28 0.11 -27 -5 6 2.22 0.13 -27 -5 5 6.23 0.22 -27 -5 5 6.24 0.21 -27 -5 4 1.43 0.11 -27 -5 3 5.09 0.2 -27 -5 2 0.98 0.09 -27 -5 1 0.5 0.06 -27 -5 1 0.7 0.06 -27 -5 0 3.67 0.15 -27 -5 0 3.47 0.14 -27 -5 -1 1.88 0.11 -27 -5 -1 1.8 0.09 -27 -5 -2 0.16 0.04 -27 -5 -2 0.15 0.04 -27 -5 -3 9.44 0.22 -27 -5 -3 8.91 0.23 -27 -7 6 5.88 0.17 -27 -7 5 1.06 0.07 -28 0 15 -0.03 0.03 -28 0 14 2.65 0.11 -28 0 13 0.02 0.03 -28 0 12 2.68 0.13 -28 0 11 0 0.04 -28 0 10 1.08 0.09 -28 0 9 0.01 0.04 -28 0 8 11.46 0.31 -28 0 7 0 0.05 -28 0 6 18.79 0.43 -28 0 5 0.08 0.05 -28 0 4 1.79 0.12 -28 0 4 1.76 0.12 -28 0 3 0 0.04 -28 0 2 8.77 0.29 -28 0 2 9.44 0.28 -28 0 1 0.01 0.04 28 0 0 9.32 0.26 28 0 1 0 0.04 28 0 2 0.1 0.04 28 0 3 0.01 0.03 28 0 4 2.32 0.11 28 0 5 0.04 0.03 -28 -2 15 1.24 0.08 -28 -2 14 0.1 0.04 -28 -2 14 0.15 0.03 -28 2 14 0.18 0.03 -28 -2 13 0.07 0.04 -28 -2 13 0.16 0.04 -28 2 13 0.13 0.03 -28 -2 12 0.08 0.05 -28 -2 12 0.12 0.04 -28 2 12 0.06 0.04 -28 -2 11 5.69 0.18 -28 -2 11 5.51 0.18 -28 2 11 5.73 0.18 -28 -2 10 0.07 0.04 -28 2 10 0.05 0.04 -28 -2 10 0.05 0.04 -28 -2 9 4.58 0.17 -28 -2 9 4.49 0.17 -28 2 9 4.7 0.17 -28 -2 8 0.26 0.05 -28 2 8 0.31 0.06 -28 -2 8 0.2 0.05 -28 -2 7 0.97 0.08 -28 2 7 0.92 0.09 -28 -2 7 0.9 0.08 -28 -2 6 0.3 0.07 -28 -2 6 0.35 0.06 -28 2 6 0.34 0.06 -28 -2 5 4.35 0.2 -28 -2 5 4.77 0.19 -28 -2 5 4.85 0.18 -28 2 5 4.8 0.18 -28 -2 4 0.56 0.08 -28 -2 4 0.39 0.07 -28 -2 3 9.6 0.31 -28 -2 3 10.56 0.3 -28 -2 2 0.06 0.04 -28 -2 2 0.04 0.04 -28 -2 1 0.58 0.07 -28 -2 1 0.38 0.07 -28 -2 0 0.9 0.09 -28 -2 0 1.08 0.09 28 2 0 1.09 0.08 28 -2 0 1.16 0.08 -28 -2 -1 6.37 0.22 -28 -2 -1 6.94 0.22 28 2 1 6.72 0.2 28 -2 1 7.19 0.21 28 2 2 0.91 0.07 28 -2 2 0.95 0.07 -28 -2 -2 1.05 0.08 28 2 3 10.51 0.25 28 -2 3 10.43 0.25 -28 -2 -3 10.7 0.27 28 2 4 0.01 0.03 28 -2 4 0.03 0.03 -28 -2 -4 0.05 0.03 28 -2 5 0.25 0.04 -28 -2 -5 0.27 0.04 -28 -4 13 0.07 0.03 -28 -4 13 0.1 0.03 -28 -4 12 4.3 0.16 -28 -4 12 5.09 0.15 -28 -4 11 0.08 0.04 -28 -4 11 0.08 0.03 -28 -4 10 0.32 0.06 -28 -4 10 0.34 0.05 -28 -4 9 0.06 0.04 -28 -4 9 0.14 0.04 -28 -4 8 5.08 0.19 -28 -4 8 5.64 0.18 -28 -4 7 0.22 0.05 -28 -4 7 0.19 0.05 -28 -4 7 0.19 0.05 -28 -4 6 6.8 0.23 -28 -4 6 6.9 0.22 -28 -4 5 0.46 0.06 -28 -4 5 0.44 0.07 -28 -4 4 0.09 0.04 -28 -4 4 0.1 0.05 -28 -4 3 0.17 0.05 -28 -4 3 0.19 0.05 -28 -4 2 6.85 0.23 -28 -4 2 7.63 0.23 -28 -4 1 0.46 0.06 -28 -4 1 0.43 0.06 -28 -4 0 10.46 0.26 -28 -4 0 9.71 0.27 -28 -4 -1 0.07 0.03 -28 -4 -1 0.06 0.04 -28 -4 -2 0.6 0.06 -28 -4 -2 0.57 0.06 -28 -4 -3 0.45 0.05 -28 -4 -3 0.43 0.05 -28 -6 9 1.95 0.09 -28 -6 8 0.79 0.06 -28 -6 7 0.09 0.03 -28 -6 6 0.2 0.04 -28 -6 5 2.07 0.1 -28 -6 3 4.41 0.15 -28 -6 2 0.21 0.04 -28 -6 1 0.05 0.03 -29 -1 14 1.67 0.08 -29 1 14 1.65 0.08 -29 -1 13 0.6 0.05 -29 1 13 0.63 0.06 -29 -1 12 0.85 0.07 -29 1 12 0.82 0.07 -29 -1 11 3.34 0.14 -29 1 11 3.47 0.14 -29 -1 10 1 0.08 -29 1 10 1.06 0.08 -29 -1 9 1.98 0.11 -29 1 9 1.94 0.11 -29 -1 8 1.34 0.09 -29 1 8 1.34 0.09 -29 -1 7 0.03 0.04 -29 1 7 0.03 0.04 -29 -1 6 2.68 0.14 -29 -1 6 2.65 0.13 -29 1 6 2.79 0.14 -29 -1 5 2.01 0.13 -29 -1 5 2.11 0.12 -29 -1 5 2.24 0.12 -29 1 5 2.21 0.12 -29 -1 4 -0.02 0.04 -29 -1 4 0.02 0.04 -29 -1 3 3.33 0.17 -29 -1 3 3.63 0.16 -29 -1 2 4.05 0.18 -29 -1 2 4.48 0.18 29 1 -1 0.14 0.04 29 -1 -1 0.19 0.04 -29 -1 1 0.17 0.05 -29 -1 1 0.11 0.05 -29 -1 0 5.92 0.2 29 1 0 5.67 0.18 29 -1 0 5.9 0.19 29 1 1 4.15 0.15 29 -1 1 4.21 0.15 -29 -1 -1 4.18 0.16 -29 -1 -2 0.13 0.04 29 1 2 0.2 0.04 29 -1 2 0.23 0.04 29 1 3 3.23 0.12 29 -1 3 3.15 0.12 29 1 4 1.5 0.08 29 -1 4 1.58 0.08 -29 -3 13 0.14 0.04 -29 -3 12 1.55 0.08 -29 -3 12 1.21 0.08 -29 -3 11 1.45 0.08 -29 -3 11 1.12 0.08 -29 -3 10 0.09 0.04 -29 -3 9 1.08 0.08 -29 -3 9 1.01 0.08 -29 -3 8 3.12 0.13 -29 -3 8 3.24 0.14 -29 -3 7 0.67 0.07 -29 -3 7 0.47 0.07 -29 -3 6 3.79 0.17 -29 -3 6 4.68 0.17 -29 -3 5 2.16 0.12 -29 -3 5 2.03 0.12 -29 -3 4 0.03 0.04 -29 -3 4 0.04 0.04 -29 -3 3 1.26 0.1 -29 -3 3 1.45 0.1 -29 -3 2 4.19 0.18 -29 -3 2 4.95 0.18 -29 -3 1 0.17 0.04 -29 -3 1 0.12 0.04 -29 -3 0 4.89 0.17 -29 -3 0 4.47 0.17 -29 -3 -1 2.12 0.11 -29 -3 -1 2.42 0.11 -29 -3 -2 0.06 0.03 -29 -3 -3 4.57 0.14 -29 -5 10 0.04 0.03 -29 -5 9 2.41 0.11 -29 -5 8 0.84 0.07 -29 -5 7 0.73 0.06 -29 -5 5 2.83 0.12 -29 -5 4 0.36 0.05 -29 -5 3 2.92 0.12 -29 -5 2 1.49 0.09 -29 -5 1 0.09 0.03 -29 -5 0 1.38 0.08 -30 0 13 0.01 0.03 -30 0 12 2.03 0.1 -30 0 11 0 0.03 -30 0 10 1.24 0.08 -30 0 9 -0.01 0.03 -30 0 8 11.5 0.29 -30 0 7 0.01 0.04 -30 0 6 2.44 0.12 -30 0 6 2.37 0.12 -30 0 5 0.02 0.04 -30 0 4 0.6 0.08 -30 0 4 0.61 0.07 -30 0 3 -0.03 0.04 -30 0 3 0 0.03 -30 0 2 5.35 0.18 30 0 -1 0.05 0.03 30 0 0 1.55 0.09 30 0 1 0 0.03 30 0 2 0.21 0.04 30 0 3 -0.01 0.02 -30 -2 12 0.02 0.02 -30 2 12 0.02 0.03 -30 -2 11 3.88 0.13 -30 2 11 4.16 0.14 -30 -2 10 0.04 0.04 -30 -2 10 0 0.03 -30 2 10 0.05 0.03 -30 -2 9 1.42 0.08 -30 2 9 1.34 0.08 -30 -2 9 1.28 0.1 -30 -2 8 0.04 0.04 -30 -2 8 0.1 0.04 -30 2 8 0.08 0.04 -30 -2 8 0.03 0.03 -30 -2 7 0.46 0.07 -30 -2 7 0.55 0.06 -30 -2 7 0.5 0.06 -30 2 7 0.59 0.06 -30 -2 6 0.27 0.06 -30 -2 6 0.38 0.06 -30 -2 5 5.08 0.2 -30 -2 5 5.26 0.19 -30 -2 4 0.23 0.06 -30 -2 4 0.35 0.06 -30 -2 3 1.67 0.11 -30 -2 3 1.95 0.11 -30 -2 2 0.13 0.05 30 2 -2 0.09 0.03 30 -2 -2 0.09 0.03 -30 -2 2 0.14 0.04 -30 -2 1 0.01 0.03 30 2 -1 0.1 0.03 30 -2 -1 0.1 0.03 -30 -2 1 0.12 0.04 -30 -2 0 0.08 0.04 -30 -2 0 0.19 0.04 30 2 0 0.13 0.03 30 -2 0 0.17 0.04 30 -2 1 5.62 0.16 -30 -2 -1 6.09 0.17 30 -2 2 0.07 0.02 -30 -2 -2 0.08 0.03 -30 -4 7 0.24 0.05 -30 -4 6 3.42 0.14 -30 -4 6 3.92 0.14 -30 -4 5 0.43 0.05 -30 -4 5 0.42 0.06 -30 -4 4 0.25 0.04 -30 -4 4 0.16 0.04 -30 -4 3 0.11 0.03 -30 -4 3 0.08 0.04 -30 -4 2 6.04 0.19 -30 -4 2 6.88 0.18 -30 -4 1 0.02 0.03 -30 -4 1 0 0.03 -31 -1 12 0.28 0.04 -31 1 12 0.23 0.04 -31 -1 11 3.57 0.12 -31 1 11 3.74 0.12 -31 -1 10 0.57 0.05 -31 1 10 0.61 0.06 -31 -1 10 0.48 0.06 -31 -1 9 0.27 0.05 -31 -1 9 0.34 0.04 -31 1 9 0.37 0.05 -31 -1 8 1.8 0.1 -31 1 8 1.56 0.09 -31 -1 8 1.53 0.1 -31 -1 8 1.74 0.09 -31 1 8 1.77 0.09 -31 -1 7 0.52 0.07 -31 -1 7 0.69 0.06 -31 -1 6 3.3 0.15 -31 -1 6 3.42 0.14 -31 1 5 2.66 0.13 -31 -1 5 2.48 0.13 -31 -1 5 2.9 0.13 -31 -1 4 0.15 0.05 -31 -1 4 0.18 0.04 -31 -1 3 0.76 0.07 -31 -1 3 0.94 0.07 -31 -1 2 3.57 0.14 -31 -1 2 3.91 0.14 31 1 -2 3.8 0.13 31 -1 -2 4.03 0.14 -31 -1 1 0.13 0.04 31 1 -1 0.09 0.03 31 -1 -1 0.14 0.03 31 1 0 0.72 0.06 31 -1 0 0.68 0.05 -31 -1 0 0.63 0.05 31 1 1 3.25 0.11 31 -1 1 3.2 0.11 -31 -3 9 1.07 0.07 -31 -3 8 3.2 0.13 -31 -3 8 3.54 0.13 -31 -3 7 0.45 0.05 -31 -3 7 0.32 0.05 -31 -3 6 0.8 0.07 -31 -3 6 0.95 0.07 -31 -3 5 0.87 0.07 -31 -3 5 0.93 0.07 -31 -3 4 0.22 0.04 -31 -3 4 0.18 0.04 -31 -3 3 0.67 0.06 -31 -3 3 0.8 0.06 -31 -3 2 3.61 0.13 -31 -3 2 3.18 0.13 -31 -3 1 0.1 0.03 -31 -3 1 0.1 0.03 -32 0 10 0.85 0.06 -32 0 10 0.71 0.06 -32 0 9 -0.02 0.03 -32 0 9 0.03 0.03 -32 0 8 9.09 0.24 -32 0 8 9.93 0.23 -32 0 7 0.03 0.03 -32 0 7 0 0.03 -32 0 6 1.7 0.1 -32 0 6 1.91 0.09 -32 0 5 0 0.03 -32 0 5 0.02 0.03 -32 0 4 2.39 0.11 32 0 -3 0.01 0.02 32 0 -2 5.1 0.15 32 0 -1 0.01 0.02 -32 -2 8 0.16 0.03 -32 -2 8 0.17 0.04 -32 -2 7 1.63 0.09 -32 -2 7 1.95 0.09 -32 -2 6 0.03 0.03 -32 -2 6 0 0.03 -32 -2 5 3.92 0.14 32 2 -5 3.75 0.12 -32 -2 4 0.07 0.03 32 2 -4 0.13 0.03 32 -2 -4 0.09 0.03 -32 -2 4 0.08 0.03 -32 -2 3 1.61 0.09 -32 -2 3 1.89 0.09 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Cd1 O1 99.3(13) . . y O2 Cd1 O1 54.5(2) . . y O2 Cd1 N1 90.9(14) . . y N2 Cd1 O1 86.3(7) 8_465 . y N2 Cd1 N1 174.3(15) 8_465 . y N2 Cd1 O2 92.7(8) 8_465 . y O3 Cd1 O1 142.26(19) 1_565 . y O3 Cd1 N1 87.3(8) 1_565 . y O3 Cd1 O2 88.6(2) 1_565 . y O3 Cd1 N2 88.5(6) 1_565 8_465 y O4 Cd1 O1 84.4(2) 3_565 . y O4 Cd1 N1 89.8(10) 3_565 . y O4 Cd1 O2 138.4(2) 3_565 . y O4 Cd1 N2 90.3(6) 3_565 8_465 y O4 Cd1 O3 132.99(19) 3_565 1_565 y N1A Cd1 O1 99.5(13) . . y N1A Cd1 N1 1(3) . . y N1A Cd1 O2 91.6(15) . . y N1A Cd1 N2 174.0(16) . 8_465 y N1A Cd1 O3 87.5(9) . 1_565 y N1A Cd1 O4 89.2(10) . 3_565 y N2A Cd1 O1 86.9(8) 8_465 . y N2A Cd1 N1 172.7(17) 8_465 . y N2A Cd1 O2 95.7(8) 8_465 . y N2A Cd1 N2 3.4(13) 8_465 8_465 y N2A Cd1 O3 90.1(6) 8_465 1_565 y N2A Cd1 O4 87.0(7) 8_465 3_565 y N2A Cd1 N1A 172.2(17) 8_465 . y C16 O1 Cd1 92.9(4) . . ? C1 N1 Cd1 126(2) . . ? C5 N1 Cd1 117(2) . . ? C5 N1 C1 118(3) . . ? H1 C1 N1 119.5(16) . . ? C2 C1 N1 121(2) . . ? C2 C1 H1 119.5(16) . . ? H1Wb O1W H1Wa 104.5 . . ? C16 O2 Cd1 93.0(5) . . ? C11 N2 Cd1 125.0(17) . 8_566 ? C15 N2 Cd1 114.7(16) . 8_566 ? C15 N2 C11 119(2) . . ? H2 C2 C1 120.4(16) . . ? C3 C2 C1 119(2) . . ? C3 C2 H2 120.4(13) . . ? H2Wb O2W H2Wa 104.5 . . ? C22 O3 Cd1 108.2(5) . 1_545 ? C6 N3 H3 119.2(11) . . ? C7 N3 H3 119.2(12) . . ? C7 N3 C6 121.7(18) . . ? H3a C3 C2 120.0(13) . . ? C4 C3 C2 120(2) . . ? C4 C3 H3a 120.0(12) . . ? C22 O4 Cd1 173.9(5) . 3_565 ? C9 N4 H4 121.8(12) . . ? C10 N4 H4 121.8(12) . . ? C10 N4 C9 116.4(19) . . ? C5 C4 C3 115(2) . . ? C6 C4 C3 123.2(18) . . ? C6 C4 C5 122(2) . . ? C20 O5 H5 109.5 . . ? C4 C5 N1 126(3) . . ? H5a C5 N1 116.8(18) . . ? H5a C5 C4 116.8(16) . . ? C4 C6 N3 118.8(17) . . ? O6 C6 N3 122.3(18) . . ? O6 C6 C4 118.8(17) . . ? H7a C7 N3 109.1(11) . . ? H7b C7 N3 109.1(13) . . ? H7b C7 H7a 107.82413477(2) . . ? C8 C7 N3 112.6(18) . . ? C8 C7 H7a 109.1(12) . . ? C8 C7 H7b 109.1(12) . . ? H8a C8 C7 108.5(12) . . ? H8b C8 C7 108.5(12) . . ? H8b C8 H8a 107.53581142(4) . . ? C9 C8 C7 114.9(19) . . ? C9 C8 H8a 108.5(17) . . ? C9 C8 H8b 108.5(16) . . ? C8 C9 N4 98.9(19) . . ? H9a C9 N4 112.0(18) . . ? H9a C9 C8 112.0(17) . . ? H9b C9 N4 112.0(17) . . ? H9b C9 C8 112.0(16) . . ? H9b C9 H9a 109.667690974(15) . . ? O7 C10 N4 121.4(17) . . ? C14 C10 N4 116.7(16) . . ? C14 C10 O7 121.8(16) . . ? H11 C11 N2 118.5(14) . . ? C12 C11 N2 123(2) . . ? C12 C11 H11 118.5(14) . . ? H12 C12 C11 121.1(14) . . ? C13 C12 C11 118(2) . . ? C13 C12 H12 121.1(14) . . ? H13 C13 C12 119.3(14) . . ? C14 C13 C12 121(2) . . ? C14 C13 H13 119.3(11) . . ? C13 C14 C10 118.9(16) . . ? C15 C14 C10 122.6(16) . . ? C15 C14 C13 116.6(17) . . ? C14 C15 N2 116(2) . . ? H15 C15 N2 121.8(15) . . ? H15 C15 C14 121.8(12) . . ? O2 C16 O1 119.5(7) . . ? C17 C16 O1 118.6(6) . . ? C17 C16 O2 121.8(7) . . ? C18 C17 C16 123.7(7) . . ? C23 C17 C16 117.6(7) . . ? C23 C17 C18 118.6(7) . . ? H18 C18 C17 119.5(4) . . ? C21 C18 C17 121.0(6) . . ? C21 C18 H18 119.5(4) . . ? C20 C19 H19 120.1(5) . . ? C21 C19 H19 120.1(4) . . ? C21 C19 C20 119.8(7) . . ? C19 C20 O5 116.6(7) . . ? C23 C20 O5 122.0(7) . . ? C23 C20 C19 121.4(7) . . ? C19 C21 C18 119.9(7) . . ? C22 C21 C18 122.5(6) . . ? C22 C21 C19 117.6(6) . . ? O4 C22 O3 124.1(7) . . ? C21 C22 O3 117.7(6) . . ? C21 C22 O4 118.1(7) . . ? C20 C23 C17 119.2(7) . . ? H23 C23 C17 120.4(4) . . ? H23 C23 C20 120.4(4) . . ? O7A C10A N4A 123.9(16) . . ? C14A C10A N4A 117.2(15) . . ? C14A C10A O7A 118.8(13) . . ? C1A N1A Cd1 121(2) . . ? C5A N1A Cd1 124(2) . . ? C5A N1A C1A 115(3) . . ? H1A C1A N1A 117.3(15) . . ? C2A C1A N1A 125(2) . . ? C2A C1A H1A 117.3(14) . . ? H5Aa C5A N1A 116.9(19) . . ? C4A C5A N1A 126(3) . . ? C4A C5A H5Aa 116.9(15) . . ? H2A C2A C1A 121.5(14) . . ? C3A C2A C1A 117(2) . . ? C3A C2A H2A 121.5(13) . . ? C3A C4A C5A 117(2) . . ? C6A C4A C5A 119(2) . . ? C6A C4A C3A 123.8(19) . . ? C4A C3A C2A 119.2(19) . . ? H3Aa C3A C2A 120.4(13) . . ? H3Aa C3A C4A 120.4(12) . . ? N3A C6A C4A 115.7(17) . . ? O6A C6A C4A 118.2(16) . . ? O6A C6A N3A 126.0(17) . . ? H3Ab N3A C6A 118.1(11) . . ? C7A N3A C6A 123.8(18) . . ? C7A N3A H3Ab 118.1(11) . . ? H7Aa C7A N3A 109.5(12) . . ? H7Ab C7A N3A 109.5(11) . . ? H7Ab C7A H7Aa 108.0 . . ? C8A C7A N3A 110.9(17) . . ? C8A C7A H7Aa 109.5(12) . . ? C8A C7A H7Ab 109.5(13) . . ? H8Aa C8A C7A 108.8(13) . . ? H8Ab C8A C7A 108.8(12) . . ? H8Ab C8A H8Aa 107.6 . . ? C9A C8A C7A 114.0(19) . . ? C9A C8A H8Aa 108.8(18) . . ? C9A C8A H8Ab 108.8(15) . . ? H9Aa C9A C8A 109.1(18) . . ? H9Ab C9A C8A 109.1(14) . . ? H9Ab C9A H9Aa 107.85007377(4) . . ? N4A C9A C8A 112(2) . . ? N4A C9A H9Aa 109.1(17) . . ? N4A C9A H9Ab 109.1(14) . . ? C9A N4A C10A 123(2) . . ? H4A N4A C10A 118.3(11) . . ? H4A N4A C9A 118.3(17) . . ? C13A C14A C10A 122.9(16) . . ? C15A C14A C10A 122.1(15) . . ? C15A C14A C13A 114.3(18) . . ? H13A C13A C14A 120.7(11) . . ? C12A C13A C14A 118.6(19) . . ? C12A C13A H13A 120.7(14) . . ? H15A C15A C14A 119.8(11) . . ? N2A C15A C14A 120(2) . . ? N2A C15A H15A 119.8(14) . . ? H12A C12A C13A 119.7(14) . . ? C11A C12A C13A 121(2) . . ? C11A C12A H12A 119.7(14) . . ? C15A N2A Cd1 126.5(17) . 8_566 ? C11A N2A Cd1 117.2(17) . 8_566 ? C11A N2A C15A 116(2) . . ? N2A C11A C12A 122(2) . . ? H11A C11A C12A 118.9(14) . . ? H11A C11A N2A 118.9(14) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cd1 O1 2.356(5) . y Cd1 N1 2.38(3) . y Cd1 O2 2.378(6) . y Cd1 N2 2.40(2) 8_465 y Cd1 O3 2.264(5) 1_565 y Cd1 O4 2.312(5) 3_565 y Cd1 N1A 2.28(3) . y Cd1 N2A 2.26(2) 8_465 y O1 C16 1.276(9) . ? N1 C1 1.37(3) . ? N1 C5 1.33(3) . ? C1 H1 0.9300 . ? C1 C2 1.36(2) . ? O1W H1Wa 0.8503 . ? O1W H1Wb 0.8501 . ? O2 C16 1.232(9) . ? N2 C11 1.33(2) . ? N2 C15 1.35(2) . ? C2 H2 0.9300 . ? C2 C3 1.40(2) . ? O2W H2Wa 0.8500 . ? O2W H2Wb 0.8497 . ? O3 C22 1.240(9) . ? N3 H3 0.8600 . ? N3 C6 1.33(2) . ? N3 C7 1.47(2) . ? C3 H3a 0.9300 . ? C3 C4 1.40(2) . ? O4 C22 1.247(8) . ? N4 H4 0.8600 . ? N4 C9 1.52(2) . ? N4 C10 1.30(2) . ? C4 C5 1.36(2) . ? C4 C6 1.49(2) . ? O5 H5 0.8200 . ? O5 C20 1.388(9) . ? C5 H5a 0.9300 . ? O6 C6 1.22(2) . ? C7 H7a 0.9700 . ? C7 H7b 0.9700 . ? C7 C8 1.51(2) . ? O7 C10 1.198(18) . ? C8 H8a 0.9700 . ? C8 H8b 0.9700 . ? C8 C9 1.56(3) . ? C9 H9a 0.9700 . ? C9 H9b 0.9700 . ? C10 C14 1.489(19) . ? C11 H11 0.9300 . ? C11 C12 1.36(2) . ? C12 H12 0.9300 . ? C12 C13 1.37(2) . ? C13 H13 0.9300 . ? C13 C14 1.35(2) . ? C14 C15 1.46(2) . ? C15 H15 0.9300 . ? C16 C17 1.469(11) . ? C17 C18 1.391(10) . ? C17 C23 1.410(10) . ? C18 H18 0.9300 . ? C18 C21 1.370(10) . ? C19 H19 0.9300 . ? C19 C20 1.376(11) . ? C19 C21 1.378(10) . ? C20 C23 1.369(11) . ? C21 C22 1.513(10) . ? C23 H23 0.9300 . ? C10A N4A 1.31(2) . ? C10A O7A 1.223(17) . ? C10A C14A 1.501(18) . ? N1A C1A 1.36(2) . ? N1A C5A 1.33(3) . ? C1A H1A 0.9300 . ? C1A C2A 1.36(2) . ? C5A H5Aa 0.9300 . ? C5A C4A 1.36(2) . ? C2A H2A 0.9300 . ? C2A C3A 1.41(2) . ? C4A C3A 1.39(2) . ? C4A C6A 1.48(2) . ? C3A H3Aa 0.9300 . ? C6A N3A 1.33(2) . ? C6A O6A 1.25(2) . ? N3A H3Ab 0.8600 . ? N3A C7A 1.48(2) . ? C7A H7Aa 0.9700 . ? C7A H7Ab 0.9700 . ? C7A C8A 1.53(2) . ? C8A H8Aa 0.9700 . ? C8A H8Ab 0.9700 . ? C8A C9A 1.56(3) . ? C9A H9Aa 0.9700 . ? C9A H9Ab 0.9700 . ? C9A N4A 1.51(2) . ? N4A H4A 0.8600 . ? C14A C13A 1.36(2) . ? C14A C15A 1.46(2) . ? C13A H13A 0.9300 . ? C13A C12A 1.40(2) . ? C15A H15A 0.9300 . ? C15A N2A 1.36(2) . ? C12A H12A 0.9300 . ? C12A C11A 1.38(2) . ? N2A C11A 1.33(2) . ? C11A H11A 0.9300 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cd1 O1 C16 O2 -4.0(7) . . . . ? Cd1 O1 C16 C17 177.3(4) . . . . ? Cd1 N1 C1 C2 -178(3) . . . . ? Cd1 N1 C5 C4 171(3) . . . . ? Cd1 O2 C16 O1 4.0(7) . . . . ? Cd1 O2 C16 C17 -177.4(4) . . . . ? Cd1 N2 C11 C12 177(3) 8_566 . . . ? Cd1 N2 C15 C14 166.7(17) 8_566 . . . ? Cd1 O3 C22 O4 9.0(5) 1_545 . . . ? Cd1 O3 C22 C21 -169.6(4) 1_545 . . . ? Cd1 N1A C1A C2A -174(3) . . . . ? Cd1 N1A C5A C4A 177(4) . . . . ? Cd1 N2A C15A C14A -145(2) 8_566 . . . ? Cd1 N2A C11A C12A 166(2) 8_566 . . . ? O1 C16 C17 C18 -0.4(9) . . . . ? O1 C16 C17 C23 -179.8(8) . . . . ? N1 C1 C2 C3 8(6) . . . . ? N1 C5 C4 C3 6(8) . . . . ? N1 C5 C4 C6 -172(5) . . . . ? C1 C2 C3 C4 -7(4) . . . . ? O2 C16 C17 C18 -179.1(9) . . . . ? O2 C16 C17 C23 1.6(11) . . . . ? N2 C11 C12 C13 3(3) . . . . ? N2 C15 C14 C10 -168(2) . . . . ? N2 C15 C14 C13 28(3) . . . . ? C2 C3 C4 C5 0(4) . . . . ? C2 C3 C4 C6 179(3) . . . . ? O3 C22 C21 C18 -173.7(7) . . . . ? O3 C22 C21 C19 4.7(8) . . . . ? N3 C6 C4 C3 -9(3) . . . . ? N3 C6 C4 C5 170(4) . . . . ? N3 C7 C8 C9 -55(2) . . . . ? C3 C4 C6 O6 170(3) . . . . ? O4 C22 C21 C18 7.7(8) . . . . ? O4 C22 C21 C19 -173.9(7) . . . . ? N4 C9 C8 C7 -179.3(19) . . . . ? N4 C10 C14 C13 148(2) . . . . ? N4 C10 C14 C15 -16(3) . . . . ? O5 C20 C19 C21 -178.0(8) . . . . ? O5 C20 C23 C17 176.1(10) . . . . ? O7 C10 C14 C13 -36(3) . . . . ? O7 C10 C14 C15 161(2) . . . . ? C10 C14 C13 C12 -177(3) . . . . ? C11 C12 C13 C14 -2(5) . . . . ? C12 C13 C14 C15 -13(4) . . . . ? C16 C17 C18 C21 178.9(7) . . . . ? C16 C17 C23 C20 -177.8(9) . . . . ? C17 C18 C21 C19 0.1(9) . . . . ? C17 C18 C21 C22 178.4(7) . . . . ? C17 C23 C20 C19 -2.2(11) . . . . ? C18 C21 C19 C20 0.6(9) . . . . ? C10A N4A C9A C8A 118(2) . . . . ? C10A C14A C13A C12A -173(2) . . . . ? C10A C14A C15A N2A 156(2) . . . . ? N1A C1A C2A C3A -1(4) . . . . ? N1A C5A C4A C3A -6(9) . . . . ? N1A C5A C4A C6A 171(6) . . . . ? C1A C2A C3A C4A 3(4) . . . . ? C5A C4A C3A C2A -1(5) . . . . ? C5A C4A C6A N3A 137(4) . . . . ? C5A C4A C6A O6A -41(4) . . . . ? C2A C3A C4A C6A -177(3) . . . . ? C4A C6A N3A C7A -178.4(19) . . . . ? C6A N3A C7A C8A 128(2) . . . . ? N3A C7A C8A C9A -75(2) . . . . ? C7A C8A C9A N4A 166(2) . . . . ? C14A C13A C12A C11A 1(3) . . . . ? C14A C15A N2A C11A 29(3) . . . . ? C13A C12A C11A N2A -6(4) . . . . ? C15A N2A C11A C12A -10(4) . . . . ? loop_ _restr_equal_distance_atom_site_label_1 _restr_equal_distance_atom_site_label_2 _restr_equal_distance_site_symmetry_2 _restr_equal_distance_class_id N1 C1 1 1 N1 C2 1 25 N1 C4 1 26 N1 C5 1 4 C1 C2 1 5 C1 C3 1 27 C1 C5 1 28 N2 C11 1 2 N2 C12 1 6 N2 C14 1 7 N2 C15 1 3 C2 C3 1 8 C2 C4 1 29 N3 C4 1 30 N3 O6 1 31 N3 C6 1 9 N3 C7 1 10 N3 C8 1 32 C3 C4 1 11 C3 C5 1 33 C3 C6 1 34 N4 O7 1 35 N4 C8 1 36 N4 C9 1 12 N4 C10 1 13 N4 C14 1 37 C4 C5 1 14 C4 O6 1 38 C4 C6 1 15 C5 C6 1 39 O6 C6 1 16 C6 C7 1 40 C7 C8 1 17 C7 C9 1 41 O7 C10 1 18 O7 C14 1 42 C8 C9 1 19 C9 C10 1 43 C10 C13 1 44 C10 C14 1 20 C10 C15 1 45 C11 C12 1 21 C11 C13 1 46 C11 C15 1 47 C12 C13 1 22 C12 C14 1 48 C13 C14 1 23 C13 C15 1 49 C14 C15 1 24 C10A C14A 1 20 C10A C13A 1 44 C10A C15A 1 45 N1A C1A 1 1 N1A C5A 1 4 N1A C2A 1 25 N1A C4A 1 26 C1A C5A 1 28 C1A C2A 1 5 C1A C3A 1 27 C5A C6A 1 39 C2A C4A 1 29 C2A C3A 1 8 C4A C5A 1 14 C4A C6A 1 15 C4A O6A 1 38 C3A C5A 1 33 C3A C4A 1 11 C3A C6A 1 34 C6A C7A 1 40 N3A C4A 1 30 N3A C6A 1 9 N3A O6A 1 31 N3A C7A 1 10 N3A C8A 1 32 O6A C6A 1 16 C7A C8A 1 17 C7A C9A 1 41 C8A C9A 1 19 C9A C10A 1 43 N4A C10A 1 13 N4A C8A 1 36 N4A C9A 1 12 N4A O7A 1 35 N4A C14A 1 37 O7A C10A 1 18 O7A C14A 1 42 C14A C15A 1 24 C13A C14A 1 23 C13A C15A 1 49 C12A C14A 1 48 C12A C13A 1 22 N2A C14A 1 7 N2A C15A 1 3 N2A C12A 1 6 N2A C11A 1 2 C11A C13A 1 46 C11A C15A 1 47 C11A C12A 1 21 loop_ _restr_equal_distance_class_class_id _restr_equal_distance_class_target_weight_param _restr_equal_distance_class_average _restr_equal_distance_class_esd _restr_equal_distance_class_diff_max 1 0.0200 1.3605 0.0049 0.0049 2 0.0200 1.3302 0.0046 0.0046 3 0.0200 1.3520 0.0034 0.0034 4 0.0200 1.3266 0.0002 0.0002 5 0.0200 1.3589 0.0017 0.0017 6 0.0400 2.3672 0.0015 0.0015 7 0.0400 2.4164 0.0292 0.0292 8 0.0200 1.4068 0.0028 0.0028 9 0.0200 1.3311 0.0034 0.0034 10 0.0200 1.4762 0.0036 0.0036 11 0.0200 1.3955 0.0036 0.0036 12 0.0200 1.5107 0.0044 0.0044 13 0.0200 1.3066 0.0045 0.0045 14 0.0200 1.3616 0.0004 0.0004 15 0.0200 1.4827 0.0053 0.0053 16 0.0200 1.2336 0.0127 0.0127 17 0.0200 1.5178 0.0125 0.0125 18 0.0200 1.2107 0.0128 0.0128 19 0.0200 1.5580 0.0007 0.0007 20 0.0200 1.4951 0.0059 0.0059 21 0.0200 1.3687 0.0089 0.0089 22 0.0200 1.3814 0.0152 0.0152 23 0.0200 1.3578 0.0059 0.0059 24 0.0200 1.4610 0.0020 0.0020 25 0.0400 2.3920 0.0194 0.0194 26 0.0400 2.3987 0.0014 0.0014 27 0.0400 2.3719 0.0136 0.0136 28 0.0400 2.2797 0.0223 0.0223 29 0.0400 2.4215 0.0051 0.0051 30 0.0400 2.4037 0.0212 0.0212 31 0.0400 2.2667 0.0334 0.0334 32 0.0400 2.4789 0.0008 0.0008 33 0.0400 2.3400 0.0086 0.0086 34 0.0400 2.5358 0.0044 0.0044 35 0.0400 2.2090 0.0285 0.0285 36 0.0400 2.4408 0.1055 0.1055 37 0.0400 2.3902 0.0119 0.0119 38 0.0400 2.3384 0.0022 0.0022 39 0.0400 2.4674 0.0205 0.0205 40 0.0400 2.4648 0.0185 0.0185 41 0.0400 2.5862 0.0035 0.0035 42 0.0400 2.3511 0.0012 0.0012 43 0.0400 2.4391 0.0426 0.0426 44 0.0400 2.4823 0.0348 0.0348 45 0.0400 2.5898 0.0039 0.0039 46 0.0400 2.3716 0.0384 0.0384 47 0.0400 2.2916 0.0160 0.0160 48 0.0400 2.3724 0.0012 0.0012 49 0.0400 2.3833 0.0083 0.0083 loop_ _restr_U_iso_atom_site_label _restr_U_iso_weight_param N1 0.0050 N1 0.0500 N2 0.0050 N1A 0.0500 N1A 0.0050 N2A 0.0050 loop_ _restr_rigu_atom_site_label_1 _restr_rigu_atom_site_label_2 _restr_rigu_target_weight_param _restr_rigu_u13_diff _restr_rigu_u23_diff _restr_rigu_u33_diff N1 C1 0.004000 0.000802 0.002094 -0.002930 N1 C2 0.004000 0.002050 -0.001882 -0.003789 N1 C4 0.004000 0.000210 -0.001582 -0.002230 N1 C5 0.004000 -0.001361 0.001880 -0.000291 C1 C2 0.004000 0.000429 -0.000667 0.001424 C1 C3 0.004000 0.001720 -0.001554 0.000916 C1 C5 0.004000 0.002930 0.000427 -0.001407 N2 C11 0.004000 0.002318 -0.002046 -0.001610 N2 C12 0.004000 -0.001171 0.004108 -0.002948 N2 C14 0.004000 0.003236 0.001203 -0.002563 N2 C15 0.004000 0.000200 0.000312 -0.001121 C2 C3 0.004000 0.001259 -0.000154 0.000943 C2 C4 0.004000 0.007778 -0.003277 -0.000949 N3 C4 0.004000 -0.001912 -0.002236 0.001423 N3 O6 0.004000 0.001954 0.006678 -0.001043 N3 C6 0.004000 -0.000220 0.000899 0.000428 N3 C7 0.004000 -0.000247 0.001663 -0.000685 N3 C8 0.004000 0.002917 0.002863 0.001426 C3 C4 0.004000 0.000426 -0.000494 0.000091 C3 C5 0.004000 -0.004145 0.000315 0.000370 C3 C6 0.004000 0.009812 -0.006790 0.000113 N4 O7 0.004000 -0.005159 0.001916 -0.001852 N4 C8 0.004000 -0.007919 -0.012121 -0.008753 N4 C9 0.004000 0.002026 -0.000784 -0.002436 N4 C10 0.004000 -0.000548 0.000950 -0.000089 N4 C14 0.004000 0.000961 -0.005645 0.002378 C4 C5 0.004000 0.001240 0.000120 -0.000674 C4 O6 0.004000 0.003322 -0.002592 0.000944 C4 C6 0.004000 0.000918 -0.000861 0.000630 C5 C6 0.004000 -0.001677 0.003004 -0.000714 O6 C6 0.004000 0.002981 -0.001570 -0.000718 C6 C7 0.004000 0.003554 0.000311 -0.000535 C7 C8 0.004000 0.000534 -0.000549 0.002470 C7 C9 0.004000 0.003690 0.009369 0.004229 O7 C10 0.004000 -0.001880 -0.000228 -0.002083 O7 C14 0.004000 0.003739 -0.001059 0.000351 C8 C9 0.004000 0.002772 0.000412 -0.001005 C9 C10 0.004000 -0.000832 -0.001848 0.001579 C10 C13 0.004000 -0.007786 -0.003964 0.000480 C10 C14 0.004000 0.000445 -0.001281 0.000871 C10 C15 0.004000 0.006505 -0.001148 0.000663 C11 C12 0.004000 0.002063 -0.001323 0.004331 C11 C13 0.004000 0.008396 0.002149 0.000664 C11 C15 0.004000 -0.004464 0.008217 -0.001153 C12 C13 0.004000 -0.001536 0.000842 -0.000088 C12 C14 0.004000 -0.008053 0.004126 -0.000887 C13 C14 0.004000 0.002033 0.002359 0.001063 C13 C15 0.004000 -0.003800 -0.004681 0.004729 C14 C15 0.004000 0.000159 0.001644 -0.002319 C10A C9A 0.004000 -0.006346 0.004528 -0.003836 C10A N4A 0.004000 -0.001181 -0.000114 0.000573 C10A O7A 0.004000 -0.000580 -0.000012 -0.000485 C10A C14A 0.004000 -0.002087 0.000732 -0.000257 C10A C13A 0.004000 -0.009980 0.006060 -0.000066 C10A C15A 0.004000 0.000625 -0.006215 0.001523 N1A C1A 0.004000 0.004582 0.002953 -0.002790 N1A C5A 0.004000 -0.000137 0.002297 -0.000054 N1A C2A 0.004000 -0.001186 -0.002406 -0.003257 N1A C4A 0.004000 0.004077 -0.004301 0.001886 C1A C5A 0.004000 0.001012 -0.000530 -0.000934 C1A C2A 0.004000 0.000515 -0.000539 -0.000147 C1A C3A 0.004000 0.009087 -0.005718 0.002425 C5A C4A 0.004000 -0.000582 -0.000245 0.001712 C5A C3A 0.004000 -0.001985 -0.002747 0.002823 C5A C6A 0.004000 0.001312 -0.000991 0.000006 C2A C4A 0.004000 0.000130 0.001522 -0.000524 C2A C3A 0.004000 0.001912 0.001155 0.001091 C4A C3A 0.004000 0.001194 -0.001110 0.000930 C4A C6A 0.004000 0.000881 0.001251 -0.001009 C4A N3A 0.004000 -0.000267 0.000422 0.000848 C4A O6A 0.004000 0.001248 0.002413 -0.003591 C3A C6A 0.004000 0.000784 0.003886 -0.002970 C6A N3A 0.004000 -0.001834 -0.000010 0.001348 C6A O6A 0.004000 -0.000361 0.000557 -0.000274 C6A C7A 0.004000 0.002009 0.003015 0.004099 N3A O6A 0.004000 -0.002819 0.000380 0.000491 N3A C7A 0.004000 0.001579 0.000313 0.000507 N3A C8A 0.004000 0.002231 0.008905 0.001065 C7A C8A 0.004000 -0.001562 0.003755 0.002653 C7A C9A 0.004000 0.003803 0.004624 -0.000111 C8A C9A 0.004000 0.002369 0.002073 0.000211 C8A N4A 0.004000 -0.004915 0.009673 0.003219 C9A N4A 0.004000 0.001800 0.000509 0.001517 N4A O7A 0.004000 -0.006690 0.003776 -0.001763 N4A C14A 0.004000 -0.003870 0.000309 0.004397 O7A C14A 0.004000 -0.001062 0.001079 0.003570 C14A C13A 0.004000 -0.000792 0.000430 0.000380 C14A C15A 0.004000 -0.000110 -0.000608 -0.001925 C14A C12A 0.004000 -0.007872 0.000363 0.001160 C14A N2A 0.004000 0.005258 -0.003679 -0.000249 C13A C15A 0.004000 -0.001331 0.003826 0.005833 C13A C12A 0.004000 -0.001827 -0.001372 0.000320 C13A C11A 0.004000 0.006186 -0.004310 0.001485 C15A N2A 0.004000 0.000260 -0.000510 -0.000005 C15A C11A 0.004000 -0.002536 -0.001659 0.000687 C12A N2A 0.004000 -0.002161 -0.001086 0.003025 C12A C11A 0.004000 0.000415 0.000385 -0.001342 N2A C11A 0.004000 0.001156 0.000116 0.000376