#------------------------------------------------------------------------------ #$Date: 2023-12-04 20:10:40 +0200 (Mon, 04 Dec 2023) $ #$Revision: 288015 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/78/7247817.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7247817 loop_ _publ_author_name 'Li, Wen-Ze' 'Sheng, Yu-Shu' 'Zhang, Xiao-Sa' 'Liu, Yu' 'Li, Jing' 'Luan, Jian' _publ_section_title ; Fabrication of 5-R-isophthalic acid-modulated cadmium--organic coordination polymers and selectivity for the efficient detection of multiple analytes ; _journal_issue 43 _journal_name_full CrystEngComm _journal_page_first 6067 _journal_page_last 6079 _journal_paper_doi 10.1039/D3CE00899A _journal_volume 25 _journal_year 2023 _chemical_formula_moiety 'C33 H34 Cd2 N4 O13, 2(H2 O)' _chemical_formula_sum 'C33 H38 Cd2 N4 O15' _chemical_formula_weight 955.511 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_Int_Tables_number 2 _audit_creation_date 2023-09-29 _audit_creation_method ; Olex2 1.5-dev (compiled 2023.09.29 svn.re1ec1418 for OlexSys, GUI svn.r6697) ; _audit_update_record ; 2023-09-30 deposited with the CCDC. 2023-10-05 downloaded from the CCDC. ; _cell_angle_alpha 97.263(2) _cell_angle_beta 94.133(1) _cell_angle_gamma 119.439(2) _cell_formula_units_Z 2 _cell_length_a 10.0583(2) _cell_length_b 10.1823(2) _cell_length_c 20.6673(3) _cell_measurement_reflns_used 16944 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 68.24 _cell_measurement_theta_min 2.18 _cell_volume 1806.38(7) _computing_cell_refinement 'SAINT V8.38A (Bruker AXS Inc., 2017)' _computing_data_collection 'Bruker Instrument Service vV6.2.9' _computing_data_reduction 'SAINT V8.38A (Bruker AXS Inc., 2017)' _computing_molecular_graphics 'Olex2 1.5-dev (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5-dev (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine 1.5-dev (Bourhis et al., 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 0.9685 _diffrn_measured_fraction_theta_max 0.9616 _diffrn_measurement_device_type 'multiwire proportional' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0379 _diffrn_reflns_av_unetI/netI 0.0360 _diffrn_reflns_Laue_measured_fraction_full 0.9685 _diffrn_reflns_Laue_measured_fraction_max 0.9616 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_number 16944 _diffrn_reflns_point_group_measured_fraction_full 0.9685 _diffrn_reflns_point_group_measured_fraction_max 0.9616 _diffrn_reflns_theta_full 67.6786 _diffrn_reflns_theta_max 68.24 _diffrn_reflns_theta_min 2.18 _exptl_absorpt_coefficient_mu 10.101 _exptl_absorpt_correction_T_max 0.220 _exptl_absorpt_correction_T_min 0.203 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS _exptl_crystal_colour COLOURLESS _exptl_crystal_density_diffrn 1.757 _exptl_crystal_density_method 'not measured' _exptl_crystal_description BLOCK _exptl_crystal_F_000 964.658 _exptl_crystal_size_max 0.18 _exptl_crystal_size_mid 0.16 _exptl_crystal_size_min 0.15 _refine_diff_density_max 0.8308 _refine_diff_density_min -0.8557 _refine_diff_density_rms 0.0989 _refine_ls_d_res_high 0.8300 _refine_ls_d_res_low 20.2526 _refine_ls_extinction_coef 0.00061(8) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_goodness_of_fit_ref 1.0450 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_constraints 64 _refine_ls_number_parameters 491 _refine_ls_number_reflns 6366 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.0450 _refine_ls_R_factor_all 0.0349 _refine_ls_R_factor_gt 0.0330 _refine_ls_shift/su_max -0.0002 _refine_ls_shift/su_mean 0.0000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0572P)^2^+0.8757P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0898 _refine_ls_wR_factor_ref 0.0924 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 12 _reflns_limit_h_min -12 _reflns_limit_k_max 11 _reflns_limit_k_min -11 _reflns_limit_l_max 24 _reflns_limit_l_min 0 _reflns_number_gt 5909 _reflns_number_total 6366 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL LUAN in P-1 CELL 1.54178 10.0583 10.1823 20.6673 97.263 94.133 119.439 ZERR 2 0.0002 0.0002 0.0003 0.002 0.001 0.002 LATT 1 SFAC C H Cd N O UNIT 66 76 4 8 30 L.S. 15 PLAN 5 TEMP 23(2) CONF CONN 6 $Cd FMAP 2 ACTA BOND $H EXTI 0.000613 WGHT 0.05719 0.875735 FVAR 0.090987 REM REM REM > REM REM > REM > REM REM Cd1 3 1.42670 1.22894 -0.10663 11.00000 0.04326 0.02553 0.03193 = 0.01259 0.01501 0.02070 Cd2 3 0.51650 -0.06982 0.41515 11.00000 0.03812 0.04332 0.03879 = 0.02356 0.01845 0.02426 O1 5 1.52184 1.11538 -0.19303 11.00000 0.05483 0.02931 0.05093 = 0.01820 0.02058 0.02804 O1W 5 1.64318 1.36668 -0.02540 11.00000 0.04538 0.04630 0.04144 = 0.00092 0.00801 0.02586 AFIX 3 H1Wa 2 1.73882 1.39895 -0.02535 11.00000 -1.20000 H1Wb 2 1.63256 1.39912 0.01273 11.00000 -1.20000 AFIX 0 O2 5 1.44221 1.01149 -0.10720 11.00000 0.09066 0.05026 0.04804 = 0.02188 0.03633 0.05276 O2W 5 1.17356 1.09034 -0.17430 11.00000 0.05342 0.04043 0.03903 = 0.00637 0.01077 0.02174 AFIX 3 H2Wa 2 1.18997 1.12523 -0.20995 11.00000 -1.20000 H2Wb 2 1.14584 1.00452 -0.19857 11.00000 -1.20000 AFIX 0 O3 5 1.40475 0.50118 -0.09031 11.00000 0.05631 0.03366 0.04077 = 0.01727 0.01882 0.02449 O3W 5 0.40397 -0.22324 0.30875 11.00000 0.06238 0.05828 0.04752 = 0.01716 0.00473 0.02241 AFIX 3 H3Wa 2 0.33296 -0.31658 0.29674 11.00000 -1.20000 H3Wb 2 0.42946 -0.18594 0.27410 11.00000 -1.20000 AFIX 0 O4 5 1.49270 0.40831 -0.16746 11.00000 0.07109 0.02825 0.04343 = 0.01726 0.02004 0.03266 O5 5 0.22880 -0.11628 0.38643 11.00000 0.04689 0.08699 0.05894 = 0.03880 0.02831 0.03696 O6 5 0.33412 -0.12720 0.48066 11.00000 0.02942 0.04776 0.05188 = 0.01365 0.01339 0.02062 O7 5 0.58613 -0.21868 0.46968 11.00000 0.04471 0.07688 0.06543 = 0.03760 0.02983 0.04436 O8 5 0.73408 -0.09765 0.39984 11.00000 0.04199 0.05164 0.04174 = 0.01811 0.01361 0.03057 O9 5 1.14844 0.73555 0.01742 11.00000 0.06947 0.04679 0.05923 = 0.02830 0.03389 0.03955 O10 5 0.88468 0.19230 0.22990 11.00000 0.07810 0.03749 0.06717 = 0.01719 0.03788 0.03256 N1 4 1.28900 1.16347 -0.02081 11.00000 0.04018 0.02944 0.03190 = 0.01048 0.01151 0.01726 N2 4 0.61291 0.14651 0.37287 11.00000 0.04008 0.03955 0.03534 = 0.01896 0.01192 0.02080 N3 4 1.03039 0.76143 0.10253 11.00000 0.05173 0.04338 0.04009 = 0.02198 0.02136 0.02119 AFIX 43 H3 2 1.00760 0.82003 0.12702 11.00000 -1.20000 AFIX 0 N4 4 0.95051 0.43447 0.22749 11.00000 0.05584 0.03745 0.04170 = 0.02164 0.02673 0.02918 AFIX 43 H4 2 0.94466 0.51327 0.24359 11.00000 -1.20000 AFIX 0 C1 1 1.24647 1.25411 0.01335 11.00000 0.04009 0.03227 0.03586 = 0.00748 0.00759 0.01752 AFIX 43 H1 2 1.27498 1.34926 0.00233 11.00000 -1.20000 AFIX 0 C2 1 1.16211 1.21101 0.06410 11.00000 0.04311 0.04094 0.03745 = 0.00196 0.00928 0.02389 AFIX 43 H2 2 1.13486 1.27659 0.08707 11.00000 -1.20000 AFIX 0 C3 1 1.11825 1.06987 0.08069 11.00000 0.03703 0.04707 0.02798 = 0.00862 0.01051 0.01997 AFIX 43 H3a 2 1.06179 1.03935 0.11508 11.00000 -1.20000 AFIX 0 C4 1 1.15962 0.97431 0.04529 11.00000 0.03077 0.03441 0.02983 = 0.01102 0.00666 0.01457 C5 1 1.24602 1.02741 -0.00422 11.00000 0.04143 0.03613 0.03375 = 0.01208 0.01367 0.02192 AFIX 43 H5 2 1.27611 0.96455 -0.02742 11.00000 -1.20000 AFIX 0 C6 1 1.11366 0.81474 0.05469 11.00000 0.03340 0.04060 0.03461 = 0.01725 0.00905 0.01866 C7 1 0.97721 0.60653 0.11425 11.00000 0.04210 0.04224 0.04318 = 0.02262 0.01207 0.01478 AFIX 23 H7a 2 0.89149 0.57641 0.13894 11.00000 -1.20000 H7b 2 0.94014 0.53603 0.07223 11.00000 -1.20000 AFIX 0 C8 1 1.10438 0.59492 0.15219 11.00000 0.04001 0.05339 0.04655 = 0.02650 0.02006 0.01849 AFIX 23 H8a 2 1.18104 0.60592 0.12408 11.00000 -1.20000 H8b 2 1.15475 0.67838 0.18999 11.00000 -1.20000 AFIX 0 C9 1 1.04381 0.44392 0.17577 11.00000 0.06001 0.05969 0.04861 = 0.02809 0.03059 0.03893 AFIX 23 H9a 2 1.13006 0.43337 0.19246 11.00000 -1.20000 H9b 2 0.98189 0.36015 0.13891 11.00000 -1.20000 AFIX 0 C10 1 0.87468 0.30513 0.24984 11.00000 0.04129 0.03656 0.03418 = 0.01252 0.01189 0.01921 C11 1 0.58342 0.25737 0.39381 11.00000 0.04576 0.04704 0.03455 = 0.01581 0.01401 0.02386 AFIX 43 H11 2 0.51895 0.24348 0.42553 11.00000 -1.20000 AFIX 0 C12 1 0.74178 0.41357 0.32260 11.00000 0.05262 0.03122 0.04412 = 0.01307 0.01815 0.01867 AFIX 43 H12 2 0.78409 0.50352 0.30552 11.00000 -1.20000 AFIX 0 C13 1 0.64609 0.39211 0.36965 11.00000 0.05672 0.03804 0.04730 = 0.01041 0.01979 0.02655 AFIX 43 H13 2 0.62402 0.46808 0.38496 11.00000 -1.20000 AFIX 0 C14 1 0.70631 0.16668 0.32787 11.00000 0.03976 0.03677 0.03531 = 0.01540 0.01090 0.01866 AFIX 43 H14 2 0.72700 0.08905 0.31381 11.00000 -1.20000 AFIX 0 C15 1 0.77395 0.29913 0.30116 11.00000 0.03550 0.02882 0.02978 = 0.00858 0.00775 0.01327 C16 1 1.49802 1.01382 -0.15938 11.00000 0.03652 0.02415 0.03732 = 0.00710 0.00857 0.01643 C17 1 1.53860 0.89300 -0.18075 11.00000 0.03477 0.02351 0.02906 = 0.00596 0.00635 0.01693 C18 1 1.63431 0.91190 -0.22859 11.00000 0.04083 0.02492 0.03318 = 0.01207 0.01108 0.01945 AFIX 43 H18 2 1.67215 0.99959 -0.24724 11.00000 -1.20000 AFIX 0 C19 1 1.67416 0.80251 -0.24888 11.00000 0.04092 0.03362 0.03238 = 0.01054 0.01082 0.02146 C20 1 1.61414 0.67157 -0.22083 11.00000 0.04295 0.02959 0.03261 = 0.00687 0.00969 0.02502 AFIX 43 H20 2 1.63675 0.59543 -0.23507 11.00000 -1.20000 AFIX 0 C21 1 1.52106 0.65148 -0.17197 11.00000 0.03694 0.02359 0.02865 = 0.00608 0.00286 0.01671 C22 1 1.48403 0.76344 -0.15173 11.00000 0.03378 0.02528 0.02816 = 0.00765 0.00723 0.01570 AFIX 43 H22 2 1.42280 0.75176 -0.11882 11.00000 -1.20000 AFIX 0 C23 1 1.46759 0.51176 -0.14049 11.00000 0.03719 0.02436 0.03184 = 0.00746 0.00096 0.01707 C24 1 1.77940 0.82561 -0.29989 11.00000 0.07197 0.05234 0.05726 = 0.02444 0.03569 0.04282 AFIX 33 H24a 2 1.79450 0.73927 -0.30795 11.00000 -1.50000 H24b 2 1.73356 0.83485 -0.34017 11.00000 -1.50000 H24c 2 1.87726 0.91743 -0.28407 11.00000 -1.50000 AFIX 0 C25 1 -0.18010 -0.22219 0.46794 11.00000 0.03098 0.03293 0.03212 = 0.00275 0.00780 0.01828 C26 1 -0.21297 -0.31574 0.51443 11.00000 0.03198 0.03967 0.03388 = 0.00732 0.01223 0.01932 AFIX 43 H26 2 -0.30710 -0.35217 0.52991 11.00000 -1.20000 AFIX 0 C27 1 -0.10838 -0.35686 0.53868 11.00000 0.03846 0.03411 0.03196 = 0.00674 0.00941 0.01868 C28 1 -0.03972 -0.16596 0.44450 11.00000 0.03165 0.03129 0.03118 = 0.00814 0.00800 0.01669 AFIX 43 H28 2 -0.01792 -0.10405 0.41277 11.00000 -1.20000 AFIX 0 C29 1 0.21889 -0.14353 0.44317 11.00000 0.03151 0.03421 0.04854 = 0.01237 0.01396 0.01781 C30 1 0.06800 -0.20274 0.46873 11.00000 0.02791 0.03137 0.03573 = 0.00572 0.00992 0.01476 C31 1 0.03276 -0.29717 0.51566 11.00000 0.03264 0.03572 0.03746 = 0.00658 0.00609 0.01964 AFIX 43 H31 2 0.10544 -0.32086 0.53200 11.00000 -1.20000 AFIX 0 C32 1 0.70560 -0.17772 0.44421 11.00000 0.03548 0.04235 0.03496 = 0.00413 0.00910 0.02193 C33 1 -0.14852 -0.46258 0.58739 11.00000 0.05471 0.05295 0.04946 = 0.02321 0.02106 0.03199 AFIX 33 H33a 2 -0.25009 -0.49137 0.59723 11.00000 -1.50000 H33b 2 -0.14636 -0.55281 0.56898 11.00000 -1.50000 H33c 2 -0.07486 -0.41138 0.62720 11.00000 -1.50000 AFIX 0 AFIX 6 O4W 5 0.73325 0.75380 0.27953 11.00000 0.07605 0.08155 0.03969 = 0.00515 0.00871 0.04467 H4Wa 2 0.63779 0.69401 0.26468 11.00000 -1.50000 H4Wb 2 0.73496 0.79565 0.31811 11.00000 -1.50000 AFIX 0 O5W 5 1.00294 0.74102 0.27532 11.00000 0.07648 0.04777 0.07248 = 0.00809 0.02333 0.02921 AFIX 3 H5Wa 2 0.91624 0.73102 0.28187 11.00000 -1.20000 H5Wb 2 1.06465 0.78491 0.31159 11.00000 -1.20000 AFIX 0 HKLF 4 END Q1 1 0.472222 -0.111111 0.361111 11 0.05 0.83 Q2 1 1.472222 1.25 -0.055556 11 0.05 0.77 Q4 1 0.583333 -0.027778 0.472222 11 0.05 0.62 Q3 1 1.388889 1.222222 -0.152778 11 0.05 0.64 Q5 1 0.555556 0 0.375 11 0.05 0.54 REM The information below was added by Olex2. REM REM R1 = 0.0330 for 5909 Fo > 4sig(Fo) and 0.0349 for all 6366 data REM 491 parameters refined using 0 restraints REM Highest difference peak 0.8308, deepest hole -0.8557 REM Mean Shift 0.0000, Max Shift -0.0002. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0349 REM R1_gt = 0.0330 REM wR_ref = 0.0924 REM GOOF = 1.0450 REM Shift_max = -0.0002 REM Shift_mean = 0.0000 REM Reflections_all = 6366 REM Reflections_gt = 5909 REM Parameters = 491 REM Hole = -0.8557 REM Peak = 0.8308 REM Flack = n/a ; _cod_data_source_file d3ce00899a2.cif _cod_data_source_block Cd_CP_3 _cod_database_code 7247817 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, {H1Wa,H1Wb} of O1W, {H2Wa,H2Wb} of O2W, {H3Wa,H3Wb} of O3W, {H5Wa,H5Wb} of O5W, All C(H,H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups, {H4Wa,H4Wb} of O4W 2.a Riding coordinates: O1W(H1Wa,H1Wb), O2W(H2Wa,H2Wb), O3W(H3Wa,H3Wb), O5W(H5Wa,H5Wb) 2.b Free rotating group: O4W(H4Wa,H4Wb) 2.c Secondary CH2 refined with riding coordinates: C7(H7a,H7b), C8(H8a,H8b), C9(H9a,H9b) 2.d Me refined with riding coordinates: C24(H24a,H24b,H24c), C33(H33a,H33b,H33c) 2.e Aromatic/amide H refined with riding coordinates: N3(H3), N4(H4), C1(H1), C2(H2), C3(H3a), C5(H5), C11(H11), C12(H12), C13(H13), C14(H14), C18(H18), C20(H20), C22(H22), C26(H26), C28(H28), C31(H31) 3. First, the hydrogen atoms on a water molecule do not all have to have acceptor atoms. Second, it is normal for checkcif to differ from the actual analytical results. We do our best to find the receptors for H3WA, O3W_H3WA_O5, D_A = 3.870, D_H_A = 98.52. 4. Likely Affected by the Beamstop is due to the fact that there is disorder in the lattice water molecules, which causes the hydrogen of the water to be unable to determine the direction. ; _iucr_refine_fcf_details ; data_Cd_CP_3_CCDC1 _computing_structure_refinement 'olex2.refine 1.5-dev (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_Int_Tables_number 2 _cell_length_a 10.0583(2) _cell_length_b 10.1823(2) _cell_length_c 20.6673(3) _cell_angle_alpha 97.263(2) _cell_angle_beta 94.133(1) _cell_angle_gamma 119.439(2) _cell_volume 1806.38(7) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -12 5 1 960.280 949.011 60.651 3.625 o -12 5 2 1.468 13.062 10.687 131.498 o -12 6 1 183.359 174.603 26.131 20.837 o -12 6 2 147.190 156.777 23.754 25.079 o -12 6 3 1.942 -1.187 9.500 171.973 o -12 6 4 809.124 756.169 52.314 4.904 o -12 7 1 25.318 26.125 15.437 63.050 o -12 7 2 42.336 42.751 16.625 53.609 o -12 7 3 119.065 124.705 21.378 31.103 o -11 1 3 462.439 342.237 30.896 14.137 o -11 1 4 1061.410 780.292 51.147 5.062 o -11 2 1 878.205 785.870 54.690 4.505 o -11 2 2 61.748 41.564 15.438 61.794 o -11 2 3 1222.780 1093.110 68.989 2.816 o -11 2 4 96.052 92.633 20.189 35.456 o -11 2 5 46.974 47.501 14.250 71.281 o -11 2 6 10.730 13.062 10.687 131.448 o -11 2 7 1366.410 1268.330 73.768 2.428 o -11 2 8 5.007 2.375 8.312 222.364 o -11 2 9 568.861 464.701 35.655 10.442 o -11 3 1 22.233 22.562 9.236 168.564 o -11 3 2 682.278 677.571 49.916 5.433 o -11 3 3 198.852 198.353 29.694 16.271 o -11 3 4 247.509 279.138 33.259 12.766 o -11 3 5 237.154 239.937 30.883 14.857 o -11 3 6 1278.250 1392.850 83.261 1.931 o -11 3 7 396.381 411.073 38.018 9.540 o -11 3 8 232.004 238.752 27.320 18.547 o -11 3 9 1225.550 1105.060 66.613 2.983 o -11 3 10 206.179 162.729 21.381 30.166 o -11 3 11 2.400 3.562 7.125 299.632 o -11 4 1 161.364 157.961 26.129 21.034 o -11 4 2 508.848 539.439 47.528 6.154 o -11 4 3 216.125 213.761 21.306 29.110 o -11 4 4 13.586 4.875 7.683 256.562 o -11 4 5 24.063 35.624 16.625 54.047 o -11 4 6 2887.170 3098.720 154.936 0.548 o -11 4 7 80.401 67.691 17.813 45.813 o -11 4 8 1321.640 1375.090 82.077 1.985 o -11 4 9 4.956 9.500 10.687 132.661 o -11 4 10 87.801 72.443 16.626 51.814 o -11 4 11 19.622 23.750 10.687 127.922 o -11 5 1 833.187 936.659 68.942 2.905 o -11 5 2 22.161 35.624 16.625 54.048 o -11 5 3 1153.920 1113.020 74.915 2.431 o -11 5 4 10.717 1.187 10.687 135.429 o -11 5 5 945.589 959.392 64.197 3.277 o -11 5 6 685.013 637.045 48.133 5.854 o -11 5 7 35.145 45.125 16.625 53.476 o -11 5 8 436.754 439.605 41.584 8.051 o -11 5 9 687.740 738.087 53.485 4.741 o -11 5 10 4.952 2.375 8.312 222.365 o -11 5 11 648.113 531.445 99.841 1.520 o -11 5 12 511.416 428.965 50.508 5.661 o -11 6 1 1024.120 1021.220 71.336 2.693 o -11 6 2 155.794 191.214 32.067 14.146 o -11 6 3 0.365 -3.562 14.249 76.439 o -11 6 4 780.346 773.771 59.429 3.905 o -11 6 5 1618.300 1587.250 92.808 1.555 o -11 6 6 33.739 39.187 15.437 62.016 o -11 6 7 760.386 647.792 48.733 5.711 o -11 6 9 131.528 124.704 21.378 31.098 o -11 6 10 54.150 45.126 13.063 84.085 o -11 6 11 1158.970 1019.800 147.505 0.694 o -11 7 1 161.867 150.234 14.056 62.126 o -11 7 2 257.093 241.400 17.387 39.345 o -11 7 3 29.292 22.163 7.998 219.716 o -11 7 4 1753.260 1859.250 72.004 2.220 o -11 7 5 6.191 11.874 13.062 89.147 o -11 7 6 177.250 155.591 24.942 22.946 o -11 7 7 37.615 32.062 13.062 86.046 o -11 7 8 502.922 470.554 39.213 8.839 o -11 7 10 1230.850 925.579 52.346 4.669 o -11 8 1 1117.290 1135.010 41.944 6.047 o -11 8 2 31.844 32.462 8.322 196.195 o -11 8 3 556.363 659.118 53.474 4.837 o -11 8 4 404.913 468.242 29.930 13.947 o -11 8 5 20.611 42.749 16.625 53.630 o -11 8 6 780.691 744.146 57.059 4.225 o -11 8 7 661.206 670.355 51.109 5.225 o -11 8 8 6.143 9.500 9.500 166.835 o -11 9 1 372.403 440.509 29.656 14.384 o -11 9 2 3.789 2.327 10.271 146.177 o -11 9 3 1321.900 1428.820 95.175 1.521 o -11 9 4 90.341 116.384 24.939 23.492 o -11 9 5 79.435 91.444 21.377 31.897 o -11 9 6 13.945 11.875 13.062 89.128 o -10 0 1 152.087 114.018 20.191 34.811 o -10 0 2 1018.820 929.842 60.642 3.640 o -10 0 3 18.546 29.687 13.062 86.444 o -10 0 4 845.678 763.193 52.306 4.894 o -10 0 5 157.103 176.965 23.754 24.745 o -10 0 6 7.339 10.687 9.500 166.200 o -10 0 7 273.246 300.810 29.103 16.038 o -10 0 8 630.652 569.572 69.526 3.035 o -10 0 9 253.735 279.150 21.382 27.361 o -10 0 10 6.768 13.062 5.937 397.013 o -10 0 11 1142.120 1119.380 55.910 3.970 o -10 1 1 466.597 399.208 40.396 8.590 o -10 1 2 399.340 375.414 38.017 9.662 o -10 1 3 264.082 289.828 33.259 12.709 o -10 1 4 1484.170 1529.810 89.219 1.678 o -10 1 5 11.291 16.624 11.874 106.358 o -10 1 6 22.855 24.937 13.062 87.142 o -10 1 7 36.804 21.375 6.110 354.311 o -10 1 8 1354.470 1345.480 50.976 4.242 o -10 1 9 1.628 0.108 4.124 910.534 o -10 1 10 636.088 623.276 46.349 6.279 o -10 1 11 71.077 75.620 8.550 159.566 o -10 1 12 74.529 73.629 10.688 112.696 o -10 1 13 33.039 27.312 7.125 262.909 o -10 2 1 1521.300 1643.950 68.974 2.493 o -10 2 2 66.586 61.526 12.512 88.228 o -10 2 3 1318.520 1349.820 85.627 1.851 o -10 2 4 354.780 363.507 39.202 9.179 o -10 2 5 36.193 40.375 16.625 53.755 o -10 2 6 68.669 66.502 19.001 40.627 o -10 2 7 1113.620 1159.580 46.567 5.168 o -10 2 8 102.313 101.165 10.968 101.040 o -10 2 9 408.990 417.923 23.674 20.773 o -10 2 10 698.508 690.513 31.407 11.373 o -10 2 11 875.642 788.563 33.664 9.733 o -10 2 12 123.296 123.499 11.129 93.758 o -10 2 13 729.259 653.362 55.867 4.478 o -10 2 14 495.156 477.706 28.520 14.966 o -10 3 1 133.559 127.142 18.041 42.114 o -10 3 2 319.074 338.897 27.680 17.105 o 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96.365 1.453 o -10 6 10 5.652 -1.187 10.687 135.862 o -10 6 11 1958.700 2073.640 108.324 1.118 o -10 6 12 150.939 116.118 26.129 21.509 o -10 6 13 12.094 8.708 4.831 598.657 o -10 6 14 547.469 479.679 26.145 17.072 o -10 7 1 40.406 48.799 16.540 53.773 o -10 7 2 602.879 622.371 29.374 13.065 o -10 7 3 217.462 205.470 16.514 44.546 o -10 7 4 1155.280 1241.560 49.656 4.570 o -10 7 5 33.222 41.424 9.307 156.302 o -10 7 6 101.127 108.797 15.383 56.916 o -10 7 7 151.269 125.891 23.753 25.577 o -10 7 8 745.115 742.818 57.048 4.227 o -10 7 9 97.149 78.380 19.001 40.185 o -10 7 10 514.238 444.394 39.211 8.921 o -10 7 11 857.672 924.881 59.440 3.773 o -10 7 12 144.147 128.269 19.003 38.357 o -10 7 13 348.402 335.035 27.326 17.522 o -10 8 1 929.003 1075.260 41.881 6.223 o -10 8 2 145.898 159.088 15.026 55.133 o -10 8 3 731.415 824.339 35.200 8.970 o -10 8 4 349.206 396.274 55.833 4.719 o -10 8 5 163.484 167.359 27.317 19.276 o -10 8 6 119.498 114.011 24.940 23.517 o -10 8 7 159.129 131.832 24.941 23.271 o -10 8 8 847.143 845.181 60.625 3.712 o -10 8 9 94.550 98.570 20.189 35.285 o -10 8 10 1606.880 1660.150 89.255 1.644 o -10 8 11 52.804 41.618 8.906 168.413 o -10 8 12 133.583 96.203 15.440 57.477 o -10 9 1 1020.640 1048.860 41.855 6.298 o -10 9 2 100.149 79.453 14.921 62.523 o -10 9 3 1970.750 2447.090 92.297 1.360 o -10 9 4 1.162 1.295 8.787 200.047 o -10 9 5 1.074 13.062 15.437 64.106 o -10 9 6 41.248 51.063 20.188 36.665 o -10 9 7 742.544 878.734 59.432 3.815 o -10 9 8 68.357 88.572 14.275 66.783 o -10 9 9 675.123 839.886 73.101 2.658 o -10 9 10 420.297 392.120 33.271 12.148 o -10 10 1 80.900 72.442 15.438 59.367 o -10 10 2 746.455 851.069 55.866 4.273 o -10 10 3 577.090 844.943 77.245 2.400 o -10 10 4 120.721 211.400 36.817 10.832 o -10 10 5 354.664 465.717 49.898 5.742 o -10 10 6 402.866 645.176 55.844 4.491 o -9 -2 1 40.798 46.313 11.875 99.950 o -9 -2 2 198.101 230.426 21.380 28.546 o -9 -2 3 665.834 548.065 115.881 1.135 o -9 -2 4 5.915 7.125 5.937 415.638 o -9 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9.147 o 2 -8 0 441.074 410.890 14.599 39.165 o 2 -8 1 1072.290 1027.960 30.121 9.695 o 2 -8 2 2271.960 2122.040 44.363 3.642 o 2 -8 3 10.055 14.236 4.087 742.264 o 2 -8 4 1920.780 1801.390 53.639 3.371 o 2 -8 5 2561.850 2563.800 63.599 2.150 o 2 -8 6 0.685 5.805 3.109 1367.440 o 2 -8 7 1101.490 1097.250 33.892 8.099 o 2 -8 8 2541.380 2657.950 58.965 2.262 o 2 -8 9 684.530 697.269 28.943 12.704 o 2 -8 10 1865.420 1848.740 70.870 2.276 o 2 -8 11 2905.550 2707.700 103.621 1.093 o 2 -8 12 985.655 1001.620 37.061 7.616 o 2 -8 13 2.552 9.675 5.268 507.705 o 2 -8 14 7225.280 6587.680 229.834 0.222 o 2 -8 15 199.161 196.011 21.973 28.007 o 2 -8 16 18.637 22.087 7.904 224.669 o 2 -8 17 18.866 19.791 11.875 105.643 o 2 -8 18 2295.660 2442.970 125.635 0.833 o 2 -8 19 4.174 2.375 4.750 667.165 o 2 -8 20 1568.160 1506.750 69.030 2.573 o 2 -7 0 3702.800 3353.630 57.595 1.834 o 2 -7 1 3695.550 3457.990 64.749 1.614 o 2 -7 2 1552.050 1429.230 33.745 6.699 o 2 -7 3 2028.910 2063.570 57.071 2.858 o 2 -7 4 961.252 970.393 28.054 10.927 o 2 -7 5 634.795 683.598 20.318 19.748 o 2 -7 6 82.149 72.987 6.005 261.373 o 2 -7 7 6277.470 6412.330 121.970 0.489 o 2 -7 8 1604.980 1642.390 48.603 4.043 o 2 -7 9 740.030 744.616 20.870 18.058 o 2 -7 10 22.665 15.340 3.534 908.308 o 2 -7 11 5732.860 5222.120 119.159 0.605 o 2 -7 12 548.070 494.737 21.520 22.202 o 2 -7 13 2575.130 2419.580 87.561 1.476 o 2 -7 14 408.122 407.749 38.609 9.291 o 2 -7 15 213.281 207.053 17.925 39.030 o 2 -7 16 309.773 332.063 33.260 12.482 o 2 -7 17 2542.570 2604.200 90.607 1.356 o 2 -7 18 448.959 448.183 19.285 26.877 o 2 -7 19 714.787 653.205 28.143 13.595 o 2 -7 20 914.696 902.036 34.038 9.005 o 2 -7 21 401.618 410.594 18.483 29.618 o 2 -6 0 14598.600 13291.000 215.365 0.138 o 2 -6 1 179.548 275.539 10.263 72.755 o 2 -6 2 211.924 245.137 10.380 77.044 o 2 -6 3 205.401 215.283 8.951 96.906 o 2 -6 4 8206.840 7933.600 131.681 0.366 o 2 -6 5 88.770 61.484 4.907 356.261 o 2 -6 6 7400.000 7667.210 125.805 0.394 o 2 -6 7 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1.282 o 2 -1 11 5501.990 5279.080 110.061 0.653 o 2 -1 12 17.510 34.307 4.423 518.620 o 2 -1 13 1828.680 1716.580 42.538 4.559 o 2 -1 14 4589.770 4702.190 100.728 0.792 o 2 -1 15 1288.790 1307.450 49.187 4.522 o 2 -1 16 1553.000 1498.270 62.087 3.032 o 2 -1 17 204.954 221.918 17.222 40.896 o 2 -1 18 1585.060 1583.820 56.771 3.366 o 2 -1 19 97.425 98.478 9.972 117.781 o 2 -1 20 2772.760 2780.270 125.076 0.807 o 2 -1 21 346.957 356.379 26.134 18.612 o 2 -1 22 46.317 60.563 9.500 142.127 o 2 -1 23 8.965 7.125 4.750 629.232 o 2 0 0 19249.600 18876.600 323.213 0.071 o 2 0 1 523.981 503.609 13.029 37.764 o 2 0 2 2156.480 2035.080 41.346 4.064 o 2 0 3 149132.000 153596.000 2389.840 0.002 o 2 0 4 39055.400 37407.300 723.060 0.017 o 2 0 5 499.008 465.389 15.545 33.872 o 2 0 6 2273.010 2049.110 45.309 3.696 o 2 0 7 10281.600 9269.340 184.116 0.233 o 2 0 8 31.771 27.759 4.534 535.923 o 2 0 9 2242.510 2135.320 56.614 2.818 o 2 0 10 1832.080 1872.760 44.486 4.061 o 2 0 11 2288.000 2314.950 40.733 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14.758 o 8 -3 13 72.924 92.027 9.745 124.303 o 8 -3 14 14.428 12.980 5.029 532.473 o 8 -3 15 1.798 0.848 3.456 1272.620 o 8 -3 16 556.709 537.407 19.661 23.843 o 8 -2 0 1605.350 1884.870 77.620 1.971 o 8 -2 1 460.045 499.878 37.032 9.646 o 8 -2 2 4689.140 5095.120 415.995 0.085 o 8 -2 3 5207.880 5868.190 378.605 0.099 o 8 -2 4 121.069 130.664 20.189 34.342 o 8 -2 5 1667.510 1911.760 77.047 1.982 o 8 -2 6 21.295 34.582 9.170 164.140 o 8 -2 7 128.533 146.111 12.347 76.496 o 8 -2 8 148.476 143.628 12.060 79.575 o 8 -2 9 1326.980 1507.460 50.465 4.058 o 8 -2 10 19.523 22.528 5.991 364.052 o 8 -2 11 364.650 338.446 19.106 30.638 o 8 -2 12 7.079 10.283 5.399 482.477 o 8 -2 13 272.201 291.123 15.679 42.855 o 8 -2 14 33.756 27.583 5.399 413.820 o 8 -2 15 91.110 99.909 7.979 160.877 o 8 -1 0 764.805 810.315 40.440 7.341 o 8 -1 1 191.867 230.224 20.546 30.511 o 8 -1 2 2549.950 2931.310 103.559 1.055 o 8 -1 3 34.991 44.904 11.642 103.943 o 8 -1 4 17.101 26.932 10.271 136.666 o 8 -1 5 43.639 42.750 14.250 71.788 o 8 -1 6 1760.710 1850.080 67.867 2.424 o 8 -1 7 58.744 70.710 12.154 91.227 o 8 -1 8 1460.030 1543.460 60.971 3.077 o 8 -1 9 563.355 640.627 40.652 7.799 o 8 -1 10 21.838 30.516 6.938 270.654 o 8 -1 11 398.062 409.054 20.066 26.570 o 8 -1 12 135.800 156.250 11.616 81.912 o 8 -1 13 6.090 14.357 4.451 645.791 o 8 -1 14 570.956 459.610 26.256 17.200 o 8 0 0 170.593 189.741 14.430 56.060 o 8 0 1 123.694 117.181 11.643 88.750 o 8 0 2 306.735 299.946 18.346 33.917 o 8 0 3 426.520 437.185 36.828 9.987 o 8 0 4 111.121 84.319 16.626 51.093 o 8 0 5 1517.080 1499.920 83.263 1.896 o 8 0 6 228.089 259.243 20.104 30.762 o 8 0 7 440.743 435.053 45.146 6.948 o 8 0 8 1296.200 1322.190 129.034 0.880 o 8 0 9 5.441 4.476 5.409 507.550 o 8 0 10 291.289 295.846 19.024 32.289 o 8 0 11 0.504 2.437 3.747 1052.470 o 8 0 12 581.084 550.186 20.782 22.007 o 8 1 0 4.003 8.386 6.561 341.110 o 8 1 1 1326.640 1400.070 56.322 3.607 o 8 1 2 181.026 191.898 14.727 54.174 o 8 1 3 133.913 117.747 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7.125 8.312 218.034 o 9 -9 0 19.044 37.094 9.412 155.475 o 9 -9 1 2124.440 1975.860 75.528 2.012 o 9 -9 2 25.658 26.020 13.656 79.873 o 9 -9 3 2106.080 1970.200 60.711 2.725 o 9 -9 4 890.752 789.272 40.415 7.409 o 9 -9 5 147.106 123.408 12.342 79.951 o 9 -9 6 803.013 685.712 46.203 6.188 o 9 -9 7 1152.660 967.069 45.380 5.773 o 9 -9 8 149.295 115.458 11.796 87.207 o 9 -9 9 1199.400 1002.470 45.824 5.614 o 9 -9 10 54.992 57.751 8.227 180.980 o 9 -9 11 1.078 -0.163 4.701 702.230 o 9 -9 12 272.886 223.571 14.617 52.120 o 9 -9 13 1073.570 864.718 47.577 5.562 o 9 -8 0 1401.120 1370.730 50.446 4.264 o 9 -8 1 58.651 65.403 8.918 154.954 o 9 -8 2 2495.450 2406.670 81.705 1.633 o 9 -8 3 2704.510 2512.370 89.098 1.413 o 9 -8 4 6.006 10.654 7.479 262.790 o 9 -8 5 1430.870 1296.750 39.574 6.038 o 9 -8 6 312.652 296.230 16.954 38.169 o 9 -8 7 446.231 392.410 21.607 24.289 o 9 -8 8 13.059 12.320 7.063 289.888 o 9 -8 9 2889.010 2554.270 79.394 1.643 o 9 -8 10 103.042 101.873 10.928 101.448 o 9 -8 11 78.635 75.510 9.308 140.086 o 9 -8 12 12.459 10.539 6.561 336.138 o 9 -8 13 1590.280 1313.700 50.407 4.357 o 9 -8 14 12.209 12.044 3.456 1000.590 o 9 -7 0 655.541 678.139 31.328 11.499 o 9 -7 1 126.997 136.505 13.028 71.719 o 9 -7 2 3724.700 3646.370 111.395 0.847 o 9 -7 3 7.161 4.972 6.787 326.519 o 9 -7 4 286.076 298.983 19.041 32.139 o 9 -7 5 28.675 21.679 8.074 216.410 o 9 -7 6 2163.610 1994.430 54.389 3.095 o 9 -7 7 38.183 30.088 7.524 236.006 o 9 -7 8 3227.990 2950.000 82.744 1.423 o 9 -7 9 699.299 598.350 23.738 17.793 o 9 -7 10 36.686 30.745 7.768 222.695 o 9 -7 11 316.610 225.756 15.371 48.246 o 9 -7 12 951.211 959.316 85.004 1.982 o 9 -7 13 13.205 9.500 5.035 550.949 o 9 -7 14 528.603 526.848 84.966 2.079 o 9 -6 0 28.291 45.885 8.805 169.434 o 9 -6 1 1905.160 1922.920 53.266 3.256 o 9 -6 2 74.530 80.604 10.006 123.164 o 9 -6 3 3.915 11.170 6.087 384.945 o 9 -6 4 180.286 205.815 13.069 62.978 o 9 -6 5 2268.780 2186.190 57.583 2.712 o 9 -6 6 151.462 126.660 11.266 91.304 o 9 -6 7 569.768 486.834 25.312 17.809 o 9 -6 8 2110.290 1923.980 76.757 1.987 o 9 -6 9 20.754 21.754 10.271 138.569 o 9 -6 10 173.995 135.091 17.078 45.914 o 9 -6 11 266.291 267.477 16.514 41.133 o 9 -6 12 613.862 512.367 35.056 10.516 o 9 -6 13 2.694 0.562 4.534 748.698 o 9 -6 14 967.629 788.613 38.050 8.131 o 9 -6 15 73.847 49.878 9.501 146.634 o 9 -5 0 293.223 263.282 17.646 37.474 o 9 -5 1 876.789 877.028 58.836 3.882 o 9 -5 2 198.615 181.845 11.906 74.892 o 9 -5 3 36.433 29.067 5.983 347.789 o 9 -5 4 281.282 261.844 16.436 41.701 o 9 -5 5 2172.350 2233.650 80.749 1.724 o 9 -5 6 27.774 31.793 7.925 214.270 o 9 -5 7 1755.460 1818.220 74.260 2.139 o 9 -5 8 87.444 88.202 15.045 60.877 o 9 -5 9 77.509 76.156 13.981 70.602 o 9 -5 10 25.982 27.906 10.076 141.171 o 9 -5 11 1438.350 1461.700 46.908 4.542 o 9 -5 12 57.300 55.066 7.854 196.751 o 9 -5 13 549.448 548.188 22.276 20.212 o 9 -5 14 332.566 295.207 14.371 47.701 o 9 -5 15 141.924 147.275 10.821 92.334 o 9 -4 0 2010.180 1980.470 183.274 0.437 o 9 -4 1 114.902 119.338 12.797 76.145 o 9 -4 2 39.661 38.809 8.830 172.756 o 9 -4 3 30.163 44.026 9.121 160.547 o 9 -4 4 2569.190 2886.540 85.800 1.379 o 9 -4 5 150.629 177.103 16.361 46.913 o 9 -4 6 598.330 621.911 31.014 12.064 o 9 -4 7 1040.000 1125.000 44.122 5.660 o 9 -4 8 1093.550 1130.060 43.663 5.731 o 9 -4 9 127.184 99.067 15.116 59.430 o 9 -4 10 790.114 802.694 35.478 8.964 o 9 -4 11 620.527 622.904 26.083 15.425 o 9 -4 12 4.543 3.381 4.306 794.274 o 9 -4 13 438.147 436.778 18.919 27.897 o 9 -4 14 197.486 200.948 11.415 76.102 o 9 -3 0 2384.570 2557.370 140.489 0.680 o 9 -3 1 205.081 261.025 49.884 5.996 o 9 -3 2 763.743 881.120 45.104 6.023 o 9 -3 3 914.838 1083.240 99.846 1.450 o 9 -3 4 895.788 964.642 54.677 4.297 o 9 -3 5 11.329 11.512 7.854 238.476 o 9 -3 6 978.712 1060.820 42.008 6.234 o 9 -3 7 130.167 160.550 15.418 52.806 o 9 -3 8 17.133 19.536 7.636 241.987 o 9 -3 9 138.087 135.737 10.828 94.804 o 9 -3 10 785.759 809.907 30.819 10.858 o 9 -3 11 11.078 12.120 5.029 537.467 o 9 -3 12 569.674 588.537 23.881 17.829 o 9 -3 13 58.044 58.821 6.603 250.174 o 9 -3 14 405.827 392.111 27.329 16.908 o 9 -2 0 101.955 100.944 23.752 25.986 o 9 -2 1 1.724 2.375 13.062 90.603 o 9 -2 2 98.724 92.778 16.626 50.608 o 9 -2 3 2678.070 2995.820 249.514 0.235 o 9 -2 4 16.727 16.732 8.312 209.523 o 9 -2 5 406.419 415.798 29.109 15.032 o 9 -2 6 3.159 4.275 8.271 222.798 o 9 -2 7 349.292 415.719 36.232 10.368 o 9 -2 8 18.804 22.562 9.236 168.595 o 9 -2 9 642.227 715.106 35.082 9.534 o 9 -2 10 303.477 300.965 20.820 27.972 o 9 -2 11 12.210 13.976 5.410 464.654 o 9 -2 12 239.567 205.748 20.787 30.557 o 9 -1 0 757.571 910.247 44.325 6.123 o 9 -1 1 48.007 60.759 12.512 88.406 o 9 -1 2 2708.500 3149.030 151.863 0.564 o 9 -1 3 286.496 375.048 27.914 16.512 o 9 -1 4 184.259 185.871 18.828 36.824 o 9 -1 5 970.125 1066.340 74.894 2.451 o 9 -1 6 83.349 86.692 21.376 32.006 o 9 -1 7 2.821 10.687 11.874 107.689 o 9 -1 8 211.460 236.363 28.506 17.210 o 9 -1 9 462.264 536.207 28.061 14.786 o 9 -1 10 4.949 4.750 4.561 699.183 o 9 -1 11 76.933 93.076 9.630 126.175 o 9 0 0 46.167 54.625 14.250 70.533 o 9 0 1 166.827 173.140 13.936 60.670 o 9 0 2 1287.660 1299.430 65.214 2.956 o 9 0 3 28.947 30.067 6.939 271.141 o 9 0 4 276.717 252.340 16.273 42.843 o 9 0 5 392.039 420.226 22.043 23.032 o 9 0 6 9.403 13.761 7.100 284.919 o 9 0 7 46.347 42.835 10.094 134.877 o 9 0 8 897.939 938.252 45.775 5.765 o 9 0 9 13.354 11.875 8.312 213.741 o 9 1 0 0.557 0.822 5.409 526.107 o 9 1 1 710.273 750.215 34.425 9.629 o 9 1 2 4.653 4.750 5.700 458.104 o 9 1 3 50.920 35.033 6.603 285.568 o 9 1 4 2.349 9.768 4.826 593.680 o 9 1 5 738.379 712.534 37.423 8.643 o 9 1 6 15.478 12.643 4.177 731.829 o 9 2 0 570.000 559.742 38.029 9.000 o 9 2 1 277.130 244.713 23.759 23.586 o 9 2 2 2.750 4.750 5.937 423.658 o 10 -10 0 1083.180 1186.780 68.971 2.765 o 10 -10 1 474.897 446.760 36.834 9.947 o 10 -10 2 4.189 -20.187 13.062 90.960 o 10 -10 3 14.727 1.187 11.875 109.754 o 10 -10 4 1102.230 946.631 59.462 3.750 o 10 -10 5 136.916 97.389 17.815 44.416 o 10 -10 6 473.468 332.710 30.895 14.202 o 10 -10 7 13.974 5.937 8.312 218.989 o 10 -9 0 149.734 160.222 16.546 47.041 o 10 -9 1 1282.210 1284.730 54.848 3.889 o 10 -9 2 214.500 210.466 19.404 34.162 o 10 -9 3 1445.250 1363.650 57.393 3.546 o 10 -9 4 118.841 113.255 15.383 56.553 o 10 -9 5 147.747 121.141 15.384 55.917 o 10 -9 6 121.938 98.878 12.996 77.031 o 10 -9 7 199.138 147.059 15.118 55.481 o 10 -9 8 20.373 4.156 6.717 334.382 o 10 -9 9 278.711 189.564 15.960 47.923 o 10 -9 10 550.094 418.882 22.258 22.703 o 10 -8 0 729.392 757.549 34.406 9.598 o 10 -8 1 0.910 13.079 8.392 209.022 o 10 -8 2 754.663 779.379 39.753 7.639 o 10 -8 3 1535.840 1466.100 60.407 3.188 o 10 -8 4 8.774 17.164 9.122 175.792 o 10 -8 5 895.259 824.975 33.209 9.720 o 10 -8 6 148.086 124.093 12.753 75.826 o 10 -8 7 593.147 526.327 25.078 17.520 o 10 -8 8 7.647 15.919 7.063 284.343 o 10 -8 9 2408.070 2001.090 58.157 2.849 o 10 -8 10 21.602 16.974 7.100 279.694 o 10 -8 11 31.278 26.955 6.256 328.227 o 10 -7 0 658.955 618.234 29.802 12.819 o 10 -7 1 0.201 11.521 7.167 283.604 o 10 -7 2 1977.920 1956.490 64.230 2.541 o 10 -7 3 9.786 9.859 7.077 292.853 o 10 -7 4 140.108 115.104 15.383 56.386 o 10 -7 5 202.215 145.479 13.494 66.689 o 10 -7 6 946.826 876.565 46.615 5.722 o 10 -7 7 1.067 0.821 6.238 396.401 o 10 -7 8 816.589 692.217 35.761 9.355 o 10 -7 9 976.824 844.517 39.874 7.388 o 10 -7 10 55.597 36.382 9.123 164.381 o 10 -7 11 216.331 155.080 14.204 60.562 o 10 -7 12 476.788 364.517 24.955 19.927 o 10 -6 0 397.925 383.800 22.421 23.183 o 10 -6 1 812.981 817.483 45.717 6.028 o 10 -6 2 349.404 303.535 20.733 28.070 o 10 -6 3 54.884 44.199 9.581 147.162 o 10 -6 4 189.240 190.780 16.350 46.125 o 10 -6 5 570.428 506.478 26.958 15.997 o 10 -6 6 432.728 409.580 32.671 12.428 o 10 -6 7 137.472 130.957 30.285 16.142 o 10 -6 8 1918.910 1682.570 83.421 1.830 o 10 -6 9 40.557 43.371 10.471 126.215 o 10 -6 10 89.871 74.817 16.626 51.672 o 10 -6 11 31.708 33.250 11.875 102.714 o 10 -6 12 361.248 281.578 26.138 19.525 o 10 -5 0 3.397 4.480 8.787 197.674 o 10 -5 1 1170.790 1165.950 55.414 3.968 o 10 -5 2 65.523 59.111 13.357 78.800 o 10 -5 3 136.698 109.831 17.102 47.161 o 10 -5 4 35.611 31.553 10.967 119.521 o 10 -5 5 1081.110 1112.780 43.085 5.882 o 10 -5 6 137.613 141.799 14.555 59.547 o 10 -5 7 935.581 941.450 44.456 6.020 o 10 -5 8 75.288 64.770 11.756 97.798 o 10 -5 9 13.519 14.777 7.418 261.243 o 10 -5 10 4.486 12.573 7.100 286.899 o 10 -5 11 663.303 623.936 29.379 13.046 o 10 -5 12 3.085 3.562 5.038 587.417 o 10 -4 0 2247.870 2421.400 136.903 0.721 o 10 -4 1 472.720 497.804 52.275 5.230 o 10 -4 2 31.692 40.374 20.187 36.968 o 10 -4 3 697.527 749.875 66.550 3.200 o 10 -4 4 1072.540 1103.640 53.099 4.324 o 10 -4 5 65.344 85.279 11.694 94.515 o 10 -4 6 258.832 253.984 17.811 37.368 o 10 -4 7 674.956 655.658 29.059 12.983 o 10 -4 8 342.697 317.457 18.592 32.613 o 10 -4 9 42.172 23.263 13.656 80.187 o 10 -4 10 390.036 366.032 21.794 24.573 o 10 -4 11 592.067 487.375 24.958 18.175 o 10 -3 0 1443.090 1617.010 70.647 2.418 o 10 -3 1 113.705 127.073 27.315 19.673 o 10 -3 2 251.804 276.754 39.197 9.437 o 10 -3 3 274.748 267.260 36.822 10.632 o 10 -3 4 1315.430 1494.940 96.332 1.476 o 10 -3 5 1.674 7.718 8.271 219.657 o 10 -3 6 532.296 465.704 29.084 14.608 o 10 -3 7 19.590 21.493 8.271 207.367 o 10 -3 8 32.547 34.033 8.787 177.272 o 10 -3 9 33.079 17.887 6.561 320.280 o 10 -3 10 583.049 492.031 33.278 11.578 o 10 -2 0 169.534 163.806 19.261 36.203 o 10 -2 1 2.869 -1.187 11.874 110.063 o 10 -2 2 81.896 54.627 17.813 46.406 o 10 -2 3 1183.800 1398.440 87.997 1.753 o 10 -2 4 96.102 97.382 21.376 31.753 o 10 -2 5 554.168 538.288 46.343 6.439 o 10 -2 6 119.048 129.451 21.377 30.991 o 10 -2 7 149.723 142.522 21.378 30.669 o 10 -2 8 3.202 -3.562 8.312 224.591 o 10 -1 0 119.607 132.154 15.439 54.784 o 10 -1 1 0.917 2.746 6.561 353.996 o 10 -1 2 483.533 514.478 43.962 7.122 o 10 -1 3 365.626 401.546 38.016 9.575 o 10 -1 4 18.471 17.812 10.687 129.849 o 10 -1 5 480.505 456.283 39.212 8.885 o 10 -1 6 102.981 100.948 17.814 44.278 o 10 -1 7 53.006 46.314 11.875 99.909 o 10 0 0 48.371 34.438 13.063 85.668 o 10 0 1 122.863 134.204 17.815 42.748 o 10 0 2 768.138 761.994 46.362 6.006 o 10 0 3 101.323 79.054 9.973 124.217 o 11 -9 0 467.965 444.393 36.835 9.957 o 11 -9 1 672.594 623.431 32.998 10.971 o 11 -9 2 32.083 20.943 9.123 173.335 o 11 -9 3 560.411 511.269 29.610 13.823 o 11 -9 4 912.030 702.740 49.940 5.390 o 11 -9 5 3.283 0.223 6.561 359.871 o 11 -9 6 190.296 144.911 19.005 37.728 o 11 -8 0 455.810 473.120 24.846 18.515 o 11 -8 1 104.938 109.456 12.542 80.152 o 11 -8 2 45.791 50.149 9.258 153.297 o 11 -8 3 962.388 892.149 40.964 6.952 o 11 -8 4 8.107 0.279 7.100 307.164 o 11 -8 5 417.437 367.650 23.344 22.090 o 11 -8 6 1.645 6.457 6.561 345.479 o 11 -8 7 776.333 575.916 68.358 3.132 o 11 -7 0 363.406 360.393 21.409 25.372 o 11 -7 1 2.791 0.154 6.450 372.503 o 11 -7 2 966.735 949.821 43.740 6.151 o 11 -7 3 131.553 119.868 12.337 80.597 o 11 -7 4 3.319 14.645 7.418 261.634 o 11 -7 5 323.080 268.420 19.951 30.831 o 11 -7 6 737.543 621.794 70.725 2.918 o 11 -7 7 80.383 72.442 15.438 59.368 o 11 -7 8 281.732 231.651 24.947 21.865 o 11 -6 0 38.572 34.041 10.688 124.567 o 11 -6 1 79.657 81.092 14.251 67.731 o 11 -6 2 938.817 961.816 70.141 2.804 o 11 -6 3 89.380 78.317 13.834 71.679 o 11 -6 4 134.065 128.869 16.545 48.885 o 11 -6 5 197.194 202.201 19.404 34.446 o 11 -6 6 504.623 401.632 35.648 10.722 o 11 -6 7 14.372 7.125 9.500 168.022 o 11 -6 8 785.022 614.637 42.799 7.219 o 11 -5 0 27.811 40.374 19.000 41.578 o 11 -5 1 1523.940 1610.830 99.934 1.363 o 11 -5 2 152.351 157.960 28.504 17.890 o 11 -5 3 70.949 109.254 24.939 23.590 o 11 -5 4 13.742 16.285 8.906 184.440 o 11 -5 5 602.748 568.447 32.148 11.767 o 11 -5 6 25.478 16.889 7.418 258.250 o 11 -5 7 194.841 135.407 17.817 42.641 o 11 -4 0 412.411 472.846 45.146 6.876 o 11 -4 1 340.688 365.889 40.390 8.687 o 11 -4 2 7.376 14.249 13.062 88.785 o 11 -4 3 227.689 233.995 30.883 14.897 o 11 -4 4 842.292 861.872 61.817 3.575 o 11 -4 5 129.192 134.205 22.565 27.971 o 11 -4 6 29.994 34.437 13.062 85.712 o 11 -3 0 1619.720 1688.560 95.197 1.467 o 11 -3 1 42.165 66.500 17.813 45.895 o 11 -3 2 25.770 34.437 14.250 72.701 o 11 -3 3 3.180 24.936 13.062 87.189 o 11 -3 4 470.706 485.994 40.401 8.344 o 11 -3 5 0.876 3.562 8.312 221.337 o 11 -2 0 69.451 60.905 13.657 75.462 o 11 -2 1 68.403 74.139 16.032 55.307 o 11 -2 2 68.647 58.191 14.251 70.122 o 11 -2 3 572.886 524.136 39.221 8.663 o 12 -7 0 1185.020 1112.340 72.570 2.572 o 12 -6 0 751.700 659.800 51.120 5.237 o 12 -6 1 221.514 226.880 28.509 17.292 o 12 -5 0 55.170 47.502 15.438 61.338 o ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn Cd1 Cd 1.42670(2) 1.22894(2) -0.106633(9) 0.03085(9) Uani 1.000000 . Cd2 Cd 0.51650(3) -0.06982(3) 0.415147(10) 0.03614(10) Uani 1.000000 . O1 O 1.5218(3) 1.1154(3) -0.19303(11) 0.0402(5) Uani 1.000000 . O1W O 1.6432(3) 1.3667(3) -0.02540(11) 0.0438(6) Uani 1.000000 . H1Wa H 1.7388(3) 1.3989(3) -0.02535(11) 0.0526(7) Uiso 1.000000 R H1Wb H 1.6326(3) 1.3991(3) 0.01273(11) 0.0526(7) Uiso 1.000000 R O2 O 1.4422(4) 1.0115(3) -0.10720(12) 0.0526(7) Uani 1.000000 . O2W O 1.1736(3) 1.0903(3) -0.17430(11) 0.0451(6) Uani 1.000000 . H2Wa H 1.1900(3) 1.1252(3) -0.20995(11) 0.0541(7) Uiso 1.000000 R H2Wb H 1.1458(3) 1.0045(3) -0.19857(11) 0.0541(7) Uiso 1.000000 R O3 O 1.4047(3) 0.5012(3) -0.09031(11) 0.0411(5) Uani 1.000000 . O3W O 0.4040(3) -0.2232(3) 0.30875(13) 0.0592(7) Uani 1.000000 . H3Wa H 0.3330(3) -0.3166(3) 0.29674(13) 0.0710(9) Uiso 1.000000 R H3Wb H 0.4295(3) -0.1859(3) 0.27410(13) 0.0710(9) Uiso 1.000000 R O4 O 1.4927(3) 0.4083(3) -0.16746(12) 0.0425(6) Uani 1.000000 . O5 O 0.2288(3) -0.1163(4) 0.38643(14) 0.0592(7) Uani 1.000000 . O6 O 0.3341(3) -0.1272(3) 0.48066(12) 0.0417(6) Uani 1.000000 . O7 O 0.5861(3) -0.2187(3) 0.46968(13) 0.0526(7) Uani 1.000000 . O8 O 0.7341(3) -0.0977(3) 0.39984(11) 0.0407(5) Uani 1.000000 . O9 O 1.1484(3) 0.7356(3) 0.01742(13) 0.0508(6) Uani 1.000000 . O10 O 0.8847(3) 0.1923(3) 0.22990(14) 0.0572(7) Uani 1.000000 . N1 N 1.2890(3) 1.1635(3) -0.02081(12) 0.0332(6) Uani 1.000000 . N2 N 0.6129(3) 0.1465(3) 0.37287(13) 0.0365(6) Uani 1.000000 . N3 N 1.0304(4) 0.7614(3) 0.10253(14) 0.0441(7) Uani 1.000000 . H3 H 1.0076(4) 0.8200(3) 0.12702(14) 0.0529(8) Uiso 1.000000 R N4 N 0.9505(3) 0.4345(3) 0.22749(14) 0.0400(7) Uani 1.000000 . H4 H 0.9447(3) 0.5133(3) 0.24359(14) 0.0480(8) Uiso 1.000000 R C1 C 1.2465(4) 1.2541(4) 0.01335(15) 0.0362(7) Uani 1.000000 . H1 H 1.2750(4) 1.3493(4) 0.00233(15) 0.0434(8) Uiso 1.000000 R C2 C 1.1621(4) 1.2110(4) 0.06410(16) 0.0397(8) Uani 1.000000 . H2 H 1.1349(4) 1.2766(4) 0.08707(16) 0.0476(9) Uiso 1.000000 R C3 C 1.1182(4) 1.0699(4) 0.08069(15) 0.0375(7) Uani 1.000000 . H3a H 1.0618(4) 1.0393(4) 0.11508(15) 0.0450(9) Uiso 1.000000 R C4 C 1.1596(3) 0.9743(4) 0.04529(14) 0.0319(7) Uani 1.000000 . C5 C 1.2460(4) 1.0274(4) -0.00422(15) 0.0351(7) Uani 1.000000 . H5 H 1.2761(4) 0.9646(4) -0.02742(15) 0.0421(9) Uiso 1.000000 R C6 C 1.1137(4) 0.8147(4) 0.05469(15) 0.0350(7) Uani 1.000000 . C7 C 0.9772(4) 0.6065(4) 0.11425(17) 0.0436(8) Uani 1.000000 . H7a H 0.8915(4) 0.5764(4) 0.13894(17) 0.0524(10) Uiso 1.000000 R H7b H 0.9401(4) 0.5360(4) 0.07223(17) 0.0524(10) Uiso 1.000000 R C8 C 1.1044(4) 0.5949(5) 0.15219(18) 0.0464(9) Uani 1.000000 . H8a H 1.1810(4) 0.6059(5) 0.12408(18) 0.0557(11) Uiso 1.000000 R H8b H 1.1547(4) 0.6784(5) 0.18999(18) 0.0557(11) Uiso 1.000000 R C9 C 1.0438(5) 0.4439(5) 0.17577(18) 0.0492(9) Uani 1.000000 . H9a H 1.1301(5) 0.4334(5) 0.19246(18) 0.0590(11) Uiso 1.000000 R H9b H 0.9819(5) 0.3601(5) 0.13891(18) 0.0590(11) Uiso 1.000000 R C10 C 0.8747(4) 0.3051(4) 0.24984(15) 0.0366(7) Uani 1.000000 . C11 C 0.5834(4) 0.2574(4) 0.39381(16) 0.0410(8) Uani 1.000000 . H11 H 0.5189(4) 0.2435(4) 0.42553(16) 0.0492(9) Uiso 1.000000 R C12 C 0.7418(4) 0.4136(4) 0.32260(17) 0.0426(8) Uani 1.000000 . H12 H 0.7841(4) 0.5035(4) 0.30552(17) 0.0511(10) Uiso 1.000000 R C13 C 0.6461(4) 0.3921(4) 0.36965(17) 0.0453(8) Uani 1.000000 . H13 H 0.6240(4) 0.4681(4) 0.38496(17) 0.0544(10) Uiso 1.000000 R C14 C 0.7063(4) 0.1667(4) 0.32787(15) 0.0364(7) Uani 1.000000 . H14 H 0.7270(4) 0.0891(4) 0.31381(15) 0.0437(9) Uiso 1.000000 R C15 C 0.7740(4) 0.2991(3) 0.30116(14) 0.0322(7) Uani 1.000000 . C16 C 1.4980(4) 1.0138(3) -0.15938(15) 0.0319(7) Uani 1.000000 . C17 C 1.5386(3) 0.8930(3) -0.18075(14) 0.0280(6) Uani 1.000000 . C18 C 1.6343(4) 0.9119(3) -0.22859(14) 0.0307(6) Uani 1.000000 . H18 H 1.6722(4) 0.9996(3) -0.24724(14) 0.0369(8) Uiso 1.000000 R C19 C 1.6742(4) 0.8025(4) -0.24888(15) 0.0337(7) Uani 1.000000 . C20 C 1.6141(4) 0.6716(4) -0.22083(14) 0.0318(7) Uani 1.000000 . H20 H 1.6368(4) 0.5954(4) -0.23507(14) 0.0381(8) Uiso 1.000000 R C21 C 1.5211(4) 0.6515(3) -0.17197(14) 0.0291(6) Uani 1.000000 . C22 C 1.4840(3) 0.7634(3) -0.15173(14) 0.0283(6) Uani 1.000000 . H22 H 1.4228(3) 0.7518(3) -0.11882(14) 0.0340(7) Uiso 1.000000 R C23 C 1.4676(4) 0.5118(3) -0.14049(14) 0.0305(7) Uani 1.000000 . C24 C 1.7794(5) 0.8256(5) -0.2999(2) 0.0526(10) Uani 1.000000 . H24a H 1.7945(5) 0.7393(5) -0.3080(2) 0.0789(15) Uiso 1.000000 R H24b H 1.7336(5) 0.8348(5) -0.3402(2) 0.0789(15) Uiso 1.000000 R H24c H 1.8773(5) 0.9174(5) -0.2841(2) 0.0789(15) Uiso 1.000000 R C25 C -0.1801(3) -0.2222(4) 0.46794(14) 0.0312(6) Uani 1.000000 . C26 C -0.2130(4) -0.3157(4) 0.51443(15) 0.0342(7) Uani 1.000000 . H26 H -0.3071(4) -0.3522(4) 0.52991(15) 0.0410(8) Uiso 1.000000 R C27 C -0.1084(4) -0.3569(4) 0.53868(15) 0.0344(7) Uani 1.000000 . C28 C -0.0397(3) -0.1660(4) 0.44450(14) 0.0306(6) Uani 1.000000 . H28 H -0.0179(3) -0.1041(4) 0.41277(14) 0.0367(8) Uiso 1.000000 R C29 C 0.2189(4) -0.1435(4) 0.44317(16) 0.0366(7) Uani 1.000000 . C30 C 0.0680(3) -0.2027(4) 0.46873(15) 0.0315(7) Uani 1.000000 . C31 C 0.0328(4) -0.2972(4) 0.51566(15) 0.0342(7) Uani 1.000000 . H31 H 0.1054(4) -0.3209(4) 0.53200(15) 0.0411(8) Uiso 1.000000 R C32 C 0.7056(4) -0.1777(4) 0.44421(15) 0.0367(7) Uani 1.000000 . C33 C -0.1485(5) -0.4626(5) 0.58739(18) 0.0481(9) Uani 1.000000 . H33a H -0.2501(5) -0.4914(5) 0.59723(18) 0.0722(13) Uiso 1.000000 R H33b H -0.1464(5) -0.5528(5) 0.56898(18) 0.0722(13) Uiso 1.000000 R H33c H -0.0749(5) -0.4114(5) 0.62720(18) 0.0722(13) Uiso 1.000000 R O4W O 0.7333(4) 0.7538(4) 0.27953(13) 0.0643(8) Uani 1.000000 . O5W O 1.0029(4) 0.7410(3) 0.27532(15) 0.0662(8) Uani 1.000000 . H5Wa H 0.9162(4) 0.7310(3) 0.28187(15) 0.0794(10) Uiso 1.000000 R H5Wb H 1.0647(4) 0.7849(3) 0.31159(15) 0.0794(10) Uiso 1.000000 R H4Wa H 0.6378(13) 0.694(5) 0.265(2) 0.0964(12) Uiso 1.000000 G H4Wb H 0.735(5) 0.796(6) 0.3181(11) 0.0964(12) Uiso 1.000000 G loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cd1 0.04326(15) 0.02553(14) 0.03193(13) 0.02070(11) 0.01501(9) 0.01259(9) Cd2 0.03812(15) 0.04332(16) 0.03879(14) 0.02426(12) 0.01845(10) 0.02356(10) O1 0.0548(14) 0.0293(12) 0.0509(13) 0.0280(11) 0.0206(11) 0.0182(10) O1W 0.0454(14) 0.0463(14) 0.0414(12) 0.0259(12) 0.0080(10) 0.0009(10) O2 0.091(2) 0.0503(15) 0.0480(14) 0.0528(16) 0.0363(13) 0.0219(12) O2W 0.0534(15) 0.0404(13) 0.0390(12) 0.0217(12) 0.0108(10) 0.0064(10) O3 0.0563(15) 0.0337(12) 0.0408(12) 0.0245(11) 0.0188(10) 0.0173(10) O3W 0.0624(17) 0.0583(17) 0.0475(14) 0.0224(14) 0.0047(12) 0.0172(13) O4 0.0711(16) 0.0283(12) 0.0434(12) 0.0327(12) 0.0200(11) 0.0173(10) O5 0.0469(15) 0.087(2) 0.0589(16) 0.0370(15) 0.0283(12) 0.0388(15) O6 0.0294(12) 0.0478(14) 0.0519(13) 0.0206(11) 0.0134(10) 0.0136(11) O7 0.0447(14) 0.0769(19) 0.0654(16) 0.0444(14) 0.0298(12) 0.0376(14) O8 0.0420(13) 0.0516(14) 0.0417(12) 0.0306(12) 0.0136(10) 0.0181(10) O9 0.0695(18) 0.0468(15) 0.0592(15) 0.0396(14) 0.0339(13) 0.0283(12) O10 0.0781(19) 0.0375(14) 0.0672(17) 0.0326(14) 0.0379(15) 0.0172(12) N1 0.0402(15) 0.0294(14) 0.0319(13) 0.0173(12) 0.0115(11) 0.0105(10) N2 0.0401(15) 0.0396(16) 0.0353(13) 0.0208(13) 0.0119(11) 0.0190(11) N3 0.0517(17) 0.0434(17) 0.0401(15) 0.0212(14) 0.0214(12) 0.0220(13) N4 0.0558(18) 0.0375(16) 0.0417(15) 0.0292(14) 0.0267(13) 0.0216(12) C1 0.0401(18) 0.0323(17) 0.0359(16) 0.0175(14) 0.0076(13) 0.0075(13) C2 0.0431(19) 0.0409(19) 0.0375(17) 0.0239(16) 0.0093(14) 0.0020(14) C3 0.0370(17) 0.047(2) 0.0280(14) 0.0200(15) 0.0105(12) 0.0086(13) C4 0.0308(15) 0.0344(17) 0.0298(14) 0.0146(13) 0.0067(11) 0.0110(12) C5 0.0414(18) 0.0361(18) 0.0338(16) 0.0219(15) 0.0137(13) 0.0121(13) C6 0.0334(16) 0.0406(19) 0.0346(15) 0.0187(14) 0.0090(12) 0.0173(13) C7 0.0421(19) 0.042(2) 0.0432(18) 0.0148(16) 0.0121(14) 0.0226(15) C8 0.0400(19) 0.053(2) 0.0466(19) 0.0185(17) 0.0201(15) 0.0265(17) C9 0.060(2) 0.060(2) 0.049(2) 0.039(2) 0.0306(17) 0.0281(18) C10 0.0413(18) 0.0366(18) 0.0342(16) 0.0192(15) 0.0119(13) 0.0125(13) C11 0.0458(19) 0.047(2) 0.0345(16) 0.0239(17) 0.0140(14) 0.0158(14) C12 0.053(2) 0.0312(18) 0.0441(18) 0.0187(16) 0.0182(15) 0.0131(14) C13 0.057(2) 0.0380(19) 0.0473(19) 0.0265(18) 0.0198(16) 0.0104(15) C14 0.0398(17) 0.0368(18) 0.0353(16) 0.0187(15) 0.0109(13) 0.0154(13) C15 0.0355(16) 0.0288(16) 0.0298(14) 0.0133(13) 0.0077(12) 0.0086(12) C16 0.0365(17) 0.0241(15) 0.0373(16) 0.0164(13) 0.0086(12) 0.0071(12) C17 0.0348(16) 0.0235(15) 0.0291(14) 0.0169(13) 0.0064(11) 0.0060(11) C18 0.0408(17) 0.0249(15) 0.0332(15) 0.0194(14) 0.0111(12) 0.0121(12) C19 0.0409(17) 0.0336(17) 0.0324(15) 0.0215(14) 0.0108(12) 0.0105(12) C20 0.0430(17) 0.0296(16) 0.0326(15) 0.0250(14) 0.0097(12) 0.0069(12) C21 0.0369(16) 0.0236(15) 0.0287(14) 0.0167(13) 0.0029(11) 0.0061(11) C22 0.0338(16) 0.0253(15) 0.0282(14) 0.0157(13) 0.0072(11) 0.0077(11) C23 0.0372(17) 0.0244(15) 0.0318(15) 0.0171(13) 0.0010(12) 0.0075(12) C24 0.072(3) 0.052(2) 0.057(2) 0.043(2) 0.036(2) 0.0244(18) C25 0.0310(15) 0.0329(17) 0.0321(15) 0.0183(14) 0.0078(11) 0.0027(12) C26 0.0320(16) 0.0397(18) 0.0339(15) 0.0193(14) 0.0122(12) 0.0073(13) C27 0.0385(17) 0.0341(17) 0.0320(15) 0.0187(14) 0.0094(12) 0.0067(12) C28 0.0317(16) 0.0313(16) 0.0312(14) 0.0167(13) 0.0080(11) 0.0081(12) C29 0.0315(16) 0.0342(17) 0.0485(18) 0.0178(14) 0.0140(13) 0.0124(14) C30 0.0279(15) 0.0314(16) 0.0357(15) 0.0148(13) 0.0099(12) 0.0057(12) C31 0.0326(16) 0.0357(17) 0.0375(16) 0.0196(14) 0.0061(12) 0.0066(13) C32 0.0355(17) 0.0423(19) 0.0350(16) 0.0219(15) 0.0091(13) 0.0041(13) C33 0.055(2) 0.053(2) 0.049(2) 0.0320(19) 0.0211(17) 0.0232(17) O4W 0.076(2) 0.082(2) 0.0397(14) 0.0447(18) 0.0087(13) 0.0051(13) O5W 0.076(2) 0.0478(16) 0.0725(19) 0.0292(15) 0.0233(15) 0.0081(14) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source C 0.01788 0.00908 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.21560 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' Cd 0.13958 4.66053 19.22140 17.64440 4.46100 1.60290 0.59460 6.90890 24.70080 87.48250 5.06940 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.00304 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' N 0.03110 0.01806 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750 0.58260 -11.52900 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' O 0.04960 0.03233 3.04850 2.28680 1.54630 0.86700 13.27710 5.70110 0.32390 32.90890 0.25080 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Brennan, Cowan, Rev. Sci. Instrum., 1992, 63, 850' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u 0 0 -1 0 0 0 0 -2 48.75 1.89 0 0 -2 48.02 1.89 0 0 2 51.2 1.89 0 0 -2 50.38 1.89 0 0 2 46.3 1.9 0 0 -3 64.69 2.53 0 0 -3 65.29 2.53 0 0 -3 63.35 2.53 0 0 3 71.5 2.53 0 0 3 63.71 2.55 0 0 -4 39.53 1.62 0 0 -4 41.99 1.63 0 0 4 43.68 1.63 0 0 4 44.26 1.65 0 0 -4 40.53 1.62 0 0 5 0.39 0.07 0 0 -5 0.3 0.04 0 0 -5 0.37 0.05 0 0 5 0.42 0.07 0 0 -5 0.48 0.05 0 0 5 0.33 0.05 0 0 6 71.39 2.67 0 0 -6 65.97 2.61 0 0 6 65.07 2.63 0 0 -7 70 2.72 0 0 7 69.04 2.75 0 0 -8 3.66 0.2 0 0 8 3.37 0.24 0 0 8 3.01 0.21 0 0 9 17.48 0.8 0 0 -9 16.25 0.72 0 0 10 124.69 4.8 0 0 10 117.72 4.8 0 0 11 0.6 0.11 0 0 11 0.12 0.07 0 0 12 17.21 0.83 0 0 12 17 0.85 0 0 -12 16.73 0.78 0 0 -12 16.63 0.77 0 0 13 7.18 0.45 0 0 13 7.9 0.48 0 0 -13 7.4 0.42 0 0 -13 7.68 0.41 0 0 14 37.33 1.67 0 0 14 35.71 1.63 0 0 -14 37.49 1.58 0 0 -14 38.02 1.57 0 0 15 17.2 0.91 0 0 15 16.3 0.87 0 0 -15 18.32 0.83 0 0 -15 17.86 0.82 0 0 16 14.14 0.81 0 0 16 13.96 0.79 0 0 -16 16.41 0.75 0 0 -16 15.51 0.73 0 0 17 22.22 1.17 0 0 17 21.02 1.13 0 0 -17 26.61 1.1 0 0 -17 24.57 1.08 0 0 -18 0.44 0.1 0 0 -18 0.54 0.1 0 0 -19 23.64 1.06 0 0 -19 22.79 1.04 0 0 -20 0.12 0.06 0 0 -20 0.05 0.04 0 0 -21 0.02 0.04 0 0 -21 0.08 0.05 0 0 -22 0.04 0.04 0 0 -22 0.04 0.04 0 0 -23 11.69 0.55 0 0 -24 0.8 0.09 0 1 -24 3.68 0.22 0 1 -23 4.96 0.29 0 1 -22 3.7 0.25 0 1 -21 2.47 0.21 0 1 -20 10.45 0.55 0 1 -19 6.33 0.39 0 1 -18 0.04 0.05 0 -1 17 45.15 2.16 0 -1 17 48.25 2.2 0 1 -16 6.63 0.39 0 1 -16 7 0.4 0 -1 16 6.7 0.45 0 -1 16 5.82 0.42 0 1 -15 2.09 0.19 0 1 -15 2.43 0.2 0 -1 15 2.21 0.23 0 -1 15 2.06 0.22 0 1 -14 4.35 0.29 0 1 -14 4.49 0.29 0 -1 14 4.33 0.32 0 -1 14 4.02 0.32 0 1 -13 71.94 2.82 0 1 -13 69.26 2.82 0 -1 13 68.74 2.87 0 1 -12 35.08 1.47 0 -1 12 35 1.52 0 -1 11 107.61 4.27 0 -1 10 3.41 0.25 0 -1 9 10.1 0.49 0 -1 9 10.44 0.52 0 1 -8 16.77 0.72 0 -1 8 16.37 0.75 0 1 -7 57.73 2.31 0 1 -7 59.88 2.32 0 1 -6 9.29 0.41 0 1 -6 8.49 0.41 0 1 -5 9.68 0.41 0 1 -5 8.7 0.38 0 1 -5 9.45 0.42 0 -1 4 9.62 0.37 0 1 -4 10.19 0.43 0 1 -4 9.07 0.38 0 1 -3 250.86 0.86 0 1 -3 233.89 1.1 0 1 -2 2.32 0.06 0 1 -2 1.97 0.06 0 1 -1 144.04 5.4 0 1 -1 132.53 5.41 0 -1 1 142.31 5.39 0 -1 0 133.99 0.48 0 1 0 133.65 0.54 0 1 1 1.59 0.08 0 -1 -1 1.37 0.07 0 1 2 127.27 4.91 0 1 2 128.61 4.91 0 1 3 271.8 10.99 0 1 3 302.34 11 0 1 3 291.19 11.01 0 1 4 6.41 0.31 0 -1 -4 6.77 0.31 0 1 4 6.9 0.33 0 1 4 6.5 0.33 0 1 5 92.3 3.78 0 1 5 96.69 3.81 0 -1 -5 105.2 3.78 0 1 5 93.48 3.79 0 1 6 253.31 10.36 0 1 6 252.67 10.38 0 1 7 0.16 0.06 0 1 7 0.13 0.06 0 1 7 0.44 0.08 0 1 7 0.18 0.07 0 -1 -7 0.51 0.06 0 1 8 5.73 0.34 0 1 8 6.16 0.39 0 -1 -8 6.57 0.33 0 1 8 6.11 0.37 0 1 9 12.56 0.65 0 1 9 12.26 0.64 0 -1 -9 12.89 0.58 0 1 9 12.66 0.66 0 1 10 50.84 2.17 0 -1 -10 51.07 2.1 0 1 10 53.46 2.22 0 1 10 54.5 2.2 0 1 11 20.96 1 0 1 11 19.92 0.96 0 -1 -11 19.64 0.87 0 1 11 20.07 0.95 0 -1 -11 19.49 0.89 0 1 12 127.24 5 0 1 12 121.53 4.97 0 1 12 122.62 5.02 0 -1 -12 122.93 4.88 0 -1 -12 127.28 4.91 0 -1 -12 126.78 4.9 0 1 13 0.39 0.11 0 1 13 0.43 0.11 0 1 13 0.04 0.07 0 -1 -13 0.15 0.06 0 -1 -13 0.22 0.07 0 1 14 4.76 0.37 0 1 14 4.38 0.38 0 -1 -14 4.86 0.32 0 -1 -14 4.97 0.32 0 -1 -15 0.12 0.06 0 1 15 0.09 0.08 0 1 15 0.03 0.07 0 -1 -15 0.05 0.05 0 -1 -15 0.19 0.07 0 -1 -16 15.96 0.76 0 1 16 13.69 0.84 0 -1 -16 15.77 0.76 0 -1 -16 16.2 0.76 0 1 17 0.56 0.14 0 -1 -17 0.59 0.11 0 -1 -17 0.61 0.11 0 -1 -18 4.4 0.31 0 -1 -18 4.44 0.31 0 -1 -19 1.97 0.19 0 -1 -19 2.26 0.2 0 -1 -20 8.94 0.48 0 -1 -20 8.41 0.47 0 -1 -21 2.62 0.21 0 -1 -21 2.75 0.21 0 -1 -22 8.37 0.43 0 -1 -22 8.57 0.43 0 -1 -23 0.58 0.08 0 -1 -23 0.47 0.07 0 2 -24 12.99 0.59 0 2 -23 0.34 0.07 0 2 -22 5.35 0.32 0 2 -21 0.25 0.06 0 2 -21 0.22 0.07 0 2 -20 21.22 0.97 0 2 -20 20.96 0.96 0 2 -19 0.13 0.06 0 2 -19 0.18 0.06 0 2 -18 18.06 0.88 0 2 -18 19.47 0.89 0 2 -17 0.62 0.1 0 2 -17 0.6 0.1 0 2 -17 0.49 0.1 0 -2 17 0.43 0.11 0 -2 17 0.42 0.11 0 2 -16 6.73 0.4 0 2 -16 6.74 0.4 0 2 -16 6.7 0.42 0 -2 16 6.19 0.44 0 2 -15 1.27 0.15 0 2 -15 1.36 0.15 0 -2 15 1.38 0.18 0 2 -14 97.4 3.65 0 2 -14 89.59 3.66 0 -2 14 87.3 3.7 0 2 -13 16.71 0.77 0 2 -13 16.69 0.76 0 -2 13 15.93 0.81 0 2 -12 48.67 2.02 0 2 -12 50.69 2.02 0 2 -12 49.91 2.02 0 -2 12 47.78 2.06 0 -2 11 68.68 2.86 0 2 -11 72.63 2.83 0 -2 10 15.22 0.72 0 2 -9 1.21 0.11 0 2 -9 1.29 0.13 0 -2 9 1.18 0.13 0 2 -8 54.25 2.25 0 2 -8 57.88 2.28 0 -2 8 58.42 2.27 0 2 -7 6.11 0.32 0 2 -7 6.81 0.35 0 2 -6 0.97 0.1 0 2 -5 99.79 3.85 0 2 -4 22.44 0.88 0 -2 4 20.91 0.88 0 2 -4 22.4 0.89 0 2 -4 23.02 0.94 0 2 -3 173.75 6.65 0 2 -3 173.42 6.65 0 2 -3 173.84 6.7 0 2 -2 74.44 2.72 0 2 -2 73.2 2.72 0 -2 2 68.59 2.69 0 2 -2 69.02 2.76 0 2 -1 120.06 4.48 0 2 -1 125.87 4.49 0 2 -1 113.42 4.46 0 -2 1 116.09 4.47 0 2 -1 108.18 4.51 0 2 0 121.85 4.51 0 2 0 127.66 4.52 0 2 0 118.77 4.52 0 -2 0 115.58 4.51 0 2 1 24.29 0.91 0 2 1 23.26 0.91 0 -2 -1 22.62 0.9 0 2 2 84.19 3.08 0 2 2 82.68 3.07 0 -2 -3 104.26 4.19 0 2 3 112.87 4.2 0 2 4 251.21 9.81 0 2 4 259.9 9.82 0 2 5 340.93 13.33 0 2 5 338.72 13.31 0 2 5 361.43 13.32 0 -2 -6 7.8 0.38 0 2 6 7.22 0.41 0 2 6 7.21 0.41 0 2 7 0.55 0.11 0 -2 -7 0.72 0.09 0 2 7 0.39 0.1 0 2 8 16.75 0.89 0 2 8 18.17 0.92 0 2 9 69.48 3.03 0 2 9 64.41 2.99 0 -2 -10 1.04 0.12 0 2 10 1.13 0.18 0 2 10 0.89 0.15 0 -2 -10 0.98 0.11 0 -2 -11 9.68 0.52 0 -2 -11 10.26 0.52 0 2 11 10.61 0.56 0 -2 -11 10.18 0.51 0 2 11 9.7 0.6 0 2 11 9.91 0.62 0 -2 -12 25.51 1.16 0 -2 -12 27.03 1.17 0 2 12 27.31 1.21 0 2 12 26.02 1.27 0 2 12 26.48 1.3 0 -2 -12 26.13 1.15 0 -2 -13 9.33 0.51 0 -2 -13 9.63 0.51 0 2 13 9.96 0.54 0 2 13 9.25 0.59 0 -2 -13 9.28 0.5 0 2 13 8.74 0.61 0 -2 -14 2.27 0.2 0 2 14 2.02 0.27 0 -2 -14 2.07 0.2 0 -2 -14 2.2 0.2 0 -2 -15 9.48 0.51 0 2 15 8.29 0.6 0 -2 -15 9.58 0.52 0 -2 -15 9.62 0.52 0 2 16 5.78 0.48 0 -2 -16 6.67 0.41 0 -2 -16 7.14 0.42 0 -2 -16 7.08 0.42 0 -2 -17 0.02 0.05 0 -2 -17 0.05 0.05 0 -2 -18 10.61 0.57 0 -2 -18 11.39 0.58 0 -2 -19 4.73 0.31 0 -2 -19 4.72 0.31 0 -2 -20 0.06 0.05 0 -2 -20 0.03 0.04 0 -2 -21 0.16 0.05 0 -2 -21 0.11 0.05 0 -2 -22 10.44 0.5 0 -2 -23 2.23 0.15 0 3 -24 3.81 0.22 0 3 -23 5.48 0.3 0 3 -23 4.88 0.29 0 3 -22 2.11 0.18 0 3 -22 2.34 0.19 0 3 -21 1.9 0.18 0 3 -21 1.73 0.17 0 3 -20 0.87 0.12 0 3 -20 0.96 0.13 0 3 -19 8 0.46 0 3 -19 8.36 0.47 0 3 -18 9.06 0.51 0 3 -18 9.66 0.53 0 3 -17 10.4 0.56 0 3 -17 10.9 0.56 0 3 -17 10.47 0.59 0 -3 17 9.6 0.61 0 3 -16 2.57 0.22 0 3 -16 2.7 0.23 0 3 -16 2.71 0.25 0 -3 16 2.52 0.25 0 3 -15 22.97 1.08 0 3 -15 23.97 1.07 0 3 -15 26.39 1.14 0 -3 15 22.77 1.13 0 3 -14 45.6 1.86 0 3 -14 45.91 1.89 0 -3 14 43.17 1.92 0 3 -14 44.14 1.88 0 3 -13 5.65 0.35 0 3 -13 5.6 0.33 0 -3 13 5.69 0.38 0 3 -13 5.64 0.35 0 3 -12 70.84 2.86 0 3 -12 70.05 2.84 0 3 -12 73.96 2.88 0 -3 12 69.53 2.89 0 3 -11 24.19 1.08 0 3 -11 25.92 1.11 0 -3 11 24.6 1.11 0 -3 10 8.48 0.43 0 3 -10 7.2 0.41 0 3 -9 0.99 0.12 0 3 -9 0.75 0.1 0 3 -8 176.64 6.49 0 3 -8 162.76 6.44 0 -3 8 162.3 6.41 0 3 -7 0.75 0.11 0 -3 7 0.77 0.08 0 3 -6 30.34 1.25 0 3 -6 27.97 1.16 0 -3 6 28.25 1.16 0 3 -5 8.72 0.45 0 -3 5 8.14 0.38 0 3 -5 8.07 0.38 0 3 -5 8.17 0.37 0 3 -4 255.43 9.83 0 3 -4 248.78 9.75 0 3 -4 258.89 9.74 0 3 -3 7.19 0.42 0 3 -3 8.05 0.36 0 3 -3 8.16 0.36 0 3 -2 77.33 3.35 0 3 -2 86.62 3.3 0 3 -2 87.33 3.29 0 3 -1 5.71 0.33 0 3 -1 6.55 0.29 0 -3 0 41.82 1.63 0 3 0 40.94 1.63 0 3 1 0.26 0.05 0 3 1 0.25 0.04 0 -3 -2 53.63 2.2 0 3 2 59.54 2.21 0 3 2 56.71 2.21 0 3 2 53.34 2.18 0 -3 -3 17.68 0.79 0 3 3 18.78 0.81 0 3 3 18.51 0.79 0 -3 -4 65.62 2.65 0 3 4 68.34 2.67 0 3 4 67.06 2.68 0 3 5 18.92 0.85 0 -3 -5 18.93 0.83 0 3 5 19.01 0.86 0 -3 -6 87.4 3.37 0 3 6 82.44 3.4 0 -3 -7 15.62 0.72 0 -3 -8 128.97 5.05 0 -3 -9 25.95 1.09 0 3 9 26.32 1.14 0 -3 -10 2.17 0.19 0 -3 -10 2.09 0.18 0 3 10 2.42 0.23 0 -3 -11 46.96 2.01 0 -3 -11 48.99 2.01 0 3 11 49.01 2.06 0 -3 -12 9.23 0.51 0 -3 -12 8.99 0.5 0 3 12 9.67 0.55 0 -3 -13 0.05 0.06 0 -3 -13 0.05 0.05 0 3 13 0.03 0.07 0 -3 -14 1.7 0.18 0 -3 -14 1.92 0.19 0 3 14 1.46 0.18 0 3 15 17.11 0.86 0 -3 -15 17.51 0.85 0 3 16 0.01 0.06 0 -3 -16 0.09 0.06 0 -3 -17 14.4 0.72 0 -3 -18 0.18 0.07 0 -3 -19 1.44 0.15 0 -3 -20 0.5 0.09 0 -3 -21 2.63 0.18 0 -3 -22 0.36 0.06 0 4 -24 3.7 0.22 0 4 -23 0.32 0.06 0 4 -22 9.18 0.46 0 4 -22 8.59 0.45 0 4 -21 29.32 1.27 0 4 -21 30.23 1.29 0 4 -20 4.07 0.29 0 4 -20 3.97 0.27 0 4 -19 31.11 1.35 0 4 -19 29.83 1.32 0 4 -18 1.01 0.13 0 4 -18 0.93 0.14 0 4 -17 3.13 0.26 0 4 -16 1.51 0.17 0 -4 16 1.46 0.2 0 4 -16 1.7 0.21 0 4 -15 43.22 1.81 0 4 -15 37.63 1.8 0 -4 15 41.93 1.87 0 4 -14 2.61 0.23 0 4 -14 2.66 0.24 0 -4 14 3.01 0.27 0 4 -14 2.47 0.23 0 4 -14 3.32 0.29 0 -4 13 11.86 0.64 0 4 -13 11.33 0.61 0 4 -13 12.69 0.67 0 4 -13 10.44 0.59 0 4 -13 10.91 0.59 0 -4 12 3.65 0.29 0 4 -12 3.96 0.29 0 4 -12 3.43 0.27 0 4 -12 3.62 0.27 0 4 -12 3.33 0.26 0 -4 11 67.24 2.54 0 4 -11 63.61 2.55 0 4 -11 70.19 2.61 0 4 -11 56.06 2.5 0 4 -11 59.34 2.5 0 4 -11 57.64 2.49 0 4 -10 0.09 0.06 0 4 -10 0.19 0.07 0 4 -10 0.09 0.05 0 4 -9 131.31 5.33 0 -4 9 139.58 5.31 0 4 -8 22.94 1.05 0 -4 8 21.5 0.95 0 4 -7 37.7 1.53 0 4 -7 33.15 1.39 0 -4 7 33.65 1.4 0 4 -6 191.56 7.12 0 -4 6 179.8 6.98 0 4 -6 181.51 6.98 0 4 -6 177.5 6.97 0 4 -5 160.45 6.24 0 4 -5 159.06 6.1 0 4 -5 155.81 6.11 0 4 -4 6.54 0.33 0 4 -4 5.49 0.39 0 4 -4 6.23 0.31 0 4 -4 6.6 0.33 0 4 -3 0.56 0.07 0 4 -3 0.55 0.11 0 4 -3 0.49 0.06 0 4 -3 0.55 0.07 0 4 -2 110.16 4.2 0 4 -2 107.09 4.2 0 4 -2 106.36 4.18 0 4 -1 47.3 1.89 0 4 -1 46.32 1.86 0 4 -1 47.4 1.89 0 4 0 21.44 0.89 0 4 0 19.81 0.86 0 4 1 95.95 3.67 0 4 1 95.26 3.66 0 4 1 89.31 3.62 0 4 2 43.21 1.7 0 4 2 42.48 1.71 0 4 2 39.34 1.66 0 4 2 40.88 1.7 0 -4 -3 0.25 0.06 0 4 3 0.28 0.07 0 4 3 0.24 0.07 0 4 3 0.2 0.05 0 -4 -4 40.9 1.68 0 4 4 42.63 1.71 0 4 4 41.46 1.71 0 4 4 38.4 1.67 0 4 5 91.73 3.73 0 4 5 92.45 3.73 0 -4 -5 95.29 3.7 0 4 6 2.76 0.26 0 4 6 2.27 0.21 0 -4 -6 2.44 0.2 0 4 6 2.34 0.22 0 4 6 2.02 0.21 0 4 7 0.38 0.11 0 4 7 0.47 0.11 0 -4 -7 0.54 0.09 0 4 7 0.35 0.11 0 4 8 119.3 4.53 0 4 8 104.36 4.55 0 -4 -8 113.56 4.47 0 4 9 0.03 0.07 0 4 9 0.1 0.09 0 -4 -9 0.05 0.05 0 4 10 40.53 1.74 0 -4 -10 41.63 1.69 0 4 11 3.36 0.29 0 4 11 2.73 0.32 0 -4 -11 3.39 0.26 0 -4 -11 3.01 0.25 0 4 12 6.57 0.43 0 4 12 5.22 0.46 0 -4 -12 5.98 0.39 0 -4 -12 6.07 0.39 0 4 13 0.82 0.15 0 -4 -13 0.76 0.12 0 4 13 0.72 0.18 0 -4 -13 0.68 0.12 0 -4 -13 0.82 0.14 0 -4 -14 17.34 0.85 0 4 14 17.2 0.87 0 -4 -15 1.43 0.17 0 4 15 1.42 0.18 0 -4 -16 1.92 0.19 0 4 16 1.66 0.18 0 -4 -17 3.91 0.28 0 4 17 3.88 0.32 0 4 17 4.23 0.29 0 -4 -18 5.45 0.32 0 4 18 4.39 0.34 0 4 18 4.99 0.31 0 -4 -19 1.36 0.13 0 -4 -20 6.1 0.33 0 5 -23 0.36 0.07 0 5 -22 37.07 1.53 0 5 -21 0.58 0.1 0 5 -20 8.42 0.47 0 5 -19 14.43 0.72 0 5 -18 35.37 1.54 0 5 -17 3.44 0.29 0 5 -17 3.78 0.29 0 5 -16 42.21 1.85 0 5 -16 43.09 1.84 0 5 -15 13.75 0.73 0 5 -15 13.45 0.74 0 -5 15 13.79 0.78 0 5 -15 14.91 0.73 0 -5 14 0.94 0.17 0 5 -14 1 0.16 0 5 -14 0.9 0.14 0 5 -14 1.41 0.16 0 5 -13 12.04 0.65 0 -5 13 11.27 0.64 0 5 -13 10.08 0.6 0 5 -13 10.95 0.61 0 5 -13 11.01 0.59 0 5 -12 58.37 2.35 0 5 -12 50.27 2.29 0 5 -12 52.52 2.28 0 5 -12 51.68 2.26 0 5 -11 0.82 0.15 0 5 -11 0.71 0.11 0 5 -11 0.71 0.13 0 5 -11 0.83 0.13 0 5 -10 28.55 1.25 0 5 -10 23.16 1.13 0 5 -10 27.87 1.16 0 -5 10 26.79 1.15 0 5 -10 23.65 1.17 0 5 -10 25.76 1.16 0 -5 9 110.27 4.23 0 5 -9 105.11 4.28 0 5 -9 110.77 4.23 0 5 -9 115.97 4.37 0 5 -9 100.56 4.23 0 5 -9 102.54 4.24 0 -5 8 9.49 0.47 0 5 -8 8.7 0.52 0 5 -8 9.3 0.47 0 5 -8 9.75 0.57 0 5 -8 8.17 0.47 0 5 -8 8.29 0.48 0 5 -7 29.78 1.25 0 5 -7 30.28 1.37 0 -5 7 30.32 1.24 0 5 -7 28.42 1.22 0 5 -7 27.09 1.25 0 -5 6 52.07 2.13 0 5 -6 52.61 2.12 0 5 -6 53.89 2.15 0 5 -6 54.25 2.16 0 5 -6 50.92 2.15 0 5 -6 50.68 2.17 0 5 -6 56.83 2.19 0 5 -6 52.76 2.28 0 5 -5 63.02 2.51 0 5 -5 63.54 2.53 0 5 -5 60.32 2.55 0 5 -5 66.07 2.56 0 5 -4 2.76 0.2 0 5 -4 2.6 0.19 0 5 -4 2.37 0.17 0 5 -3 41.35 1.64 0 5 -3 38.19 1.62 0 5 -3 39.03 1.6 0 5 -2 0.1 0.04 0 5 -2 0.07 0.04 0 5 -2 0.03 0.04 0 5 -1 0.64 0.09 0 5 -1 0.43 0.08 0 5 0 5.15 0.31 0 5 0 5.09 0.29 0 5 0 5.35 0.32 0 5 1 123.77 5.06 0 5 1 136.1 5.11 0 5 1 137.21 5.15 0 5 1 127.3 5.13 0 5 1 127.17 5.1 0 5 1 130.16 5.14 0 5 1 132.02 5.11 0 5 2 0.48 0.1 0 5 2 0.52 0.11 0 5 2 0.53 0.08 0 5 2 0.46 0.1 0 5 2 0.49 0.13 0 5 2 0.39 0.1 0 5 2 0.66 0.1 0 5 2 0.48 0.09 0 5 3 19.41 0.92 0 5 3 19.17 0.94 0 5 3 18.87 0.91 0 5 3 21.23 1.01 0 5 3 18.46 0.93 0 5 3 19.24 0.93 0 5 3 19.18 0.9 0 5 3 18.09 0.89 0 5 4 0.9 0.14 0 5 4 0.81 0.13 0 5 4 0.68 0.12 0 5 4 0.96 0.17 0 5 4 0.96 0.14 0 5 5 34.26 1.57 0 5 5 33.32 1.5 0 5 5 32.97 1.53 0 5 5 34.95 1.54 0 5 5 34.87 1.54 0 5 6 7.65 0.53 0 5 6 7.97 0.48 0 5 6 8.04 0.51 0 5 6 8.44 0.52 0 -5 -6 8.17 0.46 0 5 7 23.54 1.25 0 5 7 25.01 1.16 0 5 7 23.9 1.19 0 5 7 25.37 1.22 0 -5 -7 26.06 1.14 0 5 8 1.42 0.24 0 5 8 1.78 0.2 0 5 8 1.53 0.22 0 5 8 1.49 0.22 0 -5 -8 1.86 0.19 0 5 9 0.33 0.14 0 5 9 0.6 0.13 0 5 9 0.47 0.14 0 -5 -9 0.67 0.12 0 5 9 0.59 0.16 0 5 10 0.17 0.13 0 5 10 0.34 0.11 0 5 10 0.44 0.14 0 -5 -10 0.24 0.09 0 5 10 0.35 0.14 0 5 11 11.96 0.86 0 -5 -11 15.55 0.75 0 5 11 12.44 0.84 0 5 11 13.94 0.83 0 5 11 15.87 0.78 0 5 12 0.18 0.11 0 5 12 0.27 0.1 0 5 13 7.16 0.52 0 5 13 7.73 0.48 0 5 14 14.98 0.86 0 5 14 16.4 0.81 0 5 15 2.66 0.27 0 5 15 2.66 0.23 0 5 16 10.25 0.61 0 5 16 11.07 0.57 0 5 17 2.49 0.24 0 5 17 3.27 0.23 0 5 18 2.01 0.16 0 5 19 1.25 0.11 0 6 -22 7.41 0.38 0 6 -21 0.07 0.04 0 6 -20 8.54 0.46 0 6 -19 8.09 0.46 0 6 -18 1.68 0.18 0 6 -18 1.52 0.18 0 6 -17 4.81 0.33 0 6 -17 4.58 0.34 0 6 -16 65.5 2.65 0 6 -16 61.93 2.66 0 6 -15 0.59 0.13 0 6 -15 0.57 0.12 0 6 -14 10.71 0.62 0 6 -14 10.76 0.6 0 -6 13 0.56 0.13 0 6 -13 0.53 0.13 0 6 -13 0.57 0.13 0 6 -13 0.63 0.13 0 6 -13 0.57 0.11 0 -6 12 37.72 1.54 0 6 -12 35.36 1.59 0 6 -12 30.73 1.51 0 6 -12 31.49 1.48 0 6 -12 31.95 1.46 0 6 -11 2.34 0.27 0 6 -11 1.62 0.18 0 6 -11 1.84 0.22 0 6 -11 2.03 0.21 0 -6 10 100.95 3.77 0 6 -10 87.35 3.83 0 6 -10 95.34 3.76 0 6 -10 99.22 3.93 0 6 -10 89.17 3.76 0 6 -10 89.91 3.78 0 -6 9 2.02 0.19 0 6 -9 2 0.24 0 6 -9 2.01 0.2 0 6 -9 1.93 0.26 0 6 -9 2.03 0.2 0 6 -9 1.91 0.2 0 6 -8 0.12 0.09 0 -6 8 0.09 0.05 0 6 -8 0.14 0.07 0 6 -8 0.04 0.06 0 -6 7 0.34 0.07 0 6 -7 0.33 0.11 0 6 -7 0.38 0.09 0 6 -7 0.29 0.08 0 -6 6 81.9 3.22 0 6 -6 80.76 3.23 0 6 -6 77.62 3.26 0 6 -6 81.98 3.28 0 6 -6 80.69 3.24 0 6 -5 3.36 0.24 0 -6 5 3.51 0.24 0 6 -5 3.3 0.25 0 6 -5 3.38 0.27 0 6 -5 3.43 0.27 0 6 -5 3.25 0.27 0 6 -4 31.07 1.37 0 6 -4 31.5 1.39 0 6 -4 33.47 1.39 0 6 -4 31.48 1.41 0 6 -4 32.5 1.43 0 6 -4 32.95 1.42 0 6 -4 31.79 1.42 0 6 -3 19.48 0.92 0 6 -3 21.57 0.98 0 6 -3 19.34 0.94 0 6 -3 19.81 0.93 0 6 -3 19.29 0.97 0 6 -3 20.65 0.97 0 6 -3 21.5 0.94 0 6 -3 20.9 0.96 0 6 -2 5.26 0.33 0 6 -2 5.44 0.37 0 6 -2 4.54 0.33 0 6 -2 5.03 0.33 0 6 -2 5.34 0.37 0 6 -2 5.26 0.36 0 6 -2 5.2 0.33 0 6 -2 4.97 0.34 0 6 -1 13.32 0.7 0 6 -1 12.46 0.65 0 6 -1 11.89 0.66 0 6 -1 12.44 0.64 0 6 -1 12.85 0.69 0 6 -1 13.78 0.7 0 6 -1 12.88 0.67 0 6 -1 13.38 0.65 0 6 0 42.71 1.87 0 6 0 46.94 1.95 0 6 0 41.84 1.89 0 6 0 41.93 1.86 0 6 0 48.65 1.95 0 6 0 46.16 1.94 0 6 0 45.01 1.87 0 6 0 43.96 1.9 0 6 1 11.39 0.64 0 6 1 9.49 0.56 0 6 1 9.96 0.59 0 6 1 9.91 0.56 0 6 1 10.3 0.61 0 6 1 11.43 0.64 0 6 1 10.13 0.56 0 6 1 10.41 0.58 0 6 2 2.58 0.25 0 6 2 2.96 0.3 0 6 2 2.61 0.26 0 6 2 2.43 0.23 0 6 2 2.51 0.26 0 6 2 3.17 0.3 0 6 2 2.98 0.25 0 6 2 2.38 0.24 0 6 3 32.19 1.52 0 6 3 35.57 1.61 0 6 3 31.65 1.54 0 6 3 31.63 1.49 0 6 3 34.03 1.59 0 6 3 36.51 1.57 0 6 3 34.99 1.52 0 6 3 33.45 1.51 0 6 4 23.96 1.22 0 6 4 26.21 1.24 0 6 4 25.94 1.2 0 6 4 24.25 1.18 0 6 4 25.28 1.25 0 6 5 0.15 0.11 0 6 5 0.14 0.09 0 6 5 0.07 0.07 0 6 5 0.15 0.1 0 6 6 0.52 0.15 0 6 6 0.35 0.12 0 6 6 0.39 0.15 0 6 7 17.24 1.04 0 6 7 18.89 0.93 0 6 7 19.16 1 0 6 7 18.92 1.1 0 6 8 0.99 0.23 0 6 8 0.96 0.24 0 6 8 1.42 0.22 0 6 8 1.22 0.18 0 6 9 2.13 0.34 0 6 9 2.43 0.29 0 6 9 2.95 0.27 0 6 10 2.83 0.39 0 6 10 3.08 0.33 0 6 10 3.43 0.29 0 6 11 5.13 0.52 0 6 11 5.25 0.44 0 6 11 5.84 0.4 0 6 12 0.3 0.15 0 6 12 0.05 0.09 0 6 12 0.09 0.07 0 6 13 17.91 1.02 0 6 13 17.07 0.93 0 6 13 18.14 0.87 0 6 14 0.36 0.13 0 6 14 0.49 0.12 0 6 14 0.36 0.09 0 6 15 0.17 0.09 0 6 15 0.3 0.09 0 6 15 0.25 0.07 0 6 16 0.75 0.12 0 6 16 0.96 0.11 0 6 17 6.57 0.34 0 7 -21 2.84 0.19 0 7 -20 0.14 0.05 0 7 -19 11.03 0.55 0 7 -19 10.59 0.55 0 7 -18 1.4 0.15 0 7 -18 1.26 0.15 0 7 -17 31.78 1.36 0 7 -17 30.15 1.38 0 7 -16 1.29 0.16 0 7 -16 1.41 0.18 0 7 -15 0.05 0.07 0 7 -15 0.05 0.06 0 7 -14 2.16 0.23 0 7 -13 39.12 1.74 0 7 -12 1.39 0.19 0 7 -11 23.98 1.16 0 7 -11 23.67 1.18 0 7 -11 25.98 1.16 0 7 -10 18.97 1.06 0 -7 10 20.47 0.97 0 7 -10 19.13 0.98 0 7 -10 19.45 1 0 7 -10 21.08 0.97 0 7 -9 13.98 0.86 0 -7 9 14.34 0.74 0 7 -9 14.19 0.76 0 7 -9 14.29 0.78 0 7 -9 14.62 0.74 0 7 -8 3.32 0.36 0 -7 8 3.04 0.25 0 7 -8 3 0.27 0 7 -8 3.13 0.29 0 7 -8 3 0.26 0 -7 7 26.65 1.21 0 7 -7 29.82 1.44 0 7 -7 25.04 1.24 0 7 -7 28.22 1.29 0 7 -7 26.47 1.22 0 7 -6 20.63 1.11 0 7 -6 17.8 0.87 0 -7 6 16.88 0.84 0 7 -6 18.68 0.93 0 7 -6 17.61 0.87 0 -7 5 0.04 0.04 0 7 -5 0.06 0.06 0 7 -5 0.18 0.08 0 7 -5 0.09 0.07 0 7 -5 0.1 0.08 0 7 -5 0.05 0.05 0 7 -4 27.42 1.29 0 7 -4 27.66 1.3 0 7 -4 29.79 1.36 0 7 -4 31.65 1.37 0 7 -4 29.77 1.38 0 7 -3 5.71 0.4 0 7 -3 6.5 0.42 0 7 -3 6.17 0.41 0 7 -3 7.18 0.48 0 7 -3 6.39 0.45 0 7 -3 6.92 0.45 0 7 -2 0.05 0.06 0 7 -2 0.01 0.07 0 7 -2 0.07 0.06 0 7 -2 0.03 0.07 0 7 -2 0.15 0.11 0 7 -2 0.02 0.06 0 7 -2 0.14 0.08 0 7 -1 11.72 0.7 0 7 -1 10.31 0.61 0 7 -1 10.6 0.63 0 7 -1 10.08 0.6 0 7 -1 11.43 0.69 0 7 -1 13.37 0.72 0 7 -1 12.52 0.67 0 7 -1 11.76 0.63 0 7 0 38.7 1.71 0 7 0 33.26 1.59 0 7 0 34.89 1.62 0 7 0 31.59 1.57 0 7 0 40.16 1.71 0 7 0 38.44 1.71 0 7 0 38.64 1.64 0 7 0 36.44 1.6 0 7 1 16.97 0.92 0 7 1 13.27 0.79 0 7 1 15.03 0.83 0 7 1 13.88 0.78 0 7 1 18.36 0.91 0 7 1 16.86 0.92 0 7 1 15.56 0.83 0 7 1 15.48 0.8 0 7 2 23.23 1.21 0 7 2 20.95 1.09 0 7 2 21.35 1.12 0 7 2 19.08 1.05 0 7 2 22.53 1.2 0 7 2 26.08 1.19 0 7 2 22.63 1.09 0 7 2 23.35 1.11 0 7 3 2 0.25 0 7 3 2.09 0.3 0 7 3 2.24 0.27 0 7 3 1.81 0.23 0 7 3 2.29 0.28 0 7 3 2.01 0.23 0 7 3 2.21 0.25 0 7 4 7.45 0.57 0 7 4 9.07 0.63 0 7 4 7.39 0.54 0 7 4 9.08 0.57 0 7 4 8.79 0.57 0 7 5 2.11 0.3 0 7 5 1.93 0.25 0 7 5 2.73 0.3 0 7 6 40.49 2.05 0 7 6 41.58 1.95 0 7 7 1.24 0.2 0 7 7 0.7 0.21 0 7 8 1.82 0.25 0 7 8 1.43 0.28 0 7 9 0.95 0.23 0 7 9 1.32 0.21 0 7 9 1.61 0.18 0 7 10 4.91 0.48 0 7 10 4.97 0.41 0 7 10 4.94 0.35 0 7 11 1.76 0.27 0 7 11 1.72 0.22 0 7 11 2 0.2 0 7 12 2.56 0.3 0 7 12 2.59 0.26 0 7 12 3.11 0.24 0 7 13 0.08 0.09 0 7 13 0.13 0.07 0 7 13 0.12 0.06 0 7 14 1.87 0.21 0 7 14 2.24 0.2 0 7 14 2.53 0.18 0 7 15 0.59 0.09 0 8 -19 1 0.11 0 8 -18 3.4 0.24 0 8 -17 13.14 0.66 0 8 -16 4.49 0.32 0 8 -15 4.74 0.35 0 8 -14 17.25 0.88 0 8 -13 8.73 0.54 0 8 -12 2.52 0.26 0 8 -12 2.62 0.25 0 8 -11 69.08 2.94 0 8 -11 70.31 2.92 0 8 -10 5.12 0.37 0 8 -10 5.88 0.43 0 8 -10 5 0.39 0 8 -9 1.48 0.18 0 8 -9 1.79 0.23 0 8 -9 1.37 0.19 0 8 -8 0.49 0.11 0 8 -8 0.52 0.14 0 8 -8 0.39 0.12 0 8 -7 23.37 1.14 0 8 -7 26.62 1.25 0 8 -7 23.91 1.19 0 8 -6 0.05 0.07 0 8 -6 0.09 0.09 0 8 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0.53 1 2 -12 10.98 0.55 -1 -2 12 10.85 0.58 1 2 -12 11.42 0.56 1 2 -11 25.66 1.08 -1 -2 11 23.23 1.09 1 2 -10 28.74 1.21 -1 -2 10 27.2 1.21 1 2 -9 7.75 0.41 -1 -2 9 7.51 0.4 1 2 -8 16.33 0.75 1 2 -7 276.9 9.97 -1 -2 7 247.43 9.92 1 2 -6 6.59 0.34 1 2 -6 6.06 0.29 -1 -2 6 5.65 0.29 -1 -2 5 36.99 1.48 -1 -2 5 36.45 1.49 1 2 -5 39.34 1.49 1 2 -4 42.1 1.6 1 2 -4 38.68 1.53 -1 -2 4 37.97 1.53 1 2 -3 18.97 0.79 1 2 -3 17.56 0.74 1 2 -3 17.99 0.74 1 2 -2 4.52 0.23 1 2 -2 5.01 0.27 1 2 -2 4.83 0.23 1 2 -2 5.03 0.23 -1 -2 1 49.17 1.95 1 2 -1 52.68 2.01 1 2 -1 49.79 1.97 1 2 -1 49.68 1.98 1 2 -1 52.27 1.97 -1 -2 0 30.89 1.22 1 2 0 29.34 1.24 1 2 0 31.63 1.23 1 2 1 9.74 0.43 -1 -2 -1 9.61 0.43 1 2 1 10.38 0.44 1 2 1 9.84 0.43 -1 -2 -2 0.53 0.06 1 2 2 0.41 0.06 1 2 2 0.38 0.05 -1 -2 -3 82.38 3.29 1 2 3 85.46 3.29 1 2 3 85.04 3.29 -1 -2 -4 1.18 0.11 1 2 4 1.23 0.12 1 2 4 1.36 0.11 -1 -2 -5 47.6 1.99 1 2 5 52.29 2.04 -1 -2 -6 35.57 1.46 1 2 6 34.95 1.52 -1 -2 -7 5.57 0.32 1 2 7 5.18 0.36 1 2 8 8.01 0.49 -1 -2 -8 8.81 0.45 1 2 8 8.02 0.5 -1 -2 -9 51.28 2.21 1 2 9 55.64 2.24 1 2 9 49.82 2.29 1 2 9 52.76 2.3 -1 -2 -10 4.08 0.29 -1 -2 -10 4.7 0.3 1 2 10 4.49 0.31 -1 -2 -10 4.76 0.3 1 2 10 4.46 0.36 1 2 10 4.54 0.36 -1 -2 -11 0.17 0.07 -1 -2 -11 0.33 0.08 1 2 11 0.23 0.08 1 2 11 0.14 0.09 -1 -2 -11 0.25 0.07 1 2 11 0.16 0.1 -1 -2 -12 29.31 1.38 -1 -2 -12 31.23 1.39 1 2 12 31.64 1.39 -1 -2 -12 33.21 1.38 1 2 12 31 1.5 -1 -2 -12 33.65 1.39 -1 -2 -13 2.36 0.22 -1 -2 -13 2.63 0.23 1 2 13 2.91 0.24 -1 -2 -13 2.67 0.22 1 2 13 2.29 0.28 -1 -2 -13 2.82 0.23 -1 -2 -14 0.11 0.06 1 2 14 0.07 0.08 -1 -2 -14 0.19 0.07 -1 -2 -14 0.07 0.06 -1 -2 -14 0.08 0.06 -1 -2 -15 7.61 0.45 -1 -2 -15 7.37 0.45 -1 -2 -15 7.31 0.45 -1 -2 -16 12.88 0.67 -1 -2 -16 12.36 0.66 -1 -2 -17 0.68 0.12 -1 -2 -17 0.75 0.12 -1 -2 -18 16.35 0.79 -1 -2 -18 16.49 0.79 -1 -2 -19 3.73 0.27 -1 -2 -19 3.91 0.27 -1 -2 -20 0.16 0.06 -1 -2 -20 0.18 0.06 -1 -2 -21 0.19 0.05 -1 -2 -21 0.2 0.06 -1 -2 -22 4.92 0.27 1 3 -24 4.73 0.26 1 3 -23 5.16 0.3 1 3 -22 1.58 0.15 1 3 -22 1.52 0.15 1 3 -21 9.73 0.51 1 3 -21 9.99 0.52 1 3 -20 5.71 0.37 1 3 -20 6.17 0.37 1 3 -19 0.25 0.08 1 3 -19 0.3 0.08 1 3 -18 9.55 0.51 1 3 -18 8.6 0.51 -1 -3 17 1.17 0.18 1 3 -17 1.08 0.16 1 3 -17 1.34 0.15 1 3 -17 1.28 0.16 -1 -3 16 5.15 0.39 1 3 -16 5.26 0.36 1 3 -16 5.33 0.34 1 3 -15 36.69 1.66 -1 -3 15 39.61 1.73 1 3 -15 39.45 1.68 1 3 -15 40.14 1.66 -1 -3 14 34.97 1.55 1 3 -14 34.68 1.5 1 3 -14 34.42 1.5 1 3 -14 34.5 1.48 -1 -3 13 0.69 0.13 1 3 -13 0.72 0.1 1 3 -13 0.66 0.11 -1 -3 12 31.78 1.38 1 3 -12 31.93 1.38 1 3 -12 31.42 1.35 1 3 -12 30.16 1.33 1 3 -11 0.23 0.07 -1 -3 11 0.32 0.08 1 3 -11 0.31 0.07 1 3 -11 0.39 0.07 1 3 -10 25.8 1.15 -1 -3 10 24.89 1.11 1 3 -9 0.11 0.06 -1 -3 8 180.08 7.28 1 3 -8 205.07 7.38 -1 -3 7 0.44 0.06 1 3 -7 0.43 0.06 1 3 -7 0.49 0.1 1 3 -6 48.2 1.94 -1 -3 6 47.42 1.94 1 3 -6 48.68 1.95 1 3 -5 37.47 1.55 -1 -3 5 37.39 1.54 1 3 -5 39.08 1.55 1 3 -4 103.06 4.15 1 3 -4 107.13 4.15 1 3 -4 107.14 4.16 1 3 -4 116.33 4.26 1 3 -3 11.82 0.51 1 3 -3 11.55 0.51 1 3 -3 10.85 0.51 1 3 -3 12.04 0.59 1 3 -2 15.99 0.69 1 3 -2 16.53 0.69 1 3 -2 16.07 0.69 1 3 -2 15.61 0.76 1 3 -1 18.41 0.79 1 3 -1 19.55 0.79 1 3 -1 17.45 0.84 1 3 -1 18.65 0.79 1 3 0 11.58 0.51 1 3 0 11.16 0.52 1 3 1 1.13 0.11 1 3 1 1.22 0.11 -1 -3 -1 1.35 0.11 1 3 1 1.27 0.11 1 3 2 61.34 2.45 1 3 2 63.26 2.47 -1 -3 -2 59.9 2.46 1 3 2 64.25 2.48 1 3 3 15.49 0.69 1 3 3 15.41 0.7 1 3 3 15.9 0.71 -1 -3 -3 15.77 0.7 -1 -3 -4 28.99 1.23 1 3 4 29.2 1.23 -1 -3 -5 157.57 6.18 1 3 5 160.3 6.2 -1 -3 -6 11.63 0.57 1 3 6 10.88 0.58 1 3 7 16.25 0.82 -1 -3 -7 18.21 0.8 1 3 7 16.24 0.8 -1 -3 -8 2.08 0.18 1 3 8 1.48 0.19 -1 -3 -8 1.98 0.18 1 3 8 1.86 0.19 -1 -3 -9 18.45 0.81 1 3 9 16.34 0.86 1 3 9 17.54 0.83 -1 -3 -10 0.6 0.11 -1 -3 -10 0.48 0.1 1 3 10 0.49 0.11 -1 -3 -11 27.8 1.31 -1 -3 -11 30.11 1.32 -1 -3 -11 30.14 1.3 1 3 11 30.18 1.34 -1 -3 -12 1.24 0.17 -1 -3 -12 1.4 0.16 1 3 12 1 0.19 -1 -3 -12 1.35 0.16 1 3 12 1.39 0.17 -1 -3 -13 7.83 0.47 -1 -3 -13 7.69 0.46 1 3 13 6.35 0.51 -1 -3 -13 7.58 0.45 1 3 13 7.73 0.47 1 3 14 0.36 0.1 -1 -3 -14 0.35 0.09 1 3 15 27.29 1.23 -1 -3 -15 26.85 1.23 1 3 16 1.33 0.16 -1 -3 -16 1.26 0.16 -1 -3 -17 3.3 0.26 -1 -3 -18 0.06 0.05 -1 -3 -19 4.27 0.28 -1 -3 -20 0.57 0.09 -1 -3 -21 11.34 0.52 1 4 -23 0.18 0.05 1 4 -23 0.25 0.05 1 4 -22 1.16 0.12 1 4 -22 1.11 0.12 1 4 -21 17.54 0.81 1 4 -21 18.05 0.83 1 4 -20 0.04 0.05 1 4 -20 0.02 0.05 1 4 -19 29.16 1.28 1 4 -19 27.88 1.25 1 4 -18 6.14 0.4 1 4 -18 5.75 0.37 1 4 -17 33.2 1.48 1 4 -17 33.89 1.46 1 4 -16 6.97 0.46 1 4 -16 5.52 0.4 -1 -4 16 6.26 0.45 1 4 -16 6.99 0.43 1 4 -16 6.4 0.4 1 4 -15 31.26 1.47 -1 -4 15 31.21 1.51 1 4 -15 33.16 1.47 1 4 -15 33.75 1.44 1 4 -14 10.38 0.58 -1 -4 14 10.14 0.6 1 4 -14 10.18 0.56 1 4 -14 9.5 0.53 -1 -4 13 1.02 0.16 1 4 -13 0.78 0.13 1 4 -13 0.87 0.13 1 4 -13 0.53 0.1 -1 -4 12 11.21 0.6 1 4 -12 10 0.57 1 4 -12 10.66 0.57 1 4 -12 10.36 0.56 1 4 -11 36.44 1.57 -1 -4 11 37.28 1.53 1 4 -11 34.64 1.5 1 4 -11 32.06 1.5 1 4 -10 2.44 0.21 1 4 -10 2.77 0.26 1 4 -9 73.37 2.82 1 4 -9 64.98 2.69 -1 -4 9 65.1 2.68 1 4 -8 37.91 1.66 -1 -4 8 38.73 1.65 1 4 -8 41.38 1.65 1 4 -7 3.48 0.3 1 4 -7 3.16 0.21 -1 -4 7 2.77 0.2 -1 -4 6 34.74 1.46 1 4 -6 34.93 1.46 1 4 -6 35.32 1.47 -1 -4 5 62.98 2.61 1 4 -5 64.71 2.61 1 4 -5 67.68 2.62 1 4 -4 16.91 0.83 1 4 -4 15.51 0.69 1 4 -4 14.93 0.68 1 4 -4 14.76 0.68 1 4 -3 63.82 2.55 1 4 -3 64.92 2.54 1 4 -3 63.46 2.55 1 4 -2 106.69 4.14 1 4 -2 105.36 4.13 1 4 -2 105.21 4.14 1 4 -1 18.42 0.81 1 4 -1 17.79 0.82 1 4 -1 19.17 0.81 1 4 0 5.44 0.31 1 4 0 5.51 0.3 1 4 0 5.08 0.31 1 4 1 0.18 0.06 1 4 1 0.15 0.05 1 4 2 77.92 3.11 1 4 2 78.94 3.14 1 4 3 0.05 0.05 1 4 3 0.05 0.06 1 4 3 0.15 0.06 1 4 4 75.43 3.01 1 4 4 73.61 3.09 1 4 4 76.46 3.03 -1 -4 -4 76.04 3.01 1 4 4 73.68 3.01 1 4 4 74.73 3.04 1 4 5 7.19 0.42 1 4 5 6.49 0.47 1 4 5 7.51 0.43 1 4 5 7.6 0.45 1 4 5 7.62 0.44 -1 -4 -5 7.52 0.42 1 4 6 2.83 0.24 1 4 6 2.9 0.24 1 4 6 3.07 0.26 -1 -4 -6 2.96 0.24 1 4 6 2.64 0.25 1 4 7 0.51 0.11 -1 -4 -7 0.91 0.13 1 4 7 0.81 0.15 1 4 7 0.72 0.14 1 4 7 0.76 0.13 -1 -4 -8 58.27 2.32 1 4 8 51.88 2.36 1 4 8 56.19 2.33 1 4 8 54.25 2.36 1 4 9 3.07 0.31 -1 -4 -9 3.22 0.26 1 4 9 3.47 0.28 1 4 9 3.04 0.29 -1 -4 -9 2.8 0.25 1 4 10 7.64 0.56 -1 -4 -10 9.13 0.51 1 4 10 9.11 0.53 1 4 10 8.35 0.55 -1 -4 -10 7.83 0.49 -1 -4 -11 17.33 0.83 1 4 11 17.75 0.85 1 4 11 16.49 0.9 -1 -4 -11 15.48 0.81 -1 -4 -12 4.63 0.34 1 4 12 4.09 0.4 -1 -4 -12 4.76 0.33 -1 -4 -12 4.79 0.35 1 4 12 5.29 0.41 1 4 12 5.56 0.38 -1 -4 -13 0.15 0.08 1 4 13 0.17 0.09 1 4 13 0.37 0.11 1 4 14 10.12 0.57 -1 -4 -14 9.92 0.56 1 4 15 2.76 0.24 -1 -4 -15 2.34 0.22 1 4 16 0.23 0.08 -1 -4 -16 0.13 0.07 1 4 17 7.04 0.4 -1 -4 -17 6.84 0.4 1 4 18 3.85 0.24 -1 -4 -18 3.51 0.24 -1 -4 -19 0.06 0.04 1 5 -23 0.12 0.04 1 5 -22 16.69 0.75 1 5 -21 1.35 0.14 1 5 -20 5 0.33 1 5 -19 21.17 0.99 1 5 -18 12.43 0.66 1 5 -17 0.07 0.07 1 5 -16 32.99 1.47 1 5 -15 10.91 0.63 1 5 -15 11.59 0.62 1 5 -14 3.49 0.29 1 5 -14 3.61 0.32 -1 -5 14 3.86 0.33 1 5 -14 3.99 0.31 1 5 -13 13.22 0.71 1 5 -13 14.06 0.77 -1 -5 13 14.53 0.76 1 5 -13 13.55 0.72 1 5 -12 2.02 0.2 1 5 -12 2.02 0.22 1 5 -12 2.09 0.21 1 5 -12 1.95 0.24 -1 -5 12 2.39 0.24 1 5 -11 52.71 2.34 1 5 -11 54.14 2.31 1 5 -11 60.6 2.42 1 5 -10 0.18 0.08 -1 -5 10 0.18 0.06 1 5 -10 0.21 0.07 -1 -5 9 87.12 3.52 1 5 -9 83.84 3.54 1 5 -8 1.61 0.15 -1 -5 8 1.53 0.15 1 5 -8 1.72 0.18 1 5 -8 1.9 0.25 -1 -5 7 14.8 0.7 1 5 -7 15.34 0.7 1 5 -7 13.71 0.71 1 5 -7 14.64 0.73 1 5 -7 16.64 0.9 1 5 -6 2.56 0.19 1 5 -6 2.59 0.2 -1 -5 6 2.52 0.19 1 5 -6 2.38 0.21 1 5 -6 2.45 0.21 1 5 -5 51.93 2.07 -1 -5 5 49.98 2.06 1 5 -5 49.56 2.1 1 5 -5 50.2 2.07 1 5 -5 50.76 2.1 1 5 -5 56.46 2.14 1 5 -5 48.07 2.1 1 5 -4 1.36 0.14 1 5 -4 1.56 0.17 1 5 -4 1.55 0.14 1 5 -4 1.54 0.16 1 5 -4 1.46 0.15 1 5 -4 1.57 0.17 1 5 -4 1.59 0.17 1 5 -4 1.57 0.16 1 5 -3 36.2 1.51 1 5 -3 34.85 1.51 1 5 -3 35.47 1.55 1 5 -3 34.87 1.53 1 5 -3 36.1 1.52 1 5 -3 37.97 1.59 1 5 -3 34.93 1.55 1 5 -3 38.79 1.54 1 5 -3 37.25 1.56 1 5 -2 1.12 0.14 1 5 -2 0.96 0.12 1 5 -2 0.92 0.11 1 5 -2 0.86 0.12 1 5 -2 1.11 0.12 1 5 -2 1.01 0.14 1 5 -2 1.1 0.15 1 5 -2 1.06 0.13 1 5 -2 0.96 0.12 1 5 -1 0.1 0.05 1 5 -1 0.14 0.05 1 5 -1 0.21 0.08 1 5 -1 0.19 0.07 1 5 -1 0.16 0.05 1 5 -1 0.15 0.07 1 5 -1 0.17 0.07 1 5 -1 0.19 0.06 1 5 -1 0.34 0.08 1 5 0 7.81 0.47 1 5 0 6.61 0.39 1 5 0 6.75 0.41 1 5 0 7.22 0.43 1 5 0 7.16 0.41 1 5 0 8.12 0.47 1 5 0 7.63 0.43 1 5 0 7.71 0.43 1 5 1 52.38 2.16 1 5 1 51.69 2.2 1 5 1 57.42 2.27 1 5 1 51.39 2.21 1 5 1 49.22 2.17 1 5 1 55.79 2.26 1 5 1 54.06 2.19 1 5 2 0.09 0.07 1 5 2 0.18 0.09 1 5 2 0.04 0.04 1 5 2 0.15 0.08 1 5 2 0.02 0.04 1 5 2 0.04 0.07 1 5 2 0.07 0.06 1 5 3 15.65 0.8 1 5 3 15.31 0.84 1 5 3 14.84 0.74 1 5 3 17.07 0.83 1 5 3 15.4 0.77 1 5 3 14.1 0.8 1 5 4 12.22 0.65 1 5 4 11.92 0.68 1 5 4 11.78 0.63 1 5 5 21 1.08 1 5 5 20.7 1.01 1 5 5 21.56 1 1 5 5 21.91 1.04 1 5 6 0.26 0.09 1 5 6 0.19 0.1 1 5 6 0.17 0.07 1 5 6 0.34 0.11 1 5 6 0.15 0.09 1 5 7 9.67 0.6 1 5 7 9.61 0.67 1 5 7 10.36 0.58 1 5 7 10.49 0.63 1 5 7 9.96 0.62 1 5 8 22.45 1.24 1 5 8 21.48 1.13 1 5 8 25.16 1.12 1 5 8 25.07 1.18 1 5 8 21.31 1.15 1 5 9 4.36 0.45 -1 -5 -9 5.44 0.38 1 5 9 5.19 0.42 1 5 9 5.32 0.38 1 5 10 9.55 0.63 1 5 10 10.28 0.59 1 5 11 3.96 0.36 1 5 11 4.18 0.33 1 5 12 0.4 0.12 1 5 12 0.37 0.1 1 5 13 0.11 0.09 1 5 13 0.13 0.08 1 5 14 9.45 0.53 1 5 15 4.07 0.29 1 5 16 6.02 0.34 1 5 16 4.61 0.38 1 5 17 0.08 0.07 1 5 18 2.29 0.19 1 6 -22 12.1 0.55 1 6 -21 0.11 0.05 1 6 -20 11.4 0.57 1 6 -19 2.62 0.22 1 6 -18 5.53 0.36 1 6 -17 0.02 0.06 1 6 -17 0.11 0.07 1 6 -16 36.78 1.61 1 6 -16 36.89 1.63 1 6 -15 0.64 0.12 1 6 -15 0.59 0.13 1 6 -14 4.53 0.34 1 6 -14 4.86 0.36 1 6 -13 1.78 0.2 1 6 -13 1.71 0.2 1 6 -12 19.55 0.97 1 6 -12 20.52 1.08 -1 -6 12 20.35 1.01 1 6 -12 18.11 1.01 1 6 -12 21.81 1.01 1 6 -11 4.1 0.32 1 6 -11 4.27 0.37 1 6 -11 4.29 0.34 1 6 -11 4.35 0.41 1 6 -10 20.05 0.97 -1 -6 10 19.38 0.93 1 6 -10 18.48 1.01 -1 -6 9 15.31 0.74 1 6 -9 15.19 0.84 1 6 -9 14.87 0.77 1 6 -9 13.48 0.74 1 6 -8 6.84 0.44 -1 -6 8 7.13 0.41 1 6 -8 6.25 0.39 -1 -6 7 7.28 0.42 1 6 -7 6.74 0.41 1 6 -7 8.01 0.48 1 6 -7 7.13 0.45 -1 -6 6 43.83 1.85 1 6 -6 43.66 1.85 1 6 -6 43.65 1.89 1 6 -6 46.52 1.92 -1 -6 5 11.76 0.58 1 6 -5 11.27 0.58 1 6 -5 11.19 0.59 1 6 -5 11.77 0.63 1 6 -5 11.73 0.64 1 6 -5 10.99 0.6 1 6 -4 7.79 0.44 1 6 -4 8.44 0.5 1 6 -4 7.73 0.45 1 6 -4 7.8 0.46 1 6 -4 7.9 0.49 1 6 -4 8.64 0.51 1 6 -4 7.99 0.5 1 6 -3 28.39 1.27 1 6 -3 25.65 1.21 1 6 -3 27.11 1.2 1 6 -3 25.66 1.22 1 6 -3 26.74 1.21 1 6 -3 27.5 1.27 1 6 -3 28.57 1.28 1 6 -3 29.97 1.28 1 6 -2 4.61 0.37 1 6 -2 4.74 0.33 1 6 -2 4.93 0.32 1 6 -2 4.61 0.34 1 6 -2 4.69 0.33 1 6 -2 5.82 0.41 1 6 -2 5.33 0.39 1 6 -2 5.61 0.36 1 6 -2 4.79 0.37 1 6 -2 5.66 0.38 1 6 -1 0.83 0.13 1 6 -1 1.1 0.14 1 6 -1 1.21 0.18 1 6 -1 1.07 0.16 1 6 -1 0.88 0.13 1 6 -1 1.18 0.18 1 6 -1 1.59 0.21 1 6 -1 1.23 0.17 1 6 -1 1.34 0.16 1 6 0 4.18 0.32 1 6 0 4.28 0.3 1 6 0 4.65 0.38 1 6 0 3.87 0.32 1 6 0 3.91 0.3 1 6 0 4.01 0.36 1 6 0 4.29 0.33 1 6 0 4.71 0.33 1 6 1 27.3 1.31 1 6 1 29.59 1.4 1 6 1 27.39 1.33 1 6 1 26.12 1.28 1 6 1 30.51 1.42 1 6 1 29 1.31 1 6 2 0.18 0.09 1 6 2 0.34 0.13 1 6 2 0.14 0.09 1 6 2 0.13 0.07 1 6 2 0.41 0.15 1 6 2 0.14 0.11 1 6 2 0.18 0.08 1 6 3 19.82 1.04 1 6 3 20.71 1.13 1 6 3 18.97 1.06 1 6 3 18.26 0.99 1 6 3 21.28 1.14 1 6 3 21.71 1.03 1 6 4 3.89 0.36 1 6 4 4.16 0.42 1 6 4 4.14 0.39 1 6 4 3.16 0.31 1 6 4 4.92 0.4 1 6 4 4.33 0.35 1 6 5 5.17 0.45 1 6 5 5.67 0.52 1 6 5 5.78 0.43 1 6 5 6.21 0.5 1 6 6 -0.03 0.1 1 6 6 0.03 0.11 1 6 6 0.13 0.1 1 6 6 0.32 0.09 1 6 7 19.13 1.13 1 6 7 20.11 1.04 1 6 7 19.74 0.97 1 6 8 0.36 0.17 1 6 8 0.57 0.15 1 6 8 0.42 0.11 1 6 9 4.99 0.5 1 6 9 4.33 0.39 1 6 9 5.19 0.37 1 6 10 -0.02 0.12 1 6 10 0.06 0.08 1 6 10 0.01 0.06 1 6 11 11.03 0.77 1 6 11 11.57 0.67 1 6 11 11.17 0.61 1 6 12 0.71 0.19 1 6 12 0.49 0.12 1 6 12 0.69 0.12 1 6 13 8.72 0.6 1 6 13 8.28 0.52 1 6 13 9.64 0.5 1 6 14 0.08 0.05 1 6 14 0.15 0.09 1 6 15 0.04 0.06 1 6 16 1.29 0.14 1 7 -20 0.29 0.06 1 7 -19 12.21 0.59 1 7 -18 -0.01 0.06 1 7 -18 0.01 0.05 1 7 -17 13.19 0.68 1 7 -17 13.42 0.67 1 7 -16 10.08 0.57 1 7 -16 10.35 0.56 1 7 -15 0.31 0.1 1 7 -15 0.21 0.08 1 7 -14 4.5 0.35 1 7 -14 4.55 0.34 1 7 -13 15.75 0.84 1 7 -13 16.3 0.83 1 7 -12 6 0.43 1 7 -11 7.42 0.5 1 7 -10 14.8 0.79 1 7 -10 13.97 0.76 1 7 -9 8.84 0.55 1 7 -9 8.36 0.53 1 7 -8 3.35 0.31 1 7 -8 2.91 0.28 -1 -7 7 3.07 0.25 1 7 -7 3.11 0.3 -1 -7 6 38.16 1.68 1 7 -6 39.04 1.75 1 7 -6 42.03 1.8 1 7 -6 36.43 1.68 -1 -7 5 0.77 0.12 1 7 -5 0.82 0.15 1 7 -5 0.92 0.17 1 7 -5 0.78 0.13 -1 -7 4 32.9 1.48 1 7 -4 35.35 1.59 1 7 -4 37.82 1.64 1 7 -4 33.27 1.52 1 7 -3 0.85 0.14 1 7 -3 0.9 0.17 1 7 -3 1.07 0.19 1 7 -3 0.86 0.15 1 7 -2 0.06 0.06 1 7 -2 0.08 0.09 1 7 -2 0.01 0.08 1 7 -2 0.06 0.08 1 7 -2 0.11 0.07 1 7 -1 1.05 0.2 1 7 -1 1 0.16 1 7 -1 1.15 0.21 1 7 -1 1.39 0.2 1 7 -1 1.18 0.17 1 7 -1 0.9 0.16 1 7 0 33.19 1.59 1 7 0 27.73 1.45 1 7 0 34.67 1.61 1 7 0 36.69 1.55 1 7 0 35.62 1.5 1 7 0 29.21 1.48 1 7 1 1 0.22 1 7 1 0.87 0.2 1 7 1 0.87 0.15 1 7 1 0.82 0.16 1 7 2 1.21 0.24 1 7 2 1.42 0.26 1 7 2 1.4 0.24 1 7 2 1.16 0.18 1 7 2 0.87 0.18 1 7 3 2.38 0.34 1 7 3 2.37 0.34 1 7 3 2.75 0.28 1 7 3 2.72 0.31 1 7 4 2.12 0.32 1 7 4 1.6 0.29 1 7 4 2.23 0.25 1 7 4 2.45 0.31 1 7 5 0.35 0.17 1 7 5 0.41 0.13 1 7 5 0.29 0.15 1 7 6 11.87 0.69 1 7 6 10.08 0.73 1 7 7 4.07 0.35 1 7 7 3.72 0.4 1 7 8 0.26 0.1 1 7 8 0.09 0.13 1 7 9 3.14 0.29 1 7 9 2.72 0.34 1 7 10 7.25 0.48 1 7 10 7.61 0.55 1 7 11 0.32 0.09 1 7 11 0.22 0.11 1 7 12 0.9 0.13 1 7 12 0.61 0.14 1 7 13 5 0.35 1 8 -18 0.14 0.05 1 8 -17 14.71 0.7 1 8 -16 0.85 0.12 1 8 -15 3.22 0.26 1 8 -14 3.45 0.29 1 8 -13 9.45 0.56 1 8 -12 0.09 0.07 1 8 -11 28.87 1.36 1 8 -10 0.35 0.11 1 8 -10 0.23 0.09 1 8 -9 3.42 0.32 1 8 -9 2.99 0.29 1 8 -8 0.53 0.14 1 8 -8 0.59 0.13 1 8 -7 48.1 2.08 1 8 -7 43.79 2.01 1 8 -6 0.4 0.13 1 8 -6 0.3 0.11 1 8 -5 5.19 0.44 1 8 -5 4.18 0.33 1 8 -4 9.14 0.63 1 8 -4 7.86 0.5 1 8 -3 8.47 0.53 1 8 -3 9.63 0.63 1 8 -2 0.57 0.13 1 8 -2 0.41 0.15 1 8 -1 17.41 0.93 1 8 -1 19.99 1.08 1 8 0 1.75 0.23 1 8 0 2.08 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1.25 0.18 -2 5 6 1.27 0.17 2 -5 -6 1.37 0.14 -2 5 6 1.26 0.18 -2 5 6 1.16 0.18 -2 5 6 1.45 0.19 -2 5 6 1.21 0.16 -2 5 5 0.58 0.16 -2 5 5 0.39 0.1 2 -5 -5 0.74 0.1 -2 5 5 0.72 0.13 -2 5 5 0.75 0.11 -2 5 5 0.48 0.12 -2 5 5 0.82 0.14 -2 5 4 2.83 0.23 2 -5 -4 2.93 0.22 -2 5 4 3.28 0.26 -2 5 4 2.83 0.22 2 -5 -3 57.74 2.32 -2 5 3 57.36 2.37 -2 5 3 59.77 2.34 -2 5 3 55.55 2.32 -2 5 2 0.12 0.06 -2 5 2 0.04 0.04 -2 5 1 64.01 2.56 -2 5 1 63.09 2.53 -2 5 0 20.23 0.9 -2 5 0 21.43 0.92 -2 5 0 21.03 0.9 -2 5 -1 22.97 1 -2 5 -1 23.25 1.02 -2 5 -1 24.36 1 -2 5 -2 55.69 2.18 -2 5 -2 54.75 2.18 -2 5 -2 52.02 2.27 -2 5 -3 167.05 6.98 -2 5 -3 185.71 6.96 -2 5 -3 179.94 7.07 -2 5 -3 185.13 6.95 -2 5 -4 0.77 0.11 -2 5 -4 0.92 0.1 -2 5 -4 0.63 0.08 -2 5 -4 0.69 0.12 -2 5 -5 8.84 0.51 2 -5 5 9.37 0.43 -2 5 -6 52.37 2.33 2 -5 6 59.53 2.26 -2 5 -6 55.09 2.35 -2 5 -7 7.05 0.45 -2 5 -7 7.31 0.43 -2 5 -7 7.45 0.46 2 -5 7 8.31 0.4 -2 5 -8 1.42 0.17 2 -5 8 1.59 0.14 -2 5 -8 1.46 0.17 -2 5 -8 1.43 0.14 -2 5 -8 1.91 0.2 -2 5 -8 1.54 0.16 -2 5 -8 1.35 0.15 -2 5 -9 0.27 0.09 2 -5 9 0.28 0.07 -2 5 -9 0.34 0.1 -2 5 -9 0.39 0.08 -2 5 -9 0.6 0.12 -2 5 -9 0.46 0.09 -2 5 -9 0.33 0.08 -2 5 -10 25.16 1.13 -2 5 -10 25.93 1.08 -2 5 -10 23.52 1.08 -2 5 -10 22.03 1.07 -2 5 -10 22.45 1.09 -2 5 -10 22.35 1.12 2 -5 11 3.46 0.26 -2 5 -11 3.01 0.26 -2 5 -11 2.77 0.23 -2 5 -11 2.72 0.24 -2 5 -11 2.52 0.23 -2 5 -11 2.85 0.24 -2 5 -11 2.63 0.27 -2 5 -11 2.5 0.24 -2 5 -12 39.7 1.73 2 -5 12 42.99 1.74 -2 5 -12 41.33 1.69 -2 5 -12 40.08 1.72 -2 5 -12 38.7 1.71 -2 5 -12 37.21 1.69 -2 5 -12 43.12 1.8 -2 5 -12 34.7 1.69 2 -5 13 0.15 0.07 -2 5 -13 0.1 0.06 -2 5 -13 0.14 0.06 -2 5 -13 0.06 0.08 -2 5 -13 0.05 0.07 -2 5 -13 0.08 0.05 -2 5 -13 0.07 0.06 -2 5 -14 2.27 0.23 2 -5 14 2.51 0.26 -2 5 -14 2.94 0.24 -2 5 -14 2.79 0.27 -2 5 -14 2.52 0.24 -2 5 -14 3.41 0.31 -2 5 -15 0.09 0.07 -2 5 -15 0.09 0.06 -2 5 -15 0.11 0.08 -2 5 -15 0.07 0.07 -2 5 -15 0.12 0.07 -2 5 -16 50.86 2.23 -2 5 -16 54.01 2.23 -2 5 -16 55.53 2.29 -2 5 -17 1.22 0.16 -2 5 -17 1.14 0.15 -2 5 -17 1.46 0.19 -2 5 -18 15.62 0.77 -2 5 -18 15.52 0.76 -2 5 -19 4.99 0.33 -2 5 -19 5.39 0.34 -2 5 -20 15.65 0.75 -2 5 -21 4.05 0.27 -2 5 -22 21.3 0.93 -2 5 -23 5.84 0.31 2 -4 -21 0.08 0.04 2 -4 -20 8.66 0.44 2 -4 -19 0.53 0.09 -2 4 18 6.42 0.4 2 -4 -18 6.49 0.38 -2 4 17 2.71 0.25 2 -4 -17 2.76 0.23 -2 4 16 20.07 0.99 2 -4 -16 20.61 0.95 -2 4 15 0.6 0.13 2 -4 -15 0.36 0.09 -2 4 14 38.51 1.74 2 -4 -14 38.23 1.66 2 -4 -14 40.34 1.67 -2 4 13 5.59 0.41 2 -4 -13 5.59 0.36 2 -4 -13 5.97 0.37 -2 4 12 1.2 0.18 2 -4 -12 0.92 0.13 -2 4 11 15.29 0.82 -2 4 11 14.72 0.85 2 -4 -11 15.33 0.74 -2 4 11 17.11 0.9 -2 4 10 55.63 2.26 2 -4 -10 51.01 2.15 -2 4 10 49.99 2.27 -2 4 10 54.24 2.31 -2 4 9 0.53 0.13 -2 4 9 0.5 0.13 2 -4 -9 0.83 0.11 -2 4 9 0.55 0.15 -2 4 8 54.23 2.22 -2 4 8 49.76 2.24 -2 4 8 50.96 2.23 2 -4 -8 51.76 2.11 -2 4 7 42.53 1.83 -2 4 7 40.32 1.78 2 -4 -7 42.34 1.73 -2 4 6 14.24 0.75 -2 4 6 14.63 0.71 2 -4 -6 14.87 0.68 -2 4 5 23.61 1.07 2 -4 -5 23.7 1 -2 4 5 22.96 1.02 -2 4 5 22.46 1 2 -4 -4 89.18 3.52 -2 4 4 89.85 3.57 -2 4 4 91.49 3.53 -2 4 4 85.37 3.51 -2 4 4 96.22 3.69 -2 4 3 14.96 0.66 -2 4 3 14.48 0.71 -2 4 3 15.38 0.79 -2 4 3 14.31 0.65 -2 4 2 35.17 1.43 -2 4 2 34.51 1.39 -2 4 2 34.35 1.52 -2 4 2 32.68 1.37 -2 4 1 93 3.58 -2 4 1 93.45 3.61 -2 4 1 87.61 3.7 -2 4 1 90.96 3.57 -2 4 0 45.87 1.79 -2 4 0 45.79 1.76 -2 4 0 41.49 1.82 -2 4 0 42.36 1.88 -2 4 -1 0.99 0.09 -2 4 -1 1.07 0.09 -2 4 -1 1.04 0.1 -2 4 -1 1.04 0.14 -2 4 -1 0.94 0.12 -2 4 -1 1.02 0.09 -2 4 -2 0.32 0.06 -2 4 -2 0.27 0.05 -2 4 -2 0.41 0.06 -2 4 -2 0.43 0.08 -2 4 -2 0.4 0.05 -2 4 -3 223.26 8.37 -2 4 -3 208.8 8.4 -2 4 -3 215.95 8.45 -2 4 -3 219.63 8.36 -2 4 -4 2.64 0.2 -2 4 -4 2.58 0.21 -2 4 -5 279.33 11.18 -2 4 -5 275.25 11.15 -2 4 -5 293.52 11.21 2 -4 5 305.72 11.12 -2 4 -6 7.52 0.44 -2 4 -6 7.82 0.42 -2 4 -6 7.67 0.45 2 -4 6 8.49 0.38 -2 4 -7 9.56 0.52 -2 4 -7 9.26 0.53 2 -4 7 10.65 0.47 -2 4 -7 9.49 0.51 -2 4 -8 13.06 0.64 -2 4 -8 11.31 0.62 -2 4 -8 12.33 0.63 2 -4 8 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2.67 0.18 -2 4 -24 6.68 0.33 2 -3 -23 6.46 0.32 2 -3 -22 1.82 0.14 2 -3 -21 15.79 0.72 2 -3 -20 0.11 0.06 2 -3 -19 0.28 0.08 2 -3 -18 2.96 0.24 2 -3 -17 10.86 0.57 2 -3 -16 0.33 0.09 -2 3 16 0.44 0.12 2 -3 -15 6.77 0.39 -2 3 15 5.95 0.42 -2 3 15 5.49 0.49 2 -3 -14 50.9 2.12 -2 3 14 50.37 2.19 2 -3 -14 49.97 2.1 -2 3 14 45.89 2.31 -2 3 13 13.11 0.67 2 -3 -13 11.37 0.6 -2 3 13 11.23 0.66 2 -3 -13 11.75 0.59 -2 3 13 11.18 0.75 -2 3 12 15.9 0.78 2 -3 -12 14.47 0.71 -2 3 12 14.19 0.77 2 -3 -12 14.96 0.7 -2 3 12 13.97 0.87 -2 3 11 9.96 0.56 2 -3 -11 9.83 0.51 -2 3 11 9.5 0.56 -2 3 11 10.56 0.66 2 -3 -11 9.07 0.49 -2 3 10 20.34 0.96 -2 3 10 20.44 0.98 2 -3 -10 22.15 0.92 2 -3 -10 20.34 0.9 2 -3 -9 0.61 0.09 -2 3 9 0.6 0.14 -2 3 8 84.09 3.67 2 -3 -8 90.33 3.56 -2 3 8 97.06 3.68 -2 3 7 11.19 0.61 2 -3 -7 10.94 0.52 -2 3 7 11.62 0.63 -2 3 6 0.31 0.08 -2 3 6 0.39 0.11 -2 3 5 4.48 0.33 -2 3 4 170.15 6.67 -2 3 3 16.27 0.68 -2 3 3 15.73 0.67 -2 3 2 46.68 1.86 -2 3 2 45.36 1.82 -2 3 2 46.29 1.82 -2 3 2 48.5 1.94 -2 3 1 4.2 0.2 -2 3 1 4.07 0.22 -2 3 1 3.6 0.19 -2 3 1 3.88 0.21 -2 3 1 3.85 0.19 -2 3 1 4.06 0.22 -2 3 1 3.95 0.27 -2 3 0 109.75 4.15 -2 3 0 102.56 4.13 -2 3 0 108.71 4.13 -2 3 0 112.2 4.17 -2 3 0 96.48 4.22 -2 3 0 107.72 4.12 -2 3 0 108.24 4.12 -2 3 -1 13.18 0.57 -2 3 -1 13.88 0.58 -2 3 -1 13.86 0.57 -2 3 -1 14.1 0.58 -2 3 -1 14.38 0.63 -2 3 -1 13.45 0.57 -2 3 -1 14.1 0.57 -2 3 -1 12.38 0.64 -2 3 -2 198.85 7.52 -2 3 -2 194.66 7.53 -2 3 -2 210.24 7.55 -2 3 -2 201.94 7.53 -2 3 -2 199.3 7.59 -2 3 -2 195.33 7.52 -2 3 -3 0.54 0.07 -2 3 -3 0.59 0.09 -2 3 -4 44.22 1.91 -2 3 -4 49.04 1.96 -2 3 -4 51.29 1.94 2 -3 4 51 1.9 -2 3 -5 20.55 0.97 -2 3 -5 21 0.92 -2 3 -5 23.63 0.96 2 -3 5 24.71 0.92 -2 3 -6 14.78 0.69 -2 3 -6 14.82 0.68 -2 3 -6 15.37 0.71 2 -3 6 15.25 0.64 -2 3 -7 6.41 0.36 -2 3 -7 6.54 0.38 -2 3 -7 6.51 0.36 -2 3 -8 29.11 1.24 2 -3 8 30.79 1.22 -2 3 -8 27.85 1.24 -2 3 -8 27.61 1.24 -2 3 -9 39.67 1.58 2 -3 9 36.72 1.55 -2 3 -9 36.69 1.59 -2 3 -9 36.85 1.58 2 -3 10 0.96 0.12 -2 3 -10 0.89 0.12 -2 3 -10 0.89 0.13 -2 3 -10 0.89 0.12 -2 3 -11 110.53 4.3 2 -3 11 101.69 4.3 -2 3 -11 117.95 4.31 -2 3 -11 100.94 4.31 -2 3 -11 107.02 4.3 -2 3 -11 116.64 4.35 -2 3 -12 26.78 1.2 2 -3 12 26.4 1.21 -2 3 -12 28.09 1.21 -2 3 -12 26.22 1.22 -2 3 -12 27.93 1.21 -2 3 -12 29.38 1.26 2 -3 13 4.55 0.32 -2 3 -13 4.75 0.31 -2 3 -13 4.42 0.32 -2 3 -13 4.41 0.31 -2 3 -13 4.89 0.34 -2 3 -14 1.6 0.17 -2 3 -14 1.62 0.18 -2 3 -14 1.49 0.16 -2 3 -14 1.47 0.18 -2 3 -15 54.03 2.33 -2 3 -15 58.62 2.39 -2 3 -15 57.89 2.35 -2 3 -16 0.69 0.11 -2 3 -16 0.71 0.12 -2 3 -16 0.55 0.12 2 -3 16 0.62 0.12 -2 3 -17 6.27 0.38 -2 3 -17 6.3 0.38 -2 3 -17 5.46 0.39 2 -3 17 5.25 0.39 -2 3 -18 0.1 0.05 -2 3 -18 0.13 0.06 -2 3 -19 15.12 0.74 -2 3 -19 15.87 0.76 -2 3 -20 0.98 0.12 -2 3 -20 0.8 0.12 -2 3 -21 10.59 0.54 -2 3 -21 10.2 0.52 -2 3 -22 2.92 0.2 -2 3 -22 2.71 0.2 -2 3 -23 0.06 0.04 -2 3 -23 0.01 0.03 2 -2 -23 0.07 0.04 2 -2 -22 0.8 0.1 2 -2 -21 16.23 0.75 2 -2 -20 3.46 0.25 2 -2 -19 22.54 1.02 2 -2 -18 8.43 0.47 2 -2 -17 10.38 0.56 2 -2 -16 0.19 0.07 -2 2 16 0.19 0.1 -2 2 15 42.26 1.73 2 -2 -15 38.39 1.63 -2 2 14 5.72 0.39 2 -2 -14 5.07 0.32 -2 2 14 4.49 0.41 -2 2 13 2.56 0.3 -2 2 13 2.81 0.29 -2 2 13 2.92 0.27 2 -2 -13 2.99 0.22 -2 2 13 2.8 0.26 -2 2 13 2.78 0.27 -2 2 12 0.34 0.12 2 -2 -12 0.6 0.09 -2 2 12 0.53 0.14 2 -2 -12 0.55 0.09 -2 2 12 0.53 0.12 -2 2 12 0.48 0.12 -2 2 11 77.15 3.23 2 -2 -11 75.55 3.09 -2 2 11 82.63 3.29 -2 2 11 78.13 3.18 -2 2 11 76.95 3.19 -2 2 11 80.48 3.22 2 -2 -11 78.95 3.11 -2 2 10 5.33 0.38 2 -2 -10 4.91 0.29 -2 2 10 5.45 0.4 -2 2 10 5.44 0.37 -2 2 9 103.14 4.54 2 -2 -9 116.68 4.45 -2 2 9 110.54 4.59 -2 2 9 125.59 4.59 -2 2 8 1.08 0.16 -2 2 8 0.95 0.14 -2 2 8 1.15 0.15 -2 2 8 1.3 0.16 -2 2 7 2.85 0.22 -2 2 7 2.56 0.23 -2 2 7 2.9 0.23 -2 2 7 2.92 0.24 -2 2 6 24.56 1.11 -2 2 6 26.12 1.09 -2 2 6 24.96 1.11 -2 2 6 25.22 1.12 -2 2 5 92.36 3.64 -2 2 5 96.16 3.62 -2 2 5 87.17 3.65 -2 2 4 6.74 0.35 -2 2 4 6.9 0.37 -2 2 4 7.37 0.39 -2 2 3 8.96 0.39 -2 2 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0.15 -2 -3 -19 2.77 0.2 -2 -3 -20 0.09 0.04 2 4 -23 1.37 0.12 2 4 -23 1.36 0.12 2 4 -22 0.12 0.05 2 4 -22 0.16 0.05 2 4 -21 27.38 1.19 2 4 -21 27.29 1.18 2 4 -20 0.01 0.05 2 4 -20 0.03 0.04 2 4 -19 13.69 0.71 2 4 -19 14.51 0.71 2 4 -18 1.6 0.18 2 4 -18 1.5 0.17 2 4 -17 40.38 1.74 2 4 -17 39.65 1.71 2 4 -16 2.86 0.25 2 4 -16 2.53 0.23 2 4 -15 41.29 1.67 2 4 -15 41.13 1.7 2 4 -15 34.86 1.68 -2 -4 15 36.17 1.71 2 4 -14 2.13 0.2 2 4 -14 2.36 0.22 -2 -4 14 2.21 0.24 2 4 -13 10.78 0.57 2 4 -13 10.59 0.59 2 4 -13 10.74 0.63 -2 -4 13 10.48 0.61 2 4 -12 20.95 0.97 2 4 -12 22.82 1.08 -2 -4 12 20.73 1.02 2 4 -12 21.19 1 2 4 -11 22.8 1.08 2 4 -11 27.24 1.23 -2 -4 11 25.62 1.15 2 4 -11 24.94 1.13 2 4 -10 0.35 0.07 2 4 -10 0.28 0.08 2 4 -10 0.26 0.09 -2 -4 9 7.81 0.44 2 4 -9 8.37 0.45 2 4 -9 7.43 0.45 -2 -4 8 39.73 1.71 2 4 -8 42.61 1.72 2 4 -8 38.84 1.74 -2 -4 7 0.82 0.1 2 4 -7 0.84 0.1 2 4 -7 0.6 0.1 2 4 -7 0.94 0.17 -2 -4 6 27.65 1.21 2 4 -6 29.21 1.22 2 4 -6 27.57 1.24 2 4 -5 22.25 1.02 2 4 -5 25.28 1.02 2 4 -5 22.12 1.03 -2 -4 5 22.48 0.99 2 4 -4 8.29 0.41 -2 -4 4 7.72 0.39 2 4 -4 7.62 0.42 2 4 -4 7 0.41 2 4 -3 12.81 0.6 2 4 -3 13.12 0.59 2 4 -3 11.08 0.6 2 4 -2 134.83 4.95 2 4 -2 122.04 4.93 2 4 -2 127.83 4.93 2 4 -2 119.57 4.96 2 4 -1 0.76 0.1 2 4 -1 0.65 0.1 2 4 -1 0.52 0.09 2 4 0 7.27 0.41 2 4 0 7.55 0.4 2 4 0 8.1 0.46 2 4 0 7.11 0.41 2 4 1 16.35 0.81 2 4 1 17.19 0.8 2 4 1 17.4 0.81 2 4 1 16.97 0.84 2 4 2 98.96 4.04 2 4 2 102.86 4.02 2 4 2 104.83 4.03 2 4 2 96.77 4.09 2 4 3 1.03 0.15 2 4 3 0.92 0.17 2 4 3 1.09 0.13 2 4 3 1.05 0.13 2 4 3 1.18 0.15 2 4 4 53.06 2.19 2 4 4 53.12 2.23 2 4 4 52.15 2.16 2 4 4 53.72 2.2 2 4 4 48.96 2.27 2 4 5 0.19 0.07 2 4 5 0.19 0.1 2 4 5 0.17 0.07 -2 -4 -6 1.94 0.2 2 4 6 2.42 0.22 2 4 6 2.27 0.23 2 4 6 1.61 0.25 -2 -4 -7 2.07 0.22 2 4 7 2.5 0.23 2 4 7 2.4 0.24 2 4 7 2.04 0.28 -2 -4 -8 33.73 1.44 2 4 8 33.65 1.43 2 4 8 31.13 1.47 -2 -4 -8 30.1 1.41 2 4 8 28.79 1.54 -2 -4 -9 0.97 0.15 2 4 9 0.83 0.14 2 4 9 0.91 0.16 -2 -4 -9 1.2 0.17 -2 -4 -10 2.22 0.23 -2 -4 -10 2.05 0.22 2 4 10 1.7 0.23 2 4 10 2.53 0.24 2 4 11 23.56 1.07 -2 -4 -11 20.35 1.04 2 4 12 9.17 0.52 -2 -4 -12 8 0.51 2 4 13 3.65 0.29 -2 -4 -13 3.09 0.27 2 4 14 1.4 0.17 -2 -4 -14 1.28 0.17 2 4 15 5.28 0.34 -2 -4 -15 5.34 0.35 -2 -4 -16 0.26 0.08 -2 -4 -17 2.95 0.22 -2 -4 -18 0.49 0.08 2 4 18 0.49 0.1 2 5 -22 14.51 0.65 2 5 -21 6.3 0.35 2 5 -20 0.15 0.06 2 5 -19 20.46 0.95 2 5 -18 16.48 0.81 2 5 -17 0.69 0.13 2 5 -16 0.2 0.09 2 5 -15 61.88 2.59 2 5 -14 12.62 0.69 2 5 -14 13.02 0.7 2 5 -13 17.73 0.86 2 5 -13 18.15 0.88 2 5 -13 15.2 0.9 2 5 -12 15.71 0.87 2 5 -12 18.12 0.87 2 5 -11 20.74 1.01 2 5 -11 21.23 1.13 2 5 -10 1.37 0.17 2 5 -10 1.71 0.25 2 5 -9 73.57 2.95 2 5 -9 67.71 2.97 2 5 -8 2.21 0.2 2 5 -8 2.21 0.22 2 5 -8 2.64 0.33 2 5 -7 7.32 0.42 2 5 -7 6.85 0.44 2 5 -7 7.58 0.59 2 5 -6 0.23 0.07 2 5 -6 0.22 0.07 2 5 -6 0.18 0.07 2 5 -6 0.31 0.08 2 5 -5 68.76 2.74 2 5 -5 65.22 2.76 2 5 -5 70.38 2.79 2 5 -5 66.25 2.76 2 5 -4 2.07 0.21 2 5 -4 2.11 0.19 2 5 -4 2.73 0.24 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2.75 0.27 2 8 3 2.61 0.32 2 8 4 0.09 0.08 2 8 4 0.11 0.11 2 8 5 2.47 0.25 2 8 6 6.61 0.44 2 8 7 6 0.39 2 8 8 1.15 0.15 2 9 -12 0.82 0.12 2 9 -11 11.75 0.62 2 9 -10 7.61 0.47 2 9 -9 1.66 0.2 2 9 -8 1.02 0.17 2 9 -8 0.98 0.15 2 9 -7 5.72 0.42 2 9 -7 4.84 0.36 2 9 -6 0.08 0.1 2 9 -6 0.09 0.08 2 9 -5 7.24 0.48 2 9 -4 2.49 0.26 2 9 -3 2.09 0.25 2 9 -2 0.06 0.09 2 9 -1 14.8 0.83 2 9 0 0.05 0.09 2 9 1 4.1 0.35 2 9 2 0.14 0.09 -3 11 5 0.09 0.08 -3 11 4 0.07 0.08 -3 11 3 16.34 0.87 -3 11 2 0.66 0.15 -3 11 2 0.58 0.14 -3 11 1 10 0.59 -3 11 1 7.64 0.54 -3 11 0 0.17 0.1 -3 11 -1 1.74 0.22 -3 11 -2 2.02 0.24 -3 11 -3 19.38 0.98 -3 11 -4 0.61 0.15 -3 11 -5 2.77 0.27 -3 11 -5 3.65 0.39 -3 11 -6 5.66 0.4 -3 11 -6 6.41 0.51 -3 11 -7 15.49 0.83 -3 11 -7 17.79 0.96 -3 11 -8 2.9 0.26 -3 11 -8 3.12 0.32 -3 11 -9 3.93 0.32 -3 11 -9 4.58 0.38 -3 11 -10 8.85 0.52 -3 11 -11 0.45 0.13 -3 11 -12 8.99 0.5 -3 11 -13 4.98 0.33 -3 10 9 0.78 0.13 -3 10 9 0.59 0.12 -3 10 9 0.93 0.14 -3 10 8 8.09 0.49 -3 10 8 9.24 0.5 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-5 0.69 0.16 -10 4 -5 0.69 0.2 -10 4 -6 2.12 0.24 -10 4 -6 2.17 0.25 -10 4 -6 2.12 0.3 -10 4 -7 5.52 0.4 -10 4 -7 5.34 0.41 -10 4 -7 5.73 0.47 -10 4 -8 2.48 0.25 -10 4 -8 2.59 0.27 -10 4 -8 2.99 0.3 -10 4 -9 0.32 0.1 -10 4 -9 0.09 0.08 -10 4 -10 2.93 0.25 -10 4 -10 3.24 0.27 -10 4 -11 4.3 0.29 -10 4 -11 3.88 0.29 -10 3 14 0.12 0.07 -10 3 13 11.74 0.62 -10 3 13 10.62 0.58 -10 3 12 0.16 0.09 -10 3 11 0.01 0.08 -10 3 10 0.42 0.13 -10 3 9 16.01 0.88 -10 3 8 0.17 0.11 -10 3 7 12.05 0.74 -10 3 6 4 0.38 -10 3 5 0.43 0.16 -10 3 4 0.17 0.12 -10 3 3 5.2 0.43 -10 3 3 5.34 0.47 -10 3 2 2.89 0.32 -10 3 2 2.81 0.34 -10 3 1 1.08 0.21 -10 3 1 1.06 0.22 -10 3 0 13.64 0.84 -10 3 0 13.55 0.84 -10 3 -1 1.07 0.23 -10 3 -2 2.33 0.33 -10 3 -3 2.25 0.31 -10 3 -4 12.57 0.81 -10 3 -5 0.11 0.09 -10 3 -5 0.01 0.11 -10 3 -6 3.89 0.32 -10 3 -6 3.96 0.38 -10 3 -7 0.19 0.09 -10 3 -7 0.17 0.11 -10 3 -8 0.31 0.1 -10 3 -8 0.26 0.11 -10 3 -9 0.12 0.07 -10 3 -9 0.19 0.09 -10 3 -10 4.14 0.28 10 -2 -14 4.02 0.24 -10 2 13 4.93 0.35 10 -2 -13 5.87 0.31 -10 2 12 0.95 0.15 10 -2 -12 1.09 0.12 -10 2 11 6.43 0.44 10 -2 -11 6.77 0.37 -10 2 10 5.7 0.42 10 -2 -10 5.88 0.34 -10 2 9 3.63 0.33 10 -2 -9 3.45 0.25 -10 2 8 0.9 0.17 10 -2 -8 0.83 0.11 -10 2 7 10.17 0.63 10 -2 -7 9.47 0.5 -10 2 6 0.56 0.16 -10 2 5 0.34 0.14 -10 2 4 3.06 0.33 -10 2 3 11.35 0.72 -10 2 2 0.54 0.16 -10 2 2 0.5 0.14 -10 2 1 13.44 0.82 -10 2 1 14.18 0.82 -10 2 0 1.27 0.22 -10 2 0 1.49 0.24 -10 2 -1 -0.01 0.1 -10 2 -2 0.46 0.15 -10 2 -3 11.76 0.74 -10 2 -4 0.82 0.18 -10 2 -5 4.53 0.39 -10 2 -6 1.09 0.18 -10 2 -7 1.2 0.18 -10 2 -8 -0.03 0.07 10 -1 -13 0.23 0.06 10 -1 -12 0.62 0.09 -10 1 11 0.54 0.12 10 -1 -11 0.68 0.09 -10 1 10 4.78 0.36 10 -1 -10 5.56 0.32 -10 1 9 0.02 0.07 10 -1 -9 -0.01 0.04 -10 1 8 11.14 0.65 10 -1 -8 11.44 0.57 -10 1 7 0.18 0.1 10 -1 -7 0.18 0.06 -10 1 6 0.21 0.11 -10 1 5 0.14 0.1 -10 1 4 12.86 0.75 -10 1 3 2.44 0.28 -10 1 2 3.16 0.32 -10 1 1 3.36 0.34 -10 1 0 1.22 0.17 -10 1 0 0.96 0.18 -10 1 -1 0.01 0.07 -10 1 -1 0.04 0.09 -10 1 -2 4.33 0.37 -10 1 -3 3.38 0.32 -10 1 -4 0.15 0.09 -10 1 -5 3.84 0.33 -10 1 -6 0.85 0.15 -10 1 -7 0.39 0.1 10 0 -11 9.41 0.47 10 0 -10 0.11 0.05 10 0 -9 2.35 0.18 -10 0 8 4.08 0.33 10 0 -8 5.25 0.3 -10 0 7 2.22 0.24 10 0 -7 2.71 0.2 -10 0 6 0.09 0.08 -10 0 5 1.49 0.2 -10 0 4 6.42 0.44 -10 0 3 0.25 0.11 -10 0 2 7.82 0.51 -10 0 1 0.96 0.17 -10 0 0 0.29 0.11 -10 0 -1 1.13 0.15 -10 0 -2 6.41 0.39 -10 0 -3 0.6 0.11 -10 0 -3 0.74 0.13 -11 9 6 0.1 0.11 -11 9 5 0.77 0.18 -11 9 4 0.98 0.21 -11 9 3 12.01 0.8 -11 9 2 0.07 0.14 -11 9 2 -0.02 0.11 -11 9 1 3.93 0.45 -11 9 1 3.6 0.3 -11 9 0 3.74 0.31 -11 9 -1 5.21 0.37 -11 9 -1 5.29 0.42 -11 9 -2 0.14 0.1 -11 9 -2 0.22 0.12 -11 9 -3 4.14 0.33 -11 9 -3 4.5 0.38 -11 9 -4 6.27 0.4 -11 9 -4 5.43 0.43 -11 9 -5 -0.02 0.07 -11 9 -5 0.03 0.09 -11 9 -6 1.22 0.16 -11 8 8 0.08 0.08 -11 8 7 5.64 0.43 -11 8 6 6.26 0.48 -11 8 5 0.36 0.14 -11 8 4 3.66 0.39 -11 8 4 4.12 0.33 -11 8 3 4.98 0.48 -11 8 3 5.88 0.4 -11 8 2 0.28 0.15 -11 8 2 0.21 0.1 -11 8 2 0.35 0.13 -11 8 1 10.08 0.73 -11 8 1 9.79 0.56 -11 8 1 8.87 0.58 -11 8 0 3.83 0.45 -11 8 0 4.04 0.32 -11 8 0 4 0.35 -11 8 -1 0.94 0.25 -11 8 -1 0.97 0.16 -11 8 -1 0.85 0.17 -11 8 -2 0.4 0.18 -11 8 -2 0.39 0.11 -11 8 -2 0.48 0.14 -11 8 -3 7.29 0.46 -11 8 -3 7.76 0.52 -11 8 -4 0.04 0.08 -11 8 -4 -0.04 0.09 -11 8 -5 3.01 0.26 -11 8 -5 3.2 0.3 -11 8 -6 0.05 0.07 -11 8 -6 0.06 0.09 -11 8 -7 4.3 0.32 -11 8 -7 5.45 0.38 -11 7 10 7.78 0.44 -11 7 8 3.96 0.33 -11 7 7 0.27 0.11 -11 7 6 1.31 0.21 -11 7 5 0.1 0.11 -11 7 4 15.42 0.91 -11 7 4 15.78 0.81 -11 7 3 0.22 0.14 -11 7 3 0.19 0.12 -11 7 3 0.16 0.1 -11 7 2 2.28 0.31 -11 7 2 1.91 0.23 -11 7 2 1.99 0.24 -11 7 1 1.24 0.25 -11 7 1 1.32 0.19 -11 7 1 1.22 0.19 -11 7 0 2.99 0.38 -11 7 0 3.06 0.28 -11 7 0 3.03 0.3 -11 7 -1 -0.02 0.13 -11 7 -1 -0.02 0.08 -11 7 -1 0.04 0.09 -11 7 -2 8.46 0.65 -11 7 -2 7.33 0.47 -11 7 -2 8.42 0.54 -11 7 -3 1.19 0.24 -11 7 -3 0.89 0.15 -11 7 -3 1.04 0.18 -11 7 -4 0.11 0.08 -11 7 -4 0.14 0.1 -11 7 -5 2.19 0.22 -11 7 -5 2.35 0.26 -11 7 -6 4.68 0.34 -11 7 -6 5.87 0.41 -11 7 -7 0.61 0.13 -11 7 -8 1.95 0.21 -11 6 11 9.84 0.52 -11 6 11 7.36 0.44 -11 6 10 0.38 0.11 -11 6 9 1.05 0.18 -11 6 7 5.45 0.41 -11 6 6 0.33 0.13 -11 6 5 13.34 0.78 -11 6 4 6.51 0.5 -11 6 3 -0.03 0.12 -11 6 2 1.61 0.27 -11 6 1 9.29 0.66 -11 6 1 8.09 0.52 -11 6 0 0.4 0.17 -11 6 0 0.22 0.1 -11 6 -1 0.65 0.2 -11 6 -1 0.7 0.15 -11 6 -2 8.78 0.65 -11 6 -2 7.6 0.51 -11 6 -3 0.75 0.21 -11 6 -3 0.61 0.14 -11 6 -4 1.01 0.22 -11 6 -4 1.13 0.18 -11 6 -5 1.79 0.26 -11 6 -5 1.64 0.21 -11 6 -6 3.38 0.3 -11 6 -7 0.06 0.08 -11 6 -8 5.17 0.36 -11 5 12 4.05 0.28 -11 5 12 3.2 0.24 -11 5 11 5.34 0.35 -11 5 11 3.66 0.28 -11 5 10 0.02 0.07 -11 5 9 6.21 0.45 -11 5 8 3.7 0.35 -11 5 7 0.38 0.14 -11 5 6 4.99 0.4 -11 5 6 5.8 0.47 -11 5 5 8.07 0.54 -11 5 4 0.01 0.09 -11 5 3 9.36 0.63 -11 5 2 0.3 0.14 -11 5 1 7.88 0.58 -11 5 0 0.34 0.16 -11 5 -1 13.54 0.84 -11 5 -2 1.33 0.24 -11 5 -3 0.92 0.21 -11 5 -4 0.08 0.08 -11 5 -4 0.23 0.13 -11 5 -5 4.86 0.36 -11 5 -5 4.68 0.41 -11 5 -6 0.12 0.08 -11 5 -6 0.17 0.1 -11 5 -7 1.14 0.15 -11 4 11 0.2 0.09 -11 4 10 0.61 0.14 -11 4 9 0.08 0.09 -11 4 8 11.56 0.69 -11 4 7 0.57 0.15 -11 4 6 26 1.3 -11 4 5 0.3 0.14 -11 4 4 0.07 0.11 -11 4 4 0.02 0.08 -11 4 3 1.87 0.27 -11 4 3 1.74 0.24 -11 4 2 4.54 0.4 -11 4 1 1.33 0.22 -11 4 0 3.98 0.38 -11 4 -1 3.08 0.34 -11 4 -2 0.12 0.11 -11 4 -3 1.97 0.26 -11 4 -4 7.25 0.52 -11 4 -5 1.13 0.19 -11 4 -6 0.29 0.11 -11 3 11 0.03 0.06 -11 3 10 1.37 0.18 -11 3 9 9.29 0.56 -11 3 8 2.01 0.23 -11 3 7 3.46 0.32 -11 3 6 11.71 0.7 -11 3 5 2.02 0.26 -11 3 4 2.35 0.28 -11 3 3 1.67 0.25 -11 3 2 5.25 0.44 -11 3 2 6.09 0.44 -11 3 1 0.15 0.11 -11 3 1 0.23 0.11 -11 3 0 14.19 0.8 -11 3 -1 0.56 0.15 -11 3 -2 0.29 0.12 -11 3 -3 0.21 0.11 -11 3 -4 4.09 0.34 -11 3 -5 0.03 0.07 -11 2 9 3.91 0.3 -11 2 8 0.02 0.07 -11 2 7 10.66 0.62 -11 2 6 0.11 0.09 -11 2 5 0.4 0.12 -11 2 4 0.78 0.17 -11 2 3 9.19 0.58 -11 2 2 0.35 0.13 -11 2 1 6.61 0.46 -11 2 0 0.38 0.12 -11 2 0 0.61 0.13 -11 2 -1 0.48 0.12 -11 2 -1 0.75 0.14 -11 2 -2 0.49 0.12 -11 2 -3 4.41 0.33 -11 1 4 6.56 0.43 -11 1 3 2.88 0.26 -12 7 3 1.05 0.18 -12 7 2 0.36 0.14 -12 7 1 0.22 0.13 -12 7 0 9.35 0.61 -12 6 4 6.36 0.44 -12 6 3 -0.01 0.08 -12 6 2 1.32 0.2 -12 6 1 1.47 0.22 -12 6 0 5.55 0.43 -12 6 -1 1.91 0.24 -12 5 2 0.11 0.09 -12 5 1 7.98 0.51 -12 5 0 0.4 0.13 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1W Cd1 O1 102.23(8) . . y O2 Cd1 O1 53.89(8) . . y O2 Cd1 O1W 90.73(10) . . y O2W Cd1 O1 88.54(8) . . y O2W Cd1 O1W 168.75(8) . . y O2W Cd1 O2 93.08(10) . . y O4 Cd1 O1 82.84(8) 1_565 . y O4 Cd1 O1W 96.31(9) 1_565 . y O4 Cd1 O2 136.63(9) 1_565 . y O4 Cd1 O2W 88.17(9) 1_565 . y N1 Cd1 O1 139.94(8) . . y N1 Cd1 O1W 85.57(9) . . y N1 Cd1 O2 87.19(9) . . y N1 Cd1 O2W 84.05(9) . . y N1 Cd1 O4 135.91(9) . 1_565 y O6 Cd2 O3W 109.78(9) . . y O6 Cd2 O3W 170.76(9) 2_656 . y O7 Cd2 O3W 102.64(10) . . y O7 Cd2 O6 85.78(9) . . y O7 Cd2 O6 82.55(9) . 2_656 y O8 Cd2 O3W 86.29(9) . . y O8 Cd2 O6 140.72(8) . . y O8 Cd2 O6 90.55(8) . 2_656 y O8 Cd2 O7 55.31(8) . . y N2 Cd2 O3W 91.35(10) . . y N2 Cd2 O6 80.11(9) . 2_656 y N2 Cd2 O6 121.44(10) . . y N2 Cd2 O7 143.21(10) . . y N2 Cd2 O8 92.60(9) . . y C16 O1 Cd1 87.51(18) . . ? H1Wa O1W Cd1 133.3 . . ? H1Wb O1W Cd1 118.8 . . ? H1Wb O1W H1Wa 107.7 . . ? C16 O2 Cd1 97.37(19) . . ? H2Wa O2W Cd1 103.5 . . ? H2Wb O2W Cd1 118.8 . . ? H2Wb O2W H2Wa 84.8 . . ? H3Wa O3W Cd2 130.9 . . ? H3Wb O3W Cd2 121.4 . . ? H3Wb O3W H3Wa 107.7 . . ? C23 O4 Cd1 109.31(19) . 1_545 ? C29 O6 Cd2 103.6(2) . . ? C29 O6 Cd2 127.8(2) . 2_656 ? C32 O7 Cd2 92.7(2) . . ? C32 O8 Cd2 90.00(19) . . ? C1 N1 Cd1 123.4(2) . . ? C5 N1 Cd1 118.9(2) . . ? C5 N1 C1 117.7(3) . . ? C11 N2 Cd2 121.3(2) . . ? C14 N2 Cd2 119.3(2) . . ? C14 N2 C11 119.3(3) . . ? C6 N3 H3 119.2(2) . . ? C7 N3 H3 119.20(19) . . ? C7 N3 C6 121.6(3) . . ? C9 N4 H4 119.91(19) . . ? C10 N4 H4 119.9(2) . . ? C10 N4 C9 120.2(3) . . ? H1 C1 N1 118.90(18) . . ? C2 C1 N1 122.2(3) . . ? C2 C1 H1 118.9(2) . . ? H2 C2 C1 120.2(2) . . ? C3 C2 C1 119.5(3) . . ? C3 C2 H2 120.24(19) . . ? H3a C3 C2 120.55(19) . . ? C4 C3 C2 118.9(3) . . ? C4 C3 H3a 120.55(19) . . ? C5 C4 C3 117.8(3) . . ? C6 C4 C3 125.4(3) . . ? C6 C4 C5 116.8(3) . . ? C4 C5 N1 123.9(3) . . ? H5 C5 N1 118.05(18) . . ? H5 C5 C4 118.0(2) . . ? N3 C6 O9 122.2(3) . . ? C4 C6 O9 120.0(3) . . ? C4 C6 N3 117.7(3) . . ? H7a C7 N3 109.24(19) . . ? H7b C7 N3 109.24(18) . . ? H7b C7 H7a 107.9 . . ? C8 C7 N3 111.9(3) . . ? C8 C7 H7a 109.24(18) . . ? C8 C7 H7b 109.2(2) . . ? H8a C8 C7 109.16(19) . . ? H8b C8 C7 109.2(2) . . ? H8b C8 H8a 107.9 . . ? C9 C8 C7 112.2(3) . . ? C9 C8 H8a 109.2(2) . . ? C9 C8 H8b 109.2(2) . . ? C8 C9 N4 111.2(3) . . ? H9a C9 N4 109.4(2) . . ? H9a C9 C8 109.4(2) . . ? H9b C9 N4 109.4(2) . . ? H9b C9 C8 109.4(2) . . ? H9b C9 H9a 108.0 . . ? N4 C10 O10 121.8(3) . . ? C15 C10 O10 120.1(3) . . ? C15 C10 N4 118.1(3) . . ? H11 C11 N2 119.19(18) . . ? C13 C11 N2 121.6(3) . . ? C13 C11 H11 119.2(2) . . ? C13 C12 H12 120.5(2) . . ? C15 C12 H12 120.49(19) . . ? C15 C12 C13 119.0(3) . . ? C12 C13 C11 119.5(3) . . ? H13 C13 C11 120.2(2) . . ? H13 C13 C12 120.2(2) . . ? H14 C14 N2 118.7(2) . . ? C15 C14 N2 122.5(3) . . ? C15 C14 H14 118.7(2) . . ? C12 C15 C10 125.2(3) . . ? C14 C15 C10 116.8(3) . . ? C14 C15 C12 118.0(3) . . ? O2 C16 O1 121.2(3) . . ? C17 C16 O1 120.4(3) . . ? C17 C16 O2 118.5(3) . . ? C18 C17 C16 120.2(3) . . ? C22 C17 C16 120.2(3) . . ? C22 C17 C18 119.6(3) . . ? H18 C18 C17 119.36(17) . . ? C19 C18 C17 121.3(3) . . ? C19 C18 H18 119.36(18) . . ? C20 C19 C18 118.1(3) . . ? C24 C19 C18 120.7(3) . . ? C24 C19 C20 121.2(3) . . ? H20 C20 C19 119.14(19) . . ? C21 C20 C19 121.7(3) . . ? C21 C20 H20 119.14(18) . . ? C22 C21 C20 119.2(3) . . ? C23 C21 C20 119.2(3) . . ? C23 C21 C22 121.5(3) . . ? C21 C22 C17 120.0(3) . . ? H22 C22 C17 120.01(17) . . ? H22 C22 C21 120.01(17) . . ? O4 C23 O3 122.6(3) . . ? C21 C23 O3 121.0(3) . . ? C21 C23 O4 116.4(3) . . ? H24a C24 C19 109.5 . . ? H24b C24 C19 109.5 . . ? H24b C24 H24a 109.5 . . ? H24c C24 C19 109.5 . . ? H24c C24 H24a 109.5 . . ? H24c C24 H24b 109.5 . . ? C28 C25 C26 120.0(3) . . ? C32 C25 C26 119.9(3) 1_455 . ? C32 C25 C28 120.0(3) 1_455 . ? H26 C26 C25 119.22(18) . . ? C27 C26 C25 121.6(3) . . ? C27 C26 H26 119.22(18) . . ? C31 C27 C26 117.6(3) . . ? C33 C27 C26 120.7(3) . . ? C33 C27 C31 121.7(3) . . ? H28 C28 C25 120.18(19) . . ? C30 C28 C25 119.6(3) . . ? C30 C28 H28 120.18(18) . . ? O6 C29 O5 121.5(3) . . ? C30 C29 O5 120.5(3) . . ? C30 C29 O6 118.0(3) . . ? C29 C30 C28 119.8(3) . . ? C31 C30 C28 119.4(3) . . ? C31 C30 C29 120.7(3) . . ? C30 C31 C27 121.6(3) . . ? H31 C31 C27 119.18(19) . . ? H31 C31 C30 119.18(18) . . ? O8 C32 O7 121.5(3) . . ? C25 C32 O7 119.2(3) 1_655 . ? C25 C32 O8 119.3(3) 1_655 . ? H33a C33 C27 109.5 . . ? H33b C33 C27 109.5 . . ? H33b C33 H33a 109.5 . . ? H33c C33 C27 109.5 . . ? H33c C33 H33a 109.5 . . ? H33c C33 H33b 109.5 . . ? H4Wb O4W H4Wa 104.5 . . ? H5Wb O5W H5Wa 107.7 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cd1 O1 2.501(2) . y Cd1 O1W 2.324(2) . y Cd1 O2 2.294(2) . y Cd1 O2W 2.426(2) . y Cd1 O4 2.206(2) 1_565 y Cd1 N1 2.292(3) . y Cd2 O3W 2.365(3) . y Cd2 O6 2.246(2) . y Cd2 O6 2.529(2) 2_656 y Cd2 O7 2.328(3) . y Cd2 O8 2.378(2) . y Cd2 N2 2.251(3) . y O1 C16 1.254(4) . ? O1W H1Wa 0.8500 . ? O1W H1Wb 0.8500 . ? O2 C16 1.249(4) . ? O2W H2Wa 0.8499 . ? O2W H2Wb 0.8500 . ? O3 C23 1.242(4) . ? O3W H3Wa 0.8500 . ? O3W H3Wb 0.8499 . ? O4 C23 1.272(4) . ? O5 C29 1.238(4) . ? O6 C29 1.273(4) . ? O7 C32 1.245(4) . ? O8 C32 1.259(4) . ? O9 C6 1.235(4) . ? O10 C10 1.225(4) . ? N1 C1 1.342(4) . ? N1 C5 1.333(4) . ? N2 C11 1.332(5) . ? N2 C14 1.332(4) . ? N3 H3 0.8600 . ? N3 C6 1.335(4) . ? N3 C7 1.455(5) . ? N4 H4 0.8600 . ? N4 C9 1.454(4) . ? N4 C10 1.322(4) . ? C1 H1 0.9300 . ? C1 C2 1.375(5) . ? C2 H2 0.9300 . ? C2 C3 1.379(5) . ? C3 H3a 0.9300 . ? C3 C4 1.385(5) . ? C4 C5 1.379(4) . ? C4 C6 1.499(5) . ? C5 H5 0.9300 . ? C7 H7a 0.9700 . ? C7 H7b 0.9700 . ? C7 C8 1.514(5) . ? C8 H8a 0.9700 . ? C8 H8b 0.9700 . ? C8 C9 1.511(5) . ? C9 H9a 0.9700 . ? C9 H9b 0.9700 . ? C10 C15 1.505(4) . ? C11 H11 0.9300 . ? C11 C13 1.378(5) . ? C12 H12 0.9300 . ? C12 C13 1.379(5) . ? C12 C15 1.386(5) . ? C13 H13 0.9300 . ? C14 H14 0.9300 . ? C14 C15 1.388(4) . ? C16 C17 1.502(4) . ? C17 C18 1.394(4) . ? C17 C22 1.392(4) . ? C18 H18 0.9300 . ? C18 C19 1.386(5) . ? C19 C20 1.390(4) . ? C19 C24 1.505(5) . ? C20 H20 0.9300 . ? C20 C21 1.392(4) . ? C21 C22 1.390(4) . ? C21 C23 1.506(4) . ? C22 H22 0.9300 . ? C24 H24a 0.9600 . ? C24 H24b 0.9600 . ? C24 H24c 0.9600 . ? C25 C26 1.381(4) . ? C25 C28 1.389(4) . ? C25 C32 1.501(5) 1_455 ? C26 H26 0.9300 . ? C26 C27 1.394(5) . ? C27 C31 1.390(5) . ? C27 C33 1.497(5) . ? C28 H28 0.9300 . ? C28 C30 1.390(4) . ? C29 C30 1.498(4) . ? C30 C31 1.393(4) . ? C31 H31 0.9300 . ? C33 H33a 0.9600 . ? C33 H33b 0.9600 . ? C33 H33c 0.9600 . ? O4W H4Wa 0.8500 . ? O4W H4Wb 0.8500 . ? O5W H5Wa 0.8499 . ? O5W H5Wb 0.8501 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cd1 O1 C16 O2 1.9(2) . . . . ? Cd1 O1 C16 C17 -177.23(14) . . . . ? Cd1 O2 C16 O1 -2.0(2) . . . . ? Cd1 O2 C16 C17 177.06(15) . . . . ? Cd1 O4 C23 O3 -4.8(2) 1_545 . . . ? Cd1 O4 C23 C21 174.10(17) 1_545 . . . ? Cd1 N1 C1 C2 179.1(2) . . . . ? Cd1 N1 C5 C4 -178.2(2) . . . . ? Cd2 O6 C29 O5 111.9(3) 2_656 . . . ? Cd2 O6 C29 O5 -5.4(2) . . . . ? Cd2 O6 C29 C30 -70.4(3) 2_656 . . . ? Cd2 O6 C29 C30 172.29(18) . . . . ? Cd2 O7 C32 O8 -6.9(2) . . . . ? Cd2 O7 C32 C25 171.81(14) . . . 1_655 ? Cd2 O8 C32 O7 6.8(2) . . . . ? Cd2 O8 C32 C25 -171.96(14) . . . 1_655 ? Cd2 N2 C11 C13 177.9(3) . . . . ? Cd2 N2 C14 C15 -177.9(2) . . . . ? O1 C16 C17 C18 14.9(3) . . . . ? O1 C16 C17 C22 -166.7(3) . . . . ? O2 C16 C17 C18 -164.3(3) . . . . ? O2 C16 C17 C22 14.1(4) . . . . ? O3 C23 C21 C20 169.0(3) . . . . ? O3 C23 C21 C22 -8.7(3) . . . . ? O4 C23 C21 C20 -9.9(3) . . . . ? O4 C23 C21 C22 172.3(3) . . . . ? O5 C29 C30 C28 -28.4(4) . . . . ? O5 C29 C30 C31 150.3(3) . . . . ? O6 C29 C30 C28 153.9(3) . . . . ? O6 C29 C30 C31 -27.5(4) . . . . ? O7 C32 C25 C26 4.1(4) . . 1_655 1_655 ? O7 C32 C25 C28 -174.1(3) . . 1_655 1_655 ? O8 C32 C25 C26 -177.1(3) . . 1_655 1_655 ? O8 C32 C25 C28 4.7(4) . . 1_655 1_655 ? O9 C6 N3 C7 0.9(4) . . . . ? O9 C6 C4 C3 175.2(3) . . . . ? O9 C6 C4 C5 -2.6(4) . . . . ? O10 C10 N4 C9 2.7(4) . . . . ? O10 C10 C15 C12 -173.3(3) . . . . ? O10 C10 C15 C14 5.4(4) . . . . ? N1 C1 C2 C3 -0.4(4) . . . . ? N1 C5 C4 C3 -1.5(4) . . . . ? N1 C5 C4 C6 176.5(3) . . . . ? N2 C11 C13 C12 0.0(4) . . . . ? N2 C14 C15 C10 -178.9(3) . . . . ? N2 C14 C15 C12 -0.1(4) . . . . ? N3 C6 C4 C3 -2.4(4) . . . . ? N3 C6 C4 C5 179.8(3) . . . . ? N3 C7 C8 C9 169.2(3) . . . . ? N4 C9 C8 C7 -69.5(4) . . . . ? N4 C10 C15 C12 6.7(4) . . . . ? N4 C10 C15 C14 -174.6(3) . . . . ? C1 C2 C3 C4 -0.4(4) . . . . ? C2 C3 C4 C5 1.3(4) . . . . ? C2 C3 C4 C6 -176.5(3) . . . . ? C10 C15 C12 C13 179.4(3) . . . . ? C11 C13 C12 C15 -0.6(4) . . . . ? C16 C17 C18 C19 179.6(3) . . . . ? C16 C17 C22 C21 179.6(3) . . . . ? C17 C18 C19 C20 0.9(3) . . . . ? C17 C18 C19 C24 -179.1(3) . . . . ? C17 C22 C21 C20 0.6(3) . . . . ? C17 C22 C21 C23 178.4(3) . . . . ? C18 C19 C20 C21 -2.3(4) . . . . ? C19 C20 C21 C22 1.5(4) . . . . ? C19 C20 C21 C23 -176.2(3) . . . . ? C25 C26 C27 C31 1.6(4) . . . . ? C25 C26 C27 C33 -178.0(3) . . . . ? C25 C28 C30 C29 179.5(3) . . . . ? C25 C28 C30 C31 0.8(3) . . . . ? C26 C27 C31 C30 -1.6(4) . . . . ? C27 C31 C30 C28 0.5(4) . . . . ? C27 C31 C30 C29 -178.2(3) . . . . ?