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Information card for entry 7247829
Preview
Coordinates | 7247829.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C28 H25 O P |
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Calculated formula | C28 H25 O P |
SMILES | P(=O)(/C(=C/c1ccc(cc1)C)c1ccc(cc1)C)(c1ccccc1)c1ccccc1 |
Title of publication | Direct air-induced arylphosphinoyl radicals for the synthesis of benzo[b]phosphole oxides |
Authors of publication | Huang, Mingqing; Huang, Haiyang; You, Mengyao; Zhang, Xinxin; Sun, Longgen; Chen, Chao; Mei, Zhichao; Yang, Ruchun; Xiao, Qiang |
Journal of publication | Green Chemistry |
Year of publication | 2024 |
Journal volume | 26 |
Journal issue | 1 |
Pages of publication | 295 - 299 |
a | 13.961 ± 0.002 Å |
b | 9.9168 ± 0.0016 Å |
c | 21.452 ± 0.003 Å |
α | 90° |
β | 106.577 ± 0.003° |
γ | 90° |
Cell volume | 2846.6 ± 0.7 Å3 |
Cell temperature | 296.15 K |
Ambient diffraction temperature | 296.15 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.1132 |
Residual factor for significantly intense reflections | 0.0555 |
Weighted residual factors for significantly intense reflections | 0.1352 |
Weighted residual factors for all reflections included in the refinement | 0.1541 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.836 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
289563 (current) | 2024-02-04 | cif/ Updating files of 7247828, 7247829 Original log message: Adding full bibliography for 7247828--7247829.cif. |
7247829.cif |
288026 | 2023-12-05 | cif/ Adding structures of 7247828, 7247829 via cif-deposit CGI script. |
7247829.cif |
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Users of the data should acknowledge the original authors of the
structural data.