Crystallography Open Database

Information card for entry 7248369

Preview

Coordinates	7248369.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	H29.2 Mo12 Na5.8 O55.5 U
Calculated formula	Mo12 Na5.8 O55.5 U
Title of publication	Highly-stable Silverton-type UIV-containing polyoxomolybdate frameworks for the heterogeneous catalytic synthesis of quinazolinones
Authors of publication	Li, Ke; Liu, Yufeng; Yang, Guoping; Zheng, Zhijian; Lin, Xiaoling; Zhang, Zhibin; Li, Shujun; Liu, Yunhai; Wei, Yongge
Journal of publication	Green Chemistry
Year of publication	2024
Journal volume	26
Journal issue	11
Pages of publication	6454 - 6460
a	19.0319 ± 0.0003 Å
b	19.0319 ± 0.0003 Å
c	11.446 ± 0.0005 Å
α	90°
β	90°
γ	120°
Cell volume	3590.45 ± 0.18 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	5
Space group number	148
Hermann-Mauguin space group symbol	R -3 :H
Hall space group symbol	-R 3
Residual factor for all reflections	0.0215
Residual factor for significantly intense reflections	0.0201
Weighted residual factors for significantly intense reflections	0.0487
Weighted residual factors for all reflections included in the refinement	0.0494
Goodness-of-fit parameter for all reflections included in the refinement	1.093
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
293169 (current)	2024-07-05	cif/ Updating files of 7248368, 7248369, 7248370, 7248371 Original log message: Adding full bibliography for 7248368--7248371.cif.	7248369.cif
290742	2024-04-03	cif/ Adding structures of 7248368, 7248369, 7248370, 7248371 via cif-deposit CGI script.	7248369.cif