#------------------------------------------------------------------------------ #$Date: 2024-04-03 04:32:36 +0300 (Wed, 03 Apr 2024) $ #$Revision: 290746 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/83/7248375.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7248375 loop_ _publ_author_name 'Ma, Chi Thanh' 'Huang, Tianqi' 'Yu, Jae Sik' 'Ly, Tu Loan' 'Vu Huynh, Kim Long' 'Kwon, Sung Won' 'Park, Jeong Hill' 'Yang, Hyun Ok' _publ_section_title ; Sesquiterpenoids and hexanorcucurbitacin from Aquilaria malaccensis agarwood with anti-inflammatory effects by inhibiting the STAT1/AKT/MAPK/NLRP3 pathway ; _journal_issue 13 _journal_name_full 'RSC Advances' _journal_page_first 9391 _journal_page_last 9405 _journal_paper_doi 10.1039/D3RA08686K _journal_volume 14 _journal_year 2024 _chemical_absolute_configuration unk _chemical_formula_moiety 'C24 H30 O4, C H4 O' _chemical_formula_sum 'C25 H34 O5' _chemical_formula_weight 414.52 _chemical_name_systematic 'Compound 19' _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _audit_creation_date 2017-03-17 _audit_creation_method ; Olex2 1.2 (compiled 2017.03.02 svn.r3394 for OlexSys, GUI svn.r5324) ; _audit_update_record ; 2020-09-24 deposited with the CCDC. 2024-03-28 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.0589(2) _cell_length_b 14.2921(3) _cell_length_c 15.1181(3) _cell_measurement_reflns_used 12450 _cell_measurement_temperature 99.8(7) _cell_measurement_theta_max 73.6990 _cell_measurement_theta_min 4.2240 _cell_volume 2173.42(8) _computing_cell_refinement 'CrysAlisPro 1.171.38.44a (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.44a (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.44a (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 99.8(7) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 5.2262 _diffrn_detector_type AtlasS2 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -113.00 -13.00 1.00 6.50 -- -41.24 -57.00 0.00 100 2 \w -113.00 -13.00 1.00 6.50 -- -41.24 -57.00 90.00 100 3 \w 23.00 97.00 1.00 6.50 -- 41.24-125.00 60.00 74 4 \w 36.00 116.00 1.00 25.00 -- 112.00-111.00 30.00 80 5 \w 86.00 178.00 1.00 25.00 -- 112.00 45.00-180.00 92 6 \w 86.00 178.00 1.00 25.00 -- 112.00 45.00 0.00 92 7 \w 100.00 178.00 1.00 25.00 -- 112.00 111.00-150.00 78 8 \w 29.00 109.00 1.00 25.00 -- 112.00 -94.00 -30.00 80 9 \w 29.00 109.00 1.00 25.00 -- 112.00 -94.00-150.00 80 10 \w 57.00 135.00 1.00 25.00 -- 112.00 178.00 0.00 78 11 \w 41.00 132.00 1.00 25.00 -- 112.00 -45.00 90.00 91 12 \w 33.00 106.00 1.00 25.00 -- 112.00 -94.00 60.00 73 13 \w -115.00 -64.00 1.00 39.51 -- -41.49-140.00 32.00 51 14 \w -115.00 -13.00 1.00 39.51 -- -41.49 -57.00-120.00 102 15 \w 84.00 178.00 1.00 50.84 -- 112.00 30.00 120.00 94 16 \w 86.00 178.00 1.00 50.84 -- 112.00 45.00 60.00 92 17 \w 83.00 178.00 1.00 50.84 -- 112.00 61.00 -60.00 95 18 \w 83.00 178.00 1.00 50.84 -- 112.00 61.00-150.00 95 19 \w 86.00 161.00 1.00 50.84 -- 112.00 45.00 150.00 75 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, AtlasS2' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.1306933000 _diffrn_orient_matrix_UB_12 -0.0269419000 _diffrn_orient_matrix_UB_13 -0.0465782000 _diffrn_orient_matrix_UB_21 0.0653821000 _diffrn_orient_matrix_UB_22 0.0179770000 _diffrn_orient_matrix_UB_23 -0.0905822000 _diffrn_orient_matrix_UB_31 0.0459652000 _diffrn_orient_matrix_UB_32 -0.1027624000 _diffrn_orient_matrix_UB_33 -0.0035965000 _diffrn_radiation_collimation '0.2 mm sinlge-pinhole' _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0390 _diffrn_reflns_av_unetI/netI 0.0242 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 21475 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.992 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 76.678 _diffrn_reflns_theta_min 4.257 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.697 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.81985 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.44a (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear light colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.267 _exptl_crystal_description block _exptl_crystal_F_000 896 _exptl_crystal_size_max 0.15 _exptl_crystal_size_mid 0.04 _exptl_crystal_size_min 0.02 _refine_diff_density_max 0.219 _refine_diff_density_min -0.236 _refine_diff_density_rms 0.056 _refine_ls_abs_structure_details ; Flack x determined using 1822 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.01(8) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.067 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 280 _refine_ls_number_reflns 4530 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.067 _refine_ls_R_factor_all 0.0382 _refine_ls_R_factor_gt 0.0369 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0589P)^2^+0.3557P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0976 _refine_ls_wR_factor_ref 0.0987 _reflns_Friedel_coverage 0.759 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.989 _reflns_number_gt 4390 _reflns_number_total 4530 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d3ra08686k3.cif _cod_data_source_block exp_823 _cod_original_cell_volume 2173.43(8) _cod_database_code 7248375 _shelx_shelxl_version_number 2014/7 _chemical_oxdiff_formula C24H30O4 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _reflns_odcompleteness_completeness 100.00 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 74.33 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2.a Ternary CH refined with riding coordinates: C8(H8), C10(H10) 2.b Secondary CH2 refined with riding coordinates: C7(H7A,H7B), C12(H12A,H12B), C15(H15A,H15B) 2.c Aromatic/amide H refined with riding coordinates: C1(H1), C6(H6), C16(H16) 2.d Idealised Me refined as rotating group: C18(H18A,H18B,H18C), C19(H19A,H19B,H19C), C20(H20A,H20B,H20C), C22(H22A,H22B, H22C), C23(H23B,H23A,H23C), C24(H24A,H24B,H24C), C25(H25A,H25B,H25C) 2.e Idealised tetrahedral OH refined as rotating group: O2(H2), O25(H25) ; _shelx_res_file ; exp_823.res created by SHELXL-2014/7 TITL exp_823_a.res in P2(1)2(1)2(1) REM Old TITL exp_823 in P212121 #19 REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.102, Rweak 0.027, Alpha 0.001, Orientation as input REM Flack x = -0.134 ( 0.101 ) from Parsons' quotients REM Formula found by SHELXT: C25 O5 CELL 1.54184 10.058927 14.292073 15.118122 90 90 90 ZERR 4 0.000216 0.000311 0.000298 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H O UNIT 100 136 20 L.S. 10 PLAN 20 BOND $H LIST 6 fmap 2 acta REM REM REM WGHT 0.058900 0.355700 FVAR 0.42540 O2 3 0.821777 0.791343 0.860428 11.00000 0.06394 0.02206 = 0.02867 -0.00160 -0.00710 -0.00991 AFIX 147 H2 2 0.836242 0.844390 0.842141 11.00000 -1.50000 AFIX 0 O3 3 0.748301 0.866992 0.703487 11.00000 0.04886 0.02094 = 0.04019 0.00482 -0.00362 -0.00143 O11 3 0.799604 0.445403 0.886380 11.00000 0.05456 0.02456 = 0.01999 -0.00146 -0.00781 0.00100 O21 3 0.880622 0.128934 0.749920 11.00000 0.04694 0.02293 = 0.03136 0.00173 -0.00913 0.00195 C1 1 0.782815 0.641954 0.800495 11.00000 0.03084 0.02307 = 0.01963 0.00096 -0.00414 -0.00208 AFIX 43 H1 2 0.805770 0.616515 0.855016 11.00000 -1.20000 AFIX 0 C2 1 0.787363 0.735089 0.791523 11.00000 0.03486 0.02378 = 0.02197 -0.00140 -0.00165 -0.00299 C3 1 0.756274 0.781728 0.706822 11.00000 0.02607 0.02198 = 0.02857 0.00394 0.00034 -0.00128 C4 1 0.744315 0.719460 0.625387 11.00000 0.02581 0.02562 = 0.02165 0.00492 -0.00064 0.00182 C5 1 0.676766 0.628022 0.652144 11.00000 0.02456 0.02097 = 0.01955 0.00030 0.00141 0.00526 C6 1 0.569258 0.596120 0.611200 11.00000 0.02723 0.02447 = 0.02436 -0.00269 -0.00469 0.00682 AFIX 43 H6 2 0.535260 0.631757 0.564967 11.00000 -1.20000 AFIX 0 C7 1 0.498696 0.507299 0.633737 11.00000 0.02532 0.02608 = 0.03370 -0.00457 -0.00570 0.00244 AFIX 23 H7A 2 0.475447 0.475732 0.579085 11.00000 -1.20000 H7B 2 0.416412 0.522995 0.663723 11.00000 -1.20000 AFIX 0 C8 1 0.576579 0.438793 0.691974 11.00000 0.02321 0.02089 = 0.02499 -0.00375 -0.00028 -0.00013 AFIX 13 H8 2 0.509044 0.402963 0.724154 11.00000 -1.20000 AFIX 0 C9 1 0.658774 0.491282 0.765133 11.00000 0.02628 0.01967 = 0.02045 -0.00171 0.00189 -0.00068 C10 1 0.742785 0.575962 0.727648 11.00000 0.02507 0.01649 = 0.02021 -0.00022 -0.00192 0.00024 AFIX 13 H10 2 0.825150 0.549301 0.703910 11.00000 -1.20000 AFIX 0 C11 1 0.764833 0.428496 0.810973 11.00000 0.03363 0.01642 = 0.01940 0.00107 -0.00130 -0.00424 C12 1 0.829112 0.347511 0.761015 11.00000 0.02884 0.01943 = 0.01933 0.00095 -0.00169 -0.00103 AFIX 23 H12A 2 0.871004 0.304754 0.802319 11.00000 -1.20000 H12B 2 0.896626 0.370997 0.720943 11.00000 -1.20000 AFIX 0 C13 1 0.720196 0.296740 0.708897 11.00000 0.02660 0.01721 = 0.01990 -0.00035 0.00123 -0.00215 C14 1 0.657289 0.365994 0.640468 11.00000 0.02527 0.01962 = 0.02094 -0.00129 -0.00140 0.00036 C15 1 0.577558 0.297738 0.581030 11.00000 0.03166 0.02509 = 0.02709 -0.00618 -0.00687 0.00103 AFIX 23 H15A 2 0.491168 0.283693 0.606259 11.00000 -1.20000 H15B 2 0.565917 0.322676 0.521862 11.00000 -1.20000 AFIX 0 C16 1 0.666218 0.213125 0.580865 11.00000 0.03482 0.02185 = 0.02422 -0.00429 -0.00007 -0.00065 AFIX 43 H16 2 0.662593 0.166156 0.538358 11.00000 -1.20000 AFIX 0 C17 1 0.751417 0.213298 0.649400 11.00000 0.02934 0.01816 = 0.02199 -0.00130 0.00370 -0.00184 C18 1 0.619330 0.259047 0.777523 11.00000 0.03369 0.02216 = 0.02672 -0.00165 0.00683 -0.00477 AFIX 137 H18A 2 0.540132 0.238867 0.747664 11.00000 -1.50000 H18B 2 0.597483 0.307733 0.818785 11.00000 -1.50000 H18C 2 0.657820 0.207165 0.808680 11.00000 -1.50000 AFIX 0 C19 1 0.558445 0.526619 0.834358 11.00000 0.03593 0.02352 = 0.02832 -0.00510 0.00883 -0.00269 AFIX 137 H19A 2 0.505892 0.475098 0.855272 11.00000 -1.50000 H19B 2 0.501392 0.572618 0.807896 11.00000 -1.50000 H19C 2 0.605470 0.554181 0.883085 11.00000 -1.50000 AFIX 0 C20 1 0.762229 0.409702 0.578789 11.00000 0.03155 0.02305 = 0.01945 0.00184 0.00123 0.00314 AFIX 137 H20A 2 0.822825 0.446889 0.613007 11.00000 -1.50000 H20B 2 0.718874 0.448553 0.535764 11.00000 -1.50000 H20C 2 0.810372 0.360897 0.549167 11.00000 -1.50000 AFIX 0 C21 1 0.837218 0.135009 0.674114 11.00000 0.02769 0.01899 = 0.02847 0.00102 0.00091 -0.00331 C22 1 0.866985 0.059611 0.607663 11.00000 0.03575 0.02269 = 0.03444 -0.00308 0.00205 0.00214 AFIX 137 H22A 2 0.952705 0.033069 0.619901 11.00000 -1.50000 H22B 2 0.866870 0.085955 0.549251 11.00000 -1.50000 H22C 2 0.800387 0.011661 0.611404 11.00000 -1.50000 AFIX 0 C23 1 0.887787 0.699851 0.594010 11.00000 0.02771 0.03603 = 0.02945 0.00820 0.00372 0.00296 AFIX 137 H23B 2 0.929766 0.757674 0.577762 11.00000 -1.50000 H23A 2 0.885692 0.658799 0.543769 11.00000 -1.50000 H23C 2 0.937063 0.670895 0.640999 11.00000 -1.50000 AFIX 0 C24 1 0.672950 0.772522 0.551734 11.00000 0.03489 0.03120 = 0.02782 0.00793 -0.00211 0.00427 AFIX 137 H24A 2 0.672132 0.735125 0.498988 11.00000 -1.50000 H24B 2 0.718591 0.830263 0.540315 11.00000 -1.50000 H24C 2 0.583248 0.785547 0.569579 11.00000 -1.50000 AFIX 0 O25 3 1.083082 0.469803 0.651938 11.00000 0.04305 0.02169 = 0.03220 0.00153 -0.00483 -0.00209 AFIX 147 H25 2 1.102183 0.505548 0.692416 11.00000 -1.50000 AFIX 0 C25 1 1.119187 0.510398 0.570892 11.00000 0.03932 0.03689 = 0.03352 0.00203 0.00590 0.00783 AFIX 137 H25A 2 1.118377 0.577309 0.576440 11.00000 -1.50000 H25B 2 1.057078 0.491711 0.526032 11.00000 -1.50000 H25C 2 1.206802 0.489943 0.554769 11.00000 -1.50000 AFIX 0 HKLF 4 REM exp_823_a.res in P2(1)2(1)2(1) REM R1 = 0.0369 for 4390 Fo > 4sig(Fo) and 0.0382 for all 4530 data REM 280 parameters refined using 0 restraints END WGHT 0.0589 0.3557 REM Highest difference peak 0.219, deepest hole -0.236, 1-sigma level 0.056 Q1 1 0.7401 0.2569 0.6815 11.00000 0.05 0.22 Q2 1 0.7527 0.6063 0.7636 11.00000 0.05 0.21 Q3 1 0.7501 0.2235 0.8267 11.00000 0.05 0.21 Q4 1 0.7235 0.6033 0.6905 11.00000 0.05 0.21 Q5 1 0.7508 0.7472 0.6628 11.00000 0.05 0.20 Q6 1 0.7281 0.3822 0.6220 11.00000 0.05 0.20 Q7 1 0.7252 0.4374 0.8891 11.00000 0.05 0.20 Q8 1 0.6723 0.2818 0.7416 11.00000 0.05 0.19 Q9 1 0.7711 0.3257 0.7370 11.00000 0.05 0.19 Q10 1 0.7470 0.8164 0.7833 11.00000 0.05 0.18 Q11 1 0.7748 0.0007 0.6591 11.00000 0.05 0.18 Q12 1 0.7738 0.1380 0.7670 11.00000 0.05 0.18 Q13 1 0.7588 0.2245 0.5751 11.00000 0.05 0.18 Q14 1 0.6181 0.4635 0.7278 11.00000 0.05 0.18 Q15 1 0.7502 0.6086 0.8831 11.00000 0.05 0.18 Q16 1 0.7496 0.8088 0.7013 11.00000 0.05 0.18 Q17 1 1.2475 0.5595 0.5654 11.00000 0.05 0.18 Q18 1 1.1596 0.4684 0.6210 11.00000 0.05 0.17 Q19 1 0.7082 0.5373 0.7399 11.00000 0.05 0.17 Q20 1 0.7641 0.0501 0.5555 11.00000 0.05 0.17 ; _shelx_res_checksum 21790 _shelx_hkl_file ; 0 0 -1 0.95 0.09 0 0 1 0.12 0.18 0 0 2 7956.80 25.57 0 0 -2 7904.87 9.34 0 0 -3 0.07 0.16 0 0 3 0.22 0.48 0 0 -4 1860.20 6.82 0 0 4 1896.98 18.84 0 0 5 0.38 0.97 0 0 -5 0.27 0.29 0 0 -6 277.25 3.48 0 0 6 286.69 8.85 0 0 6 276.82 9.49 0 0 -7 0.00 0.29 0 0 7 -0.08 1.15 0 0 7 -0.41 0.97 0 0 8 7.63 2.08 0 0 8 11.19 2.11 0 0 -8 7.94 0.77 0 0 -9 0.16 0.35 0 0 9 -0.43 0.66 0 0 9 -0.04 0.91 0 0 -10 0.67 0.41 0 0 10 -0.31 1.16 0 0 10 0.61 0.93 0 0 -11 -0.07 0.35 0 0 11 1.05 1.34 0 0 -12 24.60 1.59 0 0 12 25.76 1.60 0 0 -12 25.53 1.59 0 0 12 24.35 1.87 0 0 -12 25.94 2.04 0 0 -13 -0.31 0.44 0 0 -13 -0.46 0.68 0 0 13 0.24 0.55 0 0 13 -0.81 0.62 0 0 -13 0.42 0.57 0 0 -14 104.11 4.13 0 0 14 95.55 3.38 0 0 -14 101.24 3.41 0 0 15 -0.17 0.54 0 0 -15 0.35 0.48 0 0 -15 0.53 0.60 0 0 16 0.25 0.49 0 0 -16 0.86 0.55 0 0 -16 0.08 0.76 0 0 -17 -0.17 0.62 0 0 17 0.22 0.44 0 0 -17 0.23 0.37 0 0 18 29.17 1.32 0 0 -18 32.68 1.36 0 0 -18 29.16 1.80 0 0 19 0.23 0.18 0 -1 0 0.07 0.25 0 -1 1 83.54 1.92 0 -1 1 82.31 1.96 0 1 -1 77.54 0.90 0 1 1 81.39 1.77 0 -1 -1 80.25 0.80 0 1 -2 414.68 2.46 0 -1 2 418.06 6.14 0 1 2 397.31 5.74 0 -1 -2 396.53 2.24 0 1 -3 261.26 2.33 0 1 3 249.67 5.78 0 -1 3 250.36 5.89 0 -1 -3 249.39 2.18 0 1 4 452.60 9.13 0 -1 -4 451.19 3.46 0 -1 4 457.54 9.48 0 1 -4 461.87 3.55 0 -1 5 21.77 2.44 0 1 5 22.13 2.41 0 1 -5 22.84 0.92 0 -1 -5 22.64 0.92 0 1 -6 136.65 2.44 0 1 6 141.11 6.96 0 -1 -6 131.84 2.42 0 -1 6 152.19 5.84 0 1 6 135.62 6.58 0 -1 6 148.07 7.28 0 1 7 122.72 6.93 0 1 -7 124.82 2.57 0 1 7 124.79 6.99 0 -1 -7 118.86 2.58 0 -1 7 127.71 7.18 0 -1 7 122.62 5.42 0 1 8 117.52 7.18 0 1 8 114.60 7.31 0 -1 -8 107.34 2.69 0 1 -8 114.52 2.68 0 -1 8 115.35 7.42 0 -1 8 113.66 5.45 0 1 9 152.90 8.48 0 1 -9 155.46 3.41 0 -1 9 165.00 9.61 0 -1 -9 152.57 3.46 0 1 9 154.86 9.24 0 1 10 4.86 1.81 0 1 -10 4.31 0.71 0 1 10 5.81 1.87 0 -1 10 4.77 1.97 0 -1 -10 4.67 0.74 0 -1 11 35.68 5.20 0 1 11 28.66 3.70 0 -1 -11 30.19 1.75 0 1 -11 37.12 1.93 0 1 11 27.94 4.46 0 -1 -12 193.30 4.45 0 1 -12 203.77 4.30 0 -1 12 248.62 6.43 0 1 12 197.23 11.89 0 -1 -12 203.19 4.37 0 1 -12 208.28 4.58 0 -1 12 240.20 4.85 0 -1 -12 206.66 5.92 0 1 12 197.19 4.32 0 -1 13 51.10 2.95 0 1 -13 48.13 2.32 0 -1 -13 54.93 2.46 0 -1 -13 53.30 3.13 0 1 13 51.95 2.42 0 1 -13 54.15 2.38 0 -1 -13 47.77 2.27 0 -1 13 50.76 2.39 0 -1 -14 7.53 1.29 0 -1 14 7.89 1.07 0 1 -14 8.09 1.04 0 -1 14 8.61 1.27 0 1 14 7.85 1.09 0 -1 14 5.17 1.76 0 -1 -14 7.67 1.00 0 1 -15 53.85 2.42 0 -1 15 49.21 2.45 0 -1 15 51.01 2.76 0 -1 -15 55.85 3.62 0 -1 -15 54.14 3.13 0 1 15 52.73 2.50 0 -1 -15 54.31 2.53 0 -1 15 50.17 4.52 0 1 16 110.31 3.41 0 -1 -16 117.68 3.50 0 -1 16 114.84 5.79 0 -1 -16 117.87 4.86 0 -1 16 118.30 3.51 0 1 -16 116.15 3.41 0 1 -17 120.84 4.53 0 1 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3.00 -1 -12 -2 106.19 5.43 1 -12 2 100.28 4.48 -1 -12 -1 52.94 3.88 1 -12 1 49.10 4.81 1 -12 1 46.65 2.92 1 -12 1 39.77 5.19 1 12 -1 40.09 2.01 -1 -12 -1 40.86 5.63 1 -12 1 44.03 3.40 -1 -12 -1 44.23 3.56 -1 -12 -1 40.12 3.15 1 -12 1 45.43 3.14 1 12 0 61.60 2.49 1 -12 0 71.91 4.06 1 -12 0 75.77 3.93 -1 -12 0 67.42 4.26 -1 -12 0 69.43 3.85 1 -12 0 80.51 5.88 -1 -12 0 64.77 6.72 1 -12 0 66.08 6.85 -1 -12 0 76.72 4.47 1 -12 0 78.91 4.35 -1 -12 1 42.37 2.86 -1 -12 1 45.74 3.58 1 12 1 39.31 1.95 1 -12 -1 47.05 4.48 1 -12 -1 40.63 5.45 1 -12 -1 45.81 3.39 -1 -12 1 39.35 4.90 1 -12 -1 48.67 3.34 -1 -12 1 42.96 3.43 1 -12 -1 44.58 3.09 1 -12 -2 111.89 4.36 1 -12 -2 110.72 5.18 1 -12 -2 97.71 8.63 1 -12 -2 103.93 5.28 1 -12 -2 101.41 4.38 -1 -12 2 103.38 5.41 -1 -12 2 102.94 5.17 -1 -12 2 112.25 4.31 -1 -12 2 107.60 6.35 -1 -12 3 19.88 2.45 1 -12 -3 18.68 2.01 1 -12 -3 17.69 1.93 -1 -12 3 18.98 2.88 -1 -12 3 19.87 2.28 1 -12 -3 19.76 1.88 1 -12 -3 18.21 2.36 1 -12 -3 19.06 2.29 1 -12 -4 95.33 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143.94 6.20 1 -13 2 151.10 6.57 1 -13 2 156.36 5.68 -1 -13 -2 148.94 6.60 -1 -13 -1 3.68 1.11 1 -13 1 5.60 1.89 1 -13 1 3.70 1.25 1 -13 1 4.33 0.97 -1 -13 -1 4.10 2.18 1 -13 1 5.14 1.30 -1 -13 -1 5.16 1.37 1 -13 0 50.54 3.32 1 -13 0 51.94 4.96 -1 -13 0 53.71 4.24 -1 -13 0 52.38 3.97 1 -13 0 46.29 3.45 1 -13 0 50.76 3.61 -1 -13 0 48.74 3.31 1 -13 -1 4.37 1.18 -1 -13 1 4.40 1.38 -1 -13 1 4.37 1.06 -1 -13 1 4.17 1.66 1 -13 -1 2.51 1.04 1 -13 -1 4.84 1.25 -1 -13 2 145.34 4.78 1 -13 -2 157.81 4.90 -1 -13 2 149.65 6.36 -1 -13 2 161.53 7.58 1 -13 -2 154.40 6.13 -1 -13 2 178.36 7.22 1 -13 -2 173.98 5.83 1 -13 -2 155.90 6.43 1 -13 -3 43.84 3.64 -1 -13 3 41.16 3.32 -1 -13 3 38.74 3.97 1 -13 -3 44.09 2.81 -1 -13 3 41.47 3.65 1 -13 -3 43.33 2.94 1 -13 -3 42.15 3.30 1 -13 -4 41.86 3.40 -1 -13 4 43.06 4.48 -1 -13 4 42.42 3.60 1 -13 -4 43.38 3.33 -1 -13 4 42.47 3.20 1 -13 -4 43.74 2.98 1 -13 -5 16.90 2.02 1 -13 -5 19.29 2.29 1 -13 -5 18.95 1.81 -1 -13 5 19.23 2.46 -1 -13 5 21.52 3.42 1 -13 -5 17.51 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9 77.89 4.49 -2 -9 -9 84.81 3.60 2 -9 8 15.59 3.05 -2 -9 -8 16.13 1.74 2 9 -8 15.01 1.26 -2 9 8 13.80 3.50 -2 -9 -8 11.56 1.74 -2 -9 -8 14.42 1.45 2 -9 8 15.36 2.18 -2 -9 -8 16.44 4.06 2 9 -7 67.01 2.66 -2 9 7 72.24 7.75 2 -9 7 75.27 4.40 -2 -9 -7 75.89 4.29 2 -9 7 74.40 6.00 -2 -9 -7 63.74 7.99 -2 -9 -7 79.79 3.87 -2 -9 -6 68.16 3.98 2 9 -6 67.15 2.69 2 -9 6 67.95 5.50 2 -9 6 72.21 4.25 -2 9 6 65.99 7.26 -2 -9 -6 64.77 8.12 -2 -9 -6 71.04 3.70 2 9 -5 17.92 1.44 -2 9 5 13.98 3.36 -2 -9 -5 16.83 4.10 2 9 -4 2.48 0.86 -2 9 4 1.64 1.19 2 9 -3 42.97 2.27 -2 9 3 44.00 4.87 -2 -9 -3 47.19 6.56 -2 9 2 1.01 0.81 2 -9 2 0.69 1.13 -2 -9 -2 0.46 1.49 2 -9 1 153.00 9.92 -2 -9 -1 167.45 11.52 2 -9 0 74.05 7.04 -2 -9 0 70.22 6.73 2 -9 -1 165.51 11.08 -2 -9 1 142.91 9.05 2 9 1 154.21 7.59 -2 -9 2 1.62 1.22 2 9 2 1.03 0.79 2 -9 -2 0.98 1.46 2 9 3 40.52 4.78 2 -9 -3 41.13 5.56 2 -9 -4 3.85 2.11 -2 9 -4 2.28 0.41 -2 9 -5 18.63 1.09 2 9 5 22.64 4.04 2 -9 -5 18.56 3.82 2 -9 -6 72.80 4.30 2 -9 -6 68.97 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10.55 2.00 2 -10 -11 11.02 0.86 -2 -10 11 11.14 1.04 -2 -10 11 8.45 2.70 -2 -10 12 10.16 2.47 2 -10 -12 10.34 1.72 2 -10 -12 9.07 0.76 2 -10 -12 10.39 1.50 -2 -10 12 11.21 0.98 2 -10 -13 7.99 1.20 -2 -10 13 8.30 0.71 2 -10 -13 7.74 1.34 2 10 13 12.81 1.17 -2 -10 13 8.90 2.35 2 -10 -14 23.26 1.77 2 -10 -14 21.53 1.42 -2 -10 14 22.55 2.73 -2 -10 14 23.39 0.92 2 10 14 22.94 1.11 2 -10 -15 2.58 0.47 2 10 15 2.70 0.35 -2 -11 -14 0.46 0.45 2 -11 14 -0.53 0.67 -2 -11 -13 6.32 1.23 2 -11 13 7.06 1.55 -2 -11 -12 7.33 1.48 2 -11 12 5.18 1.67 -2 -11 -11 19.75 2.51 2 -11 11 19.88 3.55 -2 -11 -11 18.55 1.57 2 -11 11 19.37 1.87 -2 -11 -10 10.46 2.14 -2 -11 -10 10.35 1.48 -2 -11 -9 33.40 2.84 -2 -11 -9 30.21 3.27 -2 -11 -9 35.23 2.49 2 -11 9 29.66 2.89 2 -11 9 38.47 4.77 2 -11 8 94.98 5.32 -2 -11 -8 88.64 4.88 -2 -11 -8 81.72 5.19 -2 -11 -8 98.14 4.51 2 -11 8 103.81 7.81 -2 -11 -7 3.34 1.27 -2 -11 -7 2.66 1.06 2 -11 7 3.16 1.24 2 -11 7 5.31 2.44 -2 -11 -7 4.57 1.15 2 -11 6 206.55 8.18 -2 -11 -6 189.75 7.42 -2 -11 -6 171.43 6.58 2 -11 6 202.43 10.59 -2 -11 -6 192.43 6.80 2 11 -5 86.71 3.06 -2 -11 -5 85.06 5.03 -2 -11 -5 88.28 4.44 2 -11 5 86.93 5.20 -2 -11 -5 84.00 8.90 2 -11 5 96.94 7.35 -2 -11 -5 86.04 4.68 -2 -11 -4 96.80 5.26 2 -11 4 97.95 7.23 -2 -11 -4 91.78 9.04 2 11 -4 87.55 3.06 2 -11 4 94.63 5.30 -2 -11 -4 94.35 4.87 2 11 -3 32.78 1.96 -2 -11 -3 32.56 3.04 -2 -11 -3 34.08 2.98 -2 -11 -3 35.01 5.62 2 -11 3 37.81 4.36 2 -11 3 33.98 3.17 2 -11 2 39.17 2.52 2 11 -2 34.93 2.03 -2 -11 -2 36.62 3.08 2 -11 2 31.93 4.68 2 -11 2 39.88 4.49 -2 -11 -2 36.50 5.55 -2 -11 -2 39.72 3.15 -2 -11 -2 39.04 3.54 2 -11 2 38.04 3.22 -2 -11 -1 38.46 3.03 -2 -11 -1 34.36 3.23 2 11 -1 36.34 2.11 2 -11 1 38.35 2.63 2 -11 1 43.57 4.52 -2 -11 -1 35.09 5.10 2 -11 1 38.92 2.67 2 -11 1 37.00 3.02 -2 -11 -1 42.38 3.41 2 -11 1 40.44 5.35 -2 -11 0 60.74 3.63 -2 -11 0 60.35 6.45 2 -11 0 64.72 5.35 2 -11 0 65.68 6.93 2 -11 0 62.12 3.65 -2 -11 0 54.76 3.81 2 -11 0 60.62 3.42 -2 -11 0 63.48 3.98 2 -11 0 62.27 3.03 2 -11 0 71.17 3.78 2 -11 -1 42.29 2.92 2 -11 -1 54.98 3.39 2 -11 -1 35.86 2.74 -2 -11 1 35.37 3.04 -2 -11 1 39.67 2.82 2 -11 -1 44.01 5.83 -2 -11 1 39.86 4.95 2 -11 -1 43.08 2.74 2 -11 -1 41.34 3.07 -2 -11 1 42.19 3.31 2 -11 -2 38.78 2.85 2 -11 -2 37.52 2.67 -2 -11 2 42.08 3.26 2 -11 -2 40.08 2.72 2 -11 -2 37.92 2.47 2 -11 -2 39.32 5.61 -2 -11 2 39.88 3.21 2 -11 -2 36.46 2.83 2 -11 -3 37.39 2.70 2 -11 -3 34.77 2.79 2 -11 -3 37.52 2.82 2 -11 -3 37.69 5.35 -2 -11 3 36.45 3.03 2 -11 -3 33.58 2.84 -2 -11 3 31.29 2.84 2 -11 -4 93.40 4.62 2 -11 -4 91.09 4.65 -2 -11 4 98.05 4.97 -2 -11 4 95.18 5.99 2 -11 -4 85.96 8.01 2 -11 -4 95.34 4.40 2 -11 -4 90.72 4.77 -2 -11 4 88.95 4.76 2 -11 -5 93.85 5.02 2 -11 -5 93.12 4.91 2 -11 -5 87.13 4.52 -2 -11 5 91.86 6.25 -2 -11 5 94.71 4.87 2 -11 -5 94.16 4.52 2 -11 -5 87.42 8.12 -2 -11 5 88.34 4.73 2 11 5 78.05 6.83 2 -11 -6 201.65 7.54 -2 -11 6 172.69 6.48 2 -11 -6 194.81 6.68 -2 -11 6 193.42 9.45 -2 -11 6 204.40 6.88 2 -11 -6 201.26 6.78 -2 -11 6 199.41 4.10 2 -11 -6 203.88 7.46 2 -11 -7 3.18 1.14 -2 -11 7 5.98 2.28 2 -11 -7 4.64 1.41 2 -11 -7 5.24 1.21 -2 -11 7 3.49 0.99 -2 -11 7 5.21 1.26 2 -11 -7 4.99 1.48 -2 -11 7 4.33 0.70 2 -11 -8 96.20 4.36 2 -11 -8 96.17 5.54 -2 -11 8 95.66 2.89 2 -11 -8 97.51 5.21 2 -11 -8 98.38 4.78 -2 -11 8 95.56 7.23 -2 -11 8 97.02 4.29 -2 -11 8 91.36 4.20 2 -11 -9 35.44 2.44 2 -11 -9 34.99 2.89 2 -11 -9 32.22 3.03 -2 -11 9 36.51 4.66 -2 -11 9 34.43 1.74 2 -11 -9 37.31 3.40 2 -11 -10 11.02 1.20 2 -11 -10 10.98 1.59 2 -11 -10 11.76 1.97 2 -11 -11 18.41 2.21 -2 -11 11 19.42 3.40 2 -11 -11 18.20 1.83 -2 -11 11 19.29 1.15 2 -11 -12 7.28 1.37 -2 -11 12 6.66 0.60 -2 -11 12 4.43 1.74 2 -11 -12 5.99 1.00 2 11 13 7.06 0.63 2 -11 -13 7.96 1.16 -2 -11 13 8.44 1.87 2 -11 -13 6.20 0.82 2 -11 -14 1.39 0.48 -2 -11 14 0.18 0.78 2 11 14 0.95 0.24 2 -12 13 36.11 2.61 -2 -12 -13 38.10 2.01 2 -12 12 81.29 4.89 -2 -12 -12 74.46 3.43 -2 -12 -11 33.76 1.77 -2 -12 -11 37.70 2.87 2 -12 11 31.69 2.01 2 -12 11 37.99 3.98 -2 -12 -10 3.86 0.93 2 -12 10 4.87 1.10 2 -12 10 4.38 1.96 -2 -12 -10 4.08 1.26 -2 -12 -9 0.53 0.94 -2 -12 -9 1.20 0.79 2 -12 9 1.47 0.93 2 -12 9 1.11 1.66 -2 -12 -9 1.02 0.71 -2 -12 -8 15.33 2.16 2 -12 8 15.25 3.17 -2 -12 -8 15.28 2.01 -2 -12 -8 16.74 1.91 2 -12 8 13.58 2.09 -2 -12 -7 5.19 1.42 -2 -12 -7 5.84 1.43 2 -12 7 5.81 1.50 2 -12 7 8.36 2.67 -2 -12 -7 6.47 1.32 -2 -12 -6 38.29 3.18 -2 -12 -6 38.49 2.97 2 -12 6 44.66 3.82 2 -12 6 44.27 5.11 -2 -12 -6 40.29 3.53 -2 -12 -5 8.69 1.78 2 -12 5 7.91 2.29 2 -12 5 7.83 1.76 -2 -12 -5 7.89 1.65 -2 -12 -4 79.01 4.97 2 -12 4 80.67 5.08 2 -12 4 89.85 7.08 -2 -12 -4 80.28 4.79 2 -12 3 34.26 4.48 2 -12 3 31.06 2.14 2 -12 3 36.13 3.28 -2 -12 -3 32.29 3.07 -2 -12 -3 32.02 3.15 -2 -12 -2 22.09 2.60 2 -12 2 24.46 3.70 2 -12 2 25.19 2.79 2 -12 2 22.63 2.00 -2 -12 -2 21.73 2.57 2 12 -1 32.69 1.97 2 -12 1 36.44 2.67 2 -12 1 36.43 3.18 -2 -12 -1 37.65 3.20 2 -12 1 40.80 4.73 -2 -12 -1 38.18 3.87 -2 -12 -1 35.80 5.14 2 -12 1 40.15 5.37 2 -12 1 39.17 2.75 -2 -12 -1 39.10 3.37 2 12 0 92.23 3.28 2 -12 0 113.99 4.85 2 -12 0 109.00 3.98 2 -12 0 101.95 8.49 -2 -12 0 92.99 5.38 -2 -12 0 103.38 8.05 -2 -12 0 97.98 4.76 -2 -12 0 105.17 5.49 2 -12 0 104.39 4.62 2 -12 0 96.50 4.73 2 -12 0 111.19 7.42 -2 -12 1 36.80 3.29 2 -12 -1 40.31 3.00 2 -12 -1 38.41 2.57 -2 -12 1 35.87 2.69 2 -12 -1 36.85 2.73 2 -12 -1 38.30 3.00 2 -12 -2 23.78 2.16 2 -12 -2 26.69 2.40 2 -12 -2 24.91 2.51 2 -12 -2 26.36 2.25 -2 -12 2 19.88 2.69 -2 -12 2 24.11 2.71 2 -12 -2 25.48 2.57 2 -12 -3 33.69 2.69 2 -12 -3 35.52 2.94 2 -12 -3 31.88 2.87 -2 -12 3 34.49 3.18 -2 -12 3 43.17 3.66 2 -12 -3 35.47 2.76 2 -12 -4 88.67 4.72 -2 -12 4 87.82 5.06 2 -12 -4 85.70 4.51 2 -12 -4 93.15 4.48 -2 -12 4 91.16 5.88 2 -12 -4 88.74 4.94 -2 -12 4 78.15 4.67 2 -12 -5 8.91 1.59 -2 -12 5 6.76 1.41 2 -12 -5 7.49 1.48 -2 -12 5 8.29 2.25 -2 -12 5 8.28 1.88 2 -12 -5 8.34 1.47 2 -12 -5 8.63 1.71 2 -12 -6 44.68 3.51 2 -12 -6 41.03 3.23 -2 -12 6 42.63 3.50 -2 -12 6 40.46 4.32 2 -12 -6 44.36 3.57 2 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2.28 -2 -13 -8 25.64 2.44 2 -13 8 27.77 3.79 2 -13 8 29.33 2.70 -2 -13 -8 26.90 2.27 2 -13 7 35.78 3.17 -2 -13 -7 39.31 3.19 2 -13 7 41.25 4.66 -2 -13 -7 39.19 2.71 -2 -13 -7 42.73 3.07 -2 -13 -6 29.14 2.91 2 -13 6 30.60 4.18 2 -13 6 28.00 2.94 -2 -13 -6 29.09 2.73 2 -13 5 7.62 2.67 -2 -13 -5 8.33 1.84 2 -13 5 6.56 1.68 -2 -13 -5 7.86 1.65 2 -13 4 89.81 7.01 -2 -13 -4 86.60 5.12 -2 -13 -4 81.56 4.81 2 -13 4 76.71 4.89 -2 -13 -3 2.37 1.23 2 -13 3 0.50 1.62 2 -13 3 1.86 1.06 2 -13 3 0.81 0.52 -2 -13 -3 1.33 1.25 2 -13 2 52.58 2.96 -2 -13 -2 48.93 3.86 -2 -13 -2 50.27 3.83 2 -13 2 53.58 5.51 2 -13 2 46.20 3.64 2 -13 2 54.74 3.07 2 -13 1 30.01 2.42 -2 -13 -1 24.33 2.60 2 -13 1 25.54 2.36 -2 -13 -1 26.99 3.00 2 -13 1 27.62 3.93 2 -13 1 29.70 2.88 2 -13 0 0.06 0.71 -2 -13 0 0.14 0.84 2 -13 0 0.26 0.70 -2 -13 0 0.19 0.72 2 -13 0 0.12 0.70 -2 -13 0 -0.87 2.72 2 -13 -1 27.75 2.56 2 -13 -1 30.24 2.15 2 -13 -1 26.11 2.57 2 -13 -1 25.60 2.31 -2 -13 1 25.35 3.53 -2 -13 1 28.96 3.07 -2 -13 1 25.76 2.28 2 -13 -2 48.02 3.46 2 -13 -2 51.28 2.99 -2 -13 2 50.34 3.90 -2 -13 2 50.10 4.19 2 -13 -2 48.98 2.91 2 -13 -2 48.79 3.56 2 -13 -3 2.49 1.07 -2 -13 3 2.88 1.93 -2 -13 3 3.48 1.30 2 -13 -3 1.71 0.79 2 -13 -3 0.09 0.75 2 -13 -4 89.37 4.44 2 -13 -4 91.58 4.71 -2 -13 4 90.29 5.67 2 -13 -4 95.63 4.43 -2 -13 4 84.09 4.84 2 -13 -4 85.55 4.76 -2 -13 4 83.65 5.14 -2 -13 5 6.45 1.40 2 -13 -5 8.75 1.57 2 -13 -5 6.66 1.42 -2 -13 5 6.58 1.85 -2 -13 5 5.04 2.02 2 -13 -5 8.52 1.50 2 -13 -5 7.85 1.59 2 -13 -6 29.43 2.48 2 -13 -6 27.90 2.86 2 -13 -6 29.77 2.59 -2 -13 6 28.75 2.58 2 -13 -6 31.27 2.72 -2 -13 6 29.06 3.52 -2 -13 6 30.94 3.12 2 -13 -7 39.46 2.72 2 -13 -7 44.15 3.29 2 -13 -7 43.90 3.02 -2 -13 7 38.48 4.14 -2 -13 7 42.94 2.78 2 -13 -7 38.19 3.15 -2 -13 7 45.94 3.34 2 -13 -8 28.07 2.16 2 -13 -8 29.45 2.29 2 -13 -8 27.93 2.65 2 -13 -8 29.22 2.62 -2 -13 8 27.96 3.56 -2 -13 8 30.22 2.56 2 -13 -9 44.28 2.44 2 -13 -9 46.50 2.45 2 -13 -9 51.73 3.32 2 -13 -9 45.43 3.11 -2 -13 9 43.98 4.22 2 -13 -10 15.39 1.14 2 -13 -10 14.98 1.28 -2 -13 10 15.87 2.50 2 -13 -10 16.85 1.78 -2 -13 11 15.91 2.12 2 -13 -11 15.69 1.54 2 13 11 14.36 0.68 2 -13 -12 5.47 0.87 -2 -13 12 5.02 1.12 2 -14 11 44.63 2.77 -2 -14 -10 3.79 0.58 -2 -14 -10 3.51 0.61 2 -14 10 3.40 1.20 2 -14 10 4.16 0.74 -2 -14 -9 0.59 0.47 -2 -14 -9 1.17 0.57 2 -14 9 0.90 1.38 2 -14 9 1.08 0.71 -2 -14 -9 0.95 0.46 -2 -14 -8 75.86 3.26 -2 -14 -8 79.65 3.60 2 -14 8 84.83 5.74 -2 -14 -8 74.98 2.78 2 -14 8 72.99 3.71 2 -14 7 15.39 1.94 -2 -14 -7 20.05 2.16 -2 -14 -7 18.70 1.99 2 -14 7 14.73 2.76 2 -14 6 10.77 2.56 2 -14 6 10.18 1.80 -2 -14 -6 11.11 1.78 -2 -14 -6 10.70 1.64 -2 -14 -5 1.71 1.06 -2 -14 -5 0.81 0.91 2 -14 5 1.17 1.54 2 -14 5 2.89 1.21 -2 -14 -4 1.64 0.90 2 -14 4 0.36 1.93 -2 -14 -4 2.27 1.03 2 -14 4 3.42 1.29 -2 -14 -3 18.74 2.34 2 -14 3 21.00 2.51 2 -14 3 18.86 3.11 -2 -14 -3 19.57 2.44 2 -14 2 172.00 4.97 -2 -14 -2 175.45 6.65 2 -14 2 173.91 9.33 2 -14 2 164.96 6.69 2 -14 2 172.39 5.03 -2 -14 -2 167.89 6.91 2 -14 1 13.13 2.02 2 -14 1 13.27 1.61 -2 -14 -1 17.04 3.02 -2 -14 -1 14.31 2.46 2 -14 1 11.29 1.56 2 -14 0 369.69 8.53 -2 -14 0 362.24 10.17 -2 -14 0 345.54 8.39 2 -14 0 364.22 8.99 2 -14 0 338.66 8.33 2 -14 -1 16.72 1.61 2 -14 -1 14.13 2.06 -2 -14 1 15.74 2.29 -2 -14 1 11.81 1.50 2 -14 -1 12.24 1.89 2 -14 -2 182.51 6.36 2 -14 -2 174.36 5.20 2 -14 -2 174.55 4.98 2 -14 -2 160.08 6.20 -2 -14 2 172.96 7.49 -2 -14 2 169.81 6.92 -2 -14 3 18.50 2.22 2 -14 -3 16.84 2.22 2 -14 -3 19.18 1.82 -2 -14 3 16.33 3.09 2 -14 -3 19.43 2.16 2 -14 -4 3.13 1.09 2 -14 -4 2.57 0.86 -2 -14 4 1.20 0.87 2 -14 -4 0.89 0.90 2 -14 -5 2.08 0.91 2 -14 -5 1.43 0.74 -2 -14 5 1.66 0.78 -2 -14 5 1.23 2.11 -2 -14 5 2.51 1.18 2 -14 -5 1.61 0.91 2 -14 -6 12.27 1.59 -2 -14 6 9.99 1.86 -2 -14 6 12.26 2.45 2 -14 -6 11.26 1.56 -2 -14 6 10.17 1.40 2 -14 -6 11.17 1.68 2 -14 -7 21.20 1.96 -2 -14 7 15.09 1.39 -2 -14 7 12.54 2.17 2 -14 -7 17.86 2.17 2 -14 -7 19.73 2.01 2 -14 -8 78.96 3.23 2 -14 -8 83.42 3.71 -2 -14 8 79.32 4.76 2 -14 -8 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4 -12 68.61 2.72 4 -4 -12 73.80 3.08 -4 -4 12 67.92 3.02 4 -4 -13 37.89 3.34 4 4 13 38.26 2.71 -4 4 -13 37.60 2.02 4 -4 -13 40.23 2.22 -4 -4 13 40.56 1.97 -4 -4 13 37.13 2.21 4 -4 -14 12.43 2.02 4 4 14 13.00 1.52 -4 -4 14 12.28 3.04 -4 -4 14 14.07 1.10 -4 4 -14 14.67 1.23 -4 -4 14 12.45 1.31 4 4 14 13.25 1.15 4 -4 -14 12.10 1.25 -4 -4 15 12.13 0.84 4 4 15 11.49 1.21 4 -4 -15 12.39 1.16 -4 -4 15 9.95 2.45 -4 4 -15 13.62 1.11 -4 -4 15 13.15 1.22 4 4 15 13.22 1.05 4 -4 -15 11.28 1.68 4 -4 -16 5.76 0.73 4 -4 -16 5.10 1.14 -4 -4 16 4.62 1.62 -4 4 -16 5.67 0.64 -4 -4 16 5.57 0.73 4 4 16 5.01 0.60 4 -4 -17 14.51 1.26 -4 -4 17 13.96 1.83 -4 4 -17 14.80 0.71 4 -4 -17 14.56 0.82 -4 -4 17 15.87 0.87 4 4 17 13.61 0.68 -4 5 17 5.59 0.47 -4 -5 -17 5.94 0.65 -4 5 16 9.82 0.81 4 5 -16 9.88 1.01 -4 -5 -16 9.84 1.15 -4 -5 -16 9.13 0.58 -4 5 15 15.95 1.15 4 5 -15 15.01 1.51 4 -5 15 15.82 1.67 4 -5 15 11.75 2.13 -4 -5 -15 15.69 1.65 -4 -5 -15 13.43 0.87 4 -5 14 46.75 4.16 4 -5 14 55.14 3.33 -4 -5 -14 56.74 3.37 -4 -5 -14 54.69 1.90 4 -5 13 26.33 2.48 4 -5 13 19.58 2.89 -4 -5 -13 24.94 2.42 -4 -5 -13 22.98 1.33 4 -5 12 39.36 3.07 4 -5 12 33.86 3.53 -4 -5 -12 40.93 3.14 -4 -5 -12 40.09 1.73 4 -5 11 87.19 4.43 4 -5 11 85.93 5.39 -4 -5 -11 86.33 4.48 -4 -5 -11 84.71 2.50 4 -5 11 85.55 4.34 4 5 -10 74.32 2.34 4 -5 10 80.32 4.12 4 -5 10 85.66 4.92 -4 5 10 71.72 7.14 -4 -5 -10 78.18 4.13 -4 -5 -10 83.12 3.03 4 -5 10 87.94 4.57 4 5 -9 22.14 1.32 4 -5 9 23.81 2.20 4 -5 9 23.39 2.38 -4 -5 -9 24.24 1.59 -4 -5 -9 21.53 2.06 4 -5 9 21.57 2.33 -4 5 9 18.88 3.78 -4 5 8 1.44 1.41 4 5 -8 1.35 0.46 -4 -5 -8 1.10 0.45 4 5 -7 94.37 2.74 -4 5 7 92.10 7.61 4 5 -6 -0.19 0.42 -4 5 6 2.44 1.80 4 5 -5 84.14 2.66 -4 5 5 45.30 5.03 4 5 -4 141.79 3.53 -4 5 4 131.52 8.15 -4 5 3 55.36 5.17 4 5 -3 61.83 4.52 -4 5 2 33.28 3.94 4 5 -2 32.61 3.37 4 -5 1 17.76 1.61 4 5 -1 15.43 2.52 -4 5 1 17.04 3.00 4 5 0 30.51 3.66 4 -5 0 39.27 2.47 4 5 1 20.97 3.29 4 -5 -1 18.36 1.75 4 -5 -2 31.99 2.15 4 -5 -2 36.82 4.24 -4 -5 2 29.77 3.06 4 5 2 33.24 4.08 4 -5 -3 57.50 5.15 4 5 3 54.51 5.36 -4 5 -4 141.45 2.29 4 -5 -4 142.27 7.89 4 5 4 136.90 8.84 4 -5 -5 45.48 4.31 4 5 5 44.01 5.33 -4 5 -6 0.76 0.37 4 5 6 0.53 0.96 -4 5 -7 92.43 2.50 -4 -5 7 100.70 6.12 4 5 7 96.42 8.32 -4 5 -8 1.43 0.42 4 -5 -8 -0.03 0.82 4 5 8 1.23 1.36 4 -5 -8 1.40 0.55 -4 -5 8 1.42 0.53 4 -5 -9 20.37 2.27 -4 5 -9 21.07 1.41 4 -5 -9 22.38 2.10 4 5 9 22.05 1.92 4 5 9 19.75 3.91 4 -5 -9 22.35 1.57 -4 -5 9 25.60 1.52 -4 -5 9 22.33 1.62 -4 -5 10 86.57 2.77 4 -5 -10 74.68 4.50 -4 5 -10 71.73 2.65 4 5 10 78.62 3.60 4 -5 -10 78.16 3.01 4 5 10 76.57 7.42 -4 -5 10 79.05 3.15 -4 5 -11 90.83 3.08 4 -5 -11 81.85 4.84 4 5 11 80.54 3.75 4 -5 -11 89.73 3.27 -4 -5 11 93.32 2.87 -4 -5 11 84.56 3.40 -4 -5 12 43.00 1.93 4 -5 -12 38.51 3.41 4 5 12 36.56 2.53 -4 -5 12 36.20 4.87 4 -5 -12 40.85 2.27 -4 5 -12 39.52 2.06 -4 -5 12 42.17 2.42 4 -5 -13 20.20 2.49 -4 -5 13 25.89 1.39 4 5 13 20.68 1.84 4 -5 -13 23.27 1.70 -4 -5 13 22.90 4.02 -4 5 -13 25.05 1.62 -4 -5 13 24.75 1.81 -4 -5 14 57.75 1.87 4 -5 -14 53.53 3.64 4 5 14 47.91 2.46 -4 5 -14 57.72 2.24 -4 -5 14 50.98 5.26 4 -5 -14 53.11 2.39 -4 -5 14 52.62 2.47 4 5 14 59.35 2.32 4 -5 -15 12.76 1.71 -4 -5 15 13.05 2.75 -4 5 -15 15.11 1.06 -4 -5 15 13.87 1.20 4 5 15 15.17 1.09 4 -5 -15 14.44 1.20 4 -5 -16 8.89 1.25 4 -5 -16 9.80 0.83 -4 5 -16 9.45 0.68 -4 -5 16 9.37 1.97 -4 -5 16 9.80 0.86 4 5 16 10.19 0.79 4 -5 -17 4.54 0.68 -4 -5 17 5.34 1.14 4 -5 -17 5.30 0.47 -4 -5 17 5.88 0.50 4 5 17 5.00 0.41 -4 6 16 1.01 0.34 4 6 -16 1.18 0.44 -4 -6 -16 0.26 0.35 -4 6 15 1.01 0.39 -4 -6 -15 1.37 0.64 4 -6 14 47.69 2.94 -4 -6 -14 47.58 2.92 4 6 -14 46.76 1.43 4 -6 13 1.81 1.39 4 -6 13 2.37 0.85 -4 -6 -13 2.42 0.95 4 -6 12 38.20 2.98 4 -6 12 36.75 3.60 4 -6 12 31.76 2.63 -4 -6 -12 37.28 2.98 4 -6 11 94.99 4.61 4 -6 11 111.02 6.34 4 -6 11 103.28 5.07 4 -6 10 62.63 3.66 4 -6 10 69.93 4.54 -4 -6 -10 62.48 3.69 4 -6 10 66.34 4.19 -4 -6 -9 125.75 3.68 4 6 -9 115.66 3.12 4 -6 9 126.06 4.79 -4 6 9 104.80 8.24 4 -6 9 130.89 5.54 4 -6 9 131.64 5.81 -4 -6 -9 102.93 10.24 -4 -6 -9 121.82 4.83 4 6 -8 10.07 0.95 4 -6 8 13.42 1.76 4 -6 8 9.62 1.34 -4 6 8 11.24 2.69 4 -6 8 9.27 1.64 -4 -6 -8 9.75 1.33 -4 -6 -8 10.63 1.07 -4 6 7 5.99 2.12 4 6 -7 6.40 0.81 -4 6 6 36.74 4.69 4 6 -6 37.83 1.94 4 6 -5 9.30 0.98 -4 6 5 9.39 2.40 4 6 -4 19.92 1.46 -4 6 4 19.05 3.24 -4 6 3 84.81 6.45 4 6 -3 88.69 5.28 4 6 -2 52.23 4.25 -4 6 2 52.09 4.98 4 6 -1 123.00 6.91 -4 6 1 121.47 7.97 4 6 0 170.79 8.45 -4 -6 0 173.95 9.73 -4 -6 1 124.14 7.47 4 6 1 132.64 7.86 4 -6 -2 59.83 5.74 4 6 2 50.69 5.10 -4 -6 2 60.97 4.47 4 6 3 91.73 7.25 4 -6 -3 92.61 6.98 4 6 4 20.48 3.63 4 -6 -4 17.87 2.99 4 6 5 10.48 2.78 4 -6 -5 9.99 2.32 4 -6 -6 38.44 4.03 4 6 6 32.45 4.88 -4 6 -7 6.05 0.68 4 6 7 5.79 2.18 -4 6 -8 10.67 0.93 4 -6 -8 9.24 1.65 4 6 8 6.80 2.11 4 6 8 11.47 1.37 4 -6 -8 11.53 1.73 4 -6 -8 11.47 1.08 -4 -6 8 7.86 2.33 -4 -6 8 9.92 1.11 4 -6 -9 120.54 5.58 -4 6 -9 114.93 3.06 4 -6 -9 128.42 5.33 4 6 9 126.68 4.43 4 -6 -9 125.09 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1.38 4 7 -14 3.67 0.47 -4 -7 -14 3.30 0.87 4 -7 13 3.22 1.50 4 -7 13 4.62 1.07 -4 -7 -13 3.64 0.96 4 -7 12 14.49 1.80 4 -7 12 13.07 2.25 -4 -7 -12 13.83 1.76 4 -7 12 12.20 1.66 4 -7 11 1.99 0.90 4 -7 11 3.28 1.42 4 -7 11 3.97 1.13 -4 -7 -11 2.43 0.88 4 -7 10 28.24 2.46 4 -7 10 25.46 2.69 4 -7 10 27.14 2.83 4 -7 10 21.30 2.89 -4 -7 -10 24.64 2.30 4 -7 9 41.97 2.85 4 -7 9 42.07 3.26 4 -7 9 44.00 4.18 -4 -7 -9 41.38 2.20 -4 -7 -9 39.19 2.75 4 -7 9 40.65 3.52 4 7 -8 66.75 2.46 4 -7 8 73.50 3.49 -4 7 8 62.44 6.02 4 -7 8 78.63 3.99 4 -7 8 65.98 4.94 4 -7 8 77.85 4.67 -4 -7 -8 70.05 2.69 -4 -7 -8 68.59 3.38 -4 -7 -8 63.93 8.33 4 7 -7 4.12 0.70 4 -7 7 4.58 1.07 4 -7 7 4.10 1.53 -4 -7 -7 4.29 0.76 -4 7 7 5.90 2.16 4 -7 7 3.26 1.25 -4 -7 -7 4.94 1.06 -4 -7 -7 3.37 2.49 4 7 -6 25.06 1.61 -4 7 6 28.01 3.96 4 -7 6 29.47 2.76 -4 -7 -6 26.62 5.45 4 7 -5 17.75 1.40 -4 7 5 17.04 3.16 -4 -7 -5 18.32 4.44 4 7 -4 71.28 2.83 -4 7 4 65.45 5.81 -4 -7 -4 72.32 8.21 -4 7 3 96.33 6.90 -4 -7 -3 98.15 9.10 4 7 -2 10.27 1.89 -4 7 2 8.38 2.12 -4 -7 -2 7.15 2.64 -4 7 1 51.82 5.03 4 7 -1 55.30 4.62 -4 -7 -1 55.69 6.22 4 7 0 37.85 4.17 -4 -7 0 38.54 4.84 -4 7 0 37.38 4.27 4 7 1 61.93 5.64 4 -7 -1 60.92 6.19 -4 -7 1 55.85 5.16 4 -7 -2 8.03 2.27 4 7 2 9.95 2.46 4 -7 -3 110.70 8.09 4 7 3 103.68 8.06 4 -7 -4 75.20 6.61 4 7 4 66.23 6.60 4 7 5 17.86 3.68 4 -7 -5 15.77 2.92 4 -7 -6 25.32 2.39 4 -7 -6 27.43 3.74 4 7 6 21.93 4.21 -4 -7 6 27.43 1.66 4 -7 -7 3.71 1.09 4 -7 -7 3.95 1.06 4 7 7 2.22 1.79 -4 -7 7 2.75 1.41 4 -7 -7 3.55 0.67 4 7 7 5.01 0.98 4 -7 -7 3.04 1.14 -4 -7 7 4.38 0.77 4 -7 -8 71.86 4.37 4 -7 -8 73.11 4.16 4 7 8 72.16 3.21 -4 -7 8 64.98 5.65 4 7 8 69.10 7.53 4 -7 -8 72.49 2.66 -4 -7 8 68.68 2.87 4 -7 -9 38.23 3.38 4 -7 -9 39.26 3.13 4 7 9 36.60 2.40 -4 -7 9 33.35 4.56 4 -7 -9 39.10 2.09 -4 -7 9 36.59 2.24 4 -7 -10 22.48 2.66 4 -7 -10 23.47 2.46 4 7 10 23.08 1.91 -4 -7 10 25.33 1.90 -4 7 -10 24.95 1.49 4 -7 -10 25.03 1.75 -4 -7 10 22.10 3.89 4 -7 -11 4.14 1.41 4 -7 -11 1.92 0.82 4 7 11 3.10 0.86 4 -7 -11 3.05 0.80 -4 -7 11 3.44 0.90 -4 7 -11 2.85 0.64 4 -7 -12 13.88 2.05 4 -7 -12 13.06 1.68 -4 7 -12 14.44 1.13 4 -7 -12 14.19 1.32 -4 -7 12 10.06 2.87 -4 -7 12 15.48 1.50 4 -7 -13 3.98 1.33 4 -7 -13 4.28 0.82 4 -7 -13 4.46 0.87 -4 -7 13 3.89 0.83 -4 7 -13 4.55 0.65 -4 -7 13 3.37 1.82 4 -7 -14 2.67 1.03 -4 -7 14 3.73 1.78 -4 -7 14 3.44 0.69 4 -7 -14 3.27 0.63 -4 7 -14 3.15 0.51 4 7 14 3.42 0.65 -4 7 -15 1.03 0.27 4 -7 -15 0.36 0.56 4 -7 -15 0.83 0.39 -4 -7 15 1.15 1.39 -4 -7 15 1.03 0.41 4 7 15 1.03 0.38 4 -7 -16 4.86 0.76 -4 -7 16 4.59 1.12 -4 -7 16 4.68 0.48 4 7 16 4.28 0.45 -4 -8 -16 1.57 0.43 -4 8 15 10.67 0.59 -4 -8 -15 9.43 1.35 -4 -8 -15 12.60 1.06 4 8 -14 6.43 0.56 -4 -8 -14 7.36 1.01 -4 8 14 6.48 0.59 4 -8 13 6.82 1.53 -4 -8 -13 8.52 1.23 4 -8 12 18.29 2.46 -4 -8 -12 22.06 2.05 4 -8 12 23.21 2.61 4 -8 12 17.74 1.86 4 -8 11 0.39 0.70 4 -8 11 0.70 0.90 4 -8 11 1.02 0.80 4 -8 11 2.09 1.18 -4 -8 -11 1.75 0.78 4 -8 10 84.26 4.03 4 -8 10 76.89 4.60 4 -8 10 83.28 4.92 4 -8 10 80.44 5.69 -4 -8 -10 83.95 4.01 -4 -8 -10 73.95 3.92 4 -8 9 57.15 3.18 -4 -8 -9 50.20 3.51 4 -8 9 52.90 3.60 4 -8 9 56.02 4.84 4 -8 9 56.50 4.19 -4 -8 -9 57.37 3.18 4 -8 8 99.47 4.01 4 -8 8 109.16 6.76 4 -8 8 103.28 4.58 -4 -8 -8 104.84 3.36 -4 -8 -8 98.25 3.97 4 -8 8 97.30 5.50 4 8 -7 2.92 0.62 4 -8 7 1.80 0.74 4 -8 7 2.02 1.45 -4 -8 -7 1.95 0.76 -4 -8 -7 -0.17 1.57 4 -8 7 1.53 1.11 -4 -8 -7 2.65 0.71 4 8 -6 17.53 1.43 4 -8 6 18.20 1.67 -4 -8 -6 20.01 1.57 -4 8 6 17.58 3.07 4 -8 6 15.32 2.48 4 -8 6 17.07 2.28 -4 -8 -6 15.26 4.25 -4 8 5 20.28 3.18 4 -8 5 26.21 3.25 4 8 -5 23.41 1.66 4 -8 5 25.12 2.64 -4 -8 -5 25.07 1.45 -4 -8 -5 23.73 5.22 -4 -8 -5 24.87 1.46 4 8 -4 144.53 4.20 -4 8 4 152.62 8.48 -4 -8 -4 147.73 12.03 4 8 -3 2.93 0.81 -4 -8 -3 2.15 1.80 -4 8 3 2.43 1.39 -4 8 2 118.65 7.39 -4 -8 -2 118.04 9.72 -4 8 1 1.45 0.84 4 8 -1 1.56 1.04 -4 -8 -1 1.19 1.35 -4 -8 0 55.32 5.77 4 8 0 58.91 5.02 -4 8 0 56.20 5.17 4 -8 -1 2.68 1.61 4 8 1 1.70 1.09 -4 -8 1 1.44 1.02 4 -8 -2 127.03 9.18 4 8 2 125.22 8.43 4 8 3 1.44 1.29 4 -8 -3 2.82 1.68 4 -8 -4 154.65 9.74 4 8 4 149.95 10.04 4 -8 -5 23.85 2.04 4 -8 -5 22.02 2.25 4 -8 -5 23.98 2.32 4 8 5 23.05 4.26 4 -8 -5 23.03 1.38 4 -8 -5 21.72 3.55 -4 -8 5 25.01 1.59 4 -8 -5 23.76 2.32 4 -8 -6 16.12 2.05 4 -8 -6 16.73 1.76 4 -8 -6 18.80 2.18 4 -8 -6 16.10 2.04 4 8 6 14.47 1.50 4 8 6 15.35 3.64 4 -8 -6 16.13 1.21 4 -8 -6 17.10 3.12 -4 -8 6 16.56 1.35 4 -8 -7 2.29 1.21 4 -8 -7 3.12 1.06 4 -8 -7 2.14 0.80 4 8 7 0.68 1.08 -4 -8 7 1.23 1.49 4 8 7 2.20 0.71 -4 -8 7 1.19 0.59 4 -8 -7 1.52 0.54 4 -8 -7 1.87 0.99 -4 -8 8 89.21 6.60 4 -8 -8 100.26 5.28 4 -8 -8 104.37 5.23 4 -8 -8 108.18 3.90 4 8 8 99.35 3.71 4 -8 -8 102.29 3.17 -4 -8 8 95.39 3.50 -4 -8 9 57.54 2.77 -4 -8 9 52.77 5.43 4 -8 -9 58.56 4.21 4 -8 -9 59.70 4.00 4 8 9 60.03 2.88 4 -8 -9 55.32 2.44 4 -8 -10 89.07 5.17 4 -8 -10 85.98 4.68 -4 -8 10 75.37 6.64 -4 -8 10 80.52 3.28 4 -8 -10 85.66 3.04 -4 8 -10 85.30 2.49 4 -8 -11 2.09 1.89 4 -8 -11 1.97 1.36 -4 -8 11 4.05 2.07 4 -8 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47.72 4.10 4 -9 7 43.41 4.52 -4 -9 -7 55.32 2.44 -4 9 6 6.87 2.59 4 9 -6 10.17 1.07 -4 -9 -6 10.98 1.14 -4 -9 -6 14.93 4.97 4 -9 6 10.34 1.98 4 -9 6 12.08 2.58 -4 -9 -5 70.54 8.53 4 9 -5 76.38 2.93 4 -9 5 73.57 5.75 4 -9 5 70.15 4.67 -4 -9 -5 79.35 2.57 -4 -9 -5 74.55 3.65 -4 -9 -4 19.83 2.04 4 9 -4 19.63 1.72 4 -9 4 20.77 1.82 -4 -9 -4 22.10 1.29 4 -9 4 23.78 3.25 -4 -9 -4 17.13 4.22 4 -9 4 19.43 2.46 -4 -9 -4 20.35 1.28 4 9 -3 41.29 2.32 4 -9 3 47.23 2.59 4 -9 3 48.75 2.77 4 -9 3 47.37 4.49 4 -9 3 41.46 3.23 -4 -9 -3 42.76 6.24 -4 -9 -3 43.06 2.98 -4 -9 -3 48.04 1.82 4 -9 2 1.00 0.73 4 -9 2 0.51 0.68 4 -9 2 2.45 1.76 -4 -9 -2 -0.48 0.74 -4 -9 -2 -0.18 1.38 -4 9 1 93.36 6.42 4 -9 1 100.34 4.27 4 -9 1 102.67 6.52 -4 -9 -1 92.95 8.46 4 -9 0 9.47 1.37 -4 9 0 8.11 1.93 -4 -9 0 9.41 2.61 4 -9 -1 97.81 4.32 4 9 1 96.56 6.77 4 -9 -1 109.11 4.49 4 -9 -1 104.32 4.61 4 -9 -2 1.23 0.90 4 -9 -2 0.15 0.70 4 -9 -2 1.14 0.75 4 -9 -2 1.86 1.93 4 9 2 0.75 0.92 4 -9 -3 45.23 3.09 4 -9 -3 43.96 2.90 4 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-9 -11 8.88 1.01 4 -9 -12 2.93 1.13 4 -9 -12 4.65 1.17 -4 -9 12 0.56 1.38 4 -9 -12 2.93 0.67 -4 -9 12 1.52 0.53 4 -9 -13 0.54 0.67 4 -9 -13 -0.56 0.50 -4 -9 13 0.84 1.28 -4 -9 13 0.47 0.44 4 -9 -14 7.20 1.06 4 -9 -14 6.15 0.68 -4 -9 14 6.82 1.58 -4 -9 14 7.39 0.68 4 9 14 6.82 0.70 4 -9 -15 5.94 0.71 -4 -9 15 5.98 1.12 -4 -9 15 6.41 0.47 4 9 15 6.27 0.49 -4 -10 -14 20.36 1.54 4 10 -14 21.08 0.74 -4 -10 -13 5.39 0.64 -4 -10 -13 5.70 1.21 4 10 -13 6.25 0.61 -4 -10 -12 3.57 1.14 4 -10 12 5.89 0.97 -4 -10 -12 4.75 0.71 4 -10 12 4.98 1.35 4 -10 11 4.70 1.08 -4 -10 -11 2.88 0.76 4 -10 11 4.92 1.62 -4 -10 -11 4.34 0.80 -4 -10 -10 18.09 2.04 4 -10 10 18.69 2.35 4 -10 10 22.98 3.31 -4 -10 -10 20.44 1.56 -4 -10 -9 40.88 3.28 4 -10 9 47.73 4.73 4 -10 9 38.43 3.44 -4 -10 -8 31.66 3.13 4 -10 8 32.44 4.08 4 -10 8 32.93 3.43 4 -10 7 14.36 2.36 -4 -10 -7 12.02 2.22 4 -10 7 11.22 2.51 4 -10 6 13.89 3.00 -4 -10 -6 8.32 1.87 4 -10 6 8.70 1.80 -4 -10 -6 11.37 1.91 -4 -10 -5 93.62 5.45 -4 -10 -5 100.16 4.54 -4 -10 -5 107.01 2.92 4 -10 5 106.69 6.08 4 -10 4 28.65 2.12 4 10 -4 30.33 1.98 4 -10 4 26.16 3.01 4 -10 4 29.83 4.18 -4 -10 -4 24.06 5.04 -4 -10 -4 25.51 2.42 4 -10 4 26.93 2.01 4 -10 3 129.87 4.57 4 -10 3 133.01 4.59 4 10 -3 114.50 3.83 -4 -10 -3 123.02 5.30 4 -10 3 139.42 8.27 -4 -10 -3 121.79 10.38 4 -10 3 118.24 5.88 -4 -10 -3 136.48 3.17 4 10 -2 36.49 2.22 4 -10 2 43.03 2.68 4 -10 2 41.80 2.73 4 -10 2 48.68 4.91 4 -10 2 37.79 3.21 -4 -10 -2 42.47 6.02 -4 -10 -2 40.88 3.14 -4 -10 -2 43.73 1.71 4 -10 1 12.15 1.48 4 -10 1 11.73 1.52 4 -10 1 8.72 2.39 4 -10 1 10.10 1.70 -4 -10 -1 10.74 3.06 -4 -10 -1 17.64 2.20 4 -10 0 25.36 2.43 4 -10 0 27.33 2.42 4 -10 0 24.46 2.18 4 -10 0 26.23 2.20 4 -10 0 31.17 4.15 -4 -10 0 22.11 2.52 -4 -10 1 10.13 1.81 4 -10 -1 15.22 1.86 4 -10 -1 15.69 1.90 4 -10 -1 15.18 1.88 -4 -10 1 10.77 1.57 4 -10 -1 17.12 1.77 4 -10 -2 44.72 3.24 4 -10 -2 48.82 3.20 4 -10 -2 40.88 2.97 4 -10 -2 35.89 4.99 4 -10 -2 43.96 2.96 -4 -10 2 38.90 3.35 4 -10 -3 130.21 5.29 4 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0.81 -4 -10 12 5.89 1.71 4 -10 -13 6.46 1.10 4 -10 -13 7.45 0.92 -4 -10 13 5.36 1.39 -4 -10 13 8.18 0.72 -4 -10 14 19.03 1.84 4 -10 -14 21.39 1.36 4 10 14 19.50 0.88 -4 -11 -13 0.64 0.46 4 11 -13 1.91 0.33 -4 -11 -12 10.68 1.39 4 -11 12 12.26 1.61 4 11 -12 12.84 0.87 4 -11 12 9.09 0.97 -4 -11 -11 15.20 1.29 -4 -11 -11 14.59 1.85 4 -11 11 18.59 2.41 4 -11 11 14.32 1.60 -4 -11 -10 12.19 1.57 -4 -11 -10 12.99 1.88 4 -11 10 11.95 1.79 4 -11 10 16.40 2.57 -4 -11 -9 1.13 0.87 -4 -11 -9 3.37 1.15 4 -11 9 5.55 1.49 4 -11 9 3.73 1.64 -4 -11 -8 7.25 1.50 -4 -11 -8 10.06 1.78 4 -11 8 13.05 2.94 4 -11 8 8.63 1.92 4 -11 7 4.06 1.55 -4 -11 -7 2.53 1.30 4 -11 7 2.96 1.76 4 -11 6 17.70 3.25 -4 -11 -6 14.34 2.42 4 -11 6 14.47 2.42 -4 -11 -6 15.97 1.81 -4 -11 -5 42.26 3.88 4 -11 5 53.05 4.43 -4 -11 -5 43.99 3.17 -4 -11 -4 92.97 5.57 4 -11 4 93.69 7.28 4 -11 4 96.29 5.62 -4 -11 -4 92.75 4.72 4 -11 3 21.72 1.93 -4 -11 -3 21.03 2.34 4 -11 3 23.83 1.98 -4 -11 -3 20.28 2.61 4 -11 3 29.48 4.24 4 -11 3 21.81 2.76 4 -11 2 65.00 3.44 4 -11 2 65.83 3.34 -4 -11 -2 58.73 4.19 4 -11 2 67.78 6.12 4 -11 2 59.60 4.12 -4 -11 -2 59.69 4.05 4 -11 1 19.21 2.01 4 -11 1 22.30 2.09 -4 -11 -1 17.35 2.33 4 -11 1 19.61 3.48 4 -11 1 17.79 2.22 -4 -11 -1 21.52 2.60 4 -11 0 110.55 4.80 4 -11 0 109.79 4.64 -4 -11 0 96.08 4.86 4 -11 0 96.77 4.55 -4 -11 0 93.65 5.32 4 -11 -1 26.98 2.63 4 -11 -1 21.85 2.26 4 -11 -1 22.01 2.25 -4 -11 1 19.57 2.14 4 -11 -1 20.48 2.03 4 -11 -1 23.14 2.12 -4 -11 1 19.56 2.49 4 -11 -2 69.42 4.13 4 -11 -2 61.77 3.82 4 -11 -2 65.67 3.86 4 -11 -2 58.27 3.45 -4 -11 2 57.61 4.34 4 -11 -3 23.56 2.40 4 -11 -3 25.66 2.66 4 -11 -3 24.87 2.46 4 -11 -3 24.36 2.43 -4 -11 3 20.61 2.71 4 -11 -4 102.03 5.10 4 -11 -4 99.98 4.76 4 -11 -4 107.59 5.21 4 -11 -4 107.67 5.16 -4 -11 4 96.80 5.63 4 -11 -5 52.42 3.73 4 -11 -5 52.86 3.47 4 -11 -5 51.02 3.68 4 -11 -5 46.60 3.63 -4 -11 5 47.34 4.03 4 -11 -6 16.83 2.00 4 -11 -6 16.83 2.23 4 -11 -6 16.90 2.33 -4 -11 6 14.58 2.29 4 -11 -6 15.42 2.22 -4 -11 7 2.47 1.08 -4 -11 7 2.30 0.68 4 -11 -7 3.34 1.26 4 -11 -7 2.79 1.25 4 -11 -7 3.90 1.02 4 -11 -7 1.82 1.14 -4 -11 8 8.78 1.62 4 -11 -8 8.58 1.70 4 -11 -8 9.25 1.31 4 -11 -8 8.24 1.62 -4 -11 8 8.08 1.88 -4 -11 8 9.92 1.12 -4 -11 9 4.38 1.21 4 -11 -9 4.30 1.33 4 -11 -9 4.75 0.91 4 -11 -9 3.55 1.12 -4 -11 9 2.30 1.42 -4 -11 9 4.07 0.82 4 -11 -10 14.56 1.86 4 -11 -10 15.75 1.86 -4 -11 10 14.34 2.36 -4 -11 10 11.99 1.43 -4 -11 10 15.06 1.19 4 -11 -11 16.32 1.78 4 -11 -11 15.89 1.69 -4 -11 11 13.16 2.14 -4 -11 11 17.96 1.17 4 -11 -12 12.05 1.23 -4 -11 12 9.31 1.67 4 -11 -12 11.51 1.32 4 -11 -13 1.74 0.52 4 -11 -13 2.17 0.45 -4 -11 13 1.72 0.80 4 11 13 2.02 0.37 -4 -12 -12 51.03 1.88 4 -12 12 52.09 2.40 4 12 -11 12.84 0.84 -4 -12 -11 10.12 0.88 -4 -12 -11 11.54 1.16 4 -12 11 11.18 1.18 4 -12 11 10.78 1.61 -4 -12 -10 10.51 1.32 4 -12 10 11.54 2.05 4 -12 10 8.05 1.33 -4 -12 -10 9.45 1.22 4 -12 9 8.10 1.91 -4 -12 -9 6.43 1.23 -4 -12 -9 5.11 1.19 4 -12 9 7.23 1.47 -4 -12 -8 25.92 2.61 4 -12 8 26.33 2.75 4 -12 8 29.72 3.74 4 -12 7 7.53 2.16 -4 -12 -7 6.48 1.60 4 -12 7 7.58 1.70 -4 -12 -7 6.71 1.09 -4 -12 -6 13.72 2.16 4 -12 6 12.87 2.20 4 -12 6 18.41 3.38 -4 -12 -6 14.31 1.74 -4 -12 -5 24.12 2.92 4 -12 5 27.04 3.13 -4 -12 -5 24.23 2.42 4 -12 5 24.40 3.81 -4 -12 -4 18.56 2.62 4 -12 4 24.96 3.91 4 -12 4 19.41 2.65 -4 -12 -4 19.46 2.35 4 -12 3 21.66 1.91 4 -12 3 22.66 1.86 -4 -12 -3 24.20 2.97 4 -12 3 25.40 4.13 4 -12 3 18.43 2.55 -4 -12 -3 20.20 2.41 4 -12 2 23.13 2.13 4 -12 2 24.60 2.06 -4 -12 -2 20.08 2.58 4 -12 2 22.04 2.55 4 -12 2 21.89 3.78 -4 -12 -2 24.05 2.82 4 -12 1 32.72 2.60 4 -12 1 30.96 2.40 -4 -12 -1 26.98 2.85 4 -12 1 28.98 2.78 -4 -12 -1 31.23 3.18 4 -12 0 10.37 1.64 4 -12 0 11.26 1.55 4 -12 0 10.83 1.67 -4 -12 0 10.53 1.76 -4 -12 0 11.53 2.14 -4 -12 1 29.21 2.55 4 -12 -1 29.85 2.48 4 -12 -1 30.12 2.63 4 -12 -1 28.88 2.32 4 -12 -1 28.99 2.37 -4 -12 1 28.68 3.12 4 -12 -2 24.64 2.54 4 -12 -2 25.97 2.54 4 -12 -2 24.18 2.41 4 -12 -2 23.77 2.34 -4 -12 2 22.22 2.81 4 -12 -3 23.36 2.50 4 -12 -3 22.01 2.33 4 -12 -3 23.27 2.40 4 -12 -3 22.86 2.41 -4 -12 3 22.63 3.32 4 -12 -4 19.99 2.31 4 -12 -4 21.38 2.34 4 -12 -4 21.99 2.34 4 -12 -4 21.38 2.37 -4 -12 4 18.87 2.61 4 -12 -5 30.99 2.88 4 -12 -5 28.72 2.74 4 -12 -5 28.76 2.54 4 -12 -5 26.68 2.76 -4 -12 5 25.11 3.00 -4 -12 6 14.25 2.17 4 -12 -6 15.94 2.15 4 -12 -6 14.25 1.78 4 -12 -6 14.78 2.00 4 -12 -6 11.94 2.02 -4 -12 7 5.76 1.41 4 -12 -7 7.10 1.48 4 -12 -7 8.56 1.58 4 -12 -7 7.31 1.25 4 -12 -8 29.51 2.13 4 -12 -8 31.18 2.69 4 -12 -8 28.08 2.53 -4 -12 8 26.22 2.49 4 -12 -9 6.98 1.36 -4 -12 9 6.48 1.13 4 -12 -9 7.77 0.97 4 -12 -9 7.89 1.38 -4 -12 9 5.22 1.36 4 -12 -10 12.01 1.47 4 -12 -10 11.13 1.42 -4 -12 10 9.24 1.57 -4 -12 10 10.54 1.14 4 -12 -11 12.00 1.32 4 -12 -11 12.66 1.32 -4 -12 11 9.76 1.40 4 -12 -12 61.83 2.20 4 -12 -12 61.28 2.15 4 12 12 58.92 1.44 4 13 -11 8.18 0.56 4 -13 11 7.44 0.74 4 13 -10 27.53 1.12 4 -13 10 27.08 1.83 4 -13 10 27.30 2.49 -4 -13 -9 19.41 1.73 4 -13 9 20.16 2.58 4 -13 9 17.02 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63.65 5.84 5 5 2 166.03 9.62 5 -5 -2 170.63 5.28 5 -5 -3 64.94 3.21 5 5 3 62.50 6.07 5 5 4 82.29 7.34 5 5 5 2.39 1.42 5 5 6 49.03 6.14 -5 -5 7 56.03 2.20 5 -5 -7 49.83 3.30 5 5 7 51.36 6.22 5 -5 -7 57.11 2.35 -5 -5 7 54.41 2.34 -5 -5 8 9.17 0.97 5 -5 -8 11.28 1.69 5 5 8 9.65 1.36 5 -5 -8 10.32 1.11 5 5 8 8.96 2.80 -5 -5 8 9.06 1.11 5 -5 -9 23.65 2.60 5 5 9 24.08 2.16 5 -5 -9 23.02 1.69 -5 -5 9 24.93 1.60 -5 -5 9 23.05 1.75 5 5 9 20.08 3.77 -5 -5 10 3.16 0.87 5 -5 -10 2.76 1.23 5 5 10 2.84 0.97 5 -5 -10 2.92 0.75 -5 -5 10 5.49 1.23 -5 -5 11 2.38 0.63 5 -5 -11 2.17 1.15 5 5 11 2.05 0.95 -5 5 -11 2.08 0.67 5 -5 -11 1.70 0.64 -5 -5 11 1.96 0.75 -5 5 -12 16.54 1.37 5 -5 -12 15.18 2.29 -5 -5 12 14.15 1.19 5 5 12 13.54 1.73 5 -5 -12 14.91 1.42 -5 -5 12 13.90 3.32 -5 -5 12 15.21 1.48 -5 -5 13 2.71 0.54 5 -5 -13 2.91 1.12 -5 5 -13 2.73 0.63 5 5 13 1.93 0.79 -5 -5 13 2.89 1.86 5 -5 -13 2.33 0.68 -5 -5 13 2.45 0.70 -5 -5 14 23.59 1.16 5 -5 -14 20.74 2.18 5 5 14 24.69 1.35 5 5 14 20.63 1.70 5 -5 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-6 -8 1.41 0.73 -5 6 7 20.82 3.78 5 6 -7 23.10 1.41 5 -6 7 25.73 1.92 5 -6 7 27.42 2.34 -5 -6 -7 23.88 1.57 -5 -6 -7 24.24 2.03 5 -6 7 26.43 2.83 5 6 -6 35.83 1.76 5 -6 6 42.57 2.87 -5 6 6 37.94 5.02 -5 -6 -6 36.67 1.83 -5 -6 -6 37.19 1.84 5 -6 6 42.04 2.03 5 6 -5 35.26 1.86 -5 6 5 29.29 4.43 5 6 -4 164.59 4.07 -5 6 4 177.72 10.41 -5 6 3 15.71 3.14 -5 6 2 76.69 6.74 5 6 -2 77.87 5.81 5 6 -1 112.75 7.22 -5 6 1 116.64 8.24 5 6 0 58.91 5.48 -5 6 0 65.24 6.21 -5 -6 0 52.95 5.35 5 6 1 115.75 7.95 -5 -6 1 102.04 6.76 5 6 2 77.61 6.93 5 6 3 15.14 3.24 5 6 4 175.26 10.96 5 6 5 35.37 5.17 5 -6 -6 36.64 2.82 5 -6 -6 37.28 2.62 5 6 6 37.86 2.43 5 -6 -6 35.51 1.81 5 6 6 33.70 5.06 -5 -6 6 34.43 2.10 -5 -6 7 23.81 1.46 5 -6 -7 23.95 2.47 5 -6 -7 25.09 2.25 5 6 7 26.17 2.07 5 -6 -7 24.29 1.62 5 6 7 19.83 4.01 -5 -6 7 23.82 1.71 5 -6 -8 1.75 1.11 5 -6 -8 2.18 0.99 5 6 8 2.03 0.86 -5 -6 8 1.01 1.49 5 6 8 2.31 1.55 -5 -6 8 1.92 0.68 5 -6 -8 1.78 0.63 -5 -6 8 1.76 0.54 5 -6 -9 31.37 3.01 5 -6 -9 32.13 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85.52 5.53 7 7 -6 81.39 2.91 7 -7 5 21.48 2.21 -7 -7 -5 15.87 1.46 -7 -7 -5 17.26 1.72 7 -7 5 21.17 1.58 7 -7 5 17.38 2.59 7 7 -5 15.91 1.34 -7 -7 -5 18.08 1.52 -7 -7 -4 3.95 0.82 7 -7 4 5.41 1.22 -7 -7 -4 3.87 0.82 7 -7 4 5.57 0.92 7 -7 4 5.71 1.58 7 7 -4 3.50 0.80 7 -7 3 117.28 4.81 -7 -7 -3 113.15 3.53 7 -7 3 116.17 3.32 7 -7 3 112.98 5.71 7 7 -3 114.77 3.33 -7 -7 -3 111.10 3.56 7 -7 2 70.89 3.67 -7 -7 -2 64.89 2.58 7 -7 2 63.73 2.37 7 -7 2 63.87 4.10 7 7 -2 65.03 2.41 -7 -7 -2 65.00 2.72 -7 7 1 65.08 6.89 7 -7 1 82.57 4.24 7 -7 1 78.66 3.83 -7 -7 -1 74.29 2.70 7 -7 1 75.80 2.49 7 -7 1 78.97 4.29 7 7 -1 74.51 2.50 -7 -7 -1 78.53 2.96 7 7 0 453.70 5.82 -7 7 0 390.70 16.33 7 -7 0 454.91 9.73 7 -7 0 450.31 9.07 -7 -7 0 439.41 6.30 7 -7 0 431.56 5.68 7 7 0 383.12 15.24 -7 -7 0 449.16 7.02 -7 7 -1 66.65 6.90 7 -7 -1 78.66 3.72 7 -7 -1 75.59 3.97 7 -7 -1 78.34 3.80 -7 -7 1 74.48 2.56 7 7 1 64.50 6.50 7 7 1 77.46 2.35 -7 -7 1 75.13 2.89 7 7 2 58.65 6.34 7 -7 -2 63.34 3.44 7 -7 -2 63.65 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9.04 0.91 -8 -5 11 6.52 0.69 -8 -5 12 24.33 1.19 8 -5 -12 22.05 1.33 8 5 12 24.08 1.82 -8 5 -12 25.51 1.27 -8 -5 13 28.19 0.97 8 5 13 29.67 1.60 -8 5 -13 31.11 1.16 8 -6 13 14.22 1.35 -8 -6 -13 17.73 1.02 8 -6 12 9.55 1.53 -8 -6 -12 10.96 1.07 8 -6 12 10.62 1.44 8 6 -12 8.99 0.51 8 6 -11 4.14 0.51 -8 -6 -11 3.52 0.82 8 -6 10 18.02 2.38 -8 -6 -10 8.81 1.28 8 -6 10 12.11 2.18 8 6 -10 22.50 1.26 8 -6 9 8.97 1.60 -8 -6 -9 10.26 1.12 -8 -6 -9 9.51 1.42 8 6 -9 10.19 0.99 8 -6 9 7.32 1.66 8 -6 8 9.50 1.73 -8 -6 -8 8.39 1.09 8 6 -8 8.74 0.97 8 -6 8 8.01 1.84 -8 -6 -8 8.36 1.44 8 -6 7 3.98 1.21 -8 -6 -7 4.65 0.89 8 -6 7 5.54 1.63 8 6 -7 4.58 0.82 -8 -6 -7 4.32 1.08 8 -6 6 2.57 1.37 -8 -6 -6 0.29 0.59 8 -6 6 2.84 1.00 8 6 -6 0.27 0.60 -8 -6 -6 0.99 0.69 8 -6 5 80.03 4.43 -8 -6 -5 72.42 3.01 8 -6 5 74.08 2.88 -8 -6 -5 72.54 3.67 8 -6 5 83.26 5.42 8 6 -5 77.53 2.81 -8 -6 -5 75.95 2.97 8 -6 4 20.91 2.33 -8 -6 -4 19.58 1.63 8 -6 4 21.79 1.65 8 -6 4 21.66 2.80 -8 -6 -4 18.80 1.86 8 6 -4 21.41 1.58 -8 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19.75 1.04 -11 -3 -7 19.52 1.44 11 3 -7 17.65 0.80 11 -3 6 4.04 0.95 -11 -3 -6 3.78 0.54 -11 3 6 3.40 0.53 11 3 -6 3.34 0.49 11 -3 6 1.10 0.61 -11 -3 -6 3.52 0.81 11 -3 5 0.84 0.61 -11 -3 -5 0.42 0.39 -11 3 5 0.15 0.35 11 -3 5 1.13 0.47 11 3 -5 0.50 0.38 11 -3 5 1.06 0.70 -11 -3 -5 0.10 0.53 11 -3 4 6.59 1.15 -11 -3 -4 5.75 0.80 -11 3 4 5.15 0.69 11 3 -4 5.94 0.75 11 -3 4 6.08 0.77 11 -3 4 2.97 0.86 -11 -3 -4 5.82 1.03 11 -3 3 10.06 1.42 -11 -3 -3 10.09 1.04 -11 3 3 10.10 0.92 11 -3 3 10.28 0.98 -11 -3 -3 11.46 1.38 11 3 -3 9.96 0.95 11 -3 3 5.82 1.08 -11 -3 -3 9.32 0.74 11 -3 2 10.51 1.48 -11 -3 -2 8.45 0.96 -11 3 2 8.06 0.84 11 -3 2 8.49 0.91 11 3 -2 8.18 0.92 -11 -3 -2 9.07 0.81 -11 -3 -2 8.11 1.26 -11 -3 -1 3.21 0.57 11 -3 1 4.68 1.09 -11 -3 -1 3.05 0.76 -11 3 1 2.16 0.52 11 -3 1 2.60 0.57 11 3 -1 2.82 0.69 -11 -3 -1 2.39 0.84 11 -3 0 32.65 2.57 -11 -3 0 30.98 1.80 -11 3 0 28.61 1.43 11 -3 0 31.81 1.57 11 3 0 29.86 1.62 -11 -3 0 32.51 2.16 -11 -3 0 31.60 1.53 -11 3 -1 2.97 0.99 -11 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7 6.99 1.00 -11 -4 -7 7.31 0.60 -11 4 7 6.10 0.54 11 4 -7 6.50 0.50 11 -4 7 4.88 0.87 -11 -4 -7 6.28 0.76 11 -4 6 5.19 0.99 -11 -4 -6 4.84 0.60 -11 4 6 4.50 0.55 11 -4 6 2.72 0.71 11 4 -6 4.41 0.52 -11 -4 -6 5.00 0.78 11 -4 5 9.22 1.25 -11 -4 -5 8.68 0.84 -11 4 5 7.81 0.71 11 -4 5 8.29 0.79 11 4 -5 9.07 0.76 -11 -4 -5 7.01 0.96 11 -4 4 27.39 2.13 -11 -4 -4 23.82 1.38 -11 4 4 22.53 1.16 11 -4 4 22.85 1.30 -11 -4 -4 23.36 1.70 11 4 -4 23.82 1.29 -11 -4 -3 4.53 0.59 11 -4 3 3.43 0.98 -11 -4 -3 3.83 0.70 -11 4 3 3.79 0.56 11 -4 3 3.52 0.63 11 -4 3 2.81 0.79 11 4 -3 4.34 0.64 -11 -4 -3 3.48 0.81 11 -4 2 25.47 2.20 -11 -4 -2 25.92 1.56 -11 4 2 22.03 1.17 11 -4 2 22.10 1.33 -11 -4 -2 23.08 1.71 11 4 -2 23.65 1.36 -11 -4 -2 24.68 1.30 -11 -4 -1 3.42 0.57 11 -4 1 2.18 0.93 -11 -4 -1 2.51 0.64 -11 4 1 1.98 0.49 11 -4 1 2.20 0.59 11 4 -1 2.25 0.65 -11 -4 -1 2.19 0.66 11 -4 0 6.09 1.16 -11 -4 0 6.78 0.85 -11 4 0 5.21 0.57 11 4 0 7.25 0.84 11 -4 0 6.00 0.71 -11 -4 0 5.49 0.84 -11 -4 0 6.88 0.76 -11 4 -1 1.93 0.74 -11 -4 1 1.47 0.43 11 -4 -1 1.66 0.79 -11 -4 1 1.62 0.60 11 -4 -1 2.19 0.52 11 4 1 3.84 0.64 -11 -4 1 1.56 0.53 11 4 2 22.79 1.34 11 -4 -2 25.66 2.12 -11 -4 2 24.07 1.47 11 -4 -2 22.89 1.09 11 4 2 22.90 1.29 -11 4 -2 25.26 1.99 -11 -4 2 23.38 1.36 -11 -4 3 4.13 0.62 11 -4 -3 4.49 1.05 11 4 3 2.41 0.57 -11 -4 3 4.08 0.66 11 -4 -3 3.22 0.44 11 4 3 3.53 0.58 -11 4 -3 3.96 0.87 11 4 4 19.65 1.29 11 -4 -4 24.35 1.95 -11 -4 4 23.78 1.30 11 4 4 20.95 1.06 -11 4 -4 25.77 1.82 -11 -4 4 24.40 1.33 11 4 5 7.49 0.88 11 -4 -5 8.18 1.17 -11 -4 5 7.82 0.71 11 4 5 7.01 0.55 -11 4 -5 7.06 0.95 -11 -4 5 8.61 0.80 -11 -4 6 3.90 0.53 11 -4 -6 4.54 0.83 11 4 6 3.53 0.62 -11 -4 6 3.96 0.47 -11 4 -6 3.73 0.59 11 -4 -7 6.27 0.85 11 4 7 5.84 0.65 -11 4 -7 6.11 0.50 -11 4 -7 5.72 0.57 -11 -4 7 7.42 0.62 11 -4 -8 9.01 0.80 -11 4 -8 8.62 0.48 -11 -4 8 9.37 0.57 11 -5 7 2.28 0.65 -11 -5 -7 2.42 0.36 -11 5 7 1.48 0.26 11 -5 7 1.58 0.48 11 5 -7 1.97 0.31 11 -5 6 6.38 0.99 -11 -5 -6 5.26 0.57 -11 5 6 5.09 0.47 11 5 -6 5.20 0.54 11 -5 6 3.52 0.69 -11 -5 -6 4.38 0.58 11 -5 5 3.61 0.90 -11 -5 -5 2.92 0.53 -11 5 5 2.68 0.41 11 -5 5 2.29 0.71 11 5 -5 4.15 0.54 -11 -5 -5 2.58 0.53 11 -5 4 2.88 0.78 -11 -5 -4 2.80 0.55 -11 5 4 2.68 0.41 11 -5 4 1.83 0.55 11 5 -4 3.53 0.58 -11 -5 -4 2.81 0.60 11 -5 3 4.76 0.96 -11 -5 -3 4.41 0.67 -11 5 3 3.89 0.48 11 -5 3 4.21 0.59 11 -5 3 2.41 0.62 11 5 -3 4.83 0.69 -11 -5 -3 3.14 0.61 -11 -5 -2 2.87 0.52 11 -5 2 2.55 0.88 -11 -5 -2 3.12 0.61 -11 5 2 2.49 0.38 11 -5 2 2.26 0.49 11 5 -2 4.27 0.65 -11 -5 -2 3.45 0.62 11 -5 1 14.82 1.66 -11 -5 -1 20.12 1.35 11 -5 1 13.69 0.94 11 5 -1 15.25 1.08 -11 -5 -1 22.60 1.30 11 -5 0 38.20 2.53 -11 -5 0 37.03 1.73 11 -5 0 36.52 1.40 11 5 0 33.67 1.56 -11 5 0 37.08 2.30 -11 -5 0 35.79 1.63 11 5 1 18.68 1.19 11 -5 -1 16.30 1.68 -11 -5 1 13.99 1.09 11 -5 -1 14.71 0.86 -11 5 -1 13.47 1.38 -11 -5 1 14.01 1.08 -11 -5 2 2.98 0.53 11 -5 -2 2.82 0.91 11 5 2 3.12 0.62 -11 -5 2 3.22 0.56 11 -5 -2 3.15 0.41 11 5 2 3.37 0.54 -11 5 -2 2.59 0.70 -11 -5 3 4.63 0.66 11 -5 -3 4.10 0.88 11 5 3 3.09 0.62 -11 -5 3 4.01 0.57 11 5 3 3.67 0.49 -11 5 -3 4.28 0.77 -11 -5 4 4.13 0.62 11 -5 -4 2.93 0.78 11 5 4 2.13 0.54 -11 -5 4 3.22 0.49 11 5 4 2.45 0.36 -11 5 -4 2.62 0.59 -11 -5 5 4.01 0.57 11 -5 -5 2.38 0.72 11 5 5 2.59 0.54 -11 -5 5 3.58 0.42 -11 5 -5 3.27 0.55 11 -5 -6 5.50 0.78 11 5 6 5.02 0.68 -11 -5 6 5.91 0.60 -11 -5 7 2.16 0.35 11 -5 -7 2.46 0.49 11 5 7 1.78 0.43 -11 5 -7 2.27 0.32 11 -6 7 7.34 0.79 -11 -6 -6 3.66 0.43 11 -6 6 2.51 0.52 11 6 -6 2.87 0.40 -11 -6 -5 1.72 0.40 11 -6 5 0.89 0.39 11 6 -5 1.49 0.38 11 -6 4 7.03 1.02 -11 -6 -4 6.34 0.67 11 6 -4 5.95 0.62 11 -6 3 1.08 0.62 -11 -6 -3 -0.16 0.32 11 6 -3 0.54 0.36 11 -6 2 16.97 1.56 -11 -6 -2 18.11 1.12 11 6 -2 15.67 1.00 -11 -6 -2 17.86 1.07 -11 6 1 2.72 0.65 -11 -6 -1 3.92 0.58 11 -6 1 3.55 0.86 -11 -6 -1 3.16 0.54 11 6 -1 2.90 0.54 -11 6 0 2.68 0.64 -11 -6 0 3.24 0.60 11 -6 0 2.94 0.82 11 6 0 2.53 0.48 -11 -6 0 2.51 0.53 11 6 0 2.81 0.56 -11 -6 1 4.11 0.60 11 -6 -1 3.49 0.82 11 6 1 3.16 0.57 -11 -6 1 3.13 0.51 11 6 1 3.26 0.49 -11 6 -1 3.57 0.75 11 6 2 15.47 1.12 11 -6 -2 18.65 1.58 -11 -6 2 16.53 0.97 11 6 2 15.20 0.83 -11 6 -2 15.66 1.17 -11 -6 2 17.16 1.07 -11 -6 3 0.10 0.30 11 -6 -3 0.18 0.42 11 6 3 -0.10 0.37 -11 -6 3 0.25 0.25 11 6 3 0.23 0.25 -11 6 -3 -0.34 0.33 11 -6 -4 6.58 0.90 11 6 4 5.04 0.69 -11 -6 4 5.07 0.47 -11 -6 4 6.56 0.67 -11 -6 5 2.40 0.44 11 -6 -5 1.42 0.48 11 6 5 1.46 0.45 11 -6 -6 3.64 0.56 -11 -6 6 4.25 0.47 -11 -6 7 7.99 0.47 11 7 -6 7.24 0.44 11 -7 5 9.89 0.92 -11 -7 -5 9.25 0.59 11 7 -5 8.57 0.57 11 -7 4 2.37 0.59 -11 -7 -4 3.34 0.44 11 7 -4 3.38 0.45 11 -7 3 23.60 1.57 -11 -7 -3 21.35 1.00 11 7 -3 20.87 0.98 -11 7 2 2.00 0.56 11 -7 2 1.40 0.55 -11 -7 -2 2.16 0.41 11 7 -2 1.87 0.39 11 7 -1 15.81 0.87 11 -7 1 19.47 1.45 -11 -7 -1 16.69 0.93 11 7 -1 16.62 0.91 -11 7 1 17.59 1.11 -11 -7 -1 18.72 1.02 11 7 0 11.63 0.88 11 -7 0 14.88 1.35 -11 -7 0 12.51 0.78 11 7 0 12.38 0.73 -11 7 0 10.48 0.86 -11 -7 0 13.92 0.95 11 7 1 17.21 1.07 11 -7 -1 18.21 1.39 -11 -7 1 17.26 0.83 11 7 1 16.21 0.77 -11 7 -1 17.63 0.99 -11 -7 1 18.98 1.05 11 -7 -2 1.63 0.48 11 7 2 1.81 0.47 -11 -7 2 1.74 0.33 11 7 3 20.28 1.19 11 -7 -3 22.40 1.37 -11 -7 3 22.86 1.07 -11 -7 4 2.80 0.40 11 -7 -4 2.31 0.47 11 7 4 2.53 0.49 11 7 5 7.42 0.68 11 -7 -5 8.99 0.71 -11 -7 5 9.04 0.58 -11 -8 -4 1.79 0.46 11 8 -4 3.03 0.31 11 -8 3 7.48 0.72 -11 -8 -3 5.83 0.73 -11 -8 -3 7.23 0.46 11 8 -3 7.16 0.47 11 -8 2 7.84 0.76 -11 -8 -2 7.45 0.48 11 8 -2 8.16 0.51 -11 -8 -1 1.35 0.43 -11 -8 -1 2.00 0.28 11 8 -1 2.25 0.30 11 -8 0 20.37 1.17 -11 -8 0 22.10 0.98 -11 -8 1 3.33 0.44 11 -8 -1 3.32 0.52 11 8 1 3.08 0.48 11 8 2 7.49 0.68 11 -8 -2 6.97 0.65 -11 -8 2 8.97 0.62 11 8 3 6.39 0.62 -11 -8 3 7.47 0.54 -11 -8 4 2.96 0.32 -12 0 0 176.57 3.15 12 0 0 173.90 3.07 -12 0 0 172.74 4.42 12 0 1 0.14 0.39 12 0 -1 0.71 0.43 -12 0 -1 0.38 0.34 -12 0 1 0.01 0.29 12 0 1 0.77 0.41 12 0 -1 1.16 0.37 -12 0 -1 0.64 0.49 -12 0 1 1.10 0.56 12 0 2 8.48 0.83 12 0 -2 7.61 0.79 -12 0 -2 8.32 0.66 -12 0 2 7.92 0.73 12 0 2 7.77 0.73 12 0 -2 8.05 0.67 -12 0 -2 8.13 1.01 -12 0 2 8.01 0.97 12 0 -3 4.34 0.63 -12 0 -3 5.12 0.47 -12 0 3 5.68 0.62 12 0 3 4.20 0.55 12 0 -3 4.33 0.47 -12 0 -3 5.05 0.81 -12 0 3 5.19 0.75 12 0 -4 16.50 1.02 -12 0 -4 15.80 0.65 -12 0 4 18.76 0.97 12 0 4 17.53 0.88 -12 0 -4 19.87 1.40 12 0 -4 17.00 0.72 -12 0 4 18.54 1.13 12 0 5 1.06 0.29 -12 0 -5 4.38 0.70 -12 0 6 7.90 0.51 -12 0 -6 8.39 0.73 -12 1 6 12.89 0.61 -12 -1 -6 15.38 0.92 -12 1 5 18.43 0.85 -12 -1 -5 19.19 1.22 -12 1 5 17.94 1.03 -12 1 4 6.03 0.74 12 -1 4 6.78 0.72 -12 -1 -4 6.26 0.49 -12 1 4 7.38 0.65 12 -1 4 6.43 0.57 -12 -1 -4 8.21 0.90 12 1 -4 7.84 0.58 -12 1 3 0.65 0.41 12 -1 3 0.82 0.45 -12 -1 -3 1.11 0.33 -12 1 3 0.82 0.33 12 -1 3 0.98 0.38 12 1 -3 0.88 0.31 -12 -1 -3 1.31 0.50 12 -1 2 22.33 1.40 -12 -1 -2 23.12 1.10 -12 1 2 23.67 1.12 12 -1 2 24.00 1.14 12 1 -2 25.27 1.11 -12 -1 -2 26.44 1.67 -12 1 2 22.85 1.58 12 -1 1 11.79 1.09 -12 -1 -1 9.12 0.76 -12 1 1 8.67 0.71 12 -1 1 12.49 0.88 12 1 -1 8.94 0.73 -12 -1 -1 9.80 1.06 -12 1 1 9.64 1.11 12 -1 0 0.65 0.45 -12 -1 0 0.48 0.36 -12 1 0 0.02 0.29 12 -1 0 0.83 0.39 12 1 0 0.68 0.37 -12 -1 0 0.38 0.43 -12 1 0 0.24 0.45 12 -1 -1 9.78 1.00 -12 1 -1 11.33 0.75 -12 -1 1 9.30 0.82 12 -1 -1 10.01 0.76 12 1 1 10.22 0.83 -12 1 -1 11.30 1.20 -12 -1 1 8.95 0.98 12 -1 -2 22.92 1.47 -12 1 -2 22.35 0.91 -12 -1 2 25.70 1.25 12 1 2 25.48 1.25 12 -1 -2 22.91 1.00 -12 1 -2 23.68 1.65 -12 -1 2 23.00 1.41 12 -1 -3 0.47 0.42 -12 1 -3 0.65 0.22 -12 -1 3 0.76 0.35 12 1 3 0.85 0.36 12 -1 -3 0.65 0.25 -12 1 -3 0.55 0.44 -12 -1 3 1.30 0.39 12 -1 -4 5.37 0.68 -12 -1 4 5.51 0.56 12 1 4 5.88 0.54 12 -1 -4 4.87 0.37 -12 -1 4 6.39 0.61 -12 1 -4 5.71 0.77 12 -1 -5 17.39 1.02 -12 -1 5 17.46 0.83 12 1 5 16.78 0.70 -12 1 -5 19.38 1.21 -12 2 5 9.82 0.57 -12 -2 -5 11.47 0.87 -12 2 5 10.56 0.81 12 -2 4 21.72 1.28 -12 -2 -4 21.69 0.89 -12 2 4 20.46 0.90 -12 -2 -4 23.05 1.33 12 -2 4 20.24 0.95 12 2 -4 22.48 0.89 -12 2 4 23.61 1.37 -12 2 3 3.50 0.67 12 -2 3 3.35 0.67 -12 -2 -3 2.41 0.40 -12 2 3 2.93 0.41 12 -2 3 2.50 0.45 12 2 -3 2.53 0.42 -12 -2 -3 2.94 0.60 12 -2 2 28.15 1.68 -12 -2 -2 28.88 1.24 -12 2 2 25.78 1.06 12 -2 2 27.60 1.18 12 2 -2 27.85 1.17 -12 -2 -2 26.18 1.54 -12 2 2 26.68 1.69 12 -2 1 12.78 1.22 -12 -2 -1 12.26 0.88 -12 2 1 11.11 0.71 12 -2 1 11.94 0.79 12 2 -1 13.01 0.87 -12 -2 -1 12.21 1.09 -12 2 1 12.28 1.23 12 -2 0 0.96 0.48 -12 -2 0 -0.08 0.34 -12 2 0 0.84 0.31 12 -2 0 0.03 0.32 12 2 0 -0.26 0.35 -12 -2 0 0.00 0.34 -12 2 0 0.71 0.49 12 -2 -1 12.89 1.17 -12 2 -1 11.72 0.66 -12 -2 1 11.97 0.89 12 -2 -1 12.71 0.82 12 2 1 11.89 0.84 -12 -2 1 12.23 1.00 -12 2 -1 14.78 1.38 12 -2 -2 28.68 1.67 -12 -2 2 27.12 1.27 12 -2 -2 24.52 0.93 12 2 2 27.85 1.17 -12 2 -2 28.84 1.75 -12 -2 2 24.87 1.26 -12 -2 2 26.11 0.80 -12 -2 3 2.35 0.27 12 -2 -3 4.15 0.67 -12 -2 3 2.76 0.45 12 -2 -3 2.94 0.33 12 2 3 3.06 0.46 -12 2 -3 3.09 0.64 -12 -2 3 2.40 0.40 12 -2 -4 22.56 1.34 -12 -2 4 21.81 0.99 12 2 4 20.36 0.83 -12 2 -4 22.28 1.36 12 -2 -5 11.27 0.84 -12 -2 5 10.69 0.60 -12 2 -5 9.84 0.80 -12 3 5 3.04 0.46 -12 3 4 4.96 0.65 12 -3 4 5.78 0.74 -12 -3 -4 5.05 0.46 -12 3 4 4.50 0.39 -12 -3 -4 5.57 0.60 12 3 -4 4.47 0.43 -12 3 3 3.66 0.62 12 -3 3 3.61 0.67 -12 -3 -3 3.29 0.44 -12 3 3 3.49 0.36 12 -3 3 3.12 0.45 12 3 -3 3.81 0.46 -12 -3 -3 2.81 0.50 -12 3 2 5.59 0.79 12 -3 2 5.49 0.78 -12 -3 -2 5.31 0.57 -12 3 2 4.95 0.44 12 -3 2 4.96 0.53 12 3 -2 4.47 0.53 -12 -3 -2 4.99 0.62 12 -3 1 0.26 0.40 -12 -3 -1 0.25 0.29 -12 3 1 0.14 0.21 12 -3 1 0.60 0.28 12 3 -1 0.80 0.37 -12 -3 -1 0.83 0.35 -12 3 1 0.66 0.43 12 -3 0 5.13 0.81 -12 -3 0 4.65 0.57 -12 3 0 4.07 0.36 12 -3 0 4.19 0.46 12 3 0 4.96 0.56 -12 -3 0 4.92 0.60 -12 -3 0 4.94 0.40 -12 3 0 5.25 0.80 -12 -3 1 0.46 0.20 12 -3 -1 0.76 0.48 -12 -3 1 0.15 0.29 12 -3 -1 0.61 0.26 12 3 1 0.43 0.32 -12 -3 1 0.55 0.29 -12 3 -1 0.41 0.36 12 -3 -2 5.88 0.82 -12 -3 2 5.71 0.58 12 -3 -2 4.14 0.37 12 3 2 5.13 0.54 -12 -3 2 5.00 0.41 -12 3 -2 5.49 0.76 12 -3 -3 3.68 0.65 -12 -3 3 4.02 0.53 12 3 3 3.43 0.40 -12 3 -3 3.48 0.59 -12 -3 3 3.58 0.38 12 -3 -4 4.94 0.64 -12 -3 4 5.59 0.47 -12 3 -4 5.12 0.61 12 -3 -5 2.55 0.44 -12 4 4 2.30 0.41 12 -4 4 1.76 0.43 -12 -4 -4 2.55 0.32 12 4 -4 2.09 0.31 -12 4 3 1.83 0.44 12 -4 3 1.95 0.51 -12 -4 -3 1.81 0.34 12 4 -3 0.65 0.28 12 -4 2 2.91 0.61 -12 -4 -2 3.43 0.45 12 4 -2 2.51 0.40 -12 4 2 2.83 0.55 12 -4 1 1.15 0.47 -12 -4 -1 1.44 0.37 12 -4 1 0.47 0.24 12 4 -1 0.79 0.30 -12 4 1 0.96 0.40 -12 -4 0 0.04 0.18 12 -4 0 0.19 0.40 -12 -4 0 0.13 0.26 12 -4 0 0.53 0.23 12 4 0 0.49 0.29 -12 4 0 0.16 0.32 -12 -4 1 0.91 0.24 12 -4 -1 1.05 0.45 -12 -4 1 1.00 0.33 12 4 1 1.18 0.32 -12 4 -1 1.04 0.43 -12 -4 2 2.29 0.31 12 -4 -2 3.34 0.62 -12 -4 2 3.15 0.40 12 4 2 2.86 0.35 -12 4 -2 2.41 0.49 -12 -4 3 1.33 0.23 12 -4 -3 0.96 0.42 -12 -4 3 1.47 0.28 12 -4 -4 2.03 0.41 12 -5 3 0.20 0.28 -12 -5 -3 0.37 0.18 12 5 -3 0.21 0.21 12 -5 2 6.94 0.76 -12 -5 -2 6.38 0.48 12 5 -2 5.79 0.46 -12 5 2 6.19 0.62 12 -5 1 7.60 0.80 12 5 -1 6.45 0.50 -12 5 1 8.34 0.72 -12 -5 0 12.15 0.67 12 5 0 9.71 0.56 -12 5 0 10.31 0.77 12 -5 -1 8.62 0.84 -12 -5 1 8.00 0.51 12 5 1 9.25 0.52 -12 -5 1 7.56 0.47 12 -5 -2 6.65 0.70 -12 -5 2 7.10 0.44 12 -5 -3 0.07 0.23 0 0 0 0.00 0.00 TITL exp_823 in P2(1)2(1)2(1) REM P2(1)2(1)2(1) (#19 in standard setting) CELL 1.54184 10.058927 14.292073 15.118122 90.0000 90.0000 90.0000 ZERR 4.00 0.000216 0.000311 0.000298 0.0000 0.0000 0.0000 LATT -1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H O UNIT 96.00 120.00 16.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 41412 _olex2_date_sample_data_collection 2017-03-16 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.310 _oxdiff_exptl_absorpt_empirical_full_min 0.654 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O2 O 0.8218(2) 0.79134(12) 0.86043(10) 0.0382(4) Uani 1 1 d . . . . . H2 H 0.8362 0.8444 0.8421 0.057 Uiso 1 1 calc GR . . . . O3 O 0.74830(19) 0.86699(12) 0.70349(11) 0.0367(4) Uani 1 1 d . . . . . O11 O 0.79960(18) 0.44540(11) 0.88638(10) 0.0330(4) Uani 1 1 d . . . . . O21 O 0.88062(18) 0.12893(11) 0.74992(10) 0.0337(4) Uani 1 1 d . . . . . C1 C 0.7828(2) 0.64195(15) 0.80049(13) 0.0245(4) Uani 1 1 d . . . . . H1 H 0.8058 0.6165 0.8550 0.029 Uiso 1 1 calc R . . . . C2 C 0.7874(2) 0.73509(16) 0.79152(13) 0.0269(4) Uani 1 1 d . . . . . C3 C 0.7563(2) 0.78173(15) 0.70682(13) 0.0255(4) Uani 1 1 d . . . . . C4 C 0.7443(2) 0.71946(15) 0.62539(13) 0.0244(4) Uani 1 1 d . . . . . C5 C 0.6768(2) 0.62802(14) 0.65214(12) 0.0217(4) Uani 1 1 d . . . . . C6 C 0.5693(2) 0.59612(15) 0.61120(13) 0.0254(4) Uani 1 1 d . . . . . H6 H 0.5353 0.6318 0.5650 0.030 Uiso 1 1 calc R . . . . C7 C 0.4987(2) 0.50730(16) 0.63374(15) 0.0284(4) Uani 1 1 d . . . . . H7A H 0.4754 0.4757 0.5791 0.034 Uiso 1 1 calc R . . . . H7B H 0.4164 0.5230 0.6637 0.034 Uiso 1 1 calc R . . . . C8 C 0.57658(19) 0.43879(14) 0.69197(13) 0.0230(4) Uani 1 1 d . . . . . H8 H 0.5090 0.4030 0.7242 0.028 Uiso 1 1 calc R . . . . C9 C 0.6588(2) 0.49128(14) 0.76513(13) 0.0221(4) Uani 1 1 d . . . . . C10 C 0.7428(2) 0.57596(14) 0.72765(12) 0.0206(4) Uani 1 1 d . . . . . H10 H 0.8252 0.5493 0.7039 0.025 Uiso 1 1 calc R . . . . C11 C 0.7648(2) 0.42850(14) 0.81097(13) 0.0232(4) Uani 1 1 d . . . . . C12 C 0.8291(2) 0.34751(14) 0.76102(12) 0.0225(4) Uani 1 1 d . . . . . H12A H 0.8710 0.3048 0.8023 0.027 Uiso 1 1 calc R . . . . H12B H 0.8966 0.3710 0.7209 0.027 Uiso 1 1 calc R . . . . C13 C 0.72020(19) 0.29674(14) 0.70890(12) 0.0212(4) Uani 1 1 d . . . . . C14 C 0.65729(19) 0.36599(14) 0.64047(12) 0.0219(4) Uani 1 1 d . . . . . C15 C 0.5776(2) 0.29774(16) 0.58103(14) 0.0279(4) Uani 1 1 d . . . . . H15A H 0.4912 0.2837 0.6063 0.034 Uiso 1 1 calc R . . . . H15B H 0.5659 0.3227 0.5219 0.034 Uiso 1 1 calc R . . . . C16 C 0.6662(2) 0.21312(15) 0.58086(13) 0.0270(4) Uani 1 1 d . . . . . H16 H 0.6626 0.1662 0.5384 0.032 Uiso 1 1 calc R . . . . C17 C 0.7514(2) 0.21330(14) 0.64940(13) 0.0232(4) Uani 1 1 d . . . . . C18 C 0.6193(2) 0.25905(15) 0.77752(14) 0.0275(4) Uani 1 1 d . . . . . H18A H 0.5401 0.2389 0.7477 0.041 Uiso 1 1 calc GR . . . . H18B H 0.5975 0.3077 0.8188 0.041 Uiso 1 1 calc GR . . . . H18C H 0.6578 0.2072 0.8087 0.041 Uiso 1 1 calc GR . . . . C19 C 0.5584(2) 0.52662(16) 0.83436(14) 0.0293(4) Uani 1 1 d . . . . . H19A H 0.5059 0.4751 0.8553 0.044 Uiso 1 1 calc GR . . . . H19B H 0.5014 0.5726 0.8079 0.044 Uiso 1 1 calc GR . . . . H19C H 0.6055 0.5542 0.8831 0.044 Uiso 1 1 calc GR . . . . C20 C 0.7622(2) 0.40970(15) 0.57879(13) 0.0247(4) Uani 1 1 d . . . . . H20A H 0.8228 0.4469 0.6130 0.037 Uiso 1 1 calc GR . . . . H20B H 0.7189 0.4486 0.5358 0.037 Uiso 1 1 calc GR . . . . H20C H 0.8104 0.3609 0.5492 0.037 Uiso 1 1 calc GR . . . . C21 C 0.8372(2) 0.13501(15) 0.67411(13) 0.0251(4) Uani 1 1 d . . . . . C22 C 0.8670(2) 0.05961(16) 0.60766(15) 0.0310(5) Uani 1 1 d . . . . . H22A H 0.9527 0.0331 0.6199 0.046 Uiso 1 1 calc GR . . . . H22B H 0.8669 0.0860 0.5493 0.046 Uiso 1 1 calc GR . . . . H22C H 0.8004 0.0117 0.6114 0.046 Uiso 1 1 calc GR . . . . C23 C 0.8878(2) 0.69985(18) 0.59401(15) 0.0311(5) Uani 1 1 d . . . . . H23B H 0.9298 0.7577 0.5778 0.047 Uiso 1 1 calc GR . . . . H23A H 0.8857 0.6588 0.5438 0.047 Uiso 1 1 calc GR . . . . H23C H 0.9371 0.6709 0.6410 0.047 Uiso 1 1 calc GR . . . . C24 C 0.6730(2) 0.77252(17) 0.55173(14) 0.0313(5) Uani 1 1 d . . . . . H24A H 0.6721 0.7351 0.4990 0.047 Uiso 1 1 calc GR . . . . H24B H 0.7186 0.8303 0.5403 0.047 Uiso 1 1 calc GR . . . . H24C H 0.5832 0.7855 0.5696 0.047 Uiso 1 1 calc GR . . . . O25 O 1.08308(17) 0.46980(11) 0.65194(11) 0.0323(4) Uani 1 1 d . . . . . H25 H 1.1022 0.5055 0.6924 0.048 Uiso 1 1 calc GR . . . . C25 C 1.1192(3) 0.51040(18) 0.57089(16) 0.0366(5) Uani 1 1 d . . . . . H25A H 1.1184 0.5773 0.5764 0.055 Uiso 1 1 calc GR . . . . H25B H 1.0571 0.4917 0.5260 0.055 Uiso 1 1 calc GR . . . . H25C H 1.2068 0.4899 0.5548 0.055 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O2 0.0639(11) 0.0221(7) 0.0287(8) -0.0016(6) -0.0071(8) -0.0099(8) O3 0.0489(9) 0.0209(8) 0.0402(9) 0.0048(7) -0.0036(8) -0.0014(7) O11 0.0546(10) 0.0246(8) 0.0200(7) -0.0015(6) -0.0078(7) 0.0010(7) O21 0.0469(9) 0.0229(8) 0.0314(8) 0.0017(6) -0.0091(7) 0.0020(7) C1 0.0308(9) 0.0231(10) 0.0196(8) 0.0010(8) -0.0041(7) -0.0021(8) C2 0.0349(10) 0.0238(10) 0.0220(9) -0.0014(8) -0.0017(8) -0.0030(8) C3 0.0261(9) 0.0220(10) 0.0286(10) 0.0039(8) 0.0003(8) -0.0013(8) C4 0.0258(9) 0.0256(10) 0.0217(9) 0.0049(8) -0.0006(7) 0.0018(8) C5 0.0246(8) 0.0210(9) 0.0195(8) 0.0003(7) 0.0014(7) 0.0053(8) C6 0.0272(9) 0.0245(10) 0.0244(9) -0.0027(8) -0.0047(8) 0.0068(8) C7 0.0253(9) 0.0261(11) 0.0337(11) -0.0046(9) -0.0057(8) 0.0024(8) C8 0.0232(8) 0.0209(9) 0.0250(9) -0.0037(8) -0.0003(8) -0.0001(8) C9 0.0263(9) 0.0197(9) 0.0204(8) -0.0017(7) 0.0019(7) -0.0007(8) C10 0.0251(8) 0.0165(9) 0.0202(8) -0.0002(7) -0.0019(7) 0.0002(7) C11 0.0336(10) 0.0164(9) 0.0194(8) 0.0011(7) -0.0013(8) -0.0042(8) C12 0.0288(9) 0.0194(9) 0.0193(8) 0.0009(7) -0.0017(7) -0.0010(8) C13 0.0266(9) 0.0172(9) 0.0199(8) -0.0003(7) 0.0012(7) -0.0022(7) C14 0.0253(9) 0.0196(9) 0.0209(8) -0.0013(7) -0.0014(7) 0.0004(8) C15 0.0317(10) 0.0251(10) 0.0271(9) -0.0062(8) -0.0069(8) 0.0010(9) C16 0.0348(10) 0.0218(10) 0.0242(9) -0.0043(8) -0.0001(8) -0.0007(9) C17 0.0293(9) 0.0182(9) 0.0220(8) -0.0013(7) 0.0037(7) -0.0018(8) C18 0.0337(10) 0.0222(10) 0.0267(10) -0.0016(8) 0.0068(8) -0.0048(8) C19 0.0359(11) 0.0235(10) 0.0283(10) -0.0051(8) 0.0088(8) -0.0027(9) C20 0.0316(10) 0.0231(9) 0.0195(8) 0.0018(7) 0.0012(8) 0.0031(8) C21 0.0277(9) 0.0190(9) 0.0285(10) 0.0010(8) 0.0009(8) -0.0033(8) C22 0.0358(11) 0.0227(10) 0.0344(11) -0.0031(8) 0.0021(9) 0.0021(9) C23 0.0277(9) 0.0360(12) 0.0295(10) 0.0082(9) 0.0037(8) 0.0030(9) C24 0.0349(10) 0.0312(12) 0.0278(10) 0.0079(9) -0.0021(8) 0.0043(10) O25 0.0431(8) 0.0217(7) 0.0322(8) 0.0015(6) -0.0048(7) -0.0021(7) C25 0.0393(11) 0.0369(13) 0.0335(11) 0.0020(10) 0.0059(9) 0.0078(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 O2 H2 109.5 . . ? C2 C1 H1 118.0 . . ? C2 C1 C10 123.93(18) . . ? C10 C1 H1 118.0 . . ? O2 C2 C3 116.80(19) . . ? C1 C2 O2 121.24(19) . . ? C1 C2 C3 121.96(19) . . ? O3 C3 C2 120.0(2) . . ? O3 C3 C4 122.94(19) . . ? C2 C3 C4 116.97(18) . . ? C3 C4 C5 108.71(16) . . ? C3 C4 C23 106.28(17) . . ? C3 C4 C24 109.65(17) . . ? C5 C4 C23 109.98(17) . . ? C24 C4 C5 114.14(17) . . ? C24 C4 C23 107.79(17) . . ? C6 C5 C4 122.21(18) . . ? C6 C5 C10 122.66(19) . . ? C10 C5 C4 115.12(17) . . ? C5 C6 H6 117.5 . . ? C5 C6 C7 124.95(19) . . ? C7 C6 H6 117.5 . . ? C6 C7 H7A 108.4 . . ? C6 C7 H7B 108.4 . . ? C6 C7 C8 115.54(17) . . ? H7A C7 H7B 107.5 . . ? C8 C7 H7A 108.4 . . ? C8 C7 H7B 108.4 . . ? C7 C8 H8 105.4 . . ? C7 C8 C9 111.62(17) . . ? C7 C8 C14 114.38(17) . . ? C9 C8 H8 105.4 . . ? C14 C8 H8 105.4 . . ? C14 C8 C9 113.77(16) . . ? C8 C9 C10 113.22(15) . . ? C11 C9 C8 113.50(16) . . ? C11 C9 C10 103.56(15) . . ? C19 C9 C8 106.87(16) . . ? C19 C9 C10 110.06(16) . . ? C19 C9 C11 109.62(16) . . ? C1 C10 C5 111.14(16) . . ? C1 C10 C9 111.13(15) . . ? C1 C10 H10 106.6 . . ? C5 C10 C9 114.30(16) . . ? C5 C10 H10 106.6 . . ? C9 C10 H10 106.6 . . ? O11 C11 C9 119.97(18) . . ? O11 C11 C12 119.51(19) . . ? C12 C11 C9 120.48(16) . . ? C11 C12 H12A 110.1 . . ? C11 C12 H12B 110.1 . . ? C11 C12 C13 108.11(16) . . ? H12A C12 H12B 108.4 . . ? C13 C12 H12A 110.1 . . ? C13 C12 H12B 110.1 . . ? C12 C13 C14 109.24(16) . . ? C12 C13 C18 106.79(16) . . ? C17 C13 C12 121.73(17) . . ? C17 C13 C14 100.82(15) . . ? C17 C13 C18 104.95(16) . . ? C18 C13 C14 113.46(17) . . ? C8 C14 C13 107.92(15) . . ? C8 C14 C15 116.60(16) . . ? C8 C14 C20 113.28(17) . . ? C15 C14 C13 101.21(16) . . ? C20 C14 C13 112.30(16) . . ? C20 C14 C15 105.00(16) . . ? C14 C15 H15A 111.5 . . ? C14 C15 H15B 111.5 . . ? H15A C15 H15B 109.3 . . ? C16 C15 C14 101.56(16) . . ? C16 C15 H15A 111.5 . . ? C16 C15 H15B 111.5 . . ? C15 C16 H16 124.0 . . ? C17 C16 C15 112.06(18) . . ? C17 C16 H16 124.0 . . ? C16 C17 C13 108.93(18) . . ? C16 C17 C21 124.88(19) . . ? C21 C17 C13 124.68(17) . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C9 C19 H19A 109.5 . . ? C9 C19 H19B 109.5 . . ? C9 C19 H19C 109.5 . . ? H19A C19 H19B 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C14 C20 H20A 109.5 . . ? C14 C20 H20B 109.5 . . ? C14 C20 H20C 109.5 . . ? H20A C20 H20B 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? O21 C21 C17 120.13(19) . . ? O21 C21 C22 120.1(2) . . ? C17 C21 C22 119.70(18) . . ? C21 C22 H22A 109.5 . . ? C21 C22 H22B 109.5 . . ? C21 C22 H22C 109.5 . . ? H22A C22 H22B 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? C4 C23 H23B 109.5 . . ? C4 C23 H23A 109.5 . . ? C4 C23 H23C 109.5 . . ? H23B C23 H23A 109.5 . . ? H23B C23 H23C 109.5 . . ? H23A C23 H23C 109.5 . . ? C4 C24 H24A 109.5 . . ? C4 C24 H24B 109.5 . . ? C4 C24 H24C 109.5 . . ? H24A C24 H24B 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C25 O25 H25 109.5 . . ? O25 C25 H25A 109.5 . . ? O25 C25 H25B 109.5 . . ? O25 C25 H25C 109.5 . . ? H25A C25 H25B 109.5 . . ? H25A C25 H25C 109.5 . . ? H25B C25 H25C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O2 H2 0.8200 . ? O2 C2 1.361(3) . ? O3 C3 1.222(3) . ? O11 C11 1.217(2) . ? O21 C21 1.229(3) . ? C1 H1 0.9300 . ? C1 C2 1.339(3) . ? C1 C10 1.505(3) . ? C2 C3 1.477(3) . ? C3 C4 1.524(3) . ? C4 C5 1.527(3) . ? C4 C23 1.545(3) . ? C4 C24 1.527(3) . ? C5 C6 1.327(3) . ? C5 C10 1.516(3) . ? C6 H6 0.9300 . ? C6 C7 1.494(3) . ? C7 H7A 0.9700 . ? C7 H7B 0.9700 . ? C7 C8 1.532(3) . ? C8 H8 0.9800 . ? C8 C9 1.572(3) . ? C8 C14 1.532(3) . ? C9 C10 1.581(3) . ? C9 C11 1.557(3) . ? C9 C19 1.539(3) . ? C10 H10 0.9800 . ? C11 C12 1.526(3) . ? C12 H12A 0.9700 . ? C12 H12B 0.9700 . ? C12 C13 1.532(3) . ? C13 C14 1.565(3) . ? C13 C17 1.526(3) . ? C13 C18 1.548(3) . ? C14 C15 1.550(3) . ? C14 C20 1.541(3) . ? C15 H15A 0.9700 . ? C15 H15B 0.9700 . ? C15 C16 1.503(3) . ? C16 H16 0.9300 . ? C16 C17 1.345(3) . ? C17 C21 1.462(3) . ? C18 H18A 0.9600 . ? C18 H18B 0.9600 . ? C18 H18C 0.9600 . ? C19 H19A 0.9600 . ? C19 H19B 0.9600 . ? C19 H19C 0.9600 . ? C20 H20A 0.9600 . ? C20 H20B 0.9600 . ? C20 H20C 0.9600 . ? C21 C22 1.503(3) . ? C22 H22A 0.9600 . ? C22 H22B 0.9600 . ? C22 H22C 0.9600 . ? C23 H23B 0.9600 . ? C23 H23A 0.9600 . ? C23 H23C 0.9600 . ? C24 H24A 0.9600 . ? C24 H24B 0.9600 . ? C24 H24C 0.9600 . ? O25 H25 0.8200 . ? O25 C25 1.403(3) . ? C25 H25A 0.9600 . ? C25 H25B 0.9600 . ? C25 H25C 0.9600 . ?