#------------------------------------------------------------------------------ #$Date: 2024-04-04 11:34:15 +0300 (Thu, 04 Apr 2024) $ #$Revision: 290785 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/83/7248381.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7248381 loop_ _publ_author_name 'Sun, Jie' 'Wang, Chaodong' 'Wu, Chunlei' 'Wang, Wenjian' 'Zeng, Yue' 'Song, Shengjie' 'Chen, Zhiwei' 'Li, Jianjun' _publ_section_title ; Photocatalyst-free H2O-regulated and regiodivergent multicomponent hydrogenation/bifunctional sulfonylation of alkynes ; _journal_issue 6 _journal_name_full 'Green Chemistry' _journal_page_first 3301 _journal_page_last 3307 _journal_paper_doi 10.1039/D3GC04960D _journal_volume 26 _journal_year 2024 _chemical_formula_moiety 'C27 H21 F2 N O6 S' _chemical_formula_sum 'C27 H21 F2 N O6 S' _chemical_formula_weight 525.534 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _symmetry_Int_Tables_number 14 _atom_sites_solution_primary iterative _audit_creation_date 2023-04-13 _audit_creation_method ; Olex2 1.5 (compiled 2023.03.06 svn.rbb2c1857 for OlexSys, GUI svn.r6748) ; _audit_update_record ; 2023-04-13 deposited with the CCDC. 2024-01-26 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 91.730(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.2939(4) _cell_length_b 9.7381(4) _cell_length_c 25.5602(11) _cell_measurement_reflns_used 9865 _cell_measurement_temperature 170.00 _cell_measurement_theta_max 27.34 _cell_measurement_theta_min 2.50 _cell_volume 2561.06(18) _computing_cell_refinement 'SAINT V8.40B (?, 2016)' _computing_data_collection 'Bruker Instrument Service vV6.2.14' _computing_data_reduction 'SAINT V8.40B (?, 2016)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine 1.5 (Bourhis et al., 2015)' _computing_structure_solution 'olex2.solve 1.5 (Bourhis et al., 2015)' _diffrn_ambient_temperature 170.00 _diffrn_measured_fraction_theta_full 0.9994 _diffrn_measured_fraction_theta_max 0.9992 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0797 _diffrn_reflns_av_unetI/netI 0.0343 _diffrn_reflns_Laue_measured_fraction_full 0.9994 _diffrn_reflns_Laue_measured_fraction_max 0.9992 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 33 _diffrn_reflns_limit_l_min -33 _diffrn_reflns_number 61900 _diffrn_reflns_point_group_measured_fraction_full 0.9994 _diffrn_reflns_point_group_measured_fraction_max 0.9992 _diffrn_reflns_theta_full 25.2417 _diffrn_reflns_theta_max 27.51 _diffrn_reflns_theta_min 2.50 _diffrn_source_current 1.4 _diffrn_source_power 0.07 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.183 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.7118 _exptl_absorpt_correction_type none _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1229 before and 0.0687 after correction. The Ratio of minimum to maximum transmission is 0.9547. The \l/2 correction factor is Not present. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.363 _exptl_crystal_description block _exptl_crystal_F_000 1089.319 _exptl_crystal_size_max 0.4 _exptl_crystal_size_mid 0.23 _exptl_crystal_size_min 0.16 _refine_diff_density_max 0.3399 _refine_diff_density_min -0.4370 _refine_diff_density_rms 0.0742 _refine_ls_d_res_high 0.7693 _refine_ls_d_res_low 8.1340 _refine_ls_goodness_of_fit_ref 1.0574 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_constraints 49 _refine_ls_number_parameters 390 _refine_ls_number_reflns 5903 _refine_ls_number_restraints 222 _refine_ls_restrained_S_all 1.0368 _refine_ls_R_factor_all 0.0662 _refine_ls_R_factor_gt 0.0446 _refine_ls_shift/su_max 1.4494 _refine_ls_shift/su_mean 0.0719 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0455P)^2^+1.2739P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1016 _refine_ls_wR_factor_ref 0.1122 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 13 _reflns_limit_h_min -13 _reflns_limit_k_max 12 _reflns_limit_k_min 0 _reflns_limit_l_max 33 _reflns_limit_l_min 0 _reflns_number_gt 4458 _reflns_number_total 5903 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL mo_230411_sj_p_och3_0m_a.res in P2(1)/c REM Old TITL mo_230411_SJ_P_OCH3_0m in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.160, Rweak 0.010, Alpha 0.032 REM 0.501 for 327 systematic absences, Orientation as input REM Formula found by SHELXT: C27 F2 N3 O5 S CELL 0.71073 10.2939 9.7381 25.5602 90 91.73 90 ZERR 4 0.0004 0.0004 0.0011 0 0.002 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H F N O S UNIT 108 84 8 4 24 4 SADI N1 C22 N1 C22A SADI C22 C23 C22A C23A SADI C22 C27 C22A C27A SADI 0.04 C25 C27 C25A C27A SADI C25 C24 C25A C24A SADI 0.04 C24 C26 C24A C26A SADI C25 C26 C25A C26A SADI C23 C24 C23A C24A SADI 0.04 C25 C23 C25A C23A SADI C27 C26 C27A C26A SADI 0.04 C23 C27 C23A C27A SADI 0.04 N1 C23 N1 C23A SADI 0.04 N1 C27 N1 C27A SADI 0.04 C22 C24 C22A C24A SADI 0.04 C22 C26 C22A C26A SIMU 0.01 0.02 2 N1 C22 > C27A L.S. 4 0 0 PLAN 1 SIZE 0.16 0.23 0.4 TEMP -103.15 CONF BOND list 4 MORE -1 HTAB BOND $H ABIN fmap 2 53 acta OMIT 0 1 1 WGHT 0.045508 1.273869 FVAR 0.371387 0.655774 REM REM REM S1 6 0.88320 0.22517 0.75174 11.00000 0.02645 0.02091 0.03244 = 0.00225 0.00413 -0.00052 F1 3 0.95502 0.60297 0.86887 11.00000 0.03492 0.03359 0.03774 = -0.00174 0.00234 -0.00549 F2 3 0.91077 0.41640 0.91102 11.00000 0.03846 0.04019 0.03032 = 0.00896 -0.00356 0.00577 O1 5 1.11069 0.68364 0.50873 11.00000 0.06600 0.04015 0.03432 = 0.00850 0.00969 -0.00465 O2 5 1.12952 0.40517 0.65616 11.00000 0.02339 0.02899 0.03398 = 0.00442 0.00430 0.00155 O3 5 1.15727 0.29098 0.72949 11.00000 0.02545 0.03450 0.04411 = 0.01046 -0.00149 0.00512 O4 5 0.74488 0.21133 0.74712 11.00000 0.02758 0.03111 0.04029 = 0.00004 0.00488 -0.00694 O5 5 0.96012 0.10211 0.75123 11.00000 0.04191 0.02002 0.04119 = 0.00395 0.00913 0.00500 O6 5 0.72800 0.65199 0.92587 11.00000 0.04567 0.06666 0.04598 = -0.02213 0.00443 0.01157 N1 4 0.64001 0.49108 0.86798 11.00000 0.02386 0.04302 0.03369 = 0.00002 0.00552 0.00554 C1 1 0.84839 0.57257 0.59258 11.00000 0.03555 0.03040 0.03446 = 0.00051 -0.00283 0.00305 AFIX 43 H1 2 0.75725 0.58278 0.59599 11.00000 -1.20000 AFIX 0 C2 1 0.90848 0.63864 0.55242 11.00000 0.05236 0.03053 0.03124 = 0.00308 -0.00495 0.00110 AFIX 43 H2 2 0.85924 0.69383 0.52845 11.00000 -1.20000 AFIX 0 C3 1 1.04230 0.62413 0.54709 11.00000 0.05243 0.02594 0.02752 = -0.00066 0.00642 -0.00605 C4 1 1.11499 0.54407 0.58202 11.00000 0.03716 0.02869 0.03265 = -0.00392 0.00654 -0.00275 AFIX 43 H4 2 1.20605 0.53388 0.57838 11.00000 -1.20000 AFIX 0 C5 1 1.05238 0.47964 0.62209 11.00000 0.03119 0.01941 0.02877 = -0.00149 0.00199 -0.00022 C6 1 0.91839 0.49025 0.62873 11.00000 0.02917 0.02098 0.02832 = -0.00146 0.00068 0.00015 C7 1 0.85927 0.41427 0.67019 11.00000 0.02426 0.01959 0.03029 = -0.00573 -0.00108 -0.00125 C8 1 0.93804 0.33488 0.70172 11.00000 0.02386 0.01798 0.02873 = -0.00121 0.00232 0.00020 C9 1 1.07993 0.33934 0.69847 11.00000 0.02604 0.01972 0.03400 = 0.00035 0.00417 0.00184 C10 1 1.04256 0.77078 0.47253 11.00000 0.08445 0.04211 0.03377 = 0.00842 -0.00296 -0.01046 AFIX 137 H10a 2 1.10071 0.79805 0.44471 11.00000 -1.50000 H10b 2 0.96767 0.72142 0.45722 11.00000 -1.50000 H10c 2 1.01243 0.85281 0.49077 11.00000 -1.50000 AFIX 0 C11 1 0.71641 0.43474 0.67684 11.00000 0.02295 0.02308 0.03265 = 0.00071 -0.00182 0.00057 C12 1 0.67651 0.55146 0.70296 11.00000 0.02585 0.02615 0.03549 = 0.00023 -0.00341 0.00117 AFIX 43 H12 2 0.73898 0.61571 0.71595 11.00000 -1.20000 AFIX 0 C13 1 0.54462 0.57430 0.71010 11.00000 0.03158 0.03497 0.04479 = -0.00248 0.00042 0.00942 AFIX 43 H13 2 0.51725 0.65291 0.72882 11.00000 -1.20000 AFIX 0 C14 1 0.45388 0.48296 0.69002 11.00000 0.02317 0.04650 0.06511 = 0.00004 0.00018 0.00495 AFIX 43 H14 2 0.36402 0.49807 0.69523 11.00000 -1.20000 AFIX 0 C15 1 0.49338 0.36989 0.66244 11.00000 0.02660 0.04386 0.07335 = -0.00667 -0.00822 -0.00689 AFIX 43 H15 2 0.43027 0.30867 0.64782 11.00000 -1.20000 AFIX 0 C16 1 0.62448 0.34431 0.65576 11.00000 0.02905 0.03037 0.05525 = -0.00935 -0.00276 -0.00033 AFIX 43 H16 2 0.65114 0.26560 0.63693 11.00000 -1.20000 AFIX 0 C17 1 0.92250 0.31383 0.81116 11.00000 0.02439 0.02943 0.03044 = 0.00127 0.00152 0.00336 AFIX 23 H17a 2 0.92140 0.24762 0.84053 11.00000 -1.20000 H17b 2 1.01186 0.35075 0.80934 11.00000 -1.20000 AFIX 0 C18 1 0.82996 0.43148 0.82256 11.00000 0.02321 0.02689 0.02753 = 0.00337 0.00224 0.00183 AFIX 13 H18 2 0.83317 0.49927 0.79324 11.00000 -1.20000 AFIX 0 C19 1 0.86330 0.50469 0.87304 11.00000 0.02612 0.03012 0.02961 = 0.00479 -0.00085 0.00156 C20 1 0.73539 0.56277 0.89310 11.00000 0.03121 0.04380 0.02994 = 0.00107 0.00237 0.00694 C21 1 0.68742 0.39045 0.83006 11.00000 0.02472 0.03715 0.03475 = -0.00203 0.00389 0.00119 AFIX 23 H21a 2 0.68138 0.29587 0.84398 11.00000 -1.20000 H21b 2 0.63684 0.39600 0.79656 11.00000 -1.20000 AFIX 0 PART 1 C22 1 0.50800 0.49480 0.88297 21.00000 0.02698 0.04225 0.03738 = 0.00320 0.00235 0.00457 C23 1 0.41636 0.43958 0.84891 21.00000 0.03594 0.06086 0.06075 = -0.01688 0.00848 -0.00177 AFIX 43 H23 2 0.44078 0.40704 0.81557 21.00000 -1.20000 AFIX 0 C24 1 0.28762 0.43168 0.86358 21.00000 0.03320 0.07300 0.07463 = -0.01373 0.00551 -0.00825 AFIX 43 H24 2 0.22437 0.39439 0.83976 21.00000 -1.20000 AFIX 0 C25 1 0.25026 0.47602 0.91117 21.00000 0.02719 0.06773 0.05562 = 0.00472 0.01401 0.00762 AFIX 43 H25 2 0.16410 0.46167 0.92231 21.00000 -1.20000 AFIX 0 C26 1 0.33971 0.54163 0.94247 21.00000 0.03521 0.08775 0.04323 = -0.00055 0.00973 0.01428 AFIX 43 H26 2 0.31281 0.58161 0.97427 21.00000 -1.20000 AFIX 0 C27 1 0.46857 0.55171 0.92930 21.00000 0.02963 0.07945 0.03540 = -0.00524 0.00060 0.01037 AFIX 43 H27 2 0.52940 0.59738 0.95193 21.00000 -1.20000 AFIX 0 PART 2 C22A 1 0.50066 0.47833 0.87781 -21.00000 0.02551 0.05433 0.03204 = -0.00065 0.00529 0.00830 C23A 1 0.40828 0.47648 0.83871 -21.00000 0.02455 0.04123 0.02922 = 0.00824 -0.00178 -0.00216 AFIX 43 H23A 2 0.43368 0.48568 0.80345 -21.00000 -1.20000 AFIX 0 C24A 1 0.27920 0.46163 0.84909 -21.00000 0.02622 0.04533 0.03277 = 0.01365 -0.00321 -0.00147 AFIX 43 H24A 2 0.21630 0.45595 0.82120 -21.00000 -1.20000 AFIX 0 C25A 1 0.24219 0.45513 0.89911 -21.00000 0.02661 0.07247 0.04011 = -0.00336 0.00175 0.00092 AFIX 43 H25A 2 0.15228 0.45664 0.90646 -21.00000 -1.20000 AFIX 0 C26A 1 0.33603 0.44600 0.94131 -21.00000 0.03901 0.09630 0.03816 = -0.00484 0.01048 -0.00259 AFIX 43 H26A 2 0.31036 0.43203 0.97630 -21.00000 -1.20000 AFIX 0 C27A 1 0.46695 0.45839 0.92920 -21.00000 0.03337 0.09236 0.03792 = -0.00219 0.00159 0.00190 AFIX 43 H27A 2 0.53242 0.45314 0.95613 -21.00000 -1.20000 AFIX 0 HKLF 4 END Q1 1 0.611111 0.555556 0.711111 11 0.05 0.34 REM The information below was added by Olex2. REM REM R1 = 0.0446 for 4458 Fo > 4sig(Fo) and 0.0662 for all 5903 data REM 390 parameters refined using 222 restraints REM Highest difference peak 0.3399, deepest hole -0.4370 REM Mean Shift 0.0719, Max Shift 1.4494. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0662 REM R1_gt = 0.0446 REM wR_ref = 0.1122 REM GOOF = 1.0574 REM Shift_max = 1.4494 REM Shift_mean = 0.0719 REM Reflections_all = 5903 REM Reflections_gt = 4458 REM Parameters = 390 REM Hole = -0.4370 REM Peak = 0.3399 REM Flack = n/a ; _cod_data_source_file d3gc04960d2.cif _cod_data_source_block mo_230411_SJ_P_OCH3_0m _cod_original_formula_sum 'C27 H21 F2 N1 O6 S1' _cod_database_code 7248381 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances N1-C22 \\sim N1-C22A with sigma of 0.02 C22-C23 \\sim C22A-C23A with sigma of 0.02 C22-C27 \\sim C22A-C27A with sigma of 0.02 C25-C27 \\sim C25A-C27A with sigma of 0.04 C25-C24 \\sim C25A-C24A with sigma of 0.02 C24-C26 \\sim C24A-C26A with sigma of 0.04 C25-C26 \\sim C25A-C26A with sigma of 0.02 C23-C24 \\sim C23A-C24A with sigma of 0.02 C25-C23 \\sim C25A-C23A with sigma of 0.04 C27-C26 \\sim C27A-C26A with sigma of 0.02 C23-C27 \\sim C23A-C27A with sigma of 0.04 N1-C23 \\sim N1-C23A with sigma of 0.04 N1-C27 \\sim N1-C27A with sigma of 0.04 C22-C24 \\sim C22A-C24A with sigma of 0.04 C22-C26 \\sim C22A-C26A with sigma of 0.04 3. Uiso/Uaniso restraints and constraints N1 \\sim C22 \\sim C23 \\sim C24 \\sim C25 \\sim C26 \\sim C27 \\sim C22A \\sim C23A \\sim C24A \\sim C25A \\sim C26A \\sim C27A: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A 4. Others Sof(C22A)=Sof(C23A)=Sof(H23A)=Sof(C24A)=Sof(H24A)=Sof(C25A)=Sof(H25A)= Sof(C26A)=Sof(H26A)=Sof(C27A)=Sof(H27A)=1-FVAR(1) Sof(C22)=Sof(C23)=Sof(H23)=Sof(C24)=Sof(H24)=Sof(C25)=Sof(H25)=Sof(C26)= Sof(H26)=Sof(C27)=Sof(H27)=FVAR(1) 5.a Ternary CH refined with riding coordinates: C18(H18) 5.b Secondary CH2 refined with riding coordinates: C17(H17a,H17b), C21(H21a,H21b) 5.c Aromatic/amide H refined with riding coordinates: C1(H1), C2(H2), C4(H4), C12(H12), C13(H13), C14(H14), C15(H15), C16(H16), C23(H23), C24(H24), C25(H25), C26(H26), C27(H27), C23A(H23A), C24A(H24A), C25A(H25A), C26A(H26A), C27A(H27A) 5.d Idealised Me refined as rotating group: C10(H10a,H10b,H10c) ; _shelx_fab_file ; -13 0 2 -0.3395 -0.0084 -13 0 4 0.2143 -0.0051 -13 0 6 0.0101 0.0042 -13 0 8 -0.0807 0.0127 -13 1 1 -0.8313 -0.0035 -13 1 2 -0.4544 -0.0008 -13 1 3 -0.0283 -0.0026 -13 1 4 0.3360 0.0002 -13 1 5 0.1187 0.0050 -13 1 6 0.8006 0.0001 -13 1 7 -0.0372 0.0149 -13 1 8 0.8102 -0.0018 -13 2 1 -0.5064 0.0013 -13 2 2 -0.4259 0.0004 -13 2 3 0.0741 0.0032 -13 2 4 -0.1166 0.0026 -13 2 5 0.7437 0.0034 -13 2 6 -0.0444 0.0094 -12 0 2 -0.2614 -0.0017 -12 0 4 -1.2274 -0.0015 -12 0 6 -0.9543 -0.0049 -12 0 8 -0.6395 -0.0096 -12 0 10 -0.6465 -0.0102 -12 0 12 -0.2592 -0.0082 -12 0 14 0.5090 -0.0078 -12 1 1 0.5825 -0.0028 -12 1 2 1.1123 0.0001 -12 1 3 -0.5401 -0.0022 -12 1 4 0.2138 -0.0011 -12 1 5 -0.7197 -0.0052 -12 1 6 -0.5436 -0.0014 -12 1 7 -0.3790 -0.0111 -12 1 8 -0.8386 0.0008 -12 1 9 -0.2652 -0.0096 -12 1 10 -1.1291 0.0026 -12 1 11 -0.1115 0.0005 -12 1 12 -1.4421 0.0010 -12 1 13 0.4264 0.0072 -12 1 14 -1.2980 -0.0027 -12 1 15 0.8230 0.0037 -12 2 1 1.0477 -0.0017 -12 2 2 0.2716 -0.0006 -12 2 3 0.6108 -0.0020 -12 2 4 0.0859 -0.0016 -12 2 5 -0.2722 -0.0014 -12 2 6 0.1308 -0.0073 -12 2 7 -0.5774 -0.0012 -12 2 8 0.2302 -0.0096 -12 2 9 -0.6739 -0.0009 -12 2 10 0.2770 -0.0021 -12 2 11 -1.0486 0.0008 -12 2 12 0.3754 0.0089 -12 2 13 -1.1679 0.0015 -12 2 14 0.4793 0.0125 -12 3 1 0.1883 -0.0000 -12 3 2 0.1366 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0 4 15 3.0729 0.0017 0 4 16 -0.2584 -0.0013 0 4 17 2.5094 0.0016 0 4 18 -0.7598 -0.0011 0 4 19 1.3959 0.0005 0 4 20 -0.5790 0.0007 0 4 21 0.5009 -0.0010 0 4 22 -0.0452 0.0026 0 4 23 -0.0755 -0.0014 0 4 24 0.2175 0.0024 0 4 25 -0.7263 -0.0002 0 4 26 0.2597 0.0010 0 4 27 -1.4038 0.0006 0 4 28 0.4498 0.0008 0 4 29 -1.4714 -0.0001 0 4 30 0.6719 0.0014 0 4 31 -0.7406 -0.0007 0 5 1 -1.5364 0.0005 0 5 2 -2.0109 -0.0010 0 5 3 -1.9430 -0.0001 0 5 4 -3.0948 -0.0011 0 5 5 -2.2248 0.0001 0 5 6 -2.5479 -0.0001 0 5 7 -2.5147 0.0016 0 5 8 -0.7743 0.0006 0 5 9 -3.1842 0.0017 0 5 10 0.9343 0.0007 0 5 11 -3.6448 -0.0004 0 5 12 1.8608 0.0006 0 5 13 -3.0746 -0.0020 0 5 14 2.1293 0.0001 0 5 15 -1.7102 -0.0021 0 5 16 1.7937 -0.0002 0 5 17 -0.3353 -0.0015 0 5 18 0.9382 -0.0003 0 5 19 0.6778 -0.0002 0 5 20 0.1907 -0.0009 0 5 21 1.1991 0.0015 0 5 22 -0.0501 -0.0013 0 5 23 1.1582 0.0019 0 5 24 -0.2527 -0.0010 0 5 25 0.8223 0.0006 0 5 26 -0.7523 -0.0016 0 5 27 0.5420 -0.0007 0 5 28 -1.0142 -0.0033 0 5 29 0.3339 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-0.0004 0 7 16 -0.6464 0.0025 0 7 17 0.6662 -0.0010 0 7 18 -0.6924 0.0036 0 7 19 0.3035 -0.0001 0 7 20 -0.4391 0.0015 0 7 21 -0.4889 0.0002 0 7 22 0.0858 -0.0007 0 7 23 -0.7069 -0.0005 0 7 24 0.4063 -0.0009 0 7 25 -0.4226 -0.0005 0 7 26 0.3151 0.0004 0 7 27 -0.3505 0.0001 0 8 0 -0.9510 0.0001 0 8 1 -0.0637 -0.0001 0 8 2 -0.8572 -0.0003 0 8 3 -0.0980 -0.0005 0 8 4 -0.5981 -0.0005 0 8 5 -0.1633 -0.0000 0 8 6 -0.0404 0.0003 0 8 7 -0.3934 0.0004 0 8 8 0.8392 0.0018 0 8 9 -0.3799 -0.0005 0 8 10 1.4032 0.0025 0 8 11 -0.0517 -0.0014 0 8 12 1.1772 0.0008 0 8 13 -0.0739 -0.0001 0 8 14 0.7462 -0.0017 0 8 15 -0.4768 0.0027 0 8 16 0.5794 -0.0019 0 8 17 -0.3928 0.0041 0 8 18 0.0788 0.0003 0 8 19 0.2952 0.0033 0 8 20 -0.9479 0.0015 0 8 21 0.7211 0.0016 0 8 22 -1.4528 0.0003 0 8 23 0.5831 0.0004 0 8 24 -0.9163 -0.0010 0 8 25 0.3477 0.0004 0 9 1 -0.1028 -0.0013 0 9 2 -0.4366 0.0002 0 9 3 0.1760 -0.0013 0 9 4 -0.9011 -0.0008 0 9 5 0.7524 -0.0008 0 9 6 -1.2977 -0.0014 0 9 7 1.1667 0.0004 0 9 8 -1.0880 -0.0009 0 9 9 1.0212 0.0011 0 9 10 -0.2131 0.0002 0 9 11 0.7020 -0.0003 0 9 12 0.1615 0.0010 0 9 13 0.6425 -0.0027 0 9 14 -0.5193 0.0009 0 9 15 0.4974 -0.0029 0 9 16 -0.8660 0.0006 0 9 17 -0.1316 -0.0002 0 9 18 0.1146 0.0012 0 9 19 -0.8631 0.0024 0 9 20 1.1741 0.0029 0 9 21 -1.0792 0.0022 0 9 22 1.0408 0.0040 0 9 23 -0.7158 0.0003 0 10 0 0.4546 -0.0023 0 10 1 -0.3302 0.0003 0 10 2 0.8125 -0.0012 0 10 3 -0.9448 0.0001 0 10 4 1.5834 0.0001 0 10 5 -1.1481 -0.0009 0 10 6 1.8740 0.0001 0 10 7 -0.5574 -0.0007 0 10 8 1.1705 -0.0006 0 10 9 0.3061 0.0013 0 10 10 0.4241 -0.0011 0 10 11 0.3506 0.0029 0 10 12 0.6000 -0.0017 0 10 13 -0.5355 0.0018 0 10 14 0.8568 -0.0019 0 10 15 -1.1643 -0.0010 0 10 16 0.1472 -0.0006 0 10 17 -0.6831 -0.0025 0 10 18 -0.7216 0.0013 0 10 19 0.2913 -0.0006 0 10 20 -0.6358 0.0020 0 11 1 0.9077 -0.0016 0 11 2 -0.6149 -0.0006 0 11 3 1.3551 0.0007 0 11 4 -0.6640 -0.0003 0 11 5 1.4788 0.0018 0 11 6 0.1862 0.0006 0 11 7 0.9505 0.0003 0 11 8 1.1091 0.0016 0 11 9 0.4706 -0.0013 0 11 10 0.8581 0.0032 0 11 11 0.6358 -0.0016 0 11 12 -0.2595 0.0039 0 11 13 0.8684 -0.0011 0 11 14 -0.8702 0.0022 0 11 15 0.4101 -0.0003 0 11 16 -0.6849 -0.0009 0 12 0 0.5411 -0.0013 0 12 1 -0.1361 -0.0008 0 12 2 0.5766 -0.0004 0 12 3 -0.1323 -0.0007 0 12 4 0.4070 0.0011 0 12 5 0.3746 0.0014 0 12 6 0.0030 0.0014 0 12 7 0.8894 0.0026 0 12 8 -0.0023 0.0001 0 12 9 0.7307 0.0027 0 12 10 0.4528 -0.0016 1 0 2 -66.6466 -0.0280 1 0 4 -48.9625 -0.0194 1 0 6 -26.2699 -0.0087 1 0 8 -7.5855 -0.0039 1 0 10 2.1126 -0.0028 1 0 12 4.2275 0.0001 1 0 14 2.8463 0.0043 1 0 16 0.6199 0.0059 1 0 18 -1.2452 0.0028 1 0 20 -1.8453 -0.0025 1 0 22 -1.1826 -0.0051 1 0 24 -0.3056 -0.0034 1 0 26 0.1709 -0.0005 1 0 28 0.5485 0.0010 1 0 30 0.8974 0.0020 1 0 32 0.7997 0.0027 1 1 0 4.8557 0.0020 1 1 1 -47.2193 -0.0195 1 1 2 -7.6104 0.0008 1 1 3 -39.7420 -0.0130 1 1 4 -15.5882 -0.0014 1 1 5 -26.4866 -0.0041 1 1 6 -15.9745 -0.0008 1 1 7 -12.7792 -0.0018 1 1 8 -10.1252 0.0016 1 1 9 -3.4518 -0.0032 1 1 10 -2.6598 0.0019 1 1 11 0.4098 -0.0024 1 1 12 2.5581 -0.0007 1 1 13 1.0058 -0.0005 1 1 14 4.7717 -0.0026 1 1 15 0.5848 -0.0001 1 1 16 4.8944 -0.0006 1 1 17 -0.0377 -0.0003 1 1 18 3.6947 0.0029 1 1 19 -0.5171 -0.0000 1 1 20 1.9904 0.0030 1 1 21 -0.4743 -0.0006 1 1 22 0.7877 -0.0003 1 1 23 -0.0274 -0.0025 1 1 24 0.3060 -0.0018 1 1 25 0.3314 -0.0032 1 1 26 -0.0236 0.0009 1 1 27 0.4424 -0.0009 1 1 28 -0.3331 0.0030 1 1 29 0.4655 0.0021 1 1 30 -0.2151 0.0020 1 1 31 0.4153 0.0016 1 1 32 0.2232 0.0011 1 2 0 -5.1974 -0.0012 1 2 1 -2.8303 0.0008 1 2 2 -5.6029 -0.0002 1 2 3 -13.1173 -0.0021 1 2 4 -6.8643 0.0019 1 2 5 -17.0398 -0.0006 1 2 6 -7.8618 0.0024 1 2 7 -13.4920 0.0021 1 2 8 -7.9433 0.0013 1 2 9 -5.9565 0.0017 1 2 10 -7.1028 0.0002 1 2 11 0.5611 -0.0001 1 2 12 -5.4579 -0.0008 1 2 13 3.7956 -0.0005 1 2 14 -3.1245 -0.0023 1 2 15 4.5052 0.0002 1 2 16 -0.6262 -0.0033 1 2 17 3.8318 0.0008 1 2 18 1.1106 -0.0016 1 2 19 2.3722 0.0009 1 2 20 1.5870 0.0017 1 2 21 0.9517 -0.0001 1 2 22 1.3016 0.0023 1 2 23 0.2868 -0.0011 1 2 24 1.0381 -0.0005 1 2 25 0.1436 -0.0007 1 2 26 0.8551 -0.0017 1 2 27 -0.0408 0.0015 1 2 28 0.3786 0.0006 1 2 29 -0.2055 0.0047 1 2 30 -0.2356 0.0020 1 2 31 -0.0822 0.0073 1 2 32 -0.4550 0.0004 1 3 0 -0.7683 0.0010 1 3 1 12.3156 0.0036 1 3 2 -3.1662 0.0008 1 3 3 7.9590 0.0011 1 3 4 -4.7985 0.0001 1 3 5 0.7378 -0.0004 1 3 6 -4.5020 0.0002 1 3 7 -5.7741 0.0008 1 3 8 -2.3864 0.0004 1 3 9 -8.9399 0.0015 1 3 10 -0.2482 0.0002 1 3 11 -8.5499 0.0002 1 3 12 0.4723 0.0005 1 3 13 -5.9692 -0.0009 1 3 14 0.1490 0.0010 1 3 15 -2.5823 -0.0015 1 3 16 -0.1826 0.0005 1 3 17 0.4207 -0.0017 1 3 18 -0.2424 -0.0010 1 3 19 1.9604 -0.0006 1 3 20 -0.2355 -0.0018 1 3 21 1.9225 0.0010 1 3 22 -0.1445 -0.0007 1 3 23 1.3570 0.0011 1 3 24 0.1663 0.0006 1 3 25 1.0503 0.0001 1 3 26 0.5694 0.0011 1 3 27 0.6932 -0.0001 1 3 28 0.7118 0.0026 1 3 29 -0.0343 0.0001 1 3 30 0.4141 0.0058 1 3 31 -0.6081 0.0004 1 3 32 -0.0579 0.0078 1 4 0 6.9370 -0.0009 1 4 1 -0.0826 0.0007 1 4 2 6.0475 -0.0020 1 4 3 2.6320 0.0011 1 4 4 2.9933 -0.0027 1 4 5 3.5336 -0.0003 1 4 6 -0.8771 -0.0016 1 4 7 2.8180 -0.0001 1 4 8 -3.3492 -0.0002 1 4 9 1.2045 0.0013 1 4 10 -3.4595 0.0003 1 4 11 -0.7245 0.0008 1 4 12 -2.2237 0.0002 1 4 13 -2.3634 -0.0007 1 4 14 -0.8661 0.0001 1 4 15 -3.0576 -0.0009 1 4 16 0.2324 -0.0002 1 4 17 -2.6193 -0.0008 1 4 18 0.8392 -0.0006 1 4 19 -1.5688 -0.0014 1 4 20 0.7586 -0.0011 1 4 21 -0.5928 -0.0012 1 4 22 0.4034 -0.0013 1 4 23 0.1305 0.0004 1 4 24 0.3056 -0.0006 1 4 25 0.8166 0.0016 1 4 26 0.3304 0.0003 1 4 27 1.3627 0.0023 1 4 28 0.1239 -0.0001 1 4 29 1.2750 0.0033 1 4 30 -0.1844 -0.0013 1 4 31 0.5136 0.0039 1 5 0 -0.9813 -0.0004 1 5 1 1.7148 -0.0015 1 5 2 1.0287 -0.0002 1 5 3 2.0106 -0.0005 1 5 4 2.3450 -0.0007 1 5 5 2.1909 0.0003 1 5 6 2.0708 0.0002 1 5 7 2.3693 0.0004 1 5 8 0.4383 0.0021 1 5 9 2.9663 0.0013 1 5 10 -1.2852 0.0016 1 5 11 3.4851 0.0018 1 5 12 -2.2531 -0.0008 1 5 13 3.0883 0.0005 1 5 14 -2.4682 -0.0020 1 5 15 1.8961 -0.0009 1 5 16 -2.0230 -0.0013 1 5 17 0.6091 -0.0001 1 5 18 -1.0899 -0.0002 1 5 19 -0.4023 0.0013 1 5 20 -0.2546 0.0006 1 5 21 -0.9579 0.0011 1 5 22 0.1586 0.0006 1 5 23 -0.9205 0.0001 1 5 24 0.5247 -0.0002 1 5 25 -0.5449 -0.0001 1 5 26 1.0221 -0.0001 1 5 27 -0.2532 0.0001 1 5 28 1.1506 0.0015 1 5 29 -0.1079 0.0001 1 5 30 0.6537 0.0020 1 6 0 2.4638 0.0006 1 6 1 -0.9612 0.0005 1 6 2 2.4402 0.0014 1 6 3 -1.1622 -0.0006 1 6 4 2.8018 0.0013 1 6 5 -1.2639 -0.0005 1 6 6 3.4081 0.0005 1 6 7 -1.8311 0.0002 1 6 8 3.8350 0.0010 1 6 9 -2.2785 0.0001 1 6 10 3.7738 0.0016 1 6 11 -1.8180 -0.0004 1 6 12 3.1247 -0.0001 1 6 13 -0.9076 -0.0006 1 6 14 1.9228 -0.0026 1 6 15 -0.2378 -0.0009 1 6 16 0.4885 -0.0019 1 6 17 0.3096 -0.0006 1 6 18 -0.6255 0.0014 1 6 19 0.7146 0.0012 1 6 20 -1.1178 0.0041 1 6 21 0.5573 0.0028 1 6 22 -1.1330 0.0044 1 6 23 0.1349 0.0016 1 6 24 -0.8970 0.0020 1 6 25 0.1419 -0.0010 1 6 26 -0.5115 -0.0012 1 6 27 0.3786 -0.0020 1 6 28 -0.1320 -0.0016 1 6 29 0.2548 -0.0009 1 7 0 -0.2598 0.0009 1 7 1 2.4334 -0.0002 1 7 2 -0.9696 0.0012 1 7 3 2.0798 -0.0001 1 7 4 -1.5523 0.0004 1 7 5 1.9521 -0.0010 1 7 6 -1.8545 -0.0011 1 7 7 1.6656 -0.0013 1 7 8 -1.7134 -0.0022 1 7 9 0.7828 -0.0010 1 7 10 -0.9999 -0.0014 1 7 11 0.0086 -0.0015 1 7 12 -0.0399 0.0001 1 7 13 -0.1282 -0.0025 1 7 14 0.6165 0.0000 1 7 15 -0.2468 -0.0021 1 7 16 0.8634 -0.0010 1 7 17 -0.6049 -0.0009 1 7 18 0.8621 -0.0007 1 7 19 -0.5504 0.0005 1 7 20 0.5354 0.0013 1 7 21 -0.0892 0.0017 1 7 22 -0.0722 0.0031 1 7 23 0.0330 0.0014 1 7 24 -0.4610 0.0030 1 7 25 -0.1521 -0.0017 1 7 26 -0.3487 0.0006 1 7 27 -0.0701 -0.0045 1 8 0 1.1808 -0.0012 1 8 1 0.6675 0.0006 1 8 2 1.1693 -0.0012 1 8 3 0.2221 0.0010 1 8 4 0.9473 -0.0010 1 8 5 -0.1196 0.0003 1 8 6 0.4118 -0.0012 1 8 7 0.2086 -0.0010 1 8 8 -0.5555 -0.0013 1 8 9 0.6227 -0.0012 1 8 10 -1.3029 -0.0007 1 8 11 0.5569 -0.0004 1 8 12 -1.1059 0.0005 1 8 13 0.5059 -0.0001 1 8 14 -0.4660 0.0013 1 8 15 0.7386 -0.0004 1 8 16 -0.2016 0.0003 1 8 17 0.5736 -0.0007 1 8 18 0.0099 -0.0026 1 8 19 -0.1893 -0.0011 1 8 20 0.6318 -0.0056 1 8 21 -0.7692 -0.0006 1 8 22 1.0228 -0.0070 1 8 23 -0.7614 0.0017 1 8 24 0.6393 -0.0066 1 8 25 -0.5286 0.0033 1 9 0 1.0773 0.0013 1 9 1 0.3980 -0.0001 1 9 2 1.1477 0.0003 1 9 3 0.1863 -0.0006 1 9 4 1.1075 0.0002 1 9 5 -0.5464 -0.0005 1 9 6 1.4235 0.0003 1 9 7 -1.1667 0.0002 1 9 8 1.6091 -0.0002 1 9 9 -1.0260 0.0015 1 9 10 0.9762 -0.0010 1 9 11 -0.4940 0.0031 1 9 12 0.2547 -0.0012 1 9 13 -0.2165 0.0036 1 9 14 0.3951 -0.0004 1 9 15 -0.0678 0.0022 1 9 16 0.5934 0.0006 1 9 17 0.3222 -0.0010 1 9 18 -0.2078 0.0003 1 9 19 0.7619 -0.0058 1 9 20 -1.1779 -0.0015 1 9 21 0.8608 -0.0107 1 9 22 -1.0991 -0.0026 1 9 23 0.6025 -0.0122 1 10 0 -0.3522 0.0009 1 10 1 0.6967 0.0016 1 10 2 -0.7201 0.0005 1 10 3 1.1684 0.0005 1 10 4 -1.6062 -0.0007 1 10 5 1.4678 0.0002 1 10 6 -2.1051 -0.0005 1 10 7 1.1603 -0.0001 1 10 8 -1.3382 0.0009 1 10 9 0.4278 -0.0013 1 10 10 -0.1603 0.0019 1 10 11 0.0435 -0.0022 1 10 12 0.0063 0.0015 1 10 13 0.2851 -0.0022 1 10 14 -0.3944 0.0002 1 10 15 0.5069 -0.0013 1 10 16 -0.0914 -0.0009 1 10 17 0.1196 0.0000 1 10 18 0.5539 -0.0020 1 10 19 -0.5277 0.0004 1 10 20 0.4770 -0.0043 1 11 0 -0.3426 0.0007 1 11 1 -0.9294 0.0011 1 11 2 0.2954 0.0014 1 11 3 -1.5535 0.0006 1 11 4 0.6758 0.0018 1 11 5 -1.7437 -0.0006 1 11 6 0.1976 0.0014 1 11 7 -1.0606 -0.0003 1 11 8 -0.6083 0.0005 1 11 9 -0.1882 0.0000 1 11 10 -0.5479 -0.0008 1 11 11 -0.0143 -0.0007 1 11 12 0.2063 -0.0023 1 11 13 -0.3223 -0.0019 1 11 14 0.4453 -0.0036 1 11 15 -0.2686 -0.0024 1 11 16 0.0604 -0.0036 1 12 0 -0.3522 0.0009 1 12 1 -0.3195 -0.0006 1 12 2 -0.6459 0.0011 1 12 3 -0.1626 0.0016 1 12 4 -0.6038 0.0006 1 12 5 -0.4619 0.0025 1 12 6 -0.0699 0.0003 1 12 7 -0.8485 0.0023 1 12 8 0.1853 0.0003 1 12 9 -0.6839 0.0016 1 12 10 -0.1208 0.0000 2 0 0 56.1363 0.0245 2 0 2 53.0662 0.0210 2 0 4 38.5371 0.0097 2 0 6 19.3360 -0.0010 2 0 8 3.4963 -0.0052 2 0 10 -4.6837 -0.0039 2 0 12 -6.2111 -0.0011 2 0 14 -4.4162 0.0001 2 0 16 -1.8088 -0.0009 2 0 18 0.2126 -0.0010 2 0 20 0.9169 0.0017 2 0 22 0.6411 0.0041 2 0 24 0.3512 0.0028 2 0 26 0.2789 -0.0003 2 0 28 -0.0213 -0.0023 2 0 30 -0.4371 -0.0042 2 0 32 -0.3961 -0.0061 2 1 0 -7.4669 -0.0019 2 1 1 37.0140 0.0131 2 1 2 3.9625 0.0000 2 1 3 31.0947 0.0058 2 1 4 12.1536 0.0017 2 1 5 19.8734 -0.0024 2 1 6 13.9994 0.0020 2 1 7 8.3070 -0.0042 2 1 8 10.1965 0.0011 2 1 9 0.5648 -0.0015 2 1 10 4.1654 -0.0005 2 1 11 -2.4397 0.0005 2 1 12 -0.9309 -0.0011 2 1 13 -2.4750 0.0011 2 1 14 -3.8867 0.0000 2 1 15 -1.5149 0.0010 2 1 16 -4.7152 0.0007 2 1 17 -0.5394 0.0001 2 1 18 -3.7854 -0.0004 2 1 19 0.0210 -0.0006 2 1 20 -2.0097 -0.0005 2 1 21 0.0332 0.0006 2 1 22 -0.5130 0.0017 2 1 23 -0.1834 0.0027 2 1 24 0.3682 0.0025 2 1 25 -0.2371 0.0026 2 1 26 0.9166 -0.0002 2 1 27 -0.1544 -0.0011 2 1 28 1.0282 -0.0016 2 1 29 -0.1379 -0.0058 2 1 30 0.4426 0.0008 2 1 31 -0.1458 -0.0072 2 1 32 -0.3379 0.0022 2 2 0 2.8610 -0.0039 2 2 1 0.8287 -0.0000 2 2 2 2.9200 -0.0032 2 2 3 10.9337 0.0029 2 2 4 3.8567 -0.0029 2 2 5 15.7180 0.0018 2 2 6 4.8715 -0.0024 2 2 7 13.8950 -0.0002 2 2 8 5.3892 -0.0006 2 2 9 7.9718 -0.0003 2 2 10 5.2253 0.0008 2 2 11 1.8245 -0.0002 2 2 12 4.2920 -0.0000 2 2 13 -2.2775 -0.0005 2 2 14 2.6121 -0.0014 2 2 15 -4.0572 0.0001 2 2 16 0.6501 -0.0010 2 2 17 -3.9169 0.0007 2 2 18 -0.7939 -0.0003 2 2 19 -2.5282 0.0005 2 2 20 -1.3190 -0.0013 2 2 21 -0.9658 0.0007 2 2 22 -1.3134 -0.0016 2 2 23 0.0008 0.0016 2 2 24 -1.2785 0.0003 2 2 25 0.4567 0.0011 2 2 26 -1.0995 0.0009 2 2 27 0.6745 -0.0006 2 2 28 -0.5114 -0.0015 2 2 29 0.5457 -0.0022 2 2 30 0.1210 -0.0034 2 2 31 0.0842 -0.0033 2 2 32 0.2430 -0.0020 2 3 0 1.6425 -0.0016 2 3 1 -12.1148 -0.0042 2 3 2 4.3694 -0.0002 2 3 3 -8.5501 0.0006 2 3 4 6.2639 0.0013 2 3 5 -2.0245 0.0029 2 3 6 6.2370 0.0008 2 3 7 4.1840 0.0014 2 3 8 4.3648 -0.0001 2 3 9 7.6394 0.0003 2 3 10 2.0707 0.0002 2 3 11 7.8527 -0.0003 2 3 12 0.6432 0.0007 2 3 13 5.7240 -0.0020 2 3 14 0.1508 -0.0002 2 3 15 2.5960 -0.0025 2 3 16 0.0571 -0.0016 2 3 17 -0.1287 -0.0004 2 3 18 0.0684 -0.0014 2 3 19 -1.4784 0.0007 2 3 20 0.0869 -0.0001 2 3 21 -1.6153 -0.0012 2 3 22 -0.0213 0.0002 2 3 23 -1.4733 -0.0027 2 3 24 -0.3074 -0.0008 2 3 25 -1.4494 -0.0021 2 3 26 -0.6014 -0.0016 2 3 27 -1.1376 -0.0009 2 3 28 -0.6163 -0.0025 2 3 29 -0.4233 0.0002 2 3 30 -0.2646 -0.0041 2 3 31 0.1080 0.0011 2 4 0 -7.3128 0.0014 2 4 1 1.7716 -0.0013 2 4 2 -6.6368 0.0033 2 4 3 -0.5940 0.0004 2 4 4 -3.6745 0.0042 2 4 5 -1.6668 0.0022 2 4 6 0.2173 0.0023 2 4 7 -1.4788 0.0004 2 4 8 2.9742 -0.0001 2 4 9 -0.4651 -0.0017 2 4 10 3.5384 -0.0011 2 4 11 1.0137 -0.0003 2 4 12 2.5004 -0.0010 2 4 13 2.3939 0.0016 2 4 14 0.9574 -0.0002 2 4 15 2.9664 -0.0001 2 4 16 -0.3260 0.0009 2 4 17 2.5198 -0.0023 2 4 18 -0.8610 0.0013 2 4 19 1.5149 -0.0013 2 4 20 -0.6641 0.0003 2 4 21 0.4901 0.0006 2 4 22 -0.3669 -0.0011 2 4 23 -0.3919 0.0005 2 4 24 -0.4108 -0.0022 2 4 25 -1.1069 -0.0007 2 4 26 -0.5397 -0.0023 2 4 27 -1.3983 -0.0017 2 4 28 -0.4278 -0.0008 2 4 29 -1.0097 -0.0022 2 4 30 -0.1811 0.0016 2 5 0 1.4608 -0.0005 2 5 1 -1.8202 0.0013 2 5 2 -0.2765 0.0010 2 5 3 -1.9924 0.0004 2 5 4 -1.6224 0.0027 2 5 5 -2.0339 -0.0003 2 5 6 -1.6631 0.0008 2 5 7 -2.0075 -0.0009 2 5 8 -0.3804 -0.0028 2 5 9 -2.3742 -0.0020 2 5 10 1.2608 -0.0029 2 5 11 -2.8425 -0.0018 2 5 12 2.3765 0.0003 2 5 13 -2.6797 0.0009 2 5 14 2.6632 0.0019 2 5 15 -1.8422 0.0028 2 5 16 2.1333 0.0006 2 5 17 -0.7858 0.0014 2 5 18 1.1465 -0.0006 2 5 19 0.2235 -0.0013 2 5 20 0.3117 -0.0004 2 5 21 0.9395 -0.0020 2 5 22 -0.1913 0.0010 2 5 23 1.0622 -0.0008 2 5 24 -0.6543 0.0029 2 5 25 0.7200 0.0005 2 5 26 -1.0347 0.0035 2 5 27 0.3642 0.0013 2 5 28 -0.9308 0.0023 2 5 29 0.1782 0.0018 2 6 0 -1.7756 -0.0010 2 6 1 0.9691 -0.0002 2 6 2 -1.6699 -0.0021 2 6 3 1.2403 0.0008 2 6 4 -2.0471 -0.0019 2 6 5 1.2954 0.0004 2 6 6 -2.7719 -0.0007 2 6 7 1.8277 -0.0014 2 6 8 -3.3552 -0.0007 2 6 9 2.4170 -0.0021 2 6 10 -3.4214 -0.0010 2 6 11 2.1470 -0.0007 2 6 12 -2.8545 0.0008 2 6 13 1.2084 0.0010 2 6 14 -1.7605 0.0029 2 6 15 0.3324 0.0014 2 6 16 -0.5045 0.0020 2 6 17 -0.3209 0.0001 2 6 18 0.4971 -0.0009 2 6 19 -0.6782 -0.0018 2 6 20 1.1001 -0.0030 2 6 21 -0.5073 -0.0021 2 6 22 1.3347 -0.0028 2 6 23 -0.1567 0.0007 2 6 24 1.1819 0.0005 2 6 25 -0.1994 0.0044 2 6 26 0.7474 0.0054 2 6 27 -0.4134 0.0058 2 6 28 0.3644 0.0072 2 7 0 0.0542 -0.0007 2 7 1 -2.1022 0.0002 2 7 2 0.8834 -0.0014 2 7 3 -1.6110 -0.0006 2 7 4 1.6381 -0.0014 2 7 5 -1.5058 -0.0001 2 7 6 2.0711 -0.0009 2 7 7 -1.4930 0.0003 2 7 8 2.0105 -0.0003 2 7 9 -0.8505 -0.0000 2 7 10 1.2727 0.0003 2 7 11 -0.0607 0.0003 2 7 12 0.1139 0.0010 2 7 13 0.1451 0.0012 2 7 14 -0.7926 0.0007 2 7 15 0.1383 0.0015 2 7 16 -1.1246 -0.0012 2 7 17 0.3583 0.0010 2 7 18 -1.0345 -0.0031 2 7 19 0.4452 -0.0001 2 7 20 -0.6125 -0.0029 2 7 21 0.2610 -0.0011 2 7 22 0.0052 -0.0017 2 7 23 0.2016 -0.0001 2 7 24 0.3300 -0.0012 2 7 25 0.2479 0.0046 2 7 26 0.1098 -0.0002 2 7 27 0.0993 0.0092 2 8 0 -1.5572 0.0015 2 8 1 -0.8579 -0.0004 2 8 2 -1.4664 0.0014 2 8 3 -0.1434 -0.0006 2 8 4 -1.0859 0.0008 2 8 5 0.5362 -0.0007 2 8 6 -0.5546 0.0004 2 8 7 0.2382 -0.0005 2 8 8 0.3325 -0.0007 2 8 9 -0.5057 0.0000 2 8 10 1.1685 -0.0024 2 8 11 -0.7518 0.0008 2 8 12 1.1076 -0.0027 2 8 13 -0.7094 0.0003 2 8 14 0.3492 -0.0010 2 8 15 -0.8195 -0.0023 2 8 16 -0.1492 0.0005 2 8 17 -0.6822 -0.0045 2 8 18 -0.2988 0.0006 2 8 19 -0.0389 -0.0029 2 8 20 -0.5945 0.0014 2 8 21 0.5342 -0.0002 2 8 22 -0.8232 0.0040 2 8 23 0.5829 -0.0016 2 8 24 -0.5796 0.0065 2 8 25 0.3042 -0.0052 2 9 0 -1.2462 -0.0008 2 9 1 -0.8643 0.0007 2 9 2 -1.0406 0.0008 2 9 3 -0.7928 0.0015 2 9 4 -0.6521 0.0013 2 9 5 -0.0928 0.0016 2 9 6 -0.9433 0.0007 2 9 7 0.6411 0.0002 2 9 8 -1.6049 0.0006 2 9 9 0.6453 -0.0025 2 9 10 -1.4018 0.0007 2 9 11 0.1779 -0.0036 2 9 12 -0.4605 -0.0003 2 9 13 -0.1107 -0.0010 2 9 14 -0.0358 -0.0023 2 9 15 -0.2362 0.0015 2 9 16 -0.1180 -0.0035 2 9 17 -0.4903 0.0005 2 9 18 0.2595 -0.0029 2 9 19 -0.7420 -0.0004 2 9 20 0.8853 -0.0010 2 9 21 -0.7313 0.0038 2 9 22 0.8457 -0.0003 2 10 0 0.0974 0.0014 2 10 1 -0.6518 -0.0005 2 10 2 0.2318 0.0006 2 10 3 -0.8398 0.0012 2 10 4 0.8291 0.0006 2 10 5 -1.2620 0.0014 2 10 6 1.2931 0.0003 2 10 7 -1.4358 0.0012 2 10 8 0.5629 -0.0004 2 10 9 -1.0807 0.0007 2 10 10 -0.7706 0.0008 2 10 11 -0.4726 -0.0009 2 10 12 -1.0480 0.0046 2 10 13 -0.0189 -0.0020 2 10 14 -0.3236 0.0074 2 10 15 0.2177 -0.0007 2 10 16 -0.0501 0.0056 2 10 17 0.4145 0.0006 2 10 18 -0.3961 0.0011 2 10 19 0.5739 -0.0007 2 11 0 0.2276 0.0000 2 11 1 0.7131 0.0014 2 11 2 -0.1643 0.0011 2 11 3 1.2488 -0.0012 2 11 4 -0.7106 -0.0001 2 11 5 1.3556 -0.0026 2 11 6 -0.6603 -0.0021 2 11 7 0.5010 -0.0022 2 11 8 -0.0837 -0.0037 2 11 9 -0.7426 0.0015 2 11 10 0.0538 -0.0046 2 11 11 -1.2371 0.0076 2 11 12 -0.2523 -0.0038 2 11 13 -0.7434 0.0112 2 11 14 -0.0929 -0.0003 2 11 15 -0.1454 0.0101 2 12 0 0.1112 0.0009 2 12 1 0.3689 0.0028 2 12 2 0.5552 -0.0001 2 12 3 0.0694 0.0009 2 12 4 0.7230 -0.0016 2 12 5 0.1573 -0.0035 2 12 6 0.1448 -0.0029 2 12 7 0.4611 -0.0076 2 12 8 -0.4387 -0.0017 2 12 9 0.4189 -0.0093 3 0 0 -37.1106 -0.0049 3 0 2 -36.2064 -0.0025 3 0 4 -25.5594 0.0014 3 0 6 -10.9309 0.0044 3 0 8 1.0357 0.0063 3 0 10 7.0817 0.0061 3 0 12 7.9263 0.0025 3 0 14 5.8731 -0.0019 3 0 16 2.9602 -0.0030 3 0 18 0.6975 -0.0019 3 0 20 -0.2686 -0.0020 3 0 22 -0.5142 -0.0016 3 0 24 -0.8308 0.0014 3 0 26 -1.0272 0.0041 3 0 28 -0.5983 0.0041 3 0 30 0.0492 0.0044 3 0 32 0.1661 0.0067 3 1 0 7.6438 0.0005 3 1 1 -24.6676 -0.0008 3 1 2 -2.0034 -0.0012 3 1 3 -20.5547 0.0023 3 1 4 -9.5162 -0.0010 3 1 5 -11.9672 0.0046 3 1 6 -11.9738 -0.0009 3 1 7 -3.2138 0.0043 3 1 8 -9.6795 -0.0013 3 1 9 2.4502 0.0030 3 1 10 -5.0591 -0.0001 3 1 11 4.4380 0.0018 3 1 12 -0.4843 0.0020 3 1 13 3.9819 -0.0000 3 1 14 2.6808 0.0015 3 1 15 2.5268 -0.0012 3 1 16 3.8177 -0.0011 3 1 17 1.1071 -0.0006 3 1 18 3.0812 -0.0022 3 1 19 0.3333 0.0005 3 1 20 1.5227 -0.0020 3 1 21 0.2075 0.0006 3 1 22 0.1954 -0.0020 3 1 23 0.2296 0.0003 3 1 24 -0.7537 -0.0011 3 1 25 0.0639 0.0004 3 1 26 -1.4803 0.0007 3 1 27 -0.1348 0.0013 3 1 28 -1.5902 -0.0007 3 1 29 -0.1518 0.0034 3 1 30 -0.8252 -0.0057 3 1 31 -0.0686 0.0058 3 1 32 0.0790 -0.0079 3 2 0 -0.5190 0.0045 3 2 1 -0.0651 -0.0019 3 2 2 -0.2394 0.0034 3 2 3 -9.2358 -0.0026 3 2 4 -0.7782 0.0020 3 2 5 -14.0470 -0.0001 3 2 6 -1.6848 0.0014 3 2 7 -13.3233 0.0009 3 2 8 -2.4800 0.0001 3 2 9 -8.9111 -0.0001 3 2 10 -2.8452 -0.0012 3 2 11 -3.5554 -0.0000 3 2 12 -2.5673 -0.0000 3 2 13 0.7909 0.0005 3 2 14 -1.6302 0.0025 3 2 15 3.1240 -0.0007 3 2 16 -0.4035 0.0031 3 2 17 3.2592 -0.0017 3 2 18 0.5664 0.0017 3 2 19 2.0106 -0.0011 3 2 20 1.1158 0.0011 3 2 21 0.6568 -0.0006 3 2 22 1.5242 0.0009 3 2 23 -0.1860 -0.0009 3 2 24 1.8333 -0.0007 3 2 25 -0.6879 -0.0008 3 2 26 1.5900 -0.0024 3 2 27 -0.9301 -0.0017 3 2 28 0.6804 -0.0021 3 2 29 -0.7053 -0.0045 3 2 30 -0.1505 -0.0009 3 2 31 -0.1639 -0.0063 3 3 0 -1.9449 0.0008 3 3 1 10.8941 0.0027 3 3 2 -4.9268 -0.0002 3 3 3 8.3672 -0.0009 3 3 4 -6.8860 -0.0007 3 3 5 3.0220 -0.0020 3 3 6 -6.9485 0.0003 3 3 7 -2.3202 -0.0010 3 3 8 -5.3812 0.0008 3 3 9 -5.6395 -0.0014 3 3 10 -3.2694 -0.0007 3 3 11 -6.3455 -0.0015 3 3 12 -1.5410 -0.0024 3 3 13 -4.8405 0.0014 3 3 14 -0.4987 -0.0018 3 3 15 -2.2287 0.0034 3 3 16 -0.0821 0.0011 3 3 17 0.0372 0.0014 3 3 18 -0.0769 0.0029 3 3 19 1.1521 -0.0008 3 3 20 -0.1337 0.0020 3 3 21 1.5214 -0.0002 3 3 22 0.0366 0.0003 3 3 23 1.8268 0.0008 3 3 24 0.4379 -0.0003 3 3 25 1.9355 -0.0001 3 3 26 0.7975 -0.0005 3 3 27 1.3823 -0.0014 3 3 28 0.7799 -0.0016 3 3 29 0.4561 -0.0028 3 3 30 0.3521 -0.0026 3 3 31 -0.0665 -0.0040 3 4 0 6.7341 -0.0003 3 4 1 -2.5757 0.0020 3 4 2 6.3770 -0.0012 3 4 3 -0.7303 -0.0005 3 4 4 3.8001 -0.0017 3 4 5 0.3807 -0.0022 3 4 6 0.3066 -0.0010 3 4 7 0.5959 -0.0003 3 4 8 -2.3761 -0.0002 3 4 9 0.0438 0.0013 3 4 10 -3.3008 -0.0002 3 4 11 -1.1134 -0.0010 3 4 12 -2.6248 0.0001 3 4 13 -2.3054 -0.0027 3 4 14 -1.1146 0.0003 3 4 15 -2.7464 0.0002 3 4 16 0.2535 -0.0006 3 4 17 -2.2670 0.0037 3 4 18 0.7517 -0.0013 3 4 19 -1.3793 0.0029 3 4 20 0.5090 -0.0008 3 4 21 -0.4830 -0.0003 3 4 22 0.2429 0.0002 3 4 23 0.4048 -0.0016 3 4 24 0.2509 0.0009 3 4 25 1.1307 -0.0009 3 4 26 0.2590 0.0014 3 4 27 1.2553 0.0003 3 4 28 0.1365 0.0009 3 4 29 0.6729 0.0008 3 4 30 0.0263 -0.0010 3 5 0 -1.4182 0.0014 3 5 1 1.2804 -0.0001 3 5 2 -0.0595 -0.0010 3 5 3 1.4068 0.0006 3 5 4 1.1292 -0.0030 3 5 5 1.4167 0.0004 3 5 6 1.4084 -0.0014 3 5 7 1.2793 -0.0000 3 5 8 0.5860 0.0018 3 5 9 1.4247 0.0004 3 5 10 -0.8288 0.0019 3 5 11 1.7722 0.0007 3 5 12 -2.0894 -0.0004 3 5 13 1.7746 -0.0001 3 5 14 -2.5684 -0.0010 3 5 15 1.2886 -0.0005 3 5 16 -2.0849 0.0003 3 5 17 0.5427 0.0003 3 5 18 -1.1556 0.0005 3 5 19 -0.3306 0.0008 3 5 20 -0.4455 -0.0007 3 5 21 -1.1069 -0.0004 3 5 22 0.0066 -0.0018 3 5 23 -1.4003 -0.0017 3 5 24 0.4270 -0.0024 3 5 25 -1.1667 -0.0019 3 5 26 0.5755 -0.0018 3 5 27 -0.7664 -0.0015 3 5 28 0.2012 -0.0001 3 5 29 -0.4687 -0.0011 3 6 0 0.6467 0.0003 3 6 1 -0.4768 -0.0003 3 6 2 0.5522 0.0008 3 6 3 -0.9255 -0.0014 3 6 4 0.9747 0.0007 3 6 5 -1.0132 -0.0009 3 6 6 1.7426 0.0002 3 6 7 -1.3936 0.0010 3 6 8 2.4156 0.0000 3 6 9 -1.9548 0.0018 3 6 10 2.6419 -0.0003 3 6 11 -1.9087 0.0004 3 6 12 2.2426 -0.0008 3 6 13 -1.1858 -0.0013 3 6 14 1.3183 0.0000 3 6 15 -0.3602 -0.0015 3 6 16 0.2946 0.0017 3 6 17 0.2470 -0.0003 3 6 18 -0.4915 0.0013 3 6 19 0.4948 0.0006 3 6 20 -1.0548 -0.0011 3 6 21 0.2976 -0.0002 3 6 22 -1.3623 -0.0030 3 6 23 -0.0075 -0.0022 3 6 24 -1.1907 -0.0046 3 6 25 -0.0386 -0.0033 3 6 26 -0.6698 -0.0070 3 6 27 0.0065 -0.0028 3 6 28 -0.3233 -0.0081 3 7 0 0.4343 0.0006 3 7 1 1.5225 -0.0009 3 7 2 -0.4190 0.0008 3 7 3 0.9818 -0.0001 3 7 4 -1.2263 0.0002 3 7 5 0.8499 0.0006 3 7 6 -1.6981 0.0004 3 7 7 1.0666 0.0009 3 7 8 -1.7647 0.0013 3 7 9 0.7873 0.0004 3 7 10 -1.2478 0.0007 3 7 11 0.1403 -0.0004 3 7 12 -0.2278 -0.0017 3 7 13 -0.1377 -0.0003 3 7 14 0.7003 -0.0020 3 7 15 -0.0943 0.0005 3 7 16 1.0975 0.0016 3 7 17 -0.1483 0.0007 3 7 18 1.0375 0.0038 3 7 19 -0.2176 -0.0000 3 7 20 0.6501 0.0004 3 7 21 -0.1417 -0.0007 3 7 22 0.0816 -0.0044 3 7 23 -0.0233 -0.0019 3 7 24 -0.2140 -0.0047 3 7 25 0.1280 -0.0053 3 7 26 0.0223 -0.0024 3 8 0 1.6424 -0.0003 3 8 1 0.7992 0.0004 3 8 2 1.4734 -0.0001 3 8 3 0.2712 -0.0007 3 8 4 0.9135 0.0003 3 8 5 -0.4147 -0.0007 3 8 6 0.4196 0.0002 3 8 7 -0.2449 0.0011 3 8 8 -0.2055 0.0009 3 8 9 0.4281 0.0019 3 8 10 -0.9513 0.0026 3 8 11 0.6278 0.0000 3 8 12 -1.0961 0.0025 3 8 13 0.4535 -0.0010 3 8 14 -0.4853 0.0001 3 8 15 0.4996 0.0021 3 8 16 0.1055 -0.0000 3 8 17 0.5917 0.0050 3 8 18 0.3283 0.0041 3 8 19 0.3152 0.0012 3 8 20 0.5336 0.0073 3 8 21 -0.1163 -0.0060 3 8 22 0.7287 0.0049 3 8 23 -0.2625 -0.0073 3 8 24 0.6295 -0.0002 3 9 0 0.6727 -0.0006 3 9 1 1.1414 0.0014 3 9 2 0.6581 -0.0018 3 9 3 1.1315 0.0005 3 9 4 0.3675 -0.0018 3 9 5 0.4784 -0.0012 3 9 6 0.6504 0.0001 3 9 7 -0.2754 -0.0012 3 9 8 1.4673 0.0012 3 9 9 -0.3886 0.0015 3 9 10 1.4809 0.0006 3 9 11 -0.0969 0.0025 3 9 12 0.4050 0.0008 3 9 13 -0.0020 -0.0016 3 9 14 -0.4011 0.0020 3 9 15 -0.0458 -0.0042 3 9 16 -0.3252 0.0017 3 9 17 0.1162 0.0022 3 9 18 -0.1994 -0.0008 3 9 19 0.3954 0.0112 3 9 20 -0.4089 -0.0036 3 9 21 0.4870 0.0113 3 10 0 0.2894 -0.0011 3 10 1 0.3565 -0.0021 3 10 2 0.3806 0.0000 3 10 3 0.4261 -0.0027 3 10 4 0.0410 0.0004 3 10 5 0.8969 -0.0010 3 10 6 -0.4735 0.0009 3 10 7 1.3235 0.0004 3 10 8 -0.0254 0.0013 3 10 9 1.2673 0.0004 3 10 10 1.1674 -0.0015 3 10 11 0.6782 0.0018 3 10 12 1.4472 -0.0083 3 10 13 -0.0774 0.0027 3 10 14 0.5157 -0.0129 3 10 15 -0.5360 -0.0007 3 10 16 -0.1590 -0.0087 3 10 17 -0.5697 -0.0051 3 10 18 0.0345 0.0011 3 11 0 0.0924 -0.0013 3 11 1 -0.3330 -0.0041 3 11 2 0.1266 -0.0056 3 11 3 -0.7086 -0.0001 3 11 4 0.5929 -0.0046 3 11 5 -0.8194 0.0042 3 11 6 0.7442 -0.0005 3 11 7 -0.1129 0.0062 3 11 8 0.3288 0.0032 3 11 9 1.1041 0.0012 3 11 10 0.1306 0.0056 3 11 11 1.7479 -0.0093 3 11 12 0.2998 0.0055 3 11 13 1.2465 -0.0165 3 11 14 0.0899 0.0013 3 12 0 -0.1522 -0.0039 3 12 1 -0.2557 -0.0053 3 12 2 -0.5950 -0.0031 3 12 3 -0.0040 -0.0080 3 12 4 -0.8848 0.0001 3 12 5 0.0231 -0.0039 3 12 6 -0.3468 0.0043 3 12 7 -0.2060 0.0035 4 0 0 21.2267 -0.0075 4 0 2 21.9139 -0.0062 4 0 4 15.0885 -0.0015 4 0 6 4.8393 0.0028 4 0 8 -3.7724 0.0021 4 0 10 -8.2830 -0.0015 4 0 12 -8.9428 -0.0022 4 0 14 -6.9677 0.0002 4 0 16 -3.8387 0.0019 4 0 18 -1.2065 0.0023 4 0 20 0.0902 0.0025 4 0 22 0.5958 0.0006 4 0 24 1.0050 -0.0038 4 0 26 1.0575 -0.0055 4 0 28 0.4179 -0.0025 4 0 30 -0.3047 -0.0003 4 1 0 -6.6873 0.0008 4 1 1 14.4037 -0.0022 4 1 2 0.7916 0.0015 4 1 3 12.0223 -0.0013 4 1 4 7.0631 -0.0008 4 1 5 6.0582 0.0012 4 1 6 9.5177 -0.0021 4 1 7 -0.1646 0.0026 4 1 8 8.1811 -0.0009 4 1 9 -4.2302 0.0010 4 1 10 4.7815 0.0000 4 1 11 -5.6789 -0.0007 4 1 12 1.0588 -0.0007 4 1 13 -5.1164 0.0002 4 1 14 -1.7256 -0.0008 4 1 15 -3.3913 0.0014 4 1 16 -2.7466 0.0004 4 1 17 -1.5244 0.0011 4 1 18 -2.1386 0.0010 4 1 19 -0.3943 0.0003 4 1 20 -1.0176 0.0001 4 1 21 -0.1150 -0.0008 4 1 22 -0.2086 -0.0014 4 1 23 -0.1476 -0.0023 4 1 24 0.4953 -0.0031 4 1 25 -0.0857 -0.0020 4 1 26 1.3038 -0.0028 4 1 27 0.0220 0.0023 4 1 28 1.6276 0.0020 4 1 29 0.0360 0.0063 4 1 30 1.0743 0.0088 4 1 31 -0.0088 0.0046 4 2 0 -0.8349 0.0007 4 2 1 -0.6867 0.0030 4 2 2 -1.3398 0.0009 4 2 3 7.0028 0.0006 4 2 4 -1.1751 0.0010 4 2 5 11.2927 -0.0035 4 2 6 -0.4977 0.0004 4 2 7 11.1453 -0.0034 4 2 8 0.3214 0.0004 4 2 9 7.9735 -0.0004 4 2 10 0.9131 0.0014 4 2 11 3.6981 0.0010 4 2 12 1.0339 0.0015 4 2 13 -0.1448 0.0005 4 2 14 0.6614 0.0002 4 2 15 -2.3210 0.0002 4 2 16 0.0709 -0.0007 4 2 17 -2.4230 -0.0002 4 2 18 -0.4159 -0.0004 4 2 19 -1.3672 -0.0011 4 2 20 -0.8551 -0.0002 4 2 21 -0.4285 -0.0010 4 2 22 -1.4895 -0.0003 4 2 23 0.0575 -0.0007 4 2 24 -2.0233 0.0009 4 2 25 0.4395 -0.0014 4 2 26 -1.7193 0.0042 4 2 27 0.7310 -0.0001 4 2 28 -0.5605 0.0078 4 2 29 0.6477 0.0053 4 2 30 0.4118 0.0088 4 3 0 1.1172 0.0009 4 3 1 -8.9051 -0.0001 4 3 2 4.0264 0.0005 4 3 3 -7.4778 0.0003 4 3 4 5.8722 -0.0009 4 3 5 -3.5530 -0.0005 4 3 6 5.9496 -0.0019 4 3 7 0.6575 -0.0013 4 3 8 4.7144 -0.0013 4 3 9 3.6089 0.0006 4 3 10 3.0343 0.0007 4 3 11 4.7002 0.0024 4 3 12 1.5057 0.0024 4 3 13 3.8840 0.0011 4 3 14 0.4543 0.0018 4 3 15 1.8921 -0.0005 4 3 16 0.0441 -0.0009 4 3 17 0.0607 0.0006 4 3 18 0.1268 -0.0025 4 3 19 -0.9168 0.0024 4 3 20 0.2792 -0.0008 4 3 21 -1.4830 0.0025 4 3 22 0.1492 0.0021 4 3 23 -2.0055 0.0023 4 3 24 -0.3053 0.0025 4 3 25 -1.9792 0.0027 4 3 26 -0.7905 0.0008 4 3 27 -1.0480 0.0030 4 3 28 -0.8651 0.0005 4 3 29 0.0742 0.0037 4 3 30 -0.4423 0.0022 4 4 0 -5.4568 -0.0005 4 4 1 2.2064 -0.0014 4 4 2 -5.4779 -0.0011 4 4 3 0.8292 0.0001 4 4 4 -3.5107 -0.0016 4 4 5 -0.1880 0.0010 4 4 6 -0.7058 -0.0012 4 4 7 -0.5803 -0.0001 4 4 8 1.6219 0.0004 4 4 9 -0.2667 -0.0008 4 4 10 2.7683 0.0014 4 4 11 0.7448 0.0007 4 4 12 2.5881 0.0006 4 4 13 1.8981 0.0014 4 4 14 1.4321 -0.0005 4 4 15 2.3468 -0.0008 4 4 16 0.1904 0.0002 4 4 17 1.9498 -0.0024 4 4 18 -0.3673 0.0017 4 4 19 1.2941 -0.0003 4 4 20 -0.3491 0.0024 4 4 21 0.6900 0.0030 4 4 22 -0.2671 0.0021 4 4 23 -0.0390 0.0036 4 4 24 -0.1588 0.0009 4 4 25 -0.7599 0.0011 4 4 26 0.1403 -0.0016 4 4 27 -0.9084 -0.0023 4 4 28 0.3923 -0.0036 4 4 29 -0.3756 -0.0042 4 5 0 1.1441 -0.0013 4 5 1 -0.5487 -0.0006 4 5 2 0.0203 0.0007 4 5 3 -0.6638 -0.0013 4 5 4 -0.9752 0.0015 4 5 5 -0.6970 -0.0009 4 5 6 -1.3324 0.0001 4 5 7 -0.5556 0.0004 4 5 8 -0.8622 -0.0012 4 5 9 -0.5737 0.0011 4 5 10 0.2825 -0.0005 4 5 11 -0.7689 0.0002 4 5 12 1.5837 0.0004 4 5 13 -0.7471 -0.0016 4 5 14 2.2358 -0.0003 4 5 15 -0.3804 -0.0032 4 5 16 1.8813 -0.0008 4 5 17 0.1379 -0.0031 4 5 18 1.1008 0.0005 4 5 19 0.7118 -0.0006 4 5 20 0.5607 0.0015 4 5 21 1.2524 0.0019 4 5 22 0.1810 0.0002 4 5 23 1.5043 0.0017 4 5 24 -0.1984 -0.0028 4 5 25 1.3421 -0.0008 4 5 26 -0.1808 -0.0058 4 5 27 0.9428 -0.0035 4 5 28 0.3599 -0.0077 4 6 0 0.2582 0.0002 4 6 1 0.1559 0.0004 4 6 2 0.3032 0.0007 4 6 3 0.6833 0.0012 4 6 4 -0.1587 0.0008 4 6 5 0.8036 0.0003 4 6 6 -0.8697 -0.0001 4 6 7 1.0057 -0.0008 4 6 8 -1.4904 -0.0001 4 6 9 1.4171 -0.0004 4 6 10 -1.7845 0.0012 4 6 11 1.4938 0.0010 4 6 12 -1.5232 0.0014 4 6 13 1.0127 0.0017 4 6 14 -0.7385 -0.0018 4 6 15 0.3243 0.0011 4 6 16 0.1055 -0.0044 4 6 17 -0.2217 0.0000 4 6 18 0.6869 -0.0016 4 6 19 -0.4445 -0.0001 4 6 20 1.1285 0.0039 4 6 21 -0.3234 0.0000 4 6 22 1.3836 0.0058 4 6 23 -0.0914 -0.0014 4 6 24 1.1059 0.0037 4 6 25 0.0781 -0.0046 4 6 26 0.4496 0.0016 4 6 27 0.2982 -0.0067 4 7 0 -0.6427 -0.0012 4 7 1 -1.0792 0.0012 4 7 2 0.1514 -0.0006 4 7 3 -0.6841 0.0017 4 7 4 0.8779 0.0014 4 7 5 -0.5684 0.0004 4 7 6 1.2352 0.0020 4 7 7 -0.8452 -0.0009 4 7 8 1.3221 0.0002 4 7 9 -0.7710 0.0006 4 7 10 1.0543 -0.0003 4 7 11 -0.2471 0.0028 4 7 12 0.3414 0.0017 4 7 13 0.1079 0.0024 4 7 14 -0.4442 0.0020 4 7 15 0.1228 0.0001 4 7 16 -0.9096 -0.0015 4 7 17 0.1157 -0.0003 4 7 18 -1.0504 -0.0025 4 7 19 0.1904 0.0019 4 7 20 -0.8761 0.0034 4 7 21 0.2046 0.0040 4 7 22 -0.3812 0.0096 4 7 23 0.0370 0.0043 4 7 24 0.0456 0.0084 4 7 25 -0.2971 0.0038 4 8 0 -1.4617 -0.0011 4 8 1 -0.7418 -0.0017 4 8 2 -1.4148 -0.0005 4 8 3 -0.5866 0.0010 4 8 4 -0.8316 -0.0004 4 8 5 -0.1224 0.0030 4 8 6 -0.3736 0.0001 4 8 7 -0.1922 0.0009 4 8 8 0.0106 0.0009 4 8 9 -0.5899 -0.0017 4 8 10 0.5905 0.0005 4 8 11 -0.5171 -0.0004 4 8 12 0.9167 0.0004 4 8 13 -0.1164 0.0014 4 8 14 0.6491 0.0017 4 8 15 -0.1075 -0.0007 4 8 16 0.2584 0.0003 4 8 17 -0.4823 -0.0019 4 8 18 0.0948 -0.0055 4 8 19 -0.6456 0.0048 4 8 20 -0.0855 -0.0096 4 8 21 -0.3802 0.0149 4 8 22 -0.3397 -0.0069 4 8 23 -0.0277 0.0179 4 9 0 -0.1987 -0.0001 4 9 1 -1.1953 -0.0036 4 9 2 -0.6600 0.0006 4 9 3 -1.2173 -0.0023 4 9 4 -0.7245 0.0006 4 9 5 -0.5322 0.0002 4 9 6 -0.9350 -0.0020 4 9 7 0.2470 0.0017 4 9 8 -1.5232 -0.0031 4 9 9 0.3845 -0.0002 4 9 10 -1.4684 -0.0007 4 9 11 0.1787 -0.0018 4 9 12 -0.3653 0.0021 4 9 13 0.2924 0.0013 4 9 14 0.5530 0.0032 4 9 15 0.6483 0.0029 4 9 16 0.4330 0.0052 4 9 17 0.7280 -0.0052 4 9 18 -0.0172 0.0090 4 9 19 0.4241 -0.0164 4 9 20 -0.0662 0.0118 4 10 0 -0.7199 -0.0013 4 10 1 -0.1231 0.0020 4 10 2 -0.8947 -0.0008 4 10 3 -0.3692 0.0018 4 10 4 -0.5709 0.0004 4 10 5 -0.8273 -0.0022 4 10 6 0.1864 0.0000 4 10 7 -1.1154 -0.0046 4 10 8 0.1958 -0.0023 4 10 9 -1.0371 -0.0020 4 10 10 -0.7080 -0.0017 4 10 11 -0.5874 0.0015 4 10 12 -1.0290 0.0042 4 10 13 0.0098 0.0042 4 10 14 -0.1539 0.0092 4 10 15 0.3644 0.0092 4 10 16 0.6546 0.0057 4 10 17 0.3266 0.0138 4 11 0 -0.1612 0.0006 4 11 1 -0.1789 0.0047 4 11 2 -0.0054 0.0070 4 11 3 0.1724 0.0039 4 11 4 -0.3556 0.0067 4 11 5 0.4369 0.0003 4 11 6 -0.4861 0.0020 4 11 7 0.1729 -0.0053 4 11 8 -0.0502 -0.0015 4 11 9 -0.6056 -0.0052 4 11 10 0.1688 -0.0025 4 11 11 -1.1711 0.0031 4 11 12 -0.1346 -0.0010 4 12 0 0.2092 0.0052 4 12 1 0.2191 0.0058 4 12 2 0.6300 0.0057 4 12 3 0.1594 0.0126 5 0 0 -11.2260 0.0062 5 0 2 -12.6274 0.0041 5 0 4 -8.8083 -0.0018 5 0 6 -2.0260 -0.0068 5 0 8 4.1890 -0.0059 5 0 10 7.8422 -0.0015 5 0 12 8.6677 0.0013 5 0 14 7.0414 0.0021 5 0 16 3.9759 0.0018 5 0 18 1.1740 -0.0002 5 0 20 -0.2488 -0.0023 5 0 22 -0.6159 -0.0013 5 0 24 -0.6338 0.0019 5 0 26 -0.3449 0.0016 5 0 28 0.2778 -0.0032 5 0 30 0.6971 -0.0063 5 1 0 5.5018 -0.0008 5 1 1 -8.0082 -0.0013 5 1 2 0.1930 -0.0011 5 1 3 -6.9481 -0.0015 5 1 4 -4.6716 0.0009 5 1 5 -3.1324 -0.0038 5 1 6 -6.9158 0.0025 5 1 7 1.2255 -0.0051 5 1 8 -6.2832 0.0017 5 1 9 4.3427 -0.0031 5 1 10 -3.9343 -0.0003 5 1 11 5.6731 -0.0009 5 1 12 -1.1095 -0.0016 5 1 13 5.2894 -0.0009 5 1 14 1.1747 -0.0011 5 1 15 3.5985 -0.0009 5 1 16 2.1157 0.0006 5 1 17 1.5475 -0.0001 5 1 18 1.7730 0.0018 5 1 19 0.1840 -0.0000 5 1 20 1.1025 0.0020 5 1 21 -0.1714 0.0001 5 1 22 0.6928 0.0027 5 1 23 0.0401 0.0020 5 1 24 0.1774 0.0036 5 1 25 0.2844 0.0018 5 1 26 -0.6619 0.0016 5 1 27 0.3423 -0.0049 5 1 28 -1.2022 -0.0044 5 1 29 0.2496 -0.0128 5 1 30 -0.9831 -0.0094 5 2 0 1.0645 -0.0040 5 2 1 1.6273 -0.0026 5 2 2 1.5246 -0.0025 5 2 3 -4.3439 0.0003 5 2 4 1.5562 -0.0009 5 2 5 -7.9912 0.0039 5 2 6 1.1552 0.0003 5 2 7 -8.2855 0.0033 5 2 8 0.5625 0.0009 5 2 9 -6.1727 -0.0002 5 2 10 0.0562 0.0003 5 2 11 -2.9887 -0.0021 5 2 12 -0.1948 -0.0010 5 2 13 0.0989 -0.0013 5 2 14 -0.1450 -0.0018 5 2 15 1.9411 0.0007 5 2 16 0.0566 -0.0011 5 2 17 2.0939 0.0025 5 2 18 0.2152 -0.0002 5 2 19 1.3439 0.0026 5 2 20 0.4573 0.0001 5 2 21 0.7103 0.0008 5 2 22 1.0292 0.0005 5 2 23 0.3451 0.0006 5 2 24 1.5736 0.0011 5 2 25 -0.0575 0.0036 5 2 26 1.3015 -0.0006 5 2 27 -0.4356 0.0051 5 2 28 0.2175 -0.0054 5 2 29 -0.5333 0.0011 5 3 0 0.1957 -0.0019 5 3 1 6.7318 -0.0005 5 3 2 -2.2413 -0.0010 5 3 3 6.0783 0.0004 5 3 4 -3.9197 0.0008 5 3 5 3.4102 0.0019 5 3 6 -4.1531 0.0010 5 3 7 0.3164 0.0027 5 3 8 -3.3263 -0.0005 5 3 9 -2.1086 0.0013 5 3 10 -2.1140 -0.0014 5 3 11 -3.3535 -0.0004 5 3 12 -0.9532 -0.0009 5 3 13 -3.1070 -0.0010 5 3 14 -0.1501 0.0004 5 3 15 -1.7314 -0.0011 5 3 16 0.1199 0.0012 5 3 17 -0.3030 -0.0019 5 3 18 -0.0191 0.0003 5 3 19 0.5712 -0.0025 5 3 20 -0.2621 -0.0028 5 3 21 1.1981 -0.0023 5 3 22 -0.3338 -0.0053 5 3 23 1.6768 -0.0013 5 3 24 -0.0656 -0.0029 5 3 25 1.4337 0.0009 5 3 26 0.4038 0.0034 5 3 27 0.3635 0.0030 5 3 28 0.5935 0.0075 5 3 29 -0.6177 0.0026 5 4 0 4.2726 0.0001 5 4 1 -1.2039 0.0001 5 4 2 4.5273 0.0005 5 4 3 -0.1520 -0.0001 5 4 4 3.1043 0.0014 5 4 5 0.6223 -0.0004 5 4 6 0.9669 0.0011 5 4 7 0.9251 -0.0007 5 4 8 -0.9019 -0.0008 5 4 9 0.6598 -0.0006 5 4 10 -2.0527 -0.0017 5 4 11 -0.2635 0.0003 5 4 12 -2.2626 -0.0005 5 4 13 -1.4008 0.0017 5 4 14 -1.6103 0.0007 5 4 15 -1.9330 0.0021 5 4 16 -0.7241 -0.0001 5 4 17 -1.6989 0.0001 5 4 18 -0.1674 -0.0016 5 4 19 -1.2844 -0.0032 5 4 20 0.1420 -0.0017 5 4 21 -0.9560 -0.0050 5 4 22 0.3501 -0.0000 5 4 23 -0.4205 -0.0033 5 4 24 0.1888 0.0031 5 4 25 0.2720 0.0016 5 4 26 -0.3455 0.0070 5 4 27 0.5456 0.0070 5 4 28 -0.6666 0.0096 5 5 0 -0.8196 0.0007 5 5 1 0.2614 -0.0002 5 5 2 0.2842 -0.0005 5 5 3 0.2988 0.0003 5 5 4 1.1696 0.0003 5 5 5 0.2721 0.0010 5 5 6 1.4359 0.0017 5 5 7 0.1299 0.0002 5 5 8 1.0365 0.0010 5 5 9 0.1336 -0.0012 5 5 10 0.0356 -0.0004 5 5 11 0.2677 -0.0010 5 5 12 -1.2116 0.0002 5 5 13 0.1543 0.0014 5 5 14 -1.9040 0.0016 5 5 15 -0.2921 0.0035 5 5 16 -1.6409 0.0009 5 5 17 -0.7454 0.0029 5 5 18 -0.9959 -0.0009 5 5 19 -1.0106 0.0007 5 5 20 -0.5487 -0.0003 5 5 21 -1.1583 0.0011 5 5 22 -0.1316 0.0039 5 5 23 -1.2086 0.0051 5 5 24 0.3277 0.0092 5 5 25 -1.0738 0.0095 5 5 26 0.3232 0.0125 5 5 27 -0.7445 0.0114 5 6 0 -0.4940 0.0011 5 6 1 -0.1214 -0.0007 5 6 2 -0.5669 -0.0004 5 6 3 -0.4979 -0.0006 5 6 4 -0.1708 -0.0009 5 6 5 -0.5859 0.0010 5 6 6 0.3842 0.0012 5 6 7 -0.7336 0.0015 5 6 8 0.8648 0.0019 5 6 9 -1.0884 -0.0001 5 6 10 1.1691 -0.0006 5 6 11 -1.2326 -0.0016 5 6 12 1.0293 -0.0018 5 6 13 -0.8874 -0.0012 5 6 14 0.3749 0.0009 5 6 15 -0.2697 0.0002 5 6 16 -0.3300 0.0027 5 6 17 0.2867 0.0008 5 6 18 -0.7534 -0.0005 5 6 19 0.6086 0.0006 5 6 20 -1.0822 -0.0041 5 6 21 0.6915 0.0018 5 6 22 -1.2962 -0.0022 5 6 23 0.6170 0.0065 5 6 24 -1.0005 0.0035 5 6 25 0.3786 0.0123 5 6 26 -0.3268 0.0074 5 7 0 0.4372 0.0008 5 7 1 0.9852 -0.0000 5 7 2 -0.2832 0.0009 5 7 3 0.7665 -0.0024 5 7 4 -0.8768 -0.0010 5 7 5 0.6663 -0.0012 5 7 6 -1.0586 -0.0024 5 7 7 0.8377 0.0012 5 7 8 -1.0406 -0.0012 5 7 9 0.7657 -0.0002 5 7 10 -0.8383 0.0003 5 7 11 0.3320 -0.0035 5 7 12 -0.3118 0.0002 5 7 13 0.0030 -0.0035 5 7 14 0.3158 0.0012 5 7 15 -0.0216 -0.0015 5 7 16 0.7777 0.0036 5 7 17 -0.0112 -0.0019 5 7 18 1.1066 0.0016 5 7 19 -0.1658 -0.0049 5 7 20 1.2017 -0.0062 5 7 21 -0.3483 -0.0071 5 7 22 0.8271 -0.0108 5 7 23 -0.2802 -0.0062 5 7 24 0.2404 -0.0066 5 8 0 1.2885 0.0010 5 8 1 0.6307 0.0030 5 8 2 1.4856 -0.0010 5 8 3 0.6168 0.0005 5 8 4 1.0033 -0.0006 5 8 5 0.3416 -0.0030 5 8 6 0.5202 0.0001 5 8 7 0.4602 -0.0023 5 8 8 0.1990 -0.0010 5 8 9 0.8026 0.0006 5 8 10 -0.2302 -0.0020 5 8 11 0.6859 0.0009 5 8 12 -0.5386 -0.0019 5 8 13 0.2113 0.0005 5 8 14 -0.4617 -0.0011 5 8 15 0.0982 0.0023 5 8 16 -0.3375 0.0013 5 8 17 0.5128 0.0010 5 8 18 -0.3978 0.0050 5 8 19 0.8806 -0.0080 5 8 20 -0.3440 0.0050 5 8 21 0.7144 -0.0180 5 8 22 -0.0797 -0.0003 5 9 0 0.1605 0.0026 5 9 1 1.0473 0.0020 5 9 2 0.8804 0.0013 5 9 3 1.1988 0.0010 5 9 4 1.1720 -0.0000 5 9 5 0.5044 0.0001 5 9 6 1.2910 0.0021 5 9 7 -0.3145 -0.0009 5 9 8 1.6242 0.0032 5 9 9 -0.4350 0.0002 5 9 10 1.5335 -0.0007 5 9 11 -0.1438 0.0020 5 9 12 0.6213 -0.0057 5 9 13 -0.2284 0.0016 5 9 14 -0.1791 -0.0078 5 9 15 -0.7716 0.0026 5 9 16 -0.0942 -0.0093 5 9 17 -1.1771 0.0093 5 9 18 0.3159 -0.0121 5 9 19 -1.0336 0.0151 5 10 0 0.7518 0.0030 5 10 1 0.0734 0.0007 5 10 2 1.0249 0.0001 5 10 3 0.6104 -0.0007 5 10 4 0.7332 -0.0041 5 10 5 1.0672 0.0034 5 10 6 -0.1679 -0.0047 5 10 7 1.0696 0.0069 5 10 8 -0.5297 0.0002 5 10 9 0.7707 0.0028 5 10 10 0.1071 0.0042 5 10 11 0.4265 -0.0055 5 10 12 0.5217 0.0025 5 10 13 0.1642 -0.0121 5 10 14 -0.0973 -0.0004 5 10 15 0.0624 -0.0168 5 11 0 0.0143 0.0019 5 11 1 0.5297 -0.0018 5 11 2 -0.0434 -0.0035 5 11 3 0.2016 -0.0073 5 11 4 0.3406 -0.0036 5 11 5 -0.1126 -0.0098 5 11 6 0.4000 0.0002 5 11 7 -0.2117 -0.0036 5 11 8 -0.1837 0.0023 5 11 9 0.0444 0.0037 5 11 10 -0.5328 0.0009 6 0 0 6.1961 -0.0011 6 0 2 7.5663 -0.0002 6 0 4 5.6266 0.0023 6 0 6 1.2884 0.0026 6 0 8 -3.1678 0.0005 6 0 10 -6.1320 -0.0009 6 0 12 -7.0739 -0.0009 6 0 14 -5.9303 -0.0018 6 0 16 -3.3367 -0.0024 6 0 18 -0.7849 -0.0004 6 0 20 0.5380 0.0020 6 0 22 0.6877 0.0015 6 0 24 0.3159 0.0005 6 0 26 -0.1924 0.0030 6 0 28 -0.5900 0.0075 6 1 0 -4.1253 -0.0004 6 1 1 4.8087 0.0026 6 1 2 -0.6215 0.0001 6 1 3 4.5352 0.0002 6 1 4 2.9539 0.0008 6 1 5 2.2352 -0.0003 6 1 6 4.9294 0.0005 6 1 7 -0.8112 0.0003 6 1 8 4.8287 -0.0005 6 1 9 -3.2897 0.0004 6 1 10 3.3125 -0.0001 6 1 11 -4.5618 0.0006 6 1 12 1.1851 0.0019 6 1 13 -4.4202 0.0010 6 1 14 -0.8106 0.0017 6 1 15 -3.0565 -0.0000 6 1 16 -1.9119 -0.0013 6 1 17 -1.2524 -0.0016 6 1 18 -1.9477 -0.0023 6 1 19 0.0395 -0.0012 6 1 20 -1.5393 0.0002 6 1 21 0.4007 0.0003 6 1 22 -1.1596 0.0024 6 1 23 0.0808 -0.0005 6 1 24 -0.6285 0.0027 6 1 25 -0.3722 -0.0013 6 1 26 0.1224 0.0050 6 1 27 -0.5211 0.0027 6 1 28 0.6136 0.0094 6 1 29 -0.3229 0.0089 6 2 0 -0.6378 0.0019 6 2 1 -1.9544 0.0011 6 2 2 -0.8158 -0.0006 6 2 3 2.4050 0.0005 6 2 4 -0.8092 -0.0030 6 2 5 5.4780 -0.0007 6 2 6 -0.6199 -0.0031 6 2 7 6.1823 -0.0005 6 2 8 -0.3794 -0.0024 6 2 9 4.9324 0.0006 6 2 10 -0.1601 -0.0020 6 2 11 2.5911 0.0012 6 2 12 0.0253 -0.0012 6 2 13 0.0561 0.0006 6 2 14 0.0771 -0.0002 6 2 15 -1.6701 -0.0010 6 2 16 -0.0239 -0.0008 6 2 17 -2.1042 -0.0019 6 2 18 -0.1237 -0.0019 6 2 19 -1.7040 -0.0003 6 2 20 -0.2466 -0.0010 6 2 21 -1.1295 0.0024 6 2 22 -0.6052 -0.0001 6 2 23 -0.5675 0.0014 6 2 24 -0.9890 -0.0028 6 2 25 -0.0421 -0.0039 6 2 26 -0.7954 -0.0060 6 2 27 0.2832 -0.0077 6 2 28 -0.0239 -0.0043 6 3 0 -0.8490 0.0014 6 3 1 -4.6828 -0.0006 6 3 2 0.9362 0.0012 6 3 3 -4.3371 -0.0011 6 3 4 2.4724 0.0001 6 3 5 -2.5346 -0.0016 6 3 6 3.0148 0.0009 6 3 7 -0.3910 -0.0014 6 3 8 2.6237 0.0026 6 3 9 1.3733 -0.0013 6 3 10 1.7239 0.0020 6 3 11 2.4364 -0.0017 6 3 12 0.7503 -0.0008 6 3 13 2.4550 -0.0014 6 3 14 0.0830 -0.0021 6 3 15 1.5405 -0.0006 6 3 16 -0.1469 -0.0005 6 3 17 0.4533 -0.0002 6 3 18 -0.0757 0.0025 6 3 19 -0.3126 0.0001 6 3 20 0.1750 0.0047 6 3 21 -0.8818 0.0005 6 3 22 0.4724 0.0041 6 3 23 -1.1805 -0.0013 6 3 24 0.4987 -0.0012 6 3 25 -0.7968 -0.0066 6 3 26 0.1476 -0.0098 6 3 27 0.0980 -0.0113 6 3 28 -0.1384 -0.0148 6 4 0 -3.2912 0.0007 6 4 1 0.5274 0.0001 6 4 2 -3.5717 0.0022 6 4 3 -0.2707 -0.0006 6 4 4 -2.5009 0.0014 6 4 5 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0.0030 8 9 11 0.6071 0.0051 8 10 0 0.6239 -0.0017 8 10 1 0.3250 0.0041 8 10 2 0.2474 -0.0018 8 10 3 0.0796 0.0127 9 0 0 -2.0407 0.0052 9 0 2 -2.9644 -0.0008 9 0 4 -2.1846 -0.0059 9 0 6 -0.5531 -0.0034 9 0 8 0.9226 0.0028 9 0 10 2.1677 0.0046 9 0 12 3.0996 0.0023 9 0 14 3.0509 0.0002 9 0 16 1.8792 -0.0010 9 0 18 0.4260 -0.0002 9 0 20 -0.5748 0.0059 9 0 22 -1.0427 0.0132 9 1 0 1.1076 -0.0025 9 1 1 -1.6753 0.0008 9 1 2 -0.3227 0.0013 9 1 3 -1.6987 -0.0021 9 1 4 -1.5714 0.0024 9 1 5 -0.8419 -0.0017 9 1 6 -2.0131 -0.0004 9 1 7 0.1839 -0.0008 9 1 8 -1.9188 -0.0013 9 1 9 1.0452 -0.0014 9 1 10 -1.5644 0.0012 9 1 11 1.7091 -0.0011 9 1 12 -0.6958 0.0011 9 1 13 1.9300 0.0012 9 1 14 0.5591 -0.0023 9 1 15 1.5703 0.0020 9 1 16 1.3460 -0.0034 9 1 17 0.9356 0.0001 9 1 18 1.2080 -0.0004 9 1 19 0.3460 -0.0004 9 1 20 0.6257 0.0033 9 1 21 -0.1187 0.0014 9 1 22 0.1726 0.0053 9 1 23 -0.3438 0.0011 9 2 0 0.3574 -0.0008 9 2 1 0.5548 -0.0010 9 2 2 0.5431 -0.0012 9 2 3 -1.1735 0.0014 9 2 4 0.4859 0.0013 9 2 5 -2.2466 0.0017 9 2 6 0.3266 0.0018 9 2 7 -2.5039 0.0006 9 2 8 0.1601 -0.0021 9 2 9 -2.2585 0.0002 9 2 10 -0.1272 -0.0049 9 2 11 -1.4041 -0.0004 9 2 12 -0.4961 -0.0023 9 2 13 -0.0353 -0.0017 9 2 14 -0.5200 0.0013 9 2 15 1.0264 -0.0021 9 2 16 0.0202 0.0005 9 2 17 1.2014 -0.0015 9 2 18 0.6809 -0.0044 9 2 19 0.7785 -0.0005 9 2 20 0.9519 -0.0105 9 2 21 0.2208 0.0018 9 2 22 0.8661 -0.0150 9 2 23 -0.2342 0.0043 9 3 0 0.3555 -0.0009 9 3 1 1.8893 -0.0014 9 3 2 -0.3666 -0.0003 9 3 3 1.9520 0.0009 9 3 4 -1.0320 0.0006 9 3 5 1.2174 0.0031 9 3 6 -1.3339 0.0004 9 3 7 0.2884 0.0011 9 3 8 -1.2456 -0.0009 9 3 9 -0.7239 -0.0025 9 3 10 -0.7497 -0.0027 9 3 11 -1.6708 -0.0023 9 3 12 -0.0494 -0.0031 9 3 13 -1.9118 0.0006 9 3 14 0.3751 -0.0015 9 3 15 -1.2276 0.0013 9 3 16 0.3680 0.0012 9 3 17 -0.2495 -0.0027 9 3 18 0.2068 0.0040 9 3 19 0.4653 -0.0105 9 3 20 0.0076 0.0070 9 3 21 0.8479 -0.0178 9 3 22 -0.2753 0.0089 9 4 0 1.2980 0.0001 9 4 1 -0.8781 -0.0004 9 4 2 1.6178 0.0003 9 4 3 -0.5480 -0.0002 9 4 4 1.1492 0.0024 9 4 5 -0.2785 -0.0002 9 4 6 0.2779 0.0025 9 4 7 0.0304 -0.0013 9 4 8 -0.6441 0.0001 9 4 9 0.4373 -0.0025 9 4 10 -1.4126 -0.0001 9 4 11 0.6106 -0.0017 9 4 12 -1.6184 0.0030 9 4 13 0.4066 0.0003 9 4 14 -1.1814 0.0049 9 4 15 0.1511 0.0009 9 4 16 -0.6335 0.0023 9 4 17 0.0222 0.0014 9 4 18 -0.2756 -0.0039 9 4 19 -0.1310 0.0052 9 4 20 0.0620 -0.0099 9 4 21 -0.2592 0.0104 9 5 0 -1.2837 0.0005 9 5 1 0.2291 0.0000 9 5 2 -0.8663 -0.0012 9 5 3 0.0537 0.0010 9 5 4 -0.2839 -0.0017 9 5 5 -0.2910 0.0031 9 5 6 0.1356 -0.0005 9 5 7 -0.6854 0.0020 9 5 8 0.4731 0.0004 9 5 9 -0.8196 -0.0008 9 5 10 0.5915 0.0023 9 5 11 -0.6396 0.0005 9 5 12 0.4025 0.0051 9 5 13 -0.4286 0.0058 9 5 14 0.2571 0.0035 9 5 15 -0.3395 0.0078 9 5 16 0.2614 -0.0034 9 5 17 -0.2212 0.0021 9 5 18 0.0748 -0.0075 9 5 19 -0.0301 -0.0057 9 5 20 -0.2089 -0.0037 9 6 0 -0.3972 -0.0013 9 6 1 -0.3131 0.0005 9 6 2 -0.6444 -0.0004 9 6 3 -0.1114 -0.0029 9 6 4 -0.5823 0.0020 9 6 5 0.0554 -0.0025 9 6 6 -0.4141 0.0029 9 6 7 -0.0184 0.0007 9 6 8 -0.1756 -0.0015 9 6 9 -0.1398 0.0031 9 6 10 0.1147 -0.0067 9 6 11 -0.0293 0.0045 9 6 12 0.1288 -0.0038 9 6 13 0.2520 0.0042 9 6 14 -0.1465 0.0043 9 6 15 0.3443 -0.0006 9 6 16 -0.1980 0.0045 9 6 17 0.0987 -0.0083 9 6 18 0.0631 -0.0043 9 7 0 0.6396 0.0017 9 7 1 -0.3261 -0.0014 9 7 2 0.6504 0.0001 9 7 3 -0.3768 0.0018 9 7 4 0.5192 -0.0016 9 7 5 -0.0287 0.0032 9 7 6 0.1971 -0.0009 9 7 7 0.3953 0.0001 9 7 8 -0.2000 0.0001 9 7 9 0.4559 -0.0080 9 7 10 -0.2262 -0.0022 9 7 11 0.1345 -0.0131 9 7 12 0.1541 -0.0048 9 7 13 -0.1985 -0.0088 9 7 14 0.3051 -0.0027 9 7 15 -0.2405 -0.0022 9 8 0 0.1652 -0.0015 9 8 1 0.7143 0.0003 9 8 2 -0.0264 0.0008 9 8 3 0.6885 0.0006 9 8 4 -0.0224 0.0038 9 8 5 0.3847 0.0002 9 8 6 0.2485 0.0041 9 8 7 0.1617 -0.0007 9 8 8 0.2737 -0.0007 9 8 9 0.1292 -0.0042 9 8 10 -0.1468 -0.0085 9 8 11 0.1484 -0.0101 9 8 12 -0.4448 -0.0133 9 9 0 -0.0777 -0.0007 9 9 1 0.0083 0.0001 9 9 2 0.1602 -0.0018 9 9 3 -0.0618 0.0016 9 9 4 0.0419 -0.0035 9 9 5 -0.0927 0.0043 9 9 6 -0.0044 -0.0027 10 0 0 1.3692 -0.0026 10 0 2 2.3286 -0.0017 10 0 4 1.4024 -0.0000 10 0 6 0.0106 -0.0013 10 0 8 -0.7776 -0.0042 10 0 10 -1.4463 -0.0038 10 0 12 -2.2017 -0.0008 10 0 14 -2.1675 0.0007 10 0 16 -1.1119 0.0000 10 0 18 -0.0420 -0.0023 10 0 20 0.3917 -0.0075 10 1 0 -1.1382 0.0032 10 1 1 1.1192 -0.0022 10 1 2 0.3294 0.0004 10 1 3 0.9760 -0.0006 10 1 4 1.4097 -0.0024 10 1 5 0.0439 -0.0016 10 1 6 1.5196 0.0001 10 1 7 -0.6424 -0.0029 10 1 8 1.3111 0.0028 10 1 9 -0.9580 -0.0011 10 1 10 1.1370 0.0002 10 1 11 -1.2531 0.0004 10 1 12 0.4693 -0.0021 10 1 13 -1.3313 -0.0017 10 1 14 -0.6630 0.0022 10 1 15 -0.9318 -0.0030 10 1 16 -1.2627 0.0078 10 1 17 -0.3941 -0.0001 10 1 18 -0.9014 0.0066 10 1 19 -0.0827 0.0017 10 1 20 -0.2866 -0.0003 10 1 21 0.1018 -0.0010 10 2 0 -0.5611 -0.0024 10 2 1 -0.4369 0.0015 10 2 2 -0.8423 -0.0005 10 2 3 1.2066 -0.0008 10 2 4 -0.9818 -0.0019 10 2 5 1.8688 -0.0010 10 2 6 -0.9698 -0.0045 10 2 7 1.7846 0.0005 10 2 8 -0.7534 -0.0023 10 2 9 1.6044 0.0004 10 2 10 -0.2221 0.0015 10 2 11 1.0175 -0.0009 10 2 12 0.4385 -0.0002 10 2 13 -0.1817 -0.0007 10 2 14 0.6770 -0.0043 10 2 15 -1.1161 0.0003 10 2 16 0.2819 -0.0021 10 2 17 -1.0937 0.0005 10 2 18 -0.2451 0.0057 10 2 19 -0.5667 -0.0005 10 2 20 -0.3981 0.0114 10 3 0 -0.5398 -0.0001 10 3 1 -1.6157 -0.0004 10 3 2 0.2143 -0.0003 10 3 3 -1.6538 -0.0005 10 3 4 0.7281 0.0005 10 3 5 -1.1729 -0.0029 10 3 6 0.8103 0.0013 10 3 7 -0.6354 -0.0024 10 3 8 0.7044 0.0008 10 3 9 0.1949 0.0010 10 3 10 0.3982 0.0009 10 3 11 1.2749 0.0009 10 3 12 -0.1362 0.0016 10 3 13 1.7433 -0.0031 10 3 14 -0.5248 -0.0005 10 3 15 1.2280 -0.0038 10 3 16 -0.5245 -0.0052 10 3 17 0.4473 0.0025 10 3 18 -0.3668 -0.0086 10 3 19 0.0038 0.0113 10 4 0 -1.0942 -0.0000 10 4 1 0.2479 -0.0002 10 4 2 -1.1723 0.0007 10 4 3 -0.0196 0.0005 10 4 4 -0.7041 -0.0006 10 4 5 -0.1857 0.0012 10 4 6 -0.1683 0.0003 10 4 7 -0.3940 0.0013 10 4 8 0.4053 0.0034 10 4 9 -0.6645 0.0023 10 4 10 1.1185 0.0029 10 4 11 -0.6889 0.0038 10 4 12 1.4708 -0.0020 10 4 13 -0.4291 0.0029 10 4 14 1.1428 -0.0051 10 4 15 -0.2464 -0.0010 10 4 16 0.6527 -0.0024 10 4 17 -0.2250 -0.0051 10 4 18 0.4150 0.0042 10 5 0 0.9728 -0.0001 10 5 1 -0.3500 0.0007 10 5 2 0.5201 0.0010 10 5 3 -0.0960 -0.0002 10 5 4 0.1089 0.0007 10 5 5 0.1965 -0.0012 10 5 6 -0.1890 -0.0014 10 5 7 0.4534 0.0017 10 5 8 -0.5302 -0.0013 10 5 9 0.5688 0.0053 10 5 10 -0.6285 0.0004 10 5 11 0.5288 0.0036 10 5 12 -0.3509 0.0000 10 5 13 0.4348 -0.0027 10 5 14 -0.1785 -0.0008 10 5 15 0.3277 -0.0067 10 5 16 -0.2598 0.0009 10 6 0 0.2203 -0.0002 10 6 1 0.7656 0.0001 10 6 2 0.3369 -0.0018 10 6 3 0.5727 0.0028 10 6 4 0.2159 -0.0043 10 6 5 0.3527 0.0013 10 6 6 0.0689 -0.0042 10 6 7 0.2097 -0.0028 10 6 8 -0.1094 0.0019 10 6 9 0.1192 -0.0049 10 6 10 -0.2974 0.0093 10 6 11 0.0009 -0.0050 10 6 12 -0.1934 0.0082 10 6 13 -0.1738 -0.0046 10 6 14 0.1103 -0.0014 10 7 0 0.0135 -0.0003 10 7 1 0.5844 -0.0017 10 7 2 0.0243 0.0026 10 7 3 0.3996 -0.0059 10 7 4 -0.0104 0.0054 10 7 5 -0.0778 -0.0069 10 7 6 0.0261 0.0035 10 7 7 -0.5483 -0.0024 10 7 8 0.1833 -0.0014 10 7 9 -0.6603 0.0074 10 7 10 0.1546 -0.0029 10 7 11 -0.3413 0.0142 10 8 0 0.4790 0.0017 10 8 1 -0.5295 0.0016 10 8 2 0.4941 -0.0021 10 8 3 -0.5680 0.0031 10 8 4 0.2681 -0.0051 10 8 5 -0.4350 0.0045 10 8 6 -0.2275 -0.0036 11 0 0 -1.2084 -0.0031 11 0 2 -2.0495 -0.0006 11 0 4 -0.9651 0.0003 11 0 6 0.2530 0.0008 11 0 8 0.5041 0.0016 11 0 10 0.6766 -0.0002 11 0 12 1.2387 -0.0041 11 0 14 1.2269 -0.0052 11 0 16 0.3502 -0.0023 11 0 18 -0.2966 0.0014 11 1 0 1.2214 -0.0011 11 1 1 -1.1033 -0.0007 11 1 2 -0.1451 -0.0012 11 1 3 -0.7675 -0.0027 11 1 4 -1.0915 0.0015 11 1 5 0.3073 -0.0015 11 1 6 -1.0256 -0.0001 11 1 7 0.8325 0.0015 11 1 8 -0.7924 -0.0029 11 1 9 0.8093 0.0008 11 1 10 -0.7982 0.0010 11 1 11 0.8638 -0.0017 11 1 12 -0.3557 0.0066 11 1 13 0.8472 -0.0002 11 1 14 0.6017 0.0029 11 1 15 0.4138 0.0022 11 1 16 1.0396 -0.0070 11 1 17 -0.0541 0.0000 11 2 0 0.1969 0.0032 11 2 1 0.2847 -0.0013 11 2 2 0.4212 -0.0008 11 2 3 -1.2417 -0.0006 11 2 4 0.7823 -0.0017 11 2 5 -1.6247 -0.0010 11 2 6 1.0962 0.0026 11 2 7 -1.3213 -0.0015 11 2 8 1.1197 0.0038 11 2 9 -1.2100 0.0020 11 2 10 0.6779 0.0009 11 2 11 -0.8654 0.0071 11 2 12 -0.0226 0.0026 11 2 13 0.1428 0.0078 11 2 14 -0.4157 0.0078 11 2 15 0.9533 0.0041 11 2 16 -0.2715 0.0061 11 2 17 0.8190 0.0007 11 3 0 0.4201 0.0006 11 3 1 0.8094 0.0012 11 3 2 -0.3245 0.0011 11 3 3 0.7125 -0.0011 11 3 4 -0.7601 -0.0006 11 3 5 0.5464 0.0004 11 3 6 -0.7314 -0.0011 11 3 7 0.6074 0.0008 11 3 8 -0.6623 0.0029 11 3 9 0.2915 -0.0017 11 3 10 -0.5367 0.0063 11 3 11 -0.5741 -0.0008 11 3 12 -0.1334 0.0055 11 3 13 -1.0820 0.0052 11 3 14 0.2664 0.0047 11 3 15 -0.7564 0.0076 11 3 16 0.3358 0.0075 11 4 0 0.5392 -0.0005 11 4 1 0.3495 0.0020 11 4 2 0.2986 -0.0021 11 4 3 0.5457 0.0019 11 4 4 -0.1563 -0.0020 11 4 5 0.4710 0.0015 11 4 6 -0.2439 -0.0044 11 4 7 0.3709 0.0030 11 4 8 -0.2624 -0.0090 11 4 9 0.3260 0.0029 11 4 10 -0.6733 -0.0086 11 4 11 0.1337 -0.0010 11 4 12 -0.9936 -0.0024 11 4 13 -0.1416 -0.0036 11 4 14 -0.7267 0.0025 11 5 0 -0.1983 0.0011 11 5 1 0.0758 -0.0021 11 5 2 0.3882 0.0014 11 5 3 -0.2179 -0.0018 11 5 4 0.5498 0.0027 11 5 5 -0.3560 -0.0023 11 5 6 0.4564 0.0052 11 5 7 -0.3417 -0.0066 11 5 8 0.4404 0.0037 11 5 9 -0.3033 -0.0103 11 5 10 0.2292 -0.0022 11 5 11 -0.2921 -0.0085 11 5 12 -0.2543 -0.0058 11 6 0 -0.1324 0.0011 11 6 1 -0.5879 0.0002 11 6 2 -0.2061 0.0021 11 6 3 -0.4097 -0.0014 11 6 4 -0.0811 0.0034 11 6 5 -0.2722 0.0006 11 6 6 0.0237 0.0030 11 6 7 -0.1543 0.0038 11 6 8 0.1666 -0.0014 11 6 9 -0.1290 0.0035 11 7 0 -0.5074 -0.0015 11 7 1 -0.4080 0.0036 11 7 2 -0.6028 -0.0039 11 7 3 -0.2420 0.0068 12 0 0 1.5379 0.0023 12 0 2 2.1577 0.0027 12 0 4 1.0668 0.0048 12 0 6 -0.0094 0.0062 12 0 8 -0.0645 0.0047 12 0 10 -0.0615 0.0041 12 0 12 -0.5521 0.0065 12 1 0 -1.1222 -0.0006 12 1 1 1.4914 0.0029 12 1 2 -0.1991 0.0017 12 1 3 1.0444 0.0094 12 1 4 0.4464 -0.0005 12 1 5 -0.0689 0.0109 12 1 6 0.2750 -0.0002 12 1 7 -0.5693 0.0060 12 1 8 0.0901 0.0022 12 1 9 -0.5112 0.0025 12 1 10 0.2896 -0.0019 12 1 11 -0.5714 0.0031 12 1 12 0.1883 -0.0094 12 1 13 -0.6070 0.0021 12 2 0 0.4803 -0.0012 12 2 1 -0.2078 0.0016 12 2 2 0.3373 0.0047 12 2 3 0.8695 0.0020 12 2 4 -0.1705 0.0083 12 2 5 0.9463 0.0031 12 2 6 -0.7340 0.0036 12 2 7 0.5440 0.0029 12 2 8 -1.0360 -0.0011 12 2 9 0.5592 -0.0028 12 2 10 -0.8891 -0.0007 12 2 11 0.5428 -0.0103 12 2 12 -0.4146 -0.0026 12 3 0 -0.0535 0.0005 12 3 1 0.0694 -0.0001 12 3 2 0.4953 -0.0010 12 3 3 0.2242 0.0026 12 3 4 0.7360 0.0009 12 3 5 0.1390 0.0018 12 3 6 0.5817 0.0012 12 3 7 -0.3460 0.0009 12 3 8 0.5395 -0.0052 12 3 9 -0.4938 0.0029 12 3 10 0.5666 -0.0117 12 3 11 -0.0019 0.0020 12 4 0 0.0542 -0.0001 12 4 1 -0.4024 -0.0026 12 4 2 0.4136 0.0007 12 4 3 -0.5264 -0.0033 12 4 4 0.7629 0.0008 12 4 5 -0.3157 -0.0032 12 4 6 0.5230 0.0044 12 4 7 -0.0527 -0.0066 12 4 8 0.1637 0.0102 12 4 9 0.1317 -0.0092 12 5 0 -0.3573 -0.0018 12 5 1 0.2734 0.0011 12 5 2 -0.9214 -0.0029 12 5 3 0.4761 0.0013 12 5 4 -0.8301 -0.0043 12 5 5 0.4334 0.0029 13 0 0 -1.5112 0.0066 13 0 2 -1.9157 0.0012 13 0 4 -1.1088 -0.0066 13 0 6 -0.3087 -0.0110 13 1 0 0.7982 0.0001 13 1 1 -1.4629 0.0012 13 1 2 0.4642 -0.0025 13 1 3 -1.0776 -0.0095 13 1 4 0.1787 -0.0001 13 1 5 -0.2125 -0.0149 13 1 6 0.3463 0.0008 13 2 0 -0.7203 0.0004 13 2 1 0.2477 -0.0016 13 2 2 -0.6016 -0.0056 13 2 3 -0.2243 -0.0020 13 2 4 -0.1264 -0.0109 0 0 0 0.0 0.0 ; _iucr_refine_fcf_details ; data_mo_230411_SJ_P_OCH3_0m_CCDC1 _computing_structure_refinement 'olex2.refine 1.5 (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,y+1/2,-z+1/2 3 -x,-y,-z 4 x,-y-1/2,z-1/2 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_Int_Tables_number 14 _cell_length_a 10.2939(4) _cell_length_b 9.7381(4) _cell_length_c 25.5602(11) _cell_angle_alpha 90 _cell_angle_beta 91.730(2) _cell_angle_gamma 90 _cell_volume 2561.06(18) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -13 0 2 20.386 29.644 25.639 23.260 o -13 0 4 223.396 296.520 29.032 12.454 o -13 0 6 601.853 617.818 49.603 4.005 o -13 0 8 680.120 880.238 49.906 3.483 o -13 1 1 37.622 88.013 16.298 46.944 o -13 1 2 7.598 0.528 13.925 79.796 o -13 1 3 38.703 92.033 21.454 29.716 o -13 1 4 11.813 13.789 15.241 64.436 o -13 1 5 0.759 -26.558 15.563 65.928 o -13 1 6 2.043 -14.272 14.923 71.341 o -13 1 7 0.263 16.745 13.239 87.657 o -13 1 8 1.864 -5.223 12.640 99.233 o -13 2 1 66.677 51.672 28.619 17.683 o -13 2 2 292.117 330.590 27.052 12.196 o -13 2 3 33.946 13.172 15.990 54.904 o -13 2 4 176.476 203.281 23.759 18.364 o -13 2 5 2.609 8.103 10.571 136.338 o -13 2 6 46.283 72.265 13.263 63.499 o -12 0 2 130.593 158.136 20.093 25.732 o -12 0 4 4.406 -1.515 15.906 62.357 o -12 0 6 0.891 6.829 16.038 61.370 o -12 0 8 814.424 949.201 30.222 4.526 o -12 0 10 225.477 233.396 23.345 16.973 o -12 0 12 2.765 7.037 30.574 17.031 o -12 0 14 12.956 11.361 21.016 34.972 o -12 1 1 23.669 21.524 12.481 86.030 o -12 1 2 303.233 341.341 28.321 11.345 o -12 1 3 1.762 -3.909 15.791 63.828 o -12 1 4 153.122 179.722 18.105 27.208 o -12 1 5 23.534 11.060 8.430 165.888 o -12 1 6 22.535 35.313 9.560 126.056 o -12 1 7 89.085 91.503 13.157 52.608 o -12 1 8 76.596 60.767 12.059 64.871 o -12 1 9 39.806 57.489 10.441 93.325 o -12 1 10 0.970 13.825 11.749 110.583 o -12 1 11 224.582 222.112 26.225 14.874 o -12 1 12 32.807 37.585 14.089 65.412 o -12 1 13 1.838 10.046 20.079 39.146 o -12 1 14 15.607 -1.776 14.688 69.849 o -12 1 15 197.710 186.574 20.599 21.365 o -12 2 1 219.778 224.710 14.017 27.602 o -12 2 2 58.271 51.388 9.627 93.924 o -12 2 3 57.901 78.501 10.754 77.405 o -12 2 4 9.114 -5.455 9.770 155.051 o -12 2 5 59.900 45.145 9.712 93.842 o -12 2 6 59.533 28.676 13.053 67.237 o -12 2 7 21.973 6.641 11.738 100.172 o -12 2 8 15.416 14.870 10.588 121.298 o -12 2 9 8.428 1.789 11.515 113.887 o -12 2 10 67.978 79.521 12.202 63.770 o -12 2 11 69.621 42.834 13.094 62.448 o -12 2 12 91.115 59.711 17.013 39.470 o -12 2 13 76.107 61.873 18.281 36.753 o -12 2 14 23.480 -8.124 14.912 65.940 o -12 3 1 71.656 76.959 14.705 49.890 o -12 3 2 22.497 29.954 12.832 80.951 o -12 3 3 75.016 70.825 13.098 57.895 o -12 3 4 14.370 -3.338 10.188 137.793 o -12 3 5 1.639 3.037 13.462 87.062 o -12 3 6 58.350 61.707 16.003 47.205 o -12 3 7 91.808 137.331 15.341 40.501 o -12 3 8 78.776 104.530 15.196 44.723 o -12 3 9 37.496 9.835 12.577 81.746 o -12 3 10 231.564 233.254 18.519 21.341 o -12 3 11 40.709 41.887 13.158 69.925 o -12 3 12 30.468 44.307 14.336 63.343 o -12 3 13 3.996 20.792 20.564 36.785 o -12 4 1 23.959 16.920 10.487 115.628 o -12 4 2 25.685 28.088 16.940 49.701 o -12 4 3 51.586 37.368 12.274 74.519 o -12 4 4 143.388 135.851 15.688 34.310 o -12 4 5 5.479 -0.618 13.393 86.991 o -12 4 6 34.214 53.324 17.846 42.857 o -12 4 7 36.501 29.511 13.357 71.365 o -12 4 8 77.466 81.525 20.475 30.068 o -12 4 9 0.095 -3.378 15.312 68.266 o -12 4 10 25.831 46.083 15.238 58.031 o -12 4 11 1.951 -4.836 13.382 88.592 o -12 5 1 28.755 25.554 13.545 72.671 o -12 5 2 202.280 250.913 22.697 17.943 o -12 5 3 48.171 40.762 15.241 54.309 o -12 5 4 122.086 153.470 21.127 24.574 o -12 5 5 81.216 61.685 20.033 31.516 o -12 5 6 119.751 136.232 16.728 33.931 o -12 5 7 6.199 6.108 13.112 89.023 o -11 0 2 103.904 53.427 20.558 29.151 o -11 0 4 292.412 241.955 24.848 14.222 o -11 0 6 39.797 64.636 12.824 69.469 o -11 0 8 454.774 440.052 25.648 9.704 o -11 0 10 362.205 366.150 23.319 12.504 o -11 0 12 14.141 -3.184 14.940 68.018 o -11 0 14 234.543 279.173 25.077 14.888 o -11 0 16 40.698 -14.836 23.650 26.891 o -11 0 18 261.041 237.301 32.280 10.694 o -11 1 1 7.265 2.674 9.844 153.555 o -11 1 2 149.899 138.858 12.066 42.569 o -11 1 3 0.860 19.412 7.528 243.512 o -11 1 4 426.842 412.867 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21.128 9.460 130.846 o 10 5 6 199.517 188.056 24.449 17.284 o 10 5 7 9.774 16.953 12.109 98.567 o 10 5 8 372.800 396.022 22.168 12.547 o 10 5 9 86.172 76.183 14.312 49.329 o 10 5 10 39.210 43.867 11.212 88.422 o 10 5 11 50.805 88.165 9.590 88.540 o 10 5 12 1.174 -5.901 9.962 159.742 o 10 5 13 23.918 7.830 19.162 40.893 o 10 5 14 1.022 2.141 10.571 141.027 o 10 5 15 21.776 5.648 13.750 76.059 o 10 5 16 23.401 9.337 14.949 64.551 o 10 6 0 2.446 4.509 8.931 191.114 o 10 6 1 252.101 255.964 16.318 22.175 o 10 6 2 6.741 16.449 12.103 100.452 o 10 6 3 45.998 77.526 12.746 66.424 o 10 6 4 13.487 17.328 12.059 97.233 o 10 6 5 1.511 14.330 11.187 120.772 o 10 6 6 73.934 74.897 13.770 54.161 o 10 6 7 34.477 48.835 12.119 80.025 o 10 6 8 1.136 5.256 12.668 97.811 o 10 6 9 9.476 19.660 11.238 111.946 o 10 6 10 10.146 23.401 13.094 84.079 o 10 6 11 0.171 -9.147 13.656 85.790 o 10 6 12 4.230 9.132 18.402 46.250 o 10 6 13 153.383 138.136 19.883 25.424 o 10 6 14 1.869 -1.139 17.988 49.242 o 10 7 0 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234.104 o 11 2 7 5.729 11.098 8.808 183.455 o 11 2 8 9.631 3.104 9.523 159.649 o 11 2 9 2.329 -0.004 8.495 215.943 o 11 2 10 8.796 5.407 9.871 149.174 o 11 2 11 51.457 54.070 9.478 98.731 o 11 2 12 15.534 19.106 10.478 121.590 o 11 2 13 0.844 1.102 9.950 159.802 o 11 2 14 11.083 31.803 11.123 108.685 o 11 2 15 30.186 43.498 12.369 80.226 o 11 2 16 3.597 5.764 13.941 80.097 o 11 2 17 85.540 88.405 15.827 42.565 o 11 3 0 38.047 51.711 7.894 133.043 o 11 3 1 27.776 32.956 10.076 113.622 o 11 3 2 361.944 364.334 18.929 14.650 o 11 3 3 33.734 18.600 12.650 80.752 o 11 3 4 300.928 313.920 18.387 17.405 o 11 3 5 42.806 25.038 9.313 117.271 o 11 3 6 45.587 39.274 9.312 109.656 o 11 3 7 0.032 2.949 9.918 160.693 o 11 3 8 60.643 55.209 8.451 104.286 o 11 3 9 1.785 14.580 8.120 217.188 o 11 3 10 269.518 306.330 15.218 21.207 o 11 3 11 28.582 20.665 9.135 135.810 o 11 3 12 169.807 155.471 14.088 34.424 o 11 3 13 0.935 6.748 13.137 90.838 o 11 3 14 58.746 59.148 12.423 67.694 o 11 3 15 92.922 108.931 15.720 40.817 o 11 3 16 9.253 15.872 17.401 50.404 o 11 4 0 45.040 35.562 9.745 105.373 o 11 4 1 0.090 3.655 9.571 171.735 o 11 4 2 52.871 58.286 9.737 93.828 o 11 4 3 2.410 2.277 10.609 138.536 o 11 4 4 85.837 90.994 9.777 71.799 o 11 4 5 85.343 97.565 11.063 63.321 o 11 4 6 219.372 210.851 14.965 26.825 o 11 4 7 1.415 30.939 9.561 151.026 o 11 4 8 3.366 17.624 14.432 73.193 o 11 4 9 1.857 21.787 10.800 125.470 o 11 4 10 88.094 110.905 11.392 59.156 o 11 4 11 26.813 16.279 10.258 117.697 o 11 4 12 7.825 10.923 10.724 126.621 o 11 4 13 19.468 38.051 12.942 79.442 o 11 4 14 0.239 -15.558 12.005 110.934 o 11 5 0 171.759 192.197 15.348 30.261 o 11 5 1 56.697 85.169 11.854 68.451 o 11 5 2 56.773 57.944 11.980 71.761 o 11 5 3 1.483 20.016 9.768 152.066 o 11 5 4 66.117 60.837 11.082 75.042 o 11 5 5 31.877 57.468 10.960 91.508 o 11 5 6 228.521 247.785 16.258 23.618 o 11 5 7 0.014 0.184 10.203 153.671 o 11 5 8 36.014 42.570 10.884 94.101 o 11 5 9 47.654 51.378 10.984 85.213 o 11 5 10 11.318 1.326 13.061 88.506 o 11 5 11 39.645 30.304 11.223 91.355 o 11 5 12 2.668 -6.277 21.183 35.501 o 11 6 0 117.020 127.559 17.709 32.200 o 11 6 1 3.643 10.166 11.448 115.582 o 11 6 2 23.458 23.011 11.716 95.264 o 11 6 3 19.425 22.052 13.059 81.176 o 11 6 4 3.373 1.481 12.907 94.136 o 11 6 5 114.814 114.973 15.475 38.755 o 11 6 6 43.689 46.448 14.393 59.721 o 11 6 7 250.588 224.693 21.094 18.310 o 11 6 8 1.491 -6.058 15.572 65.683 o 11 6 9 32.690 30.009 13.630 70.111 o 11 7 0 1.398 11.866 17.381 51.919 o 11 7 1 198.379 219.110 24.532 16.843 o 11 7 2 1.359 19.466 16.686 55.606 o 11 7 3 63.568 67.476 28.502 17.717 o 12 0 0 31.097 46.763 22.575 28.663 o 12 0 2 24.739 33.972 16.568 51.396 o 12 0 4 131.128 191.613 32.702 12.226 o 12 0 6 28.614 3.166 18.386 43.923 o 12 0 8 3.589 -10.937 29.066 18.884 o 12 0 10 618.195 554.269 46.754 4.346 o 12 0 12 133.656 143.480 25.561 18.475 o 12 1 0 50.900 63.048 11.513 76.678 o 12 1 1 131.352 166.838 14.496 36.807 o 12 1 2 0.031 -2.670 14.387 77.350 o 12 1 3 230.689 298.770 23.552 15.846 o 12 1 4 77.934 109.674 19.311 31.901 o 12 1 5 18.039 21.961 14.068 71.692 o 12 1 6 246.431 267.647 19.667 18.997 o 12 1 7 2.507 -17.931 13.859 82.444 o 12 1 8 511.762 617.557 27.894 7.644 o 12 1 9 83.081 92.972 24.966 21.383 o 12 1 10 255.890 313.475 31.418 10.716 o 12 1 11 304.361 328.234 29.627 10.836 o 12 1 12 171.074 159.347 17.918 27.052 o 12 1 13 7.891 22.546 21.118 34.612 o 12 2 0 1.246 20.611 10.166 141.338 o 12 2 1 23.715 52.158 15.440 56.584 o 12 2 2 0.026 8.539 14.584 74.007 o 12 2 3 0.787 31.618 16.035 58.980 o 12 2 4 7.675 17.727 15.601 62.135 o 12 2 5 70.524 95.487 20.206 30.696 o 12 2 6 180.487 186.431 28.912 14.078 o 12 2 7 36.927 25.298 24.658 24.543 o 12 2 8 176.497 229.378 25.037 16.816 o 12 2 9 3.313 2.459 16.341 59.102 o 12 2 10 1.409 37.255 13.274 82.714 o 12 2 11 4.713 14.368 14.158 75.995 o 12 2 12 32.555 11.431 16.761 50.867 o 12 3 0 37.741 55.576 13.667 64.982 o 12 3 1 4.728 14.219 11.406 114.134 o 12 3 2 549.047 559.700 24.282 8.313 o 12 3 3 6.863 11.852 11.510 111.577 o 12 3 4 279.199 294.443 22.110 15.723 o 12 3 5 8.028 -1.179 19.184 42.708 o 12 3 6 8.325 2.043 10.636 132.175 o 12 3 7 41.298 0.145 11.084 100.338 o 12 3 8 30.720 44.495 13.039 73.587 o 12 3 9 7.496 20.029 16.901 53.232 o 12 3 10 22.724 35.473 13.153 76.653 o 12 3 11 21.268 3.710 16.853 52.644 o 12 4 0 0.022 -22.209 9.609 173.366 o 12 4 1 78.434 101.224 17.341 37.618 o 12 4 2 11.492 10.151 13.615 80.177 o 12 4 3 198.121 202.166 18.207 23.969 o 12 4 4 6.799 5.107 12.415 98.738 o 12 4 5 16.472 -18.475 12.042 100.549 o 12 4 6 15.127 31.523 13.402 77.458 o 12 4 7 13.612 17.089 10.147 130.999 o 12 4 8 15.946 19.542 10.652 117.797 o 12 4 9 3.915 41.222 16.823 52.602 o 12 5 0 205.423 218.493 19.926 21.195 o 12 5 1 8.507 -7.906 14.018 78.571 o 12 5 2 1.437 7.009 14.106 78.793 o 12 5 3 4.214 16.325 14.729 70.350 o 12 5 4 3.592 24.267 15.928 59.904 o 12 5 5 15.219 27.742 13.793 74.216 o 13 0 0 80.731 68.515 21.035 28.991 o 13 0 2 0.108 7.689 29.092 18.844 o 13 0 4 25.212 29.786 29.498 17.679 o 13 0 6 30.689 22.277 31.182 15.862 o 13 1 0 0.415 -7.546 14.016 81.357 o 13 1 1 2.305 -3.289 13.893 82.126 o 13 1 2 62.567 102.968 19.466 32.827 o 13 1 3 112.292 114.378 28.464 16.329 o 13 1 4 0.076 -5.036 25.011 25.594 o 13 1 5 0.838 -7.558 20.260 38.939 o 13 1 6 41.776 21.852 25.429 23.073 o 13 2 0 19.942 17.006 14.080 71.751 o 13 2 1 428.946 468.301 32.428 7.929 o 13 2 2 3.591 0.244 22.708 30.860 o 13 2 3 157.979 163.840 32.441 12.231 o 13 2 4 138.698 177.057 33.113 11.976 o ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,y+1/2,-z+1/2 3 -x,-y,-z 4 x,-y-1/2,z-1/2 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_group S1 S 0.88320(4) 0.22517(5) 0.751743(17) 0.02653(12) Uani 1.000000 . . . . F1 F 0.95502(10) 0.60297(11) 0.86887(4) 0.0354(3) Uani 1.000000 . . . . F2 F 0.91077(11) 0.41640(12) 0.91102(4) 0.0364(3) Uani 1.000000 . . . . O1 O 1.11069(16) 0.68364(15) 0.50873(5) 0.0467(4) Uani 1.000000 . . . . O2 O 1.12952(11) 0.40517(13) 0.65616(5) 0.0287(3) Uani 1.000000 . . . . O3 O 1.15727(12) 0.29098(14) 0.72949(5) 0.0347(3) Uani 1.000000 . . . . O4 O 0.74488(12) 0.21133(13) 0.74712(5) 0.0329(3) Uani 1.000000 . . . . O5 O 0.96012(13) 0.10211(12) 0.75123(5) 0.0342(3) Uani 1.000000 . . . . O6 O 0.72800(15) 0.65199(18) 0.92587(6) 0.0527(4) Uani 1.000000 . . . . N1 N 0.64001(15) 0.49108(18) 0.86798(6) 0.0334(4) Uani 1.000000 D U . . C1 C 0.84839(19) 0.5726(2) 0.59258(7) 0.0335(4) Uani 1.000000 . . . . H1 H 0.75725(19) 0.5828(2) 0.59599(7) 0.0403(5) Uiso 1.000000 R . . . C2 C 0.9085(2) 0.6386(2) 0.55242(8) 0.0382(5) Uani 1.000000 . . . . H2 H 0.8592(2) 0.6938(2) 0.52845(8) 0.0458(6) Uiso 1.000000 R . . . C3 C 1.0423(2) 0.6241(2) 0.54709(7) 0.0352(4) Uani 1.000000 . . . . C4 C 1.11499(19) 0.5441(2) 0.58202(7) 0.0327(4) Uani 1.000000 . . . . H4 H 1.20605(19) 0.5339(2) 0.57838(7) 0.0393(5) Uiso 1.000000 R . . . C5 C 1.05238(17) 0.47964(18) 0.62209(7) 0.0264(4) Uani 1.000000 . . . . C6 C 0.91839(17) 0.49025(18) 0.62873(7) 0.0262(4) Uani 1.000000 . . . . C7 C 0.85927(16) 0.41427(17) 0.67019(7) 0.0248(4) Uani 1.000000 . . . . C8 C 0.93804(16) 0.33488(17) 0.70172(7) 0.0235(3) Uani 1.000000 . . . . C9 C 1.07993(17) 0.33934(18) 0.69847(7) 0.0265(4) Uani 1.000000 . . . . C10 C 1.0426(3) 0.7708(2) 0.47253(9) 0.0535(6) Uani 1.000000 . . . . H10a H 1.1007(6) 0.7980(15) 0.4447(4) 0.0803(9) Uiso 1.000000 GR . . . H10b H 0.9677(10) 0.7214(7) 0.4572(5) 0.0803(9) Uiso 1.000000 GR . . . H10c H 1.0124(15) 0.8528(9) 0.49077(16) 0.0803(9) Uiso 1.000000 GR . . . C11 C 0.71641(16) 0.43474(18) 0.67684(7) 0.0263(4) Uani 1.000000 . . . . C12 C 0.67651(17) 0.55146(19) 0.70296(7) 0.0292(4) Uani 1.000000 . . . . H12 H 0.73898(17) 0.61571(19) 0.71595(7) 0.0351(5) Uiso 1.000000 R . . . C13 C 0.54462(19) 0.5743(2) 0.71010(8) 0.0371(5) Uani 1.000000 . . . . H13 H 0.51725(19) 0.6529(2) 0.72882(8) 0.0446(5) Uiso 1.000000 R . . . C14 C 0.4539(2) 0.4830(2) 0.69002(9) 0.0450(5) Uani 1.000000 . . . . H14 H 0.3640(2) 0.4981(2) 0.69523(9) 0.0539(6) Uiso 1.000000 R . . . C15 C 0.4934(2) 0.3699(2) 0.66244(10) 0.0481(6) Uani 1.000000 . . . . H15 H 0.4303(2) 0.3087(2) 0.64782(10) 0.0578(7) Uiso 1.000000 R . . . C16 C 0.62448(18) 0.3443(2) 0.65576(9) 0.0383(5) Uani 1.000000 . . . . H16 H 0.65114(18) 0.2656(2) 0.63693(9) 0.0460(6) Uiso 1.000000 R . . . C17 C 0.92250(17) 0.31383(19) 0.81116(7) 0.0281(4) Uani 1.000000 . . . . H17a H 0.92140(17) 0.24762(19) 0.84053(7) 0.0337(5) Uiso 1.000000 R . . . H17b H 1.01186(17) 0.35075(19) 0.80934(7) 0.0337(5) Uiso 1.000000 R . . . C18 C 0.82996(16) 0.43148(18) 0.82256(7) 0.0258(4) Uani 1.000000 . . . . H18 H 0.83317(16) 0.49927(18) 0.79324(7) 0.0310(4) Uiso 1.000000 R . . . C19 C 0.86330(17) 0.50469(19) 0.87304(7) 0.0287(4) Uani 1.000000 . . . . C20 C 0.73539(18) 0.5628(2) 0.89310(7) 0.0350(4) Uani 1.000000 . . . . C21 C 0.68742(17) 0.3904(2) 0.83006(7) 0.0321(4) Uani 1.000000 . . . . H21a H 0.68138(17) 0.2959(2) 0.84398(7) 0.0386(5) Uiso 1.000000 R . . . H21b H 0.63684(17) 0.3960(2) 0.79656(7) 0.0386(5) Uiso 1.000000 R . . . C22 C 0.5080(9) 0.4948(12) 0.8830(4) 0.0355(13) Uani 0.656(6) D U P 1 C22A C 0.5007(18) 0.478(3) 0.8778(7) 0.0372(19) Uani 0.344(6) D U P 2 C23 C 0.4164(6) 0.4396(7) 0.8489(3) 0.0524(13) Uani 0.656(6) D U P 1 H23 H 0.4408(6) 0.4070(7) 0.8156(3) 0.0629(16) Uiso 0.656(6) R . P 1 C23A C 0.4083(10) 0.4765(11) 0.8387(4) 0.0317(16) Uani 0.344(6) D U P 2 H23A H 0.4337(10) 0.4857(11) 0.8035(4) 0.0381(19) Uiso 0.344(6) R . P 2 C24 C 0.2876(6) 0.4317(7) 0.8636(3) 0.0602(14) Uani 0.656(6) D U P 1 H24 H 0.2244(6) 0.3944(7) 0.8398(3) 0.0722(17) Uiso 0.656(6) R . P 1 C24A C 0.2792(10) 0.4616(11) 0.8491(4) 0.0349(15) Uani 0.344(6) D U P 2 H24A H 0.2163(10) 0.4560(11) 0.8212(4) 0.0418(18) Uiso 0.344(6) R . P 2 C25 C 0.2503(7) 0.4760(9) 0.9112(3) 0.0499(14) Uani 0.656(6) D U P 1 H25 H 0.1641(7) 0.4617(9) 0.9223(3) 0.0599(16) Uiso 0.656(6) R . P 1 C25A C 0.2422(14) 0.4551(18) 0.8991(5) 0.046(2) Uani 0.344(6) D U P 2 H25A H 0.1523(14) 0.4566(18) 0.9065(5) 0.056(2) Uiso 0.344(6) R . P 2 C26 C 0.3397(3) 0.5416(6) 0.94247(15) 0.0552(11) Uani 0.656(6) D U P 1 H26 H 0.3128(3) 0.5816(6) 0.97427(15) 0.0663(13) Uiso 0.656(6) R . P 1 C26A C 0.3360(7) 0.4460(12) 0.9413(3) 0.0576(17) Uani 0.344(6) D U P 2 H26A H 0.3104(7) 0.4320(12) 0.9763(3) 0.069(2) Uiso 0.344(6) R . P 2 C27 C 0.4686(3) 0.5517(6) 0.92930(13) 0.0482(10) Uani 0.656(6) D U P 1 H27 H 0.5294(3) 0.5974(6) 0.95193(13) 0.0578(12) Uiso 0.656(6) R . P 1 C27A C 0.4669(7) 0.4584(12) 0.9292(3) 0.0545(17) Uani 0.344(6) D U P 2 H27A H 0.5324(7) 0.4531(12) 0.9561(3) 0.065(2) Uiso 0.344(6) R . P 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 S1 0.0264(2) 0.0209(2) 0.0324(2) -0.00052(17) 0.00413(17) 0.00225(18) F1 0.0349(6) 0.0336(6) 0.0377(6) -0.0055(5) 0.0023(5) -0.0017(5) F2 0.0385(6) 0.0402(7) 0.0303(6) 0.0058(5) -0.0036(5) 0.0090(5) O1 0.0660(10) 0.0402(8) 0.0343(8) -0.0047(7) 0.0097(7) 0.0085(6) O2 0.0234(6) 0.0290(7) 0.0340(7) 0.0015(5) 0.0043(5) 0.0044(5) O3 0.0254(6) 0.0345(8) 0.0441(8) 0.0051(6) -0.0015(6) 0.0105(6) O4 0.0276(7) 0.0311(7) 0.0403(7) -0.0069(5) 0.0049(5) 0.0000(6) O5 0.0419(8) 0.0200(7) 0.0412(7) 0.0050(6) 0.0091(6) 0.0040(6) O6 0.0457(9) 0.0667(11) 0.0460(9) 0.0116(8) 0.0044(7) -0.0221(8) N1 0.0239(8) 0.0430(10) 0.0337(8) 0.0055(7) 0.0055(6) 0.0000(7) C1 0.0356(10) 0.0304(10) 0.0345(10) 0.0031(8) -0.0028(8) 0.0005(8) C2 0.0524(13) 0.0305(11) 0.0312(10) 0.0011(9) -0.0050(9) 0.0031(8) C3 0.0524(12) 0.0259(10) 0.0275(9) -0.0061(9) 0.0064(8) -0.0007(8) C4 0.0372(10) 0.0287(10) 0.0327(10) -0.0028(8) 0.0065(8) -0.0039(8) C5 0.0312(9) 0.0194(9) 0.0288(9) -0.0002(7) 0.0020(7) -0.0015(7) C6 0.0292(9) 0.0210(9) 0.0283(9) 0.0002(7) 0.0007(7) -0.0015(7) C7 0.0243(9) 0.0196(9) 0.0303(9) -0.0012(7) -0.0011(7) -0.0057(7) C8 0.0239(8) 0.0180(8) 0.0287(9) 0.0002(7) 0.0023(7) -0.0012(7) C9 0.0260(9) 0.0197(9) 0.0340(9) 0.0018(7) 0.0042(7) 0.0004(7) C10 0.0844(18) 0.0421(13) 0.0338(11) -0.0105(12) -0.0030(11) 0.0084(10) C11 0.0229(8) 0.0231(9) 0.0327(9) 0.0006(7) -0.0018(7) 0.0007(7) C12 0.0259(9) 0.0261(9) 0.0355(10) 0.0012(7) -0.0034(7) 0.0002(8) C13 0.0316(10) 0.0350(11) 0.0448(11) 0.0094(8) 0.0004(8) -0.0025(9) C14 0.0232(10) 0.0465(13) 0.0651(14) 0.0050(9) 0.0002(9) 0.0000(11) C15 0.0266(10) 0.0439(13) 0.0734(16) -0.0069(9) -0.0082(10) -0.0067(12) C16 0.0291(10) 0.0304(11) 0.0553(13) -0.0003(8) -0.0028(9) -0.0093(9) C17 0.0244(9) 0.0294(10) 0.0304(9) 0.0034(7) 0.0015(7) 0.0013(7) C18 0.0232(8) 0.0269(9) 0.0275(9) 0.0018(7) 0.0022(7) 0.0034(7) C19 0.0261(9) 0.0301(10) 0.0296(9) 0.0016(7) -0.0009(7) 0.0048(7) C20 0.0312(10) 0.0438(12) 0.0299(10) 0.0069(9) 0.0024(8) 0.0011(9) C21 0.0247(9) 0.0372(11) 0.0348(10) 0.0012(8) 0.0039(7) -0.0020(8) C22 0.027(2) 0.042(2) 0.037(3) 0.0046(14) 0.0024(15) 0.0032(17) C22A 0.026(3) 0.054(4) 0.032(3) 0.0083(19) 0.0053(19) -0.001(2) C23 0.036(2) 0.061(3) 0.061(3) -0.0018(18) 0.0085(18) -0.0169(19) C23A 0.025(3) 0.041(4) 0.029(3) -0.002(2) -0.0018(18) 0.008(2) C24 0.033(2) 0.073(3) 0.075(4) -0.0083(18) 0.006(2) -0.014(2) C24A 0.026(3) 0.045(3) 0.033(3) -0.0015(19) -0.0032(19) 0.014(2) C25 0.027(2) 0.068(3) 0.056(3) 0.0076(16) 0.0140(18) 0.005(2) C25A 0.027(3) 0.072(4) 0.040(4) 0.001(2) 0.002(2) -0.003(2) C26 0.0352(17) 0.088(3) 0.0432(18) 0.0143(17) 0.0097(12) -0.0006(17) C26A 0.039(3) 0.096(4) 0.038(3) -0.003(2) 0.0105(18) -0.005(2) C27 0.0296(16) 0.079(3) 0.0354(16) 0.0104(16) 0.0006(11) -0.0052(16) C27A 0.033(3) 0.092(4) 0.038(3) 0.002(2) 0.0016(17) -0.002(2) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source C 0.00347 0.00161 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.21560 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' F 0.01794 0.01033 3.53920 2.64120 1.51700 1.02430 10.28250 4.29440 0.26150 26.14760 0.27760 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.00304 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' N 0.00653 0.00323 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750 0.58260 -11.52900 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' O 0.01158 0.00611 3.04850 2.28680 1.54630 0.86700 13.27710 5.70110 0.32390 32.90890 0.25080 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' S 0.12424 0.12443 6.90530 5.20340 1.43790 1.58630 1.46790 22.21510 0.25360 56.17200 0.86690 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u -2 0 0 2357.36 49.3 2 0 0 2338.17 45.8 -3 0 0 747.13 20.2 -3 0 0 691.23 17 -3 0 0 742.33 15.5 3 0 0 700.83 17.1 -4 0 0 355.36 13.7 -4 0 0 384.76 11.2 -4 0 0 337.47 8.7 4 0 0 359.46 10.9 -5 0 0 4781.92 100.29 -5 0 0 4735.53 91.99 -5 0 0 4677.63 92.79 -5 0 0 4695.03 96.09 -5 0 0 4806.02 101.99 -6 0 0 160.68 7.8 -6 0 0 149.99 10.1 -6 0 0 157.88 4.9 -6 0 0 147.29 5.4 -6 0 0 137.59 9 -6 0 0 147.99 4.7 -6 0 0 155.68 4.2 -7 0 0 -2.5 2.3 -7 0 0 3.4 0.9 -7 0 0 5.5 2.9 -7 0 0 4.2 1 -7 0 0 4.6 0.9 -7 0 0 4.9 1.2 -7 0 0 4.1 1.6 -8 0 0 136.79 5 -8 0 0 128.99 6.2 -8 0 0 138.09 10.5 -8 0 0 135.39 11.1 -8 0 0 120.69 7.9 -9 0 0 33.1 6.5 -9 0 0 34.8 7.4 -9 0 0 40.7 5.2 -9 0 0 33.9 3.1 -10 0 0 73.59 4.9 -10 0 0 80.99 10.8 -10 0 0 81.09 9.5 -10 0 0 87.49 8 -11 0 0 3.6 5.3 -11 0 0 4 3.3 -11 0 0 4.7 2.4 -12 0 0 9.6 4.7 -12 0 0 2.7 5.3 -12 0 0 6.7 6.7 -13 0 0 2.2 6.2 -13 0 0 12.8 5.7 -13 0 0 12.7 4.5 -13 0 0 8.2 8.9 0 -1 0 0.2 0.3 0 -1 0 0 0.2 0 -1 0 0.2 0.2 0 -1 0 0.1 0.3 0 1 0 0.1 0.3 0 1 0 0.2 0.4 0 1 0 0.1 0.2 -1 -1 0 487.85 11.5 1 -1 0 502.95 11.7 1 -1 0 497.95 11.8 -1 1 0 502.25 11.9 -1 1 0 521.55 12.7 -1 1 0 505.25 12.2 -1 1 0 503.95 11.9 -1 1 0 503.95 12.7 -1 1 0 514.45 12.6 1 1 0 417.06 12.3 2 -1 0 445.46 10.6 2 -1 0 451.45 11.8 -2 -1 0 470.65 10.5 2 -1 0 487.25 11.2 -2 -1 0 485.75 14.5 2 -1 0 474.35 11.7 -2 1 0 463.45 13.4 -2 1 0 466.05 11.3 2 1 0 448.56 10 -2 1 0 473.25 12.7 -2 1 0 473.85 11.6 -2 1 0 480.55 11.9 -2 1 0 456.25 12 3 -1 0 954.6 19.5 3 -1 0 970.2 19.3 -3 -1 0 944.21 26.1 3 -1 0 947.61 22.3 -3 -1 0 986.3 19.6 -3 1 0 977.5 23.2 -3 1 0 945.91 22.7 -3 1 0 977.8 21.8 -3 1 0 959.4 22.8 -3 1 0 977.3 25.1 -3 1 0 935.01 20.9 -3 1 0 975 22.8 -4 -1 0 651.33 16.5 4 -1 0 632.34 16.6 -4 -1 0 613.84 20.8 -4 1 0 611.84 16.6 -4 1 0 617.14 18.2 -4 1 0 633.64 14.8 -4 1 0 610.64 16.5 -4 1 0 614.64 19.5 -4 1 0 614.84 16.4 -4 1 0 615.24 16.9 5 -1 0 0.5 1 -5 -1 0 2.1 1 -5 -1 0 5.1 2.1 -5 1 0 1.4 1.1 -5 1 0 1.7 0.8 -5 1 0 -0.2 0.9 -5 1 0 0.7 1.1 -5 1 0 2.8 1.3 -5 1 0 0.5 1.4 -5 1 0 2.2 1.4 -6 -1 0 -1.3 1.9 -6 -1 0 0.6 0.8 6 -1 0 -0.2 0.9 -6 -1 0 -1.8 1.6 -6 1 0 1.1 0.9 -6 1 0 0.4 1.5 -6 1 0 -0.1 1.1 -6 1 0 1 1.1 -6 1 0 1 1.2 -6 1 0 0.1 1 -6 1 0 1.5 1.5 -7 -1 0 151.08 9.8 -7 -1 0 148.69 7.9 -7 -1 0 144.89 11.3 7 -1 0 145.89 8 -7 1 0 142.59 7 -7 1 0 136.59 8.2 -7 1 0 142.59 10.4 -7 1 0 146.19 6.2 -7 1 0 141.19 9.9 -7 1 0 152.58 6.6 -7 1 0 164.18 7.5 -8 -1 0 84.79 6.4 -8 -1 0 75.59 7.6 -8 -1 0 74.89 8.9 -8 1 0 86.09 4.8 -8 1 0 84.79 6.9 -8 1 0 99.49 9.2 -8 1 0 85.39 5.3 -8 1 0 76.19 5.9 -8 1 0 79.79 5 -8 1 0 71.69 8 -9 -1 0 3.3 1.9 -9 -1 0 2.8 2.6 -9 -1 0 -0.3 0.8 -9 -1 0 0.2 3.6 -9 1 0 1.4 1.2 -9 1 0 -1 3.6 -9 1 0 -2.9 1.7 -9 1 0 2.9 1.6 -9 1 0 -0.9 2.9 -9 1 0 -0.4 1.7 -10 -1 0 28 7.2 -10 -1 0 20.5 2.3 -10 -1 0 17 5 -10 -1 0 22.8 4.6 -10 1 0 21.7 6.4 -10 1 0 20.2 2.5 -10 1 0 25.4 6.4 -10 1 0 23.8 4.3 -10 1 0 20 2.2 -10 1 0 13.4 3.7 -11 -1 0 45 3.7 -11 -1 0 35.7 5.7 -11 -1 0 44.7 8.4 -11 -1 0 54.29 10.3 -11 1 0 54.69 5.9 -11 1 0 46.7 8.9 -11 1 0 50.49 9.4 -11 1 0 51.59 7.3 -12 -1 0 6.9 4.1 -12 -1 0 14.1 5.3 -12 -1 0 3.7 7.2 -12 -1 0 9.3 2.9 -12 1 0 6.9 4.1 -12 1 0 11.5 5.1 -12 1 0 12.6 6.1 -12 1 0 4.3 5.1 -13 -1 0 5.9 6.3 -13 -1 0 -1.3 5 -13 -1 0 -6.7 3.4 -13 1 0 4.5 6.6 -13 1 0 -0.6 5 -13 1 0 -5.1 8.8 -13 1 0 -0.3 5 0 2 0 3419.66 70.39 -1 -2 0 1720.23 32.8 1 -2 0 1619.64 36.2 -1 -2 0 1631.04 36.5 1 -2 0 1644.04 36 1 -2 0 1682.23 36.9 1 -2 0 1645.14 36.2 -1 2 0 1631.74 37.8 1 2 0 1675.83 32.5 -1 2 0 1615.94 36.9 -1 2 0 1683.13 37.7 -1 2 0 1691.43 36.3 -1 2 0 1708.53 36.4 -1 2 0 1707.83 36.5 -2 -2 0 8.2 2.2 2 -2 0 9 1.7 2 -2 0 6 1.3 2 -2 0 12.3 1.7 -2 -2 0 8.4 1.6 2 2 0 9.5 1.7 -2 2 0 6.5 1.7 -2 2 0 7.3 1.4 -2 2 0 8.3 1.9 -2 2 0 12.9 2.5 -2 2 0 9.4 1.8 -2 2 0 10.6 2.2 -3 -2 0 7.9 2.4 3 -2 0 11.9 1.6 3 -2 0 8.9 1.7 -3 -2 0 10.7 1.6 3 -2 0 10.6 2.1 -3 2 0 8.2 2 3 2 0 7.6 1.3 -3 2 0 11.6 2.5 -3 2 0 7.9 1.7 -3 2 0 7.3 1.9 3 2 0 7 1.4 -3 2 0 11.8 2.8 -3 2 0 10 2 -3 2 0 9.7 1.3 -4 -2 0 75.09 3.6 4 -2 0 79.99 4.9 4 -2 0 74.89 3.5 4 -2 0 76.79 3.8 -4 -2 0 72.29 6.7 4 2 0 68.09 3.3 4 2 0 77.79 2.8 -4 2 0 65.99 4.9 -4 2 0 71.99 4.3 -4 2 0 60.09 4.9 -4 2 0 93.99 8.1 -4 2 0 71.99 6.2 -4 2 0 74.69 5.1 -4 2 0 76.89 4.7 5 -2 0 3.3 1.4 5 -2 0 4.4 0.8 -5 -2 0 0.1 1.6 5 -2 0 4.9 0.9 -5 2 0 4.2 1.5 -5 2 0 2 1.3 -5 2 0 5.2 2 -5 2 0 2.7 1.6 -5 2 0 6.5 2.1 -5 2 0 6.4 1.9 -5 2 0 4 1.9 6 -2 0 129.29 7.2 -6 -2 0 134.19 10.7 -6 -2 0 133.49 7.8 -6 -2 0 134.09 7.1 -6 2 0 126.19 9.5 -6 2 0 116.79 7.2 -6 2 0 116.89 6.4 -6 2 0 122.99 7.5 -6 2 0 125.49 7.7 -6 2 0 126.29 7.5 -6 2 0 132.39 7.9 -7 -2 0 3.6 1.5 7 -2 0 -0.4 1.2 -7 -2 0 -1 1.5 -7 2 0 3.4 2.1 -7 2 0 0.4 1.8 -7 2 0 1.8 1.8 -7 2 0 0.4 1.8 -7 2 0 3 1.8 -7 2 0 2.2 1.7 -7 2 0 1.4 1.9 8 -2 0 59.79 5.9 -8 -2 0 61.79 5.6 -8 -2 0 59.79 6.5 -8 -2 0 39.7 7.7 -8 2 0 55.59 7.6 -8 2 0 51.49 6.3 -8 2 0 52.39 5.3 -8 2 0 68.29 6.6 -8 2 0 57.09 5.3 -8 2 0 56.09 7.8 -9 -2 0 16.7 6.1 -9 -2 0 9.7 3.6 9 -2 0 19.7 4.3 -9 -2 0 19.5 4 -9 2 0 16.5 3.6 -9 2 0 21.1 5.9 -9 2 0 17.9 3.7 -9 2 0 25.2 6 -9 2 0 20.8 3.5 -9 2 0 22.4 4.5 -10 -2 0 32.2 2.4 -10 -2 0 39.4 9.1 -10 -2 0 43 5.8 -10 -2 0 40.6 7 -10 2 0 44.4 5 -10 2 0 44.2 5.7 -10 2 0 41.1 7 -10 2 0 36.1 7.1 -10 2 0 35 4.4 -11 -2 0 1.4 3.5 -11 -2 0 2.9 1.3 -11 -2 0 1.3 2.8 -11 -2 0 3.5 5.8 -11 2 0 -2.2 2.2 -11 2 0 1.7 3.4 -11 2 0 -8.7 3.7 -11 2 0 -2.3 2 -11 2 0 -3.3 4.3 -11 2 0 1.2 3.6 -12 -2 0 4.8 3.7 -12 -2 0 0 7.9 -12 -2 0 5.4 1.9 -12 2 0 -2.7 4.4 -12 2 0 8.3 5.9 -12 2 0 0.2 5.8 -12 2 0 -0.2 4.2 -13 -2 0 0 2.8 -13 -2 0 -4.8 6.2 -13 -2 0 7.4 5.1 -13 2 0 8.5 8 -13 2 0 1.6 6 -13 2 0 4.4 5.8 0 -3 0 -0.4 0.7 0 -3 0 0.8 0.6 0 -3 0 -0.5 0.7 0 -3 0 1 0.9 0 3 0 0.4 0.6 0 3 0 -0.3 1 0 3 0 0.7 0.8 0 3 0 1.5 1.2 -1 -3 0 617.34 14.1 1 -3 0 627.94 18.5 -1 -3 0 625.84 17.2 1 -3 0 608.84 17.7 -1 -3 0 627.94 18.5 -1 -3 0 645.24 18 -1 -3 0 615.04 18.3 1 -3 0 616.74 17.4 1 -3 0 617.14 17.1 1 3 0 633.14 18.4 1 3 0 621.64 18.7 -1 3 0 606.24 19.3 -1 3 0 625.34 17 -1 3 0 574.44 17.5 -1 3 0 605.34 17.5 1 3 0 608.94 13.6 -1 3 0 625.64 19.2 -2 -3 0 8 2 2 -3 0 5 1.8 2 -3 0 9 1.8 -2 -3 0 9.2 2.6 2 -3 0 5.1 1.7 -2 3 0 5.1 2.2 -2 3 0 10.3 2.6 -2 3 0 4.3 1.9 2 3 0 10.3 2.3 -2 3 0 8.6 1.9 -2 3 0 9 2.1 -2 3 0 4.4 1.4 -3 -3 0 25.4 1.6 -3 -3 0 18.8 3.9 3 -3 0 26.3 3.2 3 -3 0 27 3 -3 -3 0 20.2 2.8 3 -3 0 23.6 2.9 3 3 0 25.7 3 -3 3 0 20.8 3.1 -3 3 0 22.6 4.1 -3 3 0 27.6 3.8 3 3 0 28 2.8 -3 3 0 26.1 3.1 -3 3 0 20.3 3.6 -3 3 0 25.5 3.6 4 -3 0 4.2 1.4 4 -3 0 1.8 1.3 4 -3 0 3 1.5 -4 -3 0 5.1 1.6 -4 -3 0 1.8 1.9 4 3 0 2.8 1.4 -4 3 0 3.7 1.6 -4 3 0 3.9 1.7 -4 3 0 4.5 2 -4 3 0 4 1.7 -4 3 0 5.2 2 -4 3 0 3.8 1.8 5 -3 0 204.18 7.5 5 -3 0 192.18 7.9 5 -3 0 209.08 9.6 -5 -3 0 191.88 12.7 -5 3 0 194.58 10.3 5 3 0 205.08 7.4 -5 3 0 205.68 10.2 -5 3 0 209.88 10.9 -5 3 0 188.88 10.5 5 3 0 215.58 6.5 -5 3 0 203.58 9.8 -5 3 0 192.18 11.5 -6 -3 0 191.88 13.7 6 -3 0 204.48 6.8 6 -3 0 194.58 6.4 -6 -3 0 211.88 9.4 6 -3 0 198.58 9.8 -6 3 0 209.08 11.2 -6 3 0 199.18 12.5 -6 3 0 198.58 10.6 -6 3 0 214.98 10.3 -6 3 0 205.68 10.9 -6 3 0 186.58 10.8 7 -3 0 135.49 8.4 -7 -3 0 160.78 13.3 -7 -3 0 137.59 8.6 -7 3 0 148.19 9.8 -7 3 0 139.79 11.1 -7 3 0 155.88 9.1 -7 3 0 138.19 9.4 -7 3 0 147.89 9.5 -7 3 0 144.79 9.5 -8 -3 0 8 1.8 -8 -3 0 11.2 4.6 -8 -3 0 6.5 2.5 -8 -3 0 8.7 3.3 8 -3 0 8.9 3 -8 3 0 11.2 3.5 -8 3 0 3 2.5 -8 3 0 2.9 3 -8 3 0 6.3 3.3 -8 3 0 4.4 3.1 9 -3 0 48.1 5.9 -9 -3 0 60.19 5.9 -9 -3 0 49.6 6.4 -9 -3 0 43.4 8.6 -9 -3 0 48.1 3.5 -9 3 0 36.7 6.7 -9 3 0 38.7 6.4 -9 3 0 47.5 6.2 -9 3 0 41.1 6.1 -9 3 0 45.9 5.7 10 -3 0 37 6 -10 -3 0 44.8 10.2 -10 -3 0 59.59 6.7 -10 -3 0 49.3 7.5 -10 -3 0 62.69 3.7 -10 3 0 57.99 7.7 -10 3 0 46.7 6.9 -10 3 0 61.69 6.8 -10 3 0 56.79 10.6 -10 3 0 53.79 6.4 11 -3 0 10.1 3.5 -11 -3 0 2.5 7.2 -11 -3 0 4 3.9 -11 -3 0 5.9 2.9 -11 -3 0 6.4 1.8 -11 3 0 5.1 3.9 -11 3 0 10.9 4.4 -11 3 0 12 3.5 -11 3 0 12 5.5 -11 3 0 2.7 3.4 -12 -3 0 1.9 2 -12 -3 0 8.9 4.1 -12 -3 0 9.2 5.3 -12 3 0 4.4 3.2 -12 3 0 26.5 6 -12 3 0 9.7 6.6 -12 3 0 6.3 3.7 -12 3 0 1.8 4.7 0 -4 0 9.7 2.4 0 -4 0 7.2 2.2 0 -4 0 9.3 2.1 0 -4 0 9 2.6 0 -4 0 12.1 2.1 0 4 0 8.7 2.1 0 4 0 7.5 2.7 0 4 0 7.7 1.6 0 4 0 8.8 2.5 -1 -4 0 114.59 7.2 1 -4 0 104.19 6.9 -1 -4 0 108.79 6.6 -1 -4 0 115.99 7.3 -1 -4 0 115.49 4.8 1 -4 0 117.69 7.5 1 -4 0 112.29 5.3 1 -4 0 109.19 6.6 -1 4 0 108.69 6.1 1 4 0 117.59 4.4 -1 4 0 111.49 7.9 1 4 0 95.19 7.2 1 4 0 114.79 7.5 -1 4 0 118.69 7.1 -1 4 0 107.29 7.8 -2 -4 0 217.88 10.2 -2 -4 0 220.58 6.2 -2 -4 0 246.48 12 2 -4 0 219.98 10.7 2 -4 0 201.68 9.8 2 -4 0 271.17 12.4 -2 4 0 230.08 12 2 4 0 221.88 10.8 -2 4 0 212.48 11.4 -2 4 0 210.28 9.9 -2 4 0 206.78 11.9 2 4 0 190.98 9.8 3 -4 0 160.98 8.6 3 -4 0 167.48 8.7 -3 -4 0 179.28 8.8 -3 -4 0 178.38 11 3 -4 0 170.88 10.8 3 4 0 170.68 9.1 -3 4 0 170.58 9.2 -3 4 0 167.08 9.3 3 4 0 154.08 8.5 -3 4 0 175.98 10.5 -3 4 0 169.68 10 -3 4 0 177.78 9.8 -3 4 0 172.68 10.6 -4 -4 0 188.48 5.6 4 -4 0 190.58 10.2 4 -4 0 188.88 9.6 -4 -4 0 200.18 12.6 4 -4 0 184.08 9 -4 -4 0 200.78 9.1 4 4 0 188.88 8.7 -4 4 0 204.78 11.8 -4 4 0 191.08 11.1 4 4 0 200.58 9.5 -4 4 0 182.78 10.1 -4 4 0 201.88 10.5 -4 4 0 200.58 11.5 -4 4 0 191.58 11 5 -4 0 0.9 1.5 5 -4 0 -1.1 1.5 -5 -4 0 1.3 1.5 -5 -4 0 0.5 2.2 5 -4 0 2 1.5 5 4 0 -1.5 1.5 -5 4 0 0.1 1.8 5 4 0 1.7 1.2 -5 4 0 0 2.1 -5 4 0 4.8 2.2 -5 4 0 0.3 2.1 -5 4 0 1.5 1.5 -5 4 0 -0.4 1.8 -6 -4 0 -2.1 2.7 -6 -4 0 -1.5 1.6 6 -4 0 3.5 1.5 6 -4 0 3.8 1.6 6 -4 0 -0.1 1.5 -6 -4 0 0.9 1.4 6 4 0 5.3 1.7 -6 4 0 2.2 2 -6 4 0 3 2.2 -6 4 0 1.4 2.4 -6 4 0 3.7 2.8 -6 4 0 0.7 2.2 6 4 0 2.9 1.1 -7 -4 0 23.4 3.3 7 -4 0 13.3 2.1 -7 -4 0 15.5 5.4 7 -4 0 19.7 2.6 -7 -4 0 21.8 3.7 7 -4 0 16.6 3.7 -7 4 0 13 3.9 -7 4 0 7.3 3.1 -7 4 0 17 4.8 -7 4 0 13.7 3.9 -8 -4 0 81.29 5.7 -8 -4 0 80.19 10.7 8 -4 0 83.39 7.3 -8 -4 0 75.19 6.4 -8 4 0 73.99 9.6 -8 4 0 69.49 8 -8 4 0 87.29 8.5 -8 4 0 68.29 7.7 -8 4 0 83.89 7.9 -9 -4 0 74.19 5.4 -9 -4 0 76.99 7.2 9 -4 0 77.59 7.5 -9 -4 0 81.59 12.7 -9 -4 0 77.69 7.2 -9 4 0 74.09 8.2 -9 4 0 87.49 10.8 -9 4 0 81.99 8.5 -9 4 0 74.59 8.5 -9 4 0 83.89 10.1 -10 -4 0 4.8 2.7 -10 -4 0 4.7 6.1 -10 -4 0 -0.9 2 -10 -4 0 7.5 3.2 -10 4 0 3.2 3.2 -10 4 0 13 4.5 -10 4 0 -0.6 3.5 -10 4 0 -2.3 3.7 -11 -4 0 2 3.8 -11 -4 0 5.3 5.1 -11 -4 0 11.2 2.6 -11 -4 0 -0.7 7.3 11 -4 0 3.2 3.9 -11 4 0 2.4 4 -11 4 0 4.5 6.5 -11 4 0 -2.9 4.8 -11 4 0 3.6 4.3 -11 4 0 10.9 5.8 -12 -4 0 0.5 4.8 -12 -4 0 -5.3 2.3 12 -4 0 -3.1 4.2 -12 -4 0 -4.1 3.7 -12 4 0 0.7 6.4 -12 4 0 -8.2 4.9 -12 4 0 -1.8 4.4 -12 4 0 -6.5 4 -12 4 0 6.4 6.1 0 -5 0 1.3 1.2 0 -5 0 0.6 1 0 -5 0 -1.4 1.6 0 -5 0 1.8 1.7 0 5 0 -3.1 1.7 0 5 0 2.2 1.8 0 5 0 0.2 1 -1 -5 0 32.5 4.6 1 -5 0 24.7 4.4 -1 -5 0 28.5 4.1 1 -5 0 28.1 3.1 1 -5 0 20.9 3.9 1 -5 0 25.9 4.3 -1 -5 0 26.4 3.7 -1 -5 0 25.4 4.6 -1 -5 0 24.6 2.6 -1 5 0 26.1 5 1 5 0 25 4.8 -1 5 0 19.1 3.3 1 5 0 21.5 2.2 1 5 0 16.3 3.7 -1 5 0 23.7 5.1 -1 5 0 27.6 4.5 2 -5 0 490.35 18.7 2 -5 0 488.75 17.8 -2 -5 0 471.15 17.9 -2 -5 0 473.95 12 2 -5 0 468.65 17.2 -2 -5 0 478.45 19 -2 -5 0 459.85 16.9 -2 5 0 460.95 19.8 2 5 0 453.05 18.3 2 5 0 468.45 18.1 2 5 0 477.05 11.1 -2 5 0 437.86 17.2 3 -5 0 20.9 4.2 3 -5 0 17.6 3.9 -3 -5 0 13.1 3.8 3 -5 0 12.6 2.6 -3 -5 0 16.3 3.5 -3 5 0 17.2 3.9 -3 5 0 15.6 4.5 -3 5 0 16.3 3.9 3 5 0 17.6 3.8 -3 5 0 13.7 3.4 -3 5 0 21.4 5.2 4 -5 0 53.49 5.7 4 -5 0 58.79 5.6 4 -5 0 55.99 5.6 -4 -5 0 49.6 7.1 -4 5 0 48.4 5.8 4 5 0 56.29 5.9 -4 5 0 56.69 6.8 -4 5 0 49.99 6.5 -4 5 0 59.59 6.4 -4 5 0 50.99 5.8 4 5 0 51.69 5.4 5 -5 0 14.8 3.1 -5 -5 0 17.8 5.6 5 -5 0 19.6 3.8 5 -5 0 22.2 3.9 -5 -5 0 22 4.6 -5 5 0 18.6 4.8 -5 5 0 26.9 5 -5 5 0 10.8 2.9 -5 5 0 30.2 6.2 -5 5 0 26.1 5.5 5 5 0 21.5 4 -6 -5 0 75.89 3.8 6 -5 0 76.99 7 6 -5 0 81.59 6.1 -6 -5 0 86.69 6.9 -6 -5 0 92.19 10.6 -6 -5 0 80.99 4.6 6 -5 0 69.59 6.2 -6 5 0 91.59 8.3 -6 5 0 85.19 8.9 6 5 0 77.89 5.2 6 5 0 81.79 6.2 -6 5 0 87.79 8.8 -6 5 0 80.89 7.7 -6 5 0 87.89 8.9 7 -5 0 134.49 7.1 -7 -5 0 125.59 6.6 -7 -5 0 131.19 8.4 7 -5 0 125.39 10.8 -7 -5 0 114.19 12.9 7 -5 0 121.49 9 7 5 0 123.19 6.7 -7 5 0 131.29 11.1 -7 5 0 118.99 10.1 -7 5 0 126.99 10.2 -7 5 0 120.29 11.3 7 5 0 117.49 5.6 -7 5 0 123.59 10.7 -8 -5 0 30.7 4.1 8 -5 0 31 3.2 8 -5 0 28.3 5.5 -8 -5 0 19.8 4 8 -5 0 36.3 3.4 -8 5 0 31.1 7 -8 5 0 22.1 5.4 -8 5 0 26.3 5.9 -8 5 0 34 6.4 -8 5 0 31.4 6.7 -9 -5 0 5.9 3.4 -9 -5 0 9.2 5.7 -9 -5 0 10.4 3 -9 5 0 -1.5 4 -9 5 0 1.8 4.1 -9 5 0 1 3.6 -9 5 0 4.4 3.9 -10 -5 0 -2.7 6.6 -10 -5 0 -3.6 3 -10 -5 0 3.6 2.9 10 -5 0 -0.6 3.7 -10 5 0 0 3.8 -10 5 0 2.9 4.4 -10 5 0 -9.9 4.5 -10 5 0 0.3 4.7 -10 5 0 5.2 4.4 -11 -5 0 20.3 5.2 -11 -5 0 22.1 4.8 -11 -5 0 32.9 5.7 11 -5 0 25.8 5.8 -11 5 0 31.4 7.6 -11 5 0 26.6 6.6 -11 5 0 28.2 6.8 -11 5 0 33.8 12.4 -11 5 0 19.3 8.5 -12 -5 0 33.1 5 -12 -5 0 25.1 7 -12 -5 0 21.6 6.6 -12 5 0 19.2 10.2 -12 5 0 24.9 8.7 -12 5 0 38.9 7.9 -12 5 0 24.3 7.1 -12 5 0 41 9.2 0 -6 0 143.19 9.9 0 -6 0 140.29 9.2 0 -6 0 149.49 9 0 -6 0 144.49 10.2 0 6 0 134.49 10.6 0 6 0 146.69 7.3 0 6 0 140.59 10.7 1 -6 0 144.99 9.4 1 -6 0 138.49 7.6 -1 -6 0 127.49 9.1 -1 -6 0 147.69 9.4 1 -6 0 136.99 9.7 -1 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3.9 -1 8 0 6.5 2.6 -1 8 0 5.2 4.4 1 8 0 4.2 3.9 1 8 0 8.4 4.3 1 8 0 9.4 2 -1 8 0 12.5 4.9 2 -8 0 142.79 11.4 -2 -8 0 145.29 11.9 2 -8 0 133.69 10.7 2 -8 0 134.59 12.1 -2 -8 0 127.79 10.7 -2 -8 0 137.49 12 2 -8 0 140.79 7.4 -2 -8 0 144.79 11.8 2 8 0 134.89 5.5 2 8 0 144.49 12.1 -2 8 0 138.69 12.8 -2 8 0 150.18 11.6 -2 8 0 132.99 13.2 -2 8 0 149.88 10 2 8 0 131.79 12.5 3 -8 0 31.2 6.7 3 -8 0 22 6 3 -8 0 22 5.5 -3 -8 0 24.9 5.7 -3 -8 0 26.8 6.2 -3 -8 0 26.8 6.1 -3 -8 0 26.2 5.4 3 8 0 22.9 6.9 3 8 0 24.6 5.9 -3 8 0 26.4 7.4 -3 8 0 18.6 4.5 -3 8 0 25.2 6.7 -3 8 0 14 4.9 -4 -8 0 -0.2 3.7 -4 -8 0 -0.6 3.5 4 -8 0 -1.4 3.6 4 -8 0 -0.8 3.6 -4 -8 0 -1 4.5 -4 -8 0 -4.2 2.8 4 8 0 2.4 3.6 -4 8 0 6.6 4.9 -4 8 0 1.3 2.7 -4 8 0 -2.7 2.5 -4 8 0 -3.5 4.1 -5 -8 0 -4.1 3.3 -5 -8 0 4.9 4 -5 -8 0 1 3.3 -5 -8 0 5.2 4.6 5 -8 0 3.6 3.8 5 -8 0 3 3.7 -5 8 0 0.9 3.2 -5 8 0 -1.2 4.3 -5 8 0 -0.9 5 5 8 0 -2.6 3.6 6 -8 0 5.7 4.4 -6 -8 0 7.3 4.3 -6 -8 0 1.7 4.1 6 -8 0 2.4 3.6 -6 -8 0 -1.3 3.4 6 -8 0 3.3 3.4 -6 8 0 7.6 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349.67 14.4 7 -5 -4 334.27 12.4 -7 -5 4 339.07 14.1 -7 5 4 332.27 19.2 7 5 -4 292.97 11.1 -7 5 4 333.97 17.5 -7 5 4 344.87 17.3 -7 5 4 325.67 18.3 7 5 -4 355.66 14.3 -7 5 4 353.66 17.5 6 -5 -4 0.2 2 -6 -5 4 6.5 2.6 -6 -5 4 1 1.3 -6 -5 4 2 2.8 -6 -5 4 5.9 2.4 6 -5 -4 1.7 1.9 6 -5 -4 4.4 2.8 6 5 -4 -1.6 1.5 -6 5 4 -0.4 2.4 -6 5 4 2.5 2.6 -6 5 4 3.4 3.4 -6 5 4 -2.5 1.9 5 -5 -4 8.6 2.5 -5 -5 4 10 2 -5 -5 4 3.9 2.6 -5 -5 4 5 2.2 5 -5 -4 5.9 2.8 -5 5 4 3.6 2.8 -5 5 4 6.7 2.6 -5 5 4 12 3.8 -5 5 4 3.7 3.1 -5 5 4 8.1 3.3 5 5 -4 10.5 2.7 4 -5 -4 -0.5 1.3 -4 -5 4 2 2 4 -5 -4 0.2 1.8 4 -5 -4 1.1 2.3 -4 -5 4 0.1 0.8 4 -5 -4 -1.5 2.3 -4 -5 4 4.3 1.8 -4 5 4 1.8 2.1 -4 5 4 0.2 1.5 -4 5 4 4.6 2.6 -4 5 4 4.1 2.6 3 -5 -4 6.4 2.8 3 -5 -4 19.8 3.8 3 -5 -4 12.1 3 -3 -5 4 5.2 2.9 -3 -5 4 7.3 1.7 -3 -5 4 11.4 3 3 -5 -4 9.9 3.8 -3 5 4 10.3 2.9 -3 5 4 7.6 2.2 3 5 -4 14.2 3.2 -3 5 4 12.6 4 -3 5 4 6.7 2.9 -2 -5 4 338.27 16.1 2 -5 -4 362.16 16.4 -2 -5 4 391.56 15.7 -2 -5 4 349.87 11.6 2 -5 -4 343.37 14.1 2 -5 -4 380.46 17.9 2 -5 -4 348.17 14.5 -2 5 4 339.57 14.6 -2 5 4 358.56 15.5 2 5 -4 361.76 10.9 2 5 -4 360.56 15.1 -2 5 4 358.16 17 -1 -5 4 46 5.2 -1 -5 4 40.7 5.5 1 -5 -4 31.6 4 1 -5 -4 40.3 5.7 -1 -5 4 39.4 3.6 1 -5 -4 43.1 4.8 -1 -5 4 30.2 4.1 1 5 -4 36.1 3.1 1 5 -4 39 4.9 -1 5 4 37.8 4 1 5 -4 33.4 4.8 -1 5 4 40.2 5.5 -1 5 4 34.4 4.2 -1 5 4 42.2 5 0 -5 4 101.39 6.4 0 -5 -4 94.69 6.3 0 -5 4 90.29 7.3 0 -5 -4 98.19 6.7 0 -5 -4 98.69 7.3 0 -5 -4 98.59 8.4 0 -5 4 89.89 7 0 -5 4 91.79 8 0 5 -4 99.19 8 0 5 4 99.49 8.1 0 5 4 93.59 6.8 0 5 4 104.19 7.3 0 5 4 105.29 5.7 0 5 -4 109.59 6.1 0 5 4 91.19 8 0 5 -4 87.19 7.4 1 -5 4 152.78 9.5 -1 -5 -4 170.48 10.9 1 -5 4 142.09 8.8 1 -5 4 148.19 8.6 -1 -5 -4 155.08 9.1 1 -5 4 169.48 9.9 -1 -5 -4 149.29 8.4 -1 -5 -4 158.58 9.1 1 -5 4 136.69 9.9 -1 5 -4 143.89 8.3 1 5 4 158.78 10.1 -1 5 -4 147.59 9.9 1 5 4 148.79 5.8 -1 5 -4 154.18 10.1 1 5 4 149.39 10 2 -5 4 175.78 10 2 -5 4 170.68 9.6 2 -5 4 160.68 9.6 -2 -5 -4 177.48 9.1 -2 -5 -4 149.69 8.9 -2 -5 -4 145.69 9.8 2 -5 4 168.78 10 2 -5 4 162.28 11.2 -2 5 -4 160.28 9.1 2 5 4 147.49 9.8 -2 5 -4 169.98 9.9 2 5 4 153.68 9.7 -2 5 -4 161.38 10.7 -2 5 -4 157.18 10.5 3 -5 4 32.9 4.3 3 -5 4 25.2 4.8 -3 -5 -4 19.3 4.1 3 -5 4 32.3 5.2 -3 -5 -4 29.1 4.6 -3 -5 -4 33.3 4.2 3 -5 4 29.3 4.9 3 -5 4 32.8 6.6 -3 5 -4 22 3.8 -3 5 -4 42.4 5.8 3 5 4 28.9 4.4 -3 5 -4 34.1 4.6 -3 5 -4 34.2 6.1 4 -5 4 5.7 2.3 -4 -5 -4 0 2.4 4 -5 4 1.4 2.5 -4 -5 -4 3 2 4 -5 4 3.3 2.6 -4 -5 -4 5.5 2.2 4 -5 4 7.1 2.3 -4 5 -4 8.7 3.3 -4 5 -4 2 2.7 -4 5 -4 6.4 3.3 4 5 4 5.8 2.2 4 5 4 4.5 2.2 -4 5 -4 8.9 3 -4 5 -4 6.2 3.2 5 -5 4 -0.6 1.7 -5 -5 -4 -3.6 1.8 5 -5 4 1 1.9 -5 -5 -4 2.9 3.2 5 -5 4 0.3 1.4 5 -5 4 -2.5 1.9 -5 5 -4 1.9 2.8 -5 5 -4 4.4 2.7 5 5 4 3.9 2.1 -5 5 -4 -2.2 2.2 5 5 4 0.5 1.8 -5 5 -4 -1.5 1.5 -6 -5 -4 33.3 4.7 6 -5 4 32.8 6.2 6 -5 4 35.2 4.3 6 -5 4 43.1 4.1 6 -5 4 32.1 4.5 -6 -5 -4 34.7 7.5 -6 5 -4 34.3 6.2 -6 5 -4 27.7 4.8 6 5 4 37.2 4.1 -6 5 -4 19.2 4.5 -6 5 -4 35.3 6.3 -6 5 -4 38 7 6 5 4 43.2 4.4 -7 -5 -4 2.7 4 7 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6 4 5.7 5.1 -11 6 4 6.7 7 -11 6 4 5.1 5.8 -10 -6 4 8 3.8 10 -6 -4 7.1 5.3 -10 -6 4 4.1 2.5 -10 -6 4 1.1 3.4 -10 6 4 12.8 6.5 -10 6 4 4.6 6.1 -10 6 4 7.8 6.1 -10 6 4 7.4 5.2 -10 6 4 -2.1 5 -9 -6 4 5.5 2.5 9 -6 -4 4.4 2.6 -9 -6 4 8.4 3.7 9 -6 -4 5.4 5.6 -9 -6 4 6.1 3.3 -9 6 4 8.1 4.8 9 6 -4 4.4 2.2 -9 6 4 6.6 5.3 -9 6 4 6.7 4.7 -9 6 4 7.2 5.8 -8 -6 4 4.8 1.9 -8 -6 4 2.3 3.3 8 -6 -4 -3.2 2.7 8 -6 -4 6.4 2.6 -8 6 4 3.6 4.4 -8 6 4 1.9 3.4 -8 6 4 -5.4 4 8 6 -4 0.2 2.1 8 6 -4 4.4 3.8 -8 6 4 2.9 4.3 -8 6 4 -0.3 3.8 7 -6 -4 58.39 6.8 7 -6 -4 39.1 6.7 -7 -6 4 39.7 3.8 -7 -6 4 42.4 6.2 7 -6 -4 38.2 5.3 -7 -6 4 44.6 6.4 -7 6 4 44.8 8.5 -7 6 4 60.49 8.8 -7 6 4 41.5 8.5 -7 6 4 53.89 7.4 -7 6 4 23.5 5.8 7 6 -4 42.4 6.6 7 6 -4 39.8 4.8 -6 -6 4 13.9 4.3 -6 -6 4 16.8 6.4 6 -6 -4 13.6 3.9 -6 -6 4 16.8 4.4 -6 -6 4 13.5 2.4 6 -6 -4 15.4 4.6 6 -6 -4 11.1 3.6 -6 6 4 1.8 3.9 -6 6 4 15.8 4.5 -6 6 4 14.3 4.8 -6 6 4 14.8 5.2 -6 6 4 18.6 5.2 6 6 -4 11.2 4.1 6 6 -4 15.7 4.7 -5 -6 4 37.9 5.5 -5 -6 4 31.3 3 5 -6 -4 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5.1 4 -4 7 19.6 3.2 4 -4 7 15.7 4.1 4 -4 7 12 2.9 -4 -4 -7 14.7 2.7 -4 -4 -7 14.8 2.9 -4 -4 -7 9.6 3.8 4 -4 7 16.5 2.9 4 -4 7 14.4 3.4 -4 -4 -7 20.7 3.9 -4 4 -7 10.9 3.2 4 4 7 20.4 3.1 4 4 7 10.6 3.4 -4 4 -7 18.1 4.1 -4 4 -7 14.7 3.5 -4 4 -7 15.6 3.4 -5 -4 -7 9.4 2.9 5 -4 7 6.3 2.4 5 -4 7 6.8 3.5 -5 -4 -7 15.3 3 -5 -4 -7 11.8 1.6 5 -4 7 15.2 4.4 5 -4 7 12.8 3.1 -5 -4 -7 14.5 4.6 5 -4 7 18.3 3.5 5 -4 7 8.2 3.6 -5 4 -7 14.9 3.8 -5 4 -7 14.2 3.8 5 4 7 18.7 2.9 -5 4 -7 9.2 2.6 5 4 7 10.3 2.7 5 4 7 16 5.2 -5 4 -7 17.9 4.3 -6 -4 -7 183.18 14 6 -4 7 192.88 12.3 6 -4 7 173.98 9.8 6 -4 7 185.68 13.4 -6 -4 -7 194.88 7 -6 -4 -7 187.08 8.6 6 -4 7 190.38 7.7 6 -4 7 194.08 10.6 6 -4 7 197.88 8.7 6 4 7 197.08 8.5 -6 4 -7 186.88 11.6 -6 4 -7 190.68 12.8 6 4 7 198.18 7.2 -6 4 -7 179.08 11.2 -6 4 -7 202.08 11.3 6 4 7 184.58 14.5 -7 -4 -7 42.8 3.7 7 -4 7 37.9 4.9 7 -4 7 40.7 2.7 -7 -4 -7 39.8 4.5 7 -4 7 36.6 2.9 -7 -4 -7 36.7 7.8 7 4 7 33 7.5 -7 4 -7 40.3 6.7 -7 4 -7 40.3 5.6 -7 4 -7 36.3 7 -7 4 -7 38.7 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13.7 5 -4 -8 344.37 14.7 5 -4 -8 396.26 19.1 5 -4 -8 410.26 17.2 5 4 -8 358.16 13.3 -5 4 8 364.96 16.8 -5 4 8 368.06 16.2 -5 4 8 372.36 16.1 -4 -4 8 132.59 8.2 4 -4 -8 128.19 7.7 4 -4 -8 149.69 8.5 -4 -4 8 143.99 9.2 -4 -4 8 146.69 7.3 4 -4 -8 137.99 10.6 -4 4 8 131.59 8.7 -4 4 8 142.29 9.9 -4 4 8 138.39 9 4 4 -8 136.89 8 -3 -4 8 229.98 9.5 3 -4 -8 233.68 10.6 3 -4 -8 251.17 14.1 -3 -4 8 252.67 11.4 -3 -4 8 250.27 12.3 3 -4 -8 238.98 10.7 3 4 -8 245.78 10.8 -3 4 8 241.28 12.8 3 4 -8 237.18 11.1 -3 4 8 238.28 11.9 -3 4 8 231.08 11.3 2 -4 -8 183.58 8.8 -2 -4 8 197.98 9.9 -2 -4 8 176.68 8.3 -2 -4 8 189.88 10.7 2 -4 -8 172.58 11.2 2 -4 -8 179.88 9.2 -2 4 8 174.68 9.1 2 4 -8 173.08 9.7 -2 4 8 185.88 10 2 4 -8 187.38 9.5 2 4 -8 179.08 8 -2 4 8 171.18 10.4 1 -4 -8 60.69 6.4 -1 -4 8 63.09 6.3 1 -4 -8 63.49 5.4 -1 -4 8 54.69 4.6 1 -4 -8 61.99 4.7 -1 -4 8 67.19 5.5 1 4 -8 57.59 4.4 1 4 -8 58.69 5.6 1 4 -8 59.49 5.3 -1 4 8 61.39 4.8 -1 4 8 57.89 6 -1 4 8 66.69 5.8 0 -4 8 1167.98 30.8 0 -4 -8 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1.7 7.8 1 -1 32 5.8 5.7 1 -1 32 2.9 3 -1 1 -32 -10.1 6.5 1 1 32 -0.8 6 1 1 32 3.3 2.7 2 -1 32 -6.6 5.3 2 1 32 -5.9 5.7 -2 1 -32 -4.2 7.3 3 -1 32 16.7 6.9 3 1 32 14.5 7.1 -3 1 -32 5.8 12.4 3 -2 -32 18.1 9.1 -3 -2 32 6.8 9.1 -3 -2 32 5.3 4 -3 -2 32 0.6 6.1 -3 2 32 1.2 4.3 3 2 -32 -5.9 7.8 -3 2 32 -4.6 6.3 -3 2 32 -9.8 8.4 -2 -2 32 2.8 3.8 2 -2 -32 9.2 9.3 2 2 -32 0.6 7.9 -2 2 32 1.9 4 -2 2 32 5.4 7.2 -2 2 32 0.4 6.9 1 -2 -32 -4.6 8.8 -1 -2 32 1.6 8.4 -1 -2 32 -3.1 5.4 -1 2 32 8.4 4.1 -1 2 32 11.8 7.4 -1 2 32 -6.8 6.2 1 2 -32 5.5 7.5 0 -2 32 -10 5.4 0 -2 -32 5 7.7 0 -2 32 -4.4 3.2 0 -2 32 13 8.7 0 2 32 3.2 3.3 0 2 -32 -2.1 7.5 0 2 32 -7.4 5.8 -1 -2 -32 16.7 8.5 1 -2 32 -7 4.9 1 -2 32 -2.9 3.1 1 -2 32 -9.7 5.5 -1 2 -32 6.1 7.5 1 2 32 5.7 6 -2 -2 -32 24.8 9.3 2 -2 32 27 7.5 2 -2 32 34.3 4.9 2 -2 32 34.2 5.9 2 2 32 46.7 8.7 -2 2 -32 39.8 10.1 2 -3 -32 -7.3 9.5 -2 -3 32 21.8 17.9 -2 -3 32 4.6 6.9 -2 -3 32 21.9 5.9 -2 3 32 15.9 8.8 -2 3 32 15.3 12.9 2 3 -32 17.3 8.8 -2 3 32 18.4 5.8 -1 -3 32 5.3 9.8 -1 -3 32 6.6 4.2 1 -3 -32 25.6 10.4 1 3 -32 5.2 7.5 -1 3 32 9.3 4.6 -1 3 32 5.5 7.3 0 -3 -32 13.7 8.4 0 -3 32 8.7 6.4 0 -3 32 17.2 5.7 0 -3 32 19.9 9.2 0 3 -32 6 8.2 0 3 32 19.4 4.6 0 3 32 27.5 8.1 -1 -3 -32 70.79 13 1 -3 32 51.59 7.3 1 -3 32 51.29 9.4 1 -3 32 40.1 8.1 -1 3 -32 36.8 10.4 1 3 32 30.3 8.6 -1 0 33 -5.9 3.4 -1 0 33 -0.1 7.9 -1 0 33 4.1 7 1 0 -33 -3.4 7.4 0 0 33 5.2 3.6 0 0 -33 -10.2 8.4 0 0 33 7 6.4 -1 0 -33 4.2 8.4 1 0 33 3.8 3.1 1 0 33 -0.8 6.2 -1 -1 33 4.4 3.7 -1 -1 33 -6.3 8.6 1 -1 -33 -19.8 8.3 -1 1 33 6.8 12.9 -1 1 33 0.7 7.4 -1 1 33 4 3.9 1 1 -33 -2.1 8.5 0 -1 -33 9.7 9.7 0 -1 33 -7 3.2 0 -1 33 -7.4 5.8 0 1 33 -0.2 3.6 0 1 33 3.8 6.4 0 1 -33 8 8.6 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O5 S1 O4 117.90(8) . . ? C8 S1 O4 109.57(8) . . ? C8 S1 O5 107.99(8) . . ? C17 S1 O4 108.39(8) . . ? C17 S1 O5 107.50(8) . . ? C17 S1 C8 104.69(8) . . ? C10 O1 C3 117.94(18) . . ? C9 O2 C5 121.85(13) . . ? C21 N1 C20 113.97(15) . . ? C22 N1 C20 123.0(4) . . ? C22 N1 C21 122.2(4) . . ? C22A N1 C20 131.4(8) . . ? C22A N1 C21 113.7(8) . . ? C22A N1 C22 8.5(11) . . ? C2 C1 H1 119.18(12) . . ? C6 C1 H1 119.18(11) . . ? C6 C1 C2 121.65(19) . . ? H2 C2 C1 120.22(12) . . ? C3 C2 C1 119.57(18) . . ? C3 C2 H2 120.22(11) . . ? C2 C3 O1 124.31(18) . . ? C4 C3 O1 115.10(18) . . ? C4 C3 C2 120.59(18) . . ? H4 C4 C3 120.69(11) . . ? C5 C4 C3 118.63(18) . . ? C5 C4 H4 120.69(11) . . ? C4 C5 O2 116.03(16) . . ? C6 C5 O2 121.16(15) . . ? C6 C5 C4 122.80(17) . . ? C5 C6 C1 116.76(16) . . ? C7 C6 C1 123.81(17) . . ? C7 C6 C5 119.39(16) . . ? C8 C7 C6 117.90(15) . . ? C11 C7 C6 116.89(15) . . ? C11 C7 C8 125.13(16) . . ? C7 C8 S1 124.81(13) . . ? C9 C8 S1 113.48(12) . . ? C9 C8 C7 121.64(16) . . ? O3 C9 O2 116.68(15) . . ? C8 C9 O2 117.03(15) . . ? C8 C9 O3 126.29(16) . . ? H10a C10 O1 109.5 . . ? H10b C10 O1 109.5 . . ? H10b C10 H10a 109.5 . . ? H10c C10 O1 109.5 . . ? H10c C10 H10a 109.5 . . ? H10c C10 H10b 109.5 . . ? C12 C11 C7 118.00(15) . . ? C16 C11 C7 122.07(16) . . ? C16 C11 C12 119.87(16) . . ? H12 C12 C11 120.07(10) . . ? C13 C12 C11 119.87(17) . . ? C13 C12 H12 120.07(11) . . ? H13 C13 C12 119.98(11) . . ? C14 C13 C12 120.03(19) . . ? C14 C13 H13 119.98(12) . . ? H14 C14 C13 119.99(12) . . ? C15 C14 C13 120.01(19) . . ? C15 C14 H14 119.99(12) . . ? H15 C15 C14 119.66(12) . . ? C16 C15 C14 120.7(2) . . ? C16 C15 H15 119.66(13) . . ? C15 C16 C11 119.47(19) . . ? H16 C16 C11 120.26(11) . . ? H16 C16 C15 120.26(13) . . ? H17a C17 S1 108.85(6) . . ? H17b C17 S1 108.85(6) . . ? H17b C17 H17a 107.7 . . ? C18 C17 S1 113.58(12) . . ? C18 C17 H17a 108.85(9) . . ? C18 C17 H17b 108.85(10) . . ? H18 C18 C17 108.54(9) . . ? C19 C18 C17 113.12(14) . . ? C19 C18 H18 108.54(10) . . ? C21 C18 C17 115.64(15) . . ? C21 C18 H18 108.54(10) . . ? C21 C18 C19 102.13(14) . . ? F2 C19 F1 105.33(13) . . ? C18 C19 F1 114.20(14) . . ? C18 C19 F2 112.09(15) . . ? C20 C19 F1 111.96(15) . . ? C20 C19 F2 106.53(14) . . ? C20 C19 C18 106.57(14) . . ? N1 C20 O6 129.75(18) . . ? C19 C20 O6 124.60(18) . . ? C19 C20 N1 105.62(16) . . ? C18 C21 N1 104.21(15) . . ? H21a C21 N1 110.91(10) . . ? H21a C21 C18 110.91(10) . . ? H21b C21 N1 110.91(10) . . ? H21b C21 C18 110.91(10) . . ? H21b C21 H21a 108.9 . . ? C23 C22 N1 117.5(7) . . ? C27 C22 N1 123.3(6) . . ? C27 C22 C23 119.1(8) . . ? C23A C22A N1 122.7(14) . . ? C27A C22A N1 116.7(13) . . ? C27A C22A C23A 120.5(14) . . ? H23 C23 C22 120.2(5) . . ? C24 C23 C22 119.5(7) . . ? C24 C23 H23 120.2(4) . . ? H23A C23A C22A 119.3(9) . . ? C24A C23A C22A 121.3(11) . . ? C24A C23A H23A 119.3(5) . . ? H24 C24 C23 119.3(4) . . ? C25 C24 C23 121.5(6) . . ? C25 C24 H24 119.3(4) . . ? H24A C24A C23A 120.2(5) . . ? C25A C24A C23A 119.5(9) . . ? C25A C24A H24A 120.2(7) . . ? H25 C25 C24 120.9(4) . . ? C26 C25 C24 118.1(6) . . ? C26 C25 H25 120.9(3) . . ? H25A C25A C24A 119.5(7) . . ? C26A C25A C24A 121.0(12) . . ? C26A C25A H25A 119.5(7) . . ? H26 C26 C25 119.1(3) . . ? C27 C26 C25 121.8(4) . . ? C27 C26 H26 119.1(2) . . ? H26A C26A C25A 121.2(7) . . ? C27A C26A C25A 117.5(9) . . ? C27A C26A H26A 121.2(4) . . ? C26 C27 C22 119.3(5) . . ? H27 C27 C22 120.3(4) . . ? H27 C27 C26 120.3(2) . . ? C26A C27A C22A 119.6(9) . . ? H27A C27A C22A 120.2(8) . . ? H27A C27A C26A 120.2(4) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S1 O4 1.4316(13) . ? S1 O5 1.4366(13) . ? S1 C8 1.7716(17) . ? S1 C17 1.7828(18) . ? F1 C19 1.351(2) . ? F2 C19 1.375(2) . ? O1 C3 1.354(2) . ? O1 C10 1.424(3) . ? O2 C5 1.368(2) . ? O2 C9 1.369(2) . ? O3 C9 1.203(2) . ? O6 C20 1.211(2) . ? N1 C20 1.351(3) . ? N1 C21 1.472(2) . ? N1 C22 1.423(10) . ? N1 C22A 1.469(18) . ? C1 H1 0.9500 . ? C1 C2 1.374(3) . ? C1 C6 1.405(3) . ? C2 H2 0.9500 . ? C2 C3 1.395(3) . ? C3 C4 1.387(3) . ? C4 H4 0.9500 . ? C4 C5 1.378(3) . ? C5 C6 1.399(2) . ? C6 C7 1.442(2) . ? C7 C8 1.366(2) . ? C7 C11 1.499(2) . ? C8 C9 1.466(2) . ? C10 H10a 0.9800 . ? C10 H10b 0.9800 . ? C10 H10c 0.9800 . ? C11 C12 1.387(2) . ? C11 C16 1.389(3) . ? C12 H12 0.9500 . ? C12 C13 1.393(3) . ? C13 H13 0.9500 . ? C13 C14 1.378(3) . ? C14 H14 0.9500 . ? C14 C15 1.375(3) . ? C15 H15 0.9500 . ? C15 C16 1.388(3) . ? C16 H16 0.9500 . ? C17 H17a 0.9900 . ? C17 H17b 0.9900 . ? C17 C18 1.524(2) . ? C18 H18 1.0000 . ? C18 C19 1.505(2) . ? C18 C21 1.538(2) . ? C19 C20 1.535(3) . ? C21 H21a 0.9900 . ? C21 H21b 0.9900 . ? C22 C23 1.374(10) . ? C22 C27 1.380(10) . ? C22A C23A 1.359(18) . ? C22A C27A 1.38(2) . ? C23 H23 0.9500 . ? C23 C24 1.390(7) . ? C23A H23A 0.9500 . ? C23A C24A 1.370(12) . ? C24 H24 0.9500 . ? C24 C25 1.357(8) . ? C24A H24A 0.9500 . ? C24A C25A 1.347(16) . ? C25 H25 0.9500 . ? C25 C26 1.361(7) . ? C25A H25A 0.9500 . ? C25A C26A 1.429(14) . ? C26 H26 0.9500 . ? C26 C27 1.382(5) . ? C26A H26A 0.9500 . ? C26A C27A 1.397(9) . ? C27 H27 0.9500 . ? C27A H27A 0.9500 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag S1 C8 C7 C6 -175.49(14) . . . . ? S1 C8 C7 C11 7.82(18) . . . . ? S1 C8 C9 O2 170.55(11) . . . . ? S1 C8 C9 O3 -9.65(16) . . . . ? S1 C17 C18 C19 179.46(12) . . . . ? S1 C17 C18 C21 62.18(14) . . . . ? F1 C19 C18 C17 84.13(16) . . . . ? F1 C19 C18 C21 -150.92(16) . . . . ? F1 C19 C20 O6 -37.30(19) . . . . ? F1 C19 C20 N1 144.53(16) . . . . ? F2 C19 C18 C17 -35.55(16) . . . . ? F2 C19 C18 C21 89.41(15) . . . . ? F2 C19 C20 O6 77.34(18) . . . . ? F2 C19 C20 N1 -100.83(15) . . . . ? O1 C3 C2 C1 179.38(19) . . . . ? O1 C3 C4 C5 -179.80(16) . . . . ? O2 C5 C4 C3 -178.27(16) . . . . ? O2 C5 C6 C1 178.09(16) . . . . ? O2 C5 C6 C7 -4.03(19) . . . . ? O2 C9 C8 C7 -12.39(19) . . . . ? O3 C9 C8 C7 167.41(18) . . . . ? O6 C20 N1 C21 179.6(2) . . . . ? O6 C20 N1 C22 -10.7(7) . . . . ? O6 C20 N1 C22A -12.4(14) . . . . ? O6 C20 C19 C18 -162.8(2) . . . . ? N1 C20 C19 C18 19.01(17) . . . . ? N1 C21 C18 C17 148.10(13) . . . . ? N1 C21 C18 C19 24.83(15) . . . . ? N1 C22 C23 C24 175.2(7) . . . . ? N1 C22 C27 C26 -175.2(7) . . . . ? N1 C22A C23A C24A 178.6(15) . . . . ? N1 C22A C27A C26A 179.7(13) . . . . ? C1 C2 C3 C4 -0.2(2) . . . . ? C1 C6 C5 C4 -0.9(2) . . . . ? C1 C6 C7 C8 178.09(18) . . . . ? C1 C6 C7 C11 -4.9(2) . . . . ? C2 C3 C4 C5 -0.2(2) . . . . ? C3 C4 C5 C6 0.7(2) . . . . ? C4 C5 C6 C7 177.01(17) . . . . ? C5 C6 C7 C8 0.37(19) . . . . ? C5 C6 C7 C11 177.34(16) . . . . ? C6 C7 C8 C9 7.80(19) . . . . ? C6 C7 C11 C12 -79.65(17) . . . . ? C6 C7 C11 C16 97.43(18) . . . . ? C7 C11 C12 C13 -179.85(16) . . . . ? C7 C11 C16 C15 -178.9(2) . . . . ? C11 C12 C13 C14 -1.7(2) . . . . ? C11 C16 C15 C14 -0.5(2) . . . . ? C12 C13 C14 C15 -0.7(2) . . . . ? C13 C14 C15 C16 1.8(3) . . . . ? C17 C18 C19 C20 -151.72(16) . . . . ? C22 C23 C24 C25 -0.7(10) . . . . ? C22 C27 C26 C25 0.5(9) . . . . ? C22A C23A C24A C25A 3(2) . . . . ? C22A C27A C26A C25A -0.2(18) . . . . ? C23 C24 C25 C26 6.6(7) . . . . ? C23A C24A C25A C26A -8.0(12) . . . . ? C24 C25 C26 C27 -6.5(9) . . . . ? C24A C25A C26A C27A 6.5(18) . . . . ? loop_ _restr_equal_distance_atom_site_label_1 _restr_equal_distance_atom_site_label_2 _restr_equal_distance_site_symmetry_2 _restr_equal_distance_class_id N1 C22 1 1 N1 C22A 1 1 N1 C23 1 12 N1 C23A 1 12 N1 C27 1 13 N1 C27A 1 13 C22 C23 1 2 C22 C24 1 14 C22 C26 1 15 C22 C27 1 3 C22A C23A 1 2 C22A C24A 1 14 C22A C26A 1 15 C22A C27A 1 3 C23 C24 1 8 C23 C27 1 11 C23A C24A 1 8 C23A C27A 1 11 C24 C26 1 6 C24A C26A 1 6 C25 C23 1 9 C25 C24 1 5 C25 C26 1 7 C25 C27 1 4 C25A C23A 1 9 C25A C24A 1 5 C25A C26A 1 7 C25A C27A 1 4 C27 C26 1 10 C27A C26A 1 10 loop_ _restr_equal_distance_class_class_id _restr_equal_distance_class_target_weight_param _restr_equal_distance_class_average _restr_equal_distance_class_esd _restr_equal_distance_class_diff_max 1 0.0200 1.4462 0.0228 0.0228 2 0.0200 1.3663 0.0075 0.0075 3 0.0200 1.3811 0.0014 0.0014 4 0.0400 2.4066 0.0096 0.0096 5 0.0200 1.3520 0.0052 0.0052 6 0.0400 2.3738 0.0427 0.0427 7 0.0200 1.3948 0.0341 0.0341 8 0.0200 1.3803 0.0100 0.0100 9 0.0400 2.3722 0.0249 0.0249 10 0.0200 1.3894 0.0076 0.0076 11 0.0400 2.3769 0.0026 0.0026 12 0.0400 2.4372 0.0452 0.0452 13 0.0400 2.4473 0.0199 0.0199 14 0.0400 2.3836 0.0043 0.0043 15 0.0400 2.3930 0.0095 0.0095 loop_ _restr_U_similar_atom_site_label_1 _restr_U_similar_atom_site_label_2 _restr_U_similar_weight_param N1 C22 0.0100 N1 C22A 0.0100 C22 C22A 0.0100 C22 C23 0.0100 C22 C23A 0.0100 C22 C27 0.0100 C22 C27A 0.0100 C22A C23A 0.0100 C22A C27A 0.0100 C23 C22A 0.0100 C23 C23A 0.0100 C23 C24 0.0100 C23 C24A 0.0100 C23A C24A 0.0100 C24 C23A 0.0100 C24 C24A 0.0100 C24 C25 0.0100 C24 C25A 0.0100 C24A C25A 0.0100 C25 C24A 0.0100 C25 C25A 0.0100 C25 C26 0.0100 C25 C26A 0.0100 C25A C26A 0.0100 C26 C25A 0.0100 C26 C26A 0.0100 C26 C27 0.0100 C26 C27A 0.0100 C26A C27A 0.0100 C27 C22A 0.0100 C27 C26A 0.0100 C27 C27A 0.0100