#------------------------------------------------------------------------------ #$Date: 2024-04-04 11:34:15 +0300 (Thu, 04 Apr 2024) $ #$Revision: 290785 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/83/7248382.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7248382 loop_ _publ_author_name 'Sun, Jie' 'Wang, Chaodong' 'Wu, Chunlei' 'Wang, Wenjian' 'Zeng, Yue' 'Song, Shengjie' 'Chen, Zhiwei' 'Li, Jianjun' _publ_section_title ; Photocatalyst-free H2O-regulated and regiodivergent multicomponent hydrogenation/bifunctional sulfonylation of alkynes ; _journal_issue 6 _journal_name_full 'Green Chemistry' _journal_page_first 3301 _journal_page_last 3307 _journal_paper_doi 10.1039/D3GC04960D _journal_volume 26 _journal_year 2024 _chemical_formula_moiety 'C26 H20 Cl F2 N O5 S' _chemical_formula_sum 'C26 H20 Cl F2 N O5 S' _chemical_formula_weight 531.94 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2023-12-07 _audit_creation_method ; Olex2 1.5 (compiled 2023.03.06 svn.rbb2c1857 for OlexSys, GUI svn.r6748) ; _audit_update_record ; 2023-12-07 deposited with the CCDC. 2024-01-26 downloaded from the CCDC. ; _cell_angle_alpha 73.689(2) _cell_angle_beta 87.428(2) _cell_angle_gamma 75.023(2) _cell_formula_units_Z 2 _cell_length_a 6.3919(4) _cell_length_b 10.6731(6) _cell_length_c 18.7577(11) _cell_measurement_reflns_used 9848 _cell_measurement_temperature 170.00 _cell_measurement_theta_max 57.053 _cell_measurement_theta_min 3.876 _cell_volume 1185.92(12) _computing_cell_refinement 'SAINT V8.40B (?, 2016)' _computing_data_collection 'Bruker Instrument Service vV6.2.14' _computing_data_reduction 'SAINT V8.40B (?, 2016)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2019/2 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 170.00 _diffrn_measured_fraction_theta_full 0.985 _diffrn_measured_fraction_theta_max 0.981 _diffrn_measurement_device_type 'zju Bruker D8 Venture' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_type GaK\a _diffrn_radiation_wavelength 1.34139 _diffrn_reflns_av_R_equivalents 0.0554 _diffrn_reflns_av_unetI/netI 0.0415 _diffrn_reflns_Laue_measured_fraction_full 0.985 _diffrn_reflns_Laue_measured_fraction_max 0.981 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 37998 _diffrn_reflns_point_group_measured_fraction_full 0.985 _diffrn_reflns_point_group_measured_fraction_max 0.981 _diffrn_reflns_theta_full 53.594 _diffrn_reflns_theta_max 57.106 _diffrn_reflns_theta_min 3.876 _diffrn_source_current 3.57 _diffrn_source_power 0.24954300000000001 _diffrn_source_voltage 69.9 _exptl_absorpt_coefficient_mu 1.799 _exptl_absorpt_correction_T_max 0.7512 _exptl_absorpt_correction_T_min 0.6191 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1383 before and 0.0864 after correction. The Ratio of minimum to maximum transmission is 0.8241. The \l/2 correction factor is Not present. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.490 _exptl_crystal_description needle _exptl_crystal_F_000 548 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.03 _exptl_crystal_size_min 0.02 _refine_diff_density_max 1.541 _refine_diff_density_min -0.515 _refine_diff_density_rms 0.141 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.125 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 325 _refine_ls_number_reflns 4772 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.125 _refine_ls_R_factor_all 0.0859 _refine_ls_R_factor_gt 0.0798 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1315P)^2^+1.7519P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2190 _refine_ls_wR_factor_ref 0.2236 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4168 _reflns_number_total 4772 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d3gc04960d2.cif _cod_data_source_block 231125_sj_dmso_0m _cod_database_code 7248382 _shelx_shelxl_version_number 2019/2 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.965 _shelx_estimated_absorpt_t_min 0.715 _olex2_refinement_description ; 1.a Ternary CH refined with riding coordinates: C8(H8) 1.b Secondary CH2 refined with riding coordinates: C7(H7a,H7b), C11(H11a,H11b) 1.c Aromatic/amide H refined with riding coordinates: C1(H1), C2(H2), C4(H4), C5(H5), C14(H14), C15(H15), C16(H16), C17(H17), C18(H18), C19(H19), C22(H22), C23(H23), C24(H24), C25(H25), C26(H26) ; _shelx_res_file ; TITL 231125_sj_dmso_0m_a.res in P-1 231125_sj_dmso_0m.res created by SHELXL-2019/2 at 14:21:01 on 27-Nov-2023 REM Old TITL 231125_SJ_DMSO_0m in P-1 REM SHELXT solution in P-1: R1 0.202, Rweak 0.019, Alpha 0.067 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C26 F N O6 S2 CELL 1.34139 6.3919 10.6731 18.7577 73.689 87.428 75.023 ZERR 2 0.0004 0.0006 0.0011 0.002 0.002 0.002 LATT 1 SFAC C H Cl F N O S DISP C 0.0137 0.0067 57.1 DISP Cl 0.3281 0.5435 4162.2 DISP F 0.0583 0.04 317.7 DISP H 0 0 0.6 DISP N 0.0241 0.0134 109.9 DISP O 0.0389 0.0241 193.4 DISP S 0.2925 0.4295 3294.4 UNIT 52 40 2 4 2 10 2 L.S. 4 0 0 PLAN 5 SIZE 0.02 0.03 0.2 TEMP -103.15 CONF BOND list 4 fmap 2 53 MORE -1 HTAB BOND $H ACTA OMIT 1 9 4 OMIT -2 -1 14 OMIT 0 0 1 OMIT 7 3 11 OMIT -7 -5 2 OMIT 7 3 8 OMIT 7 4 9 OMIT -7 -3 2 OMIT 7 3 6 OMIT 7 6 3 OMIT 7 1 8 OMIT -1 1 8 OMIT -7 -4 2 OMIT 7 3 7 OMIT 7 5 9 OMIT 7 2 6 OMIT 7 8 7 OMIT -7 -5 1 OMIT -7 -8 2 OMIT 0 2 8 OMIT 0 -2 7 OMIT -7 -7 4 OMIT 7 6 9 REM REM REM WGHT 0.131500 1.751900 FVAR 0.37983 CL1 3 -0.114203 0.978386 0.761878 11.00000 0.07118 0.03417 = 0.02481 -0.01401 0.00947 0.00423 S1 7 0.453985 0.537452 0.309741 11.00000 0.03095 0.02444 = 0.02181 -0.00852 0.00830 -0.00800 F1 4 -0.053501 0.753583 0.338698 11.00000 0.03571 0.05669 = 0.03280 -0.01626 -0.00307 -0.00556 O1 6 -0.290098 0.725894 0.478089 11.00000 0.02966 0.14879 = 0.06849 -0.06895 0.02177 -0.03927 N1 5 0.041965 0.758879 0.500810 11.00000 0.02086 0.03581 = 0.02643 -0.01175 0.00739 -0.00796 C1 1 -0.184537 0.804849 0.604262 11.00000 0.03136 0.03998 = 0.03232 -0.01200 0.01059 -0.00759 AFIX 43 H1 2 -0.284349 0.761057 0.592246 11.00000 -1.20000 AFIX 0 F2 4 -0.033212 0.548241 0.404877 11.00000 0.04910 0.05542 = 0.05552 -0.02833 0.01334 -0.03244 O2 6 0.256559 0.538360 0.276888 11.00000 0.04034 0.05161 = 0.03760 -0.02202 0.01269 -0.02362 C2 1 -0.218253 0.857569 0.664828 11.00000 0.04059 0.03917 = 0.02907 -0.00594 0.01552 -0.00096 AFIX 43 H2 2 -0.343026 0.851576 0.693749 11.00000 -1.20000 AFIX 0 O3 6 0.568169 0.415100 0.362722 11.00000 0.04895 0.02761 = 0.03303 0.00101 0.01610 -0.00030 C3 1 -0.071272 0.918391 0.682951 11.00000 0.04664 0.02940 = 0.02475 -0.00871 0.00599 0.00482 O4 6 0.974426 0.595179 0.122101 11.00000 0.03986 0.03020 = 0.02506 -0.00549 0.00913 -0.00551 C4 1 0.109269 0.930525 0.641080 11.00000 0.04316 0.03072 = 0.03078 -0.01181 0.00193 -0.00348 AFIX 43 H4 2 0.209841 0.972783 0.654124 11.00000 -1.20000 AFIX 0 O5 6 1.107354 0.374731 0.183607 11.00000 0.03318 0.02735 = 0.02669 -0.01065 0.01080 -0.00676 C5 1 0.142197 0.880101 0.579517 11.00000 0.03037 0.03321 = 0.02971 -0.01123 0.00684 -0.00499 AFIX 43 H5 2 0.264878 0.889256 0.549933 11.00000 -1.20000 AFIX 0 C6 1 -0.002645 0.816605 0.561019 11.00000 0.02827 0.02919 = 0.02205 -0.00649 0.00447 -0.00163 C7 1 0.255633 0.742370 0.467026 11.00000 0.01993 0.03619 = 0.02537 -0.01363 0.00706 -0.00987 AFIX 23 H7A 2 0.372940 0.704139 0.505729 11.00000 -1.20000 H7B 2 0.273501 0.830031 0.435206 11.00000 -1.20000 AFIX 0 C8 1 0.258275 0.644043 0.420300 11.00000 0.02736 0.03258 = 0.02577 -0.01247 0.00793 -0.01019 AFIX 13 H8 2 0.318991 0.549815 0.452105 11.00000 -1.20000 AFIX 0 C9 1 0.021980 0.662877 0.405759 11.00000 0.03409 0.04606 = 0.03081 -0.01755 0.00735 -0.01828 C10 1 -0.099255 0.718914 0.466783 11.00000 0.03038 0.06320 = 0.03528 -0.02454 0.01082 -0.01859 C11 1 0.402495 0.670514 0.353087 11.00000 0.02763 0.03097 = 0.02082 -0.01158 0.00656 -0.00991 AFIX 23 H11A 2 0.541704 0.679564 0.369393 11.00000 -1.20000 H11B 2 0.330668 0.756600 0.316616 11.00000 -1.20000 AFIX 0 C12 1 0.632096 0.585807 0.236085 11.00000 0.03199 0.02785 = 0.01946 -0.01122 0.00719 -0.01116 C13 1 0.550863 0.722346 0.183769 11.00000 0.03712 0.02577 = 0.02072 -0.01165 0.01140 -0.00730 C14 1 0.673626 0.816561 0.175095 11.00000 0.05455 0.03422 = 0.03452 -0.01652 0.01682 -0.01722 AFIX 43 H14 2 0.807432 0.792648 0.201864 11.00000 -1.20000 AFIX 0 C15 1 0.599241 0.944488 0.127416 11.00000 0.07917 0.03018 = 0.04563 -0.01261 0.02555 -0.01982 AFIX 43 H15 2 0.682068 1.008725 0.121563 11.00000 -1.20000 AFIX 0 C16 1 0.406759 0.979328 0.088510 11.00000 0.09074 0.02561 = 0.03406 -0.00546 0.02516 0.00106 AFIX 43 H16 2 0.357972 1.067406 0.055552 11.00000 -1.20000 AFIX 0 C17 1 0.283236 0.888351 0.096575 11.00000 0.06630 0.03713 = 0.02251 -0.00717 0.00454 0.01109 AFIX 43 H17 2 0.149508 0.913817 0.069574 11.00000 -1.20000 AFIX 0 C18 1 0.354789 0.758757 0.144453 11.00000 0.04246 0.03294 = 0.02507 -0.01056 0.00617 -0.00261 AFIX 43 H18 2 0.270093 0.695542 0.150228 11.00000 -1.20000 AFIX 0 C19 1 0.814983 0.491451 0.235189 11.00000 0.03059 0.02770 = 0.02045 -0.00736 0.00456 -0.00853 AFIX 43 H19 2 0.848730 0.413982 0.276927 11.00000 -1.20000 AFIX 0 C20 1 0.969944 0.499020 0.173366 11.00000 0.02777 0.02946 = 0.02406 -0.01165 0.00369 -0.00793 C21 1 1.275478 0.358234 0.133018 11.00000 0.03201 0.02405 = 0.02946 -0.01224 0.01160 -0.00916 C22 1 1.484246 0.326514 0.160591 11.00000 0.03761 0.02990 = 0.03140 -0.01351 0.00617 -0.01135 AFIX 43 H22 2 1.510978 0.321420 0.210870 11.00000 -1.20000 AFIX 0 C23 1 1.655767 0.301989 0.113687 11.00000 0.02952 0.03279 = 0.04289 -0.01519 0.00700 -0.00996 AFIX 43 H23 2 1.800830 0.280291 0.131850 11.00000 -1.20000 AFIX 0 C24 1 1.614891 0.309226 0.040578 11.00000 0.03838 0.03278 = 0.04224 -0.01903 0.01786 -0.01085 AFIX 43 H24 2 1.731985 0.292255 0.008641 11.00000 -1.20000 AFIX 0 C25 1 1.403802 0.341133 0.013989 11.00000 0.04489 0.03566 = 0.02892 -0.01615 0.00909 -0.00988 AFIX 43 H25 2 1.376412 0.346420 -0.036272 11.00000 -1.20000 AFIX 0 C26 1 1.231315 0.365533 0.060474 11.00000 0.03228 0.03048 = 0.03121 -0.01177 0.00546 -0.00644 AFIX 43 H26 2 1.086055 0.386793 0.042583 11.00000 -1.20000 AFIX 0 HKLF 4 REM 231125_sj_dmso_0m_a.res in P-1 REM wR2 = 0.2236, GooF = S = 1.125, Restrained GooF = 1.125 for all data REM R1 = 0.0798 for 4168 Fo > 4sig(Fo) and 0.0859 for all 4772 data REM 325 parameters refined using 0 restraints END WGHT 0.1315 1.7513 REM Instructions for potential hydrogen bonds HTAB C1 O1 EQIV $1 x+1, y, z HTAB C7 O1_$1 EQIV $2 -x+1, -y+1, -z+1 HTAB C7 O3_$2 HTAB C11 O1_$1 EQIV $3 -x, -y+2, -z+1 HTAB C11 Cl1_$3 HTAB C19 O3 REM Highest difference peak 1.541, deepest hole -0.515, 1-sigma level 0.141 Q1 1 -0.2755 0.9789 0.7565 11.00000 0.05 1.54 Q2 1 0.0840 0.9789 0.7604 11.00000 0.05 1.14 Q3 1 0.6116 0.5397 0.3059 11.00000 0.05 1.14 Q4 1 0.8810 0.5387 0.3037 11.00000 0.05 1.11 Q5 1 0.7501 0.5379 0.3053 11.00000 0.05 1.09 ; _shelx_res_checksum 65803 _shelx_hkl_file ; -1 0 0 79.09 3.50 -1 0 0 79.49 3.40 -1 0 0 82.39 3.40 -1 0 0 76.29 3.40 -1 0 0 79.79 3.40 -1 0 0 83.69 3.40 -1 0 0 79.79 3.40 1 0 0 85.29 3.30 -2 0 0 116.09 5.00 -2 0 0 118.39 5.10 -2 0 0 122.19 4.90 -2 0 0 127.89 5.10 2 0 0 117.29 5.00 -3 0 0 79.69 3.70 -3 0 0 82.19 3.50 -3 0 0 87.69 3.70 3 0 0 78.19 3.50 3 0 0 84.79 3.80 3 0 0 89.09 3.80 3 0 0 84.09 3.90 3 0 0 85.29 4.10 3 0 0 86.99 3.70 -4 0 0 14.60 1.10 -4 0 0 15.20 1.20 -4 0 0 14.50 1.00 -4 0 0 13.70 1.20 -4 0 0 13.60 1.10 4 0 0 14.60 1.20 4 0 0 15.10 1.60 4 0 0 14.40 1.70 4 0 0 15.70 1.40 4 0 0 13.80 1.50 4 0 0 13.50 1.30 4 0 0 15.00 1.20 -5 0 0 0.50 0.50 -5 0 0 0.40 0.60 -5 0 0 0.80 1.80 -5 0 0 0.30 0.50 -5 0 0 0.50 0.60 5 0 0 1.10 1.10 5 0 0 -0.20 0.80 5 0 0 0.50 0.90 5 0 0 1.20 0.90 5 0 0 1.00 0.60 5 0 0 0.30 0.70 -6 0 0 16.20 1.50 -6 0 0 16.00 1.40 -6 0 0 16.80 1.70 -6 0 0 15.20 1.50 -6 0 0 16.80 1.70 6 0 0 13.30 1.80 6 0 0 19.30 2.60 6 0 0 11.60 1.60 6 0 0 16.30 1.90 -7 0 0 3.00 1.10 -7 0 0 5.80 1.40 7 0 0 3.20 1.40 7 0 0 4.80 1.80 7 0 0 3.90 2.00 7 0 0 3.60 1.90 7 -1 0 5.90 1.80 7 -1 0 7.30 1.50 7 -1 0 9.90 2.80 -7 1 0 3.80 1.70 -7 1 0 5.90 1.20 -7 1 0 2.10 1.30 6 -1 0 0.70 1.00 6 -1 0 0.10 1.00 6 -1 0 0.10 1.50 6 -1 0 -0.50 1.10 -6 1 0 -0.60 0.70 -6 1 0 0.10 0.60 -6 1 0 0.30 0.90 -6 1 0 -0.10 0.90 -6 1 0 -0.40 0.70 5 -1 0 10.40 1.70 5 -1 0 9.50 1.30 5 -1 0 6.60 1.30 5 -1 0 5.60 1.10 5 -1 0 8.20 1.30 -5 1 0 6.50 1.00 -5 1 0 9.80 1.10 -5 1 0 8.60 1.10 4 -1 0 77.19 3.80 4 -1 0 79.39 3.60 4 -1 0 78.99 4.30 4 -1 0 74.09 3.60 4 -1 0 77.39 3.80 4 -1 0 78.09 3.90 4 -1 0 78.09 3.80 -4 1 0 74.79 3.60 -4 1 0 75.59 3.50 -4 1 0 82.69 3.90 -4 1 0 75.59 3.80 -4 1 0 80.69 3.70 3 -1 0 2.60 0.70 3 -1 0 2.80 0.50 3 -1 0 3.90 0.60 3 -1 0 3.70 0.80 3 -1 0 3.30 1.00 3 -1 0 3.40 0.70 3 -1 0 3.30 0.70 3 -1 0 3.50 0.70 -3 1 0 2.20 0.60 -3 1 0 2.30 0.40 -3 1 0 3.30 0.50 -3 1 0 2.90 0.60 -3 1 0 2.10 0.50 -3 1 0 2.00 0.60 2 -1 0 1.70 0.60 2 -1 0 0.80 0.30 2 -1 0 1.20 0.40 2 -1 0 1.10 0.60 2 -1 0 1.20 0.30 2 -1 0 0.60 0.50 2 -1 0 1.20 0.40 2 -1 0 0.70 0.40 2 -1 0 0.50 0.40 2 -1 0 1.20 0.50 -2 1 0 0.70 0.30 -2 1 0 1.20 0.40 -2 1 0 0.80 0.40 -2 1 0 0.70 0.40 -2 1 0 0.20 0.30 -2 1 0 0.70 0.40 -2 1 0 0.90 0.30 1 -1 0 376.36 19.60 0 -1 0 1176.08 47.60 0 1 0 1093.29 47.50 -1 -1 0 74.99 3.20 -1 -1 0 74.39 3.20 -1 -1 0 71.09 3.10 -1 -1 0 74.39 3.20 -1 -1 0 81.39 3.30 -1 -1 0 70.89 3.20 -1 -1 0 76.89 3.20 2 1 0 621.74 28.40 -3 -1 0 63.99 3.40 -3 -1 0 65.59 3.00 -3 -1 0 74.69 3.20 -3 -1 0 69.19 3.20 3 1 0 65.59 3.10 3 1 0 80.19 3.50 3 1 0 77.29 3.40 3 1 0 74.49 3.50 3 1 0 77.69 3.40 3 1 0 78.69 3.40 3 1 0 74.69 3.40 3 1 0 79.19 3.60 3 1 0 70.19 3.30 3 1 0 70.49 3.10 3 1 0 77.49 3.30 3 1 0 72.79 3.40 4 1 0 256.17 10.50 -5 -1 0 55.29 3.80 -5 -1 0 51.29 2.50 -5 -1 0 51.69 2.80 -5 -1 0 54.29 2.60 -5 -1 0 44.90 2.60 5 1 0 50.59 3.30 5 1 0 54.99 3.10 5 1 0 50.89 3.00 5 1 0 52.09 2.90 5 1 0 51.49 2.80 5 1 0 52.79 3.10 5 1 0 49.40 2.80 -6 -1 0 3.20 0.90 -6 -1 0 3.00 0.80 -6 -1 0 3.10 0.80 -6 -1 0 3.50 0.80 6 1 0 2.80 1.10 6 1 0 5.70 1.60 6 1 0 3.70 1.10 -7 -1 0 6.30 1.10 -7 -1 0 8.60 1.50 7 1 0 6.90 1.40 7 1 0 5.60 2.10 7 1 0 5.40 1.40 7 1 0 7.00 1.90 7 -2 0 10.90 2.40 7 -2 0 14.00 2.30 -7 2 0 10.80 1.40 -7 2 0 8.10 1.50 -7 2 0 15.10 1.80 6 -2 0 1.00 1.40 6 -2 0 0.50 1.10 -6 2 0 -0.10 1.20 -6 2 0 0.50 1.10 -6 2 0 0.20 0.90 5 -2 0 -0.70 1.20 5 -2 0 2.60 1.30 5 -2 0 2.30 1.10 5 -2 0 0.90 1.00 -5 2 0 -0.50 0.60 -5 2 0 0.20 0.60 -5 2 0 1.20 0.80 -5 2 0 0.70 0.90 -5 2 0 0.30 0.60 4 -2 0 69.49 3.40 4 -2 0 66.09 3.40 4 -2 0 72.69 4.20 -4 2 0 66.19 3.60 -4 2 0 73.69 3.30 -4 2 0 69.29 3.30 -4 2 0 67.19 3.40 -4 2 0 67.29 3.40 3 -2 0 122.19 5.30 3 -2 0 126.89 5.40 3 -2 0 128.29 5.50 3 -2 0 128.89 5.20 3 -2 0 122.59 5.40 3 -2 0 119.79 5.20 3 -2 0 122.99 5.50 -3 2 0 118.49 5.50 2 -2 0 2.00 0.40 2 -2 0 1.80 0.60 2 -2 0 1.70 0.50 2 -2 0 1.40 0.30 2 -2 0 1.30 0.60 2 -2 0 2.40 0.80 2 -2 0 1.40 0.50 2 -2 0 1.90 0.50 2 -2 0 1.80 0.70 -2 2 0 1.60 0.40 -2 2 0 0.90 0.50 -2 2 0 1.40 0.40 -2 2 0 1.60 0.50 -2 2 0 1.40 0.40 1 -2 0 32.30 1.40 1 -2 0 31.30 1.50 1 -2 0 32.90 1.60 1 -2 0 33.50 1.50 1 -2 0 34.20 1.50 1 -2 0 31.10 1.70 -1 2 0 33.60 1.50 -1 2 0 30.30 1.50 -1 2 0 33.80 1.60 -1 2 0 32.50 1.50 0 -2 0 1.70 0.40 0 -2 0 1.60 0.20 0 -2 0 1.20 0.30 0 -2 0 1.40 0.40 0 -2 0 1.70 0.50 0 -2 0 1.90 0.40 0 -2 0 1.50 0.40 0 2 0 2.40 0.40 0 2 0 1.90 0.40 0 2 0 2.80 0.40 0 2 0 2.10 0.40 0 2 0 2.00 0.30 0 2 0 2.30 0.30 0 2 0 2.30 0.40 0 2 0 2.20 0.50 0 2 0 2.40 0.20 0 2 0 1.50 0.50 -1 -2 0 22.30 1.00 -1 -2 0 22.80 1.10 -1 -2 0 21.20 1.10 1 2 0 21.20 1.20 1 2 0 24.30 1.10 1 2 0 24.20 1.20 1 2 0 22.70 1.50 1 2 0 25.50 1.20 1 2 0 22.90 1.30 1 2 0 24.40 1.20 1 2 0 24.30 1.10 -3 -2 0 122.39 5.10 -3 -2 0 121.69 5.00 -4 -2 0 21.90 1.10 -4 -2 0 22.70 1.20 -4 -2 0 21.10 1.40 -4 -2 0 21.90 1.30 -4 -2 0 23.80 2.00 4 2 0 22.30 1.80 4 2 0 22.20 1.60 4 2 0 19.70 1.60 4 2 0 23.20 1.70 4 2 0 21.60 1.70 4 2 0 21.60 1.50 4 2 0 22.80 1.50 4 2 0 22.10 1.60 4 2 0 21.40 1.70 4 2 0 21.80 1.60 4 2 0 22.20 1.70 -5 -2 0 2.40 1.20 -5 -2 0 1.30 0.50 -5 -2 0 2.90 0.70 -5 -2 0 2.00 0.50 -5 -2 0 2.00 0.70 5 2 0 0.40 0.80 5 2 0 1.90 0.90 5 2 0 1.10 0.80 5 2 0 2.60 1.30 5 2 0 1.00 0.80 5 2 0 1.70 0.90 5 2 0 1.20 0.70 -6 -2 0 2.60 1.30 -6 -2 0 4.50 1.00 -6 -2 0 5.30 0.80 -6 -2 0 4.70 0.80 6 2 0 3.80 1.20 6 2 0 4.20 1.60 6 2 0 5.20 1.50 6 2 0 6.60 1.60 6 2 0 3.00 1.10 -7 -2 0 1.10 0.80 -7 -2 0 0.50 1.00 7 2 0 0.00 1.00 7 2 0 0.80 1.30 7 2 0 1.90 1.70 7 2 0 0.80 1.10 7 -3 0 22.90 3.20 -7 3 0 19.50 2.00 -7 3 0 17.10 1.80 -7 3 0 20.90 1.80 6 -3 0 4.60 1.00 6 -3 0 2.90 1.30 6 -3 0 2.30 1.30 6 -3 0 1.60 1.80 6 -3 0 1.10 1.30 -6 3 0 4.40 1.30 -6 3 0 2.00 1.10 -6 3 0 2.20 1.20 -6 3 0 3.50 1.00 -6 3 0 4.10 1.10 5 -3 0 42.60 2.80 5 -3 0 42.90 3.70 5 -3 0 45.90 3.00 5 -3 0 44.80 3.10 5 -3 0 43.40 3.10 -5 3 0 43.60 2.70 -5 3 0 47.40 2.80 -5 3 0 45.60 2.60 -5 3 0 41.10 2.70 -5 3 0 45.80 2.60 4 -3 0 1.20 0.80 4 -3 0 2.40 0.70 4 -3 0 1.90 0.90 4 -3 0 3.60 1.20 4 -3 0 1.60 0.90 -4 3 0 2.30 0.60 -4 3 0 2.50 0.80 -4 3 0 2.10 0.70 -4 3 0 2.40 1.00 -4 3 0 2.00 0.70 3 -3 0 1.60 0.60 3 -3 0 2.00 0.50 3 -3 0 1.90 0.80 3 -3 0 1.30 0.70 3 -3 0 1.40 0.60 3 -3 0 1.30 0.70 3 -3 0 2.40 0.50 3 -3 0 3.10 0.90 -3 3 0 1.50 0.50 -3 3 0 2.50 0.80 -3 3 0 1.60 0.60 -3 3 0 2.20 0.50 -3 3 0 2.40 0.70 2 -3 0 13.10 1.40 2 -3 0 14.30 0.90 2 -3 0 14.10 1.10 2 -3 0 14.30 1.20 2 -3 0 12.60 0.90 2 -3 0 13.80 1.50 2 -3 0 13.20 0.90 2 -3 0 14.60 1.10 -2 3 0 14.50 1.20 -2 3 0 14.00 1.00 -2 3 0 13.90 1.10 -2 3 0 13.40 1.00 -2 3 0 14.20 1.00 1 -3 0 33.10 1.80 1 -3 0 39.20 1.90 1 -3 0 36.40 1.60 1 -3 0 36.60 1.90 1 -3 0 36.60 2.00 -1 3 0 37.40 1.90 -1 3 0 38.30 2.10 -1 3 0 38.60 1.90 -1 3 0 36.00 1.80 -1 3 0 38.50 1.80 0 -3 0 431.96 26.00 0 3 0 413.16 31.20 -1 -3 0 75.79 3.10 -1 -3 0 79.19 3.30 -1 -3 0 76.59 3.30 -1 -3 0 75.79 3.40 1 3 0 71.59 3.20 -2 -3 0 1.80 0.30 -2 -3 0 1.90 0.30 -2 -3 0 2.40 0.60 -2 -3 0 1.60 0.40 2 3 0 1.70 0.50 2 3 0 3.00 0.50 2 3 0 2.70 0.60 2 3 0 1.60 0.50 2 3 0 1.90 0.50 2 3 0 1.40 0.50 -3 -3 0 5.10 0.80 -3 -3 0 4.30 0.40 -3 -3 0 4.90 0.40 -3 -3 0 5.70 1.00 -3 -3 0 4.40 0.50 3 3 0 5.60 0.90 3 3 0 7.10 1.00 3 3 0 5.30 0.80 3 3 0 5.40 0.70 3 3 0 7.30 0.90 3 3 0 6.80 0.90 3 3 0 4.20 0.70 3 3 0 5.60 0.90 3 3 0 5.60 1.10 3 3 0 7.60 1.10 3 3 0 5.40 0.80 -4 -3 0 257.47 11.70 -4 -3 0 306.07 11.50 -5 -3 0 0.60 0.50 -5 -3 0 0.30 0.40 -5 -3 0 0.70 0.50 -5 -3 0 0.20 1.20 -5 -3 0 0.30 0.60 -5 -3 0 0.00 0.30 5 3 0 0.70 0.80 5 3 0 0.50 0.80 5 3 0 -0.10 0.60 5 3 0 0.90 0.90 5 3 0 0.80 0.90 5 3 0 0.50 0.80 5 3 0 0.40 1.00 5 3 0 1.80 1.00 -6 -3 0 200.18 8.40 -6 -3 0 187.18 8.90 -6 -3 0 202.48 8.60 6 3 0 189.48 8.90 6 3 0 206.08 9.00 6 3 0 205.38 9.30 6 3 0 205.98 8.90 6 3 0 207.98 9.00 -7 -3 0 14.50 1.20 -7 -3 0 12.00 1.40 7 3 0 18.90 2.00 7 3 0 12.10 1.90 7 3 0 11.50 1.80 6 -4 0 19.70 2.80 6 -4 0 16.60 2.70 6 -4 0 23.40 2.80 -6 4 0 20.60 2.20 -6 4 0 24.10 2.30 -6 4 0 23.40 1.90 -6 4 0 24.00 2.50 -6 4 0 21.00 1.90 5 -4 0 16.00 2.20 5 -4 0 14.00 1.70 5 -4 0 10.40 1.70 5 -4 0 12.90 1.90 5 -4 0 15.10 2.60 -5 4 0 14.20 1.50 -5 4 0 13.20 1.70 -5 4 0 15.20 1.50 -5 4 0 15.90 1.70 -5 4 0 12.70 1.50 4 -4 0 29.10 2.40 4 -4 0 35.90 2.80 4 -4 0 32.70 2.20 4 -4 0 28.80 2.40 4 -4 0 29.90 2.40 -4 4 0 31.60 2.20 -4 4 0 33.70 2.20 -4 4 0 31.40 2.10 -4 4 0 34.00 2.60 -4 4 0 26.30 2.80 3 -4 0 17.10 1.50 3 -4 0 16.50 1.40 3 -4 0 17.00 1.50 3 -4 0 12.10 1.60 3 -4 0 15.50 1.60 3 -4 0 14.70 1.50 -3 4 0 16.00 1.20 -3 4 0 17.80 1.50 -3 4 0 17.80 1.40 -3 4 0 13.30 1.20 -3 4 0 14.20 1.30 2 -4 0 35.10 2.30 2 -4 0 40.70 2.10 2 -4 0 39.70 2.10 2 -4 0 41.20 2.50 2 -4 0 36.10 2.10 2 -4 0 37.80 2.00 -2 4 0 35.60 2.20 -2 4 0 35.60 1.80 -2 4 0 38.60 2.00 -2 4 0 39.90 2.10 -2 4 0 38.60 2.00 -2 4 0 38.90 2.00 1 -4 0 6.80 0.70 1 -4 0 6.70 0.80 1 -4 0 5.80 0.60 1 -4 0 5.50 0.70 -1 4 0 6.10 0.90 -1 4 0 4.20 0.70 -1 4 0 4.80 0.60 -1 4 0 4.90 0.60 -1 4 0 4.00 0.60 0 -4 0 145.29 6.20 -1 -4 0 16.20 1.20 -1 -4 0 15.40 1.10 -1 -4 0 16.30 0.90 -1 -4 0 16.90 0.90 -1 -4 0 15.90 0.80 -1 -4 0 14.90 0.80 -1 -4 0 15.80 0.80 1 4 0 17.30 1.00 1 4 0 16.70 1.00 1 4 0 16.90 0.90 1 4 0 15.90 0.90 1 4 0 16.00 1.00 1 4 0 15.30 1.00 1 4 0 15.90 1.10 -2 -4 0 73.19 3.40 -2 -4 0 76.99 3.20 2 4 0 88.09 3.70 2 4 0 78.19 3.30 -3 -4 0 6.90 1.00 -3 -4 0 6.00 0.90 -3 -4 0 6.70 0.50 -3 -4 0 6.40 0.50 3 4 0 9.90 1.00 3 4 0 7.50 0.90 3 4 0 9.10 1.30 3 4 0 7.10 0.90 3 4 0 9.20 1.00 3 4 0 8.50 0.90 3 4 0 5.10 1.10 3 4 0 6.70 0.90 3 4 0 7.20 1.30 3 4 0 8.10 1.00 -4 -4 0 71.69 3.80 -4 -4 0 73.19 3.20 -4 -4 0 71.39 3.20 4 4 0 71.79 3.90 4 4 0 72.99 4.00 4 4 0 78.59 3.70 4 4 0 77.49 3.50 4 4 0 74.49 3.60 4 4 0 74.79 3.60 4 4 0 74.29 3.80 4 4 0 74.39 3.60 4 4 0 73.09 3.70 4 4 0 75.49 3.60 4 4 0 72.59 3.70 -5 -4 0 75.29 4.10 -5 -4 0 74.99 3.30 -5 -4 0 74.19 3.30 -5 -4 0 64.59 3.10 -5 -4 0 74.09 3.10 5 4 0 72.49 3.90 5 4 0 63.09 3.90 5 4 0 71.59 3.70 5 4 0 76.29 3.80 5 4 0 72.59 3.70 5 4 0 69.19 3.90 5 4 0 67.99 3.60 5 4 0 70.99 3.60 5 4 0 73.29 3.80 5 4 0 71.09 4.00 -6 -4 0 89.89 5.30 -6 -4 0 87.99 4.00 -6 -4 0 88.59 4.20 6 4 0 88.59 4.70 6 4 0 96.39 4.90 6 4 0 89.19 4.50 6 4 0 92.29 4.60 6 4 0 94.89 4.70 -7 -4 0 7.40 2.50 7 4 0 2.70 1.20 7 4 0 0.00 1.30 7 4 0 0.60 1.00 7 4 0 0.90 1.20 6 -5 0 2.30 2.20 6 -5 0 4.60 2.50 -6 5 0 2.50 1.20 -6 5 0 2.60 1.30 -6 5 0 2.40 2.10 -6 5 0 1.90 1.10 -6 5 0 2.80 1.20 5 -5 0 4.70 1.40 5 -5 0 6.60 2.20 5 -5 0 5.60 1.60 -5 5 0 4.60 1.00 -5 5 0 6.40 1.10 -5 5 0 5.50 1.10 -5 5 0 6.00 1.10 -5 5 0 4.20 1.30 4 -5 0 14.20 2.30 4 -5 0 10.40 1.50 4 -5 0 10.80 1.70 4 -5 0 11.80 1.90 4 -5 0 11.00 1.80 -4 5 0 13.00 1.40 -4 5 0 15.00 2.20 -4 5 0 10.80 1.50 -4 5 0 13.30 1.40 -4 5 0 12.50 1.40 -4 5 0 12.10 1.40 3 -5 0 16.20 1.80 3 -5 0 19.20 2.00 3 -5 0 17.80 1.70 3 -5 0 18.50 1.60 3 -5 0 18.10 1.90 3 -5 0 18.00 1.70 -3 5 0 19.80 1.40 -3 5 0 18.20 1.50 -3 5 0 19.90 1.50 -3 5 0 18.90 1.70 -3 5 0 18.80 1.60 -3 5 0 19.00 1.40 2 -5 0 67.09 3.30 2 -5 0 63.09 3.50 2 -5 0 61.49 3.50 2 -5 0 63.09 3.20 2 -5 0 66.29 3.30 2 -5 0 62.29 3.30 -2 5 0 63.69 3.00 -2 5 0 64.49 3.20 -2 5 0 62.19 3.00 -2 5 0 63.29 3.40 -2 5 0 66.89 3.10 -2 5 0 62.89 3.10 -2 5 0 66.19 3.10 1 -5 0 8.00 1.00 1 -5 0 5.90 0.70 1 -5 0 6.10 0.80 1 -5 0 8.20 0.90 -1 5 0 6.20 0.70 -1 5 0 6.20 0.70 -1 5 0 6.50 0.90 -1 5 0 6.60 0.80 0 -5 0 4.50 0.80 0 -5 0 3.70 0.60 0 -5 0 3.70 0.60 0 -5 0 3.10 0.70 0 -5 0 3.20 0.60 0 -5 0 2.70 0.40 0 5 0 3.30 0.60 0 5 0 3.70 0.50 0 5 0 2.50 0.40 0 5 0 3.40 0.40 0 5 0 4.10 1.00 0 5 0 4.20 0.60 0 5 0 2.90 0.70 -1 -5 0 214.18 8.80 -2 -5 0 41.30 1.90 -2 -5 0 41.80 1.80 -2 -5 0 38.80 2.10 -2 -5 0 42.20 2.00 2 5 0 40.40 2.00 2 5 0 46.30 2.50 2 5 0 44.20 1.90 2 5 0 41.00 2.00 2 5 0 40.30 2.70 2 5 0 41.80 2.20 2 5 0 41.60 2.10 -3 -5 0 10.50 0.60 -3 -5 0 10.80 0.70 -3 -5 0 9.60 0.80 -3 -5 0 8.90 0.90 -3 -5 0 9.80 0.70 3 5 0 10.20 1.00 3 5 0 11.60 1.10 3 5 0 9.00 1.10 3 5 0 9.80 1.10 3 5 0 9.60 0.90 3 5 0 12.00 1.70 3 5 0 10.40 1.30 3 5 0 10.20 1.00 3 5 0 9.70 1.20 3 5 0 11.20 1.00 -4 -5 0 114.69 4.90 -4 -5 0 115.79 4.90 -4 -5 0 119.39 5.40 -4 -5 0 114.39 5.40 4 5 0 123.29 5.80 4 5 0 115.39 5.60 4 5 0 115.19 5.50 4 5 0 125.39 5.30 4 5 0 120.19 5.90 4 5 0 114.09 5.50 4 5 0 115.49 5.40 -5 -5 0 21.80 1.40 -5 -5 0 23.30 1.20 -5 -5 0 28.10 2.30 5 5 0 23.20 2.00 5 5 0 25.50 1.90 5 5 0 23.40 2.40 5 5 0 24.50 2.10 5 5 0 24.30 2.40 5 5 0 22.10 2.50 5 5 0 21.30 2.30 5 5 0 22.30 2.10 5 5 0 22.60 2.00 -6 -5 0 9.10 0.80 -6 -5 0 14.10 2.40 6 5 0 8.00 1.30 6 5 0 9.90 1.50 6 5 0 10.20 1.60 6 5 0 9.40 1.50 6 5 0 11.30 1.90 -7 -5 0 0.40 0.50 -7 -5 0 -0.90 0.70 7 5 0 -0.10 0.90 7 5 0 0.20 1.00 7 5 0 0.00 1.00 7 5 0 0.30 1.20 7 5 0 0.50 1.10 5 -6 0 3.10 2.10 5 -6 0 1.80 1.80 5 -6 0 2.90 1.80 -5 6 0 1.80 1.10 -5 6 0 2.90 1.40 -5 6 0 4.50 1.20 -5 6 0 2.30 1.00 -5 6 0 3.60 1.00 4 -6 0 2.20 1.10 4 -6 0 2.40 1.10 4 -6 0 0.60 1.10 4 -6 0 1.20 1.20 4 -6 0 2.70 1.30 -4 6 0 3.40 0.90 -4 6 0 1.80 1.30 -4 6 0 2.40 0.90 -4 6 0 2.90 1.00 -4 6 0 2.20 1.00 -4 6 0 1.60 0.80 3 -6 0 -0.20 1.00 3 -6 0 -1.40 0.70 3 -6 0 0.70 0.80 3 -6 0 -0.10 0.80 3 -6 0 -0.70 0.80 3 -6 0 0.20 0.90 -3 6 0 1.20 0.70 -3 6 0 -0.10 0.60 -3 6 0 0.90 1.60 -3 6 0 0.30 0.60 -3 6 0 0.30 0.70 -3 6 0 0.50 0.60 2 -6 0 5.60 1.30 2 -6 0 10.10 1.80 2 -6 0 5.20 1.00 2 -6 0 5.60 0.90 2 -6 0 5.00 1.00 2 -6 0 6.80 1.10 -2 6 0 6.80 0.90 -2 6 0 6.50 1.00 -2 6 0 5.80 1.10 -2 6 0 7.60 0.90 -2 6 0 6.80 0.90 -2 6 0 6.00 1.00 1 -6 0 101.09 4.80 1 -6 0 97.19 4.40 1 -6 0 98.39 4.40 1 -6 0 95.79 4.70 1 -6 0 94.29 4.30 -1 6 0 90.69 4.60 -1 6 0 98.79 4.20 -1 6 0 85.89 4.30 -1 6 0 100.39 4.50 -1 6 0 94.89 4.20 -1 6 0 101.79 4.60 0 -6 0 12.90 1.20 0 -6 0 12.40 1.30 0 -6 0 14.40 1.00 0 -6 0 12.90 1.00 0 -6 0 15.10 0.90 0 -6 0 15.10 1.20 0 6 0 13.30 1.10 0 6 0 12.80 0.70 0 6 0 14.40 1.00 0 6 0 13.70 0.90 0 6 0 14.40 1.20 0 6 0 12.30 1.50 0 6 0 14.30 1.00 1 6 0 337.97 42.90 -2 -6 0 13.90 0.90 -2 -6 0 12.90 0.70 -2 -6 0 13.20 1.10 -2 -6 0 14.10 0.80 -2 -6 0 13.40 0.90 -2 -6 0 11.70 1.00 2 6 0 13.90 0.90 2 6 0 14.20 1.20 2 6 0 15.30 1.50 2 6 0 12.80 1.00 2 6 0 15.90 1.40 2 6 0 14.10 1.10 -3 -6 0 58.89 2.60 -3 -6 0 55.89 2.70 -3 -6 0 56.69 2.40 -3 -6 0 55.49 2.60 -3 -6 0 58.29 2.40 -3 -6 0 55.09 2.60 3 6 0 55.59 3.00 3 6 0 55.39 2.70 3 6 0 58.29 3.60 3 6 0 59.39 2.70 3 6 0 59.19 3.30 3 6 0 55.49 3.10 3 6 0 55.19 2.90 -4 -6 0 25.50 1.40 -4 -6 0 28.60 1.90 -4 -6 0 24.40 1.50 -4 -6 0 26.50 1.30 -4 -6 0 24.30 1.30 4 6 0 26.00 1.90 4 6 0 29.60 1.90 4 6 0 26.60 1.70 4 6 0 28.10 1.80 4 6 0 23.30 2.00 4 6 0 30.50 2.20 4 6 0 25.40 2.30 4 6 0 26.10 2.70 4 6 0 30.00 1.80 -5 -6 0 5.50 0.60 -5 -6 0 6.50 0.80 5 6 0 5.10 0.90 5 6 0 2.60 1.30 5 6 0 5.40 1.10 5 6 0 3.20 1.00 5 6 0 7.60 1.40 5 6 0 6.50 2.60 5 6 0 6.40 1.30 5 6 0 9.10 1.30 -6 -6 0 30.70 1.50 -6 -6 0 31.10 1.80 6 6 0 32.90 2.30 6 6 0 31.40 2.90 6 6 0 32.50 2.40 6 6 0 31.00 2.20 6 6 0 31.90 2.50 6 6 0 28.10 2.80 7 6 0 8.80 1.50 7 6 0 12.70 1.90 7 6 0 13.10 2.20 5 -7 0 18.80 3.20 5 -7 0 14.70 2.50 -5 7 0 10.30 1.40 -5 7 0 8.90 1.50 4 -7 0 0.30 1.20 4 -7 0 -1.30 1.40 4 -7 0 1.00 1.10 -4 7 0 1.10 1.40 -4 7 0 -0.10 0.80 -4 7 0 0.30 0.90 -4 7 0 -0.30 0.80 -4 7 0 -0.10 0.60 -4 7 0 -0.40 0.80 3 -7 0 13.60 1.60 3 -7 0 13.00 1.90 3 -7 0 8.90 1.60 3 -7 0 14.30 1.80 3 -7 0 13.70 2.00 3 -7 0 12.90 1.60 -3 7 0 18.00 2.40 -3 7 0 11.20 1.40 -3 7 0 11.30 1.20 -3 7 0 13.30 1.70 -3 7 0 12.90 1.40 -3 7 0 12.80 1.30 2 -7 0 33.70 2.40 2 -7 0 33.80 2.40 2 -7 0 32.10 2.40 2 -7 0 31.60 3.20 -2 7 0 33.30 2.00 -2 7 0 33.00 2.20 -2 7 0 34.00 2.20 -2 7 0 31.10 1.80 1 -7 0 8.20 1.00 1 -7 0 13.80 1.80 1 -7 0 8.90 1.10 1 -7 0 10.60 1.30 1 -7 0 9.40 1.20 -1 7 0 9.70 1.30 -1 7 0 9.60 1.10 -1 7 0 10.30 0.70 -1 7 0 11.30 1.10 -1 7 0 10.90 1.20 -1 7 0 13.50 1.70 0 -7 0 -0.20 0.30 0 -7 0 0.00 0.50 0 -7 0 -0.10 0.50 0 -7 0 -0.70 0.70 0 -7 0 -0.20 0.40 0 -7 0 0.90 0.70 0 7 0 0.10 0.90 0 7 0 0.40 0.40 0 7 0 0.10 0.50 0 7 0 0.40 0.40 0 7 0 0.90 0.60 0 7 0 0.40 0.50 0 7 0 0.20 0.50 -1 -7 0 23.70 1.60 -1 -7 0 26.00 1.80 -1 -7 0 27.40 1.60 -1 -7 0 24.40 1.60 1 7 0 22.80 1.40 1 7 0 22.20 1.40 1 7 0 26.30 2.00 1 7 0 22.20 1.30 -2 -7 0 8.10 0.90 -2 -7 0 9.10 0.70 -2 -7 0 10.80 1.50 -2 -7 0 9.10 1.10 2 7 0 11.50 1.60 2 7 0 8.40 1.00 2 7 0 9.90 0.90 2 7 0 9.40 1.30 2 7 0 9.00 0.90 -3 -7 0 7.80 0.60 -3 -7 0 7.40 0.80 -3 -7 0 7.40 0.80 -3 -7 0 7.30 0.90 -3 -7 0 7.50 0.80 3 7 0 6.60 1.00 3 7 0 7.60 1.10 3 7 0 8.20 0.90 3 7 0 10.60 1.70 3 7 0 8.40 1.30 3 7 0 6.20 1.60 -4 -7 0 26.30 1.50 -4 -7 0 25.60 1.60 -4 -7 0 26.40 1.30 4 7 0 21.70 2.10 4 7 0 26.40 1.80 4 7 0 27.20 1.70 4 7 0 24.00 2.30 4 7 0 26.60 2.00 4 7 0 23.20 1.90 4 7 0 27.90 2.90 -5 -7 0 11.60 0.70 5 7 0 10.10 2.00 5 7 0 11.30 2.00 5 7 0 12.90 1.50 5 7 0 8.80 1.40 5 7 0 11.10 1.50 5 7 0 12.10 1.60 5 7 0 10.60 1.50 6 7 0 2.00 1.00 6 7 0 1.60 1.50 6 7 0 3.40 1.60 6 7 0 1.90 2.80 7 7 0 1.70 1.00 7 7 0 0.80 1.20 7 7 0 0.70 1.00 4 -8 0 -1.20 3.10 -4 8 0 -1.40 1.70 -4 8 0 0.50 1.00 -4 8 0 0.00 1.10 -4 8 0 0.30 1.00 3 -8 0 6.10 1.60 3 -8 0 7.80 2.50 -3 8 0 3.90 1.90 -3 8 0 5.90 1.30 -3 8 0 3.30 1.20 -3 8 0 6.20 1.10 2 -8 0 5.20 1.20 2 -8 0 5.30 1.30 2 -8 0 3.20 1.30 2 -8 0 2.70 1.00 2 -8 0 5.10 1.60 2 -8 0 3.90 1.20 -2 8 0 4.60 1.30 -2 8 0 5.00 1.10 -2 8 0 3.10 0.80 -2 8 0 3.70 1.00 1 -8 0 148.49 7.00 1 -8 0 145.49 6.70 1 -8 0 144.69 7.10 1 -8 0 150.08 6.80 1 -8 0 150.38 6.70 1 -8 0 138.49 6.40 -1 8 0 139.49 6.60 -1 8 0 153.78 6.60 -1 8 0 137.09 6.20 -1 8 0 128.09 6.70 -1 8 0 148.59 6.90 0 -8 0 10.80 1.90 0 -8 0 5.80 1.00 0 -8 0 10.10 1.30 0 -8 0 6.30 0.80 0 -8 0 8.40 1.10 0 -8 0 8.00 1.30 0 8 0 6.30 0.80 0 8 0 10.70 2.00 0 8 0 10.40 1.50 0 8 0 6.80 0.90 0 8 0 7.40 1.00 0 8 0 6.30 0.80 -1 -8 0 8.40 1.10 -1 -8 0 7.50 1.10 -1 -8 0 11.60 2.40 -1 -8 0 10.90 1.30 -1 -8 0 7.90 0.80 -1 -8 0 8.30 1.20 1 8 0 7.10 0.90 1 8 0 10.60 1.90 1 8 0 5.90 1.00 1 8 0 5.50 1.20 -2 -8 0 52.59 2.70 -2 -8 0 52.69 2.80 -2 -8 0 52.59 2.80 2 8 0 53.19 2.70 2 8 0 47.10 2.60 2 8 0 52.39 2.60 2 8 0 52.69 3.40 2 8 0 52.09 3.20 2 8 0 51.09 3.70 2 8 0 50.99 2.40 -3 -8 0 39.50 2.20 -3 -8 0 38.70 2.40 -3 -8 0 41.70 1.90 -3 -8 0 39.30 2.10 3 8 0 32.20 2.70 3 8 0 38.60 2.30 3 8 0 37.30 2.30 3 8 0 40.20 2.10 3 8 0 41.10 3.30 3 8 0 38.30 3.00 -4 -8 0 4.10 1.00 -4 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109.59 5.60 0 8 -4 113.79 5.70 0 -8 4 100.09 5.10 0 -8 4 98.79 5.50 0 -8 4 104.89 4.90 0 -8 4 109.69 6.60 0 -8 4 106.49 5.30 -1 8 -4 1.70 0.70 -1 8 -4 0.80 1.10 -1 8 -4 3.90 1.10 -1 8 -4 0.50 0.50 1 -8 4 0.90 0.70 1 -8 4 1.60 1.20 1 -8 4 2.20 1.10 1 -8 4 1.90 1.10 1 -8 4 1.30 1.00 -2 8 -4 20.20 1.80 -2 8 -4 19.20 1.70 -2 8 -4 23.80 2.40 -2 8 -4 17.20 2.10 -2 8 -4 17.40 1.70 2 -8 4 21.80 1.60 2 -8 4 19.50 2.60 2 -8 4 24.00 3.20 2 -8 4 19.00 2.10 2 -8 4 18.70 2.20 -3 8 -4 1.70 1.00 -3 8 -4 0.90 0.80 -3 8 -4 1.20 1.50 -3 8 -4 1.00 1.40 3 -8 4 2.00 1.40 3 -8 4 0.90 1.00 3 -8 4 2.60 1.70 3 -8 4 3.10 1.80 -4 8 -4 1.00 1.10 -4 8 -4 3.00 1.80 4 -8 4 3.60 2.60 7 7 -4 10.60 1.30 6 7 -4 8.40 1.70 6 7 -4 10.70 1.20 6 7 -4 12.60 2.40 6 7 -4 9.60 2.20 6 7 -4 11.80 2.00 5 7 -4 15.80 1.30 5 7 -4 19.00 2.30 5 7 -4 12.50 1.90 5 7 -4 16.60 1.60 5 7 -4 15.20 1.60 5 7 -4 16.70 2.40 5 7 -4 15.50 2.30 -5 -7 4 15.00 1.20 4 7 -4 77.89 3.70 4 7 -4 81.99 4.30 4 7 -4 84.29 4.00 4 7 -4 78.59 5.00 4 7 -4 79.39 3.90 4 7 -4 88.09 4.80 4 7 -4 71.19 4.70 -4 -7 4 76.99 3.90 -4 -7 4 83.29 3.50 -4 -7 4 75.59 3.80 3 7 -4 9.70 1.80 3 7 -4 6.90 0.80 3 7 -4 11.10 1.50 3 7 -4 14.20 2.70 3 7 -4 9.50 1.10 3 7 -4 10.30 1.70 3 7 -4 7.90 1.00 -3 -7 4 8.30 1.00 -3 -7 4 7.40 0.90 -3 -7 4 8.40 1.10 -3 -7 4 7.80 0.90 -3 -7 4 7.40 0.70 2 7 -4 84.49 4.20 2 7 -4 85.19 4.90 2 7 -4 83.69 4.70 2 7 -4 80.49 3.70 2 7 -4 91.89 4.60 -2 -7 4 84.39 4.00 -2 -7 4 85.09 3.90 -2 -7 4 83.89 3.90 -2 -7 4 83.69 4.00 1 7 -4 121.09 5.80 1 7 -4 114.49 5.30 1 7 -4 118.59 5.30 1 7 -4 115.89 5.90 -1 -7 4 115.69 5.30 -1 -7 4 108.59 5.60 -1 -7 4 118.39 5.30 -1 -7 4 115.29 5.30 0 7 -4 5.60 0.90 0 7 -4 9.40 1.70 0 7 -4 7.60 0.90 0 7 -4 5.50 1.00 0 7 -4 7.50 1.40 0 -7 4 5.80 1.30 0 -7 4 7.60 1.20 0 -7 4 8.50 1.30 0 -7 4 6.50 1.30 0 -7 4 6.90 1.10 0 -7 4 5.30 0.80 -1 7 -4 48.10 2.60 -1 7 -4 55.59 3.00 -1 7 -4 44.20 2.70 1 -7 4 48.70 3.00 1 -7 4 47.40 2.90 1 -7 4 46.10 2.70 1 -7 4 50.69 3.10 -2 7 -4 0.70 0.80 -2 7 -4 0.20 0.70 -2 7 -4 -0.10 0.60 -2 7 -4 0.10 0.80 -2 7 -4 0.40 0.50 2 -7 4 1.40 1.10 2 -7 4 0.60 0.80 2 -7 4 0.90 1.10 2 -7 4 0.40 1.10 2 -7 4 0.30 0.70 2 -7 4 0.30 0.60 -3 7 -4 30.50 2.40 -3 7 -4 32.70 2.20 -3 7 -4 27.70 2.60 -3 7 -4 31.80 1.70 -3 7 -4 35.80 2.90 3 -7 4 38.50 4.60 3 -7 4 31.20 2.80 3 -7 4 29.00 2.60 3 -7 4 33.90 3.10 -4 7 -4 0.40 0.60 -4 7 -4 0.30 0.90 -4 7 -4 1.30 1.00 -4 7 -4 0.10 0.90 -4 7 -4 -0.60 1.70 4 -7 4 1.40 1.60 4 -7 4 0.90 1.80 4 -7 4 1.50 2.70 7 6 -4 12.60 1.30 7 6 -4 12.40 1.50 6 6 -4 -0.10 1.60 6 6 -4 -1.30 1.00 6 6 -4 0.60 0.80 6 6 -4 -0.50 1.40 6 6 -4 -1.10 1.10 6 6 -4 0.20 0.80 6 6 -4 0.30 0.80 6 6 -4 -0.20 0.80 6 6 -4 0.20 0.70 5 6 -4 0.60 0.80 5 6 -4 0.10 0.70 5 6 -4 0.80 1.20 5 6 -4 0.20 1.00 5 6 -4 0.40 0.70 5 6 -4 0.90 1.10 5 6 -4 0.80 0.70 5 6 -4 0.50 1.30 5 6 -4 0.80 0.80 4 6 -4 0.20 0.60 4 6 -4 0.30 0.80 4 6 -4 -0.20 1.60 4 6 -4 0.20 0.60 4 6 -4 -0.30 0.90 4 6 -4 0.10 0.70 4 6 -4 0.50 1.50 4 6 -4 0.50 0.60 4 6 -4 -0.10 0.50 4 6 -4 -0.30 0.80 -4 -6 4 0.20 0.60 -4 -6 4 0.50 0.40 3 6 -4 59.69 2.80 3 6 -4 56.89 3.60 3 6 -4 60.49 3.30 3 6 -4 58.89 2.80 3 6 -4 59.69 2.90 3 6 -4 55.39 3.70 3 6 -4 66.79 3.60 3 6 -4 62.09 3.10 -3 -6 4 58.19 2.70 -3 -6 4 59.59 2.90 -3 -6 4 58.19 2.80 2 6 -4 7.10 1.00 2 6 -4 7.30 0.80 2 6 -4 6.20 1.20 2 6 -4 10.40 1.40 2 6 -4 7.60 0.90 2 6 -4 7.60 0.70 -2 -6 4 7.20 0.90 -2 -6 4 10.00 1.60 -2 -6 4 8.00 0.80 -2 -6 4 8.00 0.70 -2 -6 4 7.70 0.90 1 6 -4 20.90 1.10 1 6 -4 21.40 1.50 -1 -6 4 22.20 1.40 -1 -6 4 20.80 1.50 0 6 -4 47.20 2.20 0 6 -4 50.09 2.90 0 6 -4 49.90 2.70 0 6 -4 50.09 2.40 0 6 -4 53.49 3.10 0 6 -4 47.10 2.50 0 -6 4 49.60 2.70 0 -6 4 47.10 3.00 0 -6 4 51.99 2.50 0 -6 4 51.89 2.70 0 -6 4 50.79 2.60 0 -6 4 52.19 2.80 -1 6 -4 12.50 1.20 -1 6 -4 13.30 1.20 -1 6 -4 13.90 1.20 1 -6 4 11.70 1.30 1 -6 4 12.90 1.40 1 -6 4 11.70 1.20 1 -6 4 12.30 1.00 1 -6 4 13.00 1.60 1 -6 4 13.50 1.50 -2 6 -4 26.50 2.00 -2 6 -4 28.10 1.50 -2 6 -4 28.00 2.30 -2 6 -4 29.50 1.90 2 -6 4 26.60 2.10 2 -6 4 26.80 2.30 2 -6 4 27.40 2.50 2 -6 4 25.90 1.90 2 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2.50 4 5 -4 34.80 1.90 4 5 -4 33.20 2.10 4 5 -4 34.90 2.60 4 5 -4 33.30 2.00 -4 -5 4 33.80 1.90 -4 -5 4 32.70 1.60 3 5 -4 4.30 0.70 3 5 -4 3.80 0.80 3 5 -4 6.40 1.50 3 5 -4 6.00 0.80 3 5 -4 5.00 0.70 3 5 -4 4.20 0.80 3 5 -4 5.10 1.20 3 5 -4 5.40 0.80 3 5 -4 5.30 0.70 3 5 -4 6.10 1.20 -3 -5 4 4.70 0.50 -3 -5 4 4.60 0.50 -3 -5 4 4.00 0.60 2 5 -4 33.80 1.70 2 5 -4 32.30 2.60 2 5 -4 34.20 2.30 2 5 -4 31.50 1.80 2 5 -4 32.60 1.60 2 5 -4 36.90 2.30 2 5 -4 33.80 1.70 2 5 -4 34.60 2.00 2 5 -4 34.20 1.80 -2 -5 4 34.00 1.80 -2 -5 4 33.00 1.60 -2 -5 4 34.50 1.70 1 5 -4 1.90 0.60 1 5 -4 1.80 0.30 -1 -5 4 2.00 0.50 -1 -5 4 2.00 0.50 -1 -5 4 1.10 0.30 -1 -5 4 1.70 0.50 0 5 -4 29.40 1.70 0 5 -4 32.40 2.20 0 5 -4 29.00 1.80 0 5 -4 29.00 1.60 0 5 -4 29.30 1.40 0 5 -4 33.00 1.70 0 -5 4 31.60 1.80 0 -5 4 33.90 1.70 0 -5 4 28.60 1.80 0 -5 4 30.10 1.80 0 -5 4 32.20 1.90 0 -5 4 27.60 2.00 -1 5 -4 137.49 6.50 -1 5 -4 159.28 6.80 -1 5 -4 167.78 6.90 1 -5 4 151.08 6.50 1 -5 4 163.48 7.20 -2 5 -4 54.99 2.80 -2 5 -4 50.39 2.70 -2 5 -4 51.49 2.40 -2 5 -4 50.59 3.00 -2 5 -4 53.19 2.60 2 -5 4 50.19 2.70 2 -5 4 49.60 2.90 2 -5 4 54.19 3.10 2 -5 4 51.59 3.20 2 -5 4 45.10 2.40 2 -5 4 48.40 2.50 2 -5 4 50.79 3.00 -3 5 -4 25.50 2.10 -3 5 -4 26.70 1.90 -3 5 -4 23.70 2.40 -3 5 -4 28.10 1.90 -3 5 -4 28.90 1.70 -3 5 -4 24.70 1.70 3 -5 4 27.80 3.30 3 -5 4 27.70 1.90 3 -5 4 23.70 2.10 3 -5 4 25.20 2.40 3 -5 4 26.80 2.50 -4 5 -4 37.00 2.70 -4 5 -4 38.20 2.20 -4 5 -4 38.90 2.40 -4 5 -4 39.80 3.10 -4 5 -4 40.20 2.50 -4 5 -4 40.10 2.40 4 -5 4 38.10 3.20 4 -5 4 40.50 3.20 4 -5 4 37.50 3.40 4 -5 4 36.00 2.80 -5 5 -4 21.20 2.00 -5 5 -4 20.00 2.40 -5 5 -4 18.20 1.70 -5 5 -4 20.20 2.10 -5 5 -4 24.80 3.00 -5 5 -4 18.50 1.50 5 -5 4 17.00 3.20 5 -5 4 18.80 2.60 7 4 -4 38.90 2.80 7 4 -4 39.50 2.80 7 4 -4 43.00 2.40 7 4 -4 40.10 2.80 6 4 -4 81.19 4.80 6 4 -4 82.49 4.60 6 4 -4 86.19 4.50 6 4 -4 92.69 4.30 6 4 -4 87.99 4.50 6 4 -4 85.29 4.50 6 4 -4 90.99 4.50 6 4 -4 90.69 4.30 -6 -4 4 79.89 4.10 5 4 -4 0.10 1.20 5 4 -4 -0.30 1.00 5 4 -4 0.00 0.80 5 4 -4 0.70 0.80 5 4 -4 0.10 0.90 5 4 -4 -0.30 0.80 5 4 -4 0.80 0.70 5 4 -4 0.60 0.80 5 4 -4 -0.40 1.00 5 4 -4 0.10 1.30 -5 -4 4 -0.30 0.50 4 4 -4 0.50 0.60 4 4 -4 0.40 0.60 4 4 -4 0.90 0.90 4 4 -4 0.40 0.60 4 4 -4 1.10 0.70 4 4 -4 0.30 0.60 4 4 -4 0.60 1.00 4 4 -4 0.00 0.60 4 4 -4 0.00 0.60 4 4 -4 0.80 0.80 -4 -4 4 0.00 0.30 -4 -4 4 0.50 0.60 3 4 -4 1.90 0.60 3 4 -4 1.50 0.60 3 4 -4 1.60 0.70 3 4 -4 1.60 0.60 3 4 -4 1.00 0.50 3 4 -4 2.00 0.60 3 4 -4 2.30 0.60 3 4 -4 2.00 1.00 3 4 -4 1.70 0.60 3 4 -4 1.00 0.60 3 4 -4 0.10 0.70 -3 -4 4 1.20 0.30 -3 -4 4 1.90 0.50 -3 -4 4 2.20 0.50 -3 -4 4 2.00 0.40 -2 -4 4 177.78 7.30 1 4 -4 7.00 0.80 1 4 -4 7.20 0.50 -1 -4 4 6.80 0.70 -1 -4 4 8.10 0.60 -1 -4 4 8.40 0.70 -1 -4 4 7.00 0.70 0 4 -4 836.52 68.09 0 -4 4 784.22 54.99 1 -4 4 262.47 33.20 -2 4 -4 126.29 5.60 -2 4 -4 125.69 5.70 -2 4 -4 121.69 5.30 2 -4 4 121.49 5.30 2 -4 4 116.29 5.70 2 -4 4 120.89 5.80 2 -4 4 118.39 5.20 2 -4 4 131.39 5.70 2 -4 4 124.59 5.70 2 -4 4 123.29 5.50 -3 4 -4 34.20 2.00 -3 4 -4 35.10 2.00 -3 4 -4 34.20 2.10 -3 4 -4 35.90 2.10 -3 4 -4 37.40 2.30 -3 4 -4 34.80 2.40 3 -4 4 31.70 2.30 3 -4 4 33.40 1.90 3 -4 4 36.80 2.60 3 -4 4 36.10 2.60 3 -4 4 39.30 1.90 3 -4 4 36.00 2.10 3 -4 4 36.10 2.60 -4 4 -4 68.19 3.40 -4 4 -4 63.79 3.40 -4 4 -4 63.99 3.20 -4 4 -4 68.49 3.70 -4 4 -4 69.29 3.50 -4 4 -4 69.89 4.00 4 -4 4 65.89 3.50 4 -4 4 62.99 4.10 4 -4 4 59.29 3.70 4 -4 4 67.69 4.10 4 -4 4 65.49 5.30 -5 4 -4 14.30 1.80 -5 4 -4 12.80 2.90 -5 4 -4 14.40 1.50 -5 4 -4 12.40 1.90 -5 4 -4 8.70 1.50 -5 4 -4 11.60 1.50 5 -4 4 15.70 3.30 5 -4 4 9.60 3.00 -6 4 -4 2.10 0.90 -6 4 -4 0.70 1.90 -6 4 -4 1.00 1.20 -6 4 -4 0.70 0.80 -6 4 -4 -1.30 1.30 6 -4 4 0.20 1.80 6 -4 4 -0.40 2.30 6 -4 4 -0.50 1.40 7 3 -4 22.70 2.40 7 3 -4 20.80 1.90 7 3 -4 21.10 2.30 7 3 -4 20.90 2.30 6 3 -4 8.70 1.50 6 3 -4 13.50 1.40 6 3 -4 10.90 1.70 6 3 -4 8.00 1.50 6 3 -4 12.40 1.70 6 3 -4 10.40 1.60 -6 -3 4 11.20 0.90 -6 -3 4 12.20 1.30 5 3 -4 0.80 1.00 5 3 -4 2.10 1.20 5 3 -4 3.50 1.00 5 3 -4 1.30 1.10 5 3 -4 1.70 1.10 5 3 -4 2.90 1.10 5 3 -4 3.50 1.10 5 3 -4 1.80 0.80 5 3 -4 2.10 1.20 5 3 -4 2.60 0.90 -5 -3 4 3.40 0.80 -5 -3 4 4.70 1.20 -5 -3 4 2.60 0.40 4 3 -4 6.80 1.10 4 3 -4 5.10 1.00 4 3 -4 5.20 1.00 4 3 -4 6.80 1.00 4 3 -4 6.40 1.00 4 3 -4 5.20 1.20 4 3 -4 5.70 1.10 4 3 -4 4.70 0.80 4 3 -4 5.70 1.10 4 3 -4 5.90 1.30 4 3 -4 6.00 0.90 -4 -3 4 5.70 0.90 -4 -3 4 8.10 1.50 3 3 -4 37.90 2.10 3 3 -4 38.60 2.60 3 3 -4 43.60 2.30 3 3 -4 38.60 2.10 3 3 -4 38.90 2.50 3 3 -4 38.80 2.00 3 3 -4 42.60 2.40 3 3 -4 45.00 2.70 3 3 -4 39.00 2.10 3 3 -4 37.60 2.10 -3 -3 4 40.20 2.10 -3 -3 4 38.90 1.70 -3 -3 4 37.50 1.70 2 3 -4 4.40 0.60 2 3 -4 4.40 0.60 2 3 -4 4.40 0.80 2 3 -4 4.80 0.70 2 3 -4 6.40 0.70 2 3 -4 6.70 0.70 2 3 -4 5.50 0.70 2 3 -4 5.40 0.60 2 3 -4 5.90 0.70 2 3 -4 4.90 0.90 2 3 -4 4.60 1.00 -2 -3 4 4.90 0.40 -2 -3 4 5.30 0.60 1 3 -4 44.70 2.20 1 3 -4 43.30 1.90 1 3 -4 43.80 2.10 1 3 -4 40.60 1.90 -1 -3 4 43.00 1.90 -1 -3 4 37.60 2.20 -1 -3 4 40.70 1.90 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21.20 1.00 1 2 -4 23.00 1.40 1 2 -4 21.50 1.00 1 2 -4 20.60 1.10 1 2 -4 21.10 1.10 1 2 -4 20.10 1.20 -1 -2 4 21.00 1.20 -1 -2 4 21.90 1.00 -1 -2 4 22.60 1.10 -1 -2 4 22.50 1.10 -1 -2 4 20.10 1.00 0 2 -4 5.00 0.60 0 2 -4 4.60 0.40 0 2 -4 4.80 0.40 0 2 -4 4.50 0.30 0 2 -4 5.40 0.50 0 2 -4 5.50 0.60 0 2 -4 5.20 0.70 0 2 -4 5.20 0.60 0 -2 4 4.40 0.50 0 -2 4 4.60 0.60 0 -2 4 4.60 0.70 0 -2 4 4.40 0.40 0 -2 4 5.30 0.60 0 -2 4 4.70 0.50 0 -2 4 4.90 0.60 1 -2 4 138.39 18.70 -2 2 -4 69.39 3.10 -2 2 -4 66.49 3.30 -2 2 -4 72.69 3.10 -2 2 -4 69.89 3.20 2 -2 4 68.99 3.40 2 -2 4 67.99 3.40 2 -2 4 68.89 3.20 2 -2 4 71.09 3.30 2 -2 4 65.79 3.10 2 -2 4 67.39 3.10 2 -2 4 66.69 3.00 2 -2 4 69.59 3.30 -3 2 -4 208.88 9.30 3 -2 4 214.78 8.90 3 -2 4 206.08 9.40 3 -2 4 217.08 9.20 3 -2 4 216.58 9.10 3 -2 4 214.08 9.30 3 -2 4 221.78 8.80 -4 2 -4 2.20 1.50 -4 2 -4 0.70 0.60 -4 2 -4 0.00 0.60 -4 2 -4 1.10 1.00 -4 2 -4 0.50 0.60 -4 2 -4 1.00 0.70 -4 2 -4 0.10 0.50 4 -2 4 0.40 0.70 4 -2 4 0.60 0.70 4 -2 4 0.00 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2.10 5 5 -7 25.90 2.80 5 5 -7 28.40 1.80 5 5 -7 24.40 2.60 5 5 -7 27.50 1.80 5 5 -7 28.70 2.00 5 5 -7 30.70 4.20 5 5 -7 26.40 1.60 5 5 -7 26.30 2.20 -5 -5 7 29.00 2.90 4 5 -7 11.20 1.60 4 5 -7 6.40 1.20 4 5 -7 6.60 1.10 4 5 -7 8.60 1.60 4 5 -7 7.60 1.50 4 5 -7 7.50 1.50 4 5 -7 9.20 2.00 4 5 -7 7.70 0.90 -4 -5 7 5.60 0.70 -4 -5 7 7.10 0.70 3 5 -7 112.99 5.60 3 5 -7 110.79 4.70 3 5 -7 103.99 5.00 3 5 -7 105.59 4.90 3 5 -7 106.39 5.60 3 5 -7 109.19 5.70 3 5 -7 112.59 5.40 -3 -5 7 109.79 4.80 -3 -5 7 108.19 4.80 -3 -5 7 110.49 4.80 -3 -5 7 109.09 4.70 2 5 -7 138.59 6.30 2 5 -7 133.39 5.70 2 5 -7 120.19 6.00 2 5 -7 130.09 5.60 2 5 -7 132.69 6.30 1 5 -7 5.50 0.90 1 5 -7 9.90 1.40 1 5 -7 6.00 0.70 1 5 -7 7.80 1.00 -1 -5 7 6.30 0.90 -1 -5 7 9.50 1.60 -1 -5 7 5.80 0.70 0 5 -7 360.86 14.90 -1 5 -7 23.10 1.80 -1 5 -7 20.90 1.20 -1 5 -7 21.80 1.60 -1 5 -7 22.00 1.50 1 -5 7 20.20 1.60 1 -5 7 22.70 1.80 1 -5 7 21.30 1.90 1 -5 7 21.30 1.80 -2 5 -7 2.30 0.80 -2 5 -7 3.90 0.60 -2 5 -7 3.30 0.80 2 -5 7 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1.00 5 2 -7 8.60 1.20 5 2 -7 7.40 1.40 -5 -2 7 9.60 1.20 4 2 -7 15.40 1.50 4 2 -7 16.80 1.60 4 2 -7 16.40 1.80 4 2 -7 15.40 1.40 4 2 -7 15.20 1.10 4 2 -7 14.30 1.60 4 2 -7 14.90 1.80 4 2 -7 14.90 1.50 4 2 -7 16.90 1.60 -4 -2 7 16.50 1.00 -4 -2 7 17.10 1.00 -4 -2 7 16.40 1.00 -4 -2 7 16.40 1.40 3 2 -7 155.78 6.50 -3 -2 7 138.69 6.00 -3 -2 7 146.09 6.00 2 2 -7 20.30 1.10 2 2 -7 19.60 1.20 2 2 -7 21.20 1.10 2 2 -7 20.90 1.60 2 2 -7 20.50 1.00 2 2 -7 20.20 1.80 2 2 -7 20.70 1.30 2 2 -7 18.80 1.10 2 2 -7 20.80 1.60 2 2 -7 21.10 1.30 2 2 -7 20.30 1.30 2 2 -7 22.70 1.40 -2 -2 7 20.80 1.10 -2 -2 7 19.30 1.10 -2 -2 7 18.70 1.20 -2 -2 7 19.40 1.10 -2 -2 7 21.50 1.20 1 2 -7 35.80 1.70 1 2 -7 41.30 2.00 1 2 -7 37.50 2.20 1 2 -7 35.30 1.80 1 2 -7 39.30 1.90 1 2 -7 38.90 2.20 1 2 -7 35.30 1.70 1 2 -7 43.20 2.40 1 2 -7 39.20 1.90 -1 -2 7 38.40 2.00 -1 -2 7 35.20 2.00 -1 -2 7 37.70 1.90 -1 -2 7 36.60 1.80 -1 -2 7 39.10 1.90 0 2 -7 44.10 1.90 0 2 -7 46.10 2.20 0 2 -7 44.80 2.30 0 2 -7 44.40 2.30 0 -2 7 44.00 2.10 0 -2 7 43.50 2.30 0 -2 7 43.20 2.40 0 -2 7 46.40 2.20 -1 2 -7 57.49 2.90 -1 2 -7 60.69 2.80 -1 2 -7 59.19 2.50 -1 2 -7 55.89 2.70 -1 2 -7 59.29 2.70 -1 2 -7 58.29 2.60 1 -2 7 57.09 2.90 1 -2 7 55.49 3.00 1 -2 7 58.79 2.90 1 -2 7 57.49 2.90 1 -2 7 59.39 2.80 1 -2 7 56.19 2.80 -2 2 -7 38.20 1.80 -2 2 -7 38.30 1.90 -2 2 -7 35.10 1.90 -2 2 -7 38.70 1.90 -2 2 -7 36.30 2.20 -2 2 -7 32.80 2.10 -2 2 -7 36.80 2.00 2 -2 7 36.70 1.90 2 -2 7 38.90 2.30 2 -2 7 34.70 2.30 2 -2 7 37.50 2.30 2 -2 7 35.80 2.20 2 -2 7 34.20 2.00 2 -2 7 32.80 1.60 -3 2 -7 41.60 2.20 -3 2 -7 41.90 2.10 -3 2 -7 39.20 2.20 -3 2 -7 42.60 2.70 -3 2 -7 44.40 2.40 -3 2 -7 43.40 2.30 -3 2 -7 42.40 2.80 3 -2 7 42.40 2.70 3 -2 7 41.00 2.70 3 -2 7 42.00 2.80 3 -2 7 38.90 2.30 3 -2 7 40.50 2.10 3 -2 7 43.80 2.60 -4 2 -7 109.09 5.20 -4 2 -7 104.39 4.80 -4 2 -7 99.49 5.40 -4 2 -7 106.49 4.70 -4 2 -7 104.39 4.90 -4 2 -7 110.39 5.00 -4 2 -7 113.09 6.50 4 -2 7 97.39 4.80 4 -2 7 106.29 5.50 4 -2 7 103.99 5.60 4 -2 7 102.49 5.30 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17.10 1.80 5 5 -10 11.50 1.90 5 5 -10 17.00 2.50 5 5 -10 17.40 1.90 5 5 -10 9.80 1.80 5 5 -10 14.70 1.70 5 5 -10 15.80 1.50 -5 -5 10 16.30 1.30 4 5 -10 9.90 1.90 4 5 -10 7.00 1.90 4 5 -10 7.50 1.20 4 5 -10 5.60 1.40 4 5 -10 9.30 1.30 4 5 -10 8.30 1.00 -4 -5 10 8.60 1.00 -4 -5 10 7.10 1.10 -4 -5 10 7.00 1.50 3 5 -10 2.50 0.70 3 5 -10 1.80 1.10 3 5 -10 1.20 1.20 3 5 -10 1.50 0.80 3 5 -10 1.20 1.00 -3 -5 10 1.00 0.60 -3 -5 10 0.50 0.60 -3 -5 10 1.40 0.80 -3 -5 10 1.00 0.60 2 5 -10 50.59 2.80 2 5 -10 60.19 3.30 2 5 -10 45.50 4.30 2 5 -10 51.79 3.50 2 5 -10 54.49 3.50 -2 -5 10 49.90 2.80 -2 -5 10 56.89 3.20 -2 -5 10 55.99 2.80 -2 -5 10 54.39 3.00 -2 -5 10 53.89 3.00 1 5 -10 44.80 3.30 1 5 -10 40.30 2.20 1 5 -10 41.50 2.30 1 5 -10 43.50 2.90 -1 -5 10 45.60 2.70 -1 -5 10 41.40 2.50 -1 -5 10 41.40 2.60 0 5 -10 44.30 2.60 0 5 -10 42.50 2.80 0 5 -10 39.90 2.70 0 -5 10 43.40 2.80 0 -5 10 40.90 2.80 0 -5 10 39.80 2.70 0 -5 10 36.60 2.80 0 -5 10 44.00 2.80 -1 5 -10 2.80 1.00 -1 5 -10 2.90 1.00 -1 5 -10 3.40 0.90 -1 5 -10 4.30 1.10 -1 5 -10 3.80 1.20 1 -5 10 2.90 1.00 1 -5 10 3.50 1.20 1 -5 10 4.50 1.50 1 -5 10 3.30 0.90 1 -5 10 3.20 0.90 1 -5 10 4.40 1.60 -2 5 -10 12.50 1.50 -2 5 -10 11.70 1.60 -2 5 -10 14.50 1.10 2 -5 10 13.70 1.70 2 -5 10 14.60 2.10 2 -5 10 12.60 1.50 2 -5 10 14.20 2.20 2 -5 10 8.60 1.50 2 -5 10 11.10 1.80 -3 5 -10 27.30 2.10 -3 5 -10 27.10 2.50 -3 5 -10 30.40 3.40 -3 5 -10 29.90 2.10 3 -5 10 22.60 2.50 3 -5 10 26.50 3.10 3 -5 10 25.90 3.00 3 -5 10 23.70 2.90 -4 5 -10 4.40 1.50 -4 5 -10 2.30 0.80 -4 5 -10 2.50 1.40 -4 5 -10 3.00 2.50 4 -5 10 2.40 2.00 4 -5 10 4.50 3.30 6 4 -10 5.90 1.50 6 4 -10 5.50 1.80 6 4 -10 6.80 1.30 6 4 -10 5.10 1.60 6 4 -10 4.00 1.50 5 4 -10 -0.20 1.20 5 4 -10 1.00 1.00 5 4 -10 0.70 0.70 5 4 -10 0.90 1.00 5 4 -10 0.10 1.10 5 4 -10 0.70 1.30 -5 -4 10 1.10 0.60 -5 -4 10 0.80 1.00 4 4 -10 22.90 2.40 4 4 -10 27.90 2.10 4 4 -10 24.60 1.70 4 4 -10 23.80 2.00 4 4 -10 24.10 2.50 4 4 -10 23.70 2.50 -4 -4 10 24.90 1.80 -4 -4 10 24.10 1.50 -4 -4 10 24.20 2.50 3 4 -10 9.90 1.70 3 4 -10 11.70 1.40 3 4 -10 10.50 1.00 3 4 -10 11.60 2.00 3 4 -10 12.10 1.80 3 4 -10 11.30 1.40 -3 -4 10 9.80 1.00 -3 -4 10 11.00 1.10 -3 -4 10 6.60 1.40 -3 -4 10 11.50 1.30 2 4 -10 218.98 9.60 2 4 -10 232.08 9.60 1 4 -10 68.49 3.70 1 4 -10 64.09 3.10 1 4 -10 63.59 3.10 1 4 -10 68.19 3.70 1 4 -10 73.69 3.50 1 4 -10 60.29 3.20 -1 -4 10 68.29 3.50 -1 -4 10 68.29 3.30 -1 -4 10 62.99 3.50 -1 -4 10 64.69 3.40 -1 -4 10 68.49 3.50 -1 -4 10 67.99 3.30 0 4 -10 64.39 3.10 0 4 -10 69.69 3.70 0 4 -10 65.69 3.60 0 4 -10 66.19 3.40 0 -4 10 61.99 3.50 0 -4 10 61.39 3.60 0 -4 10 69.39 3.60 0 -4 10 67.49 3.40 0 -4 10 69.89 3.60 0 -4 10 65.29 3.40 -1 4 -10 64.79 3.50 -1 4 -10 69.09 3.10 -1 4 -10 63.19 3.50 -1 4 -10 70.99 3.70 1 -4 10 65.69 3.90 1 -4 10 65.99 3.80 1 -4 10 67.79 3.90 1 -4 10 70.49 3.50 1 -4 10 72.99 3.60 1 -4 10 67.99 3.80 -2 4 -10 -0.30 0.70 -2 4 -10 0.80 1.00 -2 4 -10 0.20 1.00 -2 4 -10 -0.10 0.50 2 -4 10 1.00 1.00 2 -4 10 0.50 1.20 2 -4 10 0.00 1.10 2 -4 10 -0.30 0.80 2 -4 10 1.10 1.10 2 -4 10 0.10 0.80 -3 4 -10 13.30 1.10 -3 4 -10 11.70 1.80 -3 4 -10 13.20 1.50 -3 4 -10 16.40 1.80 3 -4 10 14.10 2.30 3 -4 10 10.70 1.80 3 -4 10 9.80 1.60 3 -4 10 11.70 2.00 3 -4 10 14.90 1.50 -4 4 -10 1.20 1.40 -4 4 -10 1.60 1.20 -4 4 -10 1.80 1.00 -4 4 -10 1.40 0.70 4 -4 10 3.00 1.50 4 -4 10 2.50 1.70 4 -4 10 2.50 2.10 -5 4 -10 14.90 2.10 -5 4 -10 17.00 1.50 -5 4 -10 26.10 3.30 5 -4 10 17.80 2.60 5 -4 10 17.60 2.90 6 3 -10 1.30 1.00 6 3 -10 2.70 1.50 6 3 -10 1.60 1.20 6 3 -10 0.60 1.20 6 3 -10 1.40 1.20 6 3 -10 1.80 1.20 -6 -3 10 2.50 0.70 -6 -3 10 0.40 1.90 5 3 -10 0.50 1.10 5 3 -10 0.90 1.10 5 3 -10 0.50 1.20 5 3 -10 0.90 0.90 5 3 -10 -0.80 0.70 5 3 -10 0.20 0.60 5 3 -10 0.00 0.90 -5 -3 10 0.40 0.90 -5 -3 10 0.80 0.60 4 3 -10 14.20 1.80 4 3 -10 15.10 2.10 4 3 -10 14.70 1.80 4 3 -10 15.10 1.20 4 3 -10 18.20 2.00 4 3 -10 14.90 1.50 -4 -3 10 13.70 1.30 -4 -3 10 15.20 1.30 -4 -3 10 16.40 1.80 -4 -3 10 15.30 1.10 3 3 -10 15.20 1.80 3 3 -10 11.90 1.20 3 3 -10 14.10 1.50 3 3 -10 15.60 1.70 3 3 -10 15.50 1.50 3 3 -10 16.40 1.90 -3 -3 10 16.00 1.20 -3 -3 10 16.40 1.90 -3 -3 10 15.40 1.20 -3 -3 10 14.60 1.30 2 3 -10 32.60 2.30 2 3 -10 32.60 2.40 2 3 -10 32.00 2.10 2 3 -10 30.50 1.60 2 3 -10 33.90 2.00 2 3 -10 30.10 1.90 -2 -3 10 33.20 1.80 -2 -3 10 31.60 1.80 -2 -3 10 32.70 2.00 -2 -3 10 33.40 1.80 -1 -3 10 170.58 7.40 -1 -3 10 171.38 7.60 0 3 -10 357.56 14.80 -1 3 -10 1.60 0.70 -1 3 -10 0.60 0.60 -1 3 -10 0.80 0.60 1 -3 10 1.60 0.90 1 -3 10 0.80 0.70 1 -3 10 0.20 0.70 1 -3 10 0.20 0.60 1 -3 10 0.40 0.60 1 -3 10 0.00 0.70 -2 3 -10 17.30 1.50 -2 3 -10 20.60 1.80 -2 3 -10 17.10 1.00 -2 3 -10 20.60 1.70 -2 3 -10 18.50 1.20 2 -3 10 17.00 1.60 2 -3 10 17.90 1.90 2 -3 10 16.40 2.00 2 -3 10 17.50 1.90 2 -3 10 18.40 1.70 2 -3 10 16.40 1.80 2 -3 10 20.30 2.10 -3 3 -10 47.90 2.40 -3 3 -10 47.60 2.80 -3 3 -10 47.10 3.00 -3 3 -10 45.00 2.30 -3 3 -10 48.40 2.50 -3 3 -10 47.20 3.10 3 -3 10 46.70 3.30 3 -3 10 47.50 3.60 3 -3 10 46.80 3.20 3 -3 10 50.59 3.40 -4 3 -10 5.90 0.90 -4 3 -10 4.70 1.30 -4 3 -10 8.80 1.80 -4 3 -10 4.80 1.00 -4 3 -10 6.20 1.10 -4 3 -10 5.70 0.90 4 -3 10 6.40 2.00 4 -3 10 9.00 1.70 4 -3 10 7.30 1.80 -5 3 -10 9.80 2.50 -5 3 -10 7.50 1.00 -5 3 -10 6.60 1.50 -5 3 -10 3.60 1.50 5 -3 10 8.00 1.90 5 -3 10 6.60 2.90 7 2 -10 0.40 1.20 7 2 -10 1.60 1.40 7 2 -10 0.20 1.30 6 2 -10 0.80 0.80 6 2 -10 1.60 1.10 6 2 -10 -0.30 1.10 6 2 -10 0.00 1.00 6 2 -10 0.80 1.30 -6 -2 10 -1.20 1.10 -6 -2 10 -0.10 0.70 -6 -2 10 1.10 1.30 5 2 -10 1.40 1.30 5 2 -10 2.90 1.00 5 2 -10 1.60 1.20 5 2 -10 1.60 0.90 5 2 -10 2.40 1.10 5 2 -10 1.50 1.10 5 2 -10 2.10 0.70 -5 -2 10 3.10 1.10 -5 -2 10 3.20 0.80 4 2 -10 19.00 1.80 4 2 -10 17.70 2.00 4 2 -10 15.60 1.80 4 2 -10 18.20 2.00 4 2 -10 16.10 1.50 4 2 -10 19.50 2.10 4 2 -10 15.10 1.20 4 2 -10 18.60 1.70 -4 -2 10 15.80 1.20 -4 -2 10 15.80 1.70 -4 -2 10 14.40 1.20 -4 -2 10 17.60 1.30 3 2 -10 97.19 4.50 3 2 -10 95.39 5.00 3 2 -10 98.09 4.70 3 2 -10 101.99 4.80 3 2 -10 101.49 5.10 3 2 -10 101.09 4.70 -3 -2 10 97.49 4.50 -3 -2 10 98.89 4.40 -3 -2 10 91.79 4.90 -3 -2 10 92.89 4.40 2 2 -10 187.08 8.00 -2 -2 10 202.48 8.10 1 2 -10 4.00 0.50 1 2 -10 3.60 0.60 1 2 -10 4.20 0.90 1 2 -10 4.90 0.90 -1 -2 10 4.10 0.70 -1 -2 10 4.80 0.90 -1 -2 10 5.10 0.70 -1 -2 10 3.90 0.70 -1 -2 10 5.70 0.80 -1 2 -10 0.80 0.60 -1 2 -10 0.30 0.20 -1 2 -10 0.60 0.50 -1 2 -10 1.10 0.70 -1 2 -10 1.70 0.70 -1 2 -10 0.10 0.30 1 -2 10 0.30 0.70 1 -2 10 1.10 0.70 1 -2 10 0.80 0.50 1 -2 10 -0.30 0.50 1 -2 10 -1.00 0.70 1 -2 10 1.70 0.70 -2 2 -10 13.70 1.20 -2 2 -10 14.50 1.50 -2 2 -10 15.70 1.50 -2 2 -10 14.00 1.10 -2 2 -10 13.20 1.40 -2 2 -10 15.40 1.00 -2 2 -10 13.00 1.00 2 -2 10 13.90 1.40 2 -2 10 14.50 1.70 2 -2 10 14.40 1.60 2 -2 10 14.10 1.50 2 -2 10 13.50 1.70 2 -2 10 12.00 1.60 2 -2 10 12.30 1.30 -3 2 -10 23.80 1.60 -3 2 -10 24.70 1.50 -3 2 -10 25.30 1.80 -3 2 -10 27.60 2.20 -3 2 -10 28.60 2.10 -3 2 -10 27.70 2.30 -3 2 -10 24.40 2.20 3 -2 10 25.20 1.90 3 -2 10 26.10 2.20 3 -2 10 22.80 2.40 3 -2 10 22.70 2.60 -4 2 -10 13.90 1.30 -4 2 -10 13.30 2.20 -4 2 -10 10.60 1.60 -4 2 -10 13.80 1.20 -4 2 -10 13.50 1.20 -4 2 -10 14.50 2.10 -4 2 -10 14.60 1.60 4 -2 10 11.00 2.10 4 -2 10 12.90 2.00 4 -2 10 13.00 1.80 -5 2 -10 0.90 0.70 -5 2 -10 -0.80 1.00 -5 2 -10 0.00 1.10 -5 2 -10 0.60 0.70 -5 2 -10 0.00 1.50 5 -2 10 2.40 1.60 5 -2 10 0.50 1.30 5 -2 10 0.10 1.90 -6 2 -10 -0.40 0.80 -6 2 -10 -0.70 1.10 -6 2 -10 1.30 0.70 6 -2 10 -1.00 2.10 6 -2 10 -1.20 2.30 6 -2 10 0.80 1.90 7 1 -10 1.90 1.60 7 1 -10 1.20 1.50 7 1 -10 1.20 1.30 7 1 -10 0.50 1.30 6 1 -10 5.60 1.10 6 1 -10 4.30 1.40 6 1 -10 10.20 1.70 6 1 -10 4.90 1.60 6 1 -10 7.00 1.80 -6 -1 10 8.80 2.90 -6 -1 10 5.70 1.00 -6 -1 10 6.50 1.70 5 1 -10 1.60 1.00 5 1 -10 0.50 0.60 5 1 -10 -0.60 1.00 5 1 -10 0.30 0.90 5 1 -10 0.10 1.20 5 1 -10 1.40 1.80 5 1 -10 1.10 0.90 -5 -1 10 0.70 0.80 -5 -1 10 0.60 0.70 -5 -1 10 0.20 0.60 4 1 -10 60.09 3.40 4 1 -10 57.89 3.30 4 1 -10 67.99 3.80 4 1 -10 56.29 3.00 4 1 -10 59.39 3.80 4 1 -10 71.69 3.90 -4 -1 10 62.49 3.40 -4 -1 10 64.49 3.10 -4 -1 10 63.89 3.60 -4 -1 10 63.49 3.10 3 1 -10 0.00 0.50 3 1 -10 1.20 0.40 3 1 -10 1.00 0.80 3 1 -10 1.20 0.60 3 1 -10 0.10 0.80 3 1 -10 0.20 0.70 3 1 -10 1.40 0.70 3 1 -10 0.30 0.70 -3 -1 10 1.40 0.60 -3 -1 10 0.70 0.50 -3 -1 10 1.60 0.50 -3 -1 10 2.40 0.90 2 1 -10 0.00 0.40 2 1 -10 0.00 0.30 2 1 -10 0.20 0.60 2 1 -10 0.20 0.40 2 1 -10 0.50 0.50 2 1 -10 0.10 0.50 2 1 -10 0.10 0.50 2 1 -10 0.00 0.60 -2 -1 10 0.20 0.40 -2 -1 10 0.30 0.40 -2 -1 10 0.10 0.40 -2 -1 10 0.40 0.60 -2 -1 10 0.20 0.30 -2 -1 10 0.20 0.50 1 1 -10 31.50 1.80 1 1 -10 26.00 1.40 1 1 -10 28.40 1.50 1 1 -10 26.90 1.50 1 1 -10 27.50 1.80 1 1 -10 25.50 1.40 1 1 -10 26.40 1.80 -1 -1 10 26.70 1.80 -1 -1 10 25.80 1.60 -1 -1 10 26.40 1.90 -1 -1 10 26.70 1.50 -1 -1 10 27.40 1.60 -1 -1 10 28.70 1.70 0 1 -10 15.30 1.10 0 1 -10 14.50 0.80 0 1 -10 16.10 1.20 0 1 -10 14.80 1.30 0 1 -10 14.50 1.20 0 1 -10 18.40 1.20 0 -1 10 15.00 1.20 0 -1 10 14.50 1.40 0 -1 10 15.40 1.20 0 -1 10 14.30 1.20 0 -1 10 15.20 1.20 0 -1 10 15.40 1.50 0 -1 10 15.80 1.30 -1 1 -10 157.18 6.80 -1 1 -10 168.48 6.90 1 -1 10 166.28 7.10 2 -1 10 336.17 42.00 -3 1 -10 13.30 1.50 -3 1 -10 12.60 1.30 -3 1 -10 13.20 1.20 -3 1 -10 11.80 1.60 -3 1 -10 13.20 1.10 -3 1 -10 12.50 1.00 -3 1 -10 12.70 1.80 3 -1 10 9.10 1.50 3 -1 10 11.40 1.30 3 -1 10 12.40 1.60 3 -1 10 12.70 1.80 -4 1 -10 54.69 3.20 -4 1 -10 50.39 3.10 -4 1 -10 52.59 2.70 -4 1 -10 49.99 3.40 -4 1 -10 54.39 3.60 -4 1 -10 54.49 2.60 -4 1 -10 48.60 2.70 4 -1 10 52.09 3.60 4 -1 10 52.39 3.40 4 -1 10 47.30 3.20 -5 1 -10 0.60 1.00 -5 1 -10 1.30 0.80 -5 1 -10 0.20 2.90 -5 1 -10 0.00 0.90 -5 1 -10 0.40 1.50 -5 1 -10 0.60 1.40 -5 1 -10 0.80 0.80 5 -1 10 1.30 1.70 5 -1 10 1.40 1.70 5 -1 10 0.70 2.40 7 0 -10 14.90 1.90 7 0 -10 11.60 1.90 7 0 -10 14.40 2.20 -7 0 10 9.50 1.70 6 0 -10 22.70 2.40 6 0 -10 12.30 1.90 6 0 -10 20.80 2.40 6 0 -10 20.60 1.90 6 0 -10 13.90 1.90 -6 0 10 19.40 1.70 -6 0 10 18.20 3.40 -6 0 10 14.10 1.90 5 0 -10 16.20 1.50 5 0 -10 18.40 2.30 5 0 -10 18.10 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90.59 4.90 0 3 -11 103.29 4.60 0 3 -11 102.79 4.60 0 3 -11 91.19 4.40 0 3 -11 101.59 4.60 0 -3 11 105.79 4.90 0 -3 11 95.09 4.70 0 -3 11 98.39 4.90 0 -3 11 99.49 4.70 0 -3 11 101.99 4.70 0 -3 11 99.09 5.00 -1 3 -11 36.10 1.90 -1 3 -11 40.80 2.00 -1 3 -11 39.50 2.50 -1 3 -11 37.00 2.20 -1 3 -11 37.10 2.40 -1 3 -11 41.70 2.50 1 -3 11 39.10 2.40 1 -3 11 42.60 2.40 1 -3 11 38.20 2.60 1 -3 11 39.30 2.70 1 -3 11 36.00 2.60 1 -3 11 39.90 2.70 -2 3 -11 6.00 1.10 -2 3 -11 6.50 1.10 2 -3 11 4.10 1.20 2 -3 11 8.90 1.30 2 -3 11 5.10 1.20 2 -3 11 4.50 0.90 2 -3 11 3.40 1.20 2 -3 11 5.80 1.30 2 -3 11 6.30 1.50 -3 3 -11 23.00 1.80 -3 3 -11 20.50 2.30 -3 3 -11 20.30 2.00 -3 3 -11 21.50 1.40 3 -3 11 23.20 2.80 3 -3 11 18.50 2.30 3 -3 11 20.00 2.50 3 -3 11 18.90 1.80 3 -3 11 19.50 2.30 -4 3 -11 26.30 2.20 -4 3 -11 27.50 2.70 -4 3 -11 23.50 1.60 -4 3 -11 24.10 2.40 4 -3 11 27.70 2.80 4 -3 11 25.50 2.50 4 -3 11 28.10 3.40 -5 3 -11 0.80 1.30 -5 3 -11 -0.10 1.80 -5 3 -11 3.40 1.70 -5 3 -11 1.00 0.80 5 -3 11 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-22 9.00 1.70 1 0 22 10.10 1.90 1 0 22 6.50 1.50 2 -1 -22 6.90 1.40 2 -1 -22 6.00 1.30 -2 1 22 8.00 1.60 -2 1 22 7.20 1.40 -2 1 22 4.30 1.50 1 -1 -22 8.60 1.50 1 -1 -22 7.60 1.40 -1 1 22 7.60 1.50 -1 1 22 10.10 1.70 -1 1 22 5.30 1.30 -1 1 22 7.50 2.20 0 -1 -22 3.30 1.10 0 -1 -22 3.20 1.10 0 -1 -22 2.30 1.10 0 1 22 2.30 1.50 0 1 22 1.30 1.10 0 1 22 1.80 1.20 0 1 22 1.90 1.20 -1 -1 -22 0.10 0.80 -1 -1 -22 -0.60 0.90 -1 -1 -22 -0.90 1.30 1 1 22 -0.40 1.00 1 1 22 0.00 0.90 -2 -1 -22 2.20 1.40 2 1 22 3.10 1.60 2 1 22 0.50 1.20 2 1 22 0.90 1.40 2 -2 -22 56.39 3.60 2 -2 -22 57.29 4.00 -2 2 22 54.99 3.60 1 -2 -22 1.00 1.00 1 -2 -22 0.90 1.00 1 -2 -22 0.10 1.00 -1 2 22 0.00 1.00 -1 2 22 0.40 1.10 -1 2 22 1.00 1.00 -1 2 22 -0.50 1.50 -1 2 22 0.30 1.00 0 -2 -22 32.90 2.50 0 -2 -22 38.30 2.60 0 -2 -22 35.00 2.50 0 2 22 43.10 3.60 0 2 22 34.40 2.70 0 2 22 36.90 2.80 0 2 22 32.10 2.80 0 2 22 40.70 2.90 -1 -2 -22 0.30 0.90 -1 -2 -22 0.50 1.00 -1 -2 -22 -0.50 0.80 1 2 22 1.00 1.10 1 2 22 1.20 1.30 1 2 22 -0.30 1.40 -2 -2 -22 0.40 0.90 -2 -2 -22 0.30 1.50 2 2 22 1.30 1.50 2 2 22 -0.40 0.80 2 2 22 0.70 1.30 2 -3 -22 4.10 2.00 2 -3 -22 5.80 1.50 -2 3 22 3.00 1.20 1 -3 -22 9.80 1.50 1 -3 -22 16.40 1.70 1 -3 -22 9.50 1.50 -1 3 22 17.80 2.20 -1 3 22 16.00 2.00 -1 3 22 11.40 1.60 -1 3 22 13.70 1.70 0 -3 -22 55.49 3.40 0 -3 -22 56.19 3.50 0 3 22 62.69 3.70 0 3 22 59.49 3.60 0 3 22 55.59 3.60 0 3 22 60.49 4.30 -1 -3 -22 3.50 1.10 -1 -3 -22 3.90 1.20 -1 -3 -22 2.80 0.90 1 3 22 3.50 1.20 1 3 22 4.50 1.40 1 3 22 2.80 1.30 -2 -3 -22 30.60 2.60 2 3 22 33.90 2.80 2 3 22 23.20 3.20 2 3 22 27.10 2.60 2 -4 -22 16.00 1.80 2 -4 -22 20.80 2.30 -2 4 22 12.40 1.90 -2 4 22 19.20 2.40 1 -4 -22 5.40 1.20 1 -4 -22 3.90 1.20 1 -4 -22 2.90 1.10 -1 4 22 6.50 1.50 -1 4 22 5.20 1.40 -1 4 22 8.60 2.20 -1 4 22 10.60 1.80 0 -4 -22 0.70 0.90 0 -4 -22 1.80 1.10 0 -4 -22 0.20 1.00 0 4 22 1.50 1.40 0 4 22 -0.10 1.00 0 4 22 1.40 1.10 0 4 22 0.30 1.00 0 4 22 0.40 1.00 -1 -4 -22 16.80 1.90 -1 -4 -22 17.00 1.80 1 4 22 20.60 2.60 1 4 22 18.40 2.30 1 4 22 15.40 2.00 -2 -4 -22 0.50 1.10 2 4 22 -0.20 2.30 2 4 22 0.90 1.10 2 4 22 2.20 1.30 -3 -4 -22 12.90 2.10 3 4 22 13.20 2.30 1 -5 -22 0.10 1.10 1 -5 -22 0.90 1.10 1 -5 -22 -0.50 0.90 -1 5 22 0.20 1.10 -1 5 22 1.20 1.10 0 -5 -22 3.10 1.30 0 -5 -22 4.10 1.10 0 -5 -22 3.30 1.20 0 5 22 3.40 1.50 0 5 22 3.40 1.60 0 5 22 5.00 1.20 0 5 22 7.40 1.60 -1 -5 -22 0.70 0.80 -1 -5 -22 0.70 1.00 -1 -5 -22 0.90 0.90 1 5 22 0.00 1.20 1 5 22 -0.50 0.90 -2 -5 -22 29.00 2.60 -2 -5 -22 23.40 2.20 2 5 22 27.00 2.50 2 5 22 31.50 3.70 -3 -5 -22 2.20 1.40 -3 -5 -22 0.50 1.10 -3 -5 -22 0.00 1.60 3 5 22 -0.20 2.30 3 5 22 -0.40 1.10 1 -6 -22 0.90 1.10 1 -6 -22 0.70 1.90 1 -6 -22 -0.90 1.20 -1 6 22 1.40 1.60 -1 6 22 0.80 1.70 0 -6 -22 2.20 1.30 0 -6 -22 0.80 1.00 0 -6 -22 0.70 1.00 0 6 22 1.20 1.20 0 6 22 2.10 1.20 0 6 22 4.50 2.00 -1 -6 -22 14.30 1.90 -1 -6 -22 13.40 1.50 1 6 22 18.20 2.10 1 6 22 16.90 2.30 -2 -6 -22 0.30 1.30 -2 -6 -22 0.80 0.90 2 6 22 -0.70 1.20 0 -7 -22 89.29 4.50 0 -7 -22 93.69 5.00 0 7 22 100.29 5.20 0 7 22 95.09 4.80 0 7 22 83.59 5.00 -1 -7 -22 0.00 1.30 -1 -7 -22 -0.20 1.00 -1 -7 -22 0.80 1.10 1 7 22 0.70 1.80 1 7 22 -0.20 1.00 -2 -7 -22 14.50 2.40 -2 -7 -22 8.20 1.40 2 7 22 12.30 2.10 1 -2 -23 1.10 1.10 -1 2 23 1.60 1.20 -1 2 23 2.20 1.20 0 -2 -23 1.20 1.00 0 -2 -23 3.90 1.40 0 -2 -23 2.50 1.10 0 2 23 2.20 1.30 0 2 23 1.10 1.20 -1 -2 -23 5.40 1.50 -1 -2 -23 1.20 1.20 -1 -2 -23 3.40 1.10 1 2 23 1.40 1.10 1 2 23 2.00 1.30 1 -3 -23 11.00 1.60 1 -3 -23 12.80 1.70 -1 3 23 14.10 2.00 -1 3 23 14.20 1.80 0 -3 -23 20.90 3.10 0 -3 -23 14.50 2.00 0 3 23 22.80 1.90 0 3 23 17.50 2.20 -1 -3 -23 1.40 2.10 -1 -3 -23 0.20 0.90 -1 -3 -23 0.30 1.00 1 3 23 1.20 1.80 1 3 23 0.70 1.20 1 -4 -23 22.70 2.20 1 -4 -23 30.20 2.40 1 -4 -23 25.30 2.20 -1 4 23 30.30 2.40 -1 4 23 21.00 2.30 0 -4 -23 6.20 1.60 0 -4 -23 8.90 1.60 0 4 23 9.70 1.40 -1 -4 -23 1.00 1.50 -1 -4 -23 0.30 1.00 -1 -4 -23 0.10 2.30 1 4 23 -0.40 1.20 1 4 23 5.00 1.60 1 4 23 0.80 1.10 0 -5 -23 3.30 1.40 0 -5 -23 4.60 1.30 0 -5 -23 3.60 1.20 0 5 23 7.00 1.30 0 5 23 3.00 1.50 -1 -5 -23 2.20 1.10 -1 -5 -23 2.00 1.10 -1 -5 -23 3.10 1.60 1 5 23 6.50 1.50 1 5 23 4.20 1.20 -1 -6 -23 0.30 1.00 -1 -6 -23 -1.00 0.80 -1 -6 -23 -0.40 1.10 1 6 23 3.40 1.30 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 14934 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl -0.11420(18) 0.97839(9) 0.76188(5) 0.0458(3) Uani 1 1 d . . . . . S1 S 0.45398(13) 0.53745(8) 0.30974(4) 0.0254(2) Uani 1 1 d . . . . . F1 F -0.0535(4) 0.7536(3) 0.33870(12) 0.0420(6) Uani 1 1 d . . . . . O1 O -0.2901(5) 0.7259(5) 0.4781(2) 0.0717(12) Uani 1 1 d . . . . . N1 N 0.0420(4) 0.7589(3) 0.50081(16) 0.0271(6) Uani 1 1 d . . . . . C1 C -0.1845(6) 0.8048(4) 0.6043(2) 0.0348(8) Uani 1 1 d . . . . . H1 H -0.284349 0.761057 0.592246 0.042 Uiso 1 1 calc R U . . . F2 F -0.0332(4) 0.5482(3) 0.40488(14) 0.0474(6) Uani 1 1 d . . . . . O2 O 0.2566(4) 0.5384(3) 0.27689(15) 0.0393(6) Uani 1 1 d . . . . . C2 C -0.2183(7) 0.8576(4) 0.6648(2) 0.0393(9) Uani 1 1 d . . . . . H2 H -0.343026 0.851576 0.693749 0.047 Uiso 1 1 calc R U . . . O3 O 0.5682(5) 0.4151(3) 0.36272(15) 0.0408(7) Uani 1 1 d . . . . . C3 C -0.0713(7) 0.9184(4) 0.6830(2) 0.0363(8) Uani 1 1 d . . . . . O4 O 0.9744(4) 0.5952(2) 0.12210(13) 0.0331(6) Uani 1 1 d . . . . . C4 C 0.1093(6) 0.9305(4) 0.6411(2) 0.0354(8) Uani 1 1 d . . . . . H4 H 0.209841 0.972783 0.654124 0.042 Uiso 1 1 calc R U . . . O5 O 1.1074(4) 0.3747(2) 0.18361(13) 0.0289(5) Uani 1 1 d . . . . . C5 C 0.1422(6) 0.8801(4) 0.5795(2) 0.0314(7) Uani 1 1 d . . . . . H5 H 0.264878 0.889256 0.549933 0.038 Uiso 1 1 calc R U . . . C6 C -0.0026(5) 0.8166(3) 0.56102(18) 0.0279(7) Uani 1 1 d . . . . . C7 C 0.2556(5) 0.7424(4) 0.46703(18) 0.0258(7) Uani 1 1 d . . . . . H7A H 0.372940 0.704139 0.505729 0.031 Uiso 1 1 calc R U . . . H7B H 0.273501 0.830031 0.435206 0.031 Uiso 1 1 calc R U . . . C8 C 0.2583(5) 0.6440(4) 0.42030(19) 0.0274(7) Uani 1 1 d . . . . . H8 H 0.318991 0.549815 0.452105 0.033 Uiso 1 1 calc R U . . . C9 C 0.0220(6) 0.6629(4) 0.4058(2) 0.0342(8) Uani 1 1 d . . . . . C10 C -0.0993(6) 0.7189(5) 0.4668(2) 0.0397(9) Uani 1 1 d . . . . . C11 C 0.4025(5) 0.6705(3) 0.35309(17) 0.0253(7) Uani 1 1 d . . . . . H11A H 0.541704 0.679564 0.369393 0.030 Uiso 1 1 calc R U . . . H11B H 0.330668 0.756600 0.316616 0.030 Uiso 1 1 calc R U . . . C12 C 0.6321(5) 0.5858(3) 0.23609(17) 0.0250(7) Uani 1 1 d . . . . . C13 C 0.5509(6) 0.7223(3) 0.18377(18) 0.0273(7) Uani 1 1 d . . . . . C14 C 0.6736(7) 0.8166(4) 0.1751(2) 0.0390(9) Uani 1 1 d . . . . . H14 H 0.807432 0.792648 0.201864 0.047 Uiso 1 1 calc R U . . . C15 C 0.5992(9) 0.9445(4) 0.1274(3) 0.0509(12) Uani 1 1 d . . . . . H15 H 0.682068 1.008725 0.121563 0.061 Uiso 1 1 calc R U . . . C16 C 0.4068(9) 0.9793(4) 0.0885(2) 0.0546(13) Uani 1 1 d . . . . . H16 H 0.357972 1.067406 0.055552 0.065 Uiso 1 1 calc R U . . . C17 C 0.2832(8) 0.8884(4) 0.0966(2) 0.0470(11) Uani 1 1 d . . . . . H17 H 0.149508 0.913817 0.069574 0.056 Uiso 1 1 calc R U . . . C18 C 0.3548(6) 0.7588(4) 0.14445(19) 0.0345(8) Uani 1 1 d . . . . . H18 H 0.270093 0.695542 0.150228 0.041 Uiso 1 1 calc R U . . . C19 C 0.8150(5) 0.4915(3) 0.23519(18) 0.0260(7) Uani 1 1 d . . . . . H19 H 0.848730 0.413982 0.276927 0.031 Uiso 1 1 calc R U . . . C20 C 0.9699(5) 0.4990(3) 0.17337(18) 0.0262(7) Uani 1 1 d . . . . . C21 C 1.2755(6) 0.3582(3) 0.13302(19) 0.0275(7) Uani 1 1 d . . . . . C22 C 1.4842(6) 0.3265(4) 0.1606(2) 0.0316(8) Uani 1 1 d . . . . . H22 H 1.510978 0.321420 0.210870 0.038 Uiso 1 1 calc R U . . . C23 C 1.6558(6) 0.3020(4) 0.1137(2) 0.0339(8) Uani 1 1 d . . . . . H23 H 1.800830 0.280291 0.131850 0.041 Uiso 1 1 calc R U . . . C24 C 1.6149(6) 0.3092(4) 0.0406(2) 0.0362(8) Uani 1 1 d . . . . . H24 H 1.731985 0.292255 0.008641 0.043 Uiso 1 1 calc R U . . . C25 C 1.4038(6) 0.3411(4) 0.0140(2) 0.0353(8) Uani 1 1 d . . . . . H25 H 1.376412 0.346420 -0.036272 0.042 Uiso 1 1 calc R U . . . C26 C 1.2313(6) 0.3655(4) 0.0605(2) 0.0311(7) Uani 1 1 d . . . . . H26 H 1.086055 0.386793 0.042583 0.037 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0712(7) 0.0342(5) 0.0248(4) -0.0140(4) 0.0095(4) 0.0042(4) S1 0.0310(5) 0.0244(4) 0.0218(4) -0.0085(3) 0.0083(3) -0.0080(3) F1 0.0357(12) 0.0567(14) 0.0328(11) -0.0163(10) -0.0031(9) -0.0056(10) O1 0.0297(16) 0.149(4) 0.068(2) -0.069(2) 0.0218(15) -0.039(2) N1 0.0209(13) 0.0358(15) 0.0264(14) -0.0118(12) 0.0074(11) -0.0080(11) C1 0.0314(18) 0.040(2) 0.0323(18) -0.0120(16) 0.0106(14) -0.0076(15) F2 0.0491(14) 0.0554(15) 0.0555(15) -0.0283(12) 0.0133(11) -0.0324(12) O2 0.0403(15) 0.0516(16) 0.0376(14) -0.0220(13) 0.0127(11) -0.0236(13) C2 0.041(2) 0.039(2) 0.0291(18) -0.0059(16) 0.0155(15) -0.0010(16) O3 0.0490(16) 0.0276(13) 0.0330(14) 0.0010(11) 0.0161(12) -0.0003(11) C3 0.047(2) 0.0294(18) 0.0247(17) -0.0087(14) 0.0060(15) 0.0048(15) O4 0.0399(14) 0.0302(13) 0.0251(12) -0.0055(10) 0.0091(10) -0.0055(10) C4 0.043(2) 0.0307(18) 0.0308(18) -0.0118(15) 0.0019(15) -0.0035(15) O5 0.0332(13) 0.0274(12) 0.0267(12) -0.0106(10) 0.0108(9) -0.0068(10) C5 0.0304(18) 0.0332(18) 0.0297(17) -0.0112(14) 0.0068(13) -0.0050(14) C6 0.0283(17) 0.0292(17) 0.0220(15) -0.0065(13) 0.0045(12) -0.0016(13) C7 0.0199(15) 0.0362(18) 0.0254(16) -0.0136(14) 0.0071(12) -0.0099(13) C8 0.0274(17) 0.0326(17) 0.0258(16) -0.0125(13) 0.0079(13) -0.0102(13) C9 0.0341(19) 0.046(2) 0.0308(18) -0.0176(16) 0.0074(14) -0.0183(16) C10 0.0304(19) 0.063(3) 0.035(2) -0.0245(19) 0.0108(15) -0.0186(18) C11 0.0276(16) 0.0310(17) 0.0208(15) -0.0116(13) 0.0066(12) -0.0099(13) C12 0.0320(17) 0.0278(16) 0.0195(14) -0.0112(12) 0.0072(12) -0.0112(13) C13 0.0371(18) 0.0258(16) 0.0207(15) -0.0117(13) 0.0114(13) -0.0073(13) C14 0.055(2) 0.0342(19) 0.0345(19) -0.0165(16) 0.0168(17) -0.0172(17) C15 0.079(3) 0.030(2) 0.046(2) -0.0126(18) 0.026(2) -0.020(2) C16 0.091(4) 0.0256(19) 0.034(2) -0.0055(16) 0.025(2) 0.001(2) C17 0.066(3) 0.037(2) 0.0225(17) -0.0072(15) 0.0045(17) 0.0111(19) C18 0.042(2) 0.0329(18) 0.0251(17) -0.0106(14) 0.0062(14) -0.0026(15) C19 0.0306(17) 0.0277(16) 0.0204(15) -0.0074(12) 0.0046(12) -0.0085(13) C20 0.0278(17) 0.0295(16) 0.0241(16) -0.0117(13) 0.0037(12) -0.0079(13) C21 0.0320(18) 0.0240(16) 0.0295(17) -0.0122(13) 0.0116(13) -0.0092(13) C22 0.0376(19) 0.0299(17) 0.0314(18) -0.0135(14) 0.0062(14) -0.0113(14) C23 0.0295(18) 0.0328(18) 0.043(2) -0.0152(16) 0.0070(15) -0.0100(14) C24 0.038(2) 0.0328(19) 0.042(2) -0.0190(16) 0.0179(16) -0.0109(15) C25 0.045(2) 0.0357(19) 0.0289(18) -0.0161(15) 0.0091(15) -0.0099(16) C26 0.0323(18) 0.0305(18) 0.0312(18) -0.0118(14) 0.0055(14) -0.0064(14) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0137 0.0067 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3281 0.5435 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0583 0.0400 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0241 0.0134 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0389 0.0241 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.2925 0.4295 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O2 S1 O3 118.11(18) . . ? O2 S1 C11 108.77(16) . . ? O2 S1 C12 108.00(15) . . ? O3 S1 C11 108.15(16) . . ? O3 S1 C12 109.11(16) . . ? C11 S1 C12 103.78(15) . . ? C6 N1 C7 121.0(3) . . ? C10 N1 C6 126.1(3) . . ? C10 N1 C7 112.9(3) . . ? C2 C1 H1 120.2 . . ? C2 C1 C6 119.6(4) . . ? C6 C1 H1 120.2 . . ? C1 C2 H2 120.0 . . ? C3 C2 C1 120.0(3) . . ? C3 C2 H2 120.0 . . ? C2 C3 Cl1 118.7(3) . . ? C2 C3 C4 121.1(3) . . ? C4 C3 Cl1 120.1(3) . . ? C3 C4 H4 120.4 . . ? C3 C4 C5 119.2(4) . . ? C5 C4 H4 120.4 . . ? C20 O5 C21 118.2(3) . . ? C4 C5 H5 119.7 . . ? C6 C5 C4 120.5(3) . . ? C6 C5 H5 119.7 . . ? C1 C6 N1 121.1(3) . . ? C5 C6 N1 119.3(3) . . ? C5 C6 C1 119.5(3) . . ? N1 C7 H7A 110.8 . . ? N1 C7 H7B 110.8 . . ? N1 C7 C8 104.5(3) . . ? H7A C7 H7B 108.9 . . ? C8 C7 H7A 110.8 . . ? C8 C7 H7B 110.8 . . ? C7 C8 H8 108.4 . . ? C9 C8 C7 102.6(3) . . ? C9 C8 H8 108.4 . . ? C9 C8 C11 117.8(3) . . ? C11 C8 C7 110.8(3) . . ? C11 C8 H8 108.4 . . ? F1 C9 C8 113.2(3) . . ? F1 C9 C10 107.7(3) . . ? F2 C9 F1 104.9(3) . . ? F2 C9 C8 114.6(3) . . ? F2 C9 C10 109.7(3) . . ? C8 C9 C10 106.6(3) . . ? O1 C10 N1 129.5(4) . . ? O1 C10 C9 123.3(4) . . ? N1 C10 C9 107.2(3) . . ? S1 C11 H11A 109.3 . . ? S1 C11 H11B 109.3 . . ? C8 C11 S1 111.5(2) . . ? C8 C11 H11A 109.3 . . ? C8 C11 H11B 109.3 . . ? H11A C11 H11B 108.0 . . ? C13 C12 S1 115.5(2) . . ? C19 C12 S1 114.9(2) . . ? C19 C12 C13 129.6(3) . . ? C14 C13 C12 118.9(3) . . ? C18 C13 C12 121.5(3) . . ? C18 C13 C14 119.6(3) . . ? C13 C14 H14 120.2 . . ? C15 C14 C13 119.6(4) . . ? C15 C14 H14 120.2 . . ? C14 C15 H15 119.8 . . ? C16 C15 C14 120.4(4) . . ? C16 C15 H15 119.8 . . ? C15 C16 H16 119.6 . . ? C15 C16 C17 120.8(4) . . ? C17 C16 H16 119.6 . . ? C16 C17 H17 120.1 . . ? C16 C17 C18 119.8(4) . . ? C18 C17 H17 120.1 . . ? C13 C18 C17 119.7(4) . . ? C13 C18 H18 120.2 . . ? C17 C18 H18 120.2 . . ? C12 C19 H19 117.7 . . ? C12 C19 C20 124.6(3) . . ? C20 C19 H19 117.7 . . ? O4 C20 O5 124.6(3) . . ? O4 C20 C19 127.6(3) . . ? O5 C20 C19 107.8(3) . . ? C22 C21 O5 117.0(3) . . ? C22 C21 C26 121.9(3) . . ? C26 C21 O5 121.0(3) . . ? C21 C22 H22 120.5 . . ? C21 C22 C23 119.0(3) . . ? C23 C22 H22 120.5 . . ? C22 C23 H23 120.0 . . ? C24 C23 C22 120.0(4) . . ? C24 C23 H23 120.0 . . ? C23 C24 H24 120.0 . . ? C25 C24 C23 120.1(3) . . ? C25 C24 H24 120.0 . . ? C24 C25 H25 119.8 . . ? C24 C25 C26 120.3(3) . . ? C26 C25 H25 119.8 . . ? C21 C26 C25 118.7(3) . . ? C21 C26 H26 120.7 . . ? C25 C26 H26 120.7 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl1 C3 1.756(4) . ? S1 O2 1.426(3) . ? S1 O3 1.438(3) . ? S1 C11 1.780(3) . ? S1 C12 1.798(3) . ? F1 C9 1.372(4) . ? O1 C10 1.215(5) . ? N1 C6 1.417(4) . ? N1 C7 1.469(4) . ? N1 C10 1.345(5) . ? C1 H1 0.9500 . ? C1 C2 1.389(5) . ? C1 C6 1.400(5) . ? F2 C9 1.363(4) . ? C2 H2 0.9500 . ? C2 C3 1.374(6) . ? C3 C4 1.380(6) . ? O4 C20 1.199(4) . ? C4 H4 0.9500 . ? C4 C5 1.391(5) . ? O5 C20 1.356(4) . ? O5 C21 1.411(4) . ? C5 H5 0.9500 . ? C5 C6 1.386(5) . ? C7 H7A 0.9900 . ? C7 H7B 0.9900 . ? C7 C8 1.541(5) . ? C8 H8 1.0000 . ? C8 C9 1.498(5) . ? C8 C11 1.533(4) . ? C9 C10 1.528(5) . ? C11 H11A 0.9900 . ? C11 H11B 0.9900 . ? C12 C13 1.486(5) . ? C12 C19 1.334(5) . ? C13 C14 1.399(5) . ? C13 C18 1.391(5) . ? C14 H14 0.9500 . ? C14 C15 1.381(6) . ? C15 H15 0.9500 . ? C15 C16 1.370(8) . ? C16 H16 0.9500 . ? C16 C17 1.376(7) . ? C17 H17 0.9500 . ? C17 C18 1.393(5) . ? C18 H18 0.9500 . ? C19 H19 0.9500 . ? C19 C20 1.489(4) . ? C21 C22 1.376(5) . ? C21 C26 1.379(5) . ? C22 H22 0.9500 . ? C22 C23 1.392(5) . ? C23 H23 0.9500 . ? C23 C24 1.385(6) . ? C24 H24 0.9500 . ? C24 C25 1.383(6) . ? C25 H25 0.9500 . ? C25 C26 1.392(5) . ? C26 H26 0.9500 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cl1 C3 C4 C5 178.8(3) . . . . ? S1 C12 C13 C14 121.7(3) . . . . ? S1 C12 C13 C18 -57.3(4) . . . . ? S1 C12 C19 C20 169.7(3) . . . . ? F1 C9 C10 O1 70.1(6) . . . . ? F1 C9 C10 N1 -108.4(3) . . . . ? N1 C7 C8 C9 23.9(3) . . . . ? N1 C7 C8 C11 150.5(3) . . . . ? C1 C2 C3 Cl1 -177.7(3) . . . . ? C1 C2 C3 C4 1.2(6) . . . . ? F2 C9 C10 O1 -43.6(6) . . . . ? F2 C9 C10 N1 138.0(3) . . . . ? O2 S1 C11 C8 67.5(3) . . . . ? O2 S1 C12 C13 60.5(3) . . . . ? O2 S1 C12 C19 -117.3(3) . . . . ? C2 C1 C6 N1 177.2(3) . . . . ? C2 C1 C6 C5 0.4(5) . . . . ? C2 C3 C4 C5 0.0(6) . . . . ? O3 S1 C11 C8 -61.9(3) . . . . ? O3 S1 C12 C13 -169.9(2) . . . . ? O3 S1 C12 C19 12.2(3) . . . . ? C3 C4 C5 C6 -1.0(5) . . . . ? C4 C5 C6 N1 -176.1(3) . . . . ? C4 C5 C6 C1 0.8(5) . . . . ? O5 C21 C22 C23 176.5(3) . . . . ? O5 C21 C26 C25 -176.5(3) . . . . ? C6 N1 C7 C8 165.1(3) . . . . ? C6 N1 C10 O1 2.0(8) . . . . ? C6 N1 C10 C9 -179.7(3) . . . . ? C6 C1 C2 C3 -1.3(6) . . . . ? C7 N1 C6 C1 -165.2(3) . . . . ? C7 N1 C6 C5 11.7(5) . . . . ? C7 N1 C10 O1 -175.6(5) . . . . ? C7 N1 C10 C9 2.7(5) . . . . ? C7 C8 C9 F1 95.5(3) . . . . ? C7 C8 C9 F2 -144.2(3) . . . . ? C7 C8 C9 C10 -22.7(4) . . . . ? C7 C8 C11 S1 167.7(2) . . . . ? C8 C9 C10 O1 -168.2(5) . . . . ? C8 C9 C10 N1 13.4(4) . . . . ? C9 C8 C11 S1 -74.7(3) . . . . ? C10 N1 C6 C1 17.5(6) . . . . ? C10 N1 C6 C5 -165.7(4) . . . . ? C10 N1 C7 C8 -17.2(4) . . . . ? C11 S1 C12 C13 -54.8(3) . . . . ? C11 S1 C12 C19 127.3(3) . . . . ? C11 C8 C9 F1 -26.5(4) . . . . ? C11 C8 C9 F2 93.8(4) . . . . ? C11 C8 C9 C10 -144.7(3) . . . . ? C12 S1 C11 C8 -177.7(2) . . . . ? C12 C13 C14 C15 -179.2(3) . . . . ? C12 C13 C18 C17 179.3(3) . . . . ? C12 C19 C20 O4 12.3(6) . . . . ? C12 C19 C20 O5 -166.3(3) . . . . ? C13 C12 C19 C20 -7.8(6) . . . . ? C13 C14 C15 C16 -0.2(6) . . . . ? C14 C13 C18 C17 0.3(5) . . . . ? C14 C15 C16 C17 0.6(6) . . . . ? C15 C16 C17 C18 -0.4(6) . . . . ? C16 C17 C18 C13 0.0(5) . . . . ? C18 C13 C14 C15 -0.2(5) . . . . ? C19 C12 C13 C14 -60.9(5) . . . . ? C19 C12 C13 C18 120.2(4) . . . . ? C20 O5 C21 C22 114.5(3) . . . . ? C20 O5 C21 C26 -69.4(4) . . . . ? C21 O5 C20 O4 3.8(5) . . . . ? C21 O5 C20 C19 -177.6(3) . . . . ? C21 C22 C23 C24 -0.2(5) . . . . ? C22 C21 C26 C25 -0.6(5) . . . . ? C22 C23 C24 C25 0.2(5) . . . . ? C23 C24 C25 C26 -0.3(6) . . . . ? C24 C25 C26 C21 0.5(5) . . . . ? C26 C21 C22 C23 0.4(5) . . . . ?