#------------------------------------------------------------------------------ #$Date: 2024-09-19 04:15:50 +0300 (Thu, 19 Sep 2024) $ #$Revision: 294793 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/93/7249353.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7249353 loop_ _publ_author_name 'Konovalova, Irina S.' 'Shishkina, Svitlana V.' 'Wyshusek, Maik' 'Patzer, Michael' 'Reiss, Guido J.' _publ_section_title ; Supramolecular architecture of theophylline polymorphs, monohydrate and co-crystals with iodine: study from the energetic viewpoint ; _journal_issue 41 _journal_name_full 'RSC Advances' _journal_page_first 29774 _journal_page_last 29788 _journal_paper_doi 10.1039/D4RA04368E _journal_volume 14 _journal_year 2024 _chemical_formula_moiety 'C7 H8 N4 O2' _chemical_formula_sum 'C7 H8 N4 O2' _chemical_formula_weight 180.17 _space_group_crystal_system monoclinic _space_group_IT_number 7 _space_group_name_Hall 'P -2yac' _space_group_name_H-M_alt 'P 1 n 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2019/2 _audit_update_record ; 2023-05-22 deposited with the CCDC. 2024-09-11 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 98.965(8) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 3.8744(4) _cell_length_b 12.8898(9) _cell_length_c 8.1167(6) _cell_measurement_temperature 290(2) _cell_volume 400.40(6) _computing_structure_refinement 'SHELXL-2019/2 (Sheldrick, 2019)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.871 _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0240 _diffrn_reflns_av_unetI/netI 0.0419 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.871 _diffrn_reflns_limit_h_max 5 _diffrn_reflns_limit_h_min -4 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 10 _diffrn_reflns_limit_l_min -11 _diffrn_reflns_number 2386 _diffrn_reflns_point_group_measured_fraction_full 0.820 _diffrn_reflns_point_group_measured_fraction_max 0.680 _diffrn_reflns_theta_full 26.000 _diffrn_reflns_theta_max 29.318 _diffrn_reflns_theta_min 2.992 _exptl_absorpt_coefficient_mu 0.114 _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.494 _exptl_crystal_F_000 188 _refine_diff_density_max 0.174 _refine_diff_density_min -0.190 _refine_diff_density_rms 0.043 _refine_ls_abs_structure_details ; Flack x determined using 360 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -2.0(10) _refine_ls_extinction_coef 0.015(3) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2019/2 (Sheldrick 2019)' _refine_ls_goodness_of_fit_ref 1.033 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 121 _refine_ls_number_reflns 1499 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.033 _refine_ls_R_factor_all 0.0689 _refine_ls_R_factor_gt 0.0491 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0120P)^2^+0.3000P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0908 _refine_ls_wR_factor_ref 0.0983 _reflns_Friedel_coverage 0.550 _reflns_Friedel_fraction_full 0.638 _reflns_Friedel_fraction_max 0.487 _reflns_number_gt 1168 _reflns_number_total 1499 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4ra04368e2.cif _cod_data_source_block exp_276_2 _cod_original_cell_volume 400.40(5) _cod_original_sg_symbol_H-M 'P n' _cod_database_code 7249353 _shelx_shelxl_version_number 2019/2 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL exp_276_2 in Pn #7 exp_276_2.res created by SHELXL-2019/2 at 21:42:51 on 22-May-2023 CELL 0.71073 3.874417 12.889756 8.11668 90 98.9648 90 ZERR 2 0.000362 0.000914 0.000552 0 0.0076 0 LATT -1 SYMM 0.5+X,-Y,0.5+Z SFAC C H N O UNIT 14 16 8 4 LIST 4 ! automatically inserted. Change 6 to 4 for CHECKCIF!! L.S. 10 PLAN 20 REM reset to Pn #7 BOND CONF fmap 2 acta 52 REM I:/writing/VDyulgerov3/olex2_exp_276_2/exp_276_2.hkl REM ##### WGHT 0.012000 0.300000 EXTI 0.014740 FVAR 3.66480 O1 4 -0.785790 -0.421251 -0.081599 11.00000 0.10461 0.03493 = 0.06274 0.00967 0.02574 -0.01114 N1 3 -0.673593 -0.062378 0.006820 11.00000 0.05191 0.03720 = 0.02843 -0.00286 0.01202 0.00101 C1 1 -0.712910 -0.335161 -0.122217 11.00000 0.05564 0.04010 = 0.04451 0.00524 0.00789 -0.00041 O2 4 -0.388410 -0.213246 -0.468814 11.00000 0.09061 0.04297 = 0.04097 -0.00522 0.03567 -0.00371 N2 3 -0.744946 -0.249821 -0.022815 11.00000 0.04199 0.04170 = 0.03472 0.00620 0.01061 -0.00216 C2 1 -0.491989 -0.220766 -0.333585 11.00000 0.04854 0.03497 = 0.03966 -0.00104 0.00915 0.00370 C3 1 -0.535149 -0.139342 -0.220489 11.00000 0.03730 0.03096 = 0.03235 0.00138 0.00693 -0.00121 N4 3 -0.593605 -0.316728 -0.273529 11.00000 0.06030 0.02711 = 0.04138 -0.00234 0.01608 0.00162 C4 1 -0.557138 0.007723 -0.092782 11.00000 0.05832 0.03568 = 0.04025 -0.00578 0.01480 0.00012 AFIX 43 H4 2 -0.537850 0.078132 -0.068042 11.00000 -1.20000 AFIX 0 N5 3 -0.471654 -0.033820 -0.231117 11.00000 0.05103 0.03540 = 0.02926 0.00063 0.01444 -0.00140 AFIX 43 H5 2 -0.393278 -0.001844 -0.310622 11.00000 -1.20000 AFIX 0 C5 1 -0.657712 -0.152954 -0.075623 11.00000 0.03556 0.03600 = 0.02936 0.00328 0.00548 -0.00226 C6 1 -0.853248 -0.264128 0.140840 11.00000 0.06666 0.06542 = 0.03908 0.01609 0.01679 -0.00580 AFIX 137 H6A 2 -0.947777 -0.332563 0.147634 11.00000 -1.50000 H6B 2 -1.028067 -0.213615 0.155399 11.00000 -1.50000 H6C 2 -0.654836 -0.255576 0.226679 11.00000 -1.50000 AFIX 0 C7 1 -0.563977 -0.410022 -0.379889 11.00000 0.08869 0.03467 = 0.06740 -0.01406 0.02674 -0.00368 AFIX 137 H7A 2 -0.459181 -0.390483 -0.474975 11.00000 -1.50000 H7B 2 -0.792435 -0.438117 -0.416751 11.00000 -1.50000 H7C 2 -0.421291 -0.461369 -0.316232 11.00000 -1.50000 AFIX 0 HKLF 4 REM exp_276_2 in Pn #7 REM wR2 = 0.0983, GooF = S = 1.033, Restrained GooF = 1.033 for all data REM R1 = 0.0491 for 1168 Fo > 4sig(Fo) and 0.0689 for all 1499 data REM 121 parameters refined using 2 restraints END WGHT 0.0408 0.1341 REM Highest difference peak 0.174, deepest hole -0.190, 1-sigma level 0.043 Q1 1 -0.3361 -0.0940 -0.3809 11.00000 0.05 0.17 Q2 1 -0.9870 -0.0393 -0.0075 11.00000 0.05 0.16 Q3 1 -0.8712 -0.1838 0.2349 11.00000 0.05 0.15 Q4 1 -0.5627 -0.0802 -0.4780 11.00000 0.05 0.14 Q5 1 -0.3428 -0.4240 -0.4364 11.00000 0.05 0.14 Q6 1 -0.6146 -0.3833 -0.0336 11.00000 0.05 0.13 Q7 1 -0.8880 -0.1213 0.1467 11.00000 0.05 0.13 Q8 1 -0.7191 -0.2152 0.2262 11.00000 0.05 0.13 Q9 1 -0.6316 -0.1395 -0.1794 11.00000 0.05 0.13 Q10 1 -0.8740 -0.0693 0.0981 11.00000 0.05 0.13 Q11 1 -0.7870 -0.5276 -0.2462 11.00000 0.05 0.13 Q12 1 -0.5406 -0.5137 -0.2432 11.00000 0.05 0.13 Q13 1 -0.7836 -0.2524 0.0802 11.00000 0.05 0.13 Q14 1 -0.6671 -0.3260 0.1890 11.00000 0.05 0.12 Q15 1 -0.4455 -0.0419 -0.0039 11.00000 0.05 0.12 Q16 1 -1.0194 -0.3843 0.3296 11.00000 0.05 0.12 Q17 1 -0.3279 -0.2800 -0.2240 11.00000 0.05 0.12 Q18 1 -0.6501 -0.4612 -0.4070 11.00000 0.05 0.12 Q19 1 -0.7704 0.0012 -0.2830 11.00000 0.05 0.12 Q20 1 -0.5033 -0.2652 -0.5465 11.00000 0.05 0.12 ; _shelx_res_checksum 54698 _shelx_hkl_file ; -4 0 6 318.841 37.9309 3 -4 0 7 20.3684 17.8478 3 -4 0 8-6.97299 21.6513 3 -4 1 4 41.4598 14.5428 3 -4 1 5 233.347 30.1440 3 -4 1 6 48.9992 18.8862 3 -4 1 7 13.6041 14.8465 3 -4 1 8 65.7256 23.2575 3 -4 2 3 0.69340 11.6442 3 -4 2 4 88.5518 19.4911 3 -4 2 5-17.7710 17.0288 3 -4 2 6 150.236 28.5316 3 -4 2 7-0.95177 16.6406 3 -4 2 8 22.9150 17.7436 3 -4 -3 -2 110.036 22.1923 1 -4 -3 -1 45.6290 17.7342 1 -4 -3 0 5.05406 14.3873 1 -4 3 3 133.060 19.6302 3 -4 3 4 74.9390 19.2108 3 -4 3 5 107.642 23.0862 3 -4 3 6 46.0301 19.4710 3 -4 3 7-4.98277 17.8151 3 -4 -4 -2 57.5055 19.3464 1 -4 -4 -1 37.2201 17.9192 1 -4 -4 0 142.182 26.6393 1 -4 -4 1 59.1634 21.6600 1 -4 4 3 156.828 22.9043 3 -4 4 4 497.774 40.8546 3 -4 4 5 163.965 28.1087 3 -4 4 6 44.3838 20.7480 3 -4 4 7 8.74856 20.8782 3 -4 -5 -2 36.0970 17.9471 1 -4 -5 -1 98.7913 24.6074 1 -4 -5 0 13.3202 15.6648 1 -4 -5 1 19.2475 20.0267 1 -4 5 2 157.018 19.7818 3 -4 -5 2 152.532 31.7051 1 -4 5 3 548.279 40.4770 3 -4 5 4 200.630 28.9903 3 -4 5 5 223.648 32.5355 3 -4 5 6 1.72784 16.5944 3 -4 5 7 37.0410 22.9340 3 -4 -6 -2-18.5428 17.3521 1 -4 -6 -1 18.5452 17.3893 1 -4 -6 0 4.03714 17.2799 1 -4 -6 1 89.6572 26.7266 1 -4 6 2 29.5736 12.2439 3 -4 -6 2 8.48508 18.9663 1 -4 6 3 234.970 29.9707 3 -4 -6 3 194.523 37.8722 1 -4 6 4 436.060 40.9224 3 -4 6 5 51.1333 21.0619 3 -4 6 6 15.2013 16.5163 3 -4 6 7 2.26407 17.2513 3 -4 -7 -2 23.9079 19.3083 1 -4 -7 -1 44.1412 20.9977 1 -4 -7 0 98.4109 27.0557 1 -4 -7 1 49.5029 22.5711 1 -4 7 2 26.7176 13.0330 3 -4 -7 2 18.9382 22.5789 1 -4 -7 3 209.435 39.8791 1 -4 7 3 220.384 28.6547 3 -4 7 4 117.987 23.9394 3 -4 7 5 4.70173 15.0362 3 -4 7 6 20.6377 18.7655 3 -4 -8 -3 46.0822 23.9500 1 -4 -8 -2-27.9656 21.5552 1 -4 -8 -1 28.7737 21.2963 1 -4 -8 0 148.411 32.2046 1 -4 -8 1 6.36390 19.5611 1 -4 -8 2 26.1750 27.0252 1 -4 8 3 59.4664 17.2686 3 -4 -8 3 33.0643 23.2634 1 -4 -8 4 40.1478 25.4394 1 -4 8 4 59.9795 21.0289 3 -4 8 5 69.2429 25.0645 3 -4 8 6 50.7944 22.8827 3 -4 -9 -3 54.0672 24.5497 1 -4 -9 -2 1.96833 20.3389 1 -4 -9 -1 79.6157 26.7940 1 -4 -9 0 7.71662 21.3514 1 -4 -9 1 73.9203 29.0528 1 -4 -9 2 12.5619 24.0756 1 -4 -9 3 26.0641 24.7630 1 -4 9 3-22.2292 14.8513 3 -4 9 4 20.1308 15.2177 3 -4 9 5 19.7703 18.8074 3 -4 9 6 15.4068 16.4081 3 -4 -10 -2 36.5070 26.7895 1 -4 -10 -1 32.8477 23.3498 1 -4 -10 0 99.0029 30.8775 1 -4 -10 1 69.9282 31.5780 1 -4 -10 2 105.752 37.4304 1 -4 10 4 4.91524 13.4363 3 -4 10 5 24.6638 17.7833 3 -3 0 -4-5.58597 5.51192 1 -3 0 -3 815.262 26.7700 1 -3 0 -2-1.24422 6.34270 1 -3 0 2-6.54521 9.53917 3 -3 0 4-5.99686 13.0122 3 -3 0 5 65.3892 17.3061 3 -3 0 6 0.21358 14.5809 3 -3 0 7 824.430 60.5422 3 -3 0 8-2.89109 18.3298 3 -3 0 9 127.351 30.6342 3 -3 1 -7-10.7866 23.1744 4 -3 -1 -5 6.38525 7.37897 1 -3 -1 -4 4.06226 8.20397 1 -3 -1 -3 715.214 33.6215 1 -3 -1 -2 1342.63 47.6839 1 -3 -1 -1 766.760 39.2052 1 -3 -1 0 78.2512 16.7525 1 -3 1 1 82.0954 10.9001 3 -3 1 2 1364.98 46.3439 3 -3 -1 4 42.5009 13.9809 3 -3 1 4 88.0570 18.3278 3 -3 -1 5 278.374 31.9979 3 -3 1 5 258.825 30.3202 3 -3 -1 6 754.012 53.7655 3 -3 1 6 782.578 54.9466 3 -3 1 7 139.377 29.7730 3 -3 -1 7 131.216 28.5860 3 -3 1 8 46.5345 24.0008 3 -3 -1 8 27.7494 20.9979 3 -3 1 9-7.81611 21.1899 3 -3 -1 9 22.5008 21.9152 3 -3 2 -7 98.2943 28.5791 4 -3 2 -6-15.3066 20.0940 4 -3 -2 -5 33.6787 11.9086 1 -3 -2 -4 135.962 18.2752 1 -3 -2 -3 780.668 39.1704 1 -3 -2 -2 1205.05 50.4251 1 -3 -2 -1 252.482 26.2732 1 -3 -2 0 36.5283 15.0168 1 -3 -2 1 66.6019 19.5611 1 -3 2 1 65.5070 10.3994 3 -3 2 2 123.182 16.5707 3 -3 2 3 219.322 23.6916 3 -3 2 4 45.7495 17.0765 3 -3 2 5 263.668 31.2676 3 -3 2 6 31.0682 18.4557 3 -3 2 7 38.4726 21.0407 3 -3 2 8-19.6048 23.3684 3 -3 3 -7 11.2605 23.5608 4 -3 3 -6 107.756 31.2194 4 -3 3 -5 32.6068 23.3427 4 -3 -3 -5 47.0266 15.0715 1 -3 -3 -4 28.2886 13.3804 1 -3 -3 -3 226.698 25.0371 1 -3 -3 -2 332.160 29.2650 1 -3 -3 -1 96.0694 20.5440 1 -3 -3 0 324.062 33.1813 1 -3 3 0 299.024 15.7069 3 -3 -3 1 29.9217 17.2938 1 -3 3 1 28.3215 9.49169 3 -3 -3 2 206.853 29.9746 1 -3 3 3 25.5573 13.3443 3 -3 3 4 366.233 34.5324 3 -3 3 5 778.616 52.2129 3 -3 3 6 249.898 34.6030 3 -3 3 7 55.5100 22.7947 3 -3 3 8-14.3352 16.6798 3 -3 4 -6 50.9892 28.7669 4 -3 4 -5 96.7798 27.7960 4 -3 -4 -5 61.4133 17.6490 1 -3 -4 -4 31.9224 14.6841 1 -3 -4 -3 16.4008 12.5715 1 -3 -4 -2 8.08638 11.6614 1 -3 -4 -1 374.451 34.7213 1 -3 4 -1 347.736 14.9187 3 -3 4 0 94.7774 12.0611 3 -3 -4 0 131.675 24.2886 1 -3 4 1 5.94548 7.76083 3 -3 -4 1 2.00119 14.1972 1 -3 -4 2 131.444 26.1994 1 -3 -4 3 263.041 36.2779 1 -3 4 3 212.299 25.7542 3 -3 4 4 318.534 33.6286 3 -3 4 5 693.885 51.5110 3 -3 4 6 464.274 45.7971 3 -3 4 7 151.326 31.5216 3 -3 4 8 34.5580 23.3404 3 -3 5 -6-10.6595 23.0574 4 -3 -5 -6 26.6103 16.4491 1 -3 5 -5 33.7750 25.3730 4 -3 -5 -5 42.7774 17.0498 1 -3 -5 -4 80.2445 21.0101 1 -3 5 -4 114.156 31.9944 4 -3 -5 -3 11.1350 13.5499 1 -3 5 -3 14.7576 5.07028 3 -3 5 -2-0.01594 4.40913 3 -3 -5 -2 1.86037 14.0653 1 -3 -5 -1 399.376 37.4287 1 -3 5 -1 418.974 22.3298 3 -3 -5 0 710.105 50.0486 1 -3 5 0 669.358 31.4102 3 -3 -5 1 43.9633 18.5117 1 -3 -5 2 247.632 34.5854 1 -3 5 2 243.771 25.0098 3 -3 -5 3 660.816 55.7961 1 -3 5 3 693.491 44.3954 3 -3 5 4 1936.78 78.9465 3 -3 5 5 395.041 41.3402 3 -3 5 6 168.577 30.3821 3 -3 5 7 141.317 30.6992 3 -3 5 8 24.7035 21.9110 3 -3 -6 -6 14.8886 15.5384 1 -3 6 -6 23.1229 26.8611 4 -3 -6 -5 8.35709 14.7336 1 -3 6 -5-8.95911 23.5339 4 -3 6 -4 36.9745 22.3960 4 -3 -6 -4 23.9060 17.0617 1 -3 -6 -3 20.7357 16.2563 1 -3 -6 -2 92.1096 22.5481 1 -3 -6 -1 208.120 30.3991 1 -3 -6 0 331.429 38.6891 1 -3 -6 1 284.914 35.9084 1 -3 -6 2 172.246 31.4993 1 -3 6 2 182.362 23.0935 3 -3 6 3 523.630 46.2510 2 -3 6 3 512.158 39.9615 3 -3 -6 3 614.050 55.5098 1 -3 6 4 532.431 46.5778 2 -3 -6 4 641.753 59.0814 1 -3 6 4 508.105 42.9242 3 -3 6 5 863.413 59.6086 3 -3 6 6 4.26193 17.9347 3 -3 6 7 16.1052 16.1650 3 -3 6 8 20.8318 21.9195 3 -3 -7 -6-5.45902 15.7803 1 -3 7 -5 80.1812 33.0393 4 -3 -7 -5 29.6947 18.4877 1 -3 7 -4 4.01653 23.7832 4 -3 -7 -4 27.5947 17.2752 1 -3 -7 -3 98.7194 26.1241 1 -3 -7 -2 27.0497 18.0573 1 -3 -7 -1-3.14763 16.0996 1 -3 -7 0 153.171 29.4931 1 -3 -7 1 374.714 42.9102 1 -3 7 1 284.513 27.9333 3 -3 7 2 77.4714 17.0156 3 -3 -7 2 92.5898 25.9393 1 -3 -7 3 44.7928 20.8780 1 -3 7 3 39.7667 15.8490 3 -3 -7 4 857.984 69.1758 1 -3 7 4 893.914 57.8053 3 -3 7 5 184.123 31.4510 3 -3 7 6 18.0604 20.3281 3 -3 7 7 52.4705 24.6529 3 -3 -8 -6 2.70887 15.7454 1 -3 8 -5 33.7089 27.9761 4 -3 -8 -5 40.9074 22.5506 1 -3 -8 -4 180.400 32.4491 1 -3 8 -4 240.176 43.6081 4 -3 -8 -3 150.431 31.0427 1 -3 -8 -2 26.4661 20.3109 1 -3 -8 -1 97.6761 26.4406 1 -3 -8 0 124.444 29.1182 1 -3 -8 1 94.1661 26.4691 1 -3 -8 2 124.910 29.5231 1 -3 8 2 124.328 22.4359 3 -3 8 3 91.1993 21.1237 3 -3 -8 3 115.056 30.8762 1 -3 -8 4 84.6694 30.8351 1 -3 8 4 78.9437 20.1543 3 -3 -8 5 50.3449 29.0091 1 -3 8 5 48.9504 20.6971 3 -3 8 6 60.3357 22.5245 3 -3 8 7-4.44347 20.0236 3 -3 -9 -6 11.7283 16.9453 1 -3 -9 -5 30.8888 22.0818 1 -3 -9 -4 168.436 34.1199 1 -3 9 -4 175.152 40.2209 4 -3 -9 -3 258.337 39.0178 1 -3 -9 -2 112.281 28.4758 1 -3 -9 -1 47.6323 21.5949 1 -3 -9 0 82.9996 27.6267 1 -3 -9 1 82.2862 26.6203 1 -3 9 2 147.795 25.2679 3 -3 -9 2 172.678 35.1197 1 -3 -9 3 68.8891 27.6582 1 -3 9 3 66.6044 19.4430 3 -3 9 4 110.531 25.1992 3 -3 -9 4 107.515 31.3652 1 -3 9 5 44.7429 16.8774 3 -3 -9 5 89.9107 34.5247 1 -3 9 6 14.6012 20.5512 3 -3 9 7 63.3675 26.0165 3 -3 -10 -5 24.4922 26.2930 1 -3 10 -4 0.33804 20.5474 4 -3 -10 -4 40.8841 18.5598 1 -3 -10 -3 332.751 45.8780 1 -3 -10 -2 98.9633 31.9132 1 -3 -10 -1 96.4337 27.2859 1 -3 -10 0 126.434 32.2442 1 -3 -10 1 290.791 44.1706 1 -3 -10 2 229.793 41.8273 1 -3 10 3 247.797 34.4484 3 -3 -10 3 243.510 42.3549 1 -3 -10 4 5.57020 23.7041 1 -3 10 4 52.7935 23.2694 3 -3 -10 5 78.3511 29.0586 1 -3 10 5 48.4095 20.1215 3 -3 10 6 44.5326 24.8723 3 -3 -11 -4-4.74283 22.8430 1 -3 -11 -3 93.4746 28.3704 1 -3 -11 -2 64.4545 28.1334 1 -3 -11 -1 79.1829 30.6392 1 -3 -11 0 25.6132 25.9424 1 -3 -11 1 215.346 42.0259 1 -3 -11 2 50.4655 29.4197 1 -3 11 3 104.405 25.8174 3 -3 -11 3 109.952 30.6033 1 -3 11 4 122.321 30.2767 3 -3 -11 4 65.7335 33.4096 1 -3 11 5 97.4660 24.8596 3 -3 -12 -3 35.5973 28.6078 1 -3 -12 -2 110.441 34.3117 1 -3 -12 -1 220.095 42.0070 1 -3 -12 0 116.249 35.3231 1 -3 -12 1 14.3410 23.0498 1 -3 -12 2-2.63323 24.9615 1 -3 12 3 72.5470 25.2078 3 -3 -12 3 76.7727 30.2019 1 -3 12 4-17.2002 21.1023 3 -3 12 5 40.6556 19.4274 3 -3 13 3 19.0682 19.2472 3 -3 13 4 14.5866 21.1896 3 -2 0 -9 18.7220 17.5053 4 -2 0 -8 160.849 30.8079 4 -2 0 -7 5.83359 17.3724 4 -2 0 -6 9.02628 16.6203 4 -2 0 -5 9.31056 17.2741 4 -2 0 -4 170.602 25.1193 4 -2 0 -4 148.172 14.4233 1 -2 0 -3 0.39658 5.58112 1 -2 0 -3-1.96920 14.9112 4 -2 0 -2 8750.02 85.5682 1 -2 0 -1-4.27174 7.44995 1 -2 0 0 1120.53 38.0823 1 -2 0 1-0.96341 6.52923 3 -2 0 2 3540.28 68.8376 3 -2 0 4 1617.26 61.5088 3 -2 0 5 3.83801 11.7587 3 -2 0 6 711.649 50.0803 3 -2 0 7-7.81584 15.4287 3 -2 0 8 508.798 49.7150 3 -2 0 9-7.09877 18.7349 3 -2 1 -9-11.9490 19.9646 4 -2 -1 -9 19.1836 21.9719 4 -2 -1 -8 138.264 29.0656 4 -2 1 -8 168.956 31.0740 4 -2 -1 -7-0.20133 16.6545 4 -2 1 -7-0.85623 18.3422 4 -2 1 -6 206.570 31.0816 4 -2 -1 -6 201.795 28.3548 4 -2 -1 -5 15.9613 15.1894 4 -2 1 -5 50.4172 20.3979 4 -2 -1 -4 121.109 21.9256 4 -2 -1 -4 116.944 14.9105 1 -2 1 -4 115.976 22.4224 4 -2 1 -4 113.869 10.6898 1 -2 -1 -3 37.5372 9.43616 1 -2 1 -3 49.4678 6.02893 1 -2 1 -3 67.6336 20.8332 4 -2 -1 -2 5185.37 77.8978 1 -2 -1 -1 9485.59 110.270 1 -2 1 0 2172.32 31.2672 3 -2 -1 0 2210.65 58.3852 1 -2 1 1 780.803 27.6799 3 -2 -1 1 860.026 40.6964 1 -2 -1 2 78.9239 12.8392 3 -2 1 2 98.8163 14.1173 3 -2 -1 4 158.709 22.5856 3 -2 1 4 189.837 23.8724 3 -2 -1 5 452.379 37.3935 3 -2 1 5 474.754 38.1869 3 -2 1 6 541.313 43.8752 3 -2 -1 6 504.792 42.5314 3 -2 -1 7 936.007 60.8595 3 -2 1 7 923.887 61.4517 3 -2 1 8 310.499 39.9842 3 -2 -1 8 269.490 39.3574 3 -2 1 9 42.1422 25.1183 3 -2 -1 9 23.0534 22.4835 3 -2 2 -9 208.264 34.6073 4 -2 -2 -8 108.274 26.5973 4 -2 2 -8 133.973 30.3831 4 -2 -2 -7 56.8500 21.0043 4 -2 2 -7 111.969 27.1359 4 -2 2 -6 415.642 27.5114 1 -2 -2 -6 353.693 35.3853 4 -2 2 -6 391.922 29.2135 3 -2 2 -6 368.278 37.5744 4 -2 2 -5 106.131 24.6081 4 -2 -2 -5 88.2556 19.3618 4 -2 2 -5 93.0669 11.8059 1 -2 2 -5 110.380 15.0732 3 -2 2 -4 151.764 13.8165 3 -2 2 -4 156.875 9.61693 1 -2 2 -4 139.605 24.7698 4 -2 -2 -4 173.354 19.2633 1 -2 2 -4 116.526 7.58064 1 -2 -2 -3 719.441 34.5099 1 -2 2 -3 668.183 21.3006 3 -2 2 -3 673.896 44.0730 4 -2 2 -2 3582.12 92.1784 4 -2 2 -2 3401.91 33.8615 3 -2 -2 -2 3611.54 73.6783 1 -2 -2 -1 4214.69 81.4592 1 -2 2 -1 4014.61 36.9938 3 -2 2 0 801.627 23.5091 3 -2 -2 0 830.217 39.6155 1 -2 2 1 290.481 18.4791 3 -2 -2 1 270.224 26.6209 1 -2 -2 2 553.441 38.1973 1 -2 2 2 541.169 29.2789 3 -2 2 4 92.7288 19.1907 3 -2 -2 4 79.7986 16.8722 3 -2 -2 5 3.23376 14.6349 3 -2 2 5-6.31565 14.0370 3 -2 2 6 277.722 33.5933 3 -2 -2 6 333.192 36.2874 3 -2 2 7 180.824 29.7805 3 -2 -2 7 164.489 29.8315 3 -2 -2 8 66.5708 23.6405 3 -2 2 8 72.4758 22.6621 3 -2 2 9 8.12948 18.3542 3 -2 -2 9 2.36453 18.1096 3 -2 3 -8 113.757 29.0526 4 -2 -3 -8 54.3501 22.0029 4 -2 -3 -7 17.2157 17.8071 4 -2 3 -7-3.31346 20.4958 4 -2 3 -6 70.5704 22.2360 4 -2 3 -6 28.4541 11.7202 3 -2 3 -6 42.5235 9.63455 1 -2 -3 -6 27.5939 16.3967 4 -2 3 -5 539.024 44.4933 4 -2 3 -5 524.140 29.9560 3 -2 3 -5 498.783 20.2990 1 -2 3 -4 144.050 24.4124 4 -2 -3 -4 163.684 20.6498 1 -2 3 -4 188.026 16.6592 3 -2 -3 -3 310.277 26.1962 1 -2 3 -3 275.421 30.7714 4 -2 3 -3 313.102 17.7054 3 -2 -3 -2 178.772 20.4688 1 -2 3 -2 148.972 24.0787 4 -2 3 -2 172.027 11.5632 3 -2 -3 -1 63.0193 13.8092 1 -2 -3 0 458.962 32.1083 1 -2 -3 1 148.353 21.2174 1 -2 3 1 186.744 24.2460 2 -2 3 1 148.336 15.8695 3 -2 3 2 113.768 19.7812 2 -2 -3 2 108.426 21.6805 1 -2 3 2 84.3393 14.9341 3 -2 -3 3 247.315 30.9009 1 -2 3 3 183.007 21.3168 2 -2 3 4 3.67008 9.95982 2 -2 3 4 36.6001 16.6339 3 -2 3 5 1342.08 65.0256 3 -2 3 6 2182.92 89.4343 3 -2 3 7 119.905 26.6782 3 -2 3 8 31.9854 20.7720 3 -2 3 9 48.3714 26.6125 3 -2 4 -8 135.141 30.7228 4 -2 -4 -7 58.7803 18.6215 4 -2 4 -7 111.084 27.0509 4 -2 4 -6 107.705 18.0981 3 -2 4 -6 112.939 26.6955 4 -2 -4 -5 168.248 23.3809 1 -2 4 -5 162.366 19.3881 3 -2 4 -5 197.155 31.2561 4 -2 4 -4 410.159 25.7252 3 -2 -4 -4 426.400 33.0980 1 -2 4 -4 454.330 39.6382 4 -2 4 -3 11.0678 7.58395 3 -2 -4 -3 5.82592 11.5629 1 -2 4 -3 6.38610 18.4459 4 -2 -4 -2 580.868 37.7738 1 -2 4 -2 484.606 38.8513 4 -2 -4 -1 45.1271 14.7327 1 -2 -4 0 1368.63 56.9000 1 -2 4 0 1452.78 64.7739 2 -2 4 1 412.259 33.9389 2 -2 -4 1 378.012 32.8311 1 -2 -4 2 196.768 27.0246 1 -2 4 2 199.030 25.5333 2 -2 -4 3 337.748 35.5693 1 -2 4 3 326.942 28.9650 2 -2 4 3 348.389 30.0925 3 -2 4 4 369.142 29.0709 2 -2 4 4 426.375 35.9579 3 -2 4 5 922.366 42.0804 2 -2 4 5 899.877 54.9686 3 -2 4 6 511.421 46.6388 3 -2 4 6 486.243 27.8652 2 -2 4 7 481.676 47.8202 3 -2 4 8 162.940 33.2604 3 -2 4 9 3.90203 14.8264 3 -2 5 -8 143.946 33.3949 4 -2 5 -7 124.442 27.4791 4 -2 5 -6 23.8251 10.9671 3 -2 5 -6 10.9159 17.3447 4 -2 5 -5 29.9671 9.86243 3 -2 5 -5 12.6053 16.0800 4 -2 -5 -5 57.0697 17.5013 1 -2 5 -4 447.298 28.7817 3 -2 5 -4 462.720 42.6961 4 -2 -5 -4 485.111 37.9642 1 -2 5 -3 335.743 23.0752 3 -2 5 -3 366.449 37.1975 4 -2 -5 -3 380.529 33.3301 1 -2 -5 -2 89.8358 19.2997 1 -2 5 -2 48.7251 20.2503 2 -2 5 -2 68.9088 21.7848 4 -2 -5 -1 19.4156 15.2365 1 -2 5 -1 29.6832 17.3245 2 -2 -5 0 1248.98 58.0105 1 -2 5 0 1262.62 62.6282 2 -2 5 1 3220.96 94.9171 2 -2 -5 1 3253.69 95.5159 1 -2 -5 2 104.175 23.0221 1 -2 5 2 120.906 21.1352 2 -2 5 3 1177.60 54.2077 2 -2 -5 3 1211.29 65.8515 1 -2 5 3 1281.46 57.0465 3 -2 -5 4 1175.53 68.6006 1 -2 5 4 1131.56 51.3783 2 -2 5 4 1166.75 59.2101 3 -2 5 5 2936.74 99.8569 3 -2 5 5 3145.77 81.4840 2 -2 5 6 706.775 37.4932 2 -2 5 6 758.265 55.8624 3 -2 5 7 211.037 34.1981 3 -2 5 8 154.853 33.9119 3 -2 5 9 38.5514 25.3110 3 -2 6 -7 103.233 28.8177 4 -2 6 -6 44.4006 22.6259 4 -2 -6 -6 29.8332 16.8263 1 -2 6 -5 102.513 17.9755 3 -2 6 -5 80.8103 24.6033 4 -2 -6 -5 110.885 22.9556 1 -2 -6 -4 55.7802 17.4580 1 -2 6 -4 53.2327 13.3253 3 -2 6 -4 66.0757 20.8272 4 -2 -6 -3 169.857 25.4446 1 -2 6 -3 176.017 30.0805 4 -2 -6 -2 60.1484 18.0535 1 -2 6 -2 32.7678 19.4838 2 -2 6 -2 54.4861 19.3077 4 -2 6 -1 661.587 50.2615 2 -2 -6 -1 643.663 44.9665 1 -2 6 -1 625.242 43.6983 4 -2 6 0 1841.38 78.6062 2 -2 -6 0 1803.76 74.0224 1 -2 -6 1 1320.88 65.4251 1 -2 6 1 1280.09 63.3005 2 -2 6 2 1614.02 68.8070 2 -2 -6 2 1564.44 73.6859 1 -2 6 3 112.041 21.5816 3 -2 6 3 131.806 23.1721 2 -2 -6 3 100.237 25.7795 1 -2 6 4 2448.99 88.3264 3 -2 6 4 2443.97 79.0120 2 -2 -6 4 2344.09 97.9790 1 -2 6 5 874.681 57.2148 3 -2 6 5 847.458 46.0617 2 -2 6 6 677.273 54.3765 3 -2 6 6 692.564 40.7574 2 -2 6 7 259.086 38.2785 3 -2 6 8 97.1309 30.0679 3 -2 6 9-5.05178 20.0068 3 -2 -7 -8 127.839 28.9862 1 -2 7 -7 129.812 31.3641 4 -2 -7 -7 122.088 27.5260 1 -2 -7 -6 77.8476 22.5863 1 -2 7 -6 79.3138 26.4497 4 -2 7 -5 70.2703 17.5653 3 -2 7 -5 67.2138 23.1880 4 -2 -7 -5 49.9323 18.1892 1 -2 7 -4 197.947 23.4474 3 -2 -7 -4 157.851 27.3976 1 -2 7 -4 163.141 28.3061 4 -2 7 -3 202.584 31.7144 4 -2 -7 -3 206.595 29.1637 1 -2 -7 -2 112.971 23.6435 1 -2 7 -2 225.211 31.9719 4 -2 7 -1 261.056 35.0967 2 -2 7 -1 250.256 32.6629 4 -2 -7 -1 309.065 34.5412 1 -2 7 0 234.363 31.2967 2 -2 -7 0 240.545 31.1973 1 -2 -7 1 288.266 33.9393 1 -2 7 1 232.426 32.6257 2 -2 7 2 74.1793 22.9031 2 -2 -7 2 20.2459 16.0379 1 -2 7 3 297.531 33.3926 3 -2 7 3 358.424 36.5096 2 -2 -7 3 347.195 40.3473 1 -2 -7 4 525.185 50.5573 1 -2 7 4 585.484 42.7365 2 -2 7 4 519.469 43.1795 3 -2 -7 5 1578.17 87.8419 1 -2 7 5 1469.90 63.8915 2 -2 7 5 1495.24 75.7916 3 -2 7 6 181.598 31.0918 3 -2 7 6 166.667 24.4700 2 -2 7 7 16.0962 17.6546 3 -2 7 8 101.718 29.0522 3 -2 -8 -8 188.886 33.4688 1 -2 -8 -7 258.056 38.0746 1 -2 8 -7 131.230 33.4438 4 -2 -8 -6 120.360 27.7321 1 -2 8 -6 176.389 33.2880 4 -2 8 -5 133.628 32.0073 4 -2 -8 -5 129.377 27.6846 1 -2 8 -4 88.7422 18.1926 3 -2 8 -4 82.8508 26.5835 4 -2 -8 -4 109.260 23.9367 1 -2 8 -3 531.195 46.4756 4 -2 -8 -3 499.579 45.6827 1 -2 8 -2 417.926 41.2278 4 -2 -8 -2 425.173 41.6150 1 -2 8 -1 15.3504 18.2163 4 -2 -8 -1 31.8922 19.1475 1 -2 -8 0 176.860 29.8211 1 -2 8 1 647.434 51.0639 2 -2 -8 1 675.124 52.8799 1 -2 8 2 319.928 36.9790 2 -2 -8 2 382.289 42.7790 1 -2 8 3 344.741 36.4589 2 -2 -8 3 324.904 40.4256 1 -2 8 4 215.881 29.9321 2 -2 -8 4 204.002 34.4101 1 -2 8 4 188.608 29.8353 3 -2 -8 5 509.141 52.8115 1 -2 8 5 450.798 44.0634 3 -2 8 5 534.366 42.3718 2 -2 8 6 57.3608 23.2506 3 -2 8 6 46.1605 17.8474 2 -2 8 7 96.7471 28.9433 3 -2 8 8 80.0953 28.0107 3 -2 -9 -7 246.520 40.1251 1 -2 -9 -6 17.0739 19.1939 1 -2 9 -6 20.5449 21.8357 4 -2 -9 -5 13.4988 17.1467 1 -2 9 -5-5.64178 19.2808 4 -2 -9 -4 11.0979 17.7974 1 -2 9 -4 16.0540 19.7115 4 -2 9 -3 655.404 52.8691 4 -2 -9 -3 655.401 53.6540 1 -2 9 -2 701.601 51.8599 4 -2 -9 -2 725.271 55.9224 1 -2 -9 -1 122.638 27.3563 1 -2 9 -1 82.5894 23.3702 4 -2 -9 0 132.932 28.9461 1 -2 -9 1 50.8739 20.2691 1 -2 -9 2 135.851 29.2412 1 -2 -9 3 46.6326 21.5543 1 -2 9 4 514.291 46.4755 3 -2 -9 4 539.598 54.8511 1 -2 -9 5 202.216 36.5355 1 -2 9 5 143.978 29.5457 3 -2 -9 6 153.698 37.7065 1 -2 9 6 124.962 29.3689 3 -2 9 7 12.3072 18.5398 3 -2 -10 -7-0.44380 20.2947 1 -2 -10 -6-3.69950 17.1982 1 -2 10 -6 36.4861 25.1476 4 -2 10 -5 129.001 29.7009 4 -2 -10 -5 70.4841 24.1584 1 -2 10 -4 36.2101 23.4310 4 -2 -10 -4 58.3978 24.5274 1 -2 10 -3 579.530 50.9306 4 -2 -10 -3 573.760 52.9358 1 -2 -10 -2 730.753 58.8372 1 -2 10 -2 683.608 52.8857 4 -2 -10 -1 186.890 33.3746 1 -2 10 -1 178.639 29.1591 4 -2 -10 0 401.864 44.7332 1 -2 -10 1 240.166 38.6325 1 -2 -10 2 331.725 43.6880 1 -2 -10 3 448.225 50.8586 1 -2 -10 4 511.185 55.5743 1 -2 10 4 396.825 44.5622 3 -2 10 5 142.186 28.7533 3 -2 -10 5 89.7769 31.1151 1 -2 10 6 81.4679 27.4576 3 -2 -10 6 78.2431 29.5987 1 -2 10 7 37.1947 23.3800 3 -2 -11 -6 52.0372 22.8157 1 -2 -11 -5 18.2758 18.6068 1 -2 11 -5 106.075 29.8323 4 -2 -11 -4 25.7279 22.0932 1 -2 11 -4 21.9308 24.4824 4 -2 -11 -3 87.3330 28.4010 1 -2 11 -3 105.112 28.4713 4 -2 11 -2 588.661 50.7003 4 -2 -11 -2 618.858 56.3244 1 -2 11 -1 532.035 47.3680 4 -2 -11 -1 616.579 56.5444 1 -2 -11 0 254.451 41.1536 1 -2 -11 1 348.002 46.5659 1 -2 -11 2 793.055 66.5872 1 -2 -11 3 80.3432 33.0277 1 -2 -11 4 143.964 34.1731 1 -2 11 5 5.30099 20.4486 3 -2 -11 5-1.31743 22.3798 1 -2 11 6 78.7583 26.3506 3 -2 -11 6 177.106 41.9568 1 -2 -12 -5 81.9350 31.0426 1 -2 12 -5 79.5355 28.2371 4 -2 -12 -4 48.9108 26.4065 1 -2 12 -4 11.5123 23.0339 4 -2 12 -3 26.6884 21.9894 4 -2 -12 -3 60.7784 23.8925 1 -2 -12 -2 15.9752 19.3079 1 -2 12 -2 6.83542 18.5015 4 -2 -12 -1 487.237 54.1261 1 -2 -12 0 593.749 59.2516 1 -2 -12 1 37.3313 25.0229 1 -2 -12 2 161.582 36.4038 1 -2 -12 3 46.3830 23.1507 1 -2 -12 4 65.6579 25.9201 1 -2 -12 5 13.9099 26.1587 1 -2 12 5 36.8384 22.0170 3 -2 12 6 45.5638 25.6128 3 -2 -12 6 66.9571 31.9664 1 -2 -13 -4 213.375 41.6137 1 -2 13 -4 132.530 31.7904 4 -2 -13 -3 33.2872 25.2436 1 -2 13 -3 57.8444 25.9873 4 -2 13 -2 19.2183 18.2884 4 -2 -13 -2 26.7524 24.3606 1 -2 -13 -1 456.722 54.4993 1 -2 -13 0 230.872 40.6091 1 -2 -13 1 35.2154 23.8711 1 -2 -13 2 61.6130 27.2197 1 -2 -13 3 32.6026 25.7109 1 -2 -13 4 2.36357 26.1182 1 -2 13 5 43.5173 26.4042 3 -2 -13 5 21.9712 26.6360 1 -2 14 -3 30.5779 23.1438 4 -2 -14 -2-5.34947 20.4166 1 -2 14 -2 8.19028 19.4370 4 -2 -14 -1 20.5536 17.6231 1 -2 -14 0-5.20100 23.0105 1 -2 -14 1 22.3273 22.3201 1 -2 -14 2 41.5426 24.0105 1 -2 -14 3-29.7144 35.0938 1 -2 15 -3 19.3472 20.4484 4 -1 0 -10-19.0561 23.1819 4 -1 0 -9 311.736 37.0409 4 -1 0 -8-3.98445 18.2362 4 -1 0 -7 71.6983 20.7531 4 -1 0 -7 62.0914 18.6914 3 -1 0 -6 18.9219 14.4743 3 -1 0 -6-1.72428 15.7778 4 -1 0 -5 527.770 34.5222 4 -1 0 -5 595.755 34.5532 3 -1 0 -4 1.62518 8.56434 3 -1 0 -4-15.6838 15.1600 4 -1 0 -3 1863.59 43.2469 3 -1 0 -3 1785.27 49.0782 4 -1 0 -2-0.63939 5.26878 3 -1 0 -2 6.93679 12.0533 4 -1 0 -1 131219. 238.372 1 -1 0 -1 132471. 365.986 4 -1 0 0 5.16985 7.06863 1 -1 0 6-6.87659 16.0358 3 -1 0 7 2279.93 90.5177 3 -1 0 8-47.3101 21.8688 3 -1 0 9-11.9434 24.8763 3 -1 0 10-0.54341 22.7630 3 -1 1 -10 0.32927 20.5564 4 -1 -1 -10-5.62759 21.4311 4 -1 -1 -9 318.957 37.2056 4 -1 1 -9 261.992 34.9182 4 -1 1 -8 22.9682 22.7639 4 -1 -1 -8 8.76487 17.5328 4 -1 1 -7 286.303 30.3508 3 -1 -1 -7 260.027 28.8572 4 -1 1 -7 279.604 31.4469 4 -1 -1 -6 216.915 26.3267 4 -1 1 -6 231.542 25.3809 3 -1 1 -6 263.472 29.5195 4 -1 1 -5 1455.26 52.9262 3 -1 -1 -5 1520.88 52.6653 4 -1 1 -5 1481.23 55.5969 4 -1 1 -4 168.222 20.4825 4 -1 1 -4 176.881 17.4508 3 -1 -1 -4 153.473 18.9101 4 -1 1 -3 292.018 18.1280 3 -1 1 -3 308.474 23.7766 4 -1 -1 -3 284.876 20.6179 4 -1 1 -2 2781.80 41.4317 3 -1 -1 -2 2829.71 55.0568 4 -1 1 -2 2799.83 58.4162 4 -1 1 -1 15618.3 129.790 4 -1 -1 -1 15514.8 107.237 1 -1 1 -1 15556.9 64.1378 3 -1 -1 0 38237.0 178.696 1 -1 1 1 2241.56 46.8738 2 -1 -1 1 2200.92 51.3972 1 -1 1 2 1416.56 32.5158 2 -1 1 3 2954.37 38.8958 2 -1 -1 6 323.050 34.1647 3 -1 1 6 318.301 33.5390 3 -1 1 7 573.786 47.1534 3 -1 -1 7 414.422 40.7626 3 -1 1 8 507.260 47.8148 3 -1 -1 8 565.523 51.1740 3 -1 1 9 246.659 40.2083 3 -1 -1 9 190.497 36.8220 3 -1 1 10-6.02338 22.9366 3 -1 -1 10 13.3622 20.7169 3 -1 2 -10 25.6416 22.8833 4 -1 2 -9 65.4591 23.6918 4 -1 -2 -9 11.8530 18.2462 4 -1 -2 -8 373.959 35.4798 4 -1 2 -8 415.786 41.7603 4 -1 2 -7 582.055 42.2949 3 -1 2 -7 576.852 43.0099 1 -1 -2 -7 635.101 40.7785 4 -1 2 -7 624.104 45.2440 4 -1 2 -6 415.851 35.3630 4 -1 2 -6 411.655 33.2609 3 -1 -2 -6 371.489 29.8263 4 -1 2 -5 803.500 43.1345 4 -1 2 -5 747.910 38.4653 1 -1 -2 -5 747.037 36.4420 4 -1 2 -5 815.709 40.6074 3 -1 -2 -4 846.375 34.9432 4 -1 2 -4 861.521 35.5101 1 -1 2 -4 888.249 37.6519 3 -1 2 -4 940.442 43.2955 4 -1 -2 -3 1336.50 39.3292 4 -1 2 -3 1321.14 38.7509 3 -1 2 -3 1395.65 47.2341 4 -1 2 -3 1414.62 35.7189 1 -1 2 -2 1649.35 35.5496 3 -1 2 -2 1602.32 25.4461 1 -1 -2 -2 1594.29 40.3915 4 -1 2 -2 1638.54 47.6099 4 -1 -2 -1 6653.01 82.2452 1 -1 2 -1 6626.55 102.885 2 -1 2 -1 6570.39 88.4521 4 -1 2 0 4801.24 80.6504 2 -1 -2 0 4713.09 72.2655 1 -1 -2 1 6995.85 98.9553 1 -1 2 1 6921.67 87.3950 2 -1 -2 2 268.000 24.9225 1 -1 2 2 262.919 16.9676 2 -1 -2 6 141.927 24.9703 3 -1 2 6 148.368 24.2610 3 -1 2 7 201.993 30.8601 3 -1 -2 7 124.891 26.8902 3 -1 2 8 333.635 40.5074 3 -1 -2 8 259.114 36.5281 3 -1 2 9 128.747 32.1546 3 -1 -2 9 124.374 30.3878 3 -1 2 10 25.6617 24.9454 3 -1 3 -9 42.9222 24.1589 4 -1 -3 -9 1.84741 17.3808 4 -1 -3 -8 344.306 32.8951 4 -1 3 -8 472.087 43.3382 4 -1 3 -7 150.282 25.5224 4 -1 -3 -7 146.556 22.6482 4 -1 3 -7 134.402 23.8718 1 -1 3 -6 229.200 30.6199 4 -1 3 -6 237.451 26.5528 3 -1 -3 -6 215.416 22.9135 4 -1 -3 -5 11.8172 12.5610 4 -1 3 -5 19.9103 18.8823 4 -1 3 -5 36.5882 10.9591 1 -1 3 -5 12.6075 10.4906 3 -1 -3 -4 471.026 25.8441 4 -1 3 -4 470.755 29.2338 3 -1 3 -4 447.129 26.1609 1 -1 3 -4 454.929 32.1539 4 -1 3 -3 535.226 31.8474 4 -1 3 -3 591.141 28.1506 3 -1 3 -3 579.304 23.4238 1 -1 -3 -3 568.008 25.7929 4 -1 3 -2 2089.83 31.6879 1 -1 3 -2 2113.33 56.9369 4 -1 3 -2 2045.93 64.5291 2 -1 3 -1 941.138 36.0266 4 -1 -3 -1 987.772 37.5695 1 -1 3 -1 913.446 42.0766 2 -1 3 0 2024.37 49.7406 4 -1 -3 0 2083.38 54.3917 1 -1 3 0 2003.73 55.2822 2 -1 -3 1 2922.92 68.3554 1 -1 3 1 2855.19 61.1526 2 -1 -3 2 3032.90 76.9880 1 -1 -3 3 201.424 25.3796 1 -1 3 6 2228.78 86.1735 3 -1 3 7 1770.50 83.6126 3 -1 3 8 0.77991 17.6571 3 -1 3 9 42.0152 22.5693 3 -1 3 10 48.8428 27.2423 3 -1 4 -9 4.12249 22.6635 4 -1 -4 -8 423.069 33.6315 4 -1 4 -8 422.323 41.9453 4 -1 4 -7 349.911 36.5865 4 -1 4 -7 304.695 31.4816 1 -1 -4 -7 353.901 28.9611 4 -1 4 -6 237.961 27.6852 3 -1 4 -6 249.717 32.8638 4 -1 -4 -6 225.095 21.8376 4 -1 4 -5 442.506 32.8990 3 -1 4 -5 444.702 29.8451 1 -1 -4 -5 476.214 27.5104 4 -1 4 -5 486.696 37.8545 4 -1 4 -4 2338.49 70.3292 4 -1 4 -4 2460.38 66.4391 3 -1 4 -4 2429.71 60.0862 1 -1 -4 -4 2450.14 54.2630 4 -1 4 -3 1357.09 51.4425 4 -1 4 -3 1304.79 57.8007 2 -1 4 -3 1352.06 44.6043 3 -1 4 -3 1299.23 36.9140 1 -1 4 -2 897.502 40.0931 4 -1 4 -2 827.434 43.5677 2 -1 4 -2 843.306 23.6304 1 -1 4 -1 3032.99 76.4313 2 -1 4 -1 2950.53 64.3925 4 -1 -4 -1 3114.79 70.6737 1 -1 4 0 799.005 33.8901 4 -1 -4 0 880.098 40.0176 1 -1 4 0 847.925 39.0687 2 -1 -4 1 3164.56 76.6461 1 -1 -4 2 5627.97 109.534 1 -1 -4 3 67.0853 18.7719 1 -1 4 5 803.551 49.5377 3 -1 4 6 2164.24 86.3282 3 -1 4 7 85.8031 26.1361 3 -1 4 8 126.194 29.7657 3 -1 4 9 110.673 32.6651 3 -1 5 -9 116.170 31.8155 4 -1 5 -8 29.6818 22.0643 4 -1 -5 -8 45.0029 15.0325 4 -1 5 -7 103.013 26.3436 4 -1 -5 -7 80.9146 16.0709 4 -1 5 -7 68.5874 17.2403 1 -1 5 -6 301.837 31.1296 3 -1 -5 -6 278.495 23.2185 4 -1 5 -6 332.125 35.4745 4 -1 -5 -5 3.48763 9.04367 4 -1 5 -5 13.0792 16.8296 4 -1 5 -5 5.71941 12.1422 3 -1 5 -5 13.0728 9.36426 1 -1 5 -4 35.8190 17.2558 4 -1 5 -4 29.7549 9.90996 1 -1 5 -4 38.8410 12.7240 3 -1 5 -4 49.7693 18.2007 2 -1 5 -3 2333.37 68.6829 4 -1 5 -3 2226.23 77.4427 2 -1 5 -3 2188.74 50.7843 1 -1 5 -2 800.745 39.2089 4 -1 5 -2 737.849 43.8362 2 -1 -5 -2 842.123 41.7856 1 -1 5 -1 2199.54 69.2773 2 -1 -5 -1 2207.99 65.8590 1 -1 5 -1 2179.60 58.1153 4 -1 5 0 409.188 25.9187 4 -1 -5 0 450.592 31.8351 1 -1 5 0 474.277 32.5970 2 -1 -5 1 1347.40 54.2269 1 -1 -5 2 5448.23 113.765 1 -1 -5 3 794.049 47.5829 1 -1 -5 4 1835.13 75.8444 1 -1 5 5 279.272 31.8277 3 -1 5 6 1784.00 81.1140 3 -1 5 7 807.382 60.2813 3 -1 5 8 227.442 37.4196 3 -1 5 9 42.9305 24.9252 3 -1 6 -8 11.1254 22.3612 4 -1 6 -7 306.961 38.0670 4 -1 -6 -7 243.250 22.1838 4 -1 6 -7 249.900 29.9773 1 -1 6 -6 187.731 28.6855 4 -1 -6 -6 225.843 19.7882 4 -1 6 -5 100.434 25.1657 4 -1 6 -5 129.941 18.0813 1 -1 6 -5 138.534 21.3793 3 -1 6 -4 78.5706 23.1780 4 -1 6 -4 98.7382 23.4064 2 -1 6 -4 58.1545 15.4952 3 -1 6 -4 92.7824 14.4107 1 -1 6 -3 1461.26 57.6707 4 -1 6 -3 1420.03 65.4207 2 -1 6 -3 1422.47 43.7901 1 -1 6 -2 642.387 42.7164 2 -1 6 -2 588.141 36.8665 4 -1 -6 -2 587.224 37.4825 1 -1 6 -1 372.514 27.3137 4 -1 6 -1 368.837 32.7586 2 -1 -6 -1 333.626 28.9569 1 -1 6 0 2218.36 58.9760 4 -1 -6 0 2271.09 72.9328 1 -1 -6 1 7312.84 133.764 1 -1 -6 2 1677.04 67.2396 1 -1 -6 3 1517.66 67.6354 1 -1 6 4 308.329 32.0905 3 -1 -6 4 256.597 32.3478 1 -1 6 5 3700.39 111.467 3 -1 6 6 553.738 49.0113 3 -1 6 7 185.004 32.1629 3 -1 6 8 459.138 51.5598 3 -1 6 9-12.5123 24.1762 3 -1 7 -8 11.3321 24.6812 4 -1 7 -7 895.129 58.7315 4 -1 7 -6 157.769 28.6012 4 -1 7 -6 211.042 24.6381 1 -1 7 -5 366.218 33.8432 3 -1 7 -5 347.531 38.1130 2 -1 7 -5 397.700 37.7875 4 -1 7 -4 525.551 41.2071 4 -1 7 -4 534.016 32.0425 1 -1 7 -4 477.255 42.5908 2 -1 7 -3 1077.58 51.6763 4 -1 7 -3 1084.67 59.8746 2 -1 7 -3 1074.79 40.5089 1 -1 7 -2 914.553 52.9474 2 -1 7 -2 859.713 44.3005 4 -1 -7 -2 856.290 48.1045 1 -1 7 -1 308.855 26.1628 4 -1 -7 -1 302.863 30.0020 1 -1 7 -1 279.892 28.7613 2 -1 -7 0 1020.39 53.1022 1 -1 7 0 1070.42 43.1584 4 -1 -7 1 1879.68 72.5752 1 -1 -7 2 944.891 54.6547 1 -1 -7 3 873.787 54.4240 1 -1 -7 4 462.611 43.1430 1 -1 -7 5 2156.62 92.8478 1 -1 7 5 2193.09 89.5286 3 -1 7 6 909.047 61.8011 3 -1 7 7 112.266 28.4718 3 -1 7 8 37.7156 24.9123 3 -1 7 9 69.9132 26.9344 3 -1 8 -8 69.8253 25.7407 4 -1 8 -7 454.359 44.2850 4 -1 8 -6 637.463 50.0508 4 -1 8 -6 582.118 41.9230 1 -1 8 -5 85.5097 24.6620 4 -1 8 -4 136.795 27.5973 4 -1 8 -3 129.908 26.9630 2 -1 8 -3 126.389 23.1219 4 -1 -8 -3 109.958 22.9682 1 -1 8 -2 1180.71 52.8967 4 -1 8 -2 1135.32 60.7248 2 -1 -8 -2 1129.20 59.3215 1 -1 -8 -1 424.451 38.2217 1 -1 8 -1 467.733 32.4822 4 -1 8 -1 489.961 40.3084 2 -1 -8 0 799.212 49.8286 1 -1 8 0 765.800 38.7794 4 -1 -8 1 113.066 22.7995 1 -1 -8 2 851.609 53.8521 1 -1 -8 3 543.797 47.1651 1 -1 -8 4 455.338 43.8762 1 -1 8 5 190.502 31.4707 3 -1 -8 5 225.331 34.8379 1 -1 8 6 863.125 62.1093 3 -1 8 7 18.7933 19.3795 3 -1 8 8 97.6961 30.4509 3 -1 9 -7 89.2450 27.0418 4 -1 9 -6 674.465 51.5812 4 -1 9 -5 118.211 27.9616 4 -1 9 -5 165.188 22.4983 1 -1 9 -4 156.425 28.8043 4 -1 9 -4 144.800 19.6423 1 -1 -9 -4 156.098 28.9524 1 -1 -9 -3 28.6125 18.6726 1 -1 9 -3 12.6351 19.5124 4 -1 9 -2 1107.47 53.2018 4 -1 -9 -2 1125.53 63.0432 1 -1 -9 -1 769.699 52.4046 1 -1 9 -1 826.456 43.9681 4 -1 9 0-12.9802 14.1514 4 -1 -9 0-0.06443 15.4993 1 -1 -9 1 111.909 24.1404 1 -1 -9 2 557.678 46.9063 1 -1 -9 3 110.947 24.0952 1 -1 -9 4 263.022 36.6775 1 -1 9 5 1086.95 68.4566 3 -1 -9 5 1165.56 73.7293 1 -1 -9 6 26.7082 22.1011 1 -1 9 6 32.2479 21.7921 3 -1 9 7 198.758 36.9322 3 -1 9 8 42.2706 21.0287 3 -1 10 -7 24.9828 20.8339 4 -1 10 -6 7.73093 18.6097 4 -1 10 -5 68.2045 24.7318 4 -1 10 -5 76.3603 16.4547 1 -1 10 -4 101.523 24.7054 4 -1 -10 -4 67.2281 21.5414 1 -1 -10 -3 211.945 32.3870 1 -1 10 -3 144.041 25.8795 4 -1 10 -2 2107.73 74.0390 4 -1 -10 -2 2084.55 89.5173 1 -1 -10 -1 663.321 52.4993 1 -1 10 -1 707.866 42.6075 4 -1 -10 0 1356.50 73.4217 1 -1 10 0 1249.87 52.9807 4 -1 -10 1 654.011 52.3742 1 -1 -10 2 74.9622 24.6048 1 -1 -10 3 238.220 34.3289 1 -1 -10 4 460.647 48.5314 1 -1 10 5 345.682 41.9761 3 -1 -10 5 342.145 44.9113 1 -1 10 6 230.980 37.4231 3 -1 -10 6 224.952 39.3317 1 -1 10 7 26.4638 21.2035 3 -1 11 -6-33.9668 26.6091 4 -1 -11 -6 4.97175 17.2405 1 -1 -11 -5 124.185 30.7986 1 -1 11 -5 118.546 28.7073 4 -1 -11 -4 270.552 39.6298 1 -1 11 -4 186.649 30.5151 4 -1 -11 -3 29.2833 19.0468 1 -1 11 -3 0.88500 21.8792 4 -1 -11 -2 1089.46 69.2843 1 -1 11 -2 1051.03 54.8472 4 -1 -11 -1 1833.12 88.2943 1 -1 11 -1 1893.50 70.0344 4 -1 11 0 1858.79 66.5135 4 -1 -11 0 1977.12 91.8274 1 -1 -11 1 241.383 35.1806 1 -1 -11 2 608.274 54.6278 1 -1 -11 3 811.114 63.2665 1 -1 -11 4-4.88971 19.7126 1 -1 -11 5 82.3410 27.0114 1 -1 11 6 53.2039 24.6355 3 -1 -11 6 141.066 37.9968 1 -1 11 7 76.5960 25.6641 3 -1 -12 -6 13.2024 24.4830 1 -1 12 -6-7.19605 20.8630 4 -1 -12 -5 285.600 42.6906 1 -1 12 -5 270.289 37.6209 4 -1 -12 -4 227.721 37.6869 1 -1 12 -4 164.746 31.4915 4 -1 -12 -3 238.856 38.5322 1 -1 12 -3 184.409 29.7906 4 -1 -12 -2 52.9755 23.4888 1 -1 12 -2 33.6848 16.1339 4 -1 12 -1 210.976 27.6139 4 -1 -12 -1 183.131 34.5150 1 -1 12 0 944.819 49.7855 4 -1 -12 0 1065.83 71.4738 1 -1 -12 1 891.958 67.0379 1 -1 -12 2 48.0276 24.9142 1 -1 -12 3 873.659 68.1027 1 -1 -12 4-3.13249 21.9595 1 -1 -12 5-0.44421 20.4449 1 -1 -12 6-1.54365 21.4996 1 -1 12 6 19.5792 18.9495 3 -1 -13 -5 188.868 39.3350 1 -1 13 -5 127.704 32.7994 4 -1 13 -4 8.77247 21.8560 4 -1 -13 -4 45.8422 29.0174 1 -1 13 -3 245.543 33.2434 4 -1 -13 -3 283.028 42.1728 1 -1 -13 -2 46.7553 25.0542 1 -1 13 -2 22.4123 16.1271 4 -1 -13 -1 54.4407 25.3763 1 -1 13 -1 27.7495 16.9020 4 -1 -13 0 191.487 32.9776 1 -1 13 0 240.760 27.6316 4 -1 -13 1 123.271 31.8611 1 -1 -13 2 78.6305 25.3707 1 -1 -13 3-7.24391 18.2390 1 -1 -13 4 5.21764 20.2813 1 -1 -13 5 30.6104 26.4592 1 -1 -13 6 70.9796 31.3296 1 -1 14 -5-13.0238 28.3451 4 -1 14 -4 156.024 31.1755 4 -1 -14 -4 96.0457 32.3935 1 -1 -14 -3 72.6504 27.5769 1 -1 14 -3 109.698 24.9144 4 -1 -14 -2 22.4955 23.6068 1 -1 14 -2 16.0886 15.6147 4 -1 14 -1 67.3333 20.0096 4 -1 -14 -1 86.0844 27.2176 1 -1 -14 0 128.335 33.5228 1 -1 -14 1 67.3344 28.3874 1 -1 -14 2 30.4406 23.2376 1 -1 -14 3 51.1737 28.0233 1 -1 -14 4-43.3928 24.6518 1 -1 -14 5 40.1221 24.1724 1 -1 -14 6 12.2866 27.9450 1 -1 15 -4 163.757 31.5398 4 -1 15 -3 57.9406 23.8027 4 -1 -15 -2 89.5690 32.4383 1 -1 15 -2 95.1938 24.1161 4 -1 -15 -1 42.1992 21.5928 1 -1 15 -1 53.8444 19.4267 4 -1 -15 0 31.7361 21.9350 1 -1 -15 1 68.9977 29.9883 1 -1 -15 2 114.273 35.2822 1 -1 -15 3 78.2850 30.6290 1 -1 -15 4 64.1948 25.8147 1 -1 16 -4 68.3978 25.0325 4 -1 16 -3 71.0819 23.8759 4 -1 16 -2 5.34114 17.2324 4 -1 -16 1 135.169 36.9909 1 0 0 -11 42.4963 21.7160 4 0 0 -10 46.1470 21.2489 4 0 0 -6 222.797 27.2251 3 0 0 -5 8.50233 12.9224 3 0 0 -4 4820.58 89.9291 3 0 0 -3-4.64217 8.42668 3 0 0 -2 2374.11 44.9954 3 0 0 3-2.07742 11.7355 3 0 0 4 4752.98 91.5075 3 0 0 5-0.84737 13.5673 3 0 0 5 1.06768 8.73750 2 0 0 6 225.517 27.9686 3 0 0 6 219.082 20.9231 2 0 0 7 38.8812 12.4855 2 0 0 7 1.87257 15.4415 3 0 0 8 1479.21 75.5317 3 0 0 8 1493.80 53.0501 2 0 0 9-3.35648 17.1324 3 0 0 10 28.9078 22.3701 3 0 -1 -10 51.5096 21.0543 4 0 1 -10 30.1161 20.2633 4 0 -1 -9 139.318 24.4814 4 0 -1 -6 103.331 21.0132 3 0 1 -6 77.5176 18.5550 3 0 -1 -5 3108.55 82.9207 3 0 1 -5 3247.45 83.4344 3 0 -1 -4 4871.39 91.9129 3 0 1 -4 4807.72 91.0552 3 0 1 -3 1204.12 40.1235 3 0 -1 -3 1117.10 39.1420 3 0 -1 -2 1630.33 39.3489 3 0 1 -2 1604.91 37.7117 3 0 1 -2 1572.56 32.2667 2 0 1 -1 26234.8 99.7483 2 0 -1 1 26041.0 117.147 1 0 -1 2 1649.26 32.1625 2 0 1 3 1133.57 39.5621 3 0 -1 3 1120.78 38.7441 3 0 -1 3 1200.31 32.6386 2 0 1 4 4751.65 92.3974 3 0 -1 4 4742.64 90.7406 3 0 -1 4 4897.18 73.0366 2 0 1 5 3060.34 83.1958 3 0 -1 5 3122.29 83.1126 3 0 -1 5 3071.27 64.4924 2 0 -1 6 76.7781 14.3165 2 0 1 6 87.2936 19.8925 3 0 -1 6 88.6839 19.8659 3 0 -1 7 53.7811 13.3303 2 0 1 7 62.7303 19.9145 3 0 -1 7 69.6221 20.2200 3 0 1 7 58.0483 13.3424 2 0 1 8 438.227 44.1406 3 0 -1 8 489.032 45.7372 3 0 1 8 513.466 33.9979 2 0 1 9 111.612 26.2065 3 0 -1 9 154.079 30.7759 3 0 1 10-7.25506 21.1361 3 0 -1 10 32.3227 22.8368 3 0 -2 -10 136.085 25.4722 4 0 2 -10 151.612 28.5528 4 0 -2 -9 242.347 27.6275 4 0 2 -7 333.091 36.5732 1 0 2 -6 1175.84 56.8646 3 0 2 -6 1016.59 56.8251 1 0 2 -5 1465.63 57.9936 3 0 2 -4 353.751 27.0817 3 0 2 -4 344.454 27.6911 1 0 2 -3 2114.48 57.1920 1 0 2 -3 2196.81 54.8485 3 0 2 -3 2175.70 48.0925 2 0 2 -2 6565.49 80.4375 3 0 2 -2 6724.22 73.0266 2 0 -2 0 4897.17 52.4397 1 0 -2 1 318.738 16.5115 1 0 -2 2 6665.11 84.3423 1 0 2 3 2162.55 56.0673 3 0 -2 3 2074.56 53.5973 3 0 2 4 318.477 26.4911 3 0 -2 4 340.277 26.4646 3 0 -2 4 312.896 20.4738 2 0 2 5 1408.07 58.8937 3 0 -2 5 1414.07 57.3595 3 0 -2 5 1433.82 44.5642 2 0 2 6 1138.10 57.7470 3 0 -2 6 1056.35 55.4798 3 0 2 7 379.723 39.6021 3 0 -2 7 397.454 38.6368 3 0 2 8 40.8725 20.6949 3 0 -2 8 26.3406 18.0434 3 0 2 9 178.353 31.5021 3 0 2 10 115.402 30.6939 3 0 -3 -10 29.0202 18.6995 4 0 3 -10 55.8274 23.0598 4 0 -3 -9 112.880 21.1486 4 0 3 -7 1408.34 72.2043 1 0 3 -6 329.656 32.9321 3 0 3 -6 369.331 36.0641 1 0 3 -5 946.024 47.5700 3 0 3 -4 180.942 20.4558 3 0 3 -4 163.679 20.3686 1 0 3 -4 179.141 17.6548 2 0 3 -3 804.768 35.9718 3 0 3 -3 794.891 37.1715 1 0 3 -3 801.544 32.6218 2 0 3 -2 2334.62 54.2028 1 0 -3 0 3395.68 53.7198 1 0 -3 1 6273.24 77.2834 1 0 -3 2 2468.23 55.9562 1 0 3 3 807.997 39.1674 3 0 3 4 159.762 21.9337 3 0 3 5 885.815 47.7455 3 0 3 6 365.853 35.5257 3 0 3 7 1449.83 73.4649 3 0 3 8 406.883 44.3162 3 0 3 9 54.4538 22.1635 3 0 3 10 43.0836 27.8624 3 0 4 -10 21.1990 16.9912 4 0 -4 -9 31.6957 15.4381 4 0 4 -9 89.7342 22.8925 4 0 -4 -8 83.6098 17.8910 4 0 4 -7 1458.67 73.8868 1 0 4 -6 611.618 43.6888 3 0 4 -6 604.921 44.6691 1 0 4 -5 628.830 40.6228 3 0 4 -4 717.794 39.0704 3 0 4 -4 746.951 36.8467 2 0 4 -4 700.352 39.9056 1 0 4 -3 10304.5 130.382 3 0 4 -3 10129.9 133.771 1 0 4 -3 10084.1 120.648 2 0 4 -2 2528.76 60.7185 1 0 4 0 3711.92 40.0773 4 0 -4 0 3786.72 66.1999 1 0 -4 1 3811.95 69.2742 1 0 -4 2 2474.69 61.4282 1 0 -4 3 10102.1 134.932 1 0 4 4 748.807 43.1392 3 0 4 5 576.536 41.0248 3 0 4 6 587.775 44.7090 3 0 4 7 1455.30 74.7272 3 0 4 8 48.8237 24.1677 3 0 4 9 12.5508 19.9467 3 0 4 10 29.8025 20.9225 3 0 5 -9 174.565 29.7706 4 0 -5 -8 427.977 29.2291 4 0 -5 -7 451.826 26.8889 4 0 5 -6 22.2052 13.8730 1 0 5 -5 997.226 51.9712 3 0 5 -5 930.062 51.3475 1 0 5 -5 959.458 46.8528 2 0 5 -4 481.090 34.2384 3 0 5 -4 425.280 30.7668 2 0 5 -3 1722.17 58.2758 1 0 5 -3 1801.24 55.6001 2 0 5 -2 2443.46 63.3489 1 0 -5 0 6991.95 100.524 1 0 5 0 6917.27 61.3540 4 0 -5 1 727.235 34.4852 1 0 5 1 682.169 15.7536 4 0 -5 2 2426.88 65.4775 1 0 -5 3 1743.83 59.9282 1 0 5 4 409.443 35.0043 3 0 -5 4 451.623 34.5701 1 0 5 5 940.399 53.4677 3 0 5 6 12.3390 18.5978 3 0 5 7 362.429 40.6033 3 0 5 8 400.934 46.0484 3 0 5 9 155.664 33.7130 3 0 5 10 14.0845 25.9065 3 0 6 -9 277.744 35.7675 4 0 -6 -8 58.7587 14.2070 4 0 -6 -7 127.724 15.7153 4 0 6 -6 1441.80 70.8456 1 0 6 -6 1557.05 64.9079 2 0 -6 -6 1590.79 38.5902 4 0 6 -5 293.579 30.8794 3 0 6 -5 284.792 28.6402 2 0 6 -5 274.004 29.1698 1 0 -6 -5 316.439 15.2352 4 0 6 -4 30.2396 14.4154 2 0 -6 -4 31.4698 4.85845 4 0 6 -4 34.4691 14.0431 3 0 6 -2 7727.05 120.310 1 0 6 -1 1864.49 55.5781 1 0 6 0 898.425 25.6538 4 0 -6 0 960.403 42.2284 1 0 -6 1 1863.71 59.0875 1 0 6 1 1796.81 29.6682 4 0 -6 2 7736.93 124.104 1 0 -6 3 105.459 18.8570 1 0 -6 4 24.4764 14.7688 1 0 6 5 310.730 35.5515 3 0 6 6 1509.33 74.8743 3 0 6 7 107.810 27.7674 3 0 6 8 22.8096 22.7548 3 0 6 9 246.264 42.8293 3 0 7 -9 56.1255 26.1312 4 0 7 -8 132.101 29.2572 4 0 -7 -7 247.897 17.5170 4 0 7 -6 2339.50 90.9886 1 0 7 -6 2478.46 86.6247 2 0 -7 -6 2424.09 42.2993 4 0 7 -5 154.657 24.2252 2 0 7 -5 158.153 24.8937 1 0 -7 -5 149.038 8.42137 4 0 7 -4 1499.06 64.6276 1 0 7 -4 1594.77 64.3150 2 0 7 -1 1681.75 42.2721 4 0 -7 -1 1647.80 59.2899 1 0 7 0 919.862 28.5304 4 0 -7 0 864.390 44.1321 1 0 -7 1 1670.46 60.4849 1 0 7 1 1667.11 31.5942 4 0 -7 2 2673.80 78.6607 1 0 -7 3 1509.58 62.9028 1 0 -7 4 1657.32 69.6229 1 0 7 5 192.542 29.5720 3 0 7 6 2416.72 97.1707 3 0 7 7 206.075 33.3256 3 0 7 8 49.5290 25.2893 3 0 7 9 22.6512 21.4492 3 0 8 -8 147.282 30.3674 4 0 8 -6 409.015 39.5512 2 0 8 -5 1038.81 58.9124 1 0 8 -5 951.763 56.0609 2 0 8 -4 158.706 25.1654 2 0 8 -4 104.661 21.2351 1 0 8 -3 66.4133 17.2299 1 0 8 -2 10.8455 11.6274 1 0 8 -1 1736.21 45.4257 4 0 -8 -1 1736.74 65.5661 1 0 -8 0 242.124 27.3872 1 0 8 0 230.324 17.3664 4 0 -8 1 1752.26 67.0337 1 0 8 1 1671.17 34.7600 4 0 -8 2 24.4171 13.5173 1 0 -8 3 49.9114 18.3743 1 0 -8 4 116.604 23.8396 1 0 -8 5 948.471 59.6179 1 0 8 5 912.896 61.1690 3 0 8 6 478.302 47.9075 3 0 8 7 393.241 45.1688 3 0 8 8 18.4727 21.9615 3 0 8 9 55.6077 29.9758 3 0 9 -8 88.9599 25.5233 4 0 9 -7 93.8718 26.9554 4 0 9 -6 566.348 43.6694 4 0 9 -6 490.393 45.3751 2 0 9 -5 745.761 52.1297 1 0 9 -5 709.206 50.7136 2 0 9 -4 164.059 25.2958 1 0 9 -4 251.942 30.7192 2 0 9 -3 804.766 40.7475 4 0 9 -3 766.873 47.8535 1 0 9 -2 217.899 23.0480 4 0 9 -2 121.021 20.5056 1 0 9 -1 610.242 30.4515 4 0 -9 -1 540.392 41.6621 1 0 9 0 716.136 30.2418 4 0 -9 0 747.207 47.6428 1 0 -9 1 534.829 40.8538 1 0 9 1 536.629 22.1055 4 0 -9 2 122.351 23.1583 1 0 -9 3 712.153 49.7878 1 0 -9 4 227.883 31.0681 1 0 -9 5 690.070 52.4993 1 0 9 6 445.342 47.4701 3 0 9 7 26.2110 17.6665 3 0 9 8 60.9428 27.7087 3 0 10 -7 173.745 31.7740 4 0 10 -6 256.847 33.0771 4 0 10 -5 178.692 28.0467 4 0 10 -4 213.590 29.2632 1 0 10 -4 252.003 28.8298 4 0 10 -3 45.0707 18.3378 4 0 10 -3 8.95980 10.7390 1 0 -10 -2 356.201 37.2368 1 0 10 -2 415.622 30.0344 4 0 10 -1 2992.19 67.9537 4 0 -10 -1 3004.36 99.1654 1 0 -10 0 263.345 32.4894 1 0 10 0 201.512 19.1524 4 0 10 1 3030.88 54.2347 4 0 -10 1 2971.92 98.2498 1 0 -10 2 288.254 33.3424 1 0 -10 3 21.7858 18.0305 1 0 -10 4 191.662 31.0346 1 0 -10 5 100.387 26.6849 1 0 10 6 178.788 36.0702 3 0 10 7 131.047 29.9136 3 0 10 8 1.92737 25.0924 3 0 11 -7 103.356 26.0667 4 0 11 -6 37.9634 23.3931 4 0 11 -5 40.6071 20.0762 4 0 11 -4 306.040 32.0202 4 0 -11 -3 669.989 53.8555 1 0 11 -3 647.963 40.0393 4 0 11 -2 211.598 24.5029 4 0 -11 -2 176.924 29.3747 1 0 11 -1 2632.12 67.9443 4 0 -11 -1 2502.37 97.1263 1 0 -11 0 2826.65 102.449 1 0 11 0 2887.06 65.5135 4 0 11 1 2608.17 53.1192 4 0 -11 1 2479.20 95.5546 1 0 -11 2 187.634 29.9368 1 0 -11 3 605.184 50.4862 1 0 -11 4 252.299 35.7811 1 0 -11 5 11.2255 17.0416 1 0 11 6 31.1520 17.9809 3 0 11 7 108.033 32.4938 3 0 12 -7 21.8334 21.6256 4 0 12 -6 65.0458 26.0018 4 0 12 -5 30.4683 22.1121 4 0 12 -4 963.768 54.5565 4 0 12 -3 330.678 32.0043 4 0 -12 -3 365.773 43.6514 1 0 12 -2 562.862 37.8008 4 0 -12 -2 570.856 51.1979 1 0 -12 -1 446.689 45.4745 1 0 12 -1 506.314 33.5379 4 0 -12 0 464.410 45.0822 1 0 12 0 487.146 28.9357 4 0 -12 1 496.465 47.3443 1 0 12 1 509.203 25.2594 4 0 -12 2 521.079 49.0846 1 0 -12 3 286.903 38.8996 1 0 -12 4 939.787 67.2536 1 0 -12 5 0.86809 19.2380 1 0 -12 6 70.3162 26.1061 1 0 12 6 53.5974 24.5863 3 0 12 7-1.52546 19.0603 3 0 13 -6 49.8204 25.2864 4 0 13 -5 37.2749 24.5180 4 0 13 -4 129.782 26.6631 4 0 -13 -4 71.9848 25.5811 1 0 13 -3 39.8938 19.9691 4 0 -13 -3 30.2567 20.1114 1 0 13 -2 6.22009 15.1119 4 0 -13 -2 29.7201 21.7097 1 0 -13 -1 27.7464 21.4303 1 0 13 -1 31.8379 14.6361 4 0 -13 0 35.4291 19.6790 1 0 13 0 73.9864 15.7498 4 0 -13 1 20.7398 18.7330 1 0 -13 2 17.0293 18.5581 1 0 -13 3 34.3165 20.9169 1 0 -13 4 69.0617 23.5205 1 0 -13 5-6.92786 16.9634 1 0 -13 6 41.3035 23.6001 1 0 13 6 71.0665 27.8656 3 0 14 -6 1.13221 20.3891 4 0 14 -5 28.9227 23.2741 4 0 -14 -5 29.9168 25.8857 1 0 14 -4 117.747 27.8425 4 0 -14 -4 53.8846 24.3171 1 0 14 -3 92.4270 23.3886 4 0 -14 -3 58.6285 27.0098 1 0 -14 -2 173.837 34.8295 1 0 14 -2 223.393 28.6793 4 0 -14 -1 113.397 31.6342 1 0 14 -1 103.697 19.8454 4 0 -14 0 151.920 33.1219 1 0 14 0 154.635 20.1258 4 0 -14 1 80.2885 27.6212 1 0 -14 2 203.242 35.4350 1 0 -14 3 83.5205 25.2224 1 0 -14 4 32.9923 21.1037 1 0 -14 5 44.7241 27.7363 1 0 -14 6 15.2857 21.7496 1 0 15 -5 13.6638 22.7095 4 0 15 -4 3.36293 21.9024 4 0 -15 -3 102.558 33.7317 1 0 15 -3 100.486 26.0106 4 0 -15 -2 66.1754 28.5839 1 0 15 -2 23.7648 18.0876 4 0 -15 -1 174.857 35.9428 1 0 15 -1 108.409 19.8861 4 0 -15 0 188.515 35.9433 1 0 -15 1 93.1998 25.2658 1 0 -15 2 54.0839 23.6906 1 0 -15 3 123.468 33.5018 1 0 -15 4-80.3618 30.3090 1 0 -15 5 18.1780 24.6436 1 0 16 -4 115.318 31.4037 4 0 16 -3 101.232 26.8427 4 0 -16 -2 28.1825 21.4549 1 0 -16 -1-0.49182 21.5121 1 0 -16 0 106.921 32.8987 1 0 -16 1 19.0104 22.1241 1 0 -16 2 48.7054 25.5831 1 0 -16 3 166.437 36.9656 1 0 -16 4 95.2094 32.9487 1 0 -17 1 41.6384 24.2348 1 0 -17 2 86.1441 29.7569 1 1 0 -6 2.73100 14.1278 3 1 0 -5 1131.08 54.6669 3 1 0 -4 0.03779 11.5154 3 1 0 -3 10015.9 123.555 3 1 0 -2-7.96889 6.91836 2 1 0 -2-2.55868 8.05468 3 1 0 -1 998.308 26.6297 3 1 0 -1 987.378 32.3445 1 1 0 0-2.02436 5.83258 1 1 0 2-1.76418 5.13950 3 1 0 3 1861.24 43.0484 3 1 0 4-2.46347 8.47435 3 1 0 5 596.010 34.4540 3 1 0 6-10.5244 12.5448 3 1 0 6-23.9792 17.7896 2 1 0 7 71.6516 18.9850 3 1 0 7 63.6557 19.1126 2 1 0 8-14.9377 19.7839 2 1 0 8-11.0421 17.6896 3 1 0 9 375.726 41.3408 3 1 0 9 387.384 42.2101 2 1 -1 -6 337.813 33.5156 3 1 1 -6 329.729 32.6467 3 1 1 -6 298.218 35.9163 1 1 -1 -5 94.1726 19.3113 3 1 1 -5 97.8527 18.8347 3 1 -1 -4 10151.2 142.016 3 1 1 -4 10156.8 141.794 3 1 -1 -3 3012.81 69.4531 3 1 1 -3 2966.31 68.2026 3 1 -1 -2 1407.29 41.0270 3 1 1 -2 1365.12 40.1052 3 1 1 -1 2191.43 40.1029 3 1 -1 -1 2177.31 46.5577 2 1 -1 0 37099.3 131.221 1 1 1 0 36591.4 172.788 1 1 1 2 2815.95 42.5940 3 1 1 2 2729.44 50.2906 4 1 1 3 293.705 18.7994 3 1 -1 3 273.186 18.0291 3 1 -1 3 270.862 26.5910 2 1 1 4 204.878 19.8870 3 1 -1 4 197.284 18.5774 3 1 1 5 1499.92 54.0452 3 1 -1 5 1444.11 52.5603 3 1 -1 6 172.058 26.2461 2 1 1 6 248.259 26.8740 3 1 -1 6 213.471 24.5130 3 1 -1 7 197.460 30.0181 2 1 1 7 282.536 30.6351 3 1 -1 7 249.011 29.2558 3 1 1 7 251.998 32.5771 2 1 -1 8 37.4590 21.2561 2 1 1 8-11.7573 17.3662 3 1 1 8-6.72766 17.6703 2 1 1 9 280.447 37.1506 2 1 1 9 324.929 39.9321 3 1 -1 9 332.223 38.4235 2 1 1 10 3.66376 21.0160 3 1 2 -6 147.476 26.5572 1 1 -2 -6 163.145 26.3392 3 1 2 -6 171.817 26.2488 3 1 -2 -5 389.955 33.6649 3 1 2 -5 375.209 32.7746 3 1 -2 -4 2410.80 72.4535 3 1 2 -4 2396.76 70.1112 3 1 -2 -3 398.993 28.3028 3 1 2 -3 337.730 25.3341 3 1 2 -2 255.092 19.1103 3 1 2 0 4775.35 71.3906 1 1 2 1 6562.47 75.5027 4 1 2 2 1622.03 37.3402 4 1 2 3 1339.41 40.1496 3 1 -2 3 1302.27 54.4208 2 1 2 4 870.372 38.3149 3 1 2 5 725.641 40.0009 3 1 -2 5 770.249 47.5263 2 1 2 6 386.752 33.5754 3 1 -2 6 334.346 34.7386 2 1 -2 7 631.567 47.7785 2 1 2 7 566.580 42.6699 3 1 2 8 430.337 42.0394 3 1 2 8 323.500 38.7540 2 1 -2 8 462.159 43.1156 2 1 -2 9 47.5987 19.9500 2 1 2 9 53.0932 22.6727 3 1 2 9 58.6889 20.4913 2 1 2 10 45.2202 23.6905 3 1 3 -6 2072.75 89.6606 1 1 3 -5 304.524 29.6402 3 1 3 -5 283.034 32.3835 1 1 3 -4 474.936 33.3957 3 1 3 -3 218.616 21.6636 3 1 3 -2 3102.94 65.0446 3 1 -3 1 918.779 19.8002 1 1 3 2 2094.90 39.7549 4 1 3 3 573.283 30.1526 3 1 3 4 434.512 29.3504 3 1 -3 5 41.0194 18.4830 2 1 3 5 35.4100 13.6915 3 1 3 6 255.978 28.7396 3 1 -3 6 260.267 31.6681 2 1 -3 7 174.128 27.9624 2 1 3 7 127.758 23.4052 3 1 3 8 409.263 41.5458 3 1 -3 8 488.967 43.4097 2 1 3 9 64.7258 23.9930 3 1 3 9 44.3325 20.5249 2 1 3 10 69.9389 26.9044 3 1 4 -5 846.140 48.6161 3 1 4 -5 814.760 53.5429 1 1 4 -5 785.404 28.7838 2 1 4 -4 1047.09 49.6797 3 1 4 -3 69.7823 15.1350 3 1 -4 -1 3089.16 60.6097 4 1 -4 0 799.350 31.4495 4 1 -4 1 3036.57 46.5139 1 1 -4 2 851.689 26.5774 1 1 4 2 902.949 24.4901 4 1 4 4 2455.63 70.7452 3 1 -4 4 2342.92 77.7346 2 1 4 5 418.975 33.6048 3 1 -4 5 475.030 38.8759 2 1 4 6 255.744 29.2975 3 1 -4 6 246.743 31.2812 2 1 4 7 387.923 39.2530 3 1 4 8 386.286 41.0425 3 1 4 9 41.4964 21.7071 3 1 4 10 8.52025 18.8859 3 1 5 -6 1777.33 48.7638 2 1 5 -5 321.304 32.6683 3 1 5 -5 292.402 34.2685 1 1 5 -5 330.129 23.7048 2 1 5 -4 1768.06 66.1163 3 1 5 -4 1704.91 72.8836 1 1 5 -3 840.237 42.5496 3 1 -5 -2 5318.45 80.2014 4 1 -5 -1 1356.08 40.3393 4 1 -5 0 413.884 23.9503 4 1 -5 1 2132.29 51.5881 4 1 -5 1 2180.76 47.8671 1 1 -5 2 735.170 29.0920 1 1 5 2 750.728 20.3614 4 1 5 4 46.2176 16.4755 3 1 5 5 5.29500 13.1315 3 1 5 6 262.091 30.8606 3 1 5 7 102.240 24.5931 3 1 5 8 37.7783 21.9694 3 1 5 9 113.411 29.2560 3 1 6 -6 441.130 29.0601 2 1 6 -5 3907.33 119.401 1 1 6 -4 301.842 33.0954 1 1 6 -4 248.887 27.1107 3 1 -6 -2 1647.16 44.8511 4 1 -6 -1 7113.89 91.2078 4 1 -6 0 2183.30 55.5226 1 1 -6 0 2161.42 51.1602 4 1 -6 1 350.797 22.8834 1 1 -6 1 394.605 24.9031 4 1 -6 2 604.366 30.0079 1 1 6 2 574.469 16.1236 4 1 -6 3 1445.10 48.2371 1 1 6 5 112.424 22.6655 3 1 6 6 234.141 31.5256 3 1 6 7 299.956 36.9993 3 1 6 8 29.3060 19.3010 3 1 6 9 35.3162 21.3670 3 1 7 -6 854.473 44.3193 2 1 7 -4 480.111 39.3037 3 1 7 -4 456.605 41.3688 1 1 7 -3 991.941 56.4148 1 1 -7 -3 923.928 33.4527 4 1 -7 -2 923.693 33.3992 4 1 -7 -1 1955.96 48.6177 4 1 -7 0 1082.87 37.5060 4 1 -7 0 1028.84 42.6954 1 1 -7 1 240.634 21.7429 1 1 -7 2 940.130 40.9915 1 1 7 2 816.193 15.1173 4 1 -7 3 1162.34 47.1737 1 1 7 5 380.725 37.8623 3 1 7 6 177.847 29.0598 3 1 7 7 806.348 58.8825 3 1 7 8 24.2729 19.3050 3 1 7 9 102.109 29.6006 3 1 8 -6 881.129 48.7532 2 1 -8 -4 444.153 23.4878 4 1 -8 -3 602.720 26.2019 4 1 8 -3 609.052 46.9593 1 1 -8 -2 834.517 31.4575 4 1 8 -2 813.175 50.9547 1 1 -8 -1 147.496 15.8580 4 1 -8 0 830.883 41.8646 1 1 -8 1 413.604 30.3711 1 1 -8 2 1207.94 50.6985 1 1 -8 3 114.896 17.7521 1 1 -8 4 104.849 19.5698 1 1 8 5 77.8842 23.5752 3 1 8 6 588.989 50.5401 3 1 8 7 429.210 45.6388 3 1 8 8 51.8448 22.5364 3 1 8 9 30.8621 21.6814 3 1 9 -6 38.5928 18.2609 2 1 -9 -5 1058.69 33.1103 4 1 -9 -4 296.827 17.7319 4 1 -9 -3 182.071 15.3336 4 1 -9 -2 569.937 25.9830 4 1 9 -2 542.741 43.8299 1 1 9 -1 107.766 20.0383 1 1 -9 0-1.20883 11.4206 1 1 -9 1 743.657 43.0230 1 1 -9 2 1126.29 53.0089 1 1 -9 3 20.8118 12.9215 1 1 -9 4 151.505 22.9249 1 1 9 6 518.173 49.5573 3 1 9 7 120.301 29.5997 3 1 9 8 54.0866 26.7938 3 1 -10 -4 461.649 19.3537 4 1 -10 -3 345.929 18.8187 4 1 -10 -1 732.577 47.7045 1 1 -10 0 1309.86 61.5412 1 1 -10 1 732.436 45.8321 1 1 -10 2 2075.14 76.6924 1 1 -10 3 164.140 24.7974 1 1 -10 4 115.206 22.7070 1 1 10 6 13.4517 19.0134 3 1 10 7 86.0131 26.6571 3 1 10 8 13.0824 19.1715 3 1 -11 -1 269.973 32.4214 1 1 -11 0 2000.80 81.2918 1 1 -11 1 1880.82 77.1344 1 1 11 1 1877.91 34.0538 4 1 -11 2 1084.32 59.8464 1 1 -11 3 26.0326 15.3909 1 1 -11 4 226.767 30.8918 1 1 -11 5 95.2747 23.7930 1 1 11 6 3.50211 18.8521 3 1 11 7 6.86443 20.5824 3 1 -12 -2 54.4347 21.6619 1 1 -12 -1 850.090 58.0454 1 1 -12 0 959.635 60.6257 1 1 12 0 1049.04 35.6169 4 1 -12 1 198.337 28.8344 1 1 12 1 180.116 11.7363 4 1 -12 2 27.7388 16.1372 1 1 -12 3 171.795 28.6958 1 1 -12 4 229.191 33.6377 1 1 -12 5 349.008 39.6404 1 1 12 6 24.0672 21.8515 3 1 12 7 27.8979 22.2573 3 1 -13 -3-11.3846 19.1833 1 1 -13 -2 133.706 29.2756 1 1 -13 -1 93.4665 26.6194 1 1 13 -1 178.753 21.0283 4 1 13 0 282.020 20.5268 4 1 -13 0 246.917 34.4648 1 1 -13 1 18.6528 16.7720 1 1 -13 2 25.3424 15.9264 1 1 -13 3 229.510 33.5535 1 1 -13 4 38.4021 20.4554 1 1 13 6 11.3511 22.7375 3 1 -14 -4 27.1035 24.7940 1 1 14 -3 195.645 27.5104 4 1 -14 -3 126.319 30.6854 1 1 14 -2 63.8258 19.2848 4 1 -14 -2 43.6566 22.8932 1 1 14 -1 83.1986 17.3271 4 1 -14 -1 60.0439 22.2529 1 1 -14 0 128.449 28.6688 1 1 -14 1 74.3873 24.4229 1 1 -14 2 48.5400 20.2261 1 1 -14 3 83.7017 24.1060 1 1 15 -5 78.2719 27.5112 4 1 15 -4 140.421 30.0612 4 1 -15 -4 63.2260 26.5104 1 1 15 -3 103.414 24.4639 4 1 -15 -3 31.1500 18.9980 1 1 15 -2 121.871 22.9712 4 1 -15 -2 92.8153 28.9848 1 1 -15 -1 38.4905 21.9234 1 1 -15 0 70.8054 23.3405 1 1 -15 1 40.2601 19.2782 1 1 -15 2 86.3282 23.7135 1 1 -15 3 15.5833 16.8078 1 1 16 -4 77.7135 26.1227 4 1 -16 -2 35.5648 19.1995 1 1 -16 -1 126.626 32.1797 1 1 -16 0-4.57625 15.8972 1 1 -16 1 38.3982 19.7533 1 1 -16 2 18.4771 13.4654 1 1 -17 -1 78.2160 28.3887 1 1 -17 0 58.5002 25.8323 1 1 -17 1 25.4453 18.5580 1 2 0 -5 2.43993 17.2649 1 2 0 -5-13.8881 14.4995 3 2 0 -4 1670.78 61.7015 3 2 0 -4 1730.96 74.9983 1 2 0 -4 1720.27 39.7137 2 2 0 -3-11.8984 10.4605 2 2 0 -3 6.90004 11.6211 1 2 0 -3 0.38477 9.24450 3 2 0 -2 3586.40 69.6416 3 2 0 -2 3452.16 84.7460 1 2 0 -2 3568.52 79.4254 2 2 0 -1-4.08599 6.20985 3 2 0 -1 5.36074 8.97430 1 2 0 0 1068.39 36.1354 1 2 0 2 8908.05 128.839 4 2 0 3-2.83552 12.0596 4 2 0 4 183.519 22.4214 4 2 0 5-25.0037 22.6732 2 2 0 6-6.71892 20.0928 2 2 0 7-26.7914 22.8927 2 2 0 8 127.644 33.1672 2 2 0 9 5.00311 22.9649 2 2 -1 -5 488.379 38.6383 3 2 1 -5 509.313 38.8393 3 2 1 -5 425.473 41.6735 1 2 1 -4 202.333 27.6510 1 2 -1 -4 170.889 22.2684 3 2 1 -4 168.585 22.1067 3 2 1 -4 169.782 14.2645 2 2 -1 -3 6573.21 110.815 3 2 1 -3 6690.70 110.371 3 2 -1 -3 6524.91 130.067 1 2 1 -3 6596.42 131.547 1 2 -1 -3 6395.33 94.6948 2 2 -1 -2 63.5288 15.0560 2 2 -1 -2 92.1895 16.3238 1 2 -1 -2 76.8679 13.1566 3 2 1 -2 87.1478 13.6911 3 2 1 -2 81.2478 16.5250 1 2 -1 -1 704.638 40.5039 2 2 1 -1 791.314 27.9235 3 2 -1 -1 747.243 34.0284 1 2 1 -1 774.033 38.0433 1 2 1 0 2146.63 33.3128 3 2 -1 0 2165.11 47.3256 1 2 1 0 2166.62 55.1297 1 2 -1 0 2155.36 73.5460 2 2 -1 2 5162.66 100.782 4 2 1 3 60.1839 17.0289 4 2 -1 3 160.137 24.5482 4 2 -1 3 107.323 29.7296 2 2 1 4 118.704 12.2483 3 2 1 4 172.797 22.3975 4 2 -1 4 178.534 23.4820 4 2 -1 4 113.129 25.7613 2 2 1 5 17.8672 8.96905 3 2 -1 5 5.15243 19.2143 2 2 -1 6 151.500 31.3045 2 2 1 6 163.342 20.4530 3 2 -1 7-2.62704 18.9489 2 2 1 7-11.6598 14.4132 3 2 1 7-0.59569 20.8664 2 2 -1 8 195.915 36.8688 2 2 1 8 112.320 31.2462 2 2 1 9 5.63027 24.3586 2 2 -1 9-0.88208 23.0865 2 2 -2 -5-8.75534 14.9170 3 2 2 -5 3.37142 9.77692 1 2 2 -5-0.28035 12.9619 3 2 -2 -4 95.4341 19.5382 3 2 2 -4 87.6874 20.6908 1 2 2 -4 78.2630 16.2443 3 2 2 -3 542.736 33.5227 3 2 2 -3 469.844 38.0377 1 2 2 -2 553.872 29.7301 3 2 2 -2 522.437 36.5868 1 2 -2 -2 512.611 33.1502 2 2 2 -1 286.061 18.2554 3 2 -2 -1 250.319 20.2965 1 2 2 -1 263.063 24.5897 1 2 -2 -1 264.282 27.3461 2 2 2 0 783.539 24.0895 3 2 -2 0 802.474 27.3930 1 2 2 0 804.469 37.2664 1 2 -2 0 748.303 44.7616 2 2 2 2 3457.92 42.0418 3 2 2 3 694.388 24.1256 3 2 -2 3 671.051 51.6103 2 2 2 3 640.889 35.1083 4 2 -2 3 769.756 41.4792 4 2 -2 4 109.397 27.0978 2 2 2 4 166.433 16.3797 3 2 2 4 228.325 23.4751 4 2 -2 5 63.5393 22.9942 2 2 2 5 89.9290 14.8441 3 2 -2 6 370.054 44.6943 2 2 2 6 404.866 30.6069 3 2 -2 7 96.3823 28.9251 2 2 2 7 99.6873 19.8983 3 2 -2 8 148.956 35.3220 2 2 2 8 135.655 33.1430 2 2 -2 9 196.348 38.1699 2 2 2 9 135.861 33.4658 2 2 3 -5 1417.70 65.1150 3 2 3 -4 20.1953 11.9743 3 2 3 -4 30.8505 16.9479 1 2 3 -3 223.873 23.0151 3 2 3 -3 177.084 26.1261 1 2 3 -2 79.8550 17.5981 1 2 3 -2 86.3193 14.2380 3 2 -3 -1 132.792 20.6134 2 2 3 -1 165.711 15.9887 3 2 3 -1 179.261 21.6609 1 2 -3 -1 167.891 22.7781 4 2 -3 0 429.527 20.0856 1 2 3 0 443.220 30.2505 1 2 -3 0 461.398 36.4205 2 2 3 1 57.6383 14.4286 4 2 3 3 301.028 18.9816 3 2 -3 3 274.872 34.5240 2 2 -3 3 387.465 31.9964 4 2 -3 4 120.409 29.9367 2 2 3 4 155.074 16.6029 3 2 3 4 191.377 21.8690 4 2 3 5 496.623 31.6421 3 2 -3 5 487.494 48.5512 2 2 -3 6 37.0449 24.8153 2 2 3 6 21.6036 12.4232 3 2 -3 7 49.0270 25.5712 2 2 3 7 23.2247 15.8880 3 2 -3 8 73.9827 27.9356 2 2 -3 9 55.5045 24.9071 2 2 3 9 33.0491 24.7414 2 2 4 -4 419.715 34.2013 3 2 4 -4 376.826 37.7388 1 2 4 -3 330.600 27.9587 3 2 4 -3 363.630 35.8492 1 2 4 -2 188.259 24.7797 1 2 4 -2 161.421 18.8762 3 2 4 -1 347.608 30.2107 1 2 -4 -1 364.648 31.0517 4 2 -4 0 1582.16 59.1876 4 2 4 0 1416.63 55.2867 1 2 -4 0 1525.41 65.3112 2 2 4 2 588.921 31.7407 4 2 -4 2 599.433 38.2335 4 2 -4 3 86.7237 20.5511 4 2 -4 3 30.3812 22.1725 2 2 4 3 11.8744 9.53958 3 2 4 4 418.387 27.6732 3 2 -4 4 486.971 47.3665 2 2 -4 5 183.971 34.7331 2 2 4 5 154.736 20.2231 3 2 -4 6 79.7866 26.1684 2 2 4 6 77.2976 17.4557 3 2 -4 7 77.9122 28.7475 2 2 4 7 70.0873 20.6725 3 2 -4 8 107.894 30.9147 2 2 5 -4 1116.02 55.9426 3 2 5 -4 1153.76 66.0991 1 2 5 -3 1256.13 53.8859 3 2 5 -3 1248.65 65.2079 1 2 5 -2 94.3301 20.1420 1 2 5 -2 125.188 17.6805 3 2 -5 -2 89.8399 19.1878 4 2 -5 -1 3146.40 84.5020 4 2 5 -1 3309.24 95.2676 1 2 -5 0 1286.49 53.5614 4 2 5 0 1234.77 55.4057 1 2 -5 1 70.2337 23.9830 2 2 -5 1 17.2061 4.23263 1 2 -5 1 5.49844 16.7610 4 2 -5 2 108.610 21.6054 4 2 -5 2 148.114 29.4378 2 2 5 2 80.7207 14.3126 4 2 5 3 335.528 24.1206 4 2 -5 3 441.953 44.3715 2 2 5 4 468.501 31.8282 3 2 -5 4 450.519 46.4965 2 2 -5 5 81.3604 28.0008 2 2 5 5 26.2974 12.8033 3 2 -5 6 32.0403 22.7164 2 2 5 6 21.4702 13.8270 3 2 5 7 52.5882 17.3971 3 2 6 -4 2494.74 84.0017 3 2 6 -3 132.231 23.5880 1 2 6 -3 96.8854 17.6969 3 2 6 -2 1587.87 72.2493 1 2 -6 -2 1662.91 62.4330 4 2 -6 -1 1246.53 53.7038 4 2 6 -1 1292.29 62.7758 1 2 -6 0 1790.46 64.2967 4 2 6 0 1845.86 70.6805 1 2 -6 1 609.169 23.3905 1 2 -6 1 653.168 40.4190 4 2 -6 2 131.839 23.4898 4 2 6 2 69.4119 13.6032 4 2 6 3 183.527 18.9991 4 2 6 4 85.9365 17.9088 3 2 6 5 69.5760 16.2988 3 2 6 6 12.7508 15.8718 3 2 6 7 115.529 23.6121 3 2 7 -3 341.758 31.7814 3 2 -7 -3 315.536 29.4891 4 2 7 -2 31.0310 14.6541 1 2 -7 -2 49.1006 14.7276 4 2 -7 -1 276.804 26.8384 4 2 7 -1 287.500 31.6342 1 2 -7 0 242.395 26.9333 4 2 7 0 237.760 28.2035 1 2 -7 1 277.060 19.2825 1 2 -7 1 323.249 31.2909 4 2 -7 2 149.985 12.1758 1 2 7 2 151.353 16.7159 4 2 7 3 184.970 16.8913 4 2 7 5 54.8709 18.0476 3 2 7 6 69.3027 19.2445 3 2 7 7 82.2005 21.5865 3 2 -8 -4 168.476 21.9579 4 2 -8 -3 260.644 26.9213 4 2 -8 -2 336.649 29.0602 4 2 -8 -1 658.415 40.6876 4 2 -8 0 229.655 26.4243 4 2 -8 0 166.517 19.1036 1 2 -8 1 110.254 22.2382 4 2 -8 1 43.6644 11.5135 1 2 -8 2 416.256 23.9920 1 2 8 2 443.104 24.9304 4 2 8 3 542.980 23.7322 4 2 8 5 79.7976 20.6013 3 2 8 6 107.277 22.5770 3 2 8 7 168.580 28.4123 3 2 -9 -5 175.697 22.4529 4 2 -9 -4 535.573 36.0660 4 2 -9 -3 68.5813 16.1462 4 2 -9 -2 157.138 23.3252 4 2 -9 -1 32.6894 16.5937 4 2 -9 0 135.666 22.9211 4 2 -9 0 108.864 17.6045 1 2 -9 1 119.738 17.5354 1 2 -9 2 667.437 34.4863 1 2 9 2 670.181 28.5048 4 2 -9 3 710.227 32.3308 1 2 9 3 705.811 22.0763 4 2 9 5-18.9375 14.9769 3 2 9 6-8.21462 13.7425 3 2 -10 -4 424.986 31.0952 4 2 -10 -3 415.191 31.5545 4 2 -10 -2 365.278 30.6449 4 2 -10 -1 281.046 29.9353 1 2 -10 -1 279.430 27.7952 4 2 -10 0 422.435 33.6261 1 2 -10 1 228.354 24.3646 1 2 -10 2 753.799 40.3240 1 2 10 2 724.065 26.6298 4 2 -10 3 572.308 33.1833 1 2 10 5 65.2669 21.7160 3 2 10 6 56.4517 21.7189 3 2 -11 -3 52.4489 15.3822 4 2 -11 -2 799.388 41.8730 4 2 -11 -1 380.070 30.9384 4 2 -11 -1 355.121 35.0619 1 2 -11 0 238.660 28.2016 1 2 -11 1 493.110 37.4449 1 2 -11 2 577.723 38.2071 1 2 11 6 23.4118 18.0106 3 2 -12 -2 208.881 30.5615 1 2 -12 -1 31.5690 16.6208 1 2 -12 0 595.266 45.8346 1 2 -12 1 545.257 41.9886 1 2 -12 2 25.0975 13.1051 1 2 12 6 13.1288 20.4376 3 2 -13 -2 51.8277 20.7442 1 2 -13 -1 68.6744 23.0597 1 2 -13 0 260.754 33.2893 1 2 -13 1 407.863 39.9272 1 2 -14 -3-12.3246 15.9506 1 2 -14 -2 109.542 25.7621 1 2 -14 -1 22.5706 18.9284 1 2 -14 0 25.3413 18.4146 1 2 -15 -4 23.6761 21.0195 1 2 -15 -3 59.4491 24.5871 1 2 -15 -2 68.7859 25.1214 1 2 -15 -1 83.4389 24.3289 1 2 -16 -3-8.83221 19.1279 1 2 -16 -2 76.9610 23.5696 1 3 0 -4-0.88768 12.6238 2 3 0 -4-1.87818 11.6763 3 3 0 -4-2.19855 15.2009 1 3 0 -3 996.501 46.3672 3 3 0 -3 1012.77 58.0179 1 3 0 -3 1001.82 53.0150 2 3 0 -2-1.70771 10.0759 3 3 0 -2 7.98592 12.7086 1 3 0 -2-7.56808 19.6319 2 3 0 -1 561.134 36.4305 1 3 0 -1 518.045 44.0019 2 3 0 0 2.30564 7.95237 1 3 0 0-10.0186 15.8596 4 3 0 0 31.0537 21.3208 2 3 0 1 182.258 33.6039 2 3 0 2-30.1723 27.3351 2 3 0 3 1035.20 74.3484 2 3 0 4-20.0270 24.0565 2 3 0 5-21.5992 25.2597 2 3 0 6 27.2998 21.4193 2 3 0 7-3.72073 21.2802 2 3 1 -5 273.501 22.9012 2 3 1 -4 73.3176 17.1330 2 3 -1 -4 94.0601 19.7602 3 3 -1 -4 128.105 21.6524 2 3 -1 -4 98.8535 21.9682 1 3 1 -4 107.543 20.5771 3 3 -1 -3 58.5674 17.9685 2 3 -1 -3 83.7275 19.2656 1 3 1 -3 73.0163 15.0545 3 3 1 -3 46.4337 17.7029 1 3 1 -3 45.3727 16.9674 2 3 1 -2 1240.87 44.5954 3 3 -1 -2 1308.70 59.4990 1 3 1 -2 1392.11 63.3187 1 3 1 -2 1222.71 63.0462 2 3 -1 -2 1342.71 65.7102 2 3 -1 -1 50.1752 22.3527 2 3 1 -1 66.4358 15.7881 1 3 1 -1 80.3074 11.4225 3 3 -1 -1 75.3417 15.3779 1 3 1 0 107.849 17.5897 1 3 -1 0 90.7479 13.4576 1 3 1 0 59.8606 17.4764 4 3 -1 0 104.103 25.2554 2 3 1 1 764.086 49.2298 4 3 -1 1 808.838 60.6866 2 3 -1 2 1313.06 78.5336 2 3 -1 3 595.638 57.4605 2 3 -1 4-27.7304 27.6296 2 3 -1 5-18.9084 22.9058 2 3 1 5 5.81748 23.8240 2 3 -1 6-19.8662 25.7145 2 3 1 6-1.97711 19.1882 2 3 -1 7 53.8924 27.6538 2 3 1 7 28.4732 21.8883 2 3 2 -5 233.059 21.8315 2 3 -2 -4 32.9368 16.7590 1 3 2 -4 71.8742 18.5042 3 3 2 -4 30.0978 15.4568 2 3 -2 -3 208.524 27.5623 2 3 -2 -3 200.485 27.5310 1 3 2 -3 165.416 21.3588 3 3 2 -3 191.342 29.0384 1 3 2 -2 123.734 22.4705 1 3 -2 -2 127.026 24.4262 2 3 -2 -2 101.842 18.6869 1 3 2 -2 103.917 15.3437 3 3 -2 -1 50.4703 20.6744 2 3 2 -1 79.9929 11.3143 3 3 2 -1 47.9190 14.7054 1 3 -2 -1 47.3593 12.8845 1 3 -2 0 25.6109 18.6875 2 3 -2 0 39.7614 9.65474 1 3 2 0 21.8280 5.41961 3 3 2 0 23.3469 12.0029 1 3 -2 1 262.299 40.8928 2 3 2 1 248.502 30.0725 4 3 2 2 1328.00 61.1904 4 3 -2 2 1187.23 75.4207 2 3 -2 3 804.595 66.1249 2 3 -2 4 95.0130 27.7133 2 3 -2 5 51.0959 31.9969 2 3 -2 6-35.3308 28.8522 2 3 2 6 5.25076 21.9542 2 3 -2 7 75.7426 31.2853 2 3 2 7 63.5171 31.2935 2 3 3 -5 824.560 40.9051 2 3 3 -4 343.363 32.6587 3 3 -3 -4 297.290 35.7884 1 3 3 -3 33.0594 17.5199 1 3 -3 -3 15.3755 12.9962 1 3 3 -3 28.6389 13.3878 3 3 3 -2 240.329 22.7120 3 3 -3 -2 199.337 24.2645 1 3 3 -2 212.539 29.6015 1 3 -3 -2 261.687 33.7310 2 3 -3 -1 28.1632 17.5630 2 3 -3 -1 21.5746 10.9841 1 3 3 -1 31.9616 9.88757 3 3 3 -1 47.0134 17.6064 1 3 3 0 259.036 16.4578 3 3 -3 0 235.081 17.5794 1 3 -3 0 344.271 40.7791 2 3 3 0 231.183 25.7507 1 3 -3 1 84.6941 27.3753 2 3 3 1 70.2507 6.20603 3 3 3 1 51.8307 18.0189 4 3 -3 2 308.066 42.7881 2 3 3 2 355.470 33.3774 4 3 -3 3 285.240 42.0029 2 3 -3 4 58.1950 28.0477 2 3 -3 5 33.0378 26.3405 2 3 -3 6 174.236 39.8264 2 3 -3 7 10.8783 24.6227 2 3 4 -4 310.733 32.1343 3 3 4 -3 231.898 25.5447 3 3 -4 -3 193.992 25.5516 1 3 -4 -2 110.693 18.3272 1 3 4 -2 146.673 26.2326 1 3 4 -2 129.977 17.8587 3 3 4 -1-2.85697 14.3221 1 3 -4 -1 34.1616 20.4100 2 3 -4 -1 10.9603 9.39587 1 3 4 -1 4.73993 8.35541 3 3 -4 0 96.4700 28.5570 2 3 4 0 127.393 14.2830 3 3 4 0 100.085 19.9236 1 3 -4 0 116.935 12.5223 1 3 4 1 362.780 18.8658 3 3 4 1 335.387 32.9687 4 3 -4 1 404.388 46.1010 2 3 -4 2-14.7521 23.9522 2 3 4 2 9.66606 5.20158 3 3 4 2 13.0196 4.48400 3 3 4 2 23.4988 14.2648 4 3 -4 3 28.3204 21.4026 2 3 4 3 19.8647 5.22360 3 3 4 3-8.52400 15.4651 4 3 -4 4 34.1714 28.4823 2 3 -4 5 117.486 34.5218 2 3 -4 6 39.2411 25.1439 2 3 -4 7 76.0235 31.1454 2 3 5 -3 695.847 43.0749 3 3 5 -2 254.384 25.0263 3 3 -5 -1 37.7322 11.4706 1 3 5 -1 37.5493 16.9947 1 3 5 -1 42.1807 11.5412 3 3 5 0 652.313 32.3084 3 3 -5 0 636.560 27.0467 1 3 -5 0 640.161 52.6668 2 3 5 0 677.707 45.8018 1 3 5 1 395.692 35.3817 4 3 -5 1 444.921 47.7577 2 3 -5 2 7.46703 24.0335 2 3 5 2 7.80985 12.3700 4 3 -5 3 33.1505 23.4335 2 3 5 3 12.2834 7.88222 3 3 5 3 22.1671 15.7286 4 3 -5 4 112.047 30.8838 2 3 -5 5 61.4466 30.3408 2 3 -5 6 37.5111 24.9316 2 3 6 -3 449.719 36.8651 3 3 6 -2 144.997 20.9798 3 3 6 -1 336.901 27.8669 3 3 -6 0 297.141 19.6886 1 3 6 0 291.774 33.7843 1 3 6 1 152.596 23.0106 4 3 -6 2 93.1209 31.8455 2 3 6 2 107.406 19.7409 4 3 6 3 26.5724 10.8312 3 3 6 3 17.6811 13.7720 4 3 -6 4 69.8018 32.6882 2 3 -6 5 13.0822 25.9589 2 3 7 -2 82.1360 18.3572 3 3 7 -1 289.912 27.7727 3 3 -7 0 137.354 13.9726 1 3 7 1-39.5848 15.7237 4 3 7 2 45.1943 15.6573 4 3 7 3 77.1958 18.2339 4 3 -8 0 85.4335 13.2021 1 3 8 1 26.4355 13.8534 4 3 8 2 47.7109 15.3525 4 3 -9 0 56.8837 12.1773 1 3 -10 -1 298.977 29.2220 1 4 0 -5 46.8631 19.5183 2 4 0 -4 97.3889 23.0258 2 4 0 -3 30.8713 19.3257 2 4 0 -2 282.072 39.4770 2 4 0 -2 376.054 37.8733 1 4 0 -1-25.1022 27.6037 2 4 0 0 50.6041 22.3759 2 4 0 1-31.5830 28.8657 2 4 0 2-10.5615 28.1852 2 4 0 3 9.05557 23.1544 2 4 0 4 370.870 54.7125 2 4 1 -5 229.857 29.3869 2 4 1 -4 25.1704 17.0712 2 4 -1 -4 59.8239 21.8855 2 4 1 -3-0.40491 16.8097 2 4 -1 -3-5.07159 17.2734 2 4 -1 -2 25.7404 14.9489 1 4 -1 -2 17.4655 20.0163 2 4 1 -2 18.1787 20.6287 2 4 -1 -1 110.339 31.4276 2 4 1 -1 144.816 23.8654 1 4 1 -1 138.865 31.4029 2 4 -1 0-0.41713 22.6894 2 4 1 0 35.6987 24.4739 2 4 -1 1-22.6813 28.7553 2 4 1 1 1.56847 24.0174 2 4 -1 2 126.553 37.3557 2 4 1 2 186.755 42.1952 2 4 -1 3 173.851 42.6419 2 4 1 3 118.001 35.4905 2 4 -1 4 72.8504 34.4960 2 4 1 4 21.0342 28.9511 2 4 2 -4 43.3444 20.8085 2 4 -2 -3 35.8542 19.9478 2 4 2 -3-1.22735 15.7452 2 4 -2 -2 57.1455 24.8973 2 4 2 -2 7.26742 21.0130 2 4 -2 -1 117.739 31.3539 2 4 2 -1 120.493 22.1394 1 4 2 -1 133.473 32.7615 2 4 -2 0-30.8745 24.5379 2 4 -2 1 21.7836 23.2068 2 4 -2 2 102.231 35.7234 2 4 -2 3 167.250 42.5052 2 4 2 3 212.103 46.6814 2 4 -2 4 105.683 39.1983 2 4 2 4 60.6627 27.3140 2 4 3 -4 99.6417 25.0015 2 4 -3 -3 152.421 29.9269 2 4 3 -3 119.685 27.9299 2 4 -3 -2 47.8154 24.8343 2 4 -3 -1 57.5838 24.9117 2 4 -3 0-25.1742 26.4160 2 4 -3 1 76.1093 31.7565 2 4 -3 2 113.548 34.5720 2 4 -3 3 205.302 45.4624 2 4 -3 4 93.1676 37.2072 2 4 -4 -2 99.9952 27.1034 2 4 -4 -1 51.1238 26.8265 2 4 -4 0 177.030 37.9813 2 4 -4 1 72.2069 32.8942 2 4 -4 2 38.1565 27.7637 2 4 -4 3 40.4902 29.0398 2 4 -5 0 36.9335 27.4486 2 4 -5 1 74.0882 29.4558 2 4 -5 2 72.7639 29.3235 2 4 -5 3 0.39774 25.1349 2 4 -6 2 32.8901 26.4684 2 5 0 -3-34.6820 25.5056 2 5 0 -2 11.2915 20.9100 2 5 0 -1 75.1353 32.8022 2 5 1 -3 4.30727 20.0845 2 5 -1 -3 37.5972 25.3169 2 5 1 -2 26.7060 25.3011 2 5 -1 -2-3.67202 21.9120 2 5 1 -1 37.7666 30.5233 2 5 -1 -1 67.3770 34.0768 2 5 2 -3 32.0605 22.5625 2 5 -2 -3-1.39401 20.4119 2 5 2 -2 38.1951 28.8861 2 5 -2 -2 12.7457 21.8614 2 5 2 -1-3.43556 25.4985 2 5 -2 -1 11.9070 24.2945 2 5 3 -3 47.9454 27.7604 2 5 -3 -2 27.5447 22.4974 2 5 3 -2 50.9857 27.4314 2 5 -3 -1 96.3987 33.8741 2 5 3 -1 14.5373 24.2495 2 5 4 -3 80.3618 32.0821 2 5 4 -2 30.5960 29.4537 2 5 4 -1 11.3279 18.9833 2 5 5 -3 4.44294 25.7694 2 5 5 -2 145.504 40.3884 2 0 0 0 0.00 0.00 0 TITL exp_276_2 in Pn REM Pn (#7 in standard setting) CELL 0.71073 3.874417 12.889756 8.116680 90.0000 98.9648 90.0000 ZERR 2.00 0.000362 0.000914 0.000552 0.0000 0.0076 0.0000 LATT -1 SYMM x+1/2,-y, z+1/2 SFAC C H N O UNIT 16.00 20.00 2.00 8.00 TREF HKLF 4 END ; _shelx_hkl_checksum 1699 loop_ _space_group_symop_operation_xyz 'x, y, z' 'x+1/2, -y, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O -0.7858(11) -0.4213(3) -0.0816(5) 0.0661(12) Uani 1 1 d . . . . . N1 N -0.6736(10) -0.0624(3) 0.0068(5) 0.0386(9) Uani 1 1 d . . . . . C1 C -0.7129(12) -0.3352(4) -0.1222(6) 0.0467(13) Uani 1 1 d . . . . . O2 O -0.3884(10) -0.2132(3) -0.4688(4) 0.0555(10) Uani 1 1 d . . . . . N2 N -0.7449(10) -0.2498(3) -0.0228(5) 0.0390(10) Uani 1 1 d . . . . . C2 C -0.4920(13) -0.2208(4) -0.3336(6) 0.0408(12) Uani 1 1 d . . . . . C3 C -0.5351(11) -0.1393(3) -0.2205(5) 0.0334(10) Uani 1 1 d . . . . . N4 N -0.5936(10) -0.3167(3) -0.2735(5) 0.0421(10) Uani 1 1 d . . . . . C4 C -0.5571(14) 0.0077(4) -0.0928(6) 0.0440(11) Uani 1 1 d . . . . . H4 H -0.537850 0.078132 -0.068042 0.053 Uiso 1 1 calc R U . . . N5 N -0.4717(9) -0.0338(3) -0.2311(4) 0.0377(9) Uani 1 1 d . . . . . H5 H -0.393278 -0.001844 -0.310622 0.045 Uiso 1 1 calc R U . . . C5 C -0.6577(10) -0.1530(3) -0.0756(5) 0.0336(10) Uani 1 1 d . . . . . C6 C -0.8532(15) -0.2641(4) 0.1408(6) 0.0561(15) Uani 1 1 d . . . . . H6A H -0.947777 -0.332563 0.147634 0.084 Uiso 1 1 calc R U . . . H6B H -1.028067 -0.213615 0.155399 0.084 Uiso 1 1 calc R U . . . H6C H -0.654836 -0.255576 0.226679 0.084 Uiso 1 1 calc R U . . . C7 C -0.5640(16) -0.4100(4) -0.3799(8) 0.0620(16) Uani 1 1 d . . . . . H7A H -0.459181 -0.390483 -0.474975 0.093 Uiso 1 1 calc R U . . . H7B H -0.792435 -0.438117 -0.416751 0.093 Uiso 1 1 calc R U . . . H7C H -0.421291 -0.461369 -0.316232 0.093 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.105(3) 0.035(2) 0.063(3) 0.0097(18) 0.026(2) -0.011(2) N1 0.052(3) 0.0372(19) 0.0284(19) -0.0029(16) 0.0120(17) 0.0010(18) C1 0.056(4) 0.040(3) 0.045(3) 0.005(2) 0.008(2) 0.000(2) O2 0.091(3) 0.0430(19) 0.041(2) -0.0052(16) 0.0357(19) -0.0037(19) N2 0.042(2) 0.042(2) 0.035(2) 0.0062(17) 0.0106(17) -0.0022(17) C2 0.049(3) 0.035(2) 0.040(3) -0.001(2) 0.009(2) 0.004(2) C3 0.037(3) 0.031(2) 0.032(2) 0.001(2) 0.0069(19) -0.0012(18) N4 0.060(3) 0.0271(19) 0.041(2) -0.0023(16) 0.0161(19) 0.0016(18) C4 0.058(3) 0.036(2) 0.040(3) -0.006(2) 0.015(2) 0.000(2) N5 0.051(2) 0.0354(19) 0.0293(18) 0.0006(17) 0.0144(17) -0.0014(18) C5 0.036(3) 0.036(2) 0.029(2) 0.003(2) 0.0055(18) -0.0023(19) C6 0.067(4) 0.065(3) 0.039(3) 0.016(3) 0.017(3) -0.006(3) C7 0.089(4) 0.035(3) 0.067(4) -0.014(3) 0.027(3) -0.004(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C4 N1 C5 103.8(4) . . ? O1 C1 N2 121.9(5) . . ? O1 C1 N4 121.4(5) . . ? N2 C1 N4 116.7(4) . . ? C5 N2 C1 119.4(4) . . ? C5 N2 C6 120.9(4) . . ? C1 N2 C6 119.6(4) . . ? O2 C2 N4 121.7(4) . . ? O2 C2 C3 127.3(5) . . ? N4 C2 C3 111.0(4) . . ? C5 C3 N5 105.8(4) . . ? C5 C3 C2 124.1(4) . . ? N5 C3 C2 130.1(4) . . ? C1 N4 C2 127.0(4) . . ? C1 N4 C7 115.9(4) . . ? C2 N4 C7 117.1(4) . . ? N5 C4 N1 112.9(4) . . ? C4 N5 C3 105.8(4) . . ? C3 C5 N1 111.7(4) . . ? C3 C5 N2 121.8(4) . . ? N1 C5 N2 126.6(4) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C1 1.204(6) . ? N1 C4 1.337(6) . ? N1 C5 1.352(5) . ? C1 N2 1.381(6) . ? C1 N4 1.398(6) . ? O2 C2 1.230(5) . ? N2 C5 1.379(5) . ? N2 C6 1.466(6) . ? C2 N4 1.408(6) . ? C2 C3 1.421(6) . ? C3 C5 1.346(6) . ? C3 N5 1.387(6) . ? N4 C7 1.495(6) . ? C4 N5 1.332(5) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C1 N2 C5 -180.0(5) . . . . ? N4 C1 N2 C5 -0.4(6) . . . . ? O1 C1 N2 C6 3.2(7) . . . . ? N4 C1 N2 C6 -177.2(4) . . . . ? O2 C2 C3 C5 178.4(5) . . . . ? N4 C2 C3 C5 -0.1(6) . . . . ? O2 C2 C3 N5 -0.6(8) . . . . ? N4 C2 C3 N5 -179.2(4) . . . . ? O1 C1 N4 C2 -178.3(5) . . . . ? N2 C1 N4 C2 2.1(6) . . . . ? O1 C1 N4 C7 0.1(7) . . . . ? N2 C1 N4 C7 -179.5(4) . . . . ? O2 C2 N4 C1 179.5(5) . . . . ? C3 C2 N4 C1 -1.8(6) . . . . ? O2 C2 N4 C7 1.1(7) . . . . ? C3 C2 N4 C7 179.8(4) . . . . ? C5 N1 C4 N5 0.2(5) . . . . ? N1 C4 N5 C3 -0.4(6) . . . . ? C5 C3 N5 C4 0.5(5) . . . . ? C2 C3 N5 C4 179.7(4) . . . . ? N5 C3 C5 N1 -0.4(5) . . . . ? C2 C3 C5 N1 -179.7(4) . . . . ? N5 C3 C5 N2 -179.1(4) . . . . ? C2 C3 C5 N2 1.6(6) . . . . ? C4 N1 C5 C3 0.2(5) . . . . ? C4 N1 C5 N2 178.8(4) . . . . ? C1 N2 C5 C3 -1.3(6) . . . . ? C6 N2 C5 C3 175.4(4) . . . . ? C1 N2 C5 N1 -179.8(4) . . . . ? C6 N2 C5 N1 -3.1(7) . . . . ?