#------------------------------------------------------------------------------ #$Date: 2024-09-24 01:32:04 +0300 (Tue, 24 Sep 2024) $ #$Revision: 294857 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/93/7249367.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7249367 loop_ _publ_author_name 'Cui, Wen-Bo' 'Huang, Li' 'Shen, Yuan' 'Yu, Xiao-Yang' 'Li, Zi-Yi' 'Zhang, Hong' _publ_section_title ; Viologen-Based Ln-MOFs Material with Photochromic and Photoluminescence for Anticounterfeiting ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D4CE00652F _journal_year 2024 _chemical_formula_moiety 'C40 H24 Cl Eu2 N4 O18, 2(H2 O), 3(O)' _chemical_formula_sum 'C40 H28 Cl Eu2 N4 O23' _chemical_formula_weight 1272.03 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens mixed _audit_creation_date 2024-06-04 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2024-06-11 deposited with the CCDC. 2024-09-19 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 101.443(3) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 36.492(3) _cell_length_b 12.6245(10) _cell_length_c 20.7562(16) _cell_measurement_reflns_used 9976 _cell_measurement_temperature 298(2) _cell_measurement_theta_max 25.041 _cell_measurement_theta_min 2.492 _cell_volume 9372.2(13) _computing_cell_refinement 'SAINT V8.38A (?, 2016)' _computing_data_reduction 'SAINT V8.38A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 298.15 _diffrn_measured_fraction_theta_full 0.995 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device_type 'CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0476 _diffrn_reflns_av_unetI/netI 0.0307 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_limit_h_max 43 _diffrn_reflns_limit_h_min -43 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_limit_l_min -24 _diffrn_reflns_number 47815 _diffrn_reflns_point_group_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_theta_full 25.064 _diffrn_reflns_theta_max 25.064 _diffrn_reflns_theta_min 2.418 _exptl_absorpt_coefficient_mu 2.798 _exptl_absorpt_correction_T_max 0.7452 _exptl_absorpt_correction_T_min 0.5328 _exptl_absorpt_correction_type none _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1042 before and 0.0561 after correction. The Ratio of minimum to maximum transmission is 0.7150. The \l/2 correction factor is Not present.' _exptl_crystal_colour 'clear yellowish yellow' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier yellowish _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.803 _exptl_crystal_description block _exptl_crystal_F_000 4984 _exptl_crystal_size_max 0.11 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.09 _refine_diff_density_max 2.403 _refine_diff_density_min -1.422 _refine_diff_density_rms 0.185 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.073 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 632 _refine_ls_number_reflns 8256 _refine_ls_number_restraints 240 _refine_ls_restrained_S_all 1.086 _refine_ls_R_factor_all 0.0529 _refine_ls_R_factor_gt 0.0449 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0715P)^2^+145.5766P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1295 _refine_ls_wR_factor_ref 0.1353 _reflns_Friedel_coverage 0.000 _reflns_number_gt 7172 _reflns_number_total 8256 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4ce00652f2.cif _cod_data_source_block eu-2_sx_sx_sx _cod_original_cell_volume 9372.2(12) _cod_database_code 7249367 _shelx_shelxl_version_number 2016/4 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.787 _shelx_estimated_absorpt_t_min 0.748 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All O(H,H) groups 2. Uiso/Uaniso restraints and constraints Cl1 \\sim O1 \\sim O2 \\sim O3 \\sim O4 \\sim O5 \\sim O6 \\sim O7 \\sim O8 \\sim O9 \\sim O10 \\sim O11 \\sim O12: within 7.3A with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(Eu1) \\sim Ueq, Uanis(O14) \\sim Ueq, Uanis(O15) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(O14) \\sim Ueq, Uanis(O15) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 3.a Free rotating group: O20(H20A,H20B), O22(H22A,H22B) 3.b Aromatic/amide H refined with riding coordinates: C3(H3), C4(H4), C5(H5), C7(H7), C8(H8), C9(H9), C10(H10), C11(H11), C14(H14), C15(H15), C16(H16), C17(H17), C19(H19), C20(H20), C21(H21), C22(H22), C25(H25), C28(H28), C29(H29), C30(H30), C35(H35), C38(H38), C39(H39), C40(H40) ; _shelx_res_file ; TITL eu-2_a.res in C2/c eu-2_sx_sx_sx.res created by SHELXL-2016/4 at 20:33:40 on 04-Jun-2024 REM Old TITL Eu-2 in C2/c REM SHELXT solution in C2/c REM R1 0.097, Rweak 0.004, Alpha 0.060, Orientation as input REM Formula found by SHELXT: C41 N10 O16 Eu2 CELL 0.71073 36.4922 12.6245 20.7562 90 101.443 90 ZERR 8 0.0026 0.001 0.0016 0 0.003 0 LATT 7 SYMM -X,+Y,0.5-Z SFAC C H Cl Eu N O UNIT 320 224 8 16 32 184 SIMU 0.01 0.02 7.3 Cl1 O1 > O12 ISOR 0.01 0.02 Eu1 O14 O15 ISOR 0.01 0.02 O14 O15 L.S. 10 0 0 PLAN 20 SIZE 0.1 0.09 0.11 TEMP 25 BOND $H list 4 fmap 2 53 acta OMIT -9 1 1 OMIT 2 2 4 OMIT -4 4 1 OMIT 4 2 3 OMIT -4 2 4 OMIT 4 0 0 OMIT 0 2 0 OMIT 3 3 5 OMIT 2 4 1 OMIT -1 1 7 OMIT -6 2 1 REM REM REM WGHT 0.071500 145.576614 FVAR 0.10886 C1 1 0.436045 0.175664 0.431599 11.00000 0.02011 0.03412 = 0.02446 -0.00009 -0.00429 0.00268 C2 1 0.476669 0.164025 0.429414 11.00000 0.01964 0.03928 = 0.02645 -0.00317 -0.00311 0.00577 C3 1 0.487532 0.144844 0.370069 11.00000 0.02628 0.05867 = 0.02761 -0.01080 -0.00365 0.00418 AFIX 43 H3 2 0.469487 0.133615 0.332247 11.00000 -1.20000 AFIX 0 C4 1 0.524872 0.142327 0.366818 11.00000 0.03221 0.08869 = 0.02898 -0.01387 0.00243 0.01170 AFIX 43 H4 2 0.531773 0.129878 0.326696 11.00000 -1.20000 AFIX 0 C5 1 0.503698 0.177944 0.485973 11.00000 0.02199 0.04040 = 0.02771 -0.00477 -0.00221 0.00230 AFIX 43 H5 2 0.496796 0.189812 0.526157 11.00000 -1.20000 AFIX 0 C6 1 0.540796 0.173991 0.481935 11.00000 0.02330 0.05371 = 0.02798 -0.00516 -0.00562 0.00624 C7 1 0.552178 0.158067 0.422421 11.00000 0.02326 0.08712 = 0.04212 -0.00553 0.00529 0.01189 AFIX 43 H7 2 0.577384 0.158040 0.420211 11.00000 -1.20000 AFIX 0 C8 1 0.595800 0.262084 0.540618 11.00000 0.02966 0.07768 = 0.03420 0.01018 -0.00073 -0.00980 AFIX 43 H8 2 0.596000 0.302085 0.503065 11.00000 -1.20000 AFIX 0 C9 1 0.568406 0.131973 0.594822 11.00000 0.03569 0.04140 = 0.04503 0.00698 -0.01378 -0.00823 AFIX 43 H9 2 0.549748 0.081465 0.593801 11.00000 -1.20000 AFIX 0 C10 1 0.594514 0.146789 0.652034 11.00000 0.03691 0.04056 = 0.03670 0.01195 -0.01030 -0.00705 AFIX 43 H10 2 0.593364 0.106911 0.689253 11.00000 -1.20000 AFIX 0 C11 1 0.622861 0.278329 0.596483 11.00000 0.03257 0.06073 = 0.02981 0.00677 -0.00462 -0.01488 AFIX 43 H11 2 0.641587 0.328014 0.595731 11.00000 -1.20000 AFIX 0 C12 1 0.622588 0.221938 0.653564 11.00000 0.02001 0.03583 = 0.02888 0.00051 -0.00287 0.00272 C13 1 0.651267 0.242335 0.713775 11.00000 0.02191 0.02858 = 0.02477 0.00102 -0.00428 0.00023 C14 1 0.644948 0.217100 0.775478 11.00000 0.01725 0.04365 = 0.03106 0.00264 0.00116 -0.00379 AFIX 43 H14 2 0.623211 0.181412 0.779445 11.00000 -1.20000 AFIX 0 C15 1 0.685056 0.290982 0.710572 11.00000 0.02712 0.04774 = 0.02048 0.00010 0.00288 -0.00489 AFIX 43 H15 2 0.690560 0.307409 0.669856 11.00000 -1.20000 AFIX 0 C16 1 0.710099 0.314731 0.766356 11.00000 0.02191 0.04290 = 0.02276 0.00034 0.00266 -0.00993 AFIX 43 H16 2 0.732696 0.346627 0.763519 11.00000 -1.20000 AFIX 0 C17 1 0.670617 0.244405 0.831247 11.00000 0.02211 0.03958 = 0.02602 -0.00112 0.00537 -0.00243 AFIX 43 H17 2 0.665779 0.229409 0.872628 11.00000 -1.20000 AFIX 0 C18 1 0.729356 0.323684 0.884611 11.00000 0.01852 0.03658 = 0.01525 0.00016 -0.00206 -0.00125 C19 1 0.764884 0.280898 0.894336 11.00000 0.01891 0.03297 = 0.01704 -0.00138 0.00207 0.00001 AFIX 43 H19 2 0.771594 0.234148 0.864037 11.00000 -1.20000 AFIX 0 C20 1 0.717804 0.392679 0.928300 11.00000 0.02010 0.03671 = 0.02841 -0.00106 0.00667 0.00190 AFIX 43 H20 2 0.693591 0.419497 0.920693 11.00000 -1.20000 AFIX 0 C21 1 0.743799 0.420164 0.983849 11.00000 0.03095 0.03683 = 0.02709 -0.00904 0.00828 0.00182 AFIX 43 H21 2 0.737060 0.467369 1.013877 11.00000 -1.20000 AFIX 0 C22 1 0.778993 0.379502 0.995372 11.00000 0.02550 0.04178 = 0.01676 -0.00545 0.00337 -0.00175 AFIX 43 H22 2 0.795749 0.398384 1.033496 11.00000 -1.20000 AFIX 0 C23 1 0.790398 0.309879 0.950936 11.00000 0.01909 0.03269 = 0.01401 -0.00027 0.00329 -0.00233 C24 1 0.828883 0.264027 0.964001 11.00000 0.01841 0.02629 = 0.01618 0.00131 0.00050 -0.00128 C25 1 0.256548 0.268936 0.108201 11.00000 0.04172 0.05476 = 0.02809 -0.00803 0.00506 0.02157 AFIX 43 H25 2 0.271246 0.213795 0.097793 11.00000 -1.20000 AFIX 0 C26 1 0.266876 0.322121 0.167193 11.00000 0.02570 0.03883 = 0.02233 0.00765 0.00299 0.00778 C27 1 0.300566 0.287991 0.217021 11.00000 0.02994 0.03470 = 0.02458 0.00748 0.00652 0.01009 C28 1 0.244954 0.405557 0.182700 11.00000 0.02407 0.03140 = 0.02288 0.00179 0.00105 0.00307 AFIX 43 H28 2 0.251942 0.441517 0.222343 11.00000 -1.20000 AFIX 0 C29 1 0.224231 0.297946 0.064563 11.00000 0.04239 0.06221 = 0.02499 -0.00787 -0.00239 0.01905 AFIX 43 H29 2 0.217222 0.261923 0.024948 11.00000 -1.20000 AFIX 0 C30 1 0.202425 0.379963 0.079611 11.00000 0.02903 0.05245 = 0.02155 0.00579 -0.00098 0.01397 AFIX 43 H30 2 0.180741 0.398990 0.050196 11.00000 -1.20000 AFIX 0 C31 1 0.212831 0.434348 0.138803 11.00000 0.02189 0.03283 = 0.02692 0.00496 0.00524 0.00544 C32 1 0.189550 0.523259 0.155626 11.00000 0.02032 0.02970 = 0.02326 0.00566 0.00314 0.00102 C33 1 0.404243 0.423979 0.347280 11.00000 0.02961 0.04124 = 0.02202 0.00281 0.00038 -0.00032 C34 1 0.420213 0.512782 0.314888 11.00000 0.02609 0.03246 = 0.01972 0.00095 0.00402 0.00016 C35 1 0.407722 0.532109 0.247722 11.00000 0.02672 0.03624 = 0.02421 -0.00078 0.00368 -0.00488 AFIX 43 H35 2 0.389037 0.489730 0.223696 11.00000 -1.20000 AFIX 0 C36 1 0.409562 0.630186 0.145133 11.00000 0.03302 0.03781 = 0.01897 0.00471 0.00217 -0.00305 C37 1 0.422768 0.613295 0.216608 11.00000 0.03103 0.03065 = 0.01972 0.00188 0.00510 0.00213 C38 1 0.451387 0.674770 0.252370 11.00000 0.03592 0.03903 = 0.02864 0.00563 0.00374 -0.00984 AFIX 43 H38 2 0.461899 0.729069 0.231773 11.00000 -1.20000 AFIX 0 C39 1 0.464253 0.654983 0.318887 11.00000 0.03875 0.04888 = 0.02759 -0.00164 -0.00139 -0.01582 AFIX 43 H39 2 0.483738 0.695201 0.342473 11.00000 -1.20000 AFIX 0 C40 1 0.448350 0.576338 0.350003 11.00000 0.03926 0.03865 = 0.01659 0.00523 0.00297 -0.00587 AFIX 43 H40 2 0.456473 0.565553 0.394892 11.00000 -1.20000 AFIX 0 CL1 3 0.343117 0.509678 0.479023 11.00000 0.09005 0.14178 = 0.08874 0.01600 0.01211 -0.01603 EU1 4 0.396120 0.362355 0.506230 11.00000 0.02441 0.03372 = 0.01680 -0.00151 0.00371 -0.00419 EU2 4 0.355799 0.193745 0.313675 11.00000 0.01726 0.02783 = 0.01552 0.00132 -0.00066 -0.00011 N1 5 0.702451 0.292479 0.825534 11.00000 0.01890 0.03250 = 0.02026 -0.00372 -0.00170 -0.00141 N2 5 0.569398 0.189095 0.540510 11.00000 0.02205 0.04434 = 0.02829 -0.00281 -0.00670 0.00264 N3 5 0.395993 0.068733 0.228833 11.00000 0.04815 0.04856 = 0.04933 -0.00107 0.02290 0.00833 N4 5 0.458591 0.493780 0.533635 11.00000 0.10619 0.07423 = 0.07857 0.00633 0.00832 0.03670 O1 6 0.427622 0.211535 0.482929 11.00000 0.02952 0.06021 = 0.02743 -0.00710 0.00516 0.00904 O2 6 0.412957 0.149880 0.381314 11.00000 0.02153 0.05956 = 0.03325 -0.00289 -0.00127 0.00151 O3 6 0.843217 0.229985 0.917119 11.00000 0.02107 0.03482 = 0.01755 -0.00259 0.00402 0.00396 O4 6 0.846428 0.256535 1.022298 11.00000 0.02244 0.04594 = 0.01891 0.00202 0.00171 0.00509 O5 6 0.324392 0.228033 0.199721 11.00000 0.03294 0.05747 = 0.02541 0.00340 0.00092 0.01436 O6 6 0.303400 0.317230 0.276351 11.00000 0.03305 0.04593 = 0.02193 0.00109 0.00060 0.01015 O7 6 0.201443 0.579980 0.205087 11.00000 0.02737 0.04144 = 0.02572 -0.00218 -0.00084 0.00319 O8 6 0.157933 0.542020 0.119922 11.00000 0.02335 0.03929 = 0.02866 -0.00403 -0.00061 0.00829 O9 6 0.411118 0.421585 0.409031 11.00000 0.05007 0.06623 = 0.02842 0.00756 0.00654 -0.01597 O10 6 0.384621 0.356770 0.312026 11.00000 0.05161 0.05021 = 0.03288 0.00458 0.00533 -0.01240 O11 6 0.384105 0.572865 0.113277 11.00000 0.04665 0.05626 = 0.02542 0.00999 0.00077 -0.01397 O12 6 0.424514 0.701861 0.115844 11.00000 0.05437 0.05151 = 0.02413 0.01087 0.00027 -0.01779 O13 6 0.489805 0.566980 0.534760 11.00000 0.19789 O14 6 0.467911 0.406493 0.529091 11.00000 0.11337 0.12043 = 0.13448 -0.00180 -0.00115 -0.00886 O15 6 0.433185 0.526956 0.536871 11.00000 0.10898 0.10357 = 0.11913 0.00770 0.02065 -0.01460 O16 6 0.404205 0.163655 0.237043 11.00000 0.04701 0.05153 = 0.04488 0.00356 0.01694 -0.00469 O17 6 0.369468 0.033263 0.253942 11.00000 0.03865 0.03921 = 0.03877 -0.00160 0.01513 0.00352 O18 6 0.413577 0.007954 0.200822 11.00000 0.14416 0.07976 = 0.18706 -0.02331 0.13791 0.00548 AFIX 6 O20 6 0.382264 0.003123 0.508528 11.00000 0.07777 0.05995 = 0.05624 0.01208 -0.00777 0.00188 H20A 2 0.371818 0.034543 0.472875 11.00000 -1.50000 H20B 2 0.394814 0.052140 0.531889 11.00000 -1.50000 AFIX 0 O21 6 0.285808 -0.016139 0.158011 11.00000 0.10152 0.10210 = 0.05617 -0.01504 -0.01893 -0.01618 AFIX 6 O22 6 0.292459 0.492632 0.356670 11.00000 0.09734 0.04645 = 0.09399 0.00267 0.03527 0.01061 H22A 2 0.294614 0.440463 0.330984 11.00000 -1.50000 H22B 2 0.268720 0.500381 0.353211 11.00000 -1.50000 AFIX 0 O19 6 0.473133 0.121431 0.631252 11.00000 0.19500 0.09254 = 0.14942 0.02711 0.07506 0.04971 O23 6 0.338318 -0.105419 0.583597 11.00000 0.14012 0.37769 = 0.06867 0.07530 -0.01522 -0.11863 HKLF 4 REM eu-2_a.res in C2/c REM R1 = 0.0449 for 7172 Fo > 4sig(Fo) and 0.0529 for all 8256 data REM 632 parameters refined using 240 restraints END WGHT 0.0715 145.5189 REM Highest difference peak 2.403, deepest hole -1.422, 1-sigma level 0.185 Q1 1 0.3474 0.6358 0.5636 11.00000 0.05 2.40 Q2 1 0.6425 0.3462 0.4238 11.00000 0.05 2.39 Q3 1 0.5070 0.3971 0.2780 11.00000 0.05 1.89 Q4 1 0.4780 0.5792 0.6568 11.00000 0.05 1.69 Q5 1 0.3205 0.1965 0.2984 11.00000 0.05 1.40 Q6 1 0.3546 0.3654 0.4883 11.00000 0.05 1.15 Q7 1 0.3812 0.1946 0.3257 11.00000 0.05 1.14 Q8 1 0.4253 0.3622 0.5202 11.00000 0.05 1.07 Q9 1 0.3188 -0.0851 0.5830 11.00000 0.05 0.77 Q10 1 0.5197 0.0681 0.7295 11.00000 0.05 0.63 Q11 1 0.3810 0.5475 0.5104 11.00000 0.05 0.59 Q12 1 0.3963 0.4699 0.4095 11.00000 0.05 0.53 Q13 1 0.3374 -0.0519 0.6010 11.00000 0.05 0.53 Q14 1 0.1579 0.5386 0.1013 11.00000 0.05 0.48 Q15 1 0.4388 0.0864 0.6049 11.00000 0.05 0.48 Q16 1 0.3395 0.3650 0.1654 11.00000 0.05 0.46 Q17 1 0.3600 0.5281 0.3191 11.00000 0.05 0.45 Q18 1 0.3229 0.6146 0.4685 11.00000 0.05 0.45 Q19 1 0.4005 0.5440 0.1070 11.00000 0.05 0.44 Q20 1 0.4765 0.5784 0.5849 11.00000 0.05 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37.67 7 -7 0 418.73 20.78 -7 -7 0 469.18 21.58 7 -7 0 434.55 19.98 -7 -7 0 462.82 21.43 -7 7 0 432.41 20.54 -7 7 0 449.99 21.00 7 7 0 417.09 21.09 -9 -7 0 160.36 14.49 -9 -7 0 157.89 11.61 -9 -7 0 143.98 11.66 9 -7 0 137.43 10.89 9 -7 0 155.24 9.84 -9 7 0 148.26 11.21 9 7 0 134.12 11.27 -11 -7 0 66.29 10.63 11 -7 0 74.90 7.80 -11 -7 0 78.55 9.97 -11 -7 0 81.63 8.95 11 -7 0 83.00 7.82 11 7 0 75.43 8.32 -11 7 0 85.49 9.52 13 -7 0 11.71 5.02 -13 -7 0 17.17 7.87 -13 -7 0 7.79 5.32 13 -7 0 10.21 3.81 -13 -7 0 10.39 5.31 13 7 0 8.74 5.38 -13 7 0 10.50 5.07 15 -7 0 262.64 14.88 -15 -7 0 276.25 16.40 -15 -7 0 257.20 16.00 15 -7 0 259.81 13.30 -15 -7 0 245.42 21.29 15 7 0 254.62 15.54 -15 7 0 261.01 15.86 17 -7 0 106.64 8.31 17 -7 0 94.98 12.90 -17 -7 0 73.68 9.25 17 -7 0 89.04 9.82 -17 -7 0 80.54 9.57 -17 -7 0 117.12 16.26 -17 7 0 98.94 9.99 17 7 0 76.25 9.08 19 -7 0 752.04 30.22 19 -7 0 742.55 29.00 -19 -7 0 681.94 39.06 19 -7 0 685.73 36.41 -19 -7 0 661.28 32.10 -19 -7 0 721.59 40.29 19 7 0 709.82 31.10 -19 7 0 720.76 31.86 -21 -7 0 361.53 21.79 21 -7 0 377.09 18.39 21 -7 0 371.81 27.17 21 -7 0 396.04 17.53 -21 -7 0 404.53 32.62 -21 -7 0 401.78 21.80 -21 7 0 402.49 21.41 21 7 0 344.64 19.64 -23 -7 0 463.50 37.19 23 -7 0 416.92 31.04 23 -7 0 464.83 20.54 -23 -7 0 494.18 25.02 23 -7 0 465.36 19.91 -23 7 0 368.09 32.90 23 7 0 462.15 22.15 -25 -7 0 787.41 50.38 25 -7 0 791.07 31.48 -25 -7 0 787.54 36.33 25 -7 0 793.70 31.22 25 -7 0 790.16 45.00 25 7 0 750.97 33.15 -25 7 0 805.92 36.00 27 -7 0 566.38 40.89 -27 -7 0 601.05 30.86 -27 -7 0 582.21 46.47 27 7 0 635.92 26.84 -27 7 0 621.60 30.65 -29 -7 0 942.14 60.37 29 -7 0 921.37 53.15 -29 -7 0 905.17 41.59 -29 7 0 863.16 41.66 31 -7 0 121.74 22.83 -31 -7 0 129.46 15.71 -31 7 0 131.66 14.86 -33 -7 0 234.06 23.14 -33 -7 0 263.93 38.38 33 -7 0 264.59 33.06 -33 7 0 208.28 22.64 -35 -7 0 0.07 29.10 -35 -7 0 11.03 12.77 35 -7 0 5.09 19.50 -35 7 0 5.56 12.77 -37 -7 0 37.06 35.23 -37 -7 0 14.51 13.98 37 -7 0 -8.18 21.59 -37 7 0 29.22 14.54 0 -8 0 45.95 6.97 0 -8 0 25.72 6.09 0 8 0 53.41 7.36 0 8 0 38.67 6.10 2 -8 0 135.31 11.46 -2 -8 0 114.46 11.48 2 -8 0 159.74 12.53 -2 -8 0 133.79 12.25 2 8 0 142.70 11.55 2 8 0 124.00 12.45 -2 8 0 159.07 11.67 -2 8 0 147.04 12.37 -4 -8 0 57.19 8.10 -4 -8 0 53.90 7.85 4 -8 0 52.72 7.64 4 8 0 75.31 9.47 4 8 0 64.77 8.37 6 -8 0 691.96 30.78 -6 -8 0 649.44 30.71 6 -8 0 717.60 29.94 -6 -8 0 698.05 31.14 -6 8 0 722.38 30.60 6 8 0 707.58 31.10 -6 8 0 684.90 30.71 -8 -8 0 8.08 5.67 8 -8 0 8.62 4.60 8 -8 0 14.78 5.57 -8 8 0 8.82 5.59 8 8 0 17.89 5.31 -10 -8 0 1480.80 61.82 -10 -8 0 1571.86 64.89 10 -8 0 1572.94 60.35 -10 -8 0 1594.71 62.43 10 -8 0 1541.16 61.51 -10 8 0 1626.00 61.89 10 8 0 1604.23 62.17 -12 -8 0 154.52 13.93 -12 -8 0 149.78 13.55 12 -8 0 137.63 10.70 12 -8 0 149.57 12.78 -12 -8 0 139.73 17.07 -12 8 0 159.45 13.28 12 8 0 160.18 13.31 -14 -8 0 1960.03 84.64 -14 -8 0 2067.67 86.61 14 -8 0 2141.76 79.62 -14 -8 0 2087.11 81.94 14 -8 0 2173.19 81.14 -14 8 0 2170.02 81.74 14 8 0 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12.69 7.66 -4 10 0 25.86 7.98 -6 -10 0 337.21 22.35 6 -10 0 360.11 20.00 6 -10 0 342.92 21.63 -6 -10 0 327.96 21.33 -6 10 0 382.77 22.80 6 10 0 364.22 21.68 -8 -10 0 -5.19 7.03 8 -10 0 -1.90 6.07 8 -10 0 1.69 7.49 -8 -10 0 23.08 9.84 8 10 0 6.39 7.07 -8 10 0 -8.14 7.23 10 -10 0 899.86 37.48 -10 -10 0 857.88 40.19 -10 -10 0 897.50 39.86 -10 -10 0 855.19 43.26 10 10 0 880.67 39.80 -10 10 0 885.13 40.32 12 -10 0 130.03 12.35 -12 -10 0 109.71 12.94 -12 -10 0 109.20 13.14 -12 -10 0 108.94 15.85 12 -10 0 108.92 14.63 12 10 0 115.52 15.01 -12 10 0 125.57 15.72 -14 -10 0 1777.89 71.08 14 -10 0 1756.51 67.45 -14 -10 0 1734.11 75.63 -14 -10 0 1712.06 70.49 14 -10 0 1712.71 69.39 -14 10 0 1713.38 70.22 14 10 0 1789.06 70.32 16 -10 0 76.60 10.46 16 -10 0 73.08 8.22 -16 -10 0 62.20 11.01 -16 -10 0 56.77 10.63 -16 -10 0 50.86 15.97 -16 10 0 82.14 12.05 16 10 0 61.53 10.81 18 -10 0 831.59 37.17 18 -10 0 842.51 43.89 -18 -10 0 793.52 39.25 -18 -10 0 813.99 39.59 18 -10 0 817.77 34.68 -18 -10 0 827.16 48.16 -18 10 0 824.91 39.12 18 10 0 842.40 38.01 -20 -10 0 -17.02 9.06 -20 -10 0 8.90 17.47 20 -10 0 -8.97 11.13 -20 -10 0 -5.99 9.01 20 -10 0 5.24 7.37 20 -10 0 -5.40 5.70 20 10 0 -1.69 8.35 -20 10 0 -2.15 9.41 -22 -10 0 57.69 11.80 22 -10 0 65.74 16.82 -22 -10 0 53.03 12.53 -22 -10 0 26.94 20.72 22 -10 0 40.55 9.27 22 -10 0 60.90 8.21 22 10 0 51.48 10.04 -22 10 0 78.86 12.85 -24 -10 0 -7.60 10.54 24 -10 0 6.82 6.30 24 -10 0 9.46 7.20 -24 -10 0 7.07 10.64 24 -10 0 -1.76 14.84 -24 -10 0 20.52 20.89 -24 10 0 15.23 11.40 26 -10 0 68.81 8.17 -26 -10 0 47.47 14.17 -26 -10 0 48.93 17.85 26 -10 0 33.38 16.76 26 -10 0 66.77 8.62 -26 10 0 64.85 14.72 28 -10 0 94.74 12.29 -28 -10 0 124.50 18.47 28 -10 0 85.16 8.92 -28 -10 0 71.74 29.20 -28 -10 0 89.36 15.65 28 -10 0 114.49 23.56 -28 10 0 90.89 17.01 -30 -10 0 258.50 40.55 30 -10 0 179.37 29.45 -30 -10 0 243.02 28.45 -30 -10 0 176.37 20.80 -30 10 0 182.88 21.99 -1 -11 0 460.32 25.87 1 -11 0 494.06 27.37 -1 -11 0 485.02 27.17 1 -11 0 453.39 25.68 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21.63 7.52 -32 6 -4 9.92 10.81 32 6 4 21.96 22.98 -34 -6 -4 358.88 46.72 34 -6 4 204.90 32.08 -34 -6 -4 289.11 27.08 -34 6 -4 255.31 26.07 34 6 4 296.38 18.05 34 6 4 328.38 43.33 -36 -6 -4 63.38 33.22 36 -6 4 38.17 24.83 -36 -6 -4 27.05 15.25 -36 6 -4 43.45 15.10 36 6 4 49.05 8.29 -37 -7 4 4.91 12.45 37 -7 -4 12.22 24.13 -37 -7 4 22.94 33.45 -37 -7 4 -1.08 14.35 -37 7 4 -2.54 12.59 -35 -7 4 205.52 38.96 -35 -7 4 195.84 23.79 -35 -7 4 152.37 16.90 35 -7 -4 156.10 27.20 -35 7 4 181.36 18.80 -33 -7 4 32.24 10.48 33 -7 -4 35.56 17.60 -33 -7 4 37.23 26.83 -33 7 4 11.05 10.42 -31 -7 4 -6.87 8.07 -31 -7 4 -8.58 22.36 -31 -7 4 0.60 9.36 31 -7 -4 -20.33 14.75 -31 7 4 -4.34 9.07 -29 -7 4 53.02 10.18 29 -7 -4 47.57 17.14 -29 -7 4 21.52 9.63 27 -7 -4 289.49 28.45 -27 -7 4 264.75 18.50 -27 -7 4 262.11 34.73 -27 -7 4 224.62 18.71 -27 7 4 269.97 18.57 -25 -7 4 51.23 8.86 25 -7 -4 43.54 14.25 -25 -7 4 48.40 18.27 -25 -7 4 41.79 9.11 -25 7 4 57.58 9.35 -23 -7 4 732.48 32.64 -23 -7 4 701.21 43.34 23 -7 -4 748.75 40.88 23 7 -4 664.14 30.10 -23 7 4 724.17 32.05 -21 -7 4 -6.15 5.60 -21 -7 4 -6.70 5.88 -21 -7 4 0.56 11.01 21 -7 -4 8.93 10.03 21 7 -4 -4.96 5.89 -21 7 4 5.86 4.76 -21 7 4 7.65 5.93 -19 -7 4 2100.06 88.92 19 -7 -4 2158.64 87.31 19 -7 -4 2263.89 77.84 19 -7 -4 2194.09 78.31 -19 -7 4 1985.86 81.30 -19 -7 4 2125.88 81.35 -19 7 4 2164.48 80.96 19 7 -4 1968.68 80.42 -19 7 4 2147.27 80.56 -17 -7 4 15.62 11.23 17 -7 -4 25.76 4.86 17 -7 -4 21.19 3.94 -17 -7 4 22.89 6.53 -17 -7 4 25.64 6.15 17 -7 -4 23.89 9.87 17 7 -4 27.19 6.62 -17 7 4 27.48 6.34 -17 7 4 24.66 5.48 15 -7 -4 2049.57 74.21 -15 -7 4 1916.69 76.76 15 -7 -4 2042.50 80.23 -15 -7 4 2003.50 76.68 15 -7 -4 2045.08 75.14 -15 7 4 2013.00 76.35 15 7 -4 1924.28 76.83 -15 7 4 2042.22 76.18 -13 -7 4 15.34 5.46 13 -7 -4 14.54 6.62 13 -7 -4 14.17 4.47 13 -7 -4 12.27 3.89 -13 -7 4 4.13 5.02 -13 7 4 5.45 4.68 -13 7 4 15.21 5.35 -11 -7 4 419.69 20.47 11 -7 -4 401.07 19.50 11 -7 -4 410.72 18.57 -11 -7 4 428.45 20.67 11 -7 -4 438.71 21.71 -11 7 4 419.52 19.86 -11 7 4 421.98 20.46 -9 -7 4 24.10 5.93 9 -7 -4 15.14 4.38 9 -7 -4 21.83 4.95 9 -7 -4 7.89 4.91 -9 -7 4 14.96 5.55 9 7 -4 12.23 5.07 -9 7 4 8.52 3.97 -9 7 4 23.10 5.46 -7 -7 4 7.09 4.62 7 -7 -4 -1.66 3.98 7 -7 -4 2.52 4.22 -7 7 4 -4.94 4.39 -7 7 4 -8.81 3.63 5 -7 -4 422.85 21.50 5 -7 -4 421.38 20.77 -5 -7 4 494.78 22.14 -5 -7 4 538.73 22.42 -5 7 4 432.27 21.64 -5 7 4 404.71 21.04 5 7 -4 513.43 22.06 3 -7 -4 626.67 27.74 -3 -7 4 688.67 28.49 -3 -7 4 644.17 28.48 3 -7 -4 611.71 28.25 3 7 -4 637.76 28.16 -3 7 4 645.48 28.06 -3 7 4 668.95 28.46 1 -7 -4 401.22 20.07 1 -7 -4 436.02 21.06 -1 7 4 418.66 20.68 -1 7 4 408.45 20.23 -1 -7 -4 4262.94 156.79 1 -7 4 4387.67 156.52 1 -7 4 4213.23 157.00 -1 -7 -4 4199.84 155.37 -1 -7 -4 4226.43 157.31 1 7 4 4167.03 156.95 -1 7 -4 4317.83 156.79 -3 -7 -4 247.59 14.58 5 -7 4 3253.06 118.14 -5 -7 -4 3186.45 118.98 -5 -7 -4 3272.49 119.68 5 -7 4 3065.27 118.91 -5 -7 -4 3172.83 119.59 -5 7 -4 3204.74 118.78 5 7 4 3143.38 119.19 -7 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17.71 21 -7 4 322.34 18.90 21 -7 4 345.29 29.65 -21 -7 -4 326.18 32.40 21 7 4 356.41 20.26 -21 7 -4 316.44 20.99 23 -7 4 197.92 24.44 23 -7 4 194.20 13.54 -23 -7 -4 198.88 27.04 -23 -7 -4 207.15 18.33 23 -7 4 197.27 14.89 23 7 4 224.51 16.11 -23 7 -4 188.65 18.67 25 -7 4 627.74 42.00 -25 -7 -4 650.09 33.98 25 -7 4 686.01 29.59 -25 -7 -4 697.14 48.68 25 -7 4 660.21 30.19 25 7 4 698.14 31.29 -25 7 -4 647.69 33.44 27 -7 4 8.83 15.86 -27 -7 -4 55.10 20.22 27 -7 4 4.45 5.97 -27 -7 -4 4.96 8.88 27 -7 4 7.14 6.51 -27 7 -4 24.75 10.66 27 7 4 20.86 7.56 29 -7 4 521.32 42.54 29 -7 4 478.77 24.07 -29 -7 -4 483.18 30.61 29 -7 4 534.89 24.22 -29 7 -4 500.68 31.32 29 7 4 507.33 25.76 31 -7 4 44.79 7.76 31 -7 4 59.40 22.19 -31 -7 -4 52.29 24.62 31 -7 4 31.11 7.21 -31 -7 -4 56.40 13.07 31 7 4 46.20 8.79 -31 7 -4 46.40 14.06 -33 -7 -4 678.30 56.62 33 -7 4 578.62 25.56 33 -7 4 610.10 51.12 -33 -7 -4 515.19 36.33 33 7 4 587.86 28.45 -33 7 -4 575.96 36.03 -35 -7 -4 48.91 16.50 35 -7 4 27.80 23.85 -35 -7 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8.53 -20 8 4 58.28 9.19 20 8 -4 47.90 8.69 -20 8 4 55.22 7.93 18 -8 -4 65.59 7.43 18 -8 -4 77.85 8.70 -18 -8 4 88.54 10.31 18 -8 -4 74.13 12.90 -18 -8 4 82.19 9.86 18 8 -4 77.82 9.80 -18 8 4 87.00 9.83 -18 8 4 61.93 8.18 16 -8 -4 83.47 12.40 -16 -8 4 61.59 9.31 16 -8 -4 56.75 7.32 -16 -8 4 73.50 14.69 16 -8 -4 73.82 9.26 16 8 -4 78.87 9.85 -16 8 4 78.82 9.13 -16 8 4 79.74 9.72 14 -8 -4 205.99 11.73 14 -8 -4 215.01 16.88 -14 -8 4 208.32 15.32 14 -8 -4 198.84 13.36 -14 -8 4 203.03 15.55 -14 8 4 215.72 13.95 -14 8 4 203.73 14.87 -12 -8 4 452.70 22.31 12 -8 -4 405.08 22.46 12 -8 -4 443.68 19.71 -12 -8 4 427.68 22.37 12 -8 -4 438.71 20.93 -12 8 4 412.16 21.11 -12 8 4 445.08 22.19 10 -8 -4 145.92 12.80 -10 -8 4 193.25 14.25 10 -8 -4 176.28 11.43 10 -8 -4 172.53 12.85 -10 8 4 179.17 14.04 -10 8 4 197.61 13.02 8 -8 -4 1906.92 74.13 8 -8 -4 1866.65 75.11 -8 -8 4 1990.18 75.80 -8 -8 4 2043.20 75.95 -8 8 4 1900.23 75.42 8 8 -4 2101.32 75.70 -8 8 4 1900.78 75.06 6 -8 -4 1247.04 53.55 -6 -8 4 1324.70 53.91 6 -8 -4 1319.07 52.84 -6 -8 4 1407.41 54.26 -6 8 4 1288.10 53.70 -6 8 4 1331.45 53.50 6 8 -4 1518.61 54.36 4 -8 -4 2253.92 89.98 -4 -8 4 2349.24 90.21 -4 -8 4 2315.89 89.80 4 -8 -4 2398.65 89.51 -4 8 4 2473.51 90.32 4 8 -4 2355.97 89.93 -4 8 4 2395.33 89.92 -2 -8 4 944.95 42.73 2 -8 -4 1143.23 43.06 2 -8 -4 1116.05 43.65 -2 -8 4 904.95 42.07 -2 8 4 1211.31 43.57 2 8 -4 908.93 42.38 0 -8 -4 520.25 25.15 0 -8 4 463.42 24.40 0 -8 -4 551.05 24.87 0 -8 -4 575.66 22.98 0 -8 4 458.21 23.73 0 8 4 520.05 24.51 0 8 -4 466.27 24.41 -2 -8 -4 491.99 24.61 -2 -8 -4 493.91 22.71 2 -8 4 483.33 23.19 -2 -8 -4 523.83 24.27 2 -8 4 441.18 23.81 2 8 4 513.72 24.16 -2 8 -4 487.49 24.05 -4 -8 -4 140.56 13.38 -4 -8 -4 145.71 12.47 -4 -8 -4 148.51 12.66 4 -8 4 135.15 11.37 4 -8 4 152.71 13.05 -4 8 -4 147.29 12.86 4 8 4 144.94 12.52 -6 -8 -4 1.15 5.25 6 -8 4 8.30 5.18 6 -8 4 10.06 5.77 -6 -8 -4 10.23 6.74 -6 -8 -4 4.49 5.75 6 8 4 15.08 5.74 -6 8 -4 13.46 5.53 -8 -8 -4 199.59 18.18 -8 -8 -4 180.20 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58.09 -15 9 5 1384.08 56.53 -13 -9 5 458.18 24.68 13 -9 -5 438.83 20.98 13 -9 -5 465.49 25.54 -13 -9 5 452.96 24.34 13 -9 -5 457.03 22.74 -13 9 5 442.82 24.18 -13 9 5 459.03 23.35 11 -9 -5 1873.85 74.25 11 -9 -5 1915.13 72.64 11 -9 -5 1894.17 74.07 -11 -9 5 1867.27 74.98 -11 -9 5 1950.08 75.07 -11 9 5 1931.85 74.91 -11 9 5 1931.56 74.37 -9 -9 5 456.75 25.61 9 -9 -5 458.59 23.42 -9 -9 5 584.77 26.60 9 -9 -5 449.15 24.62 -9 9 5 497.78 24.87 -9 9 5 497.63 25.65 9 9 -5 592.15 26.06 7 -9 -5 1971.88 74.54 -7 -9 5 1972.97 76.07 -7 -9 5 1916.62 75.63 7 -9 -5 1882.58 75.56 -7 9 5 1880.76 75.12 7 9 -5 2015.26 75.85 -7 9 5 1913.57 75.77 -5 -9 5 691.40 32.84 5 -9 -5 775.18 32.42 5 -9 -5 693.98 33.00 -5 -9 5 612.56 32.26 -5 9 5 802.27 33.71 5 9 -5 650.20 32.70 -5 9 5 843.81 33.36 -3 -9 5 464.69 24.91 3 -9 -5 535.04 25.22 3 -9 -5 486.02 25.76 -3 -9 5 467.47 25.46 -3 9 5 521.13 25.37 -3 9 5 545.16 26.21 1 -9 -5 26.96 7.64 -1 -9 5 21.62 6.72 -1 -9 5 23.66 7.12 1 -9 -5 49.46 8.33 1 9 -5 30.72 9.45 -1 9 5 58.78 8.66 -1 -9 -5 3.92 6.49 1 -9 5 8.76 6.07 1 -9 5 4.22 6.16 -1 -9 -5 0.39 5.62 -1 9 -5 7.81 6.99 1 9 5 0.48 5.42 3 -9 5 86.15 9.63 -3 -9 -5 88.42 10.63 3 -9 5 92.11 11.25 -3 -9 -5 95.46 12.40 -3 -9 -5 74.92 10.27 -3 9 -5 70.78 9.39 3 9 5 82.47 9.87 -5 -9 -5 492.73 24.87 -5 -9 -5 478.49 26.04 5 -9 5 479.10 23.72 5 -9 5 450.76 24.96 -5 -9 -5 485.69 26.08 -5 9 -5 487.47 25.22 5 9 5 461.44 24.96 5 9 5 491.76 25.18 7 -9 5 252.85 18.04 -7 -9 -5 214.44 17.24 7 -9 5 249.16 15.99 -7 -9 -5 247.47 18.86 -7 -9 -5 242.09 20.18 7 9 5 282.94 18.19 7 9 5 234.61 17.18 -7 9 -5 226.78 17.64 9 -9 5 1405.71 58.35 -9 -9 -5 1402.28 58.43 9 -9 5 1498.33 57.13 -9 -9 -5 1448.92 59.81 -9 -9 -5 1394.09 61.85 9 9 5 1468.06 59.12 -9 9 -5 1480.80 58.91 9 9 5 1346.30 56.43 11 -9 5 193.72 16.97 -11 -9 -5 183.87 21.97 -11 -9 -5 208.57 18.93 -11 -9 -5 149.46 16.33 11 -9 5 190.42 14.07 11 9 5 197.21 16.88 -11 9 -5 148.69 17.70 11 9 5 182.57 13.78 -13 -9 -5 1974.49 83.39 13 -9 5 2016.42 75.53 13 -9 5 1889.17 76.92 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27 -9 5 4.42 7.50 -27 -9 -5 -3.44 12.05 27 -9 5 1.47 16.94 -27 9 -5 3.45 14.31 27 9 5 5.86 9.36 29 -9 5 59.36 22.24 29 -9 5 60.81 10.49 -29 -9 -5 37.87 27.57 -29 -9 -5 43.22 16.42 -29 9 -5 53.15 18.73 29 9 5 57.33 11.53 31 -9 5 30.98 10.46 31 -9 5 27.71 24.07 31 -9 5 10.90 8.92 -31 -9 -5 51.03 29.98 31 9 5 8.15 9.77 -31 9 -5 28.73 18.00 -32 -10 5 6.12 14.18 32 -10 -5 23.22 22.41 -32 -10 5 23.71 16.24 -32 -10 5 -18.55 34.22 -32 10 5 30.03 16.90 -30 -10 5 176.58 24.43 -30 -10 5 110.66 17.05 30 -10 -5 144.11 25.56 -30 -10 5 150.61 34.48 -30 10 5 129.39 17.91 -28 -10 5 4.52 11.75 -28 -10 5 -5.04 12.12 28 -10 -5 42.79 18.52 -28 -10 5 -0.88 26.76 -28 10 5 -19.64 11.72 -26 -10 5 156.56 16.58 26 -10 -5 181.62 23.78 -26 -10 5 186.11 31.08 -26 -10 5 174.58 18.61 -26 10 5 178.59 17.57 -24 -10 5 -3.89 9.45 -24 -10 5 6.41 10.91 24 -10 -5 -2.52 13.68 -24 10 5 -16.88 10.07 22 -10 -5 318.48 15.94 -22 -10 5 330.81 34.57 -22 -10 5 321.51 24.16 22 -10 -5 320.48 15.60 22 -10 -5 301.80 29.43 -22 -10 5 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115.93 13.71 -4 10 -5 106.72 12.31 4 10 5 128.72 14.49 6 -10 5 412.71 22.64 -6 -10 -5 435.10 25.65 6 -10 5 384.26 24.88 -6 -10 -5 411.62 25.86 -6 -10 -5 400.87 24.03 6 10 5 375.72 24.15 -6 10 -5 432.24 25.06 6 10 5 437.15 24.33 8 -10 5 180.51 18.80 -8 -10 -5 166.27 16.98 -8 -10 -5 172.78 21.28 -8 -10 -5 157.10 18.47 8 -10 5 176.54 15.11 8 10 5 178.66 16.92 8 10 5 169.42 16.42 10 -10 5 135.87 13.93 -10 -10 -5 127.78 16.20 10 -10 5 142.63 15.52 -10 -10 -5 142.09 18.67 10 10 5 139.08 16.19 10 10 5 117.87 14.37 12 -10 5 61.99 8.69 12 -10 5 61.06 11.16 -12 -10 -5 74.72 16.05 -12 -10 -5 46.45 10.31 12 10 5 48.40 10.07 12 10 5 50.31 8.81 14 -10 5 13.34 9.21 -14 -10 -5 20.54 10.30 14 -10 5 12.51 7.05 -14 -10 -5 17.66 14.73 -14 10 -5 35.75 10.34 14 10 5 12.25 8.74 16 -10 5 102.70 12.83 16 -10 5 73.65 11.93 -16 -10 -5 112.39 20.66 -16 -10 -5 88.29 13.61 16 10 5 93.74 13.62 -16 10 -5 106.27 13.87 -18 -10 -5 96.06 14.21 -18 -10 -5 151.68 23.70 18 -10 5 105.22 11.14 18 -10 5 95.05 12.75 -18 10 -5 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5 -11.23 13.63 -25 -11 5 186.79 22.52 25 -11 -5 258.99 32.44 -25 -11 5 195.59 20.55 -25 -11 5 242.80 32.95 -25 11 5 196.71 20.16 -23 -11 5 18.24 21.42 23 -11 -5 63.53 7.62 -23 -11 5 53.69 12.85 -23 -11 5 68.52 17.56 23 -11 -5 94.68 18.96 23 -11 -5 63.33 7.53 23 11 -5 68.03 12.01 -23 11 5 69.56 14.60 21 -11 -5 20.74 14.50 21 -11 -5 18.88 6.45 -21 -11 5 4.78 10.79 -21 -11 5 14.96 12.05 21 -11 -5 28.82 7.47 21 11 -5 17.23 10.83 -21 11 5 26.74 12.53 19 -11 -5 74.46 16.02 -19 -11 5 74.85 13.59 19 -11 -5 79.11 8.59 19 -11 -5 63.26 9.61 -19 -11 5 48.59 20.65 -19 -11 5 70.58 13.20 -19 11 5 64.51 11.69 -19 11 5 72.64 13.92 19 11 -5 66.03 12.95 -17 -11 5 -1.89 9.69 -17 -11 5 -19.01 9.35 17 -11 -5 1.44 5.72 -17 -11 5 -6.30 16.50 17 -11 -5 7.63 11.69 17 -11 -5 -9.53 7.37 -17 11 5 2.16 7.99 -17 11 5 -5.55 9.69 17 11 -5 0.89 10.41 -15 -11 5 183.11 20.70 15 -11 -5 163.92 13.81 15 -11 -5 156.52 16.72 -15 -11 5 170.32 20.16 15 -11 -5 158.50 20.28 -15 11 5 164.43 17.46 -15 11 5 154.04 19.80 13 -11 -5 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36.76 -24 4 9 775.37 30.22 -24 4 9 769.51 40.80 -24 4 9 759.84 43.93 -24 4 9 791.33 30.08 -22 -4 9 15.23 4.61 -22 -4 9 -4.70 10.17 -22 4 9 10.04 3.36 -22 4 9 10.61 3.96 22 4 -9 9.35 8.03 -22 4 9 12.83 9.95 -20 -4 9 352.20 16.32 -20 4 9 370.75 23.94 -20 4 9 329.65 26.93 20 4 -9 336.63 21.82 -20 4 9 326.20 14.95 -20 4 9 342.60 15.32 -18 -4 9 67.23 6.70 -18 4 9 54.76 6.19 18 4 -9 59.26 10.57 -18 4 9 67.23 11.61 -18 4 9 60.77 6.77 -18 4 9 88.78 14.84 -16 -4 9 45.66 5.87 -16 4 9 51.78 5.35 -16 4 9 52.97 5.46 -16 4 9 61.42 9.63 16 4 -9 43.75 9.20 -16 4 9 69.01 13.12 -14 -4 9 128.15 9.49 14 4 -9 131.18 14.57 -14 4 9 135.56 8.73 -14 4 9 139.77 8.78 -14 4 9 160.55 17.33 -14 4 9 128.85 12.69 -12 -4 9 24.70 4.81 -12 4 9 33.21 4.78 12 4 -9 17.68 7.07 -12 4 9 37.93 6.72 -12 4 9 28.88 8.78 -12 4 9 38.49 5.04 12 4 -9 28.83 3.96 -10 -4 9 2665.98 97.49 10 -4 -9 2698.79 95.78 10 -4 -9 2665.41 95.57 -10 4 9 2582.41 97.66 10 4 -9 2580.48 102.02 -10 4 9 2716.39 97.86 10 4 -9 2509.31 96.58 -10 4 9 2675.04 103.03 8 -4 -9 122.71 7.84 8 -4 -9 136.45 7.13 -8 -4 9 125.01 8.73 -8 4 9 132.89 13.59 -8 4 9 120.17 8.89 8 4 -9 113.20 8.30 -8 4 9 104.75 7.96 8 4 -9 122.84 12.82 6 -4 -9 1016.28 38.63 6 -4 -9 1007.91 38.29 -6 -4 9 914.94 38.77 6 4 -9 974.86 43.40 -6 4 9 1069.19 43.87 -6 4 9 1020.22 39.82 6 4 -9 970.27 38.79 -4 -4 9 487.68 21.68 4 -4 -9 511.71 21.58 4 -4 -9 501.28 21.69 -4 4 9 518.77 22.78 -4 4 9 544.45 26.05 4 4 -9 490.94 21.76 2 -4 -9 873.37 37.56 2 -4 -9 864.07 34.37 2 -4 -9 842.52 34.08 -2 -4 9 824.68 33.84 -2 4 9 849.73 37.47 -2 4 9 867.87 35.18 2 4 -9 833.38 34.05 0 -4 -9 717.57 31.74 0 -4 -9 665.54 29.01 0 -4 9 670.76 28.28 0 4 9 727.18 28.48 0 4 -9 684.23 28.56 0 4 9 656.28 31.21 0 4 9 720.85 29.84 2 -4 9 221.04 11.61 -2 -4 -9 194.57 12.55 -2 -4 -9 213.76 14.93 2 4 9 207.95 14.14 -2 4 -9 213.18 12.11 2 4 9 211.57 13.16 2 4 9 202.41 12.78 -4 -4 -9 1535.78 60.89 -4 -4 -9 1483.93 59.66 4 -4 9 1559.22 58.42 4 4 9 1489.48 60.66 4 4 9 1531.93 59.91 4 4 9 1543.47 60.48 -4 4 -9 1552.79 58.76 -6 -4 -9 191.23 13.25 6 -4 9 205.24 11.51 -6 -4 -9 190.65 14.19 6 4 9 180.63 12.49 6 4 9 184.69 15.39 6 4 9 199.82 13.36 -6 4 -9 199.51 12.27 8 -4 9 686.72 28.07 -8 -4 -9 633.65 29.96 -8 -4 -9 638.54 29.83 8 4 9 661.19 32.93 8 4 9 680.72 29.68 -8 4 -9 684.74 28.73 10 -4 9 1095.68 43.11 -10 -4 -9 1092.13 44.58 -10 -4 -9 1072.75 45.26 10 4 9 1070.58 48.97 -10 4 -9 1102.85 43.78 10 4 9 1064.06 44.54 12 -4 9 97.10 9.25 -12 -4 -9 76.99 9.54 -12 -4 -9 107.88 11.63 12 4 9 102.52 10.47 -12 4 -9 87.67 10.77 12 4 9 90.00 13.83 14 -4 9 966.56 39.13 -14 -4 -9 978.50 40.42 14 4 9 933.20 46.96 14 4 9 952.72 40.63 -16 -4 -9 28.58 7.97 -16 -4 -9 38.77 7.43 16 -4 9 30.50 5.96 16 4 9 26.59 6.43 -16 4 -9 47.79 8.31 16 4 9 41.68 13.23 -18 -4 -9 1898.00 75.30 18 -4 9 1962.44 75.13 -18 -4 -9 1998.62 77.90 -18 4 -9 1906.90 76.41 18 4 9 2007.26 85.26 18 4 9 1964.03 76.35 20 -4 9 64.34 17.20 20 -4 9 137.53 12.20 -20 -4 -9 104.62 12.54 -20 -4 -9 102.89 13.68 20 4 9 108.57 19.04 -20 4 -9 149.17 16.10 20 4 9 112.67 12.94 -22 -4 -9 782.71 36.38 22 -4 9 734.44 33.42 -22 -4 -9 712.96 33.67 22 -4 9 842.54 46.92 -22 4 -9 746.95 35.69 22 4 9 749.71 45.50 22 4 9 762.38 34.35 -24 -4 -9 366.64 23.76 24 -4 9 301.34 31.13 24 -4 9 334.35 19.55 24 4 9 357.80 20.65 -24 4 -9 333.34 22.91 24 4 9 296.36 32.70 -26 -4 -9 272.18 21.94 26 -4 9 257.51 31.51 26 -4 9 239.51 16.98 26 4 9 252.49 18.03 26 4 9 242.29 32.73 -26 4 -9 198.33 20.79 28 -4 9 102.58 24.21 28 -4 9 99.64 11.36 -28 -4 -9 95.00 14.96 28 4 9 138.49 25.27 -28 4 -9 99.43 14.40 28 4 9 114.59 14.75 30 -4 9 8.86 7.54 -30 -4 -9 3.55 11.51 30 -4 9 -6.82 17.84 -30 4 -9 -10.57 11.55 30 4 9 6.69 8.20 30 4 9 1.26 22.80 32 -4 9 46.63 24.05 32 -4 9 55.10 9.67 -32 -4 -9 41.71 14.09 32 4 9 46.61 23.77 -32 4 -9 62.67 15.50 32 4 9 31.23 9.64 34 -4 9 156.31 32.67 -34 -4 -9 125.23 19.16 34 -4 9 143.83 17.38 -34 4 -9 133.64 19.88 34 4 9 159.66 17.70 34 4 9 192.84 31.11 -39 -5 9 41.76 11.20 -39 -5 9 80.16 39.35 -39 -5 9 38.16 13.00 -39 5 9 48.56 11.43 -39 5 9 71.35 33.92 -37 -5 9 80.80 12.93 -37 -5 9 2.06 29.12 -37 5 9 7.86 22.15 -37 5 9 72.49 11.06 -37 5 9 172.80 32.82 -35 -5 9 66.54 28.17 -35 -5 9 155.19 15.90 -35 -5 9 148.12 14.12 -35 5 9 115.80 15.07 -35 5 9 99.78 28.67 -33 -5 9 -4.26 7.14 -33 5 9 24.44 7.49 -33 5 9 -12.04 17.72 -33 5 9 61.96 23.85 -31 -5 9 228.83 16.99 -31 -5 9 224.18 16.22 -31 5 9 241.18 15.43 -31 5 9 227.26 30.10 -31 5 9 232.47 29.25 -31 5 9 251.72 14.04 -29 -5 9 46.74 7.80 -29 -5 9 57.15 8.85 -29 5 9 63.82 7.60 -29 5 9 68.08 20.02 -29 5 9 106.15 17.70 -27 -5 9 94.73 11.65 -27 -5 9 81.84 10.58 -27 5 9 146.48 18.76 -27 5 9 95.66 10.48 -27 5 9 111.96 22.45 27 5 -9 86.52 13.68 -27 5 9 108.60 8.86 -25 -5 9 497.91 22.91 -25 -5 9 513.04 37.16 -25 -5 9 476.30 22.07 25 5 -9 438.61 27.46 -25 5 9 445.80 38.82 -25 5 9 508.35 31.24 -25 5 9 507.92 21.72 -25 5 9 486.05 21.05 -23 -5 9 19.47 12.52 -23 -5 9 16.88 5.25 -23 -5 9 18.33 5.88 -23 5 9 23.57 4.76 -23 5 9 26.40 10.52 -23 5 9 6.51 13.48 -23 5 9 25.34 5.37 23 5 -9 10.68 8.78 -21 -5 9 449.59 20.66 -21 -5 9 457.11 21.04 -21 5 9 451.45 19.65 -21 5 9 453.05 20.12 21 5 -9 407.92 25.64 -21 5 9 458.20 32.68 -21 5 9 486.29 27.05 -19 -5 9 -7.99 4.29 -19 5 9 -4.59 17.99 -19 5 9 9.61 7.79 -19 5 9 -1.40 3.23 19 5 -9 -7.69 7.27 -17 -5 9 421.38 20.21 17 5 -9 412.19 25.26 -17 5 9 466.91 19.97 -17 5 9 427.85 19.19 -17 5 9 442.31 23.83 -17 5 9 455.88 29.86 -15 -5 9 107.56 9.95 -15 5 9 115.63 8.73 15 5 -9 160.86 15.29 -15 5 9 128.72 18.80 -15 5 9 108.51 9.46 -15 5 9 118.72 12.11 -13 -5 9 414.08 19.10 -13 5 9 408.77 19.93 -13 5 9 412.96 26.70 -13 5 9 412.11 18.89 -13 5 9 403.19 18.57 13 5 -9 408.07 24.09 11 -5 -9 373.99 15.18 11 -5 -9 350.77 15.34 -11 -5 9 369.49 17.64 -11 5 9 348.78 17.23 -11 5 9 386.18 24.11 11 5 -9 379.71 22.21 -11 5 9 374.51 17.61 11 5 -9 348.04 16.52 9 -5 -9 139.53 8.85 9 -5 -9 152.07 8.49 -9 -5 9 145.34 10.30 9 5 -9 139.02 14.54 -9 5 9 141.51 15.54 -9 5 9 144.28 10.03 9 5 -9 132.76 9.69 7 -5 -9 340.89 16.09 -7 -5 9 357.27 16.81 7 -5 -9 342.76 15.88 -7 5 9 353.56 17.17 -7 5 9 367.36 21.92 7 5 -9 329.59 16.49 5 -5 -9 417.54 18.86 -5 -5 9 401.72 19.06 5 -5 -9 407.56 18.77 -5 5 9 453.12 23.55 -5 5 9 410.06 19.57 5 5 -9 389.10 18.93 3 -5 -9 64.32 7.89 3 -5 -9 66.90 7.83 3 5 -9 82.11 8.52 -3 5 9 64.41 8.22 -3 5 9 83.16 11.81 1 -5 -9 1143.43 45.34 -1 -5 9 1148.45 45.06 1 -5 -9 1097.67 45.69 -1 5 9 1213.59 46.43 1 5 -9 1124.99 45.21 -1 5 9 1157.93 48.21 -1 -5 -9 164.95 11.20 1 -5 9 173.55 10.57 -1 -5 -9 153.23 11.58 1 5 9 151.51 11.53 -1 5 -9 148.00 10.97 1 5 9 177.63 14.21 3 -5 9 557.76 24.01 -3 -5 -9 520.44 25.44 3 5 9 566.54 25.52 3 5 9 567.08 25.37 -3 5 -9 536.54 24.52 3 5 9 549.93 26.48 -5 -5 -9 338.93 18.66 5 -5 9 351.42 16.89 -5 5 -9 318.28 17.49 5 5 9 332.69 19.10 5 5 9 343.03 18.35 5 5 9 353.02 20.00 -7 -5 -9 863.18 37.85 -7 -5 -9 891.37 38.24 7 -5 9 908.94 35.91 -7 5 -9 873.18 36.43 7 5 9 841.34 39.11 7 5 9 862.71 37.04 7 5 9 869.91 37.29 9 -5 9 615.68 26.25 -9 -5 -9 601.60 28.28 -9 -5 -9 585.86 28.64 9 5 9 556.74 27.45 9 5 9 615.76 31.09 -9 5 -9 609.77 27.29 -11 -5 -9 497.70 26.17 11 -5 9 506.20 23.00 -11 -5 -9 458.82 24.50 11 5 9 537.90 29.24 -11 5 -9 477.73 24.15 11 5 9 510.94 24.64 13 -5 9 791.24 33.87 -13 -5 -9 779.66 36.52 -13 -5 -9 801.53 34.85 13 5 9 804.27 35.51 13 5 9 884.20 41.34 -13 5 -9 774.74 34.92 -15 -5 -9 75.89 10.99 15 -5 9 54.76 7.68 -15 -5 -9 65.34 9.53 15 5 9 64.67 8.66 -15 5 -9 53.12 9.00 15 5 9 84.68 14.98 -17 -5 -9 702.19 34.46 17 -5 9 694.52 30.69 17 5 9 719.21 39.84 -17 5 -9 704.93 32.86 17 5 9 688.49 32.47 -19 -5 -9 33.19 9.86 19 -5 9 40.94 7.41 -19 5 -9 55.15 9.90 19 5 9 33.11 7.65 19 5 9 68.06 16.15 21 -5 9 67.69 8.82 -21 -5 -9 52.64 10.79 21 -5 9 35.77 15.02 21 5 9 78.02 10.14 21 5 9 61.07 15.94 -21 5 -9 63.78 10.91 23 -5 9 420.60 22.79 -23 -5 -9 418.04 26.32 23 -5 9 379.95 35.60 23 5 9 406.89 23.41 -23 5 -9 440.52 26.16 23 5 9 445.96 36.09 25 -5 9 24.35 16.38 25 -5 9 26.67 7.80 -25 -5 -9 23.02 10.78 25 5 9 37.98 17.31 -25 5 -9 45.80 11.08 25 5 9 33.83 8.57 -27 -5 -9 330.25 26.00 27 -5 9 383.87 21.66 27 -5 9 339.12 36.46 27 5 9 357.78 38.64 -27 5 -9 338.52 26.86 27 5 9 340.74 22.07 -29 -5 -9 68.47 13.24 29 -5 9 49.20 9.60 29 -5 9 -2.22 18.64 29 5 9 92.27 11.67 -29 5 -9 50.90 14.12 29 5 9 106.21 25.12 31 -5 9 251.56 34.70 31 -5 9 261.83 19.56 -31 -5 -9 309.69 28.56 31 5 9 229.31 32.92 31 5 9 289.99 21.36 -31 5 -9 259.39 28.52 33 -5 9 195.11 17.77 33 -5 9 182.54 33.74 33 -5 9 140.98 14.60 -33 -5 -9 132.46 18.84 -33 5 -9 176.30 20.97 33 5 9 196.27 20.41 33 5 9 195.86 31.49 -38 -6 9 359.54 26.66 -38 -6 9 339.40 27.29 -38 6 9 440.55 60.53 -38 6 9 299.06 25.21 -36 -6 9 229.83 22.54 -36 -6 9 254.34 20.38 -36 -6 9 232.16 40.00 -36 6 9 200.28 36.20 -36 6 9 214.00 20.71 -34 -6 9 152.86 33.33 -34 -6 9 163.22 18.07 -34 -6 9 152.99 18.98 -34 6 9 146.53 17.13 -34 6 9 114.66 30.40 -32 -6 9 6.28 9.03 -32 6 9 12.92 8.64 -32 6 9 14.63 6.17 -32 6 9 9.33 21.75 -30 -6 9 -5.37 7.93 -30 -6 9 -3.17 7.14 -30 6 9 -6.10 19.67 -30 6 9 1.50 5.35 -30 6 9 26.04 7.96 -28 -6 9 96.65 10.41 -28 -6 9 115.65 13.90 -28 6 9 88.87 10.32 28 6 -9 111.57 14.62 -28 6 9 109.35 22.26 -28 6 9 99.88 12.68 -26 -6 9 83.08 9.13 -26 -6 9 76.45 9.90 -26 6 9 91.47 11.58 -26 6 9 71.80 21.26 -26 6 9 71.74 9.30 26 6 -9 74.13 12.75 -24 -6 9 1147.91 45.13 -24 -6 9 1117.71 45.56 24 6 -9 1130.52 49.30 -24 6 9 1055.63 58.47 -24 6 9 1121.28 44.48 -24 6 9 1107.75 43.86 -22 -6 9 307.23 17.06 -22 -6 9 285.08 28.55 -22 -6 9 272.63 16.35 -22 6 9 282.49 14.95 -22 6 9 264.20 30.61 -22 6 9 269.98 15.72 22 6 -9 291.75 21.31 -20 -6 9 1059.36 42.61 -20 -6 9 1046.36 42.91 -20 6 9 1091.98 42.32 -20 6 9 1077.50 41.72 -20 6 9 1025.90 53.51 20 6 -9 1015.84 47.10 -18 -6 9 396.85 20.06 -18 -6 9 429.15 20.59 -18 6 9 408.73 19.03 18 6 -9 384.99 24.82 -18 6 9 416.43 31.06 -18 6 9 412.44 19.94 -16 -6 9 1074.49 43.60 -16 -6 9 1101.62 43.96 16 6 -9 1086.53 48.48 -16 6 9 1084.71 42.99 -16 6 9 1117.69 43.49 -16 6 9 1063.18 56.92 -14 -6 9 234.74 14.62 -14 6 9 252.78 23.18 -14 6 9 227.10 14.00 -14 6 9 238.29 13.42 14 6 -9 258.94 19.77 12 -6 -9 673.65 25.79 12 -6 -9 636.73 25.59 -12 -6 9 677.19 28.40 12 6 -9 653.30 32.74 -12 6 9 652.53 27.72 -12 6 9 620.65 34.83 12 6 -9 626.70 27.04 -12 6 9 634.36 27.99 10 -6 -9 15.94 3.90 10 -6 -9 15.88 4.21 -10 -6 9 18.09 5.33 -10 6 9 17.00 5.48 -10 6 9 17.43 4.78 10 6 -9 2.72 7.13 10 6 -9 13.91 5.03 -10 6 9 29.37 9.81 8 -6 -9 29.51 5.14 8 -6 -9 41.05 5.76 -8 -6 9 29.95 5.92 -8 6 9 41.43 6.33 8 6 -9 35.16 6.05 -8 6 9 44.42 9.73 6 -6 -9 52.67 6.75 6 -6 -9 57.63 6.67 -6 -6 9 79.18 8.75 -6 6 9 61.78 11.31 -6 6 9 57.86 6.87 6 6 -9 74.27 9.24 4 -6 -9 113.30 10.25 4 -6 -9 124.85 10.28 -4 -6 9 124.11 10.16 -4 6 9 118.76 14.25 4 6 -9 119.33 10.68 -4 6 9 126.66 10.56 2 -6 -9 92.42 9.52 2 -6 -9 83.45 9.90 -2 6 9 92.71 12.94 -2 6 9 96.22 9.89 0 -6 -9 1192.73 49.63 0 -6 9 1235.96 48.47 0 -6 -9 1247.08 49.02 0 6 9 1281.83 49.76 0 6 9 1188.33 51.30 0 6 -9 1207.46 48.82 -2 -6 -9 385.34 19.09 -2 -6 -9 349.96 19.72 2 -6 9 353.23 18.03 2 6 9 356.75 19.35 2 6 9 377.39 21.47 -2 6 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1086.58 41.15 -4 0 10 8402.53 329.96 4 0 -10 8304.62 329.41 -4 0 10 9988.89 334.86 4 0 -10 9999.00 335.08 -2 0 10 3753.68 145.37 2 0 -10 4531.94 150.39 2 0 -10 3708.57 144.82 0 0 10 4648.57 174.14 0 0 -10 5054.23 178.28 0 0 -10 4665.55 173.70 2 0 10 2018.85 77.72 -2 0 -10 2023.09 77.35 -2 0 -10 2200.31 81.60 -4 0 -10 1258.19 48.93 4 0 10 1263.14 49.16 -4 0 -10 1287.86 52.52 -6 0 -10 1572.23 59.97 -6 0 -10 1565.14 63.20 6 0 10 1562.89 60.13 -8 0 -10 2011.72 74.81 -8 0 -10 1963.00 77.53 8 0 10 1927.26 74.59 10 0 10 732.98 31.44 -10 0 -10 756.91 31.82 12 0 10 20.01 4.99 -12 0 -10 23.68 5.66 -14 0 -10 5.30 5.09 14 0 10 -1.70 3.74 14 0 10 13.07 8.91 16 0 10 6.62 4.47 -16 0 -10 -3.29 7.03 16 0 10 -5.06 8.11 18 0 10 312.56 17.56 18 0 10 322.72 25.26 -18 0 -10 309.88 19.42 20 0 10 245.49 25.67 20 0 10 250.55 16.21 -20 0 -10 274.18 18.79 22 0 10 477.17 24.38 -22 0 -10 485.86 26.76 22 0 10 524.03 36.59 24 0 10 1335.98 66.92 -24 0 -10 1308.93 55.76 24 0 10 1332.35 54.03 26 0 10 420.92 23.28 26 0 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10 228.02 28.11 -23 -1 -10 236.18 19.02 23 1 10 221.39 28.14 23 1 10 229.54 16.23 -23 1 -10 203.10 18.97 -25 -1 -10 18.03 9.05 25 -1 10 0.93 14.64 25 -1 10 18.67 6.86 25 1 10 21.94 15.39 25 1 10 -2.01 6.03 -25 1 -10 13.12 8.93 27 -1 10 27.24 18.09 27 -1 10 23.28 7.62 -27 -1 -10 32.38 10.18 -27 1 -10 22.67 10.28 27 1 10 -4.76 14.88 27 1 10 22.56 7.49 29 -1 10 54.91 9.50 -29 -1 -10 49.81 12.47 29 -1 10 49.26 21.07 29 1 10 56.06 9.34 -29 1 -10 40.98 12.98 29 1 10 22.42 23.32 -31 -1 -10 95.98 15.02 31 -1 10 129.00 27.66 31 -1 10 92.14 11.35 -31 1 -10 74.49 14.50 31 1 10 84.25 10.97 31 1 10 106.11 26.79 33 -1 10 23.31 8.56 33 -1 10 19.30 22.81 -33 -1 -10 5.54 13.67 33 1 10 -4.52 23.40 -33 1 -10 -12.98 13.31 33 1 10 -5.00 7.75 -35 -1 -10 228.67 29.55 35 -1 10 251.51 20.32 35 -1 10 248.57 37.11 35 1 10 235.21 19.39 -35 1 -10 254.54 29.42 35 1 10 199.20 34.69 -40 -2 10 61.53 33.38 -40 -2 10 39.90 28.41 -40 2 10 77.09 31.75 -40 2 10 102.27 26.85 -38 -2 10 10.70 27.78 -38 -2 10 32.95 21.20 -38 2 10 -20.20 24.42 -38 2 10 5.80 23.40 -36 -2 10 33.76 25.78 -36 -2 10 26.74 19.86 -36 2 10 34.23 23.21 -36 2 10 28.07 22.48 -34 -2 10 59.94 23.53 -34 -2 10 58.31 19.29 -34 2 10 49.52 20.37 -34 2 10 3.46 18.62 -32 -2 10 10.77 15.29 -32 -2 10 7.65 17.73 -32 2 10 6.73 16.50 -32 2 10 -5.27 16.89 -30 -2 10 50.28 17.96 -30 -2 10 52.16 16.04 -30 2 10 67.19 18.37 -30 2 10 66.15 17.65 -28 -2 10 93.91 16.68 -28 -2 10 131.01 20.56 -28 2 10 76.07 17.90 -28 2 10 90.37 18.51 -26 -2 10 299.91 27.91 -26 -2 10 279.04 24.64 -26 2 10 287.85 27.62 -26 2 10 267.56 28.27 -24 -2 10 428.92 28.26 24 2 -10 437.59 26.98 -24 2 10 450.69 32.01 -24 2 10 454.19 30.34 -22 -2 10 27.67 11.02 -22 -2 10 31.82 9.80 -22 2 10 31.57 12.16 -22 2 10 21.67 9.68 22 2 -10 22.17 9.51 -20 -2 10 340.87 22.72 -20 -2 10 339.17 24.42 -20 -2 10 332.40 14.34 -20 2 10 353.29 25.60 -20 2 10 327.25 22.14 20 2 -10 284.65 21.35 -18 -2 10 147.45 8.34 -18 -2 10 120.45 14.73 18 2 -10 126.99 15.08 -18 2 10 157.14 18.30 -18 2 10 154.42 15.15 -16 -2 10 453.81 26.07 -16 -2 10 479.52 19.76 16 2 -10 455.93 26.09 -16 2 10 507.69 19.36 -16 2 10 500.71 28.49 -16 2 10 501.70 25.12 -14 -2 10 1.30 5.87 -14 -2 10 10.96 3.17 14 -2 -10 5.42 6.29 14 2 -10 4.95 6.75 -14 2 10 6.94 5.58 -14 2 10 8.16 2.86 -14 2 10 4.65 7.36 12 -2 -10 701.22 32.44 -12 -2 10 654.43 31.88 -12 -2 10 710.27 26.65 12 2 -10 613.74 32.40 -12 2 10 675.44 33.09 -12 2 10 667.02 26.58 -10 -2 10 1144.77 44.02 10 -2 -10 1245.97 49.69 -10 2 10 1238.98 50.61 10 2 -10 1062.95 49.11 -10 2 10 1135.43 44.31 -8 -2 10 413.55 17.86 8 -2 -10 446.00 17.31 8 -2 -10 417.62 16.63 8 -2 -10 442.89 23.02 -8 2 10 487.38 24.03 -8 2 10 408.98 18.43 8 2 -10 397.01 22.93 8 2 -10 401.62 17.37 6 -2 -10 1503.15 54.63 6 -2 -10 1429.45 53.96 6 -2 -10 1587.91 59.78 -6 -2 10 1341.39 54.65 -6 2 10 1476.09 55.49 6 2 -10 1389.97 54.48 6 2 -10 1328.14 59.27 -6 2 10 1638.08 60.34 4 -2 -10 57.46 8.53 4 -2 -10 64.55 5.35 -4 -2 10 60.12 5.88 4 2 -10 59.45 9.36 -4 2 10 65.25 6.70 -4 2 10 52.58 8.09 4 2 -10 62.83 6.00 2 -2 -10 1533.88 58.99 2 -2 -10 1459.52 54.45 -2 -2 10 1378.56 54.61 2 2 -10 1436.50 59.37 -2 2 10 1445.78 55.57 2 2 -10 1379.89 54.45 -2 2 10 1500.29 58.68 0 -2 -10 1332.92 52.77 0 -2 -10 1288.86 49.11 0 -2 10 1255.50 49.02 0 2 -10 1226.48 48.84 0 2 10 1240.44 49.88 0 2 10 1359.25 52.82 -2 -2 -10 217.50 12.10 2 -2 10 226.19 11.77 -2 -2 -10 237.70 15.75 2 2 10 224.86 12.69 2 2 10 216.37 14.67 -2 2 -10 219.96 11.81 -4 -2 -10 1399.07 57.88 -4 -2 -10 1436.80 55.44 4 -2 10 1453.23 54.95 4 2 10 1434.68 56.00 -4 2 -10 1447.18 54.90 -6 -2 -10 47.85 6.33 -6 -2 -10 64.52 8.71 6 -2 10 58.14 6.63 6 2 10 45.48 6.29 -6 2 -10 58.34 7.36 -8 -2 -10 1346.49 54.37 -8 -2 -10 1356.18 55.90 8 -2 10 1369.09 53.35 8 2 10 1372.58 54.43 -8 2 -10 1451.99 53.86 -10 -2 -10 3.93 5.73 10 -2 10 -0.10 3.44 -10 -2 -10 -0.52 4.36 10 2 10 0.02 6.07 10 2 10 2.11 4.01 -10 2 -10 3.04 4.56 12 -2 10 964.27 39.35 -12 -2 -10 969.14 40.87 -12 -2 -10 938.50 41.58 12 2 10 936.02 40.10 12 2 10 1035.36 44.94 -12 2 -10 982.41 40.12 -14 -2 -10 532.88 26.83 -14 -2 -10 519.92 26.23 14 -2 10 550.20 24.68 14 2 10 556.41 25.50 -14 2 -10 540.15 25.64 14 2 10 514.45 30.76 -16 -2 -10 153.42 15.19 16 -2 10 162.96 12.45 -16 -2 -10 175.28 14.65 16 2 10 168.66 19.84 16 2 10 175.56 13.09 -16 2 -10 199.77 14.60 -18 -2 -10 1106.65 48.65 -18 -2 -10 1170.65 48.57 18 -2 10 1115.42 46.55 -18 2 -10 1145.81 48.03 18 2 10 1148.46 47.47 18 2 10 1186.17 56.08 -20 -2 -10 145.98 16.19 -20 -2 -10 79.19 12.44 20 -2 10 109.90 11.75 20 -2 10 98.45 16.72 20 2 10 133.59 12.90 20 2 10 110.12 20.26 -20 2 -10 100.96 12.50 22 -2 10 702.61 31.67 -22 -2 -10 740.61 33.95 22 -2 10 724.55 42.52 -22 -2 -10 656.07 34.15 -22 2 -10 675.23 33.60 22 2 10 675.48 31.80 22 2 10 703.34 43.70 -24 -2 -10 286.96 21.62 -24 -2 -10 313.50 20.88 24 -2 10 247.71 17.16 24 -2 10 235.49 29.34 24 2 10 266.15 18.00 -24 2 -10 239.42 20.89 24 2 10 213.24 31.15 -26 -2 -10 229.69 20.29 26 -2 10 254.66 32.66 26 -2 10 223.70 16.68 -26 -2 -10 249.43 21.32 26 2 10 231.53 32.87 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12.54 -35 3 10 118.79 27.44 -35 3 10 118.08 22.91 -33 -3 10 782.31 54.20 -33 -3 10 763.00 45.84 -33 -3 10 830.77 33.26 -33 -3 10 812.49 32.27 -33 3 10 740.88 52.54 -33 3 10 759.19 51.74 -31 -3 10 115.71 22.67 -31 -3 10 140.58 19.68 -31 -3 10 159.93 12.14 -31 -3 10 162.53 10.74 -31 3 10 143.49 25.09 -31 3 10 173.61 23.95 -29 -3 10 464.46 19.46 -29 -3 10 394.09 30.97 -29 -3 10 459.69 36.80 -29 -3 10 473.81 20.37 -29 3 10 420.11 40.64 -29 3 10 373.03 38.88 -27 -3 10 211.84 11.23 -27 -3 10 221.63 29.54 -27 -3 10 218.15 12.45 -27 -3 10 193.79 22.75 -27 3 10 210.84 28.65 -27 3 10 186.33 25.54 -25 -3 10 125.15 18.07 -25 -3 10 120.03 18.83 -25 -3 10 99.63 9.12 -25 3 10 124.66 18.89 -25 3 10 148.24 20.01 25 3 -10 124.09 16.98 -23 -3 10 6.37 10.36 -23 -3 10 2.79 3.92 -23 -3 10 2.02 8.66 -23 3 10 7.79 10.41 23 3 -10 3.45 8.54 -21 -3 10 257.47 20.32 -21 -3 10 276.89 24.13 -21 -3 10 266.94 13.28 -21 3 10 302.18 25.85 21 3 -10 278.37 20.52 -21 3 10 266.35 21.65 -19 -3 10 12.51 7.62 -19 -3 10 -1.88 3.39 -19 3 10 0.68 7.69 19 3 -10 3.49 7.08 -19 3 10 0.44 2.81 -19 3 10 15.33 9.82 -17 -3 10 1090.59 48.56 -17 -3 10 1106.33 42.88 -17 3 10 1111.36 47.62 17 3 -10 1064.91 48.86 -17 3 10 1152.87 42.55 -17 3 10 1161.60 52.11 -17 3 10 1149.78 42.34 -15 -3 10 221.36 11.88 -15 3 10 235.19 20.33 -15 3 10 224.81 15.55 15 3 -10 230.08 18.54 -15 3 10 236.27 11.61 -13 -3 10 3565.79 127.77 13 3 -10 3385.47 133.21 -13 3 10 3400.72 130.04 -13 3 10 3621.69 135.04 -13 3 10 3515.18 127.91 -11 -3 10 840.48 32.52 11 -3 -10 811.46 38.04 11 3 -10 796.15 37.94 -11 3 10 877.40 39.37 11 3 -10 808.10 31.23 -11 3 10 823.47 32.87 -11 3 10 812.02 34.04 9 -3 -10 4603.95 164.73 9 -3 -10 4564.91 164.41 -9 -3 10 4413.91 165.88 9 -3 -10 4723.01 171.22 9 3 -10 4433.27 171.07 9 3 -10 4510.27 165.28 -9 3 10 4516.17 166.57 -9 3 10 4765.75 171.93 7 -3 -10 58.77 5.04 -7 -3 10 68.07 6.80 7 -3 -10 68.44 10.10 7 -3 -10 67.40 6.15 -7 3 10 64.04 6.99 7 3 -10 56.06 9.45 -7 3 10 64.54 9.93 7 3 -10 65.01 6.62 5 -3 -10 2839.72 103.27 -5 -3 10 2671.85 103.78 5 -3 -10 2898.52 103.81 5 -3 -10 2898.39 108.22 5 3 -10 2706.14 103.66 -5 3 10 2972.55 108.79 -5 3 10 2975.46 105.05 5 3 -10 2618.86 108.49 -3 -3 10 7.84 3.44 3 -3 -10 2.87 2.88 3 -3 -10 1.91 5.75 -3 3 10 5.74 3.23 3 3 -10 8.03 3.62 -3 3 10 -0.59 5.21 3 3 -10 1.81 5.44 -1 -3 10 1017.24 41.29 1 -3 -10 1081.87 45.11 1 -3 -10 1071.74 41.55 -1 3 10 1123.98 45.47 -1 3 10 1041.78 42.51 1 3 -10 1054.58 41.49 -1 -3 -10 22.20 6.49 -1 -3 -10 8.73 3.73 1 -3 10 12.01 3.68 -1 3 -10 8.77 3.52 1 3 10 10.17 5.54 1 3 10 5.39 3.75 -3 -3 -10 217.13 15.21 -3 -3 -10 217.54 12.79 3 -3 10 212.01 11.74 -3 3 -10 209.73 12.05 3 3 10 209.54 14.65 3 3 10 207.71 12.84 -5 -3 -10 142.32 11.41 5 -3 10 174.04 10.26 -5 -3 -10 159.19 13.58 5 3 10 134.74 13.37 5 3 10 178.57 12.87 -5 3 -10 153.75 10.76 5 3 10 170.66 11.58 -7 -3 -10 1759.43 69.59 7 -3 10 1751.57 66.90 -7 -3 -10 1682.58 68.12 -7 3 -10 1745.18 67.25 7 3 10 1853.56 70.31 -9 -3 -10 22.35 7.25 -9 -3 -10 27.43 6.43 9 -3 10 14.03 4.28 9 3 10 19.57 5.33 9 3 10 13.86 6.60 -9 3 -10 20.67 5.27 11 -3 10 1996.86 76.24 -11 -3 -10 2014.75 78.56 -11 -3 -10 1954.75 78.04 -11 3 -10 2038.57 76.95 11 3 10 2011.68 77.64 11 3 10 2032.17 82.06 -13 -3 -10 31.54 7.89 -13 -3 -10 32.64 7.43 13 -3 10 42.26 6.61 -13 3 -10 28.91 6.89 13 3 10 35.79 7.11 13 3 10 31.62 10.86 15 -3 10 2586.11 96.54 -15 -3 -10 2606.97 98.71 -15 -3 -10 2525.72 98.04 -15 3 -10 2527.19 97.38 15 3 10 2557.68 97.75 15 3 10 2550.94 104.30 -17 -3 -10 -2.73 6.57 17 -3 10 4.34 5.01 -17 -3 -10 6.07 6.93 17 3 10 -1.29 5.23 -17 3 -10 -1.19 6.45 17 3 10 5.35 10.51 -19 -3 -10 1673.94 67.80 19 -3 10 1655.84 66.35 -19 -3 -10 1767.24 69.34 19 3 10 1732.00 76.91 -19 3 -10 1674.33 67.85 19 3 10 1671.40 67.17 21 -3 10 92.26 19.28 -21 -3 -10 109.56 12.71 21 -3 10 121.04 12.68 -21 -3 -10 73.82 11.57 -21 3 -10 146.94 15.37 21 3 10 77.07 17.96 21 3 10 97.23 12.72 23 -3 10 669.27 41.07 23 -3 10 629.03 29.39 -23 -3 -10 607.80 31.88 -23 -3 -10 593.87 30.92 -23 3 -10 606.69 31.66 23 3 10 599.55 42.46 23 3 10 599.25 29.58 -25 -3 -10 36.89 11.06 25 -3 10 25.53 7.76 25 -3 10 18.04 15.22 -25 3 -10 15.47 9.72 25 3 10 25.17 7.73 25 3 10 4.66 16.58 27 -3 10 11.66 7.37 -27 -3 -10 9.86 10.27 27 -3 10 -6.11 15.62 -27 -3 -10 8.98 10.16 27 3 10 5.29 17.44 27 3 10 9.86 6.89 -27 3 -10 -20.48 9.98 -29 -3 -10 2.68 10.35 29 -3 10 -3.87 7.11 29 -3 10 12.43 18.64 -29 -3 -10 -3.75 11.11 -29 3 -10 -18.04 11.65 29 3 10 -0.03 7.11 31 -3 10 338.21 21.77 -31 -3 -10 338.22 28.29 31 -3 10 294.44 37.45 -31 -3 -10 349.96 26.14 31 3 10 369.84 42.25 -31 3 -10 340.56 28.62 31 3 10 350.45 22.60 33 -3 10 22.46 23.33 -33 -3 -10 19.72 13.34 33 -3 10 21.26 9.02 -33 3 -10 25.81 15.27 33 3 10 22.23 9.32 33 3 10 -8.89 21.33 -40 -4 10 7.86 21.72 -40 -4 10 -6.00 11.46 -40 -4 10 -9.92 9.01 -40 4 10 42.10 24.75 -40 4 10 18.58 32.20 -38 -4 10 289.82 42.67 -38 -4 10 219.52 34.68 -38 -4 10 252.04 18.81 -38 -4 10 280.80 21.12 -38 4 10 278.61 40.18 -38 4 10 249.22 37.46 -36 -4 10 54.36 8.77 -36 -4 10 90.71 29.29 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26.99 -16 -2 23 270.52 23.70 16 -2 -23 348.99 41.59 -16 2 23 261.87 24.01 16 2 -23 319.07 41.82 -16 2 23 250.83 33.10 -14 -2 23 -13.16 10.63 14 -2 -23 -26.04 19.68 -14 2 23 -3.04 10.71 14 2 -23 3.59 20.91 -14 2 23 15.97 21.90 12 -2 -23 35.10 22.95 -12 -2 23 20.32 10.89 -12 2 23 42.77 12.34 12 2 -23 34.28 21.57 10 -2 -23 5.35 8.10 10 -2 -23 -5.03 20.35 10 -2 -23 9.35 8.69 -10 -2 23 9.09 10.83 10 2 -23 1.33 9.42 -10 2 23 17.94 10.73 10 2 -23 1.66 22.01 -8 -2 23 78.96 17.29 8 -2 -23 162.61 17.46 8 -2 -23 149.41 17.06 8 -2 -23 108.68 24.45 8 2 -23 106.49 25.33 8 2 -23 135.60 14.48 -8 2 23 135.89 24.52 6 -2 -23 118.98 12.92 6 -2 -23 116.75 25.02 -6 -2 23 101.74 14.61 6 2 -23 87.23 26.31 -6 2 23 90.27 15.16 4 -2 -23 272.65 38.70 4 -2 -23 174.77 20.86 -4 -2 23 217.36 22.30 -4 2 23 219.63 24.76 4 2 -23 227.09 22.85 4 2 -23 260.28 34.91 2 -2 -23 187.74 23.45 2 -2 -23 247.39 32.67 -2 -2 23 183.05 22.30 -2 2 23 269.32 25.99 2 2 -23 228.93 23.89 2 2 -23 178.24 31.32 0 -2 -23 495.45 29.95 0 -2 23 453.52 30.34 0 -2 -23 504.05 45.55 0 2 23 465.71 32.14 0 2 -23 476.73 48.80 0 2 -23 433.02 31.08 2 -2 23 139.28 17.50 -2 -2 -23 132.54 27.59 -2 2 -23 106.40 27.36 2 2 23 120.27 17.37 4 -2 23 666.69 37.89 -4 -2 -23 663.44 53.52 -4 2 -23 636.16 39.73 4 2 23 705.39 38.97 -4 2 -23 656.20 55.26 -6 -2 -23 27.55 16.34 6 -2 23 49.61 14.11 -6 -2 -23 64.62 26.94 6 2 23 61.78 14.78 -6 2 -23 36.80 24.37 -6 2 -23 37.62 18.23 -21 -3 23 263.21 24.74 21 -3 -23 294.15 37.87 -21 3 23 221.58 23.44 21 3 -23 292.80 36.49 19 -3 -23 -27.01 18.35 -19 -3 23 3.17 11.11 -19 3 23 22.48 11.89 19 3 -23 1.54 23.93 -17 -3 23 144.28 16.27 17 -3 -23 162.69 28.69 -17 3 23 113.51 29.08 17 3 -23 142.26 28.35 -17 3 23 152.15 18.02 15 -3 -23 -2.56 21.65 -15 -3 23 11.42 10.82 15 3 -23 -6.83 20.87 -15 3 23 10.96 23.80 -15 3 23 12.95 12.01 -13 -3 23 34.12 11.58 13 -3 -23 35.87 22.91 -13 3 23 47.94 25.33 -13 3 23 26.62 12.22 13 3 -23 29.05 22.76 11 -3 -23 6.78 21.26 -11 3 23 5.98 21.10 11 3 -23 9.90 21.03 -11 3 23 -1.01 11.14 11 3 -23 8.62 9.55 9 -3 -23 2.45 9.40 9 -3 -23 8.98 8.81 9 -3 -23 -8.38 20.41 -9 -3 23 16.25 11.09 9 3 -23 5.14 21.53 9 3 -23 9.39 10.81 -7 -3 23 3.30 10.56 7 -3 -23 3.51 10.12 7 -3 -23 9.93 9.67 7 -3 -23 4.05 20.48 -7 3 23 3.05 11.23 7 3 -23 -41.41 21.18 7 3 -23 2.47 12.76 5 -3 -23 39.42 20.05 -5 -3 23 54.06 12.52 5 -3 -23 63.51 12.20 5 -3 -23 92.96 24.93 5 3 -23 49.41 14.13 -5 3 23 50.57 13.74 5 3 -23 58.55 24.06 3 -3 -23 -25.47 20.01 3 -3 -23 14.41 11.81 -3 -3 23 10.08 11.36 -3 3 23 2.84 11.14 3 3 -23 -4.97 12.55 3 3 -23 15.67 23.28 -1 -3 23 213.13 23.17 1 -3 -23 242.98 32.09 1 -3 -23 224.99 23.42 1 3 -23 194.48 31.66 -1 3 23 216.96 25.21 1 3 -23 200.66 25.28 -1 -3 -23 74.49 24.86 1 -3 23 52.86 14.45 -1 -3 -23 86.81 16.69 1 3 23 87.90 16.77 -1 3 -23 87.53 28.93 3 -3 23 348.70 26.51 -3 -3 -23 318.86 44.34 -3 3 -23 260.10 30.66 -3 3 -23 308.54 38.69 3 3 23 296.09 28.36 5 -3 23 39.63 13.87 -5 -3 -23 26.95 16.58 -5 -3 -23 21.27 23.80 -5 3 -23 56.37 28.43 5 3 23 44.59 14.65 -5 3 -23 51.10 17.63 -18 -4 23 144.72 16.28 -18 4 23 195.31 24.42 -18 4 23 151.49 17.17 18 4 -23 145.30 29.98 -16 -4 23 77.28 13.96 16 -4 -23 70.24 24.69 -16 4 23 54.03 13.75 -16 4 23 74.45 30.08 16 4 -23 48.57 27.54 14 -4 -23 231.76 30.96 -14 4 23 177.34 31.86 14 4 -23 195.94 31.75 -14 4 23 248.75 23.83 -12 -4 23 29.46 12.40 12 -4 -23 36.02 22.58 -12 4 23 26.91 12.65 12 4 -23 11.94 9.45 12 4 -23 9.61 24.64 -12 4 23 14.88 26.13 10 -4 -23 52.53 10.20 10 -4 -23 51.18 23.69 -10 -4 23 80.97 13.34 10 -4 -23 70.01 9.46 10 4 -23 55.63 12.52 -10 4 23 48.50 16.80 -10 4 23 69.06 24.28 10 4 -23 37.96 25.70 8 -4 -23 276.94 21.37 8 -4 -23 293.49 41.41 -8 -4 23 230.86 23.56 8 -4 -23 230.55 19.55 8 4 -23 245.65 23.85 8 4 -23 243.98 35.95 -8 4 23 243.63 25.83 6 -4 -23 19.61 11.66 6 -4 -23 -13.67 11.06 -6 -4 23 22.71 11.89 6 -4 -23 14.64 20.99 -6 4 23 -4.95 11.49 6 4 -23 -5.22 13.61 6 4 -23 -9.20 22.93 -4 -4 23 308.75 25.52 4 -4 -23 283.05 23.54 4 -4 -23 257.51 23.23 4 -4 -23 303.25 42.94 4 4 -23 272.90 35.37 -4 4 23 259.88 27.57 4 4 -23 291.55 27.24 -2 -4 23 -17.05 10.31 2 -4 -23 10.03 22.69 2 -4 -23 27.69 12.38 2 4 -23 -17.82 23.72 -2 4 23 -14.66 12.23 2 4 -23 18.75 14.57 0 -4 -23 574.95 50.63 0 -4 23 539.08 33.13 0 -4 -23 550.30 33.62 0 4 -23 638.07 56.35 0 4 23 521.25 36.24 -2 -4 -23 103.30 27.56 2 -4 23 90.36 15.18 2 4 23 44.54 21.00 -2 4 -23 86.25 18.28 -2 4 -23 41.05 28.91 2 4 23 88.58 16.17 -13 -5 23 41.20 12.53 -13 5 23 -2.11 14.92 -13 5 23 -0.35 26.86 13 5 -23 12.10 26.24 -11 -5 23 434.33 30.34 11 -5 -23 536.81 47.90 -11 5 23 480.28 50.56 -11 5 23 453.67 32.14 11 5 -23 471.74 28.39 11 5 -23 482.70 53.04 9 -5 -23 62.08 23.69 9 -5 -23 55.64 11.60 9 -5 -23 25.45 9.76 -9 -5 23 49.49 13.24 -9 5 23 32.47 14.54 9 5 -23 46.53 14.42 9 5 -23 96.98 28.08 -9 5 23 28.40 25.79 7 -5 -23 362.02 26.27 7 -5 -23 352.30 45.02 -7 -5 23 402.57 28.23 7 -5 -23 342.59 24.35 -7 5 23 375.64 46.60 7 5 -23 390.01 29.26 -7 5 23 369.28 30.00 7 5 -23 352.70 42.69 5 -5 -23 322.70 26.02 5 -5 -23 287.70 34.80 -5 -5 23 307.35 26.47 5 -5 -23 298.26 24.32 5 5 -23 268.27 28.36 -5 5 23 309.09 28.12 5 5 -23 352.14 41.57 3 -5 -23 97.91 14.71 3 -5 -23 116.98 28.86 3 -5 -23 83.21 15.43 -3 -5 23 107.58 15.49 3 5 -23 122.23 18.48 -3 5 23 115.11 18.05 3 5 -23 177.72 33.33 -18 0 24 760.94 41.26 18 0 -24 893.99 60.99 16 0 -24 219.50 30.36 -16 0 24 150.03 18.40 14 0 -24 911.66 60.32 -14 0 24 801.78 42.94 12 0 -24 351.31 44.56 -12 0 24 325.05 38.04 -10 0 24 763.57 43.12 10 0 -24 915.10 58.52 10 0 -24 869.21 36.59 8 0 -24 -3.32 10.96 -8 0 24 14.61 11.93 8 0 -24 0.46 21.33 6 0 -24 7.35 20.64 6 0 -24 53.37 16.00 -6 0 24 35.38 12.37 -4 0 24 14.66 11.77 4 0 -24 2.44 12.89 4 0 -24 25.21 23.75 2 0 -24 31.37 13.26 -2 0 24 22.24 12.14 2 0 -24 29.47 22.16 0 0 -24 83.18 27.50 0 0 24 95.36 16.71 0 0 -24 51.20 15.79 2 0 24 244.68 26.92 17 -1 -24 31.74 25.22 -17 -1 24 52.62 13.58 -17 1 24 39.13 12.96 17 1 -24 44.79 26.69 -15 -1 24 21.16 12.26 15 -1 -24 8.71 21.65 -15 1 24 -8.85 10.97 15 1 -24 15.74 22.41 -13 -1 24 24.14 15.05 13 -1 -24 50.54 25.74 -13 1 24 32.62 13.15 13 1 -24 15.40 24.36 -11 -1 24 29.27 13.86 11 -1 -24 -18.44 21.03 -11 1 24 14.90 21.12 11 1 -24 20.93 22.33 -9 -1 24 49.51 13.10 9 -1 -24 74.26 11.21 9 -1 -24 43.49 11.01 9 -1 -24 90.03 25.02 9 1 -24 72.06 12.31 -9 1 24 32.58 12.68 9 1 -24 52.70 23.92 7 -1 -24 321.28 42.23 7 -1 -24 211.35 21.04 -7 -1 24 216.03 24.41 7 1 -24 203.12 21.88 -7 1 24 219.24 25.08 7 1 -24 154.65 28.02 5 -1 -24 89.19 25.30 -5 -1 24 70.54 15.12 5 -1 -24 109.06 14.72 5 1 -24 85.53 14.54 -5 1 24 60.80 13.74 5 1 -24 47.13 23.93 3 -1 -24 148.97 29.85 3 -1 -24 134.90 18.10 -3 -1 24 127.51 17.13 3 1 -24 158.50 32.49 3 1 -24 153.03 16.79 -3 1 24 132.38 18.81 -1 -1 24 11.13 12.28 1 -1 -24 17.90 13.92 1 -1 -24 4.29 22.79 1 1 -24 13.86 14.67 -1 1 24 10.65 13.39 1 1 -24 -21.02 23.78 1 -1 24 130.21 18.34 -1 -1 -24 146.75 29.62 1 1 24 81.81 16.18 -1 1 -24 101.23 30.27 16 -2 -24 53.39 25.17 -16 -2 24 29.54 12.63 16 2 -24 80.29 28.27 -16 2 24 25.32 12.35 14 -2 -24 365.48 45.80 -14 2 24 322.53 26.98 14 2 -24 232.92 33.38 12 -2 -24 5.57 23.29 -12 -2 24 8.34 11.20 12 2 -24 9.75 21.94 -10 -2 24 124.83 16.53 10 -2 -24 168.67 16.14 10 -2 -24 143.91 28.19 -10 2 24 155.89 19.32 10 2 -24 118.13 29.37 10 2 -24 140.43 14.15 8 -2 -24 20.35 11.30 -8 -2 24 25.43 11.82 8 -2 -24 1.95 23.47 8 -2 -24 35.82 11.17 8 2 -24 21.33 24.83 8 2 -24 28.78 12.68 -8 2 24 38.61 14.10 6 -2 -24 72.24 14.57 -6 -2 24 54.29 13.28 6 -2 -24 70.24 23.48 -6 2 24 73.51 16.75 6 2 -24 101.67 15.74 6 2 -24 46.78 27.58 4 -2 -24 21.57 12.61 4 -2 -24 53.87 23.75 -4 -2 24 20.27 13.21 -4 2 24 28.40 13.38 4 2 -24 26.62 16.92 4 2 -24 28.97 27.17 2 -2 -24 22.18 23.50 2 -2 -24 18.28 13.09 -2 -2 24 12.58 11.65 2 2 -24 8.47 25.34 2 2 -24 21.73 14.43 -2 2 24 24.18 13.76 0 -2 -24 123.22 29.68 0 -2 -24 117.07 17.55 0 -2 24 113.95 16.51 0 2 -24 64.49 28.78 0 2 24 107.91 17.24 -13 -3 24 18.89 12.34 13 -3 -24 -26.51 20.39 -13 3 24 1.88 16.50 13 3 -24 10.16 24.17 11 -3 -24 367.83 45.39 -11 -3 24 296.06 26.57 -11 3 24 306.25 27.73 11 3 -24 283.53 39.47 11 3 -24 307.85 22.30 9 -3 -24 27.60 10.64 9 -3 -24 45.37 25.77 9 -3 -24 47.62 11.25 -9 -3 24 53.66 13.43 9 3 -24 23.19 25.04 9 3 -24 42.70 12.60 -9 3 24 42.20 15.21 7 -3 -24 703.04 35.74 -7 -3 24 694.19 38.57 7 -3 -24 837.27 56.88 7 -3 -24 811.50 36.83 7 3 -24 702.28 60.34 -7 3 24 677.34 40.86 5 -3 -24 2.47 23.39 -5 -3 24 42.66 12.66 5 -3 -24 -7.04 11.94 5 -3 -24 14.39 12.55 5 3 -24 -13.17 24.88 -5 3 24 19.31 13.40 5 3 -24 51.78 16.06 -3 -3 24 802.93 43.46 3 -3 -24 915.02 60.77 3 -3 -24 826.14 42.20 3 3 -24 915.99 64.83 -3 3 24 892.03 46.40 3 3 -24 868.66 43.78 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 17050 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.43605(19) 0.1757(6) 0.4316(3) 0.0274(15) Uani 1 1 d . . . . . C2 C 0.47667(19) 0.1640(6) 0.4294(3) 0.0295(16) Uani 1 1 d . . . . . C3 C 0.4875(2) 0.1448(7) 0.3701(4) 0.0388(19) Uani 1 1 d . . . . . H3 H 0.469487 0.133615 0.332247 0.047 Uiso 1 1 calc R . . . . C4 C 0.5249(2) 0.1423(8) 0.3668(4) 0.050(2) Uani 1 1 d . . . . . H4 H 0.531773 0.129878 0.326696 0.061 Uiso 1 1 calc R . . . . C5 C 0.5037(2) 0.1779(6) 0.4860(4) 0.0310(16) Uani 1 1 d . . . . . H5 H 0.496796 0.189812 0.526157 0.037 Uiso 1 1 calc R . . . . C6 C 0.5408(2) 0.1740(7) 0.4819(4) 0.0365(18) Uani 1 1 d . . . . . C7 C 0.5522(2) 0.1581(9) 0.4224(4) 0.051(2) Uani 1 1 d . . . . . H7 H 0.577384 0.158040 0.420211 0.061 Uiso 1 1 calc R . . . . C8 C 0.5958(2) 0.2621(8) 0.5406(4) 0.048(2) Uani 1 1 d . . . . . H8 H 0.596000 0.302085 0.503065 0.058 Uiso 1 1 calc R . . . . C9 C 0.5684(2) 0.1320(7) 0.5948(4) 0.044(2) Uani 1 1 d . . . . . H9 H 0.549748 0.081465 0.593801 0.052 Uiso 1 1 calc R . . . . C10 C 0.5945(2) 0.1468(7) 0.6520(4) 0.040(2) Uani 1 1 d . . . . . H10 H 0.593364 0.106911 0.689253 0.049 Uiso 1 1 calc R . . . . C11 C 0.6229(2) 0.2783(7) 0.5965(4) 0.043(2) Uani 1 1 d . . . . . H11 H 0.641587 0.328014 0.595731 0.051 Uiso 1 1 calc R . . . . C12 C 0.62259(19) 0.2219(6) 0.6536(4) 0.0293(16) Uani 1 1 d . . . . . C13 C 0.65127(19) 0.2423(6) 0.7138(3) 0.0263(15) Uani 1 1 d . . . . . C14 C 0.64495(19) 0.2171(6) 0.7755(4) 0.0312(16) Uani 1 1 d . . . . . H14 H 0.623211 0.181412 0.779445 0.037 Uiso 1 1 calc R . . . . C15 C 0.6851(2) 0.2910(6) 0.7106(4) 0.0320(16) Uani 1 1 d . . . . . H15 H 0.690560 0.307409 0.669856 0.038 Uiso 1 1 calc R . . . . C16 C 0.7101(2) 0.3147(6) 0.7664(3) 0.0294(16) Uani 1 1 d . . . . . H16 H 0.732696 0.346627 0.763519 0.035 Uiso 1 1 calc R . . . . C17 C 0.67062(19) 0.2444(6) 0.8312(3) 0.0292(15) Uani 1 1 d . . . . . H17 H 0.665779 0.229409 0.872628 0.035 Uiso 1 1 calc R . . . . C18 C 0.72936(18) 0.3237(6) 0.8846(3) 0.0242(14) Uani 1 1 d . . . . . C19 C 0.76488(18) 0.2809(6) 0.8943(3) 0.0232(14) Uani 1 1 d . . . . . H19 H 0.771594 0.234148 0.864037 0.028 Uiso 1 1 calc R . . . . C20 C 0.71780(19) 0.3927(6) 0.9283(3) 0.0282(15) Uani 1 1 d . . . . . H20 H 0.693591 0.419497 0.920693 0.034 Uiso 1 1 calc R . . . . C21 C 0.7438(2) 0.4202(6) 0.9838(3) 0.0313(16) Uani 1 1 d . . . . . H21 H 0.737060 0.467369 1.013877 0.038 Uiso 1 1 calc R . . . . C22 C 0.7790(2) 0.3795(6) 0.9954(3) 0.0281(15) Uani 1 1 d . . . . . H22 H 0.795749 0.398384 1.033496 0.034 Uiso 1 1 calc R . . . . C23 C 0.79040(18) 0.3099(5) 0.9509(3) 0.0219(14) Uani 1 1 d . . . . . C24 C 0.82888(18) 0.2640(5) 0.9640(3) 0.0207(13) Uani 1 1 d . . . . . C25 C 0.2565(2) 0.2689(7) 0.1082(4) 0.042(2) Uani 1 1 d . . . . . H25 H 0.271246 0.213795 0.097793 0.050 Uiso 1 1 calc R . . . . C26 C 0.2669(2) 0.3221(6) 0.1672(3) 0.0292(16) Uani 1 1 d . . . . . C27 C 0.3006(2) 0.2880(6) 0.2170(3) 0.0296(16) Uani 1 1 d . . . . . C28 C 0.24495(19) 0.4056(6) 0.1827(3) 0.0266(15) Uani 1 1 d . . . . . H28 H 0.251942 0.441517 0.222343 0.032 Uiso 1 1 calc R . . . . C29 C 0.2242(2) 0.2979(7) 0.0646(4) 0.044(2) Uani 1 1 d . . . . . H29 H 0.217222 0.261923 0.024948 0.053 Uiso 1 1 calc R . . . . C30 C 0.2024(2) 0.3800(7) 0.0796(4) 0.0352(18) Uani 1 1 d . . . . . H30 H 0.180741 0.398990 0.050196 0.042 Uiso 1 1 calc R . . . . C31 C 0.21283(19) 0.4343(6) 0.1388(3) 0.0272(15) Uani 1 1 d . . . . . C32 C 0.18955(18) 0.5233(6) 0.1556(3) 0.0246(14) Uani 1 1 d . . . . . C33 C 0.4042(2) 0.4240(6) 0.3473(3) 0.0316(16) Uani 1 1 d . . . . . C34 C 0.42021(19) 0.5128(6) 0.3149(3) 0.0262(15) Uani 1 1 d . . . . . C35 C 0.4077(2) 0.5321(6) 0.2477(3) 0.0292(15) Uani 1 1 d . . . . . H35 H 0.389037 0.489730 0.223696 0.035 Uiso 1 1 calc R . . . . C36 C 0.4096(2) 0.6302(6) 0.1451(3) 0.0303(16) Uani 1 1 d . . . . . C37 C 0.4228(2) 0.6133(6) 0.2166(3) 0.0271(15) Uani 1 1 d . . . . . C38 C 0.4514(2) 0.6748(6) 0.2524(4) 0.0349(17) Uani 1 1 d . . . . . H38 H 0.461899 0.729069 0.231773 0.042 Uiso 1 1 calc R . . . . C39 C 0.4643(2) 0.6550(7) 0.3189(4) 0.0395(19) Uani 1 1 d . . . . . H39 H 0.483738 0.695201 0.342473 0.047 Uiso 1 1 calc R . . . . C40 C 0.4484(2) 0.5763(6) 0.3500(3) 0.0319(16) Uani 1 1 d . . . . . H40 H 0.456473 0.565553 0.394892 0.038 Uiso 1 1 calc R . . . . Cl1 Cl 0.34312(11) 0.5097(4) 0.4790(2) 0.1076(12) Uani 1 1 d . U . . . Eu1 Eu 0.39612(2) 0.36235(3) 0.50623(2) 0.02503(12) Uani 1 1 d . U . . . Eu2 Eu 0.35580(2) 0.19374(3) 0.31367(2) 0.02074(11) Uani 1 1 d . . . . . N1 N 0.70245(15) 0.2925(5) 0.8255(3) 0.0247(12) Uani 1 1 d . . . . . N2 N 0.56940(17) 0.1891(5) 0.5405(3) 0.0332(14) Uani 1 1 d . . . . . N3 N 0.3960(2) 0.0687(6) 0.2288(4) 0.0469(18) Uani 1 1 d . . . . . N4 N 0.4586(4) 0.4938(10) 0.5336(6) 0.088(4) Uani 1 1 d . . . . . O1 O 0.42762(15) 0.2115(5) 0.4829(3) 0.0391(12) Uani 1 1 d . U . . . O2 O 0.41296(14) 0.1499(5) 0.3813(3) 0.0390(12) Uani 1 1 d . U . . . O3 O 0.84322(12) 0.2300(4) 0.9171(2) 0.0245(10) Uani 1 1 d . U . . . O4 O 0.84643(13) 0.2565(4) 1.0223(2) 0.0294(11) Uani 1 1 d . U . . . O5 O 0.32439(15) 0.2280(5) 0.1997(2) 0.0393(11) Uani 1 1 d . U . . . O6 O 0.30340(14) 0.3172(4) 0.2764(2) 0.0343(10) Uani 1 1 d . U . . . O7 O 0.20144(14) 0.5800(4) 0.2051(2) 0.0324(10) Uani 1 1 d . U . . . O8 O 0.15793(13) 0.5420(4) 0.1199(2) 0.0312(11) Uani 1 1 d . U . . . O9 O 0.41112(17) 0.4216(5) 0.4090(3) 0.0484(12) Uani 1 1 d . U . . . O10 O 0.38462(17) 0.3568(5) 0.3120(3) 0.0453(12) Uani 1 1 d . U . . . O11 O 0.38411(16) 0.5729(5) 0.1133(3) 0.0437(12) Uani 1 1 d . U . . . O12 O 0.42451(17) 0.7019(5) 0.1158(3) 0.0444(13) Uani 1 1 d . U . . . O13 O 0.4898(5) 0.5670(16) 0.5348(9) 0.198(7) Uiso 1 1 d . . . . . O14 O 0.4679(4) 0.4065(11) 0.5291(6) 0.126(4) Uani 1 1 d . U . . . O15 O 0.4332(4) 0.5270(10) 0.5369(6) 0.111(3) Uani 1 1 d . U . . . O16 O 0.40420(17) 0.1637(5) 0.2370(3) 0.0467(14) Uani 1 1 d . . . . . O17 O 0.36947(15) 0.0333(4) 0.2539(3) 0.0379(12) Uani 1 1 d . . . . . O18 O 0.4136(3) 0.0080(8) 0.2008(6) 0.123(4) Uani 1 1 d . . . . . O20 O 0.3823(2) 0.0031(6) 0.5085(4) 0.068(2) Uani 1 1 d . . . . . H20A H 0.371818 0.034543 0.472875 0.101 Uiso 1 1 d G . . . . H20B H 0.394814 0.052140 0.531889 0.101 Uiso 1 1 d G . . . . O21 O 0.2858(3) -0.0161(8) 0.1580(4) 0.091(3) Uani 1 1 d . . . . . O22 O 0.2925(2) 0.4926(6) 0.3567(5) 0.077(2) Uani 1 1 d . . . . . H22A H 0.294614 0.440463 0.330984 0.116 Uiso 1 1 d G . . . . H22B H 0.268720 0.500381 0.353211 0.116 Uiso 1 1 d G . . . . O19 O 0.4731(4) 0.1214(9) 0.6313(7) 0.140(5) Uani 1 1 d . . . . . O23 O 0.3383(4) -0.1054(17) 0.5836(5) 0.200(9) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.020(3) 0.034(4) 0.024(4) 0.000(3) -0.004(3) 0.003(3) C2 0.020(3) 0.039(4) 0.026(4) -0.003(3) -0.003(3) 0.006(3) C3 0.026(4) 0.059(5) 0.028(4) -0.011(4) -0.004(3) 0.004(4) C4 0.032(5) 0.089(7) 0.029(4) -0.014(4) 0.002(3) 0.012(5) C5 0.022(4) 0.040(4) 0.028(4) -0.005(3) -0.002(3) 0.002(3) C6 0.023(4) 0.054(5) 0.028(4) -0.005(4) -0.006(3) 0.006(3) C7 0.023(4) 0.087(7) 0.042(5) -0.006(5) 0.005(4) 0.012(4) C8 0.030(4) 0.078(7) 0.034(4) 0.010(4) -0.001(3) -0.010(4) C9 0.036(4) 0.041(5) 0.045(5) 0.007(4) -0.014(4) -0.008(4) C10 0.037(4) 0.041(5) 0.037(4) 0.012(4) -0.010(4) -0.007(4) C11 0.033(4) 0.061(6) 0.030(4) 0.007(4) -0.005(3) -0.015(4) C12 0.020(3) 0.036(4) 0.029(4) 0.001(3) -0.003(3) 0.003(3) C13 0.022(3) 0.029(4) 0.025(3) 0.001(3) -0.004(3) 0.000(3) C14 0.017(3) 0.044(4) 0.031(4) 0.003(3) 0.001(3) -0.004(3) C15 0.027(4) 0.048(4) 0.020(3) 0.000(3) 0.003(3) -0.005(3) C16 0.022(4) 0.043(4) 0.023(3) 0.000(3) 0.003(3) -0.010(3) C17 0.022(4) 0.040(4) 0.026(4) -0.001(3) 0.005(3) -0.002(3) C18 0.019(3) 0.037(4) 0.015(3) 0.000(3) -0.002(3) -0.001(3) C19 0.019(3) 0.033(4) 0.017(3) -0.001(3) 0.002(3) 0.000(3) C20 0.020(3) 0.037(4) 0.028(4) -0.001(3) 0.007(3) 0.002(3) C21 0.031(4) 0.037(4) 0.027(4) -0.009(3) 0.008(3) 0.002(3) C22 0.026(4) 0.042(4) 0.017(3) -0.005(3) 0.003(3) -0.002(3) C23 0.019(3) 0.033(4) 0.014(3) 0.000(3) 0.003(2) -0.002(3) C24 0.018(3) 0.026(3) 0.016(3) 0.001(3) 0.000(2) -0.001(3) C25 0.042(5) 0.055(5) 0.028(4) -0.008(4) 0.005(3) 0.022(4) C26 0.026(4) 0.039(4) 0.022(3) 0.008(3) 0.003(3) 0.008(3) C27 0.030(4) 0.035(4) 0.025(4) 0.007(3) 0.007(3) 0.010(3) C28 0.024(4) 0.031(4) 0.023(3) 0.002(3) 0.001(3) 0.003(3) C29 0.042(5) 0.062(6) 0.025(4) -0.008(4) -0.002(3) 0.019(4) C30 0.029(4) 0.052(5) 0.022(4) 0.006(3) -0.001(3) 0.014(3) C31 0.022(3) 0.033(4) 0.027(4) 0.005(3) 0.005(3) 0.005(3) C32 0.020(3) 0.030(4) 0.023(3) 0.006(3) 0.003(3) 0.001(3) C33 0.030(4) 0.041(4) 0.022(4) 0.003(3) 0.000(3) 0.000(3) C34 0.026(4) 0.032(4) 0.020(3) 0.001(3) 0.004(3) 0.000(3) C35 0.027(4) 0.036(4) 0.024(3) -0.001(3) 0.004(3) -0.005(3) C36 0.033(4) 0.038(4) 0.019(3) 0.005(3) 0.002(3) -0.003(3) C37 0.031(4) 0.031(4) 0.020(3) 0.002(3) 0.005(3) 0.002(3) C38 0.036(4) 0.039(4) 0.029(4) 0.006(3) 0.004(3) -0.010(3) C39 0.039(5) 0.049(5) 0.028(4) -0.002(3) -0.001(3) -0.016(4) C40 0.039(4) 0.039(4) 0.017(3) 0.005(3) 0.003(3) -0.006(3) Cl1 0.090(2) 0.142(3) 0.089(2) 0.016(2) 0.0121(19) -0.016(2) Eu1 0.0244(2) 0.0337(2) 0.01680(18) -0.00151(14) 0.00371(13) -0.00419(14) Eu2 0.01726(18) 0.0278(2) 0.01552(18) 0.00132(13) -0.00066(12) -0.00011(13) N1 0.019(3) 0.033(3) 0.020(3) -0.004(2) -0.002(2) -0.001(2) N2 0.022(3) 0.044(4) 0.028(3) -0.003(3) -0.007(3) 0.003(3) N3 0.048(4) 0.049(5) 0.049(4) -0.001(4) 0.023(4) 0.008(4) N4 0.106(10) 0.074(8) 0.079(7) 0.006(6) 0.008(7) 0.037(7) O1 0.030(2) 0.060(3) 0.027(2) -0.007(2) 0.005(2) 0.009(2) O2 0.022(2) 0.060(3) 0.033(2) -0.003(2) -0.001(2) 0.002(2) O3 0.021(2) 0.035(3) 0.018(2) -0.0026(19) 0.0040(18) 0.0040(19) O4 0.022(2) 0.046(3) 0.019(2) 0.002(2) 0.0017(19) 0.005(2) O5 0.033(2) 0.057(3) 0.025(2) 0.003(2) 0.0009(19) 0.014(2) O6 0.033(2) 0.046(2) 0.022(2) 0.0011(19) 0.0006(18) 0.010(2) O7 0.027(2) 0.041(2) 0.026(2) -0.002(2) -0.0008(19) 0.003(2) O8 0.023(2) 0.039(3) 0.029(2) -0.004(2) -0.0006(19) 0.008(2) O9 0.050(3) 0.066(3) 0.028(2) 0.008(2) 0.007(2) -0.016(2) O10 0.052(3) 0.050(3) 0.033(2) 0.005(2) 0.005(2) -0.012(2) O11 0.047(3) 0.056(3) 0.025(2) 0.010(2) 0.001(2) -0.014(2) O12 0.054(3) 0.052(3) 0.024(2) 0.011(2) 0.000(2) -0.018(3) O14 0.113(7) 0.120(7) 0.134(8) -0.002(6) -0.001(6) -0.009(6) O15 0.109(7) 0.104(7) 0.119(7) 0.008(6) 0.021(6) -0.015(6) O16 0.047(4) 0.052(4) 0.045(3) 0.004(3) 0.017(3) -0.005(3) O17 0.039(3) 0.039(3) 0.039(3) -0.002(2) 0.015(2) 0.004(2) O18 0.144(9) 0.080(6) 0.187(11) -0.023(7) 0.138(9) 0.005(6) O20 0.078(5) 0.060(4) 0.056(4) 0.012(4) -0.008(4) 0.002(4) O21 0.102(7) 0.102(7) 0.056(5) -0.015(5) -0.019(4) -0.016(5) O22 0.097(6) 0.046(4) 0.094(6) 0.003(4) 0.035(5) 0.011(4) O19 0.195(13) 0.093(8) 0.149(11) 0.027(7) 0.075(10) 0.050(8) O23 0.140(11) 0.38(2) 0.069(7) 0.075(11) -0.015(7) -0.119(14) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Eu Eu -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 C1 C2 118.2(6) . . ? O2 C1 C2 117.2(6) . . ? O2 C1 O1 124.6(7) . . ? C3 C2 C1 120.1(6) . . ? C5 C2 C1 120.2(7) . . ? C5 C2 C3 119.5(7) . . ? C2 C3 H3 119.8 . . ? C4 C3 C2 120.4(7) . . ? C4 C3 H3 119.8 . . ? C3 C4 H4 119.6 . . ? C3 C4 C7 120.8(8) . . ? C7 C4 H4 119.6 . . ? C2 C5 H5 120.4 . . ? C6 C5 C2 119.2(7) . . ? C6 C5 H5 120.4 . . ? C5 C6 C7 122.0(7) . . ? C5 C6 N2 119.9(7) . . ? C7 C6 N2 118.1(7) . . ? C4 C7 C6 118.0(8) . . ? C4 C7 H7 121.0 . . ? C6 C7 H7 121.0 . . ? C11 C8 H8 120.0 . . ? N2 C8 H8 120.0 . . ? N2 C8 C11 120.0(8) . . ? C10 C9 H9 119.3 . . ? N2 C9 H9 119.3 . . ? N2 C9 C10 121.3(8) . . ? C9 C10 H10 120.3 . . ? C9 C10 C12 119.4(8) . . ? C12 C10 H10 120.3 . . ? C8 C11 H11 119.4 . . ? C8 C11 C12 121.1(8) . . ? C12 C11 H11 119.4 . . ? C10 C12 C13 122.0(7) . . ? C11 C12 C10 117.5(7) . . ? C11 C12 C13 120.5(7) . . ? C14 C13 C12 121.4(6) . . ? C14 C13 C15 117.3(6) . . ? C15 C13 C12 121.3(6) . . ? C13 C14 H14 119.7 . . ? C17 C14 C13 120.6(7) . . ? C17 C14 H14 119.7 . . ? C13 C15 H15 119.7 . . ? C16 C15 C13 120.6(7) . . ? C16 C15 H15 119.7 . . ? C15 C16 H16 119.8 . . ? N1 C16 C15 120.5(7) . . ? N1 C16 H16 119.8 . . ? C14 C17 H17 120.1 . . ? N1 C17 C14 119.7(7) . . ? N1 C17 H17 120.1 . . ? C19 C18 C20 123.4(6) . . ? C19 C18 N1 118.1(6) . . ? C20 C18 N1 118.5(6) . . ? C18 C19 H19 121.0 . . ? C18 C19 C23 118.1(6) . . ? C23 C19 H19 121.0 . . ? C18 C20 H20 121.4 . . ? C18 C20 C21 117.2(6) . . ? C21 C20 H20 121.4 . . ? C20 C21 H21 119.4 . . ? C22 C21 C20 121.3(7) . . ? C22 C21 H21 119.4 . . ? C21 C22 H22 119.4 . . ? C21 C22 C23 121.1(6) . . ? C23 C22 H22 119.4 . . ? C19 C23 C22 119.0(6) . . ? C19 C23 C24 119.8(6) . . ? C22 C23 C24 121.1(6) . . ? C23 C24 Eu1 166.6(4) . 8_556 ? O3 C24 C23 120.6(5) . . ? O3 C24 Eu1 66.0(3) . 8_556 ? O4 C24 C23 119.1(6) . . ? O4 C24 Eu1 55.3(3) . 8_556 ? O4 C24 O3 120.3(6) . . ? C26 C25 H25 120.1 . . ? C26 C25 C29 119.9(7) . . ? C29 C25 H25 120.1 . . ? C25 C26 C27 120.8(7) . . ? C25 C26 C28 120.1(7) . . ? C28 C26 C27 119.0(6) . . ? C26 C27 Eu2 170.0(5) . . ? O5 C27 C26 119.5(6) . . ? O5 C27 Eu2 60.7(4) . . ? O5 C27 O6 121.6(6) . . ? O6 C27 C26 118.8(6) . . ? O6 C27 Eu2 61.4(4) . . ? C26 C28 H28 120.2 . . ? C31 C28 C26 119.7(7) . . ? C31 C28 H28 120.2 . . ? C25 C29 H29 119.8 . . ? C30 C29 C25 120.3(7) . . ? C30 C29 H29 119.8 . . ? C29 C30 H30 120.0 . . ? C29 C30 C31 120.1(7) . . ? C31 C30 H30 120.0 . . ? C28 C31 C30 119.9(7) . . ? C28 C31 C32 119.4(6) . . ? C30 C31 C32 120.6(6) . . ? C31 C32 Eu2 179.3(5) . 4 ? O7 C32 C31 120.0(6) . . ? O7 C32 Eu2 60.7(4) . 4 ? O7 C32 O8 120.0(6) . . ? O8 C32 C31 120.0(6) . . ? O8 C32 Eu2 59.3(3) . 4 ? O9 C33 C34 117.6(7) . . ? O10 C33 C34 118.6(6) . . ? O10 C33 O9 123.8(7) . . ? C35 C34 C33 120.2(6) . . ? C40 C34 C33 120.9(6) . . ? C40 C34 C35 118.8(6) . . ? C34 C35 H35 119.5 . . ? C37 C35 C34 120.9(7) . . ? C37 C35 H35 119.5 . . ? C37 C36 Eu1 169.0(5) . 6_565 ? O11 C36 C37 120.2(6) . . ? O11 C36 Eu1 61.5(4) . 6_565 ? O11 C36 O12 120.0(6) . . ? O12 C36 C37 119.7(7) . . ? O12 C36 Eu1 59.6(4) . 6_565 ? C35 C37 C36 119.6(7) . . ? C35 C37 C38 119.3(6) . . ? C38 C37 C36 121.0(7) . . ? C37 C38 H38 120.0 . . ? C39 C38 C37 120.0(7) . . ? C39 C38 H38 120.0 . . ? C38 C39 H39 119.8 . . ? C40 C39 C38 120.4(7) . . ? C40 C39 H39 119.8 . . ? C34 C40 H40 119.8 . . ? C39 C40 C34 120.5(7) . . ? C39 C40 H40 119.8 . . ? C36 Eu1 C24 106.9(2) 6_566 8_455 ? Cl1 Eu1 C24 77.62(16) . 8_455 ? Cl1 Eu1 C36 99.48(18) . 6_566 ? Cl1 Eu1 N4 99.1(3) . . ? Cl1 Eu1 O3 76.25(14) . 8_455 ? N4 Eu1 C24 173.9(3) . 8_455 ? N4 Eu1 C36 78.6(3) . 6_566 ? O1 Eu1 C24 84.87(19) . 8_455 ? O1 Eu1 C36 104.3(2) . 6_566 ? O1 Eu1 Cl1 153.75(16) . . ? O1 Eu1 N4 96.4(3) . . ? O1 Eu1 O3 79.47(17) . 8_455 ? O1 Eu1 O4 86.32(19) . 8_455 ? O1 Eu1 O11 129.61(19) . 6_566 ? O1 Eu1 O12 77.65(18) . 6_566 ? O1 Eu1 O14 72.2(3) . . ? O1 Eu1 O15 118.1(4) . . ? O3 Eu1 C24 25.79(16) 8_455 8_455 ? O3 Eu1 C36 132.67(18) 8_455 6_566 ? O3 Eu1 N4 148.6(3) 8_455 . ? O4 Eu1 C24 25.15(16) 8_455 8_455 ? O4 Eu1 C36 82.17(19) 8_455 6_566 ? O4 Eu1 Cl1 85.99(15) 8_455 . ? O4 Eu1 N4 160.7(3) 8_455 . ? O4 Eu1 O3 50.68(14) 8_455 8_455 ? O4 Eu1 O11 79.14(19) 8_455 6_566 ? O4 Eu1 O12 81.79(19) 8_455 6_566 ? O4 Eu1 O14 148.4(3) 8_455 . ? O4 Eu1 O15 149.6(3) 8_455 . ? O9 Eu1 C24 104.20(19) . 8_455 ? O9 Eu1 C36 148.6(2) . 6_566 ? O9 Eu1 Cl1 82.93(19) . . ? O9 Eu1 N4 70.1(3) . . ? O9 Eu1 O1 82.6(2) . . ? O9 Eu1 O3 78.49(17) . 8_455 ? O9 Eu1 O4 129.14(18) . 8_455 ? O9 Eu1 O11 141.8(2) . 6_566 ? O9 Eu1 O12 142.0(2) . 6_566 ? O9 Eu1 O14 71.9(3) . . ? O9 Eu1 O15 75.1(3) . . ? O11 Eu1 C24 99.30(19) 6_566 8_455 ? O11 Eu1 C36 26.4(2) 6_566 6_566 ? O11 Eu1 Cl1 73.16(16) 6_566 . ? O11 Eu1 N4 84.5(3) 6_566 . ? O11 Eu1 O3 122.17(17) 6_566 8_455 ? O11 Eu1 O14 96.6(3) 6_566 . ? O11 Eu1 O15 71.4(3) 6_566 . ? O12 Eu1 C24 105.9(2) 6_566 8_455 ? O12 Eu1 C36 26.7(2) 6_566 6_566 ? O12 Eu1 Cl1 125.83(15) 6_566 . ? O12 Eu1 N4 80.1(3) 6_566 . ? O12 Eu1 O3 128.06(18) 6_566 8_455 ? O12 Eu1 O11 52.74(18) 6_566 6_566 ? O12 Eu1 O14 71.3(3) 6_566 . ? O12 Eu1 O15 86.0(3) 6_566 . ? O14 Eu1 C24 157.0(3) . 8_455 ? O14 Eu1 C36 81.0(3) . 6_566 ? O14 Eu1 Cl1 123.1(3) . . ? O14 Eu1 N4 24.6(3) . . ? O14 Eu1 O3 141.1(3) . 8_455 ? O15 Eu1 C24 156.3(3) . 8_455 ? O15 Eu1 C36 74.7(3) . 6_566 ? O15 Eu1 Cl1 78.8(3) . . ? O15 Eu1 N4 21.6(3) . . ? O15 Eu1 O3 145.5(3) . 8_455 ? O15 Eu1 O14 46.0(4) . . ? C27 Eu2 C32 96.5(2) . 4_545 ? C27 Eu2 N3 99.8(2) . . ? C32 Eu2 N3 96.2(2) 4_545 . ? O2 Eu2 C27 163.1(2) . . ? O2 Eu2 C32 100.1(2) . 4_545 ? O2 Eu2 N3 75.1(2) . . ? O2 Eu2 O3 82.43(17) . 8_455 ? O2 Eu2 O5 144.21(18) . . ? O2 Eu2 O6 151.75(19) . . ? O2 Eu2 O7 125.14(19) . 4_545 ? O2 Eu2 O8 74.74(18) . 4_545 ? O2 Eu2 O16 72.70(19) . . ? O2 Eu2 O17 82.10(19) . . ? O3 Eu2 C27 102.95(18) 8_455 . ? O3 Eu2 C32 83.37(17) 8_455 4_545 ? O3 Eu2 N3 157.11(19) 8_455 . ? O3 Eu2 O7 93.75(16) 8_455 4_545 ? O3 Eu2 O16 147.44(17) 8_455 . ? O5 Eu2 C27 26.55(19) . . ? O5 Eu2 C32 99.62(19) . 4_545 ? O5 Eu2 N3 73.3(2) . . ? O5 Eu2 O3 129.45(16) . 8_455 ? O5 Eu2 O6 53.25(17) . . ? O5 Eu2 O7 74.65(18) . 4_545 ? O5 Eu2 O8 124.57(18) . 4_545 ? O5 Eu2 O16 71.56(18) . . ? O5 Eu2 O17 76.33(19) . . ? O6 Eu2 C27 26.85(19) . . ? O6 Eu2 C32 95.66(19) . 4_545 ? O6 Eu2 N3 126.44(19) . . ? O6 Eu2 O3 76.20(16) . 8_455 ? O6 Eu2 O7 75.10(18) . 4_545 ? O6 Eu2 O16 118.22(18) . . ? O6 Eu2 O17 125.42(18) . . ? O7 Eu2 C27 70.94(19) 4_545 . ? O7 Eu2 C32 25.98(17) 4_545 4_545 ? O7 Eu2 N3 95.6(2) 4_545 . ? O7 Eu2 O16 117.62(18) 4_545 . ? O8 Eu2 C27 122.06(19) 4_545 . ? O8 Eu2 C32 26.10(17) 4_545 4_545 ? O8 Eu2 N3 95.62(19) 4_545 . ? O8 Eu2 O3 74.01(16) 4_545 8_455 ? O8 Eu2 O6 115.76(17) 4_545 . ? O8 Eu2 O7 52.09(16) 4_545 4_545 ? O8 Eu2 O16 117.45(18) 4_545 . ? O8 Eu2 O17 74.23(18) 4_545 . ? O10 Eu2 C27 82.9(2) . . ? O10 Eu2 C32 163.0(2) . 4_545 ? O10 Eu2 N3 100.7(2) . . ? O10 Eu2 O2 82.3(2) . . ? O10 Eu2 O3 80.22(18) . 8_455 ? O10 Eu2 O5 87.5(2) . . ? O10 Eu2 O6 76.1(2) . . ? O10 Eu2 O7 151.2(2) . 4_545 ? O10 Eu2 O8 147.29(18) . 4_545 ? O10 Eu2 O16 76.0(2) . . ? O10 Eu2 O17 125.6(2) . . ? O16 Eu2 C27 95.9(2) . . ? O16 Eu2 C32 120.90(19) . 4_545 ? O16 Eu2 N3 24.70(19) . . ? O17 Eu2 C27 100.1(2) . . ? O17 Eu2 C32 71.29(18) . 4_545 ? O17 Eu2 N3 25.01(19) . . ? O17 Eu2 O3 147.34(17) . 8_455 ? O17 Eu2 O7 72.38(18) . 4_545 ? O17 Eu2 O16 49.66(19) . . ? C16 N1 C18 118.9(6) . . ? C17 N1 C16 121.2(6) . . ? C17 N1 C18 119.9(6) . . ? C8 N2 C6 119.5(7) . . ? C8 N2 C9 120.6(7) . . ? C9 N2 C6 119.9(7) . . ? O16 N3 Eu2 62.4(4) . . ? O16 N3 O17 117.9(7) . . ? O17 N3 Eu2 55.6(4) . . ? O18 N3 Eu2 171.4(8) . . ? O18 N3 O16 122.6(8) . . ? O18 N3 O17 119.4(8) . . ? O13 N4 Eu1 169.2(10) . . ? O14 N4 Eu1 70.1(10) . . ? O14 N4 O13 111.1(15) . . ? O15 N4 Eu1 63.0(11) . . ? O15 N4 O13 116.7(15) . . ? O15 N4 O14 132.2(19) . . ? C1 O1 Eu1 133.6(5) . . ? C1 O2 Eu2 144.5(5) . . ? C24 O3 Eu1 88.2(4) . 8_556 ? C24 O3 Eu2 135.2(4) . 8_556 ? Eu2 O3 Eu1 122.59(17) 8_556 8_556 ? C24 O4 Eu1 99.6(4) . 8_556 ? C27 O5 Eu2 92.8(4) . . ? C27 O6 Eu2 91.7(4) . . ? C32 O7 Eu2 93.3(4) . 4 ? C32 O8 Eu2 94.6(4) . 4 ? C33 O9 Eu1 149.6(5) . . ? C33 O10 Eu2 143.6(5) . . ? C36 O11 Eu1 92.2(4) . 6_565 ? C36 O12 Eu1 93.8(4) . 6_565 ? N4 O14 Eu1 85.3(11) . . ? N4 O15 Eu1 95.4(12) . . ? N3 O16 Eu2 92.9(4) . . ? N3 O17 Eu2 99.4(5) . . ? H20A O20 H20B 104.4 . . ? H22A O22 H22B 104.4 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 C2 1.499(10) . ? C1 O1 1.251(9) . ? C1 O2 1.248(8) . ? C2 C3 1.388(11) . ? C2 C5 1.387(10) . ? C3 H3 0.9300 . ? C3 C4 1.378(12) . ? C4 H4 0.9300 . ? C4 C7 1.381(12) . ? C5 H5 0.9300 . ? C5 C6 1.374(11) . ? C6 C7 1.394(12) . ? C6 N2 1.449(9) . ? C7 H7 0.9300 . ? C8 H8 0.9300 . ? C8 C11 1.381(11) . ? C8 N2 1.333(11) . ? C9 H9 0.9300 . ? C9 C10 1.380(11) . ? C9 N2 1.345(11) . ? C10 H10 0.9300 . ? C10 C12 1.392(11) . ? C11 H11 0.9300 . ? C11 C12 1.384(11) . ? C12 C13 1.485(9) . ? C13 C14 1.383(10) . ? C13 C15 1.391(10) . ? C14 H14 0.9300 . ? C14 C17 1.381(10) . ? C15 H15 0.9300 . ? C15 C16 1.359(10) . ? C16 H16 0.9300 . ? C16 N1 1.342(9) . ? C17 H17 0.9300 . ? C17 N1 1.337(9) . ? C18 C19 1.382(9) . ? C18 C20 1.382(10) . ? C18 N1 1.465(8) . ? C19 H19 0.9300 . ? C19 C23 1.395(9) . ? C20 H20 0.9300 . ? C20 C21 1.384(10) . ? C21 H21 0.9300 . ? C21 C22 1.359(10) . ? C22 H22 0.9300 . ? C22 C23 1.396(10) . ? C23 C24 1.493(9) . ? C24 Eu1 2.912(6) 8_556 ? C24 O3 1.268(8) . ? C24 O4 1.255(8) . ? C25 H25 0.9300 . ? C25 C26 1.382(11) . ? C25 C29 1.386(11) . ? C26 C27 1.504(10) . ? C26 C28 1.398(10) . ? C27 Eu2 2.810(7) . ? C27 O5 1.258(9) . ? C27 O6 1.270(9) . ? C28 H28 0.9300 . ? C28 C31 1.383(9) . ? C29 H29 0.9300 . ? C29 C30 1.379(11) . ? C30 H30 0.9300 . ? C30 C31 1.393(10) . ? C31 C32 1.490(10) . ? C32 Eu2 2.863(7) 4 ? C32 O7 1.256(8) . ? C32 O8 1.264(8) . ? C33 C34 1.485(10) . ? C33 O9 1.257(9) . ? C33 O10 1.249(9) . ? C34 C35 1.400(9) . ? C34 C40 1.390(10) . ? C35 H35 0.9300 . ? C35 C37 1.382(10) . ? C36 C37 1.482(9) . ? C36 Eu1 2.828(7) 6_565 ? C36 O11 1.257(9) . ? C36 O12 1.272(9) . ? C37 C38 1.392(10) . ? C38 H38 0.9300 . ? C38 C39 1.390(11) . ? C39 H39 0.9300 . ? C39 C40 1.374(11) . ? C40 H40 0.9300 . ? Cl1 Eu1 2.662(5) . ? Eu1 C24 2.912(6) 8_455 ? Eu1 C36 2.829(7) 6_566 ? Eu1 N4 2.786(15) . ? Eu1 O1 2.324(6) . ? Eu1 O3 2.663(5) 8_455 ? Eu1 O4 2.427(5) 8_455 ? Eu1 O9 2.317(5) . ? Eu1 O11 2.487(5) 6_566 ? Eu1 O12 2.444(5) 6_566 ? Eu1 O14 2.628(12) . ? Eu1 O15 2.492(12) . ? Eu2 C32 2.863(7) 4_545 ? Eu2 N3 2.961(7) . ? Eu2 O2 2.338(5) . ? Eu2 O3 2.478(5) 8_455 ? Eu2 O5 2.454(5) . ? Eu2 O6 2.470(5) . ? Eu2 O7 2.501(5) 4_545 ? Eu2 O8 2.469(5) 4_545 ? Eu2 O10 2.315(6) . ? Eu2 O16 2.629(6) . ? Eu2 O17 2.477(5) . ? N3 O16 1.239(10) . ? N3 O17 1.269(9) . ? N3 O18 1.219(10) . ? N4 O13 1.46(2) . ? N4 O14 1.163(15) . ? N4 O15 1.032(14) . ? O3 Eu1 2.663(4) 8_556 ? O3 Eu2 2.478(5) 8_556 ? O4 Eu1 2.427(5) 8_556 ? O7 Eu2 2.501(5) 4 ? O8 Eu2 2.469(5) 4 ? O11 Eu1 2.487(5) 6_565 ? O12 Eu1 2.444(5) 6_565 ? O20 H20A 0.8593 . ? O20 H20B 0.8600 . ? O22 H22A 0.8607 . ? O22 H22B 0.8605 . ?