#------------------------------------------------------------------------------ #$Date: 2024-09-25 04:19:45 +0300 (Wed, 25 Sep 2024) $ #$Revision: 294877 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/93/7249369.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7249369 loop_ _publ_author_name 'Dangar, Shilpa' 'Roy, Tiyasa' 'Noskar, Suman' 'Bisai, Alakesh' _publ_section_title ; Total synthesis of bicyclomahanimbine by Cu(ii)-promoted photoredox process. ; _journal_issue 41 _journal_name_full 'RSC advances' _journal_page_first 30110 _journal_page_last 30115 _journal_paper_doi 10.1039/d4ra05863a _journal_volume 14 _journal_year 2024 _chemical_formula_moiety '2(C23 H25 N O)' _chemical_formula_sum 'C46 H50 N2 O2' _chemical_formula_weight 662.88 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2024-05-14 _audit_creation_method ; Olex2 1.5 (compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817) ; _audit_update_record ; 2024-05-14 deposited with the CCDC. 2024-09-17 downloaded from the CCDC. ; _cell_angle_alpha 85.4510(10) _cell_angle_beta 82.6730(10) _cell_angle_gamma 69.423(2) _cell_formula_units_Z 2 _cell_length_a 9.8359(2) _cell_length_b 13.2198(3) _cell_length_c 15.2566(2) _cell_measurement_reflns_used 22830 _cell_measurement_temperature 100.00(13) _cell_measurement_theta_max 67.9200 _cell_measurement_theta_min 2.8890 _cell_volume 1840.79(7) _computing_cell_refinement 'CrysAlisPro 1.171.42.73a (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.42.73a (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.73a (Rigaku OD, 2022)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.00(13) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix3000 _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -52.00 26.00 0.50 0.70 -- -40.58 46.00 3.00 156 2 \w -107.00 -23.00 0.50 0.70 -- -40.58 -46.00-145.00 168 3 \w -26.00 52.00 0.50 0.70 -- 40.58 -46.00-145.00 156 4 \w -149.00 -64.00 0.50 2.78 -- -82.50 -46.00-145.00 170 5 \w -52.00 -16.00 0.50 2.78 -- -82.50 46.00 3.00 72 6 \w 79.00 163.00 0.50 2.78 -- 96.35 46.00 3.00 168 7 \w -43.00 26.00 0.50 0.70 -- -40.58 38.00-180.00 138 8 \w -24.00 35.00 0.50 0.70 -- -40.58 12.00 120.00 118 9 \w 23.00 107.00 0.50 0.70 -- 40.58 46.00 3.00 168 10 \w -35.00 24.00 0.50 0.70 -- 40.58 -12.00 60.00 118 11 \w 18.00 78.00 0.50 0.70 -- 40.58-104.00 -30.00 120 12 \w -35.00 24.00 0.50 0.70 -- 40.58 -12.00 90.00 118 13 \w 41.00 100.00 0.50 0.70 -- 40.58-138.00 0.00 118 14 \w 9.00 42.00 0.50 0.70 -- 40.58 91.00 22.99 66 15 \w -29.00 31.00 0.50 0.70 -- 40.58 -25.00 -30.00 120 16 \w 41.00 100.00 0.50 0.70 -- 40.58-138.00 -30.00 118 17 \w 13.00 43.00 0.50 0.70 -- 40.58 81.00-138.17 60 18 \w -35.00 24.00 0.50 0.70 -- 40.58 -12.00 30.00 118 19 \w 12.00 43.00 0.50 0.70 -- 40.58 83.00 176.46 62 20 \w 18.00 78.00 0.50 0.70 -- 40.58-104.00 120.00 120 21 \w -47.00 -15.00 0.50 2.78 -- -82.50 42.00 -90.00 64 22 \w -47.00 -15.00 0.50 2.78 -- -82.50 42.00-150.00 64 23 \w -47.00 -15.00 0.50 2.78 -- -82.50 42.00 30.00 64 24 \w -47.00 -15.00 0.50 2.78 -- -82.50 42.00 120.00 64 25 \w -47.00 -15.00 0.50 2.78 -- -82.50 42.00-120.00 64 26 \w -47.00 -15.00 0.50 2.78 -- -82.50 42.00-180.00 64 27 \w -57.00 -16.00 0.50 2.78 -- -82.50 50.00 90.00 82 28 \w -47.00 -15.00 0.50 2.78 -- -82.50 42.00 -30.00 64 29 \w -101.00 -23.00 0.50 2.78 -- -82.50 145.00 30.00 156 30 \w 23.00 106.00 0.50 2.78 -- 96.35 -96.00 -30.00 166 31 \w 29.00 83.00 0.50 2.78 -- 96.35 -68.00-120.00 108 32 \w 30.00 57.00 0.50 2.78 -- 96.35 -50.00 0.00 54 33 \w 83.00 164.00 0.50 2.78 -- 96.35 33.00 60.00 162 34 \w 28.00 105.00 0.50 2.78 -- 96.35 -77.00 -60.00 154 35 \w 28.00 68.00 0.50 2.78 -- 96.35 -59.00 60.00 80 36 \w 30.00 57.00 0.50 2.78 -- 96.35 -50.00 120.00 54 37 \w 28.00 68.00 0.50 2.78 -- 96.35 -59.00-150.00 80 38 \w 33.00 110.00 0.50 2.78 -- 96.35-117.00 0.00 154 39 \w 23.00 106.00 0.50 2.78 -- 96.35 -96.00-120.00 166 40 \w 29.00 83.00 0.50 2.78 -- 96.35 -68.00 120.00 108 41 \w 99.00 160.00 0.50 2.78 -- 96.35 117.00-120.00 122 42 \w 33.00 110.00 0.50 2.78 -- 96.35-117.00-120.00 154 43 \w 33.00 110.00 0.50 2.78 -- 96.35-117.00 90.00 154 44 \w 83.00 164.00 0.50 2.78 -- 96.35 33.00 90.00 162 45 \w 28.00 105.00 0.50 2.78 -- 96.35 -77.00 0.00 154 46 \w 44.00 127.00 0.50 2.78 -- 96.35-145.00-120.00 166 47 \w 30.00 57.00 0.50 2.78 -- 96.35 -50.00-150.00 54 48 \w 28.00 68.00 0.50 2.78 -- 96.35 -59.00-120.00 80 49 \w 75.00 165.00 0.50 2.78 -- 96.35 59.00 150.00 180 50 \w 28.00 68.00 0.50 2.78 -- 96.35 -59.00 30.00 80 51 \w 80.00 164.00 0.50 2.78 -- 96.35 42.00 -60.00 168 52 \w 81.00 167.00 0.50 2.78 -- 96.35 25.00-150.00 172 53 \w 33.00 110.00 0.50 2.78 -- 96.35-117.00 -30.00 154 54 \w 72.00 165.00 0.50 2.78 -- 96.35 69.00 -37.67 186 55 \w 30.00 57.00 0.50 2.78 -- 96.35 -50.00 -30.00 54 56 \w 81.00 167.00 0.50 2.78 -- 96.35 25.00 -90.00 172 57 \w 77.00 163.00 0.50 2.78 -- 96.35 50.00 120.00 172 58 \w 26.00 127.00 0.50 2.78 -- 96.35 -87.00 90.00 202 59 \w 29.00 83.00 0.50 2.78 -- 96.35 -68.00 -30.00 108 60 \w -108.00 -17.00 0.50 0.70 -- -40.58 -64.00 90.00 182 61 \w -107.00 -21.00 0.50 0.70 -- -40.58 -50.00 150.00 172 62 \w -108.00 -17.00 0.50 0.70 -- -40.58 -64.00-150.00 182 63 \w -109.00 -14.00 0.50 0.70 -- -40.58 -77.00 120.00 190 64 \w -107.00 -21.00 0.50 0.70 -- -40.58 -50.00 30.00 172 65 \w -78.00 4.00 0.50 0.70 -- -40.58 104.00-150.00 164 66 \w -107.00 -21.00 0.50 0.70 -- -40.58 -50.00 120.00 172 67 \w 18.00 108.00 0.50 0.70 -- 40.58 64.00 -60.00 180 68 \w 14.00 109.00 0.50 0.70 -- 40.58 77.00-120.00 190 69 \w 22.00 107.00 0.50 0.70 -- 40.58 50.00 90.00 170 70 \w 14.00 109.00 0.50 0.70 -- 40.58 77.00 0.00 190 71 \w 14.00 109.00 0.50 0.70 -- 40.58 77.00 -30.00 190 72 \w 14.00 109.00 0.50 0.70 -- 40.58 77.00 30.00 190 73 \w 18.00 108.00 0.50 0.70 -- 40.58 64.00-180.00 180 74 \w 7.00 35.00 0.50 0.70 -- 40.58 94.00-106.13 56 75 \w 9.00 43.00 0.50 0.70 -- 40.58 90.00 49.37 68 76 \w 8.00 42.00 0.50 0.70 -- 40.58 92.00 96.68 68 77 \w -151.00 -63.00 0.50 2.78 -- -82.50 -77.00 90.00 176 78 \w -151.00 -55.00 0.50 2.78 -- -82.50 -77.00 -79.74 192 79 \w -151.00 -55.00 0.50 2.78 -- -82.50 -77.00-150.00 192 80 \w -151.00 -55.00 0.50 2.78 -- -82.50 -77.00 30.00 192 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, HyPix3000' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0124885000 _diffrn_orient_matrix_UB_12 0.1158749000 _diffrn_orient_matrix_UB_13 0.0188822000 _diffrn_orient_matrix_UB_21 0.1485949000 _diffrn_orient_matrix_UB_22 -0.0166290000 _diffrn_orient_matrix_UB_23 -0.0547130000 _diffrn_orient_matrix_UB_31 -0.0779480000 _diffrn_orient_matrix_UB_32 0.0425694000 _diffrn_orient_matrix_UB_33 -0.0838403000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0463 _diffrn_reflns_av_unetI/netI 0.0290 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 35510 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 68.205 _diffrn_reflns_theta_min 2.922 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.557 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.56525 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.73a (Rigaku Oxford Diffraction, 2022) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear whiteish colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier whiteish _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.196 _exptl_crystal_description needle _exptl_crystal_F_000 712 _refine_diff_density_max 0.258 _refine_diff_density_min -0.191 _refine_diff_density_rms 0.038 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.057 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 459 _refine_ls_number_reflns 6683 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.057 _refine_ls_R_factor_all 0.0480 _refine_ls_R_factor_gt 0.0415 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0587P)^2^+0.4151P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1112 _refine_ls_wR_factor_ref 0.1164 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5712 _reflns_number_total 6683 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4ra05863a3.cif _cod_data_source_block ab_dgj_08scm_auto _cod_database_code 7249369 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C H N O' _chemical_oxdiff_usercomment RT _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C37(H37), C14(H14) 2.b Secondary CH2 refined with riding coordinates: C38(H38A,H38B), C15(H15A,H15B), C42(H42A,H42B), C41(H41A,H41B), C19(H19A, H19B), C18(H18A,H18B) 2.c Aromatic/amide H refined with riding coordinates: N003(H003), N004(H004), C4(H4), C5(H5), C8(H8), C6(H6), C7(H7), C27(H27), C31(H31), C28(H28), C29(H29), C30(H30) 2.d Idealised Me refined as rotating group: C13(H13A,H13B,H13C), C23(H23A,H23B,H23C), C45(H45A,H45B,H45C), C46(H46A,H46B, H46C), C17(H17A,H17B,H17C), C22(H22A,H22B,H22C), C36(H36A,H36B,H36C), C40(H40A, H40B,H40C) ; _shelx_res_file ; TITL ab_dgj_08scm_auto_a.res in P-1 ab_dgj_08scm_auto.res created by SHELXL-2018/3 at 16:42:16 on 14-May-2024 REM Old TITL ab_dgj_08scm_auto_a.res in P-1 REM SHELXT solution in P-1: R1 0.153, Rweak 0.004, Alpha 0.034 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C46 N2 O2 CELL 1.54184 9.8359 13.2198 15.2566 85.451 82.673 69.423 ZERR 2 0.0002 0.0003 0.0002 0.001 0.001 0.002 LATT 1 SFAC C H N O UNIT 92 100 4 4 L.S. 20 PLAN 5 TEMP -173 CONF BOND list 4 fmap 2 53 MORE -1 ACTA BOND $H REM REM REM WGHT 0.058700 0.415100 FVAR 0.51275 O001 4 0.817282 0.047071 0.149478 11.00000 0.02917 0.03594 = 0.03130 0.00035 0.00049 -0.00956 O002 4 0.292192 0.112915 0.212558 11.00000 0.03067 0.03199 = 0.04822 -0.00842 -0.00440 -0.01186 N003 3 0.538494 0.392458 0.288860 11.00000 0.02775 0.03814 = 0.02816 -0.00163 -0.00353 -0.01292 AFIX 43 H003 2 0.520687 0.374240 0.344736 11.00000 -1.20000 AFIX 0 N004 3 0.199430 0.437101 0.378115 11.00000 0.03099 0.04016 = 0.03113 -0.00832 0.00070 -0.01622 AFIX 43 H004 2 0.182244 0.489658 0.337318 11.00000 -1.20000 AFIX 0 C12 1 0.614420 0.320962 0.222883 11.00000 0.01955 0.03751 = 0.02993 -0.00248 -0.00478 -0.01260 C24 1 0.251309 0.280340 0.282336 11.00000 0.01905 0.03203 = 0.03244 -0.00228 -0.00325 -0.00957 C2 1 0.749502 0.157012 0.152212 11.00000 0.01989 0.03524 = 0.03209 -0.00076 -0.00416 -0.01110 C1 1 0.676228 0.208721 0.229480 11.00000 0.01986 0.03974 = 0.02823 -0.00028 -0.00470 -0.01340 C37 1 0.245189 0.343128 0.195003 11.00000 0.02335 0.03175 = 0.02933 -0.00352 -0.00355 -0.01185 AFIX 13 H37 2 0.289220 0.400270 0.197836 11.00000 -1.20000 AFIX 0 C35 1 0.233957 0.328521 0.363316 11.00000 0.02120 0.03864 = 0.03069 -0.00320 -0.00109 -0.01306 C11 1 0.619933 0.380377 0.142639 11.00000 0.02122 0.03801 = 0.03245 0.00218 -0.00733 -0.01445 C3 1 0.758579 0.213563 0.069917 11.00000 0.02141 0.04109 = 0.02924 -0.00063 -0.00438 -0.01413 C14 1 0.665172 0.143300 0.314411 11.00000 0.02339 0.03776 = 0.02867 0.00023 -0.00150 -0.01118 AFIX 13 H14 2 0.570586 0.180339 0.350476 11.00000 -1.20000 AFIX 0 C43 1 0.090211 0.395225 0.169488 11.00000 0.02277 0.03745 = 0.02485 -0.00399 -0.00076 -0.01219 C4 1 0.693359 0.324285 0.066353 11.00000 0.02364 0.04233 = 0.02841 0.00328 -0.00552 -0.01623 AFIX 43 H4 2 0.698055 0.363238 0.011652 11.00000 -1.20000 AFIX 0 C9 1 0.495280 0.496794 0.252919 11.00000 0.02436 0.03747 = 0.03743 -0.00123 -0.00831 -0.01354 C10 1 0.544159 0.493302 0.161725 11.00000 0.02211 0.03919 = 0.03685 -0.00017 -0.00762 -0.01437 C25 1 0.280277 0.169466 0.286511 11.00000 0.02068 0.03391 = 0.03937 -0.00391 -0.00137 -0.01092 C44 1 0.031546 0.499396 0.144428 11.00000 0.02378 0.04002 = 0.02567 -0.00088 0.00072 -0.00986 C38 1 0.335286 0.263150 0.124389 11.00000 0.02322 0.04216 = 0.03203 -0.00615 -0.00223 -0.01260 AFIX 23 H38A 2 0.329376 0.300127 0.065240 11.00000 -1.20000 H38B 2 0.439018 0.234114 0.136041 11.00000 -1.20000 AFIX 0 C15 1 0.668063 0.033372 0.287646 11.00000 0.02669 0.03775 = 0.03235 0.00276 -0.00111 -0.01212 AFIX 23 H15A 2 0.662142 -0.013066 0.341150 11.00000 -1.20000 H15B 2 0.582940 0.043184 0.255309 11.00000 -1.20000 AFIX 0 C42 1 0.018824 0.310506 0.169575 11.00000 0.02276 0.04069 = 0.03763 -0.00451 -0.00503 -0.01329 AFIX 23 H42A 2 -0.077863 0.344047 0.147186 11.00000 -1.20000 H42B 2 0.003306 0.283107 0.230957 11.00000 -1.20000 AFIX 0 C34 1 0.256193 0.269049 0.443838 11.00000 0.02340 0.05314 = 0.03226 0.00259 -0.00115 -0.01703 C5 1 0.516928 0.590117 0.111589 11.00000 0.02713 0.04135 = 0.04233 0.00605 -0.01129 -0.01503 AFIX 43 H5 2 0.549178 0.589578 0.050166 11.00000 -1.20000 AFIX 0 C16 1 0.808825 -0.020527 0.228961 11.00000 0.03000 0.03541 = 0.03382 0.00410 -0.00031 -0.00905 C26 1 0.302124 0.106030 0.366368 11.00000 0.02293 0.03827 = 0.05254 0.00755 -0.00238 -0.01277 C13 1 0.839795 0.150688 -0.010410 11.00000 0.03050 0.04420 = 0.03040 -0.00111 -0.00191 -0.01524 AFIX 137 H13A 2 0.942312 0.113379 -0.000495 11.00000 -1.50000 H13B 2 0.834209 0.200425 -0.062088 11.00000 -1.50000 H13C 2 0.795619 0.097419 -0.020825 11.00000 -1.50000 AFIX 0 C32 1 0.196386 0.449421 0.468150 11.00000 0.02760 0.06254 = 0.03441 -0.01556 0.00512 -0.02260 C20 1 0.791637 0.131283 0.367291 11.00000 0.02794 0.04232 = 0.03071 0.00510 -0.00442 -0.01455 C39 1 0.274951 0.171500 0.126981 11.00000 0.02774 0.04162 = 0.03997 -0.01321 -0.00154 -0.01323 C8 1 0.419243 0.594122 0.294340 11.00000 0.03487 0.04115 = 0.04218 -0.00681 -0.00835 -0.01326 AFIX 43 H8 2 0.386243 0.595516 0.355679 11.00000 -1.20000 AFIX 0 C21 1 0.778632 0.177529 0.444353 11.00000 0.03683 0.03579 = 0.03707 0.00469 -0.01020 -0.01636 C41 1 0.113006 0.215554 0.111795 11.00000 0.03072 0.04519 = 0.03954 -0.00984 -0.00535 -0.01825 AFIX 23 H41A 2 0.073050 0.156130 0.123380 11.00000 -1.20000 H41B 2 0.105060 0.239247 0.048870 11.00000 -1.20000 AFIX 0 C23 1 0.637051 0.249218 0.490181 11.00000 0.04614 0.03836 = 0.03273 -0.00017 -0.00885 -0.01759 AFIX 137 H23A 2 0.631136 0.228535 0.553293 11.00000 -1.50000 H23B 2 0.555304 0.241240 0.464322 11.00000 -1.50000 H23C 2 0.632324 0.324661 0.482834 11.00000 -1.50000 AFIX 0 C6 1 0.442268 0.686916 0.152640 11.00000 0.03506 0.03648 = 0.05639 0.00586 -0.01623 -0.01388 AFIX 43 H6 2 0.423837 0.753123 0.119052 11.00000 -1.20000 AFIX 0 C45 1 -0.116870 0.548046 0.111043 11.00000 0.02798 0.04678 = 0.03605 0.00418 -0.00296 -0.00869 AFIX 137 H45A 2 -0.171769 0.616020 0.140375 11.00000 -1.50000 H45B 2 -0.170231 0.497498 0.124087 11.00000 -1.50000 H45C 2 -0.104896 0.562181 0.047008 11.00000 -1.50000 AFIX 0 C19 1 0.937584 0.067923 0.318493 11.00000 0.02541 0.05316 = 0.03638 0.00433 -0.00623 -0.01209 AFIX 23 H19A 2 1.013561 0.049112 0.359708 11.00000 -1.20000 H19B 2 0.962955 0.114566 0.269923 11.00000 -1.20000 AFIX 0 C33 1 0.234557 0.347084 0.510903 11.00000 0.02830 0.07403 = 0.03033 -0.00633 0.00252 -0.02509 C18 1 0.939579 -0.035765 0.279849 11.00000 0.02708 0.04843 = 0.03741 0.00532 -0.00081 -0.00518 AFIX 23 H18A 2 0.941511 -0.090172 0.328603 11.00000 -1.20000 H18B 2 1.030499 -0.064721 0.239589 11.00000 -1.20000 AFIX 0 C46 1 0.105289 0.581694 0.145084 11.00000 0.03209 0.03754 = 0.05237 0.00623 -0.00526 -0.01247 AFIX 137 H46A 2 0.096588 0.623835 0.088959 11.00000 -1.50000 H46B 2 0.208768 0.544606 0.152735 11.00000 -1.50000 H46C 2 0.058496 0.630194 0.193986 11.00000 -1.50000 AFIX 0 C7 1 0.393716 0.688399 0.242854 11.00000 0.03622 0.03670 = 0.05669 -0.00699 -0.01270 -0.00966 AFIX 43 H7 2 0.341967 0.755788 0.269387 11.00000 -1.20000 AFIX 0 C27 1 0.291884 0.157256 0.443846 11.00000 0.02896 0.05259 = 0.03837 0.01327 -0.00308 -0.01722 AFIX 43 H27 2 0.309376 0.115764 0.497647 11.00000 -1.20000 AFIX 0 C17 1 0.813123 -0.125863 0.193924 11.00000 0.04304 0.03746 = 0.04516 -0.00113 0.00571 -0.01130 AFIX 137 H17A 2 0.725271 -0.113271 0.164590 11.00000 -1.50000 H17B 2 0.816949 -0.178840 0.243113 11.00000 -1.50000 H17C 2 0.899930 -0.153580 0.151416 11.00000 -1.50000 AFIX 0 C22 1 0.910382 0.164908 0.492392 11.00000 0.04503 0.04924 = 0.04634 -0.00155 -0.01660 -0.01633 AFIX 137 H22A 2 0.966889 0.206800 0.460204 11.00000 -1.50000 H22B 2 0.971886 0.088422 0.495549 11.00000 -1.50000 H22C 2 0.877226 0.191372 0.552365 11.00000 -1.50000 AFIX 0 C36 1 0.336821 -0.014088 0.365752 11.00000 0.03524 0.03971 = 0.07613 0.01257 -0.00385 -0.01534 AFIX 137 H36A 2 0.255012 -0.028903 0.345863 11.00000 -1.50000 H36B 2 0.352858 -0.045460 0.425568 11.00000 -1.50000 H36C 2 0.425218 -0.046228 0.325424 11.00000 -1.50000 AFIX 0 C40 1 0.363120 0.086241 0.061291 11.00000 0.03883 0.05575 = 0.05783 -0.02755 0.00215 -0.01532 AFIX 137 H40A 2 0.465636 0.058810 0.073188 11.00000 -1.50000 H40B 2 0.355871 0.118201 0.001118 11.00000 -1.50000 H40C 2 0.324861 0.026587 0.067095 11.00000 -1.50000 AFIX 0 C31 1 0.164554 0.544117 0.512955 11.00000 0.03927 0.07551 = 0.05096 -0.03018 0.01066 -0.02997 AFIX 43 H31 2 0.136297 0.612832 0.482835 11.00000 -1.20000 AFIX 0 C28 1 0.246398 0.339643 0.601960 11.00000 0.04317 0.10541 = 0.03292 -0.00419 0.00313 -0.03444 AFIX 43 H28 2 0.274067 0.271354 0.632761 11.00000 -1.20000 AFIX 0 C29 1 0.216921 0.433938 0.646187 11.00000 0.05286 0.13999 = 0.03368 -0.03118 0.01112 -0.05012 AFIX 43 H29 2 0.225262 0.429570 0.707838 11.00000 -1.20000 AFIX 0 C30 1 0.175533 0.534521 0.602550 11.00000 0.05137 0.11055 = 0.05118 -0.04199 0.01556 -0.04355 AFIX 43 H30 2 0.154461 0.597696 0.634952 11.00000 -1.20000 AFIX 0 HKLF 4 REM ab_dgj_08scm_auto_a.res in P-1 REM wR2 = 0.1164, GooF = S = 1.057, Restrained GooF = 1.057 for all data REM R1 = 0.0415 for 5712 Fo > 4sig(Fo) and 0.0480 for all 6683 data REM 459 parameters refined using 0 restraints END WGHT 0.0587 0.4150 REM Highest difference peak 0.258, deepest hole -0.191, 1-sigma level 0.038 Q1 1 0.0840 0.4396 0.1208 11.00000 0.05 0.26 Q2 1 0.5846 0.4403 0.1437 11.00000 0.05 0.25 Q3 1 0.1178 0.5000 0.3406 11.00000 0.05 0.24 Q4 1 0.0363 0.4593 0.1922 11.00000 0.05 0.23 Q5 1 0.4589 0.5400 0.2808 11.00000 0.05 0.22 ; _shelx_res_checksum 64107 _shelx_hkl_file ; 0 0 1 43.56 2.48 0 0 1 44.38 2.43 0 0 1 39.49 2.43 0 0 -1 44.26 2.49 0 0 1 38.19 2.49 0 0 1 48.05 2.47 0 0 -1 37.12 2.50 0 0 -1 38.20 2.43 0 0 -1 40.12 2.45 0 0 2 1517.72 80.38 0 0 2 1506.18 80.28 0 0 2 1378.40 80.26 0 0 2 1306.93 80.39 0 0 2 1502.20 80.33 0 0 -2 1424.51 80.38 0 0 -2 1376.88 80.28 0 0 -2 1469.29 80.49 0 0 -2 1389.99 80.31 0 0 3 1741.68 94.18 0 0 3 1815.45 94.03 0 0 3 1763.22 94.02 0 0 3 1438.78 93.80 0 0 3 1658.05 94.26 0 0 3 1765.86 94.25 0 0 3 1810.79 94.14 0 0 -3 1733.06 94.22 0 0 -3 1752.86 94.06 0 0 -3 1717.92 94.34 0 0 3 1736.39 94.08 0 0 -3 1736.34 94.09 0 0 4 405.66 22.95 0 0 4 388.97 22.72 0 0 4 371.06 23.16 0 0 4 413.87 22.74 0 0 4 387.19 23.07 0 0 -4 397.37 23.00 0 0 4 406.51 22.87 0 0 4 399.39 23.02 0 0 -4 407.27 23.17 0 0 -4 396.85 22.78 0 0 4 389.90 22.81 0 0 -4 400.17 22.73 0 0 -4 396.12 22.82 0 0 5 373.37 22.77 0 0 5 362.62 22.41 0 0 5 394.32 22.60 0 0 5 380.25 22.35 0 0 5 372.68 22.53 0 0 5 414.05 22.71 0 0 -5 402.48 22.80 0 0 -5 387.60 22.24 0 0 -5 407.32 22.70 0 0 -5 378.98 22.28 0 0 6 433.09 26.64 0 0 6 477.63 27.20 0 0 6 454.45 26.82 0 0 6 455.27 26.80 0 0 6 431.32 26.51 0 0 -6 504.77 27.16 0 0 -6 478.36 26.98 0 0 7 34.44 3.38 0 0 7 26.44 2.80 0 0 7 33.19 3.05 0 0 -7 32.94 3.21 0 0 -7 37.46 3.23 0 0 8 393.92 22.77 0 0 8 337.89 21.97 0 0 -8 377.11 20.93 0 0 8 350.96 22.12 0 0 -8 355.70 22.37 0 0 -8 346.24 22.17 0 0 9 164.02 11.02 0 0 -9 164.57 9.70 0 0 9 152.61 11.02 0 0 9 167.73 11.71 0 0 -9 157.71 11.15 0 0 -10 27.84 3.41 0 0 10 28.81 3.75 0 0 10 23.50 3.08 0 0 -10 27.32 2.14 0 0 -10 28.16 2.17 0 0 -10 28.65 2.22 0 0 10 27.00 3.38 0 0 -10 28.51 2.20 0 0 -10 30.64 2.24 0 0 -10 24.54 2.13 0 0 -10 25.80 2.23 0 0 -11 2.83 1.38 0 0 11 1.74 1.29 0 0 11 1.74 1.22 0 0 11 0.48 1.14 0 0 -11 2.10 0.73 0 0 -11 1.98 0.73 0 0 -11 2.43 0.70 0 0 -11 2.30 0.70 0 0 -11 2.69 0.79 0 0 -11 2.07 0.63 0 0 -12 62.60 6.96 0 0 -12 85.30 5.54 0 0 -12 87.52 5.50 0 0 12 80.24 8.02 0 0 -12 85.44 5.56 0 0 -12 82.66 5.50 0 0 -12 79.95 5.57 0 0 -12 85.09 5.53 0 0 -13 67.90 4.75 0 0 -13 65.12 4.68 0 0 -13 68.95 4.76 0 0 -13 67.00 4.65 0 0 -13 68.28 4.71 0 0 -14 169.68 10.72 0 0 -14 171.67 10.75 0 0 -14 174.55 10.68 0 0 -14 174.84 10.69 0 0 -14 176.44 10.66 0 0 -15 18.96 1.98 0 0 -15 18.87 1.94 0 0 -15 17.47 1.88 0 0 -15 21.14 1.94 0 0 -15 21.12 1.96 0 0 -16 3.31 0.87 0 0 -16 3.40 0.85 0 0 -16 3.43 0.80 0 0 -16 4.50 0.86 0 0 -17 1.82 0.69 0 0 -17 2.00 0.60 0 0 -18 17.13 1.49 0 1 -18 0.89 0.44 0 1 -17 1.78 0.68 0 1 -17 2.01 0.62 0 1 -16 -0.14 0.69 0 1 -16 -0.26 0.54 0 1 -16 0.36 0.60 0 1 -16 -0.39 0.53 0 1 -15 0.61 0.70 0 1 -15 -0.55 0.72 0 1 -15 -0.15 0.57 0 1 -15 0.29 0.71 0 1 -14 68.80 4.65 0 1 -14 63.92 4.52 0 1 -14 62.96 4.57 0 1 -14 62.35 4.54 0 1 -13 112.36 7.47 0 1 -13 113.75 7.45 0 1 -13 127.85 7.61 0 1 -13 115.21 7.44 0 1 -13 119.84 7.52 0 1 -13 113.19 7.39 0 1 -12 15.65 3.06 0 1 -12 23.67 2.02 0 1 -12 23.20 2.10 0 -1 12 20.26 3.67 0 1 -12 21.68 2.05 0 1 -12 22.97 2.02 0 1 -12 20.13 1.99 0 1 -12 22.22 2.08 0 1 -11 0.48 1.21 0 1 -11 0.81 0.55 0 1 -11 0.25 0.59 0 1 -11 0.34 0.52 0 -1 11 0.59 1.12 0 1 -11 0.25 0.57 0 1 -11 0.96 0.58 0 1 -11 -0.11 0.53 0 1 -11 0.48 0.58 0 1 -11 0.12 0.51 0 1 -11 1.06 0.60 0 1 -10 14.67 2.50 0 1 -10 13.61 1.42 0 1 -10 15.86 1.46 0 1 -10 19.58 1.62 0 -1 10 11.75 2.59 0 1 -10 17.93 1.58 0 1 -10 14.68 1.46 0 1 -10 18.45 1.59 0 1 -10 15.22 1.44 0 1 -10 16.49 1.53 0 1 -10 14.02 1.52 0 1 -9 137.27 9.89 0 -1 9 167.73 10.72 0 1 -9 127.78 8.28 0 1 -9 153.23 8.43 0 1 -9 161.03 8.44 0 -1 9 136.83 9.71 0 1 -9 120.94 8.21 0 1 -9 135.92 8.44 0 -1 8 268.05 18.49 0 1 -8 314.14 17.64 0 -1 8 308.25 18.83 0 -1 8 299.64 18.80 0 -1 8 319.00 19.48 0 1 -8 314.17 19.08 0 -1 7 20.64 2.22 0 1 -7 23.93 1.68 0 -1 7 18.48 2.22 0 -1 7 19.22 2.28 0 -1 7 22.67 2.69 0 1 -7 22.43 2.45 0 -1 6 150.76 9.87 0 -1 6 151.55 9.82 0 -1 6 159.63 10.10 0 -1 6 152.03 9.73 0 1 -6 157.03 10.07 0 -1 6 152.80 9.76 0 1 -6 170.70 10.12 0 -1 5 78.39 5.15 0 -1 5 78.46 5.35 0 -1 5 78.69 5.24 0 -1 5 82.70 5.23 0 -1 5 73.13 5.36 0 1 -5 74.51 5.41 0 -1 5 77.65 5.24 0 1 -5 79.76 5.41 0 -1 4 269.57 15.05 0 -1 4 247.13 14.83 0 -1 4 256.44 14.89 0 -1 4 262.63 14.68 0 -1 4 247.32 15.02 0 -1 4 245.96 14.61 0 -1 4 273.36 14.89 0 1 -4 263.66 15.10 0 1 -4 219.94 14.67 0 -1 4 252.71 14.93 0 1 -4 251.79 14.70 0 1 -4 269.10 15.07 0 1 -4 258.33 15.05 0 -1 3 2397.29 134.39 0 -1 3 2465.76 134.36 0 -1 3 2460.14 134.13 0 -1 3 2571.84 134.34 0 -1 3 2581.85 134.27 0 1 -3 2497.79 134.05 0 -1 3 2440.09 134.07 0 1 -3 2034.33 134.21 0 1 -3 2564.91 134.49 0 1 -3 2417.71 134.25 0 -1 3 2365.65 134.43 0 1 -3 2407.82 134.49 0 -1 2 7.80 0.82 0 -1 2 6.53 0.66 0 -1 2 7.88 0.67 0 -1 2 6.59 0.64 0 1 -2 6.56 0.70 0 -1 2 6.90 0.53 0 -1 2 7.82 0.72 0 1 -2 5.07 0.62 0 -1 2 6.74 0.64 0 1 -2 5.41 0.71 0 1 -2 6.69 0.79 0 1 -2 6.05 0.77 0 1 -2 7.96 0.79 0 1 -2 6.16 0.79 0 -1 1 3758.65 205.59 0 -1 1 3543.14 205.73 0 -1 1 3937.13 205.65 0 -1 1 3920.24 205.70 0 -1 1 3861.16 205.53 0 -1 1 3533.74 205.52 0 1 -1 3621.66 205.66 0 -1 1 3474.05 205.65 0 1 -1 3617.13 205.70 0 1 -1 3574.07 205.66 0 1 -1 3553.77 205.70 0 1 -1 3520.26 205.63 0 1 0 226.65 11.86 0 1 0 229.55 11.91 0 -1 0 195.79 11.91 0 -1 0 229.00 11.89 0 1 0 181.17 11.79 0 1 0 205.53 11.93 0 -1 0 212.70 11.88 0 1 1 3704.21 209.35 0 1 1 3724.69 209.25 0 1 1 3824.87 209.31 0 1 1 3887.04 209.31 0 -1 -1 3724.97 209.17 0 -1 -1 3801.74 209.30 0 -1 -1 3699.26 209.22 0 -1 -1 3494.13 209.27 0 1 1 3756.49 209.35 0 1 2 220.34 12.32 0 1 2 216.37 12.18 0 -1 -2 191.54 11.94 0 -1 -2 224.36 12.25 0 1 2 218.31 12.20 0 -1 -2 199.98 12.13 0 1 2 197.12 12.14 0 -1 -2 208.17 12.08 0 1 2 196.88 12.00 0 1 2 218.82 12.21 0 -1 -2 226.72 12.04 0 -1 -2 220.37 12.18 0 -1 -2 222.09 12.30 0 -1 -2 220.45 12.16 0 -1 -3 132.67 8.66 0 1 3 135.33 8.60 0 1 3 134.33 8.91 0 1 3 151.87 8.77 0 1 3 158.38 8.88 0 1 3 141.18 8.80 0 1 3 136.03 8.49 0 1 3 160.53 8.84 0 -1 -3 147.63 8.73 0 -1 -3 155.74 8.98 0 -1 -3 157.71 8.77 0 1 3 153.66 8.47 0 -1 -3 151.21 8.51 0 1 3 145.76 8.43 0 -1 -3 145.29 8.72 0 -1 -3 162.99 8.85 0 1 4 634.20 36.68 0 1 4 603.53 36.24 0 1 4 637.00 36.33 0 -1 -4 634.79 36.39 0 1 4 641.64 36.43 0 1 4 656.21 36.49 0 1 4 613.35 36.50 0 -1 -4 641.88 36.33 0 -1 -4 645.55 36.64 0 -1 -4 662.12 36.51 0 -1 -4 648.48 36.31 0 1 5 -0.19 0.70 0 1 5 -0.23 0.50 0 1 5 1.18 0.67 0 1 5 0.46 0.71 0 -1 -5 0.36 0.59 0 -1 -5 -0.23 0.53 0 -1 -5 0.30 0.56 0 -1 -5 0.43 0.50 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1.33 0.75 0 -1 -12 0.93 0.74 0 -1 -12 1.04 1.24 0 -1 -13 177.03 10.73 0 -1 -13 164.34 10.65 0 -1 -13 181.34 10.80 0 -1 -13 167.60 10.65 0 -1 -13 180.85 10.70 0 -1 -14 4.67 1.06 0 -1 -14 3.93 1.02 0 -1 -14 5.21 1.14 0 -1 -14 5.39 1.05 0 -1 -14 4.44 0.98 0 -1 -15 -0.61 0.80 0 -1 -15 -0.29 0.70 0 -1 -15 -0.14 0.69 0 -1 -15 -0.14 0.66 0 -1 -16 11.99 1.43 0 -1 -16 11.04 1.37 0 -1 -16 11.68 1.35 0 -1 -17 7.66 0.98 0 -1 -17 8.30 0.99 0 -1 -18 0.65 0.46 0 2 -17 1.88 0.68 0 2 -17 1.52 0.54 0 2 -16 38.85 2.96 0 2 -16 38.34 2.91 0 2 -16 37.60 2.90 0 2 -15 0.15 0.64 0 2 -15 1.70 0.70 0 2 -15 -0.14 0.56 0 2 -15 0.14 0.64 0 2 -14 0.93 0.71 0 2 -14 0.14 0.60 0 2 -14 -0.28 0.60 0 2 -14 1.70 0.80 0 2 -14 -0.28 0.60 0 2 -14 -0.31 0.64 0 2 -13 0.61 0.73 0 2 -13 -0.15 0.66 0 2 -13 0.28 0.65 0 2 -13 1.27 0.62 0 2 -13 0.56 0.62 0 2 -13 0.76 0.75 0 2 -12 27.82 3.96 0 2 -12 29.14 2.56 0 2 -12 29.39 2.54 0 -2 12 33.59 4.74 0 2 -12 33.82 2.65 0 2 -12 32.51 2.56 0 2 -12 33.56 2.69 0 2 -12 29.58 2.53 0 2 -12 31.57 2.56 0 2 -12 32.17 2.59 0 2 -11 0.49 1.01 0 2 -11 0.77 0.66 0 2 -11 0.60 0.59 0 2 -11 0.60 0.51 0 -2 11 1.24 1.28 0 2 -11 -0.50 0.57 0 2 -11 0.12 0.50 0 2 -11 0.24 0.49 0 2 -11 0.54 0.58 0 2 -11 0.24 0.58 0 2 -10 33.93 3.93 0 2 -10 36.47 2.62 0 2 -10 28.86 2.45 0 -2 10 39.68 4.53 0 2 -10 31.19 2.52 0 2 -10 35.54 2.58 0 2 -10 28.62 2.39 0 2 -10 36.70 2.58 0 2 -10 35.69 2.56 0 2 -10 32.08 2.49 0 2 -10 32.14 2.50 0 2 -10 37.00 2.64 0 2 -9 9.23 1.94 0 -2 9 8.18 1.99 0 -2 9 10.74 1.98 0 2 -9 11.25 1.18 0 2 -9 8.72 1.03 0 2 -9 7.60 1.02 0 2 -9 10.86 1.11 0 2 -9 8.73 1.00 0 2 -9 9.91 1.07 0 2 -9 9.60 1.07 0 2 -9 11.84 1.12 0 2 -9 11.09 1.17 0 -2 8 4.84 1.49 0 2 -8 3.11 1.12 0 -2 8 1.84 1.07 0 -2 8 4.56 1.37 0 2 -8 2.49 0.61 0 -2 7 6.35 1.53 0 -2 7 7.87 1.46 0 2 -7 6.20 1.35 0 -2 7 4.66 1.35 0 2 -7 5.78 0.77 0 -2 6 63.36 4.75 0 -2 6 57.98 4.46 0 2 -6 59.25 4.32 0 -2 6 46.59 4.07 0 -2 6 44.90 3.90 0 -2 6 52.65 4.23 0 -2 5 11.96 1.45 0 -2 5 9.23 1.43 0 -2 5 10.23 1.30 0 -2 5 10.18 1.49 0 -2 5 14.50 1.83 0 2 -5 10.02 1.41 0 2 -5 10.06 1.40 0 -2 5 9.72 1.46 0 2 -5 7.89 1.38 0 -2 4 7.64 1.22 0 -2 4 6.84 0.98 0 -2 4 7.46 1.29 0 -2 4 9.99 1.10 0 2 -4 7.88 1.12 0 2 -4 7.84 1.14 0 -2 4 8.17 1.28 0 2 -4 8.12 1.14 0 2 -4 8.59 1.14 0 2 -4 9.66 1.32 0 -2 3 1300.64 79.77 0 -2 3 1354.86 79.57 0 -2 3 1422.61 79.45 0 -2 3 1431.00 79.72 0 -2 3 1451.51 79.96 0 -2 3 1419.02 79.56 0 -2 3 1492.22 79.91 0 2 -3 1312.37 79.67 0 2 -3 1381.44 79.73 0 2 -3 1383.70 79.78 0 2 -3 1490.69 79.74 0 2 -3 1430.41 79.85 0 2 -3 1334.23 79.60 0 2 -3 1482.18 79.56 0 -2 3 1481.15 79.59 0 -2 2 677.63 5.31 0 -2 2 661.81 3.97 0 -2 2 728.42 4.10 0 -2 2 663.96 7.13 0 -2 2 733.24 6.82 0 -2 2 691.98 6.08 0 2 -2 714.03 5.85 0 2 -2 653.75 6.25 0 2 -2 627.20 5.71 0 2 -2 651.04 6.80 0 2 -2 645.95 6.66 0 -2 2 707.46 6.37 0 -2 1 387.49 19.82 0 2 -1 361.11 20.19 0 2 -1 429.04 20.13 0 -2 1 350.82 19.84 0 2 -1 418.64 19.87 0 -2 1 358.46 20.14 0 2 -1 380.96 19.71 0 -2 1 388.73 19.92 0 -2 1 418.34 20.15 0 2 -1 414.88 19.87 0 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183.59 12.17 0 -2 -9 180.70 10.75 0 -2 -9 181.44 12.50 0 -2 -10 115.36 9.89 0 2 10 120.28 10.24 0 2 10 138.66 10.05 0 -2 -10 147.63 8.29 0 -2 -10 131.80 8.28 0 -2 -10 141.12 8.30 0 2 10 126.71 9.96 0 -2 -10 131.68 9.82 0 -2 -10 138.12 8.39 0 -2 -10 131.60 8.27 0 -2 -10 133.80 8.44 0 2 11 2.38 1.60 0 2 11 4.29 1.51 0 -2 -11 1.95 0.64 0 -2 -11 3.61 0.83 0 -2 -11 2.95 0.78 0 2 11 3.01 1.53 0 2 11 5.53 1.87 0 -2 -11 2.72 1.28 0 -2 -11 4.24 0.88 0 -2 -11 3.43 0.82 0 -2 -11 4.58 0.92 0 2 12 22.36 3.99 0 2 12 25.98 3.72 0 -2 -12 26.84 2.33 0 2 12 34.51 4.32 0 -2 -12 24.87 2.35 0 -2 -12 27.25 2.32 0 -2 -12 23.34 3.48 0 2 12 21.06 3.94 0 -2 -12 30.72 2.47 0 -2 -12 25.41 2.23 0 -2 -12 28.36 2.34 0 -2 -13 48.84 3.71 0 -2 -13 44.82 3.57 0 -2 -13 52.76 3.76 0 -2 -13 56.80 3.90 0 -2 -13 50.34 3.74 0 -2 -14 5.56 1.02 0 -2 -14 6.51 1.15 0 -2 -14 5.58 1.12 0 -2 -14 5.86 1.09 0 -2 -14 5.98 1.12 0 -2 -15 0.58 0.68 0 -2 -15 0.84 0.76 0 -2 -15 1.48 0.78 0 -2 -16 14.65 1.53 0 -2 -16 12.63 1.49 0 -2 -17 0.40 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1787.28 102.52 0 3 -2 1774.72 102.59 0 -3 2 1871.65 102.72 0 3 -2 1897.84 102.76 0 3 -2 1756.98 102.48 0 3 -2 1770.07 102.34 0 -3 2 1962.96 102.68 0 3 -1 13.86 1.49 0 -3 1 14.16 1.47 0 3 -1 14.67 1.22 0 -3 1 14.87 1.48 0 -3 1 16.75 1.34 0 -3 1 12.84 1.47 0 3 -1 14.31 1.15 0 3 -1 15.36 1.40 0 -3 1 13.29 1.47 0 3 -1 18.76 1.67 0 -3 1 14.94 1.52 0 3 0 113.30 6.59 0 3 0 104.25 6.68 0 3 0 99.78 6.39 0 -3 0 102.81 6.74 0 -3 0 106.07 6.61 0 -3 0 114.96 6.74 0 -3 0 109.04 6.68 0 -3 0 111.59 6.61 0 3 0 114.60 6.87 0 3 1 6.23 1.06 0 -3 -1 7.33 0.88 0 3 1 7.95 1.02 0 3 1 7.34 1.03 0 -3 -1 6.75 1.05 0 3 1 7.96 0.77 0 -3 -1 6.19 0.93 0 -3 -1 8.85 1.13 0 3 1 7.02 0.90 0 -3 -1 7.98 1.04 0 -3 -1 6.99 0.81 0 -3 -1 7.15 1.09 0 3 2 29.63 2.39 0 3 2 31.19 2.48 0 3 2 31.13 2.32 0 -3 -2 32.61 2.55 0 3 2 29.59 2.37 0 -3 -2 32.73 2.38 0 -3 -2 35.53 2.62 0 3 2 33.00 2.67 0 -3 -2 30.98 2.49 0 3 3 204.13 12.34 0 3 3 205.88 12.17 0 3 3 192.41 11.94 0 -3 -3 195.09 12.26 0 -3 -3 190.50 12.11 0 3 3 222.55 12.09 0 3 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12.40 1.51 0 4 -13 15.06 1.59 0 4 -13 11.39 1.47 0 4 -12 45.57 3.44 0 4 -12 48.67 3.44 0 4 -12 44.35 3.34 0 4 -12 39.58 3.26 0 4 -11 17.85 1.73 0 4 -11 18.27 1.76 0 4 -11 14.58 1.55 0 -4 11 21.46 3.72 0 -4 11 15.42 3.05 0 4 -11 19.67 1.82 0 4 -11 14.82 1.62 0 4 -11 23.04 1.94 0 4 -11 17.59 1.75 0 4 -10 28.23 2.34 0 4 -10 26.88 2.23 0 4 -10 30.02 2.38 0 -4 10 25.09 3.67 0 -4 10 32.53 4.47 0 4 -10 30.81 2.42 0 4 -10 28.36 2.27 0 4 -10 31.87 2.42 0 4 -10 30.29 2.44 0 4 -9 17.52 1.56 0 4 -9 15.88 1.45 0 -4 9 18.01 2.83 0 4 -9 14.07 1.49 0 4 -9 14.90 1.44 0 4 -9 17.11 1.56 0 4 -9 17.93 1.63 0 -4 8 44.80 4.73 0 -4 8 56.35 5.14 0 4 -8 46.31 3.38 0 4 -8 52.85 3.48 0 4 -8 52.03 3.55 0 4 -8 48.68 3.40 0 4 -8 60.35 3.58 0 4 -8 54.36 3.60 0 -4 7 84.32 6.38 0 -4 7 71.98 6.03 0 -4 7 78.03 6.32 0 -4 7 76.45 6.44 0 4 -6 90.60 6.57 0 -4 6 87.89 6.64 0 4 -6 84.43 5.29 0 -4 6 87.09 6.51 0 -4 6 89.29 6.62 0 4 -6 89.44 5.35 0 4 -5 485.66 28.31 0 -4 5 489.85 28.43 0 -4 5 476.68 28.35 0 -4 5 482.77 28.32 0 4 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26.32 2.43 0 4 1 27.62 2.17 0 -4 -1 23.60 2.27 0 -4 -1 28.54 2.42 0 -4 -1 31.68 2.56 0 4 2 246.54 14.84 0 4 2 246.57 14.54 0 4 2 251.30 14.59 0 4 2 232.75 14.40 0 -4 -2 253.14 14.69 0 -4 -2 236.50 14.44 0 -4 -2 233.17 14.64 0 -4 -2 244.07 14.63 0 -4 -2 242.98 14.64 0 4 3 12.67 1.69 0 4 3 12.15 1.41 0 4 3 14.00 1.57 0 4 3 11.43 1.28 0 -4 -3 11.74 1.57 0 4 3 7.82 1.29 0 -4 -3 12.71 1.59 0 -4 -3 11.59 1.54 0 -4 -3 10.55 1.57 0 -4 -3 10.89 1.49 0 4 3 11.53 1.44 0 4 4 188.00 12.37 0 4 4 174.25 11.82 0 4 4 200.52 12.21 0 -4 -4 199.53 12.34 0 4 4 208.06 12.06 0 4 4 211.09 12.23 0 -4 -4 197.59 12.21 0 -4 -4 195.82 12.19 0 4 4 195.11 12.44 0 -4 -4 191.50 12.02 0 -4 -4 200.51 12.58 0 4 5 4.88 1.28 0 4 5 3.51 1.04 0 -4 -5 2.79 1.07 0 4 5 2.96 0.88 0 4 5 2.62 0.94 0 4 5 3.44 1.10 0 -4 -5 4.55 1.12 0 -4 -5 2.23 0.93 0 -4 -6 623.53 35.55 0 4 6 674.41 37.20 0 4 6 610.03 36.62 0 4 6 629.40 36.60 0 4 6 602.25 36.66 0 4 6 673.65 37.17 0 -4 -6 581.88 36.51 0 -4 -6 630.38 35.52 0 -4 -6 619.42 37.10 0 4 7 5.16 1.41 0 -4 -7 4.93 0.74 0 4 7 2.85 1.20 0 4 7 4.16 1.20 0 4 7 3.92 1.16 0 -4 -7 3.51 1.09 0 4 7 3.98 1.42 0 -4 -7 4.49 0.71 0 -4 -7 4.45 1.38 0 -4 -8 72.28 4.62 0 4 8 87.30 6.64 0 4 8 62.56 5.69 0 4 8 73.74 5.89 0 -4 -8 71.20 4.58 0 4 8 79.28 6.06 0 4 8 74.59 5.80 0 4 8 70.79 6.26 0 -4 -8 63.68 5.54 0 -4 -8 65.76 4.54 0 -4 -8 71.94 6.29 0 4 9 33.52 4.11 0 -4 -9 31.66 2.41 0 4 9 30.51 3.55 0 4 9 22.80 3.22 0 -4 -9 28.22 2.34 0 4 9 28.70 3.55 0 -4 -9 32.98 2.41 0 -4 -9 33.01 2.49 0 -4 -9 26.71 3.62 0 4 10 112.51 9.28 0 4 10 107.94 8.64 0 4 10 98.97 8.46 0 -4 -10 111.77 6.89 0 4 10 113.02 8.80 0 -4 -10 110.03 6.98 0 -4 -10 106.99 6.86 0 -4 -10 97.90 8.86 0 -4 -11 4.22 1.61 0 4 11 1.96 1.56 0 4 11 2.07 1.38 0 4 11 0.51 0.97 0 -4 -11 1.80 0.73 0 4 11 1.61 1.20 0 -4 -11 0.74 0.61 0 -4 -11 0.77 0.68 0 4 12 4.59 1.77 0 4 12 5.40 1.91 0 -4 -12 6.88 1.17 0 -4 -12 4.62 1.01 0 -4 -12 5.18 0.98 0 -4 -13 29.05 2.59 0 -4 -13 33.09 2.74 0 -4 -13 29.33 2.70 0 -4 -13 30.77 2.55 0 -4 -14 4.72 1.02 0 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-7 93.56 5.78 0 -5 7 84.66 7.26 0 -5 7 90.39 7.31 0 -5 7 99.56 7.91 0 5 -7 91.61 5.85 0 5 -7 90.62 5.87 0 5 -7 91.48 5.85 0 5 -7 106.90 5.91 0 5 -7 93.95 5.93 0 5 -7 93.29 5.83 0 5 -7 90.29 5.76 0 -5 6 26.57 3.19 0 -5 6 25.98 3.17 0 5 -6 28.61 2.07 0 -5 6 30.48 3.33 0 5 -6 29.57 3.20 0 -5 5 90.60 6.86 0 -5 5 92.05 6.87 0 -5 5 99.03 7.04 0 5 -5 91.94 5.61 0 5 -5 92.95 6.77 0 -5 5 88.40 6.67 0 -5 4 51.51 4.46 0 5 -4 54.36 4.35 0 5 -4 53.68 3.39 0 -5 4 55.07 4.53 0 5 -4 50.09 4.35 0 -5 4 53.72 4.39 0 -5 3 83.83 6.68 0 -5 3 95.63 6.72 0 5 -3 103.90 6.73 0 -5 3 92.57 6.79 0 5 -3 103.67 6.71 0 5 -3 96.77 6.89 0 -5 3 94.88 6.81 0 -5 3 100.47 6.65 0 -5 2 12.83 1.76 0 5 -2 13.47 1.70 0 -5 2 16.96 1.87 0 -5 2 13.72 1.71 0 5 -2 11.64 1.72 0 -5 2 8.42 1.57 0 -5 2 11.88 1.62 0 -5 2 11.27 1.66 0 5 -1 192.42 11.19 0 -5 1 160.86 10.86 0 -5 1 170.54 11.03 0 5 -1 185.07 11.07 0 5 -1 186.17 11.27 0 -5 1 171.64 10.85 0 -5 1 168.56 10.93 0 -5 1 159.78 10.92 0 -5 1 175.50 11.03 0 5 0 1.90 0.84 0 -5 0 1.80 0.71 0 -5 0 0.38 0.73 0 -5 0 1.44 0.77 0 -5 0 1.43 0.73 0 -5 0 1.18 0.76 0 5 0 1.40 0.86 0 -5 0 1.25 0.84 0 5 0 1.17 0.79 0 -5 0 1.26 0.79 0 5 1 102.31 7.22 0 5 1 108.19 6.90 0 -5 -1 108.17 7.22 0 -5 -1 103.90 6.98 0 -5 -1 96.23 6.92 0 -5 -1 93.89 7.00 0 5 1 108.80 7.12 0 -5 -1 109.51 7.17 0 -5 -1 110.43 7.10 0 5 2 25.86 2.79 0 5 2 24.62 2.51 0 5 2 28.63 2.59 0 -5 -2 24.73 2.67 0 5 2 27.28 2.42 0 -5 -2 27.63 2.56 0 -5 -2 30.45 2.75 0 5 2 28.68 2.65 0 -5 -2 32.62 2.81 0 -5 -2 26.00 2.61 0 5 3 12.94 2.02 0 5 3 12.39 1.72 0 5 3 15.47 1.73 0 5 3 13.43 1.66 0 -5 -3 12.78 1.85 0 -5 -3 10.52 1.65 0 -5 -3 10.42 1.62 0 5 3 14.88 1.83 0 -5 -3 13.26 1.80 0 5 4 0.29 0.84 0 5 4 -0.24 0.71 0 5 4 0.44 0.71 0 -5 -4 0.26 0.94 0 -5 -4 0.74 0.93 0 5 4 -0.21 0.58 0 -5 -4 -0.22 0.73 0 -5 -4 1.47 0.89 0 -5 -4 0.72 0.84 0 5 5 743.19 41.09 0 -5 -5 664.37 39.30 0 5 5 675.73 40.45 0 5 5 675.13 40.39 0 -5 -5 712.08 40.56 0 -5 -5 747.21 41.11 0 -5 -5 705.05 39.28 0 -5 -5 680.57 40.50 0 -5 -6 0.09 0.40 0 5 6 -0.37 1.07 0 5 6 -1.17 0.96 0 5 6 0.59 0.78 0 -5 -6 -0.37 0.99 0 -5 -6 -0.08 0.45 0 -5 -6 -0.29 0.85 0 5 7 102.13 7.70 0 -5 -7 96.95 5.89 0 5 7 89.86 7.06 0 5 7 76.64 6.75 0 5 7 97.00 7.19 0 5 7 92.15 7.03 0 -5 -7 90.97 7.04 0 -5 -7 93.13 5.83 0 -5 -7 99.73 7.70 0 -5 -8 6.69 1.85 0 5 8 4.79 1.68 0 -5 -8 8.21 1.07 0 5 8 6.95 1.75 0 5 8 8.60 1.79 0 -5 -8 9.98 1.11 0 -5 -8 6.63 0.95 0 5 8 6.59 1.63 0 5 8 9.52 1.85 0 -5 -8 9.25 1.05 0 -5 -8 7.03 1.71 0 -5 -8 8.64 1.06 0 -5 -9 -0.12 0.52 0 5 9 0.55 1.30 0 5 9 -0.44 1.05 0 5 9 1.24 1.05 0 -5 -9 0.12 0.62 0 5 9 -0.42 0.88 0 5 9 -0.81 1.03 0 -5 -9 -0.12 0.47 0 -5 -9 0.54 1.11 0 -5 -10 63.50 4.43 0 5 10 60.75 6.52 0 5 10 65.01 6.08 0 5 10 67.46 6.21 0 -5 -10 57.36 4.33 0 5 10 61.38 6.02 0 -5 -10 66.36 4.43 0 -5 -10 67.07 4.54 0 -5 -10 61.78 6.43 0 5 11 1.66 1.49 0 5 11 4.78 1.69 0 5 11 3.85 1.55 0 -5 -11 4.42 1.05 0 -5 -11 4.51 1.81 0 5 11 4.83 1.94 0 -5 -12 7.03 1.18 0 -5 -13 88.23 6.36 0 -5 -13 104.32 6.51 0 -5 -14 17.97 1.93 0 -5 -14 21.19 2.07 0 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4.45 0.80 0 6 -7 4.07 0.78 0 6 -7 5.49 0.79 0 -6 7 3.97 1.60 0 6 -7 6.68 0.89 0 6 -7 5.30 0.87 0 -6 6 34.38 3.80 0 -6 6 31.42 3.62 0 -6 6 34.27 3.67 0 6 -6 33.05 2.37 0 6 -6 29.26 2.41 0 6 -6 34.41 2.51 0 -6 6 28.78 3.57 0 6 -6 32.98 2.38 0 6 -6 35.14 2.55 0 -6 5 12.38 2.09 0 6 -5 14.43 1.28 0 -6 5 15.08 2.41 0 -6 5 14.24 2.28 0 -6 5 11.89 2.06 0 -6 4 39.41 4.00 0 -6 4 43.10 4.11 0 -6 4 41.79 3.95 0 -6 4 41.78 4.07 0 6 -4 46.14 2.96 0 -6 3 77.18 6.00 0 -6 3 77.64 6.22 0 6 -3 78.85 5.03 0 -6 3 79.84 6.25 0 -6 3 90.62 6.39 0 6 -3 85.83 6.46 0 6 -3 82.39 5.07 0 6 -3 90.45 6.24 0 -6 3 87.96 6.30 0 -6 2 290.89 19.04 0 -6 2 314.50 19.03 0 -6 2 281.50 18.92 0 -6 2 317.41 17.96 0 6 -2 323.40 17.87 0 6 -2 293.56 17.83 0 -6 2 306.95 19.00 0 6 -2 354.30 19.56 0 -6 2 336.57 19.27 0 6 -2 344.18 19.23 0 6 -2 304.08 17.80 0 -6 1 1.80 1.09 0 -6 1 1.99 1.01 0 -6 1 2.76 0.64 0 6 -1 3.88 0.56 0 -6 1 2.29 0.92 0 6 -1 3.25 1.12 0 -6 1 1.96 0.93 0 -6 1 2.92 1.13 0 6 -1 2.55 0.92 0 6 -1 2.85 0.54 0 -6 0 203.18 12.96 0 -6 0 218.80 13.09 0 -6 0 190.95 12.85 0 6 0 222.28 13.07 0 6 0 205.53 11.75 0 -6 0 212.76 13.09 0 -6 0 185.40 11.81 0 -6 0 193.23 12.64 0 6 0 209.33 11.79 0 6 0 218.57 13.35 0 -6 -1 1.31 0.88 0 -6 -1 0.48 0.81 0 -6 -1 0.90 0.93 0 -6 -1 2.37 1.07 0 6 1 0.25 0.74 0 6 1 0.64 0.41 0 6 1 0.21 0.61 0 -6 -1 1.24 0.50 0 6 1 1.15 0.42 0 -6 -1 0.72 0.76 0 -6 -2 884.01 51.35 0 -6 -2 932.28 51.52 0 -6 -2 896.61 51.60 0 6 2 926.40 51.56 0 -6 -2 901.37 51.60 0 6 2 866.97 50.19 0 6 2 915.70 51.36 0 6 2 889.23 50.23 0 -6 -2 877.76 50.31 0 -6 -2 907.03 51.52 0 -6 -3 47.98 4.13 0 -6 -3 45.56 4.13 0 6 3 44.47 3.95 0 6 3 46.60 2.98 0 -6 -3 48.41 4.16 0 6 3 50.80 4.14 0 6 3 47.06 4.36 0 6 3 47.61 3.02 0 -6 -3 43.68 3.09 0 -6 -3 43.27 4.02 0 6 4 2.29 0.99 0 -6 -4 3.96 1.19 0 -6 -4 4.22 1.23 0 6 4 2.35 1.05 0 -6 -4 2.47 1.09 0 6 4 3.39 1.13 0 -6 -4 2.22 0.59 0 6 4 4.15 1.31 0 -6 -4 4.99 1.36 0 6 5 303.03 19.01 0 -6 -5 314.67 19.29 0 -6 -5 294.40 19.55 0 6 5 300.46 19.14 0 -6 -5 307.23 17.80 0 6 5 312.66 19.60 0 -6 -5 278.07 19.01 0 -6 -5 316.86 17.75 0 6 6 88.95 6.77 0 -6 -6 70.95 4.71 0 6 6 68.60 5.87 0 -6 -6 66.47 6.29 0 6 6 72.41 5.96 0 -6 -6 73.37 4.66 0 6 6 72.18 4.74 0 -6 -6 73.53 4.67 0 -6 -6 67.70 5.91 0 -6 -7 0.90 0.54 0 6 7 0.95 1.14 0 6 7 -0.38 0.90 0 -6 -7 0.96 1.07 0 6 7 0.76 0.91 0 -6 -7 0.91 0.56 0 -6 -7 0.38 0.84 0 -6 -7 1.26 0.57 0 6 8 9.65 2.34 0 -6 -8 6.02 0.99 0 6 8 8.14 1.88 0 -6 -8 5.89 1.79 0 6 8 9.27 2.02 0 -6 -8 7.90 1.07 0 -6 -8 6.91 1.86 0 -6 -8 7.53 1.03 0 6 9 1.20 1.13 0 -6 -9 0.80 0.57 0 6 9 0.48 1.08 0 -6 -9 2.36 1.49 0 6 9 -0.46 0.78 0 -6 -9 0.12 0.54 0 -6 -9 0.26 0.56 0 -6 -9 1.31 1.10 0 -6 -10 72.45 7.44 0 -6 -10 75.82 5.27 0 -6 -10 83.80 5.50 0 -6 -10 81.70 5.35 0 6 10 76.30 7.73 0 6 10 73.32 7.10 0 -6 -11 12.87 1.58 0 -6 -12 7.89 1.26 0 -6 -12 5.76 1.17 0 6 13 8.86 1.41 0 -6 -13 8.02 1.29 0 -6 -13 8.79 1.35 0 6 14 0.80 0.77 0 -6 -14 1.56 0.75 0 -6 -14 0.61 0.73 0 -6 -15 0.39 0.63 0 6 15 -0.28 0.65 0 -6 -15 -0.13 0.50 0 -6 -15 -0.13 0.62 0 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87.08 5.69 0 7 0 94.72 5.66 0 7 0 92.74 7.26 0 -7 0 101.37 7.21 0 7 0 93.38 5.61 0 7 0 95.11 7.01 0 -7 -1 103.91 7.97 0 -7 -1 112.36 8.23 0 -7 -1 111.18 8.22 0 7 1 111.36 6.73 0 7 1 114.35 8.15 0 -7 -1 110.83 6.84 0 7 1 113.93 6.79 0 7 1 115.21 8.48 0 -7 -2 7.44 1.78 0 -7 -2 8.58 1.80 0 7 2 11.73 1.93 0 7 2 6.08 0.78 0 7 2 8.43 1.60 0 7 2 7.94 0.90 0 -7 -2 7.68 0.95 0 -7 -2 5.91 1.49 0 -7 -3 -0.71 0.89 0 -7 -3 1.00 1.01 0 7 3 0.22 0.40 0 -7 -3 -0.39 0.97 0 7 3 0.31 0.73 0 7 3 1.12 0.47 0 -7 -3 0.57 0.50 0 -7 -3 -0.66 1.00 0 -7 -4 3.24 0.69 0 7 4 4.36 0.67 0 -7 -4 2.23 1.27 0 -7 -4 5.06 1.57 0 7 4 1.30 1.04 0 -7 -4 1.25 1.06 0 7 4 4.35 1.30 0 7 4 2.39 0.59 0 7 4 3.48 0.74 0 -7 -4 2.65 0.68 0 -7 -4 3.22 0.67 0 -7 -4 4.58 1.37 0 -7 -5 4.98 0.83 0 -7 -5 2.36 1.31 0 -7 -5 3.62 1.28 0 7 5 3.83 0.71 0 7 5 2.93 1.22 0 7 5 3.38 0.78 0 -7 -5 5.65 0.85 0 -7 -5 5.27 0.85 0 -7 -5 4.15 1.37 0 -7 -6 90.37 5.77 0 7 6 89.58 7.13 0 -7 -6 80.72 7.45 0 7 6 80.86 7.11 0 -7 -6 93.93 5.74 0 -7 -6 85.82 5.68 0 7 6 89.99 5.82 0 -7 -6 83.51 7.19 0 -7 -6 92.89 5.70 0 -7 -7 0.50 0.56 0 7 7 1.28 1.08 0 -7 -7 2.17 1.29 0 7 7 -0.44 0.98 0 -7 -7 0.92 0.57 0 7 7 1.32 0.67 0 -7 -7 1.27 0.54 0 -7 -7 0.43 0.90 0 -7 -8 3.63 0.83 0 7 8 6.63 1.75 0 -7 -8 3.56 1.67 0 7 8 2.38 1.46 0 7 8 4.72 0.97 0 -7 -8 2.72 0.83 0 -7 -8 2.78 1.42 0 -7 -8 2.56 0.70 0 -7 -9 17.30 1.70 0 7 9 17.75 2.93 0 7 9 17.50 2.90 0 7 9 14.65 1.73 0 -7 -9 14.49 1.59 0 -7 -9 12.17 2.92 0 -7 -9 14.15 2.60 0 -7 -9 12.70 1.55 0 -7 -10 29.72 2.62 0 -7 -10 33.63 2.84 0 7 10 34.09 2.82 0 -7 -10 29.61 2.57 0 -7 -10 34.01 2.73 0 -7 -10 33.39 2.70 0 -7 -11 26.64 2.45 0 -7 -11 25.84 2.46 0 7 11 28.41 2.57 0 -7 -12 15.24 1.80 0 -7 -12 17.05 1.85 0 7 12 20.16 2.08 0 -7 -13 -0.15 0.67 0 7 13 -0.66 0.78 0 -7 -13 -0.33 0.60 0 -7 -14 0.14 0.65 0 7 14 1.19 0.66 0 -7 -14 0.87 0.57 0 -7 -14 0.15 0.67 0 -7 -15 10.43 1.23 0 7 15 12.24 1.34 0 -7 -15 8.69 1.13 0 -7 -15 9.77 1.18 0 7 16 1.75 0.57 0 -7 -16 1.40 0.50 0 -7 -16 1.16 0.53 0 8 -14 2.49 0.63 0 8 -14 2.31 0.64 0 8 -13 6.52 1.00 0 -8 13 10.06 1.41 0 8 -13 7.39 1.06 0 8 -13 9.12 1.12 0 8 -12 0.96 0.60 0 8 -12 -0.71 0.63 0 8 -12 0.52 0.65 0 8 -12 0.57 0.55 0 8 -12 1.11 0.63 0 8 -11 0.13 0.60 0 8 -11 0.51 0.57 0 8 -11 1.10 0.66 0 8 -11 -0.15 0.69 0 8 -11 0.90 0.57 0 8 -10 1.04 0.62 0 8 -10 1.96 0.84 0 8 -10 2.08 0.79 0 8 -10 1.60 0.77 0 8 -10 2.03 0.83 0 8 -9 0.64 0.69 0 8 -9 0.13 0.55 0 8 -9 0.48 0.61 0 8 -9 0.29 0.59 0 8 -9 1.40 0.67 0 8 -8 122.35 7.70 0 8 -8 129.46 7.89 0 8 -8 130.49 7.93 0 8 -8 112.60 7.69 0 8 -8 126.78 7.94 0 -8 7 16.66 2.87 0 -8 7 8.85 2.30 0 -8 7 12.12 2.91 0 8 -7 15.10 1.52 0 8 -7 17.13 1.67 0 8 -7 18.47 1.74 0 8 -7 14.37 1.51 0 -8 7 13.48 2.85 0 8 -7 16.77 1.73 0 -8 6 131.60 7.77 0 -8 6 113.57 9.52 0 -8 6 104.73 9.20 0 8 -6 106.30 7.28 0 8 -6 126.33 7.58 0 8 -6 132.44 7.60 0 8 -6 118.44 7.59 0 8 -6 114.22 7.39 0 -8 6 120.94 9.65 0 -8 5 0.47 1.26 0 -8 5 -0.14 0.69 0 -8 5 2.35 1.43 0 8 -5 0.29 0.47 0 8 -5 -0.13 0.51 0 8 -5 0.74 0.58 0 -8 5 -0.94 1.59 0 8 -5 0.33 0.50 0 -8 4 0.87 0.97 0 -8 4 0.39 0.57 0 -8 4 0.90 1.00 0 8 -4 0.71 0.52 0 8 -4 0.12 0.46 0 -8 4 0.86 1.20 0 -8 3 -0.40 0.82 0 8 -3 -0.10 0.51 0 -8 3 0.12 0.59 0 -8 3 0.43 0.95 0 -8 3 -0.41 1.10 0 8 -3 1.96 1.09 0 8 -3 0.44 0.42 0 8 -3 0.11 0.46 0 8 -3 0.12 0.48 0 8 -3 0.46 1.01 0 8 -2 40.10 2.78 0 -8 2 36.22 3.98 0 -8 2 37.53 2.82 0 -8 2 30.30 3.86 0 -8 2 36.40 4.08 0 8 -2 39.12 2.70 0 8 -2 40.52 4.16 0 -8 2 51.37 4.60 0 8 -2 33.81 2.70 0 8 -2 38.46 2.84 0 8 -2 37.58 4.25 0 8 -1 4.66 0.81 0 -8 1 4.71 0.86 0 -8 1 5.52 1.58 0 -8 1 5.80 1.62 0 -8 1 6.04 1.65 0 8 -1 5.88 0.82 0 8 -1 4.65 1.38 0 8 -1 4.47 0.81 0 8 -1 6.01 0.90 0 8 -1 5.30 1.56 0 -8 0 9.00 1.12 0 8 0 10.68 1.10 0 -8 0 10.70 2.09 0 -8 0 10.20 2.12 0 -8 0 7.20 1.85 0 8 0 10.43 1.98 0 8 0 8.26 0.97 0 -8 0 10.33 1.10 0 8 0 6.20 0.97 0 8 0 8.34 1.09 0 8 0 5.72 1.73 0 -8 -1 8.01 1.04 0 8 1 7.67 0.98 0 -8 -1 5.58 1.52 0 -8 -1 6.02 1.70 0 -8 -1 8.80 1.92 0 8 1 6.56 1.67 0 8 1 7.19 0.89 0 8 1 5.77 0.89 0 8 1 7.31 1.02 0 -8 -1 8.42 1.01 0 8 1 5.32 1.59 0 8 2 1.45 0.55 0 -8 -2 0.65 0.53 0 -8 -2 0.83 1.16 0 8 2 1.04 0.49 0 -8 -2 2.01 1.12 0 8 2 1.55 1.08 0 8 2 0.30 0.44 0 8 2 2.07 0.62 0 -8 -2 2.33 0.67 0 8 2 0.90 0.93 0 8 3 0.29 0.46 0 -8 -3 1.01 0.55 0 -8 -3 1.72 1.14 0 -8 -3 -0.41 0.96 0 8 3 -0.39 0.92 0 -8 -3 -0.45 1.01 0 8 3 1.13 0.51 0 8 3 0.10 0.44 0 -8 -3 0.43 0.57 0 8 3 -0.12 0.53 0 8 3 0.46 0.87 0 -8 -4 30.84 2.36 0 8 4 25.10 2.15 0 -8 -4 35.85 3.99 0 8 4 24.99 3.30 0 -8 -4 29.87 3.56 0 -8 -4 28.45 3.76 0 8 4 35.50 3.73 0 8 4 27.17 2.22 0 -8 -4 30.15 2.35 0 -8 -4 28.19 2.24 0 8 4 30.06 2.38 0 -8 -4 29.52 3.60 0 -8 -5 59.83 4.05 0 -8 -5 56.17 5.60 0 8 5 57.34 3.94 0 8 5 58.86 5.53 0 -8 -5 59.38 4.03 0 -8 -5 68.96 6.18 0 -8 -5 55.81 3.94 0 8 5 58.79 4.09 0 -8 -5 52.02 5.37 0 -8 -6 430.26 25.18 0 -8 -6 431.39 25.15 0 8 6 432.62 27.21 0 -8 -6 469.34 28.09 0 -8 -6 441.87 25.13 0 8 6 455.98 25.30 0 -8 -6 353.22 26.73 0 -8 -7 4.96 0.95 0 -8 -7 4.22 1.70 0 8 7 0.99 1.47 0 8 7 4.29 0.98 0 -8 -7 3.25 0.83 0 -8 -7 5.02 0.97 0 -8 -7 4.52 0.84 0 -8 -7 2.96 1.46 0 -8 -8 95.64 6.15 0 8 8 84.17 7.83 0 8 8 81.08 7.76 0 8 8 104.24 6.31 0 -8 -8 98.12 6.12 0 -8 -8 85.64 8.36 0 -8 -8 90.76 6.04 0 -8 -8 72.23 7.52 0 -8 -9 0.85 0.71 0 8 9 0.33 0.73 0 -8 -9 -0.14 0.58 0 -8 -9 0.30 0.61 0 8 10 14.25 1.74 0 -8 -10 11.50 1.44 0 -8 -10 11.88 1.44 0 -8 -10 14.29 1.68 0 -8 -10 9.62 1.38 0 8 11 4.59 1.09 0 -8 -11 2.35 0.78 0 -8 -11 3.30 0.96 0 8 12 2.79 0.93 0 -8 -12 4.31 0.96 0 8 13 2.88 0.88 0 -8 -13 4.36 0.91 0 -8 -13 2.56 0.80 0 -8 -14 -0.13 0.65 0 8 14 1.05 0.67 0 -8 -14 0.51 0.52 0 -8 -14 0.12 0.56 0 -8 -15 -0.20 0.49 0 8 15 0.43 0.52 0 -8 -15 -0.09 0.52 0 9 -14 4.58 0.69 0 9 -13 2.84 0.63 0 9 -12 10.97 1.25 0 9 -12 8.03 1.10 0 9 -12 12.62 1.33 0 9 -11 0.56 0.56 0 9 -11 -0.12 0.56 0 9 -11 -0.14 0.58 0 -9 10 33.12 2.79 0 9 -10 27.87 2.46 0 9 -10 32.41 2.56 0 9 -9 35.82 2.99 0 9 -9 40.18 3.24 0 9 -9 38.98 3.20 0 9 -9 41.41 3.20 0 9 -8 41.88 3.35 0 -9 8 56.83 3.94 0 9 -8 53.42 3.73 0 9 -8 43.51 3.49 0 9 -8 45.59 3.57 0 9 -7 434.13 26.99 0 9 -7 474.45 27.24 0 9 -7 458.52 27.22 0 -9 7 529.02 27.59 0 9 -7 474.51 27.34 0 -9 6 220.37 11.95 0 -9 6 180.31 13.89 0 -9 6 175.16 13.77 0 9 -6 175.10 11.38 0 9 -6 197.47 11.71 0 9 -6 194.20 11.67 0 9 -6 197.04 11.74 0 -9 6 166.42 13.70 0 -9 5 30.57 2.59 0 -9 5 27.78 3.88 0 -9 5 31.66 4.08 0 9 -5 27.08 2.21 0 9 -5 29.87 2.44 0 9 -5 26.12 2.37 0 -9 5 30.27 4.06 0 9 -4 11.92 1.32 0 -9 4 10.66 1.40 0 -9 4 7.96 2.08 0 9 -4 8.51 1.22 0 -9 4 8.42 2.28 0 -9 3 11.67 2.56 0 -9 3 12.95 2.55 0 9 -3 15.36 1.64 0 -9 3 19.64 1.85 0 9 -3 17.57 1.71 0 9 -3 18.21 1.76 0 9 -3 18.19 1.59 0 -9 3 17.47 1.66 0 9 -2 32.41 2.52 0 9 -2 39.46 4.27 0 -9 2 36.33 4.24 0 -9 2 34.29 4.18 0 -9 2 33.14 4.04 0 9 -2 35.44 2.65 0 -9 2 35.41 2.72 0 9 -2 29.23 2.53 0 9 -2 35.30 2.70 0 9 -2 31.50 4.08 0 -9 1 1.45 1.28 0 9 -1 0.46 0.95 0 9 -1 0.31 0.50 0 -9 1 0.47 1.04 0 -9 1 -0.47 1.26 0 9 -1 0.12 0.52 0 9 -1 -0.83 0.53 0 9 -1 -0.26 0.55 0 9 -1 0.52 0.88 0 9 0 10.10 2.12 0 9 0 7.54 1.02 0 -9 0 10.08 2.10 0 -9 0 7.38 1.94 0 -9 0 6.15 1.83 0 9 0 6.47 1.01 0 9 0 6.66 1.01 0 -9 0 6.31 0.99 0 9 0 9.14 1.19 0 9 0 8.33 2.14 0 -9 -1 15.81 2.79 0 9 1 15.56 2.64 0 9 1 15.41 1.48 0 -9 -1 12.56 2.56 0 9 1 16.73 1.59 0 -9 -1 18.95 1.65 0 9 1 12.36 1.45 0 9 1 16.10 1.64 0 9 1 19.35 3.11 0 9 2 10.85 1.17 0 9 2 15.16 2.57 0 -9 -2 7.65 2.06 0 -9 -2 7.43 2.09 0 9 2 9.46 1.20 0 -9 -2 12.31 1.34 0 9 2 9.81 1.20 0 9 2 10.22 1.28 0 9 2 12.19 1.27 0 9 2 9.53 2.30 0 9 3 2.15 0.62 0 -9 -3 2.40 1.35 0 9 3 5.97 1.73 0 -9 -3 3.06 1.55 0 9 3 1.61 0.60 0 9 3 2.59 0.71 0 -9 -3 2.12 0.77 0 9 3 2.21 0.82 0 9 3 1.62 1.29 0 9 4 1.53 0.56 0 -9 -4 0.55 0.92 0 -9 -4 2.13 0.67 0 -9 -4 1.58 1.18 0 9 4 1.14 0.60 0 9 4 0.48 0.54 0 -9 -4 2.01 0.69 0 -9 -4 1.69 0.79 0 9 4 1.58 0.72 0 9 4 1.11 1.04 0 -9 -5 296.38 20.02 0 -9 -5 296.97 19.75 0 -9 -5 301.28 17.33 0 9 5 267.07 17.15 0 -9 -5 306.53 17.34 0 9 5 268.11 19.17 0 9 5 331.08 17.49 0 -9 -5 281.06 17.20 0 9 5 285.34 19.84 0 -9 -6 14.90 1.60 0 9 6 12.81 1.43 0 9 6 13.42 2.57 0 -9 -6 15.35 2.93 0 -9 -6 10.79 1.43 0 9 6 14.12 1.61 0 -9 -6 12.36 1.55 0 9 7 543.84 39.78 0 -9 -7 664.51 37.86 0 -9 -7 658.86 37.83 0 9 7 710.26 38.04 0 -9 -7 649.80 37.84 0 -9 -7 645.54 40.90 0 9 8 -0.17 0.72 0 -9 -8 1.01 0.82 0 -9 -9 -0.15 0.67 0 9 9 1.35 0.79 0 -9 -9 -0.72 0.69 0 -9 -10 11.57 1.47 0 9 10 11.93 1.53 0 -9 -10 11.94 1.45 0 -9 -10 12.22 1.56 0 9 11 0.32 0.76 0 -9 -11 -1.07 0.75 0 -9 -11 0.33 0.63 0 9 12 -0.30 0.74 0 -9 -12 -0.36 0.61 0 -9 -12 -0.90 0.62 0 -9 -12 0.15 0.62 0 9 13 1.19 0.70 0 -9 -13 1.69 0.63 0 -9 -13 2.11 0.76 0 -9 -14 2.59 0.69 0 9 14 2.63 0.66 0 10 -13 10.22 1.00 0 10 -12 0.10 0.44 0 10 -12 0.68 0.49 0 10 -11 0.84 0.60 0 10 -11 0.71 0.57 0 10 -11 0.49 0.54 0 10 -10 44.59 3.24 0 10 -10 43.69 3.22 0 10 -10 39.76 3.01 0 10 -9 9.10 1.30 0 10 -9 9.47 1.24 0 10 -9 10.80 1.36 0 10 -9 9.05 1.16 0 10 -8 38.77 3.15 0 10 -8 41.71 3.13 0 10 -8 42.66 3.14 0 10 -8 34.40 2.83 0 10 -7 19.31 1.88 0 10 -7 16.60 1.77 0 10 -7 16.57 1.75 0 10 -7 13.48 1.51 0 10 -6 47.56 3.50 0 10 -6 44.61 3.48 0 10 -6 44.85 3.41 0 10 -6 41.60 3.16 0 10 -5 12.62 1.52 0 10 -5 10.56 1.32 0 10 -5 9.47 1.36 0 10 -5 10.67 1.40 0 10 -4 3.03 0.87 0 10 -4 4.97 0.96 0 10 -4 5.41 0.97 0 -10 3 1.74 1.55 0 10 -3 0.14 0.53 0 10 -3 -1.12 0.65 0 10 -3 1.02 0.65 0 -10 3 0.14 0.67 0 -10 2 112.73 9.78 0 10 -2 124.11 7.71 0 10 -2 123.94 7.72 0 10 -2 117.80 7.67 0 10 -2 124.57 7.77 0 -10 2 124.12 7.71 0 10 -2 139.25 10.15 0 -10 2 120.23 9.88 0 10 -2 114.43 7.52 0 -10 1 1.09 0.75 0 -10 1 1.11 1.33 0 10 -1 0.47 0.55 0 10 -1 1.59 1.26 0 -10 1 1.10 1.39 0 -10 1 -0.54 1.21 0 10 -1 0.55 0.64 0 10 -1 1.61 0.71 0 10 -1 1.61 0.77 0 10 -1 0.59 1.00 0 10 0 0.59 0.63 0 -10 0 0.56 1.48 0 -10 0 0.54 0.76 0 10 0 -1.06 1.34 0 -10 0 -0.54 1.28 0 -10 0 0.55 1.31 0 10 0 0.27 0.65 0 10 0 0.26 0.61 0 10 0 0.15 0.65 0 -10 0 0.13 0.67 0 10 0 1.78 1.66 0 10 0 1.07 0.72 0 10 1 173.77 10.77 0 -10 -1 174.47 10.91 0 10 1 198.86 13.42 0 -10 -1 170.60 13.14 0 -10 -1 195.16 13.52 0 10 1 181.70 10.92 0 -10 -1 190.46 10.95 0 10 1 158.66 10.79 0 10 1 182.47 11.00 0 10 1 194.51 10.96 0 10 1 166.47 13.26 0 10 2 71.13 5.01 0 -10 -2 82.42 5.24 0 -10 -2 63.59 6.83 0 10 2 77.69 7.12 0 -10 -2 80.95 7.44 0 10 2 74.33 5.14 0 -10 -2 77.07 5.20 0 10 2 75.07 5.13 0 10 2 82.54 5.33 0 10 2 84.47 5.20 0 10 2 72.13 7.33 0 -10 -3 1.21 0.76 0 10 3 0.53 0.99 0 -10 -3 -0.55 1.13 0 10 3 0.46 0.58 0 -10 -3 1.76 1.31 0 10 3 0.26 0.59 0 10 3 0.66 0.55 0 -10 -3 1.55 0.79 0 10 3 0.15 0.66 0 10 3 0.61 1.15 0 -10 -4 5.22 0.97 0 10 4 5.14 0.95 0 -10 -4 5.97 2.03 0 10 4 5.03 0.93 0 10 4 5.56 1.89 0 10 4 4.42 1.05 0 -10 -4 4.22 1.00 0 10 5 12.10 1.54 0 -10 -5 11.12 1.40 0 -10 -5 10.90 1.51 0 10 5 11.53 1.39 0 10 6 330.83 18.07 0 -10 -6 293.49 17.81 0 -10 -6 297.20 17.89 0 10 6 291.85 17.74 0 -10 -7 -0.14 0.75 0 -10 -7 1.51 0.81 0 10 7 2.17 0.78 0 -10 -8 10.19 1.38 0 -10 -8 10.06 1.39 0 10 8 11.68 1.53 0 -10 -9 2.71 0.87 0 10 9 2.79 0.86 0 -10 -10 10.14 1.41 0 -10 -10 11.63 1.43 0 10 10 11.91 1.50 0 -10 -10 9.47 1.31 0 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49.78 3.96 2 -4 5 197.91 12.66 2 -4 5 192.74 12.69 -2 4 -5 185.52 11.38 -2 4 -5 202.04 12.97 -2 4 -5 230.26 13.12 -2 4 -6 20.89 2.72 -2 4 -6 22.91 2.80 2 -4 6 20.91 2.62 2 -4 7 66.47 5.58 -2 4 -7 66.50 5.49 -2 4 -7 67.60 5.66 2 -4 7 57.36 5.28 -2 4 -7 62.62 3.88 -2 4 -7 58.58 3.99 -2 4 -7 57.36 3.84 -2 4 -7 56.73 3.89 -2 4 -7 56.27 3.91 -2 4 -7 61.32 3.93 -2 4 -7 56.41 3.83 -2 4 -8 51.63 4.79 2 -4 8 38.35 4.41 -2 4 -8 45.54 4.63 -2 4 -8 46.83 4.38 -2 4 -8 39.06 2.91 -2 4 -8 42.30 3.02 2 -4 8 39.53 4.38 -2 4 -8 40.74 3.08 -2 4 -8 43.96 2.98 -2 4 -8 40.83 3.01 -2 4 -8 44.66 2.99 -2 4 -8 42.04 3.05 -2 4 -8 42.99 3.04 2 -4 9 8.10 2.10 -2 4 -9 5.54 0.93 -2 4 -9 4.47 0.82 -2 4 -9 4.19 0.78 2 -4 9 5.38 1.91 -2 4 -9 5.42 1.73 -2 4 -9 4.66 0.87 -2 4 -9 5.84 0.95 -2 4 -9 4.05 0.84 -2 4 -9 4.95 0.90 2 -4 10 15.18 2.85 -2 4 -10 16.19 1.60 -2 4 -10 14.38 1.65 -2 4 -10 18.37 1.72 -2 4 -10 15.89 1.61 -2 4 -10 18.89 1.75 -2 4 -10 16.70 1.67 2 -4 11 1.77 1.41 -2 4 -11 2.60 0.81 -2 4 -11 1.11 0.74 -2 4 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48.18 2 -2 -6 873.34 49.29 -2 2 5 409.35 25.64 -2 2 5 444.24 25.78 -2 2 5 415.65 25.80 2 -2 -5 397.74 25.46 -2 2 5 463.50 26.19 -2 2 5 424.37 25.83 2 -2 -5 449.27 25.71 2 -2 -5 434.87 25.93 2 -2 -5 457.10 25.67 -2 2 4 61.43 4.83 -2 2 4 59.91 4.75 -2 2 4 70.99 5.04 -2 2 4 69.93 5.14 2 -2 -4 67.08 4.79 -2 2 4 61.44 4.91 2 -2 -4 73.81 5.09 2 -2 -4 62.92 4.82 2 -2 -4 58.22 4.67 -2 2 3 15.26 1.84 -2 2 3 15.26 1.71 -2 2 3 17.28 2.01 -2 2 3 12.73 1.74 -2 2 3 13.41 1.72 2 -2 -3 15.90 1.80 2 -2 -3 15.44 1.65 2 -2 -3 15.06 1.77 2 -2 -3 17.11 1.72 2 -2 -3 14.96 1.82 -2 2 3 14.00 1.70 2 -2 -3 15.50 1.75 -2 2 2 165.17 9.65 -2 2 2 165.36 9.94 -2 2 2 159.10 9.87 2 -2 -2 154.42 9.56 -2 2 2 145.69 9.76 2 -2 -2 152.24 9.76 2 -2 -2 160.95 9.61 -2 2 2 159.47 9.72 2 -2 -2 152.67 9.70 2 -2 -2 151.32 9.73 -2 2 2 152.95 9.78 2 -2 -2 157.57 9.76 -2 2 1 76.96 5.47 2 -2 -1 79.09 5.22 -2 2 1 75.34 5.35 2 -2 -1 78.33 5.35 2 -2 -1 80.20 5.24 2 -2 -1 82.39 5.11 -2 2 1 74.84 5.32 2 -2 -1 73.74 5.10 -2 2 1 82.23 5.43 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38.39 4.20 -2 -4 -9 37.61 2.80 -2 -4 -9 36.73 2.74 -2 -4 -9 35.19 2.79 -2 -4 -9 39.99 2.89 -2 -4 -10 2.90 0.71 2 4 10 1.69 1.35 2 4 10 5.45 1.63 2 4 10 3.16 1.30 -2 -4 -10 3.47 0.80 2 4 10 3.54 1.42 -2 -4 -10 2.38 0.71 -2 -4 -10 3.15 0.78 -2 -4 -10 2.96 0.74 2 4 11 14.11 3.03 2 4 11 10.48 2.35 2 4 11 14.33 2.94 -2 -4 -11 14.43 1.57 2 4 11 14.77 2.74 -2 -4 -11 19.16 1.76 -2 -4 -11 14.88 1.67 2 4 12 7.88 2.51 2 4 12 10.84 2.70 2 4 12 3.20 1.59 -2 -4 -12 7.01 1.11 -2 -4 -12 5.08 0.93 -2 -4 -12 6.75 1.21 2 4 12 3.41 1.47 -2 -4 -12 5.98 1.07 -2 -4 -13 7.84 1.16 -2 -4 -13 4.40 0.99 -2 -4 -13 7.68 1.23 -2 -4 -13 5.39 1.16 -2 -4 -14 17.09 1.75 -2 -4 -14 15.55 1.82 -2 -4 -14 19.32 1.90 -2 -4 -15 21.36 2.03 -2 -4 -15 21.33 1.93 -2 -4 -15 17.70 1.91 -2 -4 -16 19.59 1.80 -2 -4 -16 15.49 1.68 -2 -4 -17 1.89 0.63 2 5 -16 0.82 0.44 2 5 -16 -0.53 0.53 2 5 -15 0.11 0.50 2 5 -15 0.47 0.49 2 5 -15 0.46 0.54 2 5 -14 4.22 0.88 2 5 -14 4.26 0.90 2 5 -14 2.93 0.76 2 5 -14 3.71 0.85 2 5 -13 25.85 2.32 2 5 -13 26.54 2.36 2 5 -13 26.54 2.31 2 5 -13 26.62 2.34 2 5 -12 0.60 0.63 2 5 -12 1.08 0.65 2 5 -12 0.99 0.72 2 5 -12 1.15 0.70 2 5 -11 68.86 4.77 2 5 -11 74.95 4.77 2 5 -11 65.45 4.71 2 5 -11 70.86 4.72 2 5 -11 61.95 4.70 2 5 -10 96.78 5.88 2 5 -10 98.25 5.80 2 5 -10 87.77 5.72 -2 -5 10 106.89 9.20 2 5 -10 77.22 5.68 2 5 -10 71.38 5.61 2 5 -10 96.64 5.95 2 5 -10 87.26 5.87 2 5 -10 101.56 5.89 2 5 -10 91.40 5.90 2 5 -10 91.04 5.83 2 5 -10 87.84 5.85 2 5 -9 0.88 0.53 2 5 -9 2.29 0.69 2 5 -9 1.52 0.65 -2 -5 9 1.96 1.74 -2 -5 9 1.88 1.29 2 5 -9 1.71 0.67 2 5 -9 1.10 0.60 2 5 -9 2.35 0.73 2 5 -9 1.69 0.62 2 5 -9 0.90 0.54 2 5 -9 1.66 0.64 2 5 -9 2.45 0.70 -2 -5 8 131.25 10.77 2 5 -8 153.28 8.92 -2 -5 8 165.58 11.73 -2 -5 8 159.60 11.73 2 5 -8 148.80 9.04 2 5 -8 124.91 8.79 2 5 -8 139.19 8.97 2 5 -8 160.04 9.02 2 5 -8 156.87 8.93 2 5 -8 140.82 8.97 2 5 -8 159.40 8.98 -2 -5 7 1.61 1.27 -2 -5 7 0.85 1.02 2 5 -7 1.08 0.49 -2 -5 7 0.51 0.96 -2 -5 7 0.97 0.92 2 5 -7 0.78 0.44 2 5 -7 0.76 0.52 2 5 -7 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2.84 -2 -5 -6 25.34 2.94 2 5 6 18.41 2.49 -2 -5 -6 22.80 1.84 2 5 6 21.08 2.80 -2 -5 -6 24.52 1.77 2 5 6 27.98 3.29 2 5 7 7.13 1.47 -2 -5 -7 9.44 1.77 2 5 7 4.96 1.34 2 5 7 6.56 1.67 -2 -5 -7 9.03 1.02 2 5 7 7.54 1.91 -2 -5 -7 6.50 0.84 -2 -5 -8 17.64 1.47 2 5 8 13.28 2.58 -2 -5 -8 13.12 1.28 -2 -5 -8 13.14 1.37 2 5 8 11.76 2.36 2 5 8 14.82 2.25 2 5 8 14.81 2.20 -2 -5 -8 10.60 2.14 2 5 8 9.05 1.93 -2 -5 -8 13.98 1.46 -2 -5 -8 15.28 1.46 -2 -5 -9 18.52 1.73 2 5 9 18.84 3.22 2 5 9 20.27 2.79 2 5 9 17.09 2.58 -2 -5 -9 17.91 1.77 2 5 9 19.70 3.06 2 5 9 19.32 2.67 -2 -5 -9 19.01 1.82 -2 -5 -9 21.54 1.86 2 5 10 -0.43 1.03 2 5 10 0.86 0.89 2 5 10 2.78 1.32 -2 -5 -10 0.14 0.58 -2 -5 -10 0.70 0.64 2 5 10 0.61 1.15 -2 -5 -10 0.73 0.55 -2 -5 -11 -0.13 0.50 2 5 11 0.68 1.41 2 5 11 -0.62 1.17 2 5 11 0.48 0.99 2 5 11 -0.49 1.01 2 5 11 1.59 1.09 -2 -5 -11 1.00 0.71 -2 -5 -11 0.31 0.69 -2 -5 -12 52.85 3.84 2 5 12 41.16 5.04 2 5 12 35.66 5.01 -2 -5 -12 54.00 3.78 -2 -5 -12 48.25 3.62 -2 -5 -12 52.23 3.80 -2 -5 -13 5.58 1.19 -2 -5 -13 4.70 0.98 -2 -5 -14 0.33 0.76 -2 -5 -15 57.18 4.15 -2 -5 -16 -0.52 0.66 -2 -5 -17 6.41 0.92 2 6 -16 -0.08 0.33 2 6 -15 1.37 0.57 2 6 -15 1.71 0.61 2 6 -15 1.77 0.57 2 6 -14 10.52 1.24 2 6 -14 8.82 1.17 2 6 -14 8.09 1.14 2 6 -13 0.72 0.64 2 6 -13 1.37 0.71 2 6 -13 1.51 0.70 2 6 -12 16.85 1.74 2 6 -12 15.15 1.67 2 6 -12 13.89 1.60 2 6 -11 2.57 0.81 2 6 -11 2.07 0.77 2 6 -11 1.69 0.68 2 6 -11 1.86 0.78 2 6 -10 18.39 1.91 2 6 -10 26.64 2.11 2 6 -10 17.04 1.80 2 6 -10 16.75 1.82 2 6 -10 21.80 2.02 2 6 -10 20.52 2.01 2 6 -10 21.06 1.98 2 6 -10 25.14 2.05 2 6 -10 21.64 1.89 2 6 -9 9.08 1.12 -2 -6 9 8.24 2.35 -2 -6 9 4.89 2.08 2 6 -9 6.61 1.07 2 6 -9 7.61 1.19 2 6 -9 8.47 1.17 2 6 -9 6.80 1.01 2 6 -9 10.24 1.22 2 6 -9 6.99 1.09 2 6 -9 6.71 1.03 -2 -6 8 41.98 4.85 -2 -6 8 39.09 4.87 2 6 -8 44.49 3.15 -2 -6 8 38.97 5.07 -2 -6 8 51.80 5.70 2 6 -8 47.04 3.29 2 6 -8 35.82 3.01 2 6 -8 40.90 3.17 2 6 -8 48.09 3.25 2 6 -8 41.77 3.09 2 6 -8 52.02 3.27 2 6 -8 44.11 3.21 2 6 -7 2.93 0.70 -2 -6 7 6.08 1.72 -2 -6 7 3.24 1.41 -2 -6 7 1.64 1.31 -2 -6 7 2.82 1.65 2 6 -7 2.58 0.63 2 6 -7 4.26 0.79 2 6 -7 2.47 0.70 2 6 -7 2.82 0.70 2 6 -7 3.22 0.71 2 6 -7 2.75 0.67 2 6 -6 41.45 2.88 2 6 -6 41.16 2.83 -2 -6 6 49.04 4.60 2 6 -6 46.80 2.90 -2 -6 6 32.82 4.07 -2 -6 6 39.01 4.47 -2 -6 6 56.84 5.21 2 6 -6 35.49 2.72 2 6 -6 38.81 2.84 2 6 -6 38.05 2.85 2 6 -6 39.25 2.89 2 6 -6 38.49 2.85 -2 -6 5 18.99 2.81 -2 -6 5 12.26 2.26 2 6 -5 12.82 2.27 2 6 -5 13.88 1.29 2 6 -5 14.55 1.26 -2 -6 5 13.26 2.26 2 6 -5 12.23 1.23 -2 -6 5 9.63 2.13 -2 -6 4 33.54 3.65 -2 -6 4 46.80 4.29 -2 -6 4 43.13 4.24 -2 -6 4 33.30 3.70 2 6 -4 37.20 2.58 -2 -6 4 35.24 3.65 2 6 -4 38.29 2.67 2 6 -4 37.64 2.58 2 6 -4 43.16 4.08 -2 -6 3 50.16 4.35 -2 -6 3 48.13 4.53 -2 -6 3 44.82 4.13 -2 -6 3 37.27 4.03 2 6 -3 45.90 3.02 -2 -6 3 48.15 4.10 2 6 -3 53.64 4.53 2 6 -3 48.02 3.07 -2 -6 2 252.31 15.89 -2 -6 2 272.46 16.20 2 6 -2 239.73 14.38 -2 -6 2 252.90 15.82 2 6 -2 245.65 15.43 2 6 -2 243.61 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111.41 6.65 2 8 -6 9.21 1.15 -2 -8 6 7.01 2.04 2 8 -6 11.07 1.25 -2 -8 6 7.45 2.15 2 8 -6 7.09 1.00 2 8 -6 9.68 1.23 2 8 -6 8.46 1.14 2 8 -6 10.37 1.28 2 8 -6 11.61 1.28 2 8 -5 24.89 3.69 2 8 -5 27.30 2.10 -2 -8 5 32.43 4.16 -2 -8 5 20.75 3.47 -2 -8 5 23.68 3.40 2 8 -5 27.20 2.10 -2 -8 5 22.84 3.51 2 8 -5 22.80 2.06 2 8 -5 22.61 2.08 2 8 -5 25.05 2.14 2 8 -5 27.79 2.18 -2 -8 4 1.81 1.33 -2 -8 4 0.51 1.14 -2 -8 4 2.56 1.62 2 8 -4 3.11 0.66 -2 -8 4 2.28 1.34 -2 -8 4 3.16 0.83 2 8 -4 1.93 0.60 2 8 -4 3.46 0.78 2 8 -4 3.01 0.63 2 8 -4 2.45 1.38 -2 -8 3 135.73 7.76 -2 -8 3 112.55 9.14 2 8 -3 110.33 7.56 2 8 -3 122.80 7.51 -2 -8 3 126.18 9.51 -2 -8 3 124.51 9.64 2 8 -2 215.26 12.15 -2 -8 2 212.37 14.14 -2 -8 2 197.75 12.26 -2 -8 2 242.71 14.71 -2 -8 2 206.80 14.16 -2 -8 2 209.62 14.01 -2 -8 2 210.68 12.38 2 8 -2 202.20 12.31 2 8 -2 212.77 14.35 2 8 -2 200.98 12.19 -2 -8 1 11.27 2.05 -2 -8 1 9.95 1.08 2 8 -1 9.34 0.96 -2 -8 1 5.47 1.78 -2 -8 1 5.70 1.66 -2 -8 1 10.58 1.99 2 8 -1 8.70 1.95 -2 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7 426.26 28.78 -2 -9 -7 486.28 27.01 2 9 7 455.28 26.89 -2 -9 -7 442.40 26.84 -2 -9 -7 474.04 26.91 -2 -9 -8 49.07 5.63 2 9 8 47.20 5.69 -2 -9 -8 48.91 3.59 2 9 8 36.25 4.54 2 9 8 46.53 5.00 -2 -9 -8 43.71 3.46 -2 -9 -8 44.79 3.42 -2 -9 -8 45.74 3.45 2 9 8 50.87 3.57 -2 -9 -8 44.25 3.49 -2 -9 -9 26.77 2.34 -2 -9 -9 20.96 2.19 -2 -9 -9 24.39 2.24 -2 -9 -9 25.53 2.23 2 9 9 24.98 2.27 -2 -9 -9 21.45 2.12 -2 -9 -10 30.12 2.53 2 9 10 29.32 2.48 -2 -9 -10 30.29 2.55 -2 -9 -10 24.19 2.32 -2 -9 -10 24.11 2.34 -2 -9 -10 27.54 2.55 -2 -9 -11 0.76 0.67 -2 -9 -11 0.95 0.69 -2 -9 -11 0.85 0.71 2 9 11 0.45 0.63 -2 -9 -11 0.16 0.67 -2 -9 -11 0.17 0.73 -2 -9 -12 7.82 1.17 2 9 12 6.75 1.14 -2 -9 -12 6.07 1.17 -2 -9 -12 8.45 1.20 -2 -9 -12 8.18 1.29 -2 -9 -13 6.31 1.08 -2 -9 -13 7.63 1.24 -2 -9 -14 1.83 0.70 -2 -9 -14 2.32 0.76 -2 -9 -15 0.09 0.45 -2 -9 -15 -0.10 0.49 2 10 -13 0.70 0.38 2 10 -13 0.85 0.43 2 10 -12 20.25 1.77 2 10 -12 21.52 1.80 -2 -10 12 23.91 2.06 -2 -10 11 1.56 0.79 2 10 -11 0.97 0.57 2 10 -11 0.11 0.50 2 10 -11 0.70 0.55 2 10 -10 -0.14 0.56 -2 -10 10 0.17 0.80 2 10 -10 1.50 0.64 2 10 -10 -0.12 0.57 2 10 -10 -0.25 0.55 2 10 -10 0.27 0.58 2 10 -9 13.91 1.54 2 10 -9 16.90 1.77 -2 -10 9 18.46 2.06 2 10 -9 18.03 1.78 2 10 -9 14.10 1.62 2 10 -9 18.93 1.79 2 10 -9 18.91 1.75 2 10 -8 23.45 2.27 2 10 -8 31.59 2.63 2 10 -8 27.68 2.49 2 10 -8 32.96 2.65 -2 -10 8 37.59 2.98 2 10 -8 29.28 2.45 2 10 -8 30.88 2.49 2 10 -8 31.23 2.59 2 10 -7 129.50 8.40 2 10 -7 138.07 8.51 -2 -10 7 135.75 8.73 2 10 -7 133.22 8.47 2 10 -7 132.16 8.36 2 10 -6 1.64 0.67 2 10 -6 2.63 0.86 2 10 -6 0.99 0.67 -2 -10 6 1.65 0.91 2 10 -6 1.86 0.73 2 10 -6 3.20 0.83 2 10 -5 -0.13 0.65 -2 -10 5 0.18 0.81 2 10 -5 -0.15 0.60 2 10 -5 -0.15 0.58 2 10 -5 0.30 0.61 2 10 -4 285.36 16.73 2 10 -4 288.90 19.78 -2 -10 4 266.89 19.11 -2 -10 4 285.09 17.00 -2 -10 4 287.06 19.56 -2 -10 4 269.79 19.58 2 10 -4 287.31 16.84 2 10 -4 285.48 16.87 2 10 -4 280.45 16.83 2 10 -3 35.82 2.64 -2 -10 3 36.68 4.66 -2 -10 3 32.03 4.28 -2 -10 3 35.17 2.93 2 10 -3 38.06 2.85 2 10 -3 37.53 2.91 2 10 -3 30.51 4.54 2 10 -3 33.55 2.69 2 10 -2 66.27 4.31 2 10 -2 59.49 5.93 -2 -10 2 67.27 4.50 -2 -10 2 62.21 6.34 2 10 -2 63.15 4.34 -2 -10 2 68.04 4.63 2 10 -2 65.27 4.52 2 10 -2 55.72 6.30 -2 -10 2 58.04 6.25 -2 -10 1 10.39 2.56 2 10 -1 10.31 2.27 2 10 -1 7.18 0.99 -2 -10 1 9.19 1.22 -2 -10 1 9.47 2.24 -2 -10 1 11.60 2.58 -2 -10 1 6.45 1.19 2 10 -1 5.61 0.98 2 10 -1 8.53 1.18 2 10 -1 10.92 2.50 2 10 0 18.22 2.83 -2 -10 0 12.52 2.64 2 10 0 14.09 1.35 -2 -10 0 11.17 1.45 -2 -10 0 13.14 2.65 -2 -10 0 11.93 2.49 2 10 0 13.04 1.38 -2 -10 0 11.72 1.49 2 10 0 9.09 1.24 2 10 0 12.49 1.47 2 10 0 13.43 2.62 -2 -10 -1 5.43 2.03 2 10 1 10.03 1.11 2 10 1 6.51 1.96 -2 -10 -1 6.98 1.15 -2 -10 -1 6.41 2.10 -2 -10 -1 9.70 2.39 2 10 1 6.59 1.03 -2 -10 -1 7.10 1.20 2 10 1 5.16 0.97 2 10 1 6.56 1.99 -2 -10 -2 64.52 6.42 -2 -10 -2 60.98 4.45 2 10 2 66.85 4.32 2 10 2 69.02 6.22 -2 -10 -2 67.26 6.52 2 10 2 64.84 4.40 -2 -10 -2 67.80 4.59 -2 -10 -2 64.24 4.45 2 10 2 68.37 4.52 2 10 2 62.57 4.51 2 10 2 57.65 6.18 2 10 3 139.06 8.43 -2 -10 -3 125.88 10.63 -2 -10 -3 143.79 8.66 2 10 3 142.57 10.47 -2 -10 -3 136.83 10.95 2 10 3 135.34 8.51 -2 -10 -3 137.57 8.69 -2 -10 -3 143.39 8.66 2 10 3 140.65 8.63 2 10 3 134.80 8.66 2 10 3 129.21 10.72 -2 -10 -4 3.01 1.68 -2 -10 -4 0.54 1.45 2 10 4 2.76 0.70 -2 -10 -4 1.74 0.72 2 10 4 3.22 1.35 2 10 4 2.50 0.73 -2 -10 -4 1.50 0.75 2 10 4 1.57 0.72 -2 -10 -4 4.08 0.94 2 10 4 4.23 1.61 -2 -10 -4 1.18 1.41 -2 -10 -5 10.35 2.55 -2 -10 -5 13.02 2.79 2 10 5 11.47 1.46 -2 -10 -5 11.39 1.37 -2 -10 -5 12.88 1.53 2 10 5 11.81 1.36 -2 -10 -5 11.67 1.51 2 10 5 15.49 3.05 2 10 6 509.50 30.28 -2 -10 -6 534.24 30.59 2 10 6 555.17 33.88 2 10 6 483.28 32.31 -2 -10 -6 557.13 30.58 -2 -10 -6 570.87 33.87 -2 -10 -6 526.38 30.42 2 10 6 518.86 30.50 -2 -10 -6 522.53 30.41 -2 -10 -7 169.73 10.41 2 10 7 168.76 10.34 -2 -10 -7 162.14 10.25 -2 -10 -7 165.29 10.24 -2 -10 -7 168.71 10.37 -2 -10 -8 6.02 1.12 -2 -10 -8 6.10 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4.01 0.95 -2 -11 5 1.83 0.95 2 11 -5 0.16 0.65 2 11 -5 0.46 0.64 2 11 -5 0.92 0.70 -2 -11 4 45.24 3.48 2 11 -4 45.64 3.31 2 11 -4 41.38 3.26 2 11 -4 36.77 3.16 -2 -11 3 30.09 2.67 2 11 -3 28.03 2.49 2 11 -3 30.80 2.33 2 11 -3 25.61 2.38 -2 -11 2 46.59 3.70 2 11 -2 50.65 3.54 2 11 -2 45.15 3.38 -2 -11 2 47.35 3.59 2 11 -2 50.53 3.69 -2 -11 1 4.30 1.15 2 11 -1 3.17 0.85 2 11 -1 4.53 1.02 -2 -11 1 7.32 1.16 2 11 -1 3.67 1.61 2 11 -1 4.82 0.90 2 11 0 275.21 16.48 2 11 0 288.09 19.01 -2 -11 0 252.81 19.04 -2 -11 0 270.84 16.68 -2 -11 0 292.87 16.82 2 11 0 289.74 16.62 2 11 0 283.52 16.74 2 11 0 269.66 19.45 -2 -11 0 287.84 19.49 -2 -11 -1 13.95 2.96 2 11 1 11.80 1.34 2 11 1 15.17 2.80 -2 -11 -1 14.16 1.64 -2 -11 -1 10.28 2.58 -2 -11 -1 7.17 2.40 2 11 1 11.97 1.42 -2 -11 -1 13.34 1.65 2 11 1 10.51 1.44 2 11 1 14.07 2.95 -2 -11 -2 46.57 5.83 2 11 2 60.95 4.09 2 11 2 53.55 5.81 -2 -11 -2 58.83 4.29 -2 -11 -2 60.20 6.35 2 11 2 59.22 4.19 -2 -11 -2 62.44 4.40 -2 -11 -2 64.16 4.27 2 11 2 59.86 4.31 2 11 2 56.50 6.21 -2 -11 -3 98.32 6.45 2 11 3 95.37 6.23 2 11 3 91.77 8.22 -2 -11 -3 103.14 9.04 -2 -11 -3 97.20 6.44 2 11 3 101.47 6.48 2 11 3 94.00 6.45 -2 -11 -3 101.59 6.52 2 11 3 101.65 6.38 -2 -11 -4 25.89 2.24 -2 -11 -4 21.92 2.12 2 11 4 19.26 1.90 2 11 4 22.27 2.19 2 11 4 24.02 2.18 2 11 4 24.64 2.13 -2 -11 -4 23.27 2.23 -2 -11 -5 73.65 5.25 2 11 5 86.14 5.48 2 11 5 79.26 5.39 2 11 5 74.71 5.23 -2 -11 -5 83.54 5.49 -2 -11 -5 82.07 5.46 -2 -11 -6 3.17 0.94 2 11 6 5.03 1.03 -2 -11 -6 4.10 0.94 2 11 6 3.30 0.79 -2 -11 -6 3.43 1.02 -2 -11 -7 254.82 15.59 -2 -11 -7 243.52 15.45 2 11 7 288.96 15.70 -2 -11 -7 255.76 15.47 -2 -11 -7 261.72 15.60 -2 -11 -8 48.99 3.72 2 11 8 50.52 3.71 -2 -11 -8 50.45 3.66 -2 -11 -8 43.97 3.53 -2 -11 -8 50.97 3.72 -2 -11 -9 1.22 0.71 -2 -11 -9 4.89 1.01 -2 -11 -9 3.67 0.94 2 11 9 2.85 0.83 -2 -11 -9 2.78 0.83 -2 -11 -10 28.65 2.43 -2 -11 -10 31.13 2.46 2 11 10 30.21 2.49 -2 -11 -10 26.74 2.42 -2 -11 -10 25.63 2.32 -2 -11 -11 2.70 0.74 -2 -11 -11 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133.72 9.56 4 3 -7 129.85 9.33 4 3 -7 126.63 9.64 4 3 -7 130.91 7.72 -4 -3 7 136.42 7.93 -4 -3 7 147.74 10.34 -4 -3 7 137.48 10.06 4 3 -7 129.93 7.81 4 3 -7 105.84 7.65 -4 -3 7 141.55 10.20 4 3 -7 126.70 7.76 -4 -3 7 123.89 7.80 4 3 -6 107.66 6.18 -4 -3 6 102.50 6.29 -4 -3 6 92.05 7.67 -4 -3 6 100.32 8.10 4 3 -6 99.25 7.41 -4 -3 6 100.40 7.94 4 3 -6 89.89 7.70 4 3 -6 107.83 7.73 -4 -3 6 96.71 8.00 4 3 -6 93.11 6.15 4 3 -6 93.33 7.57 -4 -3 5 69.10 5.57 -4 -3 5 65.13 5.73 4 3 -5 59.44 5.04 -4 -3 5 48.38 5.16 4 3 -5 66.20 5.63 -4 -3 5 69.77 5.79 -4 -3 5 65.05 4.16 4 3 -5 64.96 4.05 -4 -3 5 56.32 5.26 4 3 -5 58.51 5.30 -4 -3 4 36.98 3.60 -4 -3 4 33.96 3.62 4 3 -4 34.64 3.25 -4 -3 4 28.93 3.31 4 3 -4 35.54 3.62 -4 -3 4 30.05 3.49 -4 -3 4 37.91 3.66 4 3 -4 30.08 2.27 -4 -3 4 33.58 2.39 4 3 -4 31.34 3.37 -4 -3 3 5.05 1.40 -4 -3 3 5.86 1.38 -4 -3 3 6.37 1.54 4 3 -3 5.38 1.19 4 3 -3 10.30 1.78 4 3 -3 5.61 1.24 -4 -3 3 3.91 1.25 -4 -3 3 7.16 0.85 -4 -3 3 7.82 1.64 4 3 -3 7.86 0.84 4 3 -3 9.37 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2.16 4 3 4 19.92 2.28 -4 -3 -4 15.89 2.08 4 3 4 14.84 2.19 4 3 4 17.75 2.31 -4 -3 -4 17.40 1.95 4 3 5 0.29 0.93 -4 -3 -5 0.35 0.39 -4 -3 -5 1.30 0.93 4 3 5 0.31 0.87 4 3 5 -0.31 0.75 -4 -3 -5 1.09 0.88 -4 -3 -5 0.72 0.39 4 3 5 0.59 0.93 4 3 6 -0.31 0.78 -4 -3 -6 0.15 0.38 4 3 6 1.00 0.98 -4 -3 -6 0.29 0.80 4 3 6 0.68 0.95 -4 -3 -6 0.24 0.67 4 3 6 1.31 1.13 4 3 7 14.07 2.11 -4 -3 -7 12.64 2.03 4 3 7 8.10 1.70 4 3 7 6.92 1.74 -4 -3 -8 50.75 3.59 -4 -3 -8 56.24 3.71 -4 -3 -8 54.96 3.60 -4 -3 -8 53.56 3.65 -4 -3 -8 53.58 4.88 -4 -3 -8 50.24 3.58 4 3 8 45.94 4.80 4 3 8 50.44 4.99 -4 -3 -9 1.86 0.61 -4 -3 -9 0.23 0.49 -4 -3 -9 -0.26 0.59 -4 -3 -9 0.62 0.60 -4 -3 -9 0.39 0.94 -4 -3 -9 0.12 0.50 4 3 9 0.44 1.18 4 3 9 0.46 0.95 -4 -3 -10 21.42 1.95 -4 -3 -10 18.74 1.96 -4 -3 -10 21.61 1.89 -4 -3 -10 21.01 1.98 -4 -3 -10 21.02 3.08 -4 -3 -10 23.24 1.97 4 3 10 18.46 3.04 4 3 10 16.65 3.00 -4 -3 -11 60.11 4.24 -4 -3 -11 56.94 4.27 -4 -3 -11 65.53 4.19 -4 -3 -11 59.85 4.29 -4 -3 -11 52.79 5.58 -4 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130.58 7.73 -4 -4 4 133.96 9.48 -4 -4 4 141.48 9.63 4 4 -4 136.45 8.85 -4 -4 4 117.10 9.17 4 4 -4 130.87 9.34 4 4 -4 130.27 9.24 4 4 -4 124.61 7.73 -4 -4 3 106.88 7.73 4 4 -3 106.65 6.14 -4 -4 3 100.86 6.22 -4 -4 3 106.35 7.72 -4 -4 3 93.29 7.30 -4 -4 3 102.15 7.64 4 4 -3 97.87 7.11 -4 -4 3 112.72 7.69 4 4 -3 104.28 7.59 4 4 -3 102.27 7.12 4 4 -3 111.58 7.65 4 4 -3 90.86 6.08 -4 -4 2 18.41 2.42 4 4 -2 13.22 1.15 -4 -4 2 12.26 1.21 -4 -4 2 11.71 2.00 -4 -4 2 12.93 1.92 -4 -4 2 14.49 2.01 -4 -4 2 11.84 1.90 -4 -4 2 13.60 2.07 4 4 -2 9.59 1.73 4 4 -2 15.95 1.96 4 4 -2 13.19 1.97 -4 -4 2 10.47 1.75 4 4 -2 13.12 1.97 -4 -4 1 1.77 1.20 4 4 -1 4.04 1.04 -4 -4 1 1.98 1.02 -4 -4 1 1.01 0.83 -4 -4 1 2.83 1.07 4 4 -1 1.46 0.88 -4 -4 1 1.60 0.96 4 4 -1 2.77 0.91 4 4 -1 2.43 0.94 -4 -4 1 1.21 0.96 -4 -4 0 52.21 4.90 4 4 0 63.10 4.86 4 4 0 59.46 4.72 -4 -4 0 56.41 4.81 -4 -4 0 58.25 4.94 4 4 0 55.17 4.65 -4 -4 0 62.46 4.76 4 4 0 67.29 4.81 4 4 0 65.12 4.92 -4 -4 -1 259.33 17.08 4 4 1 280.62 17.03 4 4 1 283.41 17.04 -4 -4 -1 279.13 17.22 4 4 1 266.62 16.94 4 4 1 278.74 17.01 4 4 1 285.62 17.20 4 4 2 20.62 2.42 -4 -4 -2 21.97 2.55 -4 -4 -2 21.56 2.50 4 4 2 22.81 2.51 4 4 2 23.58 2.60 -4 -4 -2 19.94 2.41 4 4 2 25.39 2.73 4 4 3 222.88 14.38 4 4 3 235.32 14.41 -4 -4 -3 222.58 14.55 4 4 3 255.26 14.98 4 4 3 228.33 14.47 -4 -4 -3 215.64 14.27 4 4 3 231.65 14.63 -4 -4 -4 65.37 4.17 4 4 4 64.95 5.11 -4 -4 -4 63.82 5.25 4 4 4 74.80 5.49 -4 -4 -4 71.31 5.23 4 4 4 68.77 5.46 4 4 4 62.66 5.36 -4 -4 -4 65.47 4.09 4 4 5 42.32 3.91 -4 -4 -5 39.38 3.70 4 4 5 43.01 4.04 -4 -4 -5 44.33 2.84 4 4 5 39.46 3.97 -4 -4 -5 40.17 2.72 4 4 6 86.71 6.30 -4 -4 -6 78.77 6.11 4 4 6 68.74 6.15 -4 -4 -6 80.81 4.97 4 4 6 71.35 6.21 -4 -4 -6 79.58 4.85 4 4 6 72.73 6.39 4 4 6 84.09 6.34 4 4 7 219.56 12.95 -4 -4 -7 207.71 12.70 4 4 7 168.43 12.67 -4 -4 -7 188.61 11.05 4 4 7 163.12 12.71 -4 -4 -8 207.24 12.50 -4 -4 -8 198.20 12.54 -4 -4 -8 215.59 12.50 -4 -4 -8 244.68 14.26 -4 -4 -8 215.71 12.60 -4 -4 -8 212.66 12.54 4 4 8 228.43 14.17 -4 -4 -8 206.83 12.51 4 4 8 186.92 14.05 4 4 8 205.62 14.44 -4 -4 -9 23.20 1.96 -4 -4 -9 20.64 1.95 -4 -4 -9 19.83 1.83 -4 -4 -9 19.31 1.86 -4 -4 -9 25.03 3.12 4 4 9 26.53 3.21 -4 -4 -9 19.83 1.86 4 4 9 20.13 3.01 4 4 9 19.58 3.18 -4 -4 -10 20.14 1.88 -4 -4 -10 18.87 1.92 -4 -4 -10 18.56 1.78 -4 -4 -10 19.41 1.90 -4 -4 -10 25.07 3.26 -4 -4 -10 22.66 1.97 4 4 10 19.50 3.06 4 4 10 15.09 3.03 -4 -4 -11 30.48 2.57 -4 -4 -11 29.72 2.63 -4 -4 -11 31.35 2.47 -4 -4 -11 29.77 2.60 4 4 11 30.37 4.07 -4 -4 -11 29.20 3.81 -4 -4 -11 30.38 2.57 4 4 11 28.78 3.98 4 4 11 28.38 4.17 -4 -4 -12 16.10 1.88 -4 -4 -12 17.67 1.86 -4 -4 -12 20.27 2.01 -4 -4 -12 18.82 1.91 -4 -4 -13 22.21 2.25 -4 -4 -13 23.80 2.28 -4 -4 -13 24.14 2.21 -4 -4 -14 0.48 0.81 -4 -4 -14 0.65 0.71 -4 -4 -14 0.45 0.66 -4 -4 -15 32.32 2.57 -4 -4 -15 27.63 2.47 -4 -4 -15 27.36 2.39 -4 -4 -16 21.76 1.82 -4 -4 -16 17.58 1.82 -4 -4 -17 3.61 0.68 -4 -4 -17 3.97 0.76 4 5 -15 12.61 1.33 4 5 -15 16.16 1.37 4 5 -14 0.35 0.61 4 5 -14 0.22 0.55 4 5 -14 0.12 0.58 -4 -5 14 0.13 0.58 -4 -5 13 32.06 2.98 4 5 -13 40.47 3.04 4 5 -13 40.46 3.00 4 5 -13 39.28 3.01 4 5 -13 42.17 3.02 -4 -5 12 71.05 4.97 4 5 -12 73.78 4.90 4 5 -12 65.54 4.80 4 5 -12 72.80 4.85 4 5 -12 65.82 4.70 4 5 -12 74.43 4.88 -4 -5 11 1.68 0.88 4 5 -11 3.42 0.89 4 5 -11 4.03 0.84 4 5 -11 1.79 0.78 -4 -5 10 8.54 1.30 4 5 -10 8.10 1.16 4 5 -10 7.77 1.22 4 5 -10 9.00 1.27 4 5 -9 74.40 4.93 -4 -5 9 74.94 5.13 4 5 -9 72.47 5.05 -4 -5 9 77.64 7.76 -4 -5 9 78.61 7.79 4 5 -9 72.38 5.04 4 5 -9 76.63 5.09 -4 -5 8 5.45 0.97 4 5 -8 3.92 0.84 -4 -5 8 3.13 1.84 -4 -5 8 3.85 1.72 4 5 -8 3.58 0.80 4 5 -8 3.76 0.89 4 5 -8 3.16 0.83 4 5 -7 27.76 3.82 -4 -5 7 32.77 2.61 4 5 -7 34.44 2.52 -4 -5 7 38.50 4.65 -4 -5 7 40.10 4.68 4 5 -7 30.74 2.52 -4 -5 7 29.12 4.02 4 5 -7 34.44 2.53 4 5 -7 30.50 2.53 4 5 -6 350.85 21.07 -4 -5 6 339.43 21.23 4 5 -6 330.80 18.83 -4 -5 6 323.68 18.94 -4 -5 6 334.52 21.44 -4 -5 6 312.10 21.19 4 5 -6 310.28 18.85 -4 -5 6 309.75 18.87 -4 -5 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4.69 -5 -5 7 32.41 4.69 -5 -5 7 41.15 4.97 5 5 -7 37.39 2.89 5 5 -7 33.46 4.27 5 5 -7 41.25 2.97 5 5 -6 28.75 4.11 -5 -5 6 33.34 4.36 5 5 -6 41.85 2.87 -5 -5 6 38.04 2.96 -5 -5 6 41.40 4.92 -5 -5 6 46.74 4.95 -5 -5 6 35.39 2.83 -5 -5 6 33.20 4.39 5 5 -6 39.88 2.89 5 5 -6 37.80 4.31 5 5 -6 37.11 2.83 5 5 -5 15.63 2.59 -5 -5 5 7.69 2.01 5 5 -5 8.60 1.14 -5 -5 5 11.40 1.31 -5 -5 5 9.23 2.16 -5 -5 5 7.43 2.13 -5 -5 5 10.14 1.21 -5 -5 5 7.16 2.06 5 5 -5 11.56 1.26 5 5 -5 13.51 2.38 5 5 -5 11.39 1.21 5 5 -4 9.76 2.16 -5 -5 4 8.53 1.12 -5 -5 4 10.20 2.17 5 5 -4 6.04 0.95 -5 -5 4 5.26 1.62 -5 -5 4 5.27 1.76 -5 -5 4 6.57 0.98 -5 -5 4 8.52 2.04 5 5 -4 9.17 1.06 5 5 -4 10.26 2.05 5 5 -4 8.53 1.01 5 5 -3 280.46 17.32 -5 -5 3 264.08 17.40 5 5 -3 272.01 15.20 -5 -5 3 257.82 15.29 -5 -5 3 249.75 17.14 5 5 -3 241.92 16.44 -5 -5 3 239.15 16.87 -5 -5 3 250.36 15.26 -5 -5 3 262.36 17.31 5 5 -3 264.98 15.25 5 5 -3 270.12 17.15 5 5 -2 53.98 4.73 -5 -5 2 53.38 3.63 -5 -5 2 50.53 5.08 5 5 -2 54.12 3.53 -5 -5 2 55.60 5.24 5 5 -2 46.65 4.86 5 5 -2 51.84 3.46 5 5 -2 59.66 5.23 -5 -5 2 58.49 5.07 5 5 -2 50.82 4.70 5 5 -1 9.87 1.83 -5 -5 1 8.15 1.90 -5 -5 1 8.61 1.02 5 5 -1 7.16 0.87 -5 -5 1 8.56 1.93 5 5 -1 6.52 1.78 5 5 -1 8.08 1.71 5 5 -1 9.25 0.96 -5 -5 1 5.42 1.46 5 5 -1 7.31 1.80 -5 -5 0 29.45 2.19 -5 -5 0 29.99 3.46 5 5 0 26.66 3.11 5 5 0 29.75 3.16 5 5 0 27.07 2.07 5 5 0 24.18 3.11 5 5 0 27.26 3.14 -5 -5 0 31.54 3.49 5 5 1 11.54 1.89 -5 -5 -1 6.53 1.70 -5 -5 -1 8.32 1.04 -5 -5 -1 11.07 1.97 5 5 1 9.26 1.86 5 5 1 10.48 1.05 -5 -5 -1 9.86 1.89 5 5 1 8.81 1.83 5 5 1 8.81 1.77 5 5 2 3.60 1.23 -5 -5 -2 3.08 1.21 -5 -5 -2 4.05 0.76 -5 -5 -2 5.14 1.44 5 5 2 4.65 0.74 5 5 2 5.91 1.56 -5 -5 -2 5.42 1.44 5 5 2 5.39 1.59 -5 -5 -3 126.77 7.66 5 5 3 128.80 7.59 5 5 3 139.49 9.21 -5 -5 -3 112.71 9.06 -5 -5 -3 113.24 8.79 5 5 3 127.23 9.10 5 5 3 128.64 9.34 -5 -5 -4 7.72 1.59 5 5 4 9.48 1.94 -5 -5 -4 7.35 0.91 5 5 4 4.67 1.49 -5 -5 -4 5.79 0.80 5 5 4 5.65 1.52 -5 -5 -4 3.34 1.26 5 5 4 5.90 0.80 -5 -5 -5 12.23 1.18 -5 -5 -5 10.71 1.18 -5 -5 -5 8.43 1.13 5 5 5 10.16 1.95 5 5 5 12.06 2.22 -5 -5 -5 9.02 1.79 5 5 5 8.99 1.98 -5 -5 -5 9.43 1.01 -5 -5 -5 8.12 1.10 -5 -5 -6 0.99 0.55 5 5 6 -0.44 0.91 -5 -5 -6 0.35 0.84 5 5 6 1.62 1.27 -5 -5 -6 1.71 0.63 -5 -5 -6 0.35 0.58 5 5 6 2.75 1.24 -5 -5 -6 0.49 0.51 5 5 6 0.45 1.07 -5 -5 -6 0.66 0.53 -5 -5 -7 96.12 8.04 5 5 7 108.09 8.67 -5 -5 -7 113.03 6.94 -5 -5 -7 108.62 6.85 -5 -5 -7 98.07 6.79 5 5 7 130.43 8.90 -5 -5 -7 106.08 6.89 -5 -5 -7 100.50 6.71 -5 -5 -7 112.07 6.85 -5 -5 -7 119.36 6.71 5 5 7 99.06 8.55 -5 -5 -7 108.85 6.64 -5 -5 -8 64.24 4.60 -5 -5 -8 69.57 4.54 -5 -5 -8 74.49 6.11 5 5 8 62.48 6.20 -5 -5 -8 68.05 4.64 -5 -5 -8 63.12 4.49 -5 -5 -8 64.51 4.54 5 5 8 72.56 6.33 -5 -5 -8 66.32 4.50 5 5 8 61.69 6.19 -5 -5 -8 67.77 4.34 -5 -5 -9 46.04 3.58 -5 -5 -9 46.55 3.45 -5 -5 -9 52.65 5.03 5 5 9 48.02 5.31 -5 -5 -9 53.67 3.68 -5 -5 -9 45.76 3.46 -5 -5 -9 47.13 3.55 -5 -5 -9 44.85 3.45 5 5 9 47.83 5.23 -5 -5 -10 11.73 1.40 -5 -5 -10 11.04 1.49 5 5 10 7.82 2.28 -5 -5 -10 7.05 1.90 -5 -5 -10 11.18 1.49 5 5 10 9.11 2.32 -5 -5 -10 9.64 1.29 -5 -5 -10 11.47 1.47 -5 -5 -11 32.80 2.85 -5 -5 -11 28.24 2.80 -5 -5 -11 37.13 2.79 -5 -5 -11 36.45 2.83 -5 -5 -12 39.48 3.16 -5 -5 -12 36.50 3.12 -5 -5 -12 39.21 2.98 -5 -5 -12 35.06 3.00 -5 -5 -13 10.22 1.47 -5 -5 -13 11.40 1.51 -5 -5 -13 11.36 1.47 -5 -5 -14 -0.31 0.81 -5 -5 -14 -0.16 0.66 -5 -5 -14 -0.14 0.60 -5 -5 -15 64.67 4.52 -5 -5 -15 64.30 4.52 -5 -5 -15 67.32 4.48 -5 -5 -16 28.10 2.25 -5 -5 -16 24.34 2.15 -5 -5 -16 30.29 2.22 -5 -5 -17 2.48 0.59 -5 -5 -17 3.80 0.62 5 6 -14 27.80 2.20 5 6 -14 31.87 2.24 5 6 -14 29.14 2.20 5 6 -13 22.48 1.87 -5 -6 13 17.78 1.85 5 6 -13 22.10 1.90 5 6 -13 21.78 1.87 5 6 -13 21.66 1.79 5 6 -12 3.27 0.77 5 6 -12 2.46 0.82 5 6 -12 1.28 0.63 5 6 -12 1.65 0.60 5 6 -12 2.45 0.70 -5 -6 12 1.62 0.71 5 6 -11 20.94 1.96 5 6 -11 20.34 1.95 5 6 -11 19.00 1.84 -5 -6 11 19.73 2.03 5 6 -10 46.93 3.51 5 6 -10 44.24 3.38 5 6 -10 45.21 3.46 -5 -6 10 47.69 3.52 5 6 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3.72 5 6 -4 50.97 5.23 5 6 -4 54.32 3.69 5 6 -3 3.15 1.33 -5 -6 3 5.10 0.87 -5 -6 3 2.02 1.43 5 6 -3 4.74 0.78 -5 -6 3 2.24 1.48 -5 -6 3 5.14 1.59 -5 -6 3 3.30 0.74 -5 -6 3 4.15 1.42 5 6 -3 4.23 0.79 5 6 -3 3.54 1.31 5 6 -2 61.81 3.75 5 6 -2 60.19 5.54 5 6 -2 67.64 5.30 -5 -6 2 56.02 5.30 -5 -6 2 57.16 3.86 -5 -6 2 47.05 5.33 5 6 -2 56.76 3.73 -5 -6 2 55.70 5.45 -5 -6 2 56.91 5.38 -5 -6 2 49.84 3.78 -5 -6 2 53.85 5.39 5 6 -2 59.44 3.88 5 6 -2 46.79 5.11 -5 -6 1 51.24 5.10 -5 -6 1 61.01 5.61 5 6 -1 59.23 3.80 5 6 -1 68.11 5.70 5 6 -1 55.87 5.09 -5 -6 1 60.20 5.43 5 6 -1 54.93 3.87 -5 -6 1 59.45 3.91 -5 -6 1 58.95 5.59 5 6 0 14.82 2.16 5 6 0 12.71 2.16 5 6 0 14.23 1.29 -5 -6 0 13.46 2.40 5 6 0 16.09 2.47 -5 -6 0 12.91 1.34 -5 -6 0 11.73 2.22 5 6 1 62.91 5.36 -5 -6 -1 63.27 5.36 -5 -6 -1 60.63 5.60 5 6 1 61.78 3.99 5 6 1 66.11 5.44 -5 -6 -1 58.16 4.06 -5 -6 -1 70.70 5.76 5 6 1 63.61 5.57 5 6 2 204.08 13.21 -5 -6 -2 183.40 12.97 5 6 2 194.07 13.24 -5 -6 -2 194.66 13.30 -5 -6 -2 181.29 11.63 -5 -6 -2 198.13 11.56 -5 -6 -2 203.52 13.63 5 6 2 211.92 11.63 5 6 2 208.02 13.27 -5 -6 -3 12.31 2.16 5 6 3 20.91 2.95 -5 -6 -3 19.08 1.63 5 6 3 14.69 2.47 -5 -6 -3 17.19 1.51 5 6 3 21.16 2.72 5 6 3 20.29 1.58 -5 -6 -3 18.59 2.79 5 6 4 30.82 2.21 -5 -6 -4 26.53 3.36 -5 -6 -4 28.61 2.29 5 6 4 30.98 3.46 -5 -6 -4 27.57 2.20 -5 -6 -4 27.57 2.27 -5 -6 -4 29.63 2.35 5 6 4 34.66 3.69 -5 -6 -4 24.25 3.09 5 6 4 25.65 3.37 5 6 4 36.20 3.69 -5 -6 -4 31.35 2.20 -5 -6 -4 28.92 2.30 -5 -6 -5 155.64 8.71 5 6 5 135.91 10.21 -5 -6 -5 120.23 9.72 5 6 5 138.25 10.45 -5 -6 -5 134.43 8.71 -5 -6 -5 133.07 8.71 5 6 5 157.76 10.57 5 6 5 129.69 10.37 -5 -6 -5 153.72 8.58 -5 -6 -5 145.39 8.76 -5 -6 -6 9.17 1.13 5 6 6 7.24 1.84 -5 -6 -6 7.78 1.19 5 6 6 9.69 2.18 -5 -6 -6 9.67 1.21 -5 -6 -6 9.52 1.14 5 6 6 5.23 1.65 -5 -6 -6 7.59 1.10 5 6 6 5.65 1.87 -5 -6 -6 7.01 0.94 5 6 7 14.83 2.83 -5 -6 -7 22.05 2.04 5 6 7 23.75 3.24 -5 -6 -7 19.88 1.90 -5 -6 -7 20.08 1.90 -5 -6 -7 20.51 1.96 -5 -6 -7 21.07 1.79 5 6 7 24.81 3.44 -5 -6 -7 22.53 1.81 5 6 8 6.60 1.85 -5 -6 -8 7.32 1.19 -5 -6 -8 6.24 1.05 -5 -6 -8 5.68 1.08 -5 -6 -8 5.05 0.99 -5 -6 -8 8.13 1.23 -5 -6 -8 7.27 1.08 -5 -6 -8 6.73 0.97 5 6 8 4.19 1.63 -5 -6 -9 148.49 9.33 -5 -6 -9 151.17 9.21 5 6 9 135.97 11.23 5 6 9 151.32 11.37 -5 -6 -9 140.71 9.32 -5 -6 -9 138.46 9.17 -5 -6 -9 145.58 9.23 5 6 9 145.10 11.10 -5 -6 -9 150.33 9.24 -5 -6 -9 166.84 9.10 5 6 9 132.41 11.23 -5 -6 -10 7.59 1.17 -5 -6 -10 8.40 1.34 5 6 10 9.01 2.18 5 6 10 3.40 1.70 -5 -6 -10 7.11 1.24 5 6 10 9.33 2.29 -5 -6 -10 7.35 1.22 -5 -6 -10 7.89 1.31 -5 -6 -11 20.02 2.12 -5 -6 -11 24.90 2.34 -5 -6 -11 22.31 2.08 -5 -6 -11 23.29 2.14 -5 -6 -11 22.69 2.25 -5 -6 -12 -0.48 0.78 -5 -6 -12 -0.27 0.58 -5 -6 -12 -0.18 0.77 -5 -6 -12 0.31 0.64 -5 -6 -13 108.81 7.07 -5 -6 -13 101.64 7.07 -5 -6 -13 113.81 7.06 -5 -6 -14 3.79 1.01 -5 -6 -14 6.97 1.17 -5 -6 -14 5.92 1.03 -5 -6 -15 0.38 0.62 -5 -6 -15 0.27 0.62 -5 -6 -15 0.48 0.56 -5 -6 -16 38.18 2.79 -5 -6 -16 43.76 2.83 -5 -6 -16 33.80 2.74 -5 -6 -17 15.05 1.27 5 7 -14 14.12 1.25 5 7 -14 12.85 1.23 5 7 -14 15.20 1.26 5 7 -13 11.15 1.27 5 7 -13 13.17 1.27 5 7 -13 13.33 1.34 5 7 -13 14.57 1.36 5 7 -12 28.89 2.35 5 7 -12 31.38 2.34 5 7 -12 27.69 2.32 5 7 -12 26.59 2.28 5 7 -11 12.41 1.44 5 7 -11 12.13 1.38 5 7 -11 10.88 1.30 5 7 -11 11.24 1.36 5 7 -11 9.68 1.25 5 7 -10 68.54 4.68 5 7 -10 71.58 4.63 5 7 -10 66.66 4.56 -5 -7 10 61.61 4.65 5 7 -10 61.76 4.59 -5 -7 10 66.73 4.67 5 7 -10 69.21 4.59 5 7 -9 6.00 1.06 5 7 -9 9.01 1.26 5 7 -9 7.23 1.12 -5 -7 9 6.45 1.14 5 7 -9 6.00 1.06 5 7 -9 6.40 1.06 5 7 -9 5.11 0.97 -5 -7 8 0.16 0.68 5 7 -8 -0.27 0.65 5 7 -8 -0.30 0.66 5 7 -8 0.30 0.61 5 7 -8 0.30 0.57 5 7 -8 -0.55 0.60 -5 -7 7 2.71 2.06 -5 -7 7 4.31 2.01 -5 -7 7 1.23 0.78 -5 -7 7 -0.67 1.39 5 7 -7 1.59 0.77 5 7 -7 2.14 0.71 -5 -7 7 0.45 0.65 5 7 -7 0.80 0.68 5 7 -7 0.71 0.60 5 7 -7 1.46 0.63 5 7 -6 6.12 1.90 -5 -7 6 2.54 1.63 -5 -7 6 10.77 2.67 -5 -7 6 6.74 1.08 -5 -7 6 6.52 2.22 5 7 -6 5.15 0.96 5 7 -6 5.10 0.92 -5 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1.24 -10 -7 0 7.20 1.09 10 7 0 8.17 1.07 10 7 0 8.03 1.07 -10 -7 0 8.51 1.07 -10 -7 0 6.94 1.02 -10 -7 -1 0.76 0.64 10 7 1 0.32 0.62 10 7 1 0.80 0.54 -10 -7 -1 1.21 0.59 -10 -7 -1 0.11 0.57 -10 -7 -2 -0.38 0.60 -10 -7 -2 -0.11 0.47 10 7 2 -0.66 0.63 10 7 2 1.01 0.56 -10 -7 -2 -0.34 0.55 -10 -7 -2 0.22 0.54 -10 -7 -3 3.83 0.81 -10 -7 -3 2.70 0.75 10 7 3 3.19 0.76 -10 -7 -3 1.83 0.64 -10 -7 -3 3.62 0.79 -10 -7 -4 4.80 0.90 -10 -7 -4 2.87 0.85 10 7 4 4.86 0.87 -10 -7 -4 4.07 0.81 -10 -7 -4 3.45 0.79 -10 -7 -5 139.29 8.40 -10 -7 -5 142.67 8.47 10 7 5 141.92 8.34 -10 -7 -5 133.92 8.34 -10 -7 -5 126.18 8.27 -10 -7 -6 1.38 0.64 10 7 6 0.32 0.55 -10 -7 -6 0.61 0.55 -10 -7 -6 1.34 0.63 -10 -7 -6 1.55 0.57 -10 -7 -6 1.12 0.56 10 7 7 0.73 0.56 -10 -7 -7 0.74 0.45 -10 -7 -7 -0.62 0.52 -10 -7 -7 -0.11 0.50 -10 -7 -8 6.82 0.94 -10 -7 -8 8.03 1.01 10 7 8 9.53 1.09 -10 -7 -9 -0.36 0.44 10 7 9 0.09 0.46 -10 -7 -10 3.72 0.64 -10 -7 -11 1.49 0.44 -10 -8 6 0.44 0.40 -10 -8 5 0.60 0.44 10 8 -5 0.36 0.43 10 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60.15 4.33 11 3 2 1.99 0.55 -11 -3 -2 2.69 0.60 -11 -3 -2 2.68 0.59 11 3 3 5.18 0.79 -11 -3 -3 8.29 0.92 -11 -3 -3 8.63 0.93 -11 -3 -3 8.02 0.93 -11 -3 -4 10.38 1.05 -11 -3 -4 10.36 1.07 -11 -3 -4 9.38 1.00 -11 -3 -5 11.12 1.15 -11 -3 -5 13.30 1.20 -11 -3 -5 12.04 1.13 -11 -3 -6 1.46 0.49 -11 -3 -6 1.57 0.52 -11 -3 -7 10.76 1.02 -11 -4 4 -0.06 0.32 11 4 -4 -0.06 0.33 -11 -4 3 3.68 0.59 11 4 -3 3.04 0.55 11 4 -2 93.68 5.69 11 4 -2 91.72 5.64 -11 -4 1 44.95 2.93 11 4 -1 43.00 2.99 11 4 0 56.20 3.95 11 4 0 57.13 3.92 -11 -4 0 59.64 3.98 -11 -4 -1 1.00 0.49 -11 -4 -1 1.52 0.50 -11 -4 -1 0.74 0.44 11 4 1 1.30 0.48 -11 -4 -1 0.90 0.51 11 4 2 -0.08 0.42 -11 -4 -2 0.89 0.46 -11 -4 -2 0.73 0.48 -11 -4 -2 0.59 0.46 11 4 3 0.33 0.43 -11 -4 -3 0.26 0.48 -11 -4 -3 0.49 0.43 -11 -4 -3 0.65 0.45 -11 -4 -3 0.26 0.45 11 4 4 0.16 0.47 -11 -4 -4 1.03 0.54 -11 -4 -4 0.57 0.50 -11 -4 -4 0.63 0.46 -11 -4 -4 1.10 0.51 -11 -4 -5 23.72 1.78 -11 -4 -5 21.71 1.76 -11 -4 -5 22.22 1.72 -11 -4 -5 20.70 1.72 -11 -4 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-2 6.06 0.78 -11 -6 1 4.38 0.71 11 6 -1 4.09 0.68 11 6 0 -0.16 0.42 -11 -6 0 -0.17 0.44 11 6 0 -0.62 0.52 -11 -6 0 0.30 0.43 -11 -6 -1 2.13 0.56 -11 -6 -1 2.48 0.59 11 6 1 2.35 0.58 -11 -6 -1 2.10 0.56 -11 -6 -2 11.69 1.23 -11 -6 -2 13.44 1.28 11 6 2 13.82 1.27 -11 -6 -2 14.98 1.30 -11 -6 -3 16.75 1.56 -11 -6 -3 20.86 1.61 -11 -6 -3 18.34 1.61 11 6 3 19.00 1.59 -11 -6 -3 18.63 1.59 -11 -6 -3 21.41 1.65 -11 -6 -4 13.85 1.19 -11 -6 -4 12.38 1.20 -11 -6 -4 13.62 1.22 -11 -6 -4 15.52 1.30 11 6 4 11.47 1.16 -11 -6 -5 36.52 2.67 -11 -6 -5 42.68 2.78 -11 -6 -5 37.41 2.64 -11 -6 -5 40.42 2.72 -11 -6 -6 331.38 19.93 -11 -6 -6 362.09 20.03 -11 -6 -6 351.85 19.97 -11 -6 -7 11.98 1.14 -11 -6 -7 11.51 1.11 -11 -6 -8 56.00 3.55 -11 -6 -8 55.90 3.58 11 7 -4 0.64 0.35 11 7 -3 0.59 0.40 -11 -7 3 0.67 0.39 11 7 -2 3.03 0.58 11 7 -1 11.54 1.12 11 7 0 -0.16 0.42 -11 -7 0 -0.16 0.48 -11 -7 0 0.07 0.40 -11 -7 -1 2.56 0.60 -11 -7 -1 3.81 0.70 11 7 1 3.38 0.61 -11 -7 -1 4.02 0.65 11 7 1 3.22 0.64 -11 -7 -2 6.53 0.86 -11 -7 -2 7.75 0.90 11 7 2 6.35 0.83 -11 -7 -2 4.36 0.77 -11 -7 -3 1.41 0.53 -11 -7 -3 1.20 0.50 11 7 3 0.96 0.48 -11 -7 -3 1.52 0.50 -11 -7 -3 1.15 0.52 -11 -7 -4 132.98 8.98 -11 -7 -4 158.66 9.09 -11 -7 -4 161.54 9.11 -11 -7 -4 153.63 9.05 11 7 4 157.85 9.05 -11 -7 -5 59.42 3.73 -11 -7 -5 52.58 3.62 -11 -7 -5 57.93 3.68 -11 -7 -6 29.22 2.13 -11 -7 -6 27.25 2.05 -11 -7 -6 30.68 2.11 -11 -7 -7 103.52 6.73 -11 -7 -7 122.10 6.79 -11 -7 -8 3.30 0.56 -11 -7 -8 3.65 0.55 11 8 -3 10.20 0.95 11 8 -2 6.91 0.79 11 8 -1 0.58 0.41 11 8 0 -0.08 0.46 -11 -8 -1 3.35 0.62 11 8 1 4.45 0.65 -11 -8 -2 5.72 0.76 11 8 2 4.74 0.70 -11 -8 -2 6.17 0.79 11 8 2 4.64 0.72 -11 -8 -3 2.06 0.55 -11 -8 -3 3.10 0.61 11 8 3 2.66 0.57 -11 -8 -3 3.14 0.58 -11 -8 -4 2.28 0.56 -11 -8 -4 2.26 0.54 -11 -8 -4 1.36 0.49 -11 -8 -5 2.95 0.62 -11 -8 -5 3.00 0.59 -11 -8 -5 4.03 0.65 -11 -8 -6 12.38 1.17 -11 -8 -6 12.00 1.12 -11 -8 -6 13.95 1.23 -11 -8 -6 13.04 1.15 -11 -8 -7 4.59 0.64 -11 -8 -7 4.51 0.67 -11 -8 -8 0.43 0.33 11 9 -2 0.06 0.35 11 9 -1 0.13 0.36 11 9 0 22.75 1.71 -11 -9 -1 -0.07 0.36 11 9 1 -0.21 0.36 -11 -9 -2 1.62 0.50 11 9 2 1.78 0.46 -11 -9 -3 22.89 1.66 -11 -9 -3 21.07 1.63 11 9 3 18.42 1.55 -11 -9 -4 0.45 0.38 -11 -9 -4 0.07 0.38 -11 -9 -5 1.68 0.48 -11 -9 -5 2.17 0.48 -11 -9 -5 1.32 0.47 -11 -9 -6 -0.20 0.33 -11 -9 -6 0.40 0.37 -11 -9 -6 0.12 0.33 -11 -9 -7 1.69 0.40 -11 -9 -7 1.49 0.44 11 10 0 15.05 1.22 11 10 1 21.37 1.48 -11 -10 -1 16.01 1.38 11 10 2 9.16 0.91 -11 -10 -2 10.09 0.94 11 10 3 1.72 0.44 -11 -10 -3 2.96 0.54 -11 -10 -3 3.45 0.53 -11 -10 -4 3.03 0.53 -11 -10 -4 2.54 0.50 -11 -10 -5 7.19 0.78 -11 -10 -5 7.72 0.81 0 0 0 0.00 0.00 TITL AB_DGJ_08SCM_auto in P-1 REM P-1 (#2 in standard setting) CELL 1.54184 9.835918 13.219830 15.256584 85.4513 82.6726 69.4225 ZERR 35.00 0.000155 0.000255 0.000234 0.0014 0.0013 0.0016 LATT 1 SFAC C H N O UNIT 35.00 35.00 35.00 35.00 REM CrysAlisPro recorded range (K): Min=99.9; max=100.1; aver:100.0 TEMP -173 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 5695 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.439 _oxdiff_exptl_absorpt_empirical_full_min 0.746 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O001 O 0.81728(10) 0.04707(7) 0.14948(6) 0.0330(2) Uani 1 1 d . . . . . O002 O 0.29219(10) 0.11292(7) 0.21256(7) 0.0363(2) Uani 1 1 d . . . . . N003 N 0.53849(12) 0.39246(9) 0.28886(7) 0.0309(3) Uani 1 1 d . . . . . H003 H 0.520687 0.374240 0.344736 0.037 Uiso 1 1 calc R U . . . N004 N 0.19943(12) 0.43710(10) 0.37812(8) 0.0330(3) Uani 1 1 d . . . . . H004 H 0.182244 0.489658 0.337318 0.040 Uiso 1 1 calc R U . . . C12 C 0.61442(13) 0.32096(11) 0.22288(9) 0.0280(3) Uani 1 1 d . . . . . C24 C 0.25131(13) 0.28034(10) 0.28234(9) 0.0275(3) Uani 1 1 d . . . . . C2 C 0.74950(13) 0.15701(11) 0.15221(9) 0.0286(3) Uani 1 1 d . . . . . C1 C 0.67623(13) 0.20872(11) 0.22948(8) 0.0283(3) Uani 1 1 d . . . . . C37 C 0.24519(13) 0.34313(10) 0.19500(8) 0.0273(3) Uani 1 1 d . . . . . H37 H 0.289220 0.400270 0.197836 0.033 Uiso 1 1 calc R U . . . C35 C 0.23396(13) 0.32852(11) 0.36332(9) 0.0295(3) Uani 1 1 d . . . . . C11 C 0.61993(13) 0.38038(11) 0.14264(9) 0.0292(3) Uani 1 1 d . . . . . C3 C 0.75858(13) 0.21356(11) 0.06992(9) 0.0296(3) Uani 1 1 d . . . . . C14 C 0.66517(14) 0.14330(11) 0.31441(9) 0.0300(3) Uani 1 1 d . . . . . H14 H 0.570586 0.180339 0.350476 0.036 Uiso 1 1 calc R U . . . C43 C 0.09021(13) 0.39522(11) 0.16949(8) 0.0279(3) Uani 1 1 d . . . . . C4 C 0.69336(14) 0.32428(11) 0.06635(9) 0.0302(3) Uani 1 1 d . . . . . H4 H 0.698055 0.363238 0.011652 0.036 Uiso 1 1 calc R U . . . C9 C 0.49528(14) 0.49679(11) 0.25292(9) 0.0319(3) Uani 1 1 d . . . . . C10 C 0.54416(14) 0.49330(11) 0.16172(9) 0.0314(3) Uani 1 1 d . . . . . C25 C 0.28028(14) 0.16947(11) 0.28651(9) 0.0309(3) Uani 1 1 d . . . . . C44 C 0.03155(14) 0.49940(11) 0.14443(9) 0.0305(3) Uani 1 1 d . . . . . C38 C 0.33529(14) 0.26315(11) 0.12439(9) 0.0319(3) Uani 1 1 d . . . . . H38A H 0.329376 0.300127 0.065240 0.038 Uiso 1 1 calc R U . . . H38B H 0.439018 0.234114 0.136041 0.038 Uiso 1 1 calc R U . . . C15 C 0.66806(14) 0.03337(11) 0.28765(9) 0.0324(3) Uani 1 1 d . . . . . H15A H 0.662142 -0.013066 0.341150 0.039 Uiso 1 1 calc R U . . . H15B H 0.582940 0.043184 0.255309 0.039 Uiso 1 1 calc R U . . . C42 C 0.01882(14) 0.31051(11) 0.16957(9) 0.0327(3) Uani 1 1 d . . . . . H42A H -0.077863 0.344047 0.147186 0.039 Uiso 1 1 calc R U . . . H42B H 0.003306 0.283107 0.230957 0.039 Uiso 1 1 calc R U . . . C34 C 0.25619(14) 0.26905(12) 0.44384(9) 0.0356(3) Uani 1 1 d . . . . . C5 C 0.51693(15) 0.59012(12) 0.11159(10) 0.0358(3) Uani 1 1 d . . . . . H5 H 0.549178 0.589578 0.050166 0.043 Uiso 1 1 calc R U . . . C16 C 0.80882(15) -0.02053(11) 0.22896(9) 0.0343(3) Uani 1 1 d . . . . . C26 C 0.30212(15) 0.10603(12) 0.36637(11) 0.0380(3) Uani 1 1 d . . . . . C13 C 0.83979(15) 0.15069(12) -0.01041(9) 0.0345(3) Uani 1 1 d . . . . . H13A H 0.942312 0.113379 -0.000495 0.052 Uiso 1 1 calc R U . . . H13B H 0.834209 0.200425 -0.062088 0.052 Uiso 1 1 calc R U . . . H13C H 0.795619 0.097419 -0.020825 0.052 Uiso 1 1 calc R U . . . C32 C 0.19639(15) 0.44942(14) 0.46815(10) 0.0396(4) Uani 1 1 d . . . . . C20 C 0.79164(15) 0.13128(12) 0.36729(9) 0.0333(3) Uani 1 1 d . . . . . C39 C 0.27495(15) 0.17150(12) 0.12698(10) 0.0356(3) Uani 1 1 d . . . . . C8 C 0.41924(16) 0.59412(12) 0.29434(10) 0.0387(3) Uani 1 1 d . . . . . H8 H 0.386243 0.595516 0.355679 0.046 Uiso 1 1 calc R U . . . C21 C 0.77863(16) 0.17753(11) 0.44435(10) 0.0353(3) Uani 1 1 d . . . . . C41 C 0.11301(15) 0.21555(12) 0.11180(10) 0.0365(3) Uani 1 1 d . . . . . H41A H 0.073050 0.156130 0.123380 0.044 Uiso 1 1 calc R U . . . H41B H 0.105060 0.239247 0.048870 0.044 Uiso 1 1 calc R U . . . C23 C 0.63705(17) 0.24922(12) 0.49018(10) 0.0379(3) Uani 1 1 d . . . . . H23A H 0.631136 0.228535 0.553293 0.057 Uiso 1 1 calc R U . . . H23B H 0.555304 0.241240 0.464322 0.057 Uiso 1 1 calc R U . . . H23C H 0.632324 0.324661 0.482834 0.057 Uiso 1 1 calc R U . . . C6 C 0.44227(16) 0.68692(12) 0.15264(11) 0.0416(4) Uani 1 1 d . . . . . H6 H 0.423837 0.753123 0.119052 0.050 Uiso 1 1 calc R U . . . C45 C -0.11687(15) 0.54805(12) 0.11104(10) 0.0384(3) Uani 1 1 d . . . . . H45A H -0.171769 0.616020 0.140375 0.058 Uiso 1 1 calc R U . . . H45B H -0.170231 0.497498 0.124087 0.058 Uiso 1 1 calc R U . . . H45C H -0.104896 0.562181 0.047008 0.058 Uiso 1 1 calc R U . . . C19 C 0.93758(15) 0.06792(13) 0.31849(10) 0.0388(3) Uani 1 1 d . . . . . H19A H 1.013561 0.049112 0.359708 0.047 Uiso 1 1 calc R U . . . H19B H 0.962955 0.114566 0.269923 0.047 Uiso 1 1 calc R U . . . C33 C 0.23456(16) 0.34708(15) 0.51090(10) 0.0425(4) Uani 1 1 d . . . . . C18 C 0.93958(15) -0.03576(13) 0.27985(10) 0.0404(4) Uani 1 1 d . . . . . H18A H 0.941511 -0.090172 0.328603 0.048 Uiso 1 1 calc R U . . . H18B H 1.030499 -0.064721 0.239589 0.048 Uiso 1 1 calc R U . . . C46 C 0.10529(16) 0.58169(12) 0.14508(11) 0.0409(4) Uani 1 1 d . . . . . H46A H 0.096588 0.623835 0.088959 0.061 Uiso 1 1 calc R U . . . H46B H 0.208768 0.544606 0.152735 0.061 Uiso 1 1 calc R U . . . H46C H 0.058496 0.630194 0.193986 0.061 Uiso 1 1 calc R U . . . C7 C 0.39372(17) 0.68840(12) 0.24285(11) 0.0430(4) Uani 1 1 d . . . . . H7 H 0.341967 0.755788 0.269387 0.052 Uiso 1 1 calc R U . . . C27 C 0.29188(15) 0.15726(13) 0.44385(10) 0.0400(4) Uani 1 1 d . . . . . H27 H 0.309376 0.115764 0.497647 0.048 Uiso 1 1 calc R U . . . C17 C 0.81312(18) -0.12586(12) 0.19392(11) 0.0436(4) Uani 1 1 d . . . . . H17A H 0.725271 -0.113271 0.164590 0.065 Uiso 1 1 calc R U . . . H17B H 0.816949 -0.178840 0.243113 0.065 Uiso 1 1 calc R U . . . H17C H 0.899930 -0.153580 0.151416 0.065 Uiso 1 1 calc R U . . . C22 C 0.91038(18) 0.16491(13) 0.49239(11) 0.0458(4) Uani 1 1 d . . . . . H22A H 0.966889 0.206800 0.460204 0.069 Uiso 1 1 calc R U . . . H22B H 0.971886 0.088422 0.495549 0.069 Uiso 1 1 calc R U . . . H22C H 0.877226 0.191372 0.552365 0.069 Uiso 1 1 calc R U . . . C36 C 0.33682(17) -0.01409(13) 0.36575(13) 0.0507(4) Uani 1 1 d . . . . . H36A H 0.255012 -0.028903 0.345863 0.076 Uiso 1 1 calc R U . . . H36B H 0.352858 -0.045460 0.425568 0.076 Uiso 1 1 calc R U . . . H36C H 0.425218 -0.046228 0.325424 0.076 Uiso 1 1 calc R U . . . C40 C 0.36312(18) 0.08624(14) 0.06129(12) 0.0503(4) Uani 1 1 d . . . . . H40A H 0.465636 0.058810 0.073188 0.075 Uiso 1 1 calc R U . . . H40B H 0.355871 0.118201 0.001118 0.075 Uiso 1 1 calc R U . . . H40C H 0.324861 0.026587 0.067095 0.075 Uiso 1 1 calc R U . . . C31 C 0.16455(18) 0.54412(16) 0.51296(12) 0.0523(4) Uani 1 1 d . . . . . H31 H 0.136297 0.612832 0.482835 0.063 Uiso 1 1 calc R U . . . C28 C 0.24640(19) 0.33964(19) 0.60196(11) 0.0587(5) Uani 1 1 d . . . . . H28 H 0.274067 0.271354 0.632761 0.070 Uiso 1 1 calc R U . . . C29 C 0.2169(2) 0.4339(2) 0.64619(12) 0.0708(7) Uani 1 1 d . . . . . H29 H 0.225262 0.429570 0.707838 0.085 Uiso 1 1 calc R U . . . C30 C 0.1755(2) 0.5345(2) 0.60255(13) 0.0666(6) Uani 1 1 d . . . . . H30 H 0.154461 0.597696 0.634952 0.080 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O001 0.0292(5) 0.0359(5) 0.0313(5) 0.0003(4) 0.0005(4) -0.0096(4) O002 0.0307(5) 0.0320(5) 0.0482(6) -0.0084(4) -0.0044(4) -0.0119(4) N003 0.0277(6) 0.0381(6) 0.0282(6) -0.0016(5) -0.0035(4) -0.0129(5) N004 0.0310(6) 0.0402(6) 0.0311(6) -0.0083(5) 0.0007(5) -0.0162(5) C12 0.0195(6) 0.0375(7) 0.0299(7) -0.0025(5) -0.0048(5) -0.0126(5) C24 0.0190(6) 0.0320(7) 0.0324(7) -0.0023(5) -0.0032(5) -0.0096(5) C2 0.0199(6) 0.0352(7) 0.0321(7) -0.0008(6) -0.0042(5) -0.0111(5) C1 0.0199(6) 0.0397(7) 0.0282(7) -0.0003(5) -0.0047(5) -0.0134(5) C37 0.0234(6) 0.0317(7) 0.0293(7) -0.0035(5) -0.0035(5) -0.0118(5) C35 0.0212(6) 0.0386(7) 0.0307(7) -0.0032(6) -0.0011(5) -0.0131(5) C11 0.0212(6) 0.0380(7) 0.0325(7) 0.0022(6) -0.0073(5) -0.0145(5) C3 0.0214(6) 0.0411(7) 0.0292(7) -0.0006(6) -0.0044(5) -0.0141(5) C14 0.0234(6) 0.0378(7) 0.0287(7) 0.0002(6) -0.0015(5) -0.0112(5) C43 0.0228(6) 0.0374(7) 0.0249(6) -0.0040(5) -0.0008(5) -0.0122(5) C4 0.0236(6) 0.0423(8) 0.0284(7) 0.0033(6) -0.0055(5) -0.0162(6) C9 0.0244(6) 0.0375(7) 0.0374(8) -0.0012(6) -0.0083(5) -0.0135(6) C10 0.0221(6) 0.0392(7) 0.0368(7) -0.0002(6) -0.0076(5) -0.0144(5) C25 0.0207(6) 0.0339(7) 0.0394(8) -0.0039(6) -0.0014(5) -0.0109(5) C44 0.0238(6) 0.0400(7) 0.0257(6) -0.0009(5) 0.0007(5) -0.0099(6) C38 0.0232(6) 0.0422(8) 0.0320(7) -0.0062(6) -0.0022(5) -0.0126(6) C15 0.0267(7) 0.0377(7) 0.0324(7) 0.0028(6) -0.0011(5) -0.0121(6) C42 0.0228(6) 0.0407(8) 0.0376(8) -0.0045(6) -0.0050(5) -0.0133(6) C34 0.0234(6) 0.0531(9) 0.0323(7) 0.0026(6) -0.0011(5) -0.0170(6) C5 0.0271(7) 0.0414(8) 0.0423(8) 0.0060(6) -0.0113(6) -0.0150(6) C16 0.0300(7) 0.0354(7) 0.0338(7) 0.0041(6) -0.0003(6) -0.0091(6) C26 0.0229(6) 0.0383(8) 0.0525(9) 0.0076(7) -0.0024(6) -0.0128(6) C13 0.0305(7) 0.0442(8) 0.0304(7) -0.0011(6) -0.0019(6) -0.0152(6) C32 0.0276(7) 0.0625(10) 0.0344(8) -0.0156(7) 0.0051(6) -0.0226(7) C20 0.0279(7) 0.0423(8) 0.0307(7) 0.0051(6) -0.0044(5) -0.0145(6) C39 0.0277(7) 0.0416(8) 0.0400(8) -0.0132(6) -0.0015(6) -0.0132(6) C8 0.0349(7) 0.0412(8) 0.0422(8) -0.0068(6) -0.0084(6) -0.0133(6) C21 0.0368(7) 0.0358(7) 0.0371(8) 0.0047(6) -0.0102(6) -0.0164(6) C41 0.0307(7) 0.0452(8) 0.0395(8) -0.0098(6) -0.0054(6) -0.0182(6) C23 0.0461(8) 0.0384(8) 0.0327(7) -0.0002(6) -0.0088(6) -0.0176(7) C6 0.0351(8) 0.0365(8) 0.0564(10) 0.0059(7) -0.0162(7) -0.0139(6) C45 0.0280(7) 0.0468(8) 0.0360(8) 0.0042(6) -0.0030(6) -0.0087(6) C19 0.0254(7) 0.0532(9) 0.0364(8) 0.0043(7) -0.0062(6) -0.0121(6) C33 0.0283(7) 0.0740(11) 0.0303(7) -0.0063(7) 0.0025(6) -0.0251(7) C18 0.0271(7) 0.0484(9) 0.0374(8) 0.0053(7) -0.0008(6) -0.0052(6) C46 0.0321(7) 0.0375(8) 0.0524(9) 0.0062(7) -0.0053(7) -0.0125(6) C7 0.0362(8) 0.0367(8) 0.0567(10) -0.0070(7) -0.0127(7) -0.0097(6) C27 0.0290(7) 0.0526(9) 0.0384(8) 0.0133(7) -0.0031(6) -0.0172(7) C17 0.0430(8) 0.0375(8) 0.0452(9) -0.0011(7) 0.0057(7) -0.0113(7) C22 0.0450(9) 0.0492(9) 0.0463(9) -0.0015(7) -0.0166(7) -0.0163(7) C36 0.0352(8) 0.0397(8) 0.0761(12) 0.0126(8) -0.0038(8) -0.0153(7) C40 0.0388(9) 0.0557(10) 0.0578(10) -0.0275(8) 0.0021(7) -0.0153(8) C31 0.0393(8) 0.0755(12) 0.0510(10) -0.0302(9) 0.0107(7) -0.0300(8) C28 0.0432(9) 0.1054(16) 0.0329(9) -0.0042(9) 0.0031(7) -0.0344(10) C29 0.0529(11) 0.140(2) 0.0337(9) -0.0312(12) 0.0111(8) -0.0501(13) C30 0.0514(11) 0.1105(18) 0.0512(11) -0.0420(12) 0.0156(9) -0.0435(12) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 O001 C16 119.73(10) . . ? C25 O002 C39 118.70(10) . . ? C12 N003 H003 125.4 . . ? C9 N003 H003 125.4 . . ? C9 N003 C12 109.24(11) . . ? C35 N004 H004 125.6 . . ? C35 N004 C32 108.73(12) . . ? C32 N004 H004 125.6 . . ? N003 C12 C1 128.60(12) . . ? N003 C12 C11 108.64(11) . . ? C1 C12 C11 122.76(12) . . ? C35 C24 C37 122.59(11) . . ? C25 C24 C37 121.46(12) . . ? C25 C24 C35 115.90(12) . . ? O001 C2 C1 122.59(12) . . ? O001 C2 C3 114.61(11) . . ? C1 C2 C3 122.80(12) . . ? C12 C1 C2 116.41(12) . . ? C12 C1 C14 123.36(12) . . ? C2 C1 C14 120.22(12) . . ? C24 C37 H37 109.5 . . ? C24 C37 C43 112.68(10) . . ? C24 C37 C38 107.22(11) . . ? C43 C37 H37 109.5 . . ? C43 C37 C38 108.49(10) . . ? C38 C37 H37 109.5 . . ? N004 C35 C24 127.66(12) . . ? N004 C35 C34 109.31(12) . . ? C24 C35 C34 122.98(13) . . ? C12 C11 C10 106.82(12) . . ? C4 C11 C12 118.59(12) . . ? C4 C11 C10 134.58(12) . . ? C2 C3 C13 119.09(12) . . ? C4 C3 C2 118.64(12) . . ? C4 C3 C13 122.26(12) . . ? C1 C14 H14 109.5 . . ? C1 C14 C15 106.57(11) . . ? C1 C14 C20 110.25(10) . . ? C15 C14 H14 109.5 . . ? C20 C14 H14 109.5 . . ? C20 C14 C15 111.38(11) . . ? C44 C43 C37 123.98(12) . . ? C44 C43 C42 125.64(12) . . ? C42 C43 C37 110.20(11) . . ? C11 C4 H4 119.6 . . ? C3 C4 C11 120.77(12) . . ? C3 C4 H4 119.6 . . ? N003 C9 C10 108.72(12) . . ? N003 C9 C8 129.34(13) . . ? C8 C9 C10 121.93(13) . . ? C9 C10 C11 106.58(12) . . ? C5 C10 C11 134.29(13) . . ? C5 C10 C9 119.11(13) . . ? O002 C25 C24 121.96(12) . . ? O002 C25 C26 115.02(12) . . ? C24 C25 C26 123.01(13) . . ? C43 C44 C45 123.63(12) . . ? C43 C44 C46 124.40(12) . . ? C46 C44 C45 111.96(12) . . ? C37 C38 H38A 110.0 . . ? C37 C38 H38B 110.0 . . ? H38A C38 H38B 108.4 . . ? C39 C38 C37 108.58(11) . . ? C39 C38 H38A 110.0 . . ? C39 C38 H38B 110.0 . . ? C14 C15 H15A 109.8 . . ? C14 C15 H15B 109.8 . . ? H15A C15 H15B 108.2 . . ? C16 C15 C14 109.49(11) . . ? C16 C15 H15A 109.8 . . ? C16 C15 H15B 109.8 . . ? C43 C42 H42A 109.3 . . ? C43 C42 H42B 109.3 . . ? C43 C42 C41 111.57(11) . . ? H42A C42 H42B 108.0 . . ? C41 C42 H42A 109.3 . . ? C41 C42 H42B 109.3 . . ? C35 C34 C33 106.20(13) . . ? C27 C34 C35 118.70(14) . . ? C27 C34 C33 135.10(14) . . ? C10 C5 H5 120.4 . . ? C6 C5 C10 119.10(14) . . ? C6 C5 H5 120.4 . . ? O001 C16 C15 109.99(11) . . ? O001 C16 C18 109.13(11) . . ? O001 C16 C17 104.03(11) . . ? C15 C16 C18 109.27(12) . . ? C17 C16 C15 112.18(12) . . ? C17 C16 C18 112.10(12) . . ? C25 C26 C36 120.22(15) . . ? C27 C26 C25 118.45(13) . . ? C27 C26 C36 121.33(14) . . ? C3 C13 H13A 109.5 . . ? C3 C13 H13B 109.5 . . ? C3 C13 H13C 109.5 . . ? H13A C13 H13B 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? N004 C32 C33 108.69(13) . . ? N004 C32 C31 128.62(16) . . ? C31 C32 C33 122.69(15) . . ? C21 C20 C14 124.81(13) . . ? C21 C20 C19 123.21(13) . . ? C19 C20 C14 111.79(12) . . ? O002 C39 C38 109.79(11) . . ? O002 C39 C41 109.58(11) . . ? O002 C39 C40 103.68(12) . . ? C38 C39 C41 110.61(12) . . ? C40 C39 C38 111.64(12) . . ? C40 C39 C41 111.32(12) . . ? C9 C8 H8 121.2 . . ? C7 C8 C9 117.53(15) . . ? C7 C8 H8 121.2 . . ? C20 C21 C23 124.53(13) . . ? C20 C21 C22 122.08(14) . . ? C23 C21 C22 113.35(13) . . ? C42 C41 H41A 108.6 . . ? C42 C41 H41B 108.6 . . ? C39 C41 C42 114.48(11) . . ? C39 C41 H41A 108.6 . . ? C39 C41 H41B 108.6 . . ? H41A C41 H41B 107.6 . . ? C21 C23 H23A 109.5 . . ? C21 C23 H23B 109.5 . . ? C21 C23 H23C 109.5 . . ? H23A C23 H23B 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? C5 C6 H6 119.6 . . ? C5 C6 C7 120.82(14) . . ? C7 C6 H6 119.6 . . ? C44 C45 H45A 109.5 . . ? C44 C45 H45B 109.5 . . ? C44 C45 H45C 109.5 . . ? H45A C45 H45B 109.5 . . ? H45A C45 H45C 109.5 . . ? H45B C45 H45C 109.5 . . ? C20 C19 H19A 108.8 . . ? C20 C19 H19B 108.8 . . ? C20 C19 C18 113.63(12) . . ? H19A C19 H19B 107.7 . . ? C18 C19 H19A 108.8 . . ? C18 C19 H19B 108.8 . . ? C32 C33 C34 107.02(13) . . ? C32 C33 C28 118.49(17) . . ? C28 C33 C34 134.48(18) . . ? C16 C18 H18A 108.8 . . ? C16 C18 H18B 108.8 . . ? C19 C18 C16 113.88(12) . . ? C19 C18 H18A 108.8 . . ? C19 C18 H18B 108.8 . . ? H18A C18 H18B 107.7 . . ? C44 C46 H46A 109.5 . . ? C44 C46 H46B 109.5 . . ? C44 C46 H46C 109.5 . . ? H46A C46 H46B 109.5 . . ? H46A C46 H46C 109.5 . . ? H46B C46 H46C 109.5 . . ? C8 C7 C6 121.51(15) . . ? C8 C7 H7 119.2 . . ? C6 C7 H7 119.2 . . ? C34 C27 H27 119.6 . . ? C26 C27 C34 120.74(13) . . ? C26 C27 H27 119.6 . . ? C16 C17 H17A 109.5 . . ? C16 C17 H17B 109.5 . . ? C16 C17 H17C 109.5 . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C21 C22 H22A 109.5 . . ? C21 C22 H22B 109.5 . . ? C21 C22 H22C 109.5 . . ? H22A C22 H22B 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? C26 C36 H36A 109.5 . . ? C26 C36 H36B 109.5 . . ? C26 C36 H36C 109.5 . . ? H36A C36 H36B 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C39 C40 H40A 109.5 . . ? C39 C40 H40B 109.5 . . ? C39 C40 H40C 109.5 . . ? H40A C40 H40B 109.5 . . ? H40A C40 H40C 109.5 . . ? H40B C40 H40C 109.5 . . ? C32 C31 H31 121.2 . . ? C30 C31 C32 117.6(2) . . ? C30 C31 H31 121.2 . . ? C33 C28 H28 120.7 . . ? C29 C28 C33 118.7(2) . . ? C29 C28 H28 120.7 . . ? C28 C29 H29 119.2 . . ? C28 C29 C30 121.57(18) . . ? C30 C29 H29 119.2 . . ? C31 C30 C29 120.97(19) . . ? C31 C30 H30 119.5 . . ? C29 C30 H30 119.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O001 C2 1.3711(16) . ? O001 C16 1.4597(16) . ? O002 C25 1.3726(17) . ? O002 C39 1.4618(18) . ? N003 H003 0.8800 . ? N003 C12 1.3883(17) . ? N003 C9 1.3825(18) . ? N004 H004 0.8800 . ? N004 C35 1.3842(18) . ? N004 C32 1.3913(18) . ? C12 C1 1.3926(19) . ? C12 C11 1.4068(18) . ? C24 C37 1.5092(18) . ? C24 C35 1.3985(19) . ? C24 C25 1.3892(18) . ? C2 C1 1.3933(19) . ? C2 C3 1.4187(18) . ? C1 C14 1.5137(18) . ? C37 H37 1.0000 . ? C37 C43 1.5233(17) . ? C37 C38 1.5305(18) . ? C35 C34 1.4034(19) . ? C11 C4 1.4043(19) . ? C11 C10 1.4493(19) . ? C3 C4 1.3759(19) . ? C3 C13 1.5087(19) . ? C14 H14 1.0000 . ? C14 C15 1.5302(19) . ? C14 C20 1.5232(19) . ? C43 C44 1.3378(19) . ? C43 C42 1.5165(18) . ? C4 H4 0.9500 . ? C9 C10 1.412(2) . ? C9 C8 1.395(2) . ? C10 C5 1.397(2) . ? C25 C26 1.418(2) . ? C44 C45 1.5106(18) . ? C44 C46 1.506(2) . ? C38 H38A 0.9900 . ? C38 H38B 0.9900 . ? C38 C39 1.5210(19) . ? C15 H15A 0.9900 . ? C15 H15B 0.9900 . ? C15 C16 1.5224(18) . ? C42 H42A 0.9900 . ? C42 H42B 0.9900 . ? C42 C41 1.5365(19) . ? C34 C33 1.454(2) . ? C34 C27 1.394(2) . ? C5 H5 0.9500 . ? C5 C6 1.385(2) . ? C16 C18 1.531(2) . ? C16 C17 1.516(2) . ? C26 C27 1.384(2) . ? C26 C36 1.503(2) . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C32 C33 1.401(2) . ? C32 C31 1.392(2) . ? C20 C21 1.339(2) . ? C20 C19 1.5158(19) . ? C39 C41 1.5332(19) . ? C39 C40 1.516(2) . ? C8 H8 0.9500 . ? C8 C7 1.381(2) . ? C21 C23 1.502(2) . ? C21 C22 1.522(2) . ? C41 H41A 0.9900 . ? C41 H41B 0.9900 . ? C23 H23A 0.9800 . ? C23 H23B 0.9800 . ? C23 H23C 0.9800 . ? C6 H6 0.9500 . ? C6 C7 1.397(2) . ? C45 H45A 0.9800 . ? C45 H45B 0.9800 . ? C45 H45C 0.9800 . ? C19 H19A 0.9900 . ? C19 H19B 0.9900 . ? C19 C18 1.527(2) . ? C33 C28 1.402(2) . ? C18 H18A 0.9900 . ? C18 H18B 0.9900 . ? C46 H46A 0.9800 . ? C46 H46B 0.9800 . ? C46 H46C 0.9800 . ? C7 H7 0.9500 . ? C27 H27 0.9500 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C22 H22A 0.9800 . ? C22 H22B 0.9800 . ? C22 H22C 0.9800 . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C40 H40A 0.9800 . ? C40 H40B 0.9800 . ? C40 H40C 0.9800 . ? C31 H31 0.9500 . ? C31 C30 1.377(3) . ? C28 H28 0.9500 . ? C28 C29 1.387(3) . ? C29 H29 0.9500 . ? C29 C30 1.388(3) . ? C30 H30 0.9500 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O001 C2 C1 C12 179.00(11) . . . . ? O001 C2 C1 C14 -1.77(18) . . . . ? O001 C2 C3 C4 179.88(10) . . . . ? O001 C2 C3 C13 -0.46(17) . . . . ? O001 C16 C18 C19 66.84(15) . . . . ? O002 C25 C26 C27 180.00(12) . . . . ? O002 C25 C26 C36 0.52(18) . . . . ? O002 C39 C41 C42 71.81(15) . . . . ? N003 C12 C1 C2 -178.69(11) . . . . ? N003 C12 C1 C14 2.1(2) . . . . ? N003 C12 C11 C4 179.37(10) . . . . ? N003 C12 C11 C10 0.36(13) . . . . ? N003 C9 C10 C11 0.30(14) . . . . ? N003 C9 C10 C5 -178.08(11) . . . . ? N003 C9 C8 C7 177.99(13) . . . . ? N004 C35 C34 C33 -0.42(14) . . . . ? N004 C35 C34 C27 179.81(11) . . . . ? N004 C32 C33 C34 -2.34(15) . . . . ? N004 C32 C33 C28 176.55(12) . . . . ? N004 C32 C31 C30 -177.03(14) . . . . ? C12 N003 C9 C10 -0.08(14) . . . . ? C12 N003 C9 C8 -178.68(13) . . . . ? C12 C1 C14 C15 150.05(12) . . . . ? C12 C1 C14 C20 -88.93(15) . . . . ? C12 C11 C4 C3 0.00(18) . . . . ? C12 C11 C10 C9 -0.41(14) . . . . ? C12 C11 C10 C5 177.62(14) . . . . ? C24 C37 C43 C44 129.61(13) . . . . ? C24 C37 C43 C42 -54.98(14) . . . . ? C24 C37 C38 C39 56.22(13) . . . . ? C24 C35 C34 C33 177.30(12) . . . . ? C24 C35 C34 C27 -2.47(19) . . . . ? C24 C25 C26 C27 1.0(2) . . . . ? C24 C25 C26 C36 -178.45(12) . . . . ? C2 O001 C16 C15 28.45(16) . . . . ? C2 O001 C16 C18 -91.42(13) . . . . ? C2 O001 C16 C17 148.77(11) . . . . ? C2 C1 C14 C15 -29.12(15) . . . . ? C2 C1 C14 C20 91.90(14) . . . . ? C2 C3 C4 C11 0.34(18) . . . . ? C1 C12 C11 C4 -1.30(18) . . . . ? C1 C12 C11 C10 179.69(11) . . . . ? C1 C2 C3 C4 0.58(19) . . . . ? C1 C2 C3 C13 -179.75(11) . . . . ? C1 C14 C15 C16 58.82(13) . . . . ? C1 C14 C20 C21 111.34(15) . . . . ? C1 C14 C20 C19 -63.78(15) . . . . ? C37 C24 C35 N004 4.9(2) . . . . ? C37 C24 C35 C34 -172.37(11) . . . . ? C37 C24 C25 O002 -5.77(18) . . . . ? C37 C24 C25 C26 173.14(11) . . . . ? C37 C43 C44 C45 174.03(12) . . . . ? C37 C43 C44 C46 -5.3(2) . . . . ? C37 C43 C42 C41 -53.40(15) . . . . ? C37 C38 C39 O002 -63.12(13) . . . . ? C37 C38 C39 C41 57.93(15) . . . . ? C37 C38 C39 C40 -177.53(12) . . . . ? C35 N004 C32 C33 2.12(15) . . . . ? C35 N004 C32 C31 -178.96(14) . . . . ? C35 C24 C37 C43 -86.75(14) . . . . ? C35 C24 C37 C38 153.95(11) . . . . ? C35 C24 C25 O002 176.55(11) . . . . ? C35 C24 C25 C26 -4.54(18) . . . . ? C35 C34 C33 C32 1.69(15) . . . . ? C35 C34 C33 C28 -176.95(16) . . . . ? C35 C34 C27 C26 -1.4(2) . . . . ? C11 C12 C1 C2 2.12(18) . . . . ? C11 C12 C1 C14 -177.08(11) . . . . ? C11 C10 C5 C6 -178.06(14) . . . . ? C3 C2 C1 C12 -1.76(18) . . . . ? C3 C2 C1 C14 177.47(11) . . . . ? C14 C15 C16 O001 -60.07(14) . . . . ? C14 C15 C16 C18 59.71(14) . . . . ? C14 C15 C16 C17 -175.34(11) . . . . ? C14 C20 C21 C23 -0.5(2) . . . . ? C14 C20 C21 C22 -178.09(13) . . . . ? C14 C20 C19 C18 -46.92(16) . . . . ? C43 C37 C38 C39 -65.74(14) . . . . ? C43 C42 C41 C39 46.91(17) . . . . ? C4 C11 C10 C9 -179.19(13) . . . . ? C4 C11 C10 C5 -1.2(3) . . . . ? C9 N003 C12 C1 -179.46(12) . . . . ? C9 N003 C12 C11 -0.18(13) . . . . ? C9 C10 C5 C6 -0.22(19) . . . . ? C9 C8 C7 C6 -0.2(2) . . . . ? C10 C11 C4 C3 178.67(13) . . . . ? C10 C9 C8 C7 -0.4(2) . . . . ? C10 C5 C6 C7 -0.4(2) . . . . ? C25 O002 C39 C38 33.96(15) . . . . ? C25 O002 C39 C41 -87.71(13) . . . . ? C25 O002 C39 C40 153.36(11) . . . . ? C25 C24 C37 C43 95.73(14) . . . . ? C25 C24 C37 C38 -23.57(15) . . . . ? C25 C24 C35 N004 -177.43(12) . . . . ? C25 C24 C35 C34 5.28(18) . . . . ? C25 C26 C27 C34 2.1(2) . . . . ? C44 C43 C42 C41 121.92(14) . . . . ? C38 C37 C43 C44 -111.83(14) . . . . ? C38 C37 C43 C42 63.58(13) . . . . ? C38 C39 C41 C42 -49.36(17) . . . . ? C15 C14 C20 C21 -130.56(14) . . . . ? C15 C14 C20 C19 54.31(14) . . . . ? C15 C16 C18 C19 -53.46(15) . . . . ? C42 C43 C44 C45 -0.7(2) . . . . ? C42 C43 C44 C46 -179.99(13) . . . . ? C34 C33 C28 C29 179.84(16) . . . . ? C5 C6 C7 C8 0.6(2) . . . . ? C16 O001 C2 C1 2.55(17) . . . . ? C16 O001 C2 C3 -176.74(11) . . . . ? C13 C3 C4 C11 -179.31(11) . . . . ? C32 N004 C35 C24 -178.61(12) . . . . ? C32 N004 C35 C34 -1.03(14) . . . . ? C32 C33 C28 C29 1.3(2) . . . . ? C32 C31 C30 C29 0.0(2) . . . . ? C20 C14 C15 C16 -61.47(14) . . . . ? C20 C19 C18 C16 47.50(17) . . . . ? C39 O002 C25 C24 0.51(17) . . . . ? C39 O002 C25 C26 -178.48(11) . . . . ? C8 C9 C10 C11 179.02(12) . . . . ? C8 C9 C10 C5 0.64(19) . . . . ? C21 C20 C19 C18 137.86(14) . . . . ? C19 C20 C21 C23 174.09(13) . . . . ? C19 C20 C21 C22 -3.5(2) . . . . ? C33 C34 C27 C26 178.92(14) . . . . ? C33 C32 C31 C30 1.8(2) . . . . ? C33 C28 C29 C30 0.4(3) . . . . ? C27 C34 C33 C32 -178.59(15) . . . . ? C27 C34 C33 C28 2.8(3) . . . . ? C17 C16 C18 C19 -178.46(12) . . . . ? C36 C26 C27 C34 -178.45(13) . . . . ? C40 C39 C41 C42 -174.09(13) . . . . ? C31 C32 C33 C34 178.66(13) . . . . ? C31 C32 C33 C28 -2.4(2) . . . . ? C28 C29 C30 C31 -1.1(3) . . . . ?