#------------------------------------------------------------------------------ #$Date: 2024-12-06 19:27:29 +0200 (Fri, 06 Dec 2024) $ #$Revision: 296452 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/93/7249376.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7249376 loop_ _publ_author_name 'Tian, Zhengfang' 'Yang, Shun-Yi' 'Zhu, Junlun' 'Ruan, Zhijun' 'Shao, Dong' _publ_section_title ; Topological and magnetic regulation in three cobalt(ii) coordination polymers constructed using a mixed bipyrimidine--tetracarboxylate strategy ; _journal_issue 41 _journal_name_full CrystEngComm _journal_page_first 5933 _journal_page_last 5940 _journal_paper_doi 10.1039/D4CE00902A _journal_volume 26 _journal_year 2024 _chemical_formula_moiety 'C9 H8 Co N2 O6, C3 H7 N O, H2 O' _chemical_formula_sum 'C12 H17 Co N3 O8' _chemical_formula_weight 390.21 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary iterative _audit_creation_date 2024-07-15 _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _audit_update_record ; 2024-07-28 deposited with the CCDC. 2024-09-25 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 100.6700(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 12.0964(5) _cell_length_b 15.9359(6) _cell_length_c 7.9797(2) _cell_measurement_reflns_used 9248 _cell_measurement_temperature 250.00 _cell_measurement_theta_max 26.86 _cell_measurement_theta_min 2.90 _cell_volume 1511.63(9) _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'olex2.solve 1.5 (Bourhis et al., 2015)' _diffrn_ambient_temperature 250.00 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0767 _diffrn_reflns_av_unetI/netI 0.0365 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_l_max 10 _diffrn_reflns_limit_l_min -9 _diffrn_reflns_number 37574 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.522 _diffrn_reflns_theta_min 2.137 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 1.185 _exptl_absorpt_correction_type none _exptl_crystal_colour orange _exptl_crystal_colour_primary orange _exptl_crystal_density_diffrn 1.715 _exptl_crystal_description block _exptl_crystal_F_000 804 _exptl_crystal_size_max 0.34 _exptl_crystal_size_mid 0.21 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.462 _refine_diff_density_min -0.811 _refine_diff_density_rms 0.096 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.044 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 219 _refine_ls_number_reflns 3480 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.044 _refine_ls_R_factor_all 0.0607 _refine_ls_R_factor_gt 0.0452 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0645P)^2^+2.9936P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1201 _refine_ls_wR_factor_ref 0.1300 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2819 _reflns_number_total 3480 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4ce00902a2.cif _cod_data_source_block Co2 _cod_depositor_comments 'Adding full bibliography for 7249374--7249376.cif.' _cod_database_code 7249376 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.871 _shelx_estimated_absorpt_t_min 0.689 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups, All O(H,H) groups 2.a Free rotating group: O8(H8A,H8B) 2.b Rotating group: O2(H2A,H2B), O3(H3A,H3B) 2.c Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C7(H7), C8(H8), C9(H9) 2.d Idealised Me refined as rotating group: C11(H11A,H11B,H11C), C13(H13A,H13B,H13C) ; _shelx_res_file ; TITL a_a.res in P2(1)/c a_a.res created by SHELXL-2017/1 at 16:32:56 on 15-Jul-2024 REM Old TITL a in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.101, Rweak 0.006, Alpha 0.048 REM 0.451 for 127 systematic absences, Orientation as input REM Formula found by SHELXT: C12 Co N4 O7 CELL 0.71073 12.0964 15.9359 7.9797 90 100.67 90 ZERR 4 0.0005 0.0006 0.0002 0 0.001 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Co N O UNIT 48 68 4 12 32 L.S. 10 PLAN 5 SIZE 0.12 0.21 0.34 TEMP -23.15 CONF BOND LIST 6 MORE -1 BOND $H fmap 2 ACTA REM REM REM WGHT 0.064500 2.993600 FVAR 0.60574 CO1 3 0.317562 0.402625 0.591842 11.00000 0.01825 0.01813 = 0.01670 0.00090 0.00646 0.00049 O1 5 0.208286 0.446430 0.378344 11.00000 0.02661 0.02364 = 0.01790 0.00056 0.00155 0.00439 O2 5 0.273950 0.278066 0.528669 11.00000 0.03166 0.02248 = 0.02242 0.00373 0.00603 -0.00477 AFIX 7 H2A 2 0.226571 0.276706 0.433829 11.00000 -1.50000 H2B 2 0.237539 0.257657 0.602318 11.00000 -1.50000 AFIX 0 O3 5 0.424987 0.360957 0.813311 11.00000 0.02332 0.02554 = 0.02150 0.00171 0.00535 0.00380 AFIX 7 H3A 2 0.399388 0.377469 0.901381 11.00000 -1.50000 H3B 2 0.489047 0.385585 0.821948 11.00000 -1.50000 AFIX 0 O4 5 -0.193143 0.574705 0.267801 11.00000 0.02097 0.04407 = 0.01894 -0.00305 0.00868 0.00474 O5 5 -0.288888 0.567758 0.001432 11.00000 0.02250 0.05387 = 0.02181 -0.00175 0.00458 0.01108 O6 5 0.169199 0.329757 0.224229 11.00000 0.04382 0.02427 = 0.02375 -0.00179 0.00453 0.00945 N1 4 0.448908 0.397014 0.440191 11.00000 0.02035 0.01637 = 0.02265 -0.00088 0.00865 -0.00038 N2 4 0.599483 0.475755 0.365866 11.00000 0.02186 0.01907 = 0.02173 0.00001 0.00985 0.00006 C1 1 -0.095369 0.533082 0.051873 11.00000 0.02102 0.02204 = 0.01671 -0.00103 0.00725 0.00148 C2 1 0.558356 0.340218 0.249505 11.00000 0.04106 0.02419 = 0.03491 -0.00975 0.01904 0.00019 AFIX 43 H2 2 0.573853 0.296339 0.178589 11.00000 -1.20000 AFIX 0 C3 1 0.472354 0.333942 0.339462 11.00000 0.03176 0.01962 = 0.03126 -0.00507 0.00923 -0.00214 AFIX 43 H3 2 0.428892 0.284694 0.330723 11.00000 -1.20000 AFIX 0 C4 1 0.513422 0.464747 0.446383 11.00000 0.02145 0.01626 = 0.01672 0.00134 0.00588 0.00077 C6 1 0.081596 0.457207 0.117596 11.00000 0.02251 0.02023 = 0.01754 -0.00071 0.00550 0.00209 C7 1 0.621349 0.412934 0.266410 11.00000 0.03179 0.02644 = 0.02829 -0.00375 0.01625 0.00069 AFIX 43 H7 2 0.680981 0.418331 0.206536 11.00000 -1.20000 AFIX 0 C8 1 -0.013472 0.491184 0.166187 11.00000 0.02444 0.02541 = 0.01396 0.00120 0.00749 0.00416 AFIX 43 H8 2 -0.022578 0.485601 0.280115 11.00000 -1.20000 AFIX 0 C10 1 -0.200539 0.562000 0.110628 11.00000 0.02211 0.02150 = 0.01897 0.00241 0.00761 0.00213 C12 1 0.161515 0.406953 0.248330 11.00000 0.02011 0.02585 = 0.01544 0.00249 0.00843 0.00389 O7 5 0.281637 0.676754 0.359550 11.00000 0.11225 0.12981 = 0.15062 -0.01063 0.04265 0.01456 N3 4 0.121971 0.707940 0.447496 11.00000 0.06609 0.08212 = 0.10746 0.01523 0.02481 -0.00213 C9 1 0.196127 0.642820 0.397260 11.00000 0.04474 0.12397 = 0.06823 0.00079 0.01416 -0.02211 AFIX 43 H9 2 0.181477 0.584856 0.394050 11.00000 -1.20000 AFIX 0 C11 1 0.010634 0.684737 0.467168 11.00000 0.07886 0.09107 = 0.23344 -0.00203 0.08132 -0.01288 AFIX 137 H11A 2 -0.041330 0.694373 0.360856 11.00000 -1.50000 H11B 2 -0.011654 0.718323 0.556700 11.00000 -1.50000 H11C 2 0.009521 0.625810 0.497264 11.00000 -1.50000 AFIX 0 C13 1 0.154263 0.797654 0.450127 11.00000 0.16607 AFIX 137 H13A 2 0.232265 0.802434 0.437626 11.00000 -1.50000 H13B 2 0.144941 0.822520 0.557590 11.00000 -1.50000 H13C 2 0.106727 0.826759 0.356887 11.00000 -1.50000 AFIX 6 O8 5 0.368739 0.577542 0.164424 11.00000 0.04049 0.06887 = 0.08015 -0.01509 0.01267 -0.01973 H8A 2 0.329707 0.599231 0.233204 11.00000 -1.50000 H8B 2 0.332888 0.532644 0.127616 11.00000 -1.50000 AFIX 0 HKLF 4 REM a_a.res in P2(1)/c REM R1 = 0.0452 for 2819 Fo > 4sig(Fo) and 0.0607 for all 3480 data REM 219 parameters refined using 0 restraints END WGHT 0.0645 2.9936 REM Highest difference peak 0.462, deepest hole -0.811, 1-sigma level 0.096 Q1 1 0.2605 0.7885 0.4702 11.00000 0.05 0.44 Q2 1 0.2252 0.7359 0.4443 11.00000 0.05 0.44 Q3 1 0.1735 0.5987 0.4272 11.00000 0.05 0.41 Q4 1 0.0521 0.7860 0.5426 11.00000 0.05 0.40 Q5 1 0.2244 0.6126 0.3583 11.00000 0.05 0.38 ; _shelx_res_checksum 86826 _shelx_hkl_file ; 0 0 -1 0.90 2.50 0 0 1 3.20 2.80 0 0 2 136.59 7.60 0 0 2 144.09 7.60 0 0 -2 122.79 13.30 0 0 2 148.99 7.60 0 0 2 137.39 13.40 0 0 2 140.69 7.60 0 0 -3 -1.90 5.00 0 0 3 -0.60 1.10 0 0 3 -0.40 4.40 0 0 3 3.30 1.10 0 0 3 -0.70 1.10 0 0 -4 466.85 34.80 0 0 4 429.86 20.50 0 0 4 416.46 20.80 0 0 4 431.06 20.50 0 0 4 417.86 20.80 0 0 4 385.96 32.20 0 0 5 -1.30 8.10 0 0 5 0.90 1.60 0 0 6 1185.48 57.79 0 0 6 1267.47 78.39 0 0 7 -0.90 12.10 0 0 7 1.50 4.10 0 0 8 90.49 11.20 0 0 8 49.60 35.50 0 0 9 16.50 8.30 0 0 9 -5.70 20.30 0 0 10 0.80 26.10 0 0 10 32.10 12.80 0 1 -1 1899.21 84.59 0 1 1 1800.42 83.99 0 1 1 1832.02 83.99 0 1 -1 1898.11 84.69 0 1 -1 1846.82 87.99 0 -1 -1 1781.42 83.99 0 -1 1 1886.91 87.99 0 -1 1 1887.31 84.69 0 -1 -1 1768.12 83.99 0 -1 1 1897.31 84.69 0 -1 1 1841.32 84.69 0 1 2 784.12 46.00 0 1 2 849.02 39.00 0 1 -2 789.82 47.30 0 1 -2 874.51 40.30 0 1 2 860.51 39.00 0 1 -2 869.11 40.30 0 -1 2 874.11 40.40 0 -1 2 846.52 40.30 0 -1 -2 874.61 39.20 0 -1 2 840.82 46.80 0 -1 -2 863.51 39.20 0 1 3 12.40 6.00 0 1 -3 7.50 6.70 0 -1 3 10.80 2.30 0 -1 3 10.40 2.40 0 -1 3 8.00 2.10 0 -1 3 5.40 1.90 0 -1 3 5.90 5.50 0 1 -4 1034.30 65.99 0 1 4 1208.48 66.69 0 -1 4 1132.89 52.89 0 -1 4 1085.69 52.49 0 -1 4 1148.99 53.39 0 -1 4 1105.69 52.79 0 -1 4 1060.59 65.19 0 -1 4 1102.69 53.19 0 1 5 1990.30 111.69 0 1 -5 2001.00 113.99 0 -1 5 2046.90 94.79 0 -1 5 2088.89 95.59 0 -1 5 2150.78 113.29 0 -1 5 2024.10 94.79 0 -1 5 2005.90 95.49 0 -1 5 2066.39 95.69 0 1 -6 2.20 12.60 0 1 6 14.00 11.90 0 -1 6 26.00 13.00 0 -1 6 9.90 2.70 0 -1 6 5.30 3.00 0 -1 6 3.10 2.40 0 -1 6 10.00 3.50 0 1 7 406.96 40.60 0 1 7 337.77 19.50 0 -1 7 338.17 22.30 0 -1 7 407.56 39.70 0 1 8 229.28 35.80 0 1 8 223.98 16.10 0 -1 8 222.08 18.80 0 -1 8 279.97 40.10 0 1 9 43.70 10.30 0 1 9 40.60 26.50 0 -1 9 46.90 11.70 0 -1 9 52.99 24.60 0 1 10 -17.80 26.10 0 1 10 6.40 11.40 0 -1 10 16.90 13.10 0 -1 10 -15.10 27.10 0 2 1 381.86 19.60 0 2 -1 414.56 23.40 0 2 1 393.46 19.50 0 2 1 401.66 19.70 0 2 -1 400.16 20.20 0 2 1 391.96 19.60 0 2 -1 386.56 20.00 0 2 -1 382.66 20.50 0 -2 -1 391.66 19.60 0 -2 1 377.36 20.10 0 -2 1 390.86 20.30 0 -2 -1 380.96 19.20 0 -2 1 411.66 20.70 0 -2 -1 400.06 19.60 0 -2 -1 354.16 19.10 0 2 -2 40.70 4.20 0 2 2 39.60 3.30 0 2 -2 43.80 4.20 0 2 -2 43.20 8.60 0 2 2 43.40 3.40 0 -2 -2 35.20 3.40 0 -2 2 28.90 7.40 0 -2 -2 36.50 3.40 0 -2 2 40.00 5.20 0 -2 2 53.99 4.70 0 -2 2 40.60 4.30 0 2 3 3654.23 169.48 0 2 3 3617.44 169.48 0 2 -3 3824.42 171.78 0 2 -3 3622.24 182.28 0 2 3 3764.82 181.18 0 2 -3 3799.72 171.78 0 -2 -3 3844.02 169.88 0 -2 3 3759.42 181.68 0 -2 3 3773.62 172.18 0 -2 -3 3791.82 169.88 0 -2 3 3591.44 172.08 0 -2 3 3866.21 172.18 0 2 4 989.50 59.79 0 2 -4 956.70 60.69 0 -2 4 984.70 48.10 0 -2 4 965.00 59.89 0 -2 4 1079.19 48.80 0 -2 4 917.61 48.00 0 -2 4 979.80 48.20 0 -2 4 952.50 48.10 0 2 5 24.10 12.60 0 2 -5 19.30 11.90 0 -2 5 14.70 4.30 0 -2 5 15.70 10.30 0 -2 5 18.90 4.50 0 -2 5 16.40 4.80 0 -2 5 11.60 3.60 0 -2 5 12.20 3.70 0 2 6 221.28 30.40 0 2 -6 192.78 31.00 0 -2 6 164.38 12.40 0 -2 6 150.98 11.40 0 -2 6 164.88 11.50 0 -2 6 181.78 14.10 0 -2 6 162.48 26.00 0 -2 6 176.78 12.60 0 2 7 89.29 7.10 0 2 7 101.69 23.00 0 2 -7 91.69 24.40 0 -2 7 76.49 6.50 0 -2 7 84.79 7.10 0 -2 7 82.69 7.20 0 -2 7 67.19 10.80 0 -2 7 93.09 23.30 0 -2 7 73.79 6.40 0 2 8 36.20 6.90 0 2 8 36.10 21.30 0 -2 8 63.19 22.10 0 -2 8 49.10 10.90 0 2 9 531.35 56.59 0 2 9 436.16 27.90 0 -2 9 430.36 51.49 0 -2 9 459.55 33.00 0 2 10 14.70 28.10 0 2 10 7.90 10.90 0 -2 10 10.50 14.10 0 -2 10 26.00 26.00 0 -2 10 -9.20 11.80 0 3 0 -0.40 2.30 0 3 0 -0.20 1.30 0 3 0 -3.00 1.40 0 3 0 -0.10 1.30 0 -3 0 2.40 1.70 0 -3 0 1.60 1.60 0 -3 0 1.10 1.50 0 -3 0 -1.70 1.40 0 3 1 2764.82 129.89 0 3 -1 3046.50 134.59 0 3 1 2719.53 129.59 0 3 1 2712.43 129.49 0 3 -1 2790.22 130.79 0 3 -1 2813.72 130.09 0 3 1 3065.79 129.89 0 3 -1 2815.12 130.29 0 -3 -1 2657.83 129.69 0 -3 -1 2539.65 129.59 0 -3 -1 2842.42 129.69 0 -3 -1 2766.92 129.39 0 -3 1 2915.01 130.29 0 -3 1 2881.71 130.59 0 -3 1 2793.42 130.29 0 -3 1 2838.72 130.89 0 3 -2 161.78 11.20 0 3 2 174.38 10.40 0 3 -2 175.08 16.60 0 3 2 187.28 10.60 0 3 -2 169.78 11.60 0 3 2 182.48 10.60 0 3 -2 170.78 11.40 0 3 2 167.28 10.30 0 -3 2 163.98 11.50 0 -3 -2 161.28 10.30 0 -3 2 171.28 11.70 0 -3 2 165.78 12.10 0 -3 -2 170.78 10.40 0 -3 2 154.48 15.00 0 3 -3 172.68 19.10 0 3 3 159.28 9.60 0 3 3 173.08 9.40 0 3 3 147.89 9.50 0 3 -3 191.88 11.90 0 3 -3 183.08 11.80 0 3 3 171.78 9.80 0 -3 -3 156.18 10.00 0 -3 3 192.68 12.90 0 -3 -3 150.78 10.00 0 -3 3 183.78 19.10 0 -3 3 164.38 11.80 0 -3 3 171.88 12.10 0 3 -4 147.39 11.20 0 3 -4 151.28 23.40 0 3 4 166.38 8.50 0 3 4 165.28 8.50 0 3 4 161.08 19.70 0 -3 4 147.99 12.50 0 -3 -4 160.98 9.20 0 -3 4 194.98 20.60 0 -3 4 154.58 12.00 0 -3 -4 168.38 9.20 0 -3 4 153.58 11.90 0 3 5 214.58 26.60 0 3 -5 240.98 30.10 0 -3 5 248.18 16.80 0 -3 5 260.97 17.10 0 -3 5 307.57 29.10 0 -3 5 260.67 18.20 0 -3 5 266.87 17.10 0 -3 5 243.98 16.60 0 3 -6 270.37 33.80 0 3 6 213.28 31.30 0 3 6 244.48 13.10 0 3 6 256.37 13.50 0 -3 6 229.78 18.70 0 -3 6 251.87 17.00 0 -3 6 217.88 31.40 0 -3 6 293.27 18.30 0 -3 6 249.58 16.90 0 -3 6 275.57 17.90 0 3 -7 3.10 18.50 0 3 7 7.40 14.30 0 3 7 12.40 4.20 0 -3 7 14.40 4.90 0 -3 7 14.10 4.80 0 -3 7 22.60 14.90 0 -3 7 14.60 6.60 0 -3 7 17.10 6.40 0 -3 7 -8.00 5.90 0 3 8 690.63 38.90 0 3 8 847.52 65.49 0 -3 8 747.53 45.20 0 -3 8 876.91 65.59 0 3 9 29.30 23.30 0 3 9 16.00 8.10 0 -3 9 11.00 11.20 0 -3 9 -3.00 21.80 0 3 10 16.00 29.20 0 3 10 28.50 10.90 0 -3 10 62.89 16.50 0 -3 10 51.59 17.70 0 -3 10 51.79 32.70 0 4 0 3548.84 165.08 0 4 0 3584.84 165.28 0 4 0 3312.27 165.28 0 4 0 3549.54 166.28 0 -4 0 3679.73 165.48 0 -4 0 3720.83 165.68 0 -4 0 3564.54 165.98 0 -4 0 3570.64 167.88 0 4 1 528.85 29.40 0 4 -1 539.55 30.00 0 4 1 600.44 30.60 0 4 1 581.04 30.00 0 4 -1 544.75 30.00 0 4 -1 562.04 31.10 0 4 1 536.95 29.40 0 -4 1 602.34 30.50 0 -4 1 569.44 31.20 0 -4 1 586.94 30.60 0 -4 -1 585.44 29.90 0 -4 -1 550.84 29.90 0 -4 1 543.85 30.30 0 4 2 1085.59 51.19 0 4 2 970.60 50.69 0 4 -2 1128.09 52.49 0 4 -2 970.10 52.29 0 4 -2 1111.19 52.49 0 4 2 945.71 50.69 0 4 2 1066.49 51.39 0 4 -2 1056.39 58.79 0 -4 2 1041.00 52.59 0 -4 -2 1095.19 51.39 0 -4 -2 1003.30 49.60 0 -4 2 985.40 52.89 0 -4 -2 1157.58 51.59 0 -4 2 1060.69 52.19 0 -4 2 1086.39 52.69 0 -4 -2 977.20 49.70 0 4 3 94.69 7.50 0 4 3 91.39 7.60 0 4 -3 86.99 14.90 0 4 -3 79.79 8.00 0 4 -3 77.19 8.00 0 4 3 92.89 8.00 0 4 3 73.09 7.40 0 -4 3 86.69 8.70 0 -4 3 76.69 13.50 0 -4 3 90.89 9.70 0 -4 3 72.59 8.20 0 4 4 13.30 8.90 0 4 -4 20.20 5.00 0 4 -4 22.50 11.70 0 4 4 24.20 4.20 0 4 4 23.60 3.40 0 4 -4 26.00 5.30 0 4 4 21.20 4.20 0 4 4 21.30 3.20 0 -4 -4 21.90 3.90 0 -4 4 28.90 6.80 0 -4 4 39.60 12.10 0 -4 4 27.80 5.80 0 -4 -4 19.40 3.70 0 -4 4 25.20 5.40 0 4 5 65.59 6.90 0 4 5 53.69 15.30 0 4 -5 59.19 16.50 0 4 5 67.29 6.30 0 -4 5 61.89 9.40 0 -4 5 73.99 10.10 0 -4 5 109.29 20.40 0 4 6 882.61 63.89 0 4 6 857.61 44.80 0 4 -6 828.32 73.39 0 4 6 903.01 45.60 0 -4 6 929.21 51.39 0 -4 6 990.10 49.10 0 -4 6 941.01 48.90 0 -4 6 936.41 49.20 0 -4 6 1092.79 68.69 0 -4 6 929.61 49.10 0 4 7 173.28 13.20 0 4 -7 223.48 38.50 0 4 7 169.58 30.00 0 -4 7 182.28 31.40 0 -4 7 205.48 16.50 0 -4 7 194.48 15.40 0 -4 7 177.78 15.90 0 -4 7 144.69 18.70 0 -4 7 162.78 15.00 0 4 -8 8.80 25.40 0 4 8 -31.30 15.20 0 4 8 4.10 5.90 0 -4 8 1.10 6.60 0 -4 8 2.50 6.70 0 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56.19 0 -6 6 944.21 52.89 0 -6 6 934.71 52.79 0 -6 -6 948.11 44.90 0 -6 6 1005.20 53.59 0 -6 6 1064.29 70.09 0 -6 6 998.10 53.49 0 -6 -6 942.91 44.90 0 6 -7 146.09 35.30 0 6 7 191.08 16.30 0 6 7 223.48 34.70 0 6 7 198.78 16.50 0 -6 7 204.08 19.20 0 -6 7 190.88 19.40 0 -6 7 208.98 19.10 0 -6 7 186.28 23.30 0 -6 7 214.18 19.10 0 -6 7 176.48 18.50 0 6 -8 -8.20 23.60 0 6 8 51.09 9.70 0 6 8 47.10 22.40 0 -6 8 47.10 12.50 0 -6 8 58.69 11.40 0 -6 8 56.09 16.30 0 -6 8 59.79 12.40 0 -6 8 48.30 12.00 0 -6 8 66.39 12.20 0 6 9 66.39 28.50 0 6 -9 52.29 41.50 0 -6 9 80.79 17.20 0 -6 9 89.79 19.90 0 -6 9 63.19 13.50 0 -6 9 51.19 13.00 0 7 0 6.70 4.70 0 7 0 6.80 5.10 0 7 0 -4.60 2.50 0 7 0 -6.70 2.70 0 -7 0 4.90 3.80 0 -7 0 -1.20 3.40 0 -7 0 1.00 3.40 0 -7 0 -2.70 3.10 0 7 1 249.78 19.80 0 7 -1 256.57 20.30 0 7 1 291.67 21.30 0 7 -1 305.57 20.60 0 7 -1 326.17 22.20 0 7 1 265.37 19.30 0 7 1 320.77 20.20 0 7 -1 303.57 20.30 0 -7 -1 272.07 20.20 0 -7 -1 304.37 21.10 0 -7 -1 283.27 20.10 0 -7 1 275.87 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204.48 15.20 0 -9 -7 181.08 18.00 0 -9 -7 220.08 19.60 0 -9 7 206.78 23.60 0 -9 -7 191.28 15.00 0 9 8 101.79 15.80 0 9 -8 120.59 42.70 0 9 8 64.69 33.60 0 9 8 63.39 16.60 0 -9 8 82.29 17.60 0 -9 8 45.00 17.00 0 -9 8 110.59 20.40 0 9 9 92.49 16.50 0 9 9 100.79 35.30 0 -9 9 73.59 25.20 0 -9 9 44.80 19.50 0 -9 9 101.09 20.80 0 -9 9 96.29 23.30 0 10 0 756.92 45.40 0 10 0 789.52 47.10 0 10 0 664.03 42.80 0 10 0 765.72 43.80 0 -10 0 711.53 45.50 0 -10 0 722.53 44.20 0 -10 0 758.32 44.60 0 -10 0 676.23 43.70 0 10 1 3.60 5.70 0 10 -1 5.50 5.40 0 10 1 4.50 5.70 0 10 -1 4.80 5.20 0 10 -1 -3.60 4.90 0 10 1 6.10 4.90 0 10 1 -3.50 6.60 0 10 -1 8.90 7.50 0 -10 1 1.40 6.20 0 -10 -1 4.30 6.00 0 -10 -1 -5.30 5.90 0 -10 1 6.50 6.50 0 -10 -1 -3.00 5.30 0 -10 -1 9.20 6.90 0 -10 1 -2.20 6.40 0 -10 1 -1.30 5.90 0 10 2 254.87 22.30 0 10 -2 242.58 29.20 0 10 2 277.57 24.10 0 10 -2 228.08 21.50 0 10 2 297.97 22.20 0 10 -2 270.17 25.20 0 10 2 291.17 21.70 0 10 -2 309.57 23.50 0 -10 2 302.47 24.40 0 -10 -2 267.47 22.60 0 -10 -2 236.28 21.80 0 -10 -2 287.27 23.10 0 -10 2 300.07 25.60 0 -10 -2 302.67 23.20 0 -10 2 279.17 23.70 0 -10 2 280.37 23.50 0 10 3 276.57 21.40 0 10 -3 301.27 24.30 0 10 3 237.18 20.20 0 10 -3 265.27 22.90 0 10 3 259.87 22.70 0 10 -3 226.28 32.50 0 10 3 282.27 24.80 0 10 -3 266.17 25.30 0 -10 3 268.47 23.60 0 -10 3 268.57 23.60 0 -10 3 302.97 26.60 0 -10 -3 303.17 23.40 0 -10 -3 281.17 22.00 0 -10 -3 290.77 22.90 0 -10 3 239.48 22.70 0 10 4 64.09 13.10 0 10 -4 16.90 14.30 0 10 4 42.20 10.20 0 10 -4 73.79 13.80 0 10 -4 59.19 12.80 0 10 4 42.50 9.20 0 10 4 55.59 10.30 0 -10 4 64.69 15.10 0 -10 4 67.89 13.30 0 -10 -4 54.49 6.90 0 -10 -4 54.19 6.80 0 -10 4 59.39 12.80 0 -10 4 48.80 12.20 0 10 5 120.59 14.00 0 10 -5 128.69 19.00 0 10 5 120.39 16.30 0 10 5 139.29 18.40 0 10 -5 118.69 27.70 0 10 5 118.39 14.40 0 10 -5 91.29 16.90 0 -10 5 114.39 17.70 0 -10 5 125.89 18.60 0 -10 -5 159.98 16.60 0 -10 -5 104.69 14.50 0 -10 5 146.59 22.00 0 -10 5 153.78 19.90 0 10 -6 446.96 53.89 0 10 6 445.56 34.10 0 10 -6 473.45 35.90 0 10 6 474.85 29.50 0 10 6 444.96 29.30 0 10 -6 430.06 35.00 0 10 6 490.95 32.80 0 -10 -6 465.45 31.30 0 -10 -6 464.45 31.40 0 -10 6 496.35 39.50 0 -10 6 454.95 35.70 0 -10 6 487.35 37.10 0 -10 6 538.65 37.00 0 10 7 50.69 12.70 0 10 7 57.09 23.50 0 10 7 40.00 14.50 0 10 -7 58.59 33.80 0 -10 7 39.20 14.90 0 -10 -7 37.70 9.30 0 -10 7 40.20 14.60 0 -10 7 60.89 15.80 0 -10 7 50.49 15.40 0 -10 7 36.20 14.90 0 -10 -7 48.80 10.00 0 -10 -7 69.99 11.10 0 -10 -7 60.59 10.30 0 10 8 29.50 16.00 0 10 -8 -0.10 34.20 0 10 8 18.20 25.30 0 10 8 46.20 14.20 0 -10 8 32.40 16.80 0 -10 8 36.60 17.10 0 -10 8 26.30 16.50 0 -10 8 41.20 19.00 0 11 0 -7.40 7.50 0 11 0 -5.80 5.20 0 11 0 7.50 7.50 0 11 0 -3.90 6.00 0 -11 0 0.00 6.50 0 -11 0 7.50 6.80 0 -11 0 5.20 8.00 0 -11 0 0.00 7.50 0 11 -1 622.44 42.20 0 11 1 678.03 40.80 0 11 1 617.74 41.50 0 11 -1 613.74 39.00 0 11 1 577.04 37.80 0 11 1 589.34 37.70 0 11 -1 568.94 39.90 0 11 -1 646.54 39.60 0 -11 -1 559.54 38.60 0 -11 1 622.34 39.90 0 -11 1 577.24 39.30 0 -11 1 539.05 40.30 0 -11 -1 568.54 38.60 0 -11 1 547.05 38.50 0 -11 -1 591.94 38.80 0 -11 -1 610.44 40.40 0 11 -2 238.38 22.50 0 11 2 235.98 22.20 0 11 2 263.67 25.10 0 11 2 278.47 22.00 0 11 2 213.48 20.50 0 11 -2 236.68 22.40 0 11 -2 253.67 30.70 0 11 -2 201.38 23.90 0 -11 -2 266.47 24.00 0 -11 -2 306.97 24.00 0 -11 2 256.47 23.60 0 -11 2 267.17 23.50 0 -11 -2 224.88 21.70 0 -11 -2 266.07 22.90 0 -11 2 264.47 23.80 0 -11 2 303.57 26.60 0 11 -3 142.19 21.00 0 11 3 109.49 15.00 0 11 3 77.69 15.70 0 11 3 124.59 15.70 0 11 3 136.39 17.70 0 11 -3 123.89 25.70 0 11 -3 85.89 17.30 0 11 -3 88.39 17.20 0 -11 -3 113.59 16.40 0 -11 -3 120.29 16.00 0 -11 3 107.59 18.80 0 -11 -3 97.49 15.20 0 -11 -3 88.39 14.40 0 11 4 3.40 9.40 0 11 -4 16.10 17.00 0 11 -4 16.30 9.70 0 11 4 8.80 8.70 0 11 4 20.40 8.80 0 11 -4 13.20 9.50 0 11 4 18.90 8.00 0 -11 4 -1.50 8.20 0 -11 4 4.80 9.10 0 -11 -4 22.40 9.30 0 -11 -4 6.80 6.30 0 -11 4 13.50 10.80 0 -11 -4 17.30 8.70 0 -11 4 31.00 10.10 0 11 5 434.36 30.30 0 11 -5 413.46 46.70 0 11 -5 440.46 35.00 0 11 5 455.65 33.20 0 11 5 449.06 30.90 0 11 -5 439.56 35.70 0 11 5 477.05 35.30 0 -11 5 488.75 38.90 0 -11 -5 452.05 33.00 0 -11 -5 472.05 33.00 0 -11 5 472.75 35.80 0 -11 5 482.05 36.00 0 -11 5 500.75 37.00 0 11 6 79.49 12.80 0 11 -6 109.69 19.00 0 11 -6 108.19 28.50 0 11 6 80.99 12.20 0 11 6 95.29 16.40 0 11 6 90.49 17.30 0 11 -6 96.19 17.80 0 -11 -6 99.89 15.40 0 -11 6 121.79 19.60 0 -11 -6 80.69 14.70 0 -11 6 108.49 19.00 0 -11 6 119.69 19.50 0 11 7 213.18 23.80 0 11 7 190.18 34.70 0 11 -7 128.49 40.30 0 11 7 180.28 24.40 0 -11 -7 169.18 19.40 0 -11 7 187.18 27.00 0 -11 -7 182.48 20.10 0 -11 7 181.28 27.30 0 11 8 7.30 16.80 0 11 8 27.70 13.90 0 11 8 -18.80 23.60 0 -11 8 21.20 19.30 0 -11 8 16.50 20.90 0 -11 8 39.70 18.10 0 -11 8 30.30 18.50 0 12 0 492.55 34.30 0 12 0 522.85 36.80 0 12 0 512.55 35.00 0 12 0 422.66 36.60 0 -12 0 520.05 35.90 0 -12 0 460.65 34.80 0 -12 0 507.25 37.40 0 -12 0 478.45 35.20 0 12 1 14.20 9.80 0 12 1 10.10 7.10 0 12 -1 -3.00 6.80 0 12 -1 2.30 11.60 0 12 -1 4.10 7.20 0 12 1 8.80 7.90 0 12 1 13.30 7.80 0 -12 1 0.60 7.80 0 -12 1 12.80 9.90 0 -12 1 8.50 9.30 0 -12 -1 14.40 8.60 0 -12 1 11.70 9.00 0 -12 -1 9.70 7.30 0 -12 -1 16.50 9.70 0 -12 -1 16.00 8.10 0 12 2 551.74 40.60 0 12 2 582.24 37.50 0 12 2 579.74 39.60 0 12 2 595.44 38.00 0 12 -2 581.74 39.30 0 12 -2 593.34 57.29 0 12 -2 572.64 39.20 0 -12 2 548.85 41.40 0 -12 -2 580.34 39.30 0 -12 2 583.14 40.00 0 -12 -2 505.55 37.60 0 -12 -2 568.14 38.70 0 -12 2 490.15 38.30 0 -12 2 595.34 40.30 0 -12 -2 564.04 38.70 0 12 -3 534.75 48.50 0 12 3 523.45 34.90 0 12 3 496.55 34.30 0 12 3 555.54 37.00 0 12 3 502.95 37.60 0 12 -3 499.15 36.90 0 12 -3 499.55 36.70 0 -12 -3 562.04 36.80 0 -12 -3 491.95 34.80 0 -12 3 521.95 38.90 0 -12 -3 511.55 35.60 0 -12 3 462.35 36.30 0 -12 -3 488.85 34.60 0 -12 3 416.56 35.40 0 -12 3 443.76 36.10 0 12 4 27.20 12.50 0 12 -4 34.60 11.90 0 12 4 32.10 10.00 0 12 4 18.40 9.30 0 12 4 38.00 10.80 0 12 -4 45.80 21.80 0 12 -4 12.30 10.10 0 -12 4 52.59 14.40 0 -12 4 21.70 11.70 0 -12 -4 16.40 9.60 0 -12 4 23.00 11.40 0 -12 -4 1.50 7.90 0 -12 -4 28.30 10.30 0 -12 4 26.70 11.20 0 -12 -4 24.40 9.30 0 12 5 7.70 9.60 0 12 5 7.90 8.10 0 12 -5 3.20 10.00 0 12 5 1.80 13.50 0 12 5 3.20 7.60 0 12 -5 -26.90 18.70 0 12 -5 4.90 10.60 0 -12 -5 -2.00 9.40 0 -12 5 -6.20 10.60 0 -12 5 1.70 10.70 0 -12 -5 7.80 10.20 0 -12 5 -14.10 10.20 0 12 6 92.79 17.70 0 12 -6 129.59 37.00 0 12 6 104.39 14.70 0 12 6 102.29 15.10 0 -12 6 104.29 20.10 0 -12 -6 107.19 17.90 0 -12 6 103.39 19.90 0 -12 6 145.69 24.90 0 -12 6 90.99 19.70 0 -12 -6 117.39 18.20 0 12 7 184.48 37.50 0 12 7 232.08 30.00 0 12 -7 209.58 48.00 0 12 7 233.98 25.70 0 -12 7 227.08 33.40 0 -12 7 185.98 28.00 0 -12 -7 257.27 24.50 0 -12 -7 177.08 21.10 0 12 8 18.30 15.90 0 12 8 42.70 30.80 0 12 8 22.20 19.10 0 -12 8 12.00 19.50 0 -12 8 13.50 22.60 0 -12 8 27.50 22.80 0 -12 8 51.19 21.30 0 13 0 -1.60 7.10 0 13 0 -2.30 7.10 0 13 0 4.40 10.20 0 13 0 1.40 8.50 0 -13 0 3.80 9.00 0 -13 0 -10.10 8.80 0 -13 0 3.40 8.40 0 -13 0 -2.20 8.50 0 13 -1 38.20 14.20 0 13 1 17.60 9.70 0 13 1 36.80 12.90 0 13 1 47.10 12.90 0 13 -1 32.90 11.30 0 13 -1 47.10 11.70 0 13 1 16.30 9.70 0 -13 -1 35.80 11.30 0 -13 -1 13.20 11.90 0 -13 -1 46.70 13.00 0 -13 1 43.50 13.70 0 -13 1 32.00 11.90 0 -13 -1 59.39 13.60 0 -13 1 36.00 12.70 0 -13 1 42.40 12.30 0 13 -2 714.03 45.50 0 13 -2 648.04 47.90 0 13 2 707.63 43.80 0 13 -2 677.13 44.90 0 13 2 713.83 47.70 0 13 2 667.13 45.00 0 13 2 582.44 42.00 0 13 -2 693.53 54.39 0 -13 -2 727.73 46.50 0 -13 -2 638.94 44.50 0 -13 2 635.34 45.10 0 -13 2 633.74 44.80 0 -13 2 650.63 46.60 0 -13 -2 698.83 44.80 0 -13 2 571.14 43.70 0 -13 -2 590.64 42.90 0 13 -3 16.20 12.90 0 13 -3 39.40 18.80 0 13 -3 8.30 9.20 0 13 3 11.30 8.50 0 13 3 32.30 12.10 0 13 3 17.70 11.40 0 13 3 2.50 7.70 0 13 -3 21.70 10.70 0 -13 -3 2.80 8.60 0 -13 3 24.20 12.00 0 -13 -3 32.80 12.60 0 -13 3 1.90 10.40 0 -13 3 4.40 11.60 0 -13 3 6.00 10.30 0 13 -4 46.00 14.20 0 13 -4 29.70 13.60 0 13 4 58.99 15.30 0 13 4 41.10 11.50 0 13 4 50.09 11.90 0 13 -4 73.69 24.20 0 13 4 19.80 10.80 0 -13 4 35.10 13.70 0 -13 4 29.40 12.90 0 -13 -4 37.60 13.60 0 -13 4 61.89 15.50 0 -13 -4 28.90 12.60 0 -13 4 31.60 14.90 0 -13 -4 34.80 11.40 0 13 5 7.90 13.60 0 13 5 22.60 10.40 0 13 -5 0.20 11.50 0 13 5 3.50 9.40 0 13 5 -2.10 9.00 0 13 -5 0.40 20.60 0 13 -5 3.20 12.10 0 -13 5 -0.90 12.80 0 -13 -5 1.20 10.60 0 -13 -5 7.70 10.10 0 -13 5 6.70 12.40 0 -13 5 0.30 11.90 0 -13 5 -16.00 11.80 0 13 6 126.89 17.10 0 13 -6 92.89 22.00 0 13 6 68.49 18.10 0 13 -6 72.49 19.70 0 13 6 105.39 16.00 0 13 6 126.89 23.30 0 13 -6 79.39 30.00 0 -13 6 82.19 20.30 0 -13 6 108.39 22.00 0 -13 6 101.39 21.60 0 -13 -6 109.49 19.10 0 -13 6 94.79 24.70 0 -13 -6 93.39 18.10 0 13 7 8.90 17.30 0 13 7 -4.70 14.30 0 -13 -7 5.60 13.80 0 -13 7 -14.10 17.40 0 -13 -7 -10.40 13.00 0 14 0 282.27 30.30 0 14 0 301.17 27.00 0 14 0 238.08 25.10 0 14 0 256.97 27.30 0 -14 0 272.97 27.10 0 -14 0 302.77 28.10 0 -14 0 274.77 29.10 0 -14 0 255.87 26.50 0 14 -1 34.50 12.50 0 14 1 12.00 9.00 0 14 1 29.50 10.50 0 14 -1 18.50 11.40 0 14 1 11.00 10.50 0 14 1 20.90 13.60 0 14 -1 7.40 13.20 0 -14 -1 -4.40 9.80 0 -14 -1 21.90 11.90 0 -14 1 24.70 13.20 0 -14 1 41.20 12.90 0 -14 1 18.90 11.40 0 -14 -1 11.00 11.20 0 -14 1 26.50 11.30 0 -14 -1 3.00 10.40 0 14 2 148.69 21.70 0 14 -2 117.89 22.30 0 14 2 82.49 16.10 0 14 2 140.29 22.90 0 14 -2 122.49 27.10 0 14 -2 131.79 22.90 0 14 -2 119.39 23.00 0 14 2 117.29 17.70 0 -14 2 92.19 18.70 0 -14 2 96.09 21.30 0 -14 -2 120.29 19.30 0 -14 2 140.89 24.10 0 -14 -2 72.19 17.70 0 -14 -2 137.09 20.70 0 -14 2 98.59 22.80 0 -14 -2 129.19 20.60 0 14 -3 749.13 53.59 0 14 3 910.11 53.69 0 14 -3 876.81 56.29 0 14 3 784.32 51.69 0 14 3 867.01 54.59 0 14 -3 814.42 67.59 0 14 3 858.91 56.89 0 14 -3 795.72 57.09 0 -14 3 829.92 55.59 0 -14 -3 781.62 52.49 0 -14 3 827.92 54.99 0 -14 3 856.31 58.69 0 -14 3 839.02 55.39 0 14 -4 206.38 27.30 0 14 4 190.38 23.30 0 14 4 215.88 24.70 0 14 4 190.18 28.50 0 14 4 265.77 24.40 0 14 -4 209.18 37.30 0 14 -4 198.18 28.30 0 -14 4 169.68 25.50 0 -14 4 188.78 26.50 0 -14 4 179.48 26.60 0 -14 4 219.88 30.80 0 -14 -4 221.98 26.60 0 -14 -4 145.89 22.90 0 -14 -4 197.38 22.20 0 14 -5 -14.30 13.70 0 14 -5 -8.80 13.90 0 14 5 10.70 11.80 0 14 5 -6.80 12.90 0 14 -5 13.80 20.90 0 14 5 -1.20 10.40 0 14 5 -8.10 10.20 0 -14 5 13.00 13.90 0 -14 5 3.20 13.00 0 -14 -5 -5.10 12.60 0 -14 -5 4.10 13.70 0 -14 5 15.10 14.00 0 -14 5 -9.10 13.00 0 14 6 287.57 29.70 0 14 6 323.97 36.50 0 14 -6 347.37 56.29 0 14 6 316.57 37.00 0 14 6 332.27 30.00 0 -14 -6 413.26 35.30 0 -14 6 256.07 37.40 0 -14 -6 338.07 33.70 0 14 7 5.90 16.90 0 14 7 55.49 24.00 0 -14 -7 52.19 17.90 0 -14 7 46.50 21.90 0 -14 7 33.00 22.20 0 -14 -7 68.99 19.50 0 15 0 -21.50 9.10 0 15 0 -8.80 12.60 0 15 0 -13.60 9.10 0 15 0 15.10 12.30 0 -15 0 -6.00 10.40 0 -15 0 23.30 12.50 0 -15 0 0.50 10.00 0 -15 0 -3.70 11.50 0 15 1 1112.39 63.59 0 15 1 1099.39 65.69 0 15 1 1070.39 62.99 0 15 -1 1025.20 68.09 0 15 -1 978.20 62.59 0 15 -1 1039.80 63.89 0 15 1 1014.70 67.29 0 -15 -1 905.21 61.99 0 -15 1 1057.89 68.19 0 -15 -1 1048.40 64.09 0 -15 1 930.61 62.79 0 -15 -1 949.71 62.99 0 -15 -1 1069.09 66.09 0 -15 1 918.11 62.59 0 -15 1 1007.30 63.99 0 15 2 29.40 12.10 0 15 2 25.90 16.30 0 15 -2 44.20 14.60 0 15 -2 55.59 20.60 0 15 2 24.20 12.30 0 15 -2 41.70 14.30 0 15 -2 70.89 20.40 0 15 2 33.90 13.30 0 -15 -2 18.50 12.10 0 -15 2 43.40 14.90 0 -15 2 26.60 13.40 0 -15 -2 23.80 12.70 0 -15 2 32.70 15.70 0 -15 -2 24.20 13.00 0 -15 -2 12.50 14.80 0 -15 2 21.40 13.00 0 15 3 26.00 12.40 0 15 -3 18.40 19.90 0 15 3 33.20 12.50 0 15 -3 33.70 18.40 0 15 -3 15.60 13.30 0 15 3 30.50 13.30 0 15 3 15.00 15.20 0 15 -3 8.20 12.40 0 -15 -3 40.40 15.00 0 -15 3 23.00 15.20 0 -15 -3 42.60 15.80 0 -15 3 25.70 14.40 0 -15 -3 18.70 15.30 0 -15 -3 11.00 13.90 0 -15 3 19.80 15.20 0 -15 3 46.40 16.50 0 15 4 84.49 16.90 0 15 -4 93.99 27.30 0 15 4 71.59 19.00 0 15 4 83.49 17.10 0 15 -4 70.69 18.80 0 15 4 69.29 20.40 0 15 -4 83.39 20.80 0 -15 4 100.09 20.50 0 -15 -4 76.09 16.30 0 -15 4 77.59 19.40 0 -15 -4 62.99 17.10 0 -15 -4 94.19 18.90 0 -15 4 42.00 17.70 0 -15 -4 49.20 17.10 0 -15 4 96.39 22.00 0 15 5 172.48 24.30 0 15 5 202.58 27.40 0 15 -5 179.68 41.80 0 15 5 161.08 28.40 0 15 5 169.38 24.20 0 -15 -5 193.18 27.90 0 -15 5 224.58 33.60 0 -15 -5 202.98 28.20 0 -15 5 197.18 30.80 0 -15 5 209.28 29.80 0 15 6 18.50 16.20 0 15 6 -17.40 13.10 0 15 6 -21.20 13.50 0 15 6 2.90 18.10 0 -15 6 14.00 18.10 0 -15 6 23.00 19.30 0 -15 -6 2.80 16.20 0 -15 -6 -19.40 16.60 0 15 7 30.20 19.20 0 15 7 0.00 25.60 0 -15 -7 8.10 18.40 0 -15 -7 28.40 19.80 0 -15 7 9.90 24.50 0 16 0 1193.08 69.59 0 16 0 1133.59 68.59 0 16 0 1030.10 71.89 0 -16 0 1077.59 68.69 0 -16 0 1040.00 68.19 0 -16 0 1152.68 72.59 0 -16 0 1064.39 68.99 0 16 -1 36.30 14.40 0 16 1 27.90 17.10 0 16 1 31.50 13.00 0 16 1 48.00 15.30 0 16 -1 55.99 20.90 0 16 1 57.69 16.90 0 16 -1 36.70 14.20 0 -16 -1 23.50 15.90 0 -16 1 34.30 16.60 0 -16 -1 69.79 16.60 0 -16 1 17.90 13.90 0 -16 1 19.80 13.70 0 -16 -1 35.40 14.70 0 -16 1 48.60 16.80 0 -16 -1 1.60 13.10 0 16 -2 86.09 26.80 0 16 2 87.69 18.50 0 16 2 76.79 17.90 0 16 2 77.59 17.50 0 16 -2 84.79 18.40 0 16 2 100.39 22.50 0 16 -2 64.39 17.70 0 16 -2 96.49 22.80 0 -16 2 53.99 17.40 0 -16 2 79.89 20.70 0 -16 -2 32.10 16.50 0 -16 2 84.89 21.90 0 -16 -2 60.79 18.10 0 -16 -2 73.59 19.20 0 -16 2 98.49 20.90 0 -16 -2 42.80 16.70 0 16 -3 33.60 15.20 0 16 -3 68.19 18.60 0 16 3 35.70 18.20 0 16 3 30.30 14.20 0 16 -3 54.69 21.50 0 16 3 14.80 14.20 0 16 -3 70.59 29.70 0 16 3 43.40 18.10 0 -16 -3 30.10 16.20 0 -16 -3 35.90 15.80 0 -16 3 33.80 15.70 0 -16 3 54.69 18.00 0 -16 3 30.40 17.00 0 -16 3 78.09 19.40 0 -16 -3 14.40 15.20 0 16 4 34.40 19.30 0 16 -4 15.80 30.50 0 16 4 -7.50 13.20 0 16 4 -3.60 13.20 0 16 -4 24.90 19.40 0 16 -4 7.20 17.70 0 16 4 -8.90 12.80 0 -16 4 13.80 16.80 0 -16 -4 7.40 13.90 0 -16 -4 15.30 16.30 0 -16 -4 3.80 15.10 0 -16 -4 16.40 16.40 0 -16 4 6.50 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10 -3 1 44.40 16.90 -10 3 -2 239.68 31.00 -10 3 -2 262.17 35.20 10 3 2 209.28 29.70 10 3 2 248.58 32.90 -10 3 -2 262.47 30.00 -10 -3 -2 211.68 32.40 10 -3 2 226.38 31.70 10 -3 2 258.77 34.10 -10 -3 -2 261.37 34.60 10 -3 2 216.18 33.00 -10 -3 -2 209.48 30.90 -10 -3 -2 249.58 14.90 10 3 3 17.90 15.50 -10 3 -3 14.30 13.60 10 3 3 16.50 15.60 -10 3 -3 -17.60 13.80 -10 3 -3 8.30 15.20 10 3 3 -0.40 14.00 10 -3 3 -15.30 15.10 -10 -3 -3 -24.50 15.40 -10 -3 -3 -10.50 14.70 -10 -3 -3 7.40 14.50 10 3 4 63.99 21.00 10 3 4 70.79 22.40 -10 3 -4 52.49 19.90 -10 3 -4 39.30 17.60 10 3 4 63.69 20.50 -10 3 -4 65.89 21.00 -10 3 -4 85.19 20.30 -10 -3 -4 63.69 21.00 10 -3 4 70.09 23.50 10 -3 4 89.19 24.30 10 -3 4 82.79 25.80 10 3 5 1.20 18.20 10 3 5 21.30 21.00 -10 3 -5 10.50 19.40 10 3 5 10.60 17.50 -10 -3 -5 2.60 11.30 10 -3 5 -12.40 20.50 10 -3 5 -6.30 19.40 -10 -3 -5 0.90 14.60 10 -3 5 6.80 21.40 -10 -3 -5 -2.80 17.90 -10 -3 -5 5.70 18.60 -10 3 -6 24.00 14.40 -10 3 -6 19.00 26.20 10 3 6 72.19 30.80 10 3 6 16.20 23.10 10 3 6 18.40 21.40 10 -3 6 27.00 26.50 -10 -3 -6 88.69 24.40 10 -3 6 42.40 29.20 -10 -3 -6 70.89 25.10 10 -3 6 18.30 25.30 -10 4 8 48.30 33.60 -10 4 8 11.10 21.90 10 -4 -8 14.90 11.00 10 -4 -8 5.20 11.30 -10 -4 8 45.00 25.20 -10 -4 8 19.10 25.10 -10 4 7 6.10 20.60 -10 4 7 -16.10 23.00 -10 -4 7 8.30 18.90 -10 -4 7 8.70 21.00 10 4 -6 155.28 25.70 -10 4 6 195.48 24.20 10 4 -6 196.68 18.40 -10 4 6 170.08 28.50 -10 4 6 187.68 23.60 10 4 -6 140.49 25.10 -10 -4 6 165.48 29.70 -10 -4 6 178.58 35.40 -10 -4 6 185.78 30.10 -10 -4 6 176.18 28.30 -10 4 5 457.05 36.90 10 4 -5 432.86 37.60 10 4 -5 439.36 38.30 10 4 -5 493.75 34.40 -10 4 5 525.85 38.70 -10 4 5 418.86 41.90 -10 -4 5 473.85 49.10 -10 -4 5 482.25 43.30 10 -4 -5 433.16 39.00 -10 -4 5 458.95 42.50 10 -4 -5 537.75 41.60 -10 -4 5 429.56 44.70 10 4 -4 245.18 24.40 10 4 -4 289.27 29.20 -10 4 4 195.68 30.90 -10 4 4 247.58 26.60 10 4 -4 242.68 29.40 -10 4 4 197.68 26.30 -10 -4 4 283.27 35.30 10 -4 -4 268.77 32.10 -10 -4 4 257.67 33.40 10 -4 -4 250.07 26.20 -10 -4 4 262.07 36.70 10 -4 -4 279.07 30.50 -10 -4 4 181.38 28.80 -10 4 3 5.50 10.90 10 4 -3 -4.90 10.60 10 4 -3 2.30 9.60 10 4 -3 -2.70 10.60 -10 4 3 12.10 14.00 -10 4 3 -3.80 10.50 10 -4 -3 -4.30 11.60 -10 -4 3 1.70 13.00 10 -4 -3 -2.10 12.10 -10 -4 3 -13.70 12.70 -10 -4 3 2.60 12.20 10 -4 -3 1.50 11.10 -10 -4 3 32.60 15.80 10 4 -2 541.05 62.59 10 4 -2 550.54 70.59 -10 4 2 601.84 48.20 -10 4 2 558.84 42.70 -10 4 2 467.95 40.40 10 4 -2 587.74 43.20 -10 -4 2 505.35 42.60 10 -4 -2 604.64 46.10 -10 -4 2 531.95 49.50 10 -4 -2 535.55 44.60 -10 -4 2 556.74 47.50 10 -4 -2 587.54 45.50 -10 -4 2 593.54 51.69 10 4 -1 673.73 48.60 -10 4 1 689.93 51.39 -10 4 1 576.84 45.60 10 4 -1 583.74 46.50 10 4 -1 598.04 46.40 -10 4 1 645.54 46.80 10 -4 -1 535.75 46.40 -10 -4 1 634.64 43.40 10 -4 -1 644.94 49.60 -10 -4 1 668.43 50.89 -10 -4 1 612.54 49.50 -10 -4 1 594.44 50.29 10 4 0 22.30 14.00 -10 4 0 30.40 14.30 10 4 0 27.20 14.30 10 4 0 16.20 13.20 -10 4 0 6.80 11.30 -10 4 0 1.90 10.80 -10 -4 0 12.10 7.70 10 -4 0 11.80 13.60 10 -4 0 27.40 15.70 10 -4 0 24.50 14.90 -10 -4 0 10.20 14.30 -10 -4 0 5.90 14.80 -10 -4 0 35.20 16.20 10 4 1 526.85 45.00 10 4 1 536.45 45.50 -10 4 -1 571.14 44.80 -10 4 -1 636.24 46.20 -10 4 -1 590.54 47.50 10 4 1 542.85 47.50 10 -4 1 566.94 49.40 10 -4 1 569.74 47.40 -10 -4 -1 585.74 48.70 -10 -4 -1 573.74 30.80 10 -4 1 750.22 51.99 -10 -4 -1 535.95 46.60 -10 -4 -1 536.65 47.30 10 4 2 164.48 27.00 -10 4 -2 204.78 31.50 -10 4 -2 192.38 27.10 10 4 2 219.08 32.20 10 4 2 187.18 29.20 -10 4 -2 199.58 28.60 10 -4 2 207.68 30.50 -10 -4 -2 206.98 31.50 -10 -4 -2 278.27 35.40 10 -4 2 205.18 30.70 -10 -4 -2 147.09 26.70 10 -4 2 174.08 30.30 -10 4 -3 0.70 13.40 -10 4 -3 11.00 13.40 10 4 3 -5.20 14.80 -10 4 -3 26.90 17.70 10 4 3 1.40 14.70 10 4 3 34.10 18.00 -10 -4 -3 17.50 17.40 10 -4 3 14.70 16.90 -10 -4 -3 28.90 18.00 -10 -4 -3 46.70 17.90 10 -4 3 40.10 20.60 10 -4 3 52.69 20.70 10 4 4 329.17 41.30 10 4 4 333.37 37.00 -10 4 -4 255.57 33.00 -10 4 -4 336.57 37.50 -10 4 -4 279.87 34.70 10 4 4 282.67 35.00 -10 4 -4 308.77 34.60 10 -4 4 244.78 35.00 -10 -4 -4 245.28 35.20 10 -4 4 268.57 41.00 10 -4 4 268.27 37.10 -10 4 -5 -16.30 16.30 10 4 5 -10.60 17.40 10 4 5 -4.50 18.00 10 4 5 26.50 21.20 -10 4 -5 -2.60 20.30 -10 -4 -5 -16.00 19.40 -10 -4 -5 -14.90 14.30 -10 -4 -5 0.40 11.60 10 -4 5 -30.20 19.30 10 -4 5 6.40 21.70 10 -4 5 -2.00 20.80 -10 -4 -5 -35.60 18.40 -10 4 -6 -17.00 15.50 10 4 6 32.70 26.10 10 4 6 15.20 22.80 -10 4 -6 13.10 25.70 10 4 6 13.50 23.30 10 -4 6 13.00 24.20 10 -4 6 -15.20 25.10 10 -4 6 -11.50 25.70 -10 -4 -6 -2.30 22.70 -10 -4 -6 -21.00 21.10 -10 5 8 26.70 34.70 -10 5 8 -4.30 23.00 -10 -5 8 12.50 29.10 10 -5 -8 12.50 10.90 -10 -5 8 10.00 25.50 10 -5 -8 -2.00 11.10 -10 5 7 230.98 34.20 10 -5 -7 178.88 22.30 -10 -5 7 200.98 36.20 10 -5 -7 223.38 24.00 -10 -5 7 248.28 45.30 -10 5 6 69.69 16.20 10 5 -6 74.29 13.00 -10 5 6 81.49 16.70 -10 5 6 84.29 23.60 -10 -5 6 96.29 22.80 -10 -5 6 142.39 26.00 -10 -5 6 59.29 25.50 10 -5 -6 82.89 19.70 10 -5 -6 83.29 18.70 -10 -5 6 90.29 24.80 10 5 -5 7.90 10.20 -10 5 5 24.50 16.40 10 5 -5 20.60 13.40 10 5 -5 26.10 13.80 10 -5 -5 9.80 7.40 -10 -5 5 26.20 15.50 -10 -5 5 32.80 17.50 10 -5 -5 4.70 9.20 -10 -5 5 -6.20 17.40 -10 -5 5 -0.40 16.10 10 5 -4 10.30 12.30 -10 5 4 37.60 14.70 10 5 -4 24.20 12.50 -10 5 4 9.50 14.60 -10 5 4 12.50 11.50 10 5 -4 49.99 14.90 -10 -5 4 18.00 16.20 -10 -5 4 56.09 19.80 -10 -5 4 2.50 15.30 10 -5 -4 33.40 15.40 -10 -5 4 59.39 19.40 10 -5 -4 46.00 14.10 10 -5 -4 29.20 14.90 -10 5 3 556.24 46.30 10 5 -3 486.25 40.60 10 5 -3 535.95 42.30 10 5 -3 532.55 39.50 -10 5 3 519.55 40.00 -10 5 3 545.25 40.80 -10 -5 3 482.15 44.70 10 -5 -3 546.25 43.10 -10 -5 3 437.96 44.00 -10 -5 3 434.36 43.20 10 -5 -3 514.85 42.00 -10 -5 3 507.55 43.50 10 -5 -3 476.45 41.90 -10 5 2 42.50 17.70 10 5 -2 32.60 14.70 10 5 -2 59.59 16.20 -10 5 2 37.50 14.60 -10 5 2 64.99 15.90 10 5 -2 55.99 15.60 -10 -5 2 31.40 12.90 -10 -5 2 61.29 18.90 -10 -5 2 25.10 17.00 10 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13.90 -10 -6 3 49.50 19.70 -10 -6 3 13.10 15.60 -10 -6 3 7.70 12.80 10 -6 -3 9.30 13.10 10 -6 -3 25.60 13.30 10 6 -2 167.98 24.10 10 6 -2 142.09 24.40 -10 6 2 133.29 22.10 10 6 -2 173.78 25.50 -10 6 2 173.38 28.10 -10 6 2 121.09 21.20 -10 -6 2 170.48 28.20 10 -6 -2 102.99 22.60 -10 -6 2 142.59 27.10 10 -6 -2 135.89 23.70 -10 -6 2 151.78 22.90 10 -6 -2 141.99 25.60 -10 -6 2 98.69 22.40 10 6 -1 -15.60 10.80 -10 6 1 19.30 14.70 -10 6 1 -3.80 11.30 10 6 -1 3.90 11.90 10 6 -1 -17.30 10.60 -10 6 1 0.80 11.50 10 -6 -1 -27.90 11.90 -10 -6 1 -30.10 13.30 -10 -6 1 -12.90 13.60 -10 -6 1 6.60 16.30 10 -6 -1 9.50 14.10 10 -6 -1 -29.40 12.40 -10 6 0 85.39 21.30 10 6 0 65.49 19.00 10 6 0 66.59 19.10 -10 6 0 80.99 18.10 -10 6 0 63.39 16.40 -10 -6 0 80.09 9.80 -10 -6 0 78.69 22.20 10 -6 0 76.89 19.50 -10 -6 0 73.69 22.10 -10 -6 0 105.29 23.40 10 -6 0 79.29 21.60 10 -6 0 72.99 20.60 10 6 1 179.68 27.10 -10 6 -1 151.28 27.00 10 6 1 129.49 23.40 -10 6 -1 210.88 28.10 10 6 1 129.39 23.50 -10 6 -1 122.59 22.90 10 -6 1 150.58 29.00 -10 -6 -1 108.39 23.40 -10 -6 -1 149.69 29.20 -10 -6 -1 135.89 26.30 10 -6 1 127.49 25.20 10 -6 1 192.48 29.50 -10 6 -2 157.78 26.80 -10 6 -2 122.29 21.60 10 6 2 134.09 23.40 -10 6 -2 138.39 23.80 10 6 2 108.89 24.80 10 6 2 138.59 24.80 10 -6 2 133.69 28.10 -10 -6 -2 205.48 32.50 -10 -6 -2 119.59 25.80 10 -6 2 127.89 27.10 -10 -6 -2 86.29 23.20 10 -6 2 132.59 26.70 -10 6 -3 180.98 28.70 10 6 3 190.48 28.10 10 6 3 161.98 29.60 10 6 3 150.18 26.10 10 -6 3 206.38 33.20 -10 -6 -3 141.59 27.00 -10 -6 -3 141.79 29.60 10 -6 3 139.69 28.20 -10 -6 -3 160.68 23.50 10 -6 3 150.28 29.80 -10 -6 -3 159.38 29.60 10 6 4 91.89 25.70 10 6 4 97.39 22.80 -10 6 -4 69.99 27.90 10 6 4 58.69 21.50 -10 6 -4 103.09 23.70 -10 -6 -4 51.89 16.30 10 -6 4 18.40 22.40 10 -6 4 33.60 25.10 10 -6 4 109.39 22.30 10 -6 4 100.39 29.20 10 -6 4 83.69 20.50 10 6 5 31.20 20.70 -10 6 -5 30.60 28.50 -10 6 -5 57.29 21.30 10 6 5 28.20 20.40 10 6 5 -0.20 20.90 -10 -6 -5 27.30 13.20 10 -6 5 35.70 24.50 -10 -6 -5 35.50 15.70 10 -6 5 -0.30 24.30 -10 -6 -5 14.70 21.30 10 -6 5 26.80 25.40 -10 -6 -5 40.30 23.20 10 6 6 26.20 25.50 -10 6 -6 -11.90 27.90 -10 6 -6 16.00 34.10 -10 -6 -6 11.60 30.60 10 -6 6 -0.80 27.60 -10 -6 -6 0.70 28.40 -10 7 8 36.50 25.40 10 -7 -8 14.40 12.40 -10 -7 8 -21.40 29.20 10 -7 -8 23.50 12.10 -10 -7 8 3.70 30.90 -10 7 7 251.87 35.30 10 -7 -7 222.28 25.30 -10 -7 7 239.28 45.10 10 -7 -7 215.78 24.80 -10 -7 7 182.58 35.00 -10 7 6 294.97 37.20 10 7 -6 212.58 31.00 10 7 -6 265.77 34.40 10 7 -6 220.88 23.70 -10 -7 6 256.97 42.90 -10 -7 6 193.58 33.10 -10 -7 6 209.28 34.40 10 -7 -6 194.28 24.50 10 -7 -6 238.28 25.20 -10 -7 6 217.08 35.20 10 7 -5 3.00 11.90 10 7 -5 29.70 24.70 -10 7 5 -6.90 15.90 -10 -7 5 48.10 23.50 -10 -7 5 29.30 19.80 10 -7 -5 4.50 8.50 10 -7 -5 -1.70 14.30 10 -7 -5 3.70 14.80 10 -7 -5 15.30 10.80 10 -7 -5 8.00 10.40 -10 -7 5 22.00 21.80 -10 -7 5 6.80 16.70 10 -7 -5 -1.50 10.20 10 7 -4 727.53 52.09 10 7 -4 671.13 50.59 10 7 -4 762.12 50.09 -10 7 4 732.13 56.49 -10 -7 4 718.93 57.09 -10 -7 4 682.13 57.09 10 -7 -4 688.43 53.49 10 -7 -4 604.44 51.49 10 -7 -4 807.62 45.20 -10 -7 4 726.03 57.49 10 -7 -4 668.73 49.20 -10 -7 4 686.53 56.39 -10 7 3 31.10 13.50 10 7 -3 31.80 15.00 -10 7 3 32.40 18.50 -10 7 3 46.50 15.30 10 7 -3 25.00 14.00 10 7 -3 23.70 13.20 -10 -7 3 34.90 15.00 10 -7 -3 29.80 15.50 -10 -7 3 41.40 17.20 -10 -7 3 23.30 17.40 -10 -7 3 29.50 17.80 10 -7 -3 33.80 16.50 10 -7 -3 32.10 15.80 10 7 -2 268.87 31.10 -10 7 2 244.58 35.00 -10 7 2 273.27 28.80 -10 7 2 304.07 30.00 10 7 -2 299.97 34.40 10 7 -2 231.38 30.20 10 -7 -2 293.17 36.20 -10 -7 2 229.88 33.80 -10 -7 2 259.87 36.40 -10 -7 2 331.27 39.20 10 -7 -2 244.58 33.20 -10 -7 2 283.67 28.70 10 -7 -2 300.87 37.40 10 7 -1 15.50 12.70 -10 7 1 26.80 16.70 10 7 -1 30.10 14.70 -10 7 1 16.10 13.00 -10 7 1 12.90 13.80 10 -7 -1 28.30 16.20 10 -7 -1 4.80 13.90 -10 -7 1 15.00 11.40 -10 -7 1 22.20 16.10 -10 -7 1 9.20 17.60 -10 -7 1 54.39 17.30 10 -7 -1 -9.80 12.30 -10 7 0 550.74 44.00 10 7 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17.30 10 7 4 27.40 16.90 -10 7 -4 4.60 20.30 -10 7 -4 28.00 24.40 10 -7 4 5.90 26.20 10 -7 4 -5.10 14.90 -10 -7 -4 20.90 14.10 10 -7 4 3.30 21.50 10 -7 4 -6.60 15.10 10 -7 4 6.10 25.90 10 7 5 -13.90 19.80 10 7 5 -36.60 18.70 -10 7 -5 -13.40 18.60 10 7 5 -13.90 20.80 -10 7 -5 -1.10 26.70 10 -7 5 16.30 25.30 10 -7 5 18.40 25.70 -10 -7 -5 58.29 26.20 -10 -7 -5 5.10 11.90 -10 -7 -5 -5.70 15.40 10 -7 5 -19.60 23.70 -10 -7 -5 8.80 23.60 -10 8 8 183.78 35.30 10 -8 -8 107.59 17.00 10 -8 -8 94.09 17.00 -10 -8 8 158.48 38.70 -10 -8 8 135.19 47.30 -10 8 7 -26.10 22.50 10 -8 -7 -14.30 11.20 -10 -8 7 -5.70 22.80 10 -8 -7 2.30 12.00 -10 8 6 -3.10 21.10 10 8 -6 1.20 12.50 10 -8 -6 24.90 11.80 -10 -8 6 -22.90 19.90 -10 -8 6 4.80 21.20 10 -8 -6 22.80 12.40 -10 8 5 203.58 33.50 10 8 -5 297.27 31.70 10 8 -5 250.07 28.40 10 8 -5 295.47 32.20 10 -8 -5 203.08 25.60 -10 -8 5 287.47 40.90 -10 -8 5 349.37 41.00 10 -8 -5 263.07 27.80 10 -8 -5 263.37 21.90 -10 -8 5 252.67 36.20 10 -8 -5 301.27 35.40 10 -8 -5 218.78 31.30 -10 -8 5 339.47 68.89 10 8 -4 -8.70 12.40 10 8 -4 8.30 14.00 10 8 -4 32.90 15.80 -10 8 4 38.70 18.10 10 -8 -4 38.90 12.60 10 -8 -4 20.20 14.50 10 -8 -4 33.40 24.90 -10 -8 4 3.30 19.20 -10 -8 4 55.59 23.40 -10 -8 4 34.70 19.60 -10 -8 4 46.30 19.70 10 8 -3 369.66 38.20 10 8 -3 592.74 46.80 -10 8 3 488.05 44.60 10 8 -3 414.06 39.70 10 -8 -3 440.76 40.80 10 -8 -3 423.86 42.30 -10 -8 3 447.56 44.40 -10 -8 3 452.05 46.50 -10 -8 3 521.65 42.90 -10 -8 3 477.25 45.70 10 -8 -3 497.25 44.20 10 8 -2 12.40 12.80 10 8 -2 9.10 12.30 10 8 -2 9.40 12.90 -10 8 2 34.90 18.30 -10 -8 2 9.30 17.30 -10 -8 2 8.70 16.10 -10 -8 2 2.50 9.40 10 -8 -2 18.70 14.90 10 -8 -2 4.90 14.60 10 -8 -2 15.80 15.20 -10 -8 2 4.80 15.30 10 8 -1 9.00 13.40 -10 8 1 20.40 16.50 10 8 -1 -0.30 12.20 10 8 -1 -0.70 11.70 -10 -8 1 4.10 13.50 10 -8 -1 11.30 15.80 -10 -8 1 1.30 16.20 10 -8 -1 31.10 17.50 -10 -8 1 25.70 17.50 -10 8 0 38.20 16.90 10 8 0 34.10 16.10 10 8 0 81.39 19.40 10 8 0 67.09 19.20 -10 -8 0 23.90 20.00 10 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18.90 -10 -8 -4 9.10 15.30 10 -8 4 20.30 17.20 10 -8 4 66.19 25.70 10 -8 4 39.40 25.00 -10 -8 -4 15.00 20.80 10 -8 4 39.20 25.50 10 8 5 29.50 22.50 10 8 5 80.29 25.40 -10 8 -5 87.69 35.40 -10 8 -5 74.89 26.20 10 8 5 54.69 22.70 -10 -8 -5 73.59 31.40 -10 -8 -5 43.90 18.30 10 -8 5 119.69 34.70 -10 -8 -5 8.90 26.80 10 -8 5 55.59 31.50 10 -8 5 38.00 28.40 -10 -8 -5 59.89 14.60 -10 9 7 47.80 26.70 10 -9 -7 34.20 14.60 -10 -9 7 28.60 28.40 -10 -9 7 70.89 33.50 10 -9 -7 43.20 15.50 10 9 -6 160.28 22.30 -10 9 6 143.49 30.00 10 -9 -6 147.29 21.20 10 -9 -6 146.59 21.10 -10 -9 6 166.98 35.40 10 9 -5 28.60 18.70 -10 9 5 14.70 18.70 10 9 -5 22.60 18.70 10 9 -5 3.20 12.40 10 -9 -5 7.70 11.70 10 -9 -5 4.90 12.80 10 -9 -5 23.00 22.30 10 -9 -5 0.40 21.00 -10 -9 5 -6.50 21.30 -10 -9 5 10.30 17.50 -10 -9 5 18.40 21.70 10 -9 -5 6.40 12.60 -10 -9 5 39.40 24.80 10 -9 -5 5.40 10.50 10 9 -4 518.75 43.40 10 9 -4 542.85 43.50 -10 9 4 426.76 45.70 10 -9 -4 534.35 36.60 -10 -9 4 486.05 49.90 10 -9 -4 456.65 43.80 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66.99 23.80 10 -9 0 61.49 25.00 10 -9 0 93.79 25.10 10 -9 0 73.99 17.70 -10 -9 0 94.89 24.20 10 -9 0 112.39 20.60 -10 -9 0 106.79 25.50 -10 -9 0 54.59 24.40 10 9 1 28.40 16.60 10 9 1 -3.10 15.20 10 9 1 17.30 15.00 -10 9 -1 -18.70 16.20 -10 -9 -1 15.90 13.80 10 -9 1 7.80 12.00 10 -9 1 6.00 13.40 10 -9 1 33.40 19.70 -10 -9 -1 -13.10 19.20 -10 -9 -1 -2.10 17.90 -10 -9 -1 1.90 19.60 10 -9 1 18.20 18.40 10 -9 1 24.80 19.00 10 9 2 169.78 28.30 10 9 2 97.79 24.30 -10 9 -2 146.79 28.70 10 9 2 190.88 31.80 10 -9 2 172.48 32.80 -10 -9 -2 150.88 26.20 10 -9 2 153.78 29.40 10 -9 2 183.98 26.20 -10 -9 -2 177.58 33.20 -10 -9 -2 146.29 30.10 10 -9 2 205.68 28.00 10 -9 2 182.18 33.20 -10 -9 -2 137.99 30.30 -10 9 -3 95.99 25.30 10 9 3 84.59 24.40 10 9 3 97.09 23.70 10 9 3 67.69 20.80 -10 -9 -3 7.70 22.70 -10 -9 -3 62.19 17.60 10 -9 3 63.59 25.70 10 -9 3 53.39 24.70 -10 -9 -3 61.89 26.30 10 -9 3 79.29 27.60 -10 -9 -3 62.59 25.80 10 9 4 -25.90 18.90 -10 9 -4 28.70 21.60 -10 9 -4 11.40 28.10 10 9 4 -8.90 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15.10 10 -10 0 19.30 14.50 10 -10 0 14.80 21.10 10 -10 0 24.60 20.30 -10 -10 0 23.90 19.80 -10 -10 0 -5.40 13.50 -10 -10 0 16.80 21.70 10 10 1 167.58 28.70 10 10 1 145.49 25.30 10 10 1 120.09 24.90 -10 10 -1 181.48 32.00 10 -10 1 139.89 24.00 -10 -10 -1 140.79 25.50 10 -10 1 159.78 24.90 -10 -10 -1 152.68 31.10 -10 -10 -1 125.09 30.10 10 -10 1 248.38 38.40 -10 -10 -1 126.19 33.30 10 10 2 335.67 39.50 10 10 2 346.07 39.10 10 10 2 332.97 39.80 -10 10 -2 398.66 43.30 10 -10 2 320.67 46.00 -10 -10 -2 287.47 42.00 10 -10 2 408.26 37.10 10 -10 2 329.77 44.40 10 -10 2 249.58 39.80 10 -10 2 396.36 38.50 -10 -10 -2 398.96 38.40 -10 -10 -2 334.37 44.50 -10 -10 -2 349.87 45.10 -10 10 -3 -4.60 21.80 10 10 3 10.70 18.10 10 10 3 -23.80 18.50 10 10 3 18.40 19.20 10 -10 3 3.10 15.40 -10 -10 -3 0.50 23.50 -10 -10 -3 -20.80 22.30 10 -10 3 7.60 23.90 10 -10 3 -18.80 21.50 10 -10 3 11.70 24.10 -10 -10 -3 20.00 24.00 10 -10 3 4.70 17.20 10 10 4 185.68 30.90 -10 10 -4 154.38 31.80 10 10 4 133.09 31.20 -10 10 -4 153.28 41.10 10 10 4 150.58 27.60 -10 -10 -4 163.88 30.20 10 -10 4 96.39 32.50 -10 -10 -4 117.99 21.90 10 -10 4 58.09 30.20 10 -10 4 157.68 38.40 10 11 -6 -2.20 16.20 -10 -11 6 7.70 20.60 -10 -11 6 14.70 24.50 10 -11 -6 11.60 14.10 -10 -11 6 0.20 30.20 10 -11 -6 -2.90 14.10 -10 11 5 -19.70 20.30 10 11 -5 14.30 14.10 -10 -11 5 0.60 19.00 -10 -11 5 -42.50 28.10 10 -11 -5 -10.70 12.80 10 -11 -5 -6.30 14.40 -10 -11 5 16.40 27.20 10 -11 -5 -5.70 12.90 10 -11 -5 11.00 11.80 -10 -11 5 -25.80 17.70 -10 -11 5 -69.59 31.60 10 11 -4 -15.20 14.30 10 11 -4 14.60 20.30 -10 11 4 2.50 20.80 10 11 -4 22.20 22.10 -10 -11 4 23.80 17.90 -10 -11 4 20.10 18.00 10 -11 -4 22.10 17.80 10 -11 -4 7.50 20.30 10 -11 -4 14.50 12.90 10 -11 -4 11.90 21.20 -10 -11 4 -14.70 23.10 -10 -11 4 -8.20 24.90 10 -11 -4 17.30 15.00 10 -11 -4 8.70 13.50 -10 -11 4 -7.30 22.70 10 11 -3 388.56 38.60 -10 11 3 303.07 40.70 10 11 -3 377.86 38.30 -10 -11 3 254.37 37.30 10 -11 -3 271.07 38.00 10 -11 -3 346.17 32.90 -10 -11 3 309.87 43.30 10 -11 -3 275.67 39.20 10 -11 -3 326.07 32.20 10 -11 -3 354.16 42.20 -10 -11 3 243.28 38.20 10 -11 -3 268.17 30.60 -10 -11 3 286.67 71.79 10 11 -2 -7.70 15.90 10 11 -2 2.60 14.90 10 11 -2 4.30 16.20 -10 11 2 13.30 14.30 10 -11 -2 -16.80 19.20 10 -11 -2 20.90 14.00 10 -11 -2 3.90 18.30 -10 -11 2 23.70 20.40 10 -11 -2 3.30 13.30 -10 -11 2 23.90 16.90 -10 -11 2 -1.20 23.10 -10 -11 2 -18.00 19.20 10 -11 -2 -4.60 18.50 10 -11 -2 -1.00 13.30 10 11 -1 248.38 34.70 10 11 -1 280.77 30.40 -10 11 1 266.27 36.00 10 11 -1 269.77 34.50 10 -11 -1 239.08 31.80 10 -11 -1 246.28 31.10 -10 -11 1 195.48 37.20 10 -11 -1 262.87 40.30 10 -11 -1 273.57 38.30 -10 -11 1 245.48 33.70 10 -11 -1 309.37 40.30 -10 -11 1 289.67 41.40 -10 -11 1 266.47 42.40 -10 11 0 67.89 24.50 10 11 0 58.69 21.00 10 11 0 43.30 16.30 10 11 0 76.09 22.00 10 -11 0 65.69 24.10 -10 -11 0 14.50 24.90 10 -11 0 61.09 20.00 -10 -11 0 40.00 18.30 -10 -11 0 44.10 23.60 10 -11 0 38.20 22.10 10 -11 0 22.20 21.30 -10 -11 0 36.00 23.40 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114.79 33.10 -11 -9 -4 112.59 35.50 -11 -9 -4 84.79 30.00 11 -9 4 84.79 33.70 11 10 -6 121.99 26.80 -11 10 6 -4.50 30.60 11 -10 -6 111.49 22.00 11 -10 -6 91.79 21.00 -11 -10 6 99.59 33.30 -11 10 5 -3.20 26.80 11 10 -5 10.20 18.00 -11 -10 5 16.50 28.90 11 -10 -5 -6.40 15.30 11 -10 -5 15.50 16.30 11 -10 -5 -14.30 14.20 -11 -10 5 -7.00 20.50 11 -10 -5 5.20 13.80 11 10 -4 283.47 34.30 11 10 -4 270.27 36.40 11 10 -4 279.07 35.80 -11 -10 4 323.17 43.60 11 -10 -4 309.57 30.50 -11 -10 4 283.67 46.50 11 -10 -4 214.48 29.00 11 -10 -4 229.38 30.20 -11 -10 4 317.47 37.40 -11 -10 4 240.58 40.90 11 -10 -4 285.77 35.00 11 10 -3 -14.80 17.30 11 10 -3 8.60 15.80 11 10 -3 31.70 18.50 -11 -10 3 -4.00 21.90 11 -10 -3 4.90 19.30 11 -10 -3 11.40 14.60 11 -10 -3 9.50 15.50 -11 -10 3 -23.40 22.00 11 -10 -3 20.70 20.40 -11 -10 3 11.80 26.40 -11 -10 3 -18.50 13.70 11 -10 -3 46.00 22.20 11 -10 -3 8.00 15.40 11 10 -2 6.30 16.40 11 10 -2 -0.20 17.40 11 10 -2 23.80 19.30 11 -10 -2 45.60 21.40 -11 -10 2 26.80 22.00 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138.59 36.90 14 8 0 -10.10 25.10 14 8 0 60.59 32.60 14 8 0 18.30 29.70 14 -8 0 12.60 31.30 -14 -8 0 -1.90 34.80 -14 -8 0 5.40 35.60 14 -8 0 43.30 33.60 14 -8 0 48.20 33.00 -14 -9 3 38.40 20.60 14 -9 -3 52.29 34.00 14 -9 -3 57.19 32.70 14 -9 -3 57.89 34.70 14 9 -2 53.19 31.70 14 9 -2 5.70 29.90 14 -9 -2 83.39 36.00 14 -9 -2 110.39 30.60 -14 -9 2 137.89 42.10 -14 -9 2 56.79 39.90 14 -9 -2 59.19 29.80 14 9 -1 64.39 32.10 14 9 -1 40.50 31.30 14 9 -1 -51.69 21.50 14 -9 -1 8.60 29.00 14 -9 -1 -2.40 34.10 14 -9 -1 -28.90 37.90 14 -9 -1 -20.00 40.40 -14 -9 1 -0.70 37.80 -14 -9 1 34.20 36.40 14 -9 -1 39.10 27.20 15 0 -4 166.28 33.70 -15 0 4 111.69 35.80 15 0 -3 26.90 23.90 -15 0 2 133.09 36.90 15 0 -2 224.28 38.10 -15 0 2 148.19 38.30 15 0 -2 159.98 37.20 15 0 -2 161.38 38.00 15 0 -1 -11.00 28.00 -15 0 1 -11.10 31.10 15 0 -1 3.20 24.40 15 0 -1 -3.80 28.30 -15 0 1 20.10 31.00 15 0 0 -13.60 31.30 -15 0 0 29.90 31.60 15 0 0 3.60 30.10 -15 0 0 -8.80 30.50 15 0 1 -21.60 33.30 15 0 1 12.50 23.80 15 0 1 -18.60 34.60 -15 0 -1 -1.20 33.30 -15 0 -1 27.70 35.40 15 1 -4 19.70 25.60 15 -1 -4 12.60 23.20 -15 -1 4 33.30 28.60 15 1 -3 75.69 42.70 15 1 -3 94.49 27.70 -15 -1 3 54.29 37.80 15 -1 -3 118.59 28.40 -15 -1 3 41.10 27.00 -15 -1 3 75.09 46.00 15 1 -2 62.69 26.40 15 1 -2 61.39 28.70 -15 1 2 62.59 31.20 15 1 -2 55.29 29.70 -15 1 2 41.10 30.10 15 -1 -2 -11.00 29.00 -15 -1 2 -22.80 29.00 15 -1 -2 20.50 26.00 -15 -1 2 26.30 23.20 15 -1 -2 49.70 31.00 -15 -1 2 27.20 29.70 15 1 -1 24.60 30.30 15 1 -1 6.10 24.90 -15 1 1 47.40 32.60 15 1 -1 38.40 30.60 -15 1 1 15.20 31.30 -15 -1 1 -14.20 29.50 15 -1 -1 -59.09 24.60 15 -1 -1 -13.00 28.80 -15 -1 1 -17.90 27.40 15 -1 -1 -11.20 27.70 15 1 0 7.70 28.80 -15 1 0 98.09 35.30 15 1 0 10.60 32.60 -15 1 0 56.19 32.20 15 1 0 59.59 35.90 -15 -1 0 27.80 34.60 -15 -1 0 58.49 35.00 15 -1 0 23.50 34.00 15 -1 0 11.20 34.20 15 -1 0 51.49 35.80 15 1 1 214.98 48.00 -15 1 -1 182.48 41.50 15 1 1 118.89 38.40 15 1 1 132.59 39.80 -15 1 -1 134.69 41.30 -15 -1 -1 83.69 39.30 -15 -1 -1 120.69 41.80 15 -1 1 176.18 45.30 15 -1 1 164.88 43.50 15 -1 1 99.29 41.80 15 2 -4 75.39 27.10 -15 -2 4 25.90 27.00 15 -2 -4 53.19 26.20 15 2 -3 9.80 24.10 15 2 -3 27.40 38.30 15 2 -3 -15.20 30.80 15 -2 -3 -16.70 26.70 -15 -2 3 8.00 40.20 -15 -2 3 -17.90 23.10 -15 -2 3 -26.80 36.70 15 2 -2 146.49 34.40 15 2 -2 120.39 31.70 -15 2 2 147.39 36.10 -15 2 2 102.49 33.40 15 2 -2 81.69 30.40 15 -2 -2 92.49 32.80 15 -2 -2 13.30 34.30 -15 -2 2 75.29 26.80 -15 -2 2 89.99 33.80 -15 -2 2 97.59 35.20 15 -2 -2 77.99 38.00 15 2 -1 355.16 49.70 -15 2 1 373.26 53.49 -15 2 1 328.07 48.70 15 2 -1 341.37 49.20 15 2 -1 482.05 52.39 -15 -2 1 341.57 52.99 15 -2 -1 361.56 52.29 -15 -2 1 329.67 42.00 15 -2 -1 433.26 54.59 -15 -2 1 321.77 51.39 15 -2 -1 319.27 48.60 -15 2 0 13.40 30.70 15 2 0 33.30 30.20 -15 2 0 20.50 33.70 15 2 0 25.50 31.60 15 2 0 0.50 28.30 -15 -2 0 33.70 35.00 15 -2 0 -16.10 31.30 15 -2 0 38.70 35.30 -15 -2 0 6.20 35.00 -15 -2 0 -33.10 15.20 15 -2 0 7.00 31.90 -15 2 -1 93.09 39.40 15 2 1 159.68 41.50 15 2 1 157.38 40.40 -15 2 -1 159.58 43.90 -15 -2 -1 157.08 44.20 15 -2 1 119.79 38.80 -15 -2 -1 129.99 23.60 15 -2 1 58.29 38.30 -15 -2 -1 122.29 43.60 15 3 -4 98.79 27.40 15 -3 -4 137.39 32.20 -15 -3 4 75.09 29.50 15 3 -3 23.20 26.90 15 -3 -3 -26.40 26.60 -15 -3 3 20.30 28.00 15 3 -2 34.10 29.70 15 3 -2 17.60 26.50 -15 3 2 62.59 31.50 -15 3 2 50.99 31.00 15 3 -2 141.79 34.00 -15 -3 2 123.69 36.60 15 -3 -2 13.40 50.79 15 -3 -2 45.10 28.60 -15 -3 2 102.59 36.10 -15 -3 2 37.80 24.60 -15 3 1 -9.00 33.30 15 3 -1 -16.50 29.90 15 3 -1 32.70 31.20 -15 3 1 -32.00 32.40 15 3 -1 25.70 27.30 15 -3 -1 -26.30 27.30 -15 -3 1 44.80 33.80 15 -3 -1 22.40 42.00 -15 -3 1 51.39 34.70 -15 -3 1 1.30 17.60 15 -3 -1 -45.10 32.60 -15 3 0 195.18 42.00 -15 3 0 97.59 37.10 15 3 0 75.69 33.60 15 3 0 131.79 37.50 15 3 0 129.09 38.20 15 -3 0 211.48 44.10 -15 -3 0 102.39 20.60 15 -3 0 134.19 39.00 15 -3 0 100.99 37.80 -15 -3 0 92.19 36.30 -15 -3 0 152.18 40.50 15 4 -4 23.10 25.70 -15 -4 4 72.39 29.60 15 -4 -4 64.39 27.30 15 4 -3 -14.40 24.80 15 -4 -3 -9.50 25.50 -15 -4 3 -21.20 21.20 -15 4 2 28.50 28.50 15 4 -2 -8.10 27.50 15 4 -2 29.70 24.90 15 4 -2 20.70 29.50 -15 4 2 25.10 28.10 -15 -4 2 -22.40 32.40 15 -4 -2 17.40 26.90 15 -4 -2 24.40 33.10 -15 -4 2 24.70 33.80 15 -4 -2 51.49 33.70 -15 -4 2 15.00 20.20 15 4 -1 228.28 40.30 15 4 -1 205.78 42.20 -15 4 1 307.17 53.39 -15 4 1 176.98 44.20 15 -4 -1 139.29 46.60 -15 -4 1 185.68 43.90 15 -4 -1 239.48 43.60 15 -4 -1 177.78 49.80 -15 -4 1 177.08 27.20 -15 -4 1 271.47 48.60 -15 4 0 27.00 33.00 15 4 0 18.30 30.50 -15 4 0 4.70 31.20 15 4 0 59.49 30.30 15 4 0 20.20 31.70 15 -4 0 44.90 35.70 -15 -4 0 10.30 12.80 15 -4 0 2.70 34.80 -15 -4 0 9.30 35.30 -15 -4 0 3.90 35.70 15 -4 0 15.80 31.80 15 5 -3 162.78 33.60 -15 -5 3 130.79 30.70 15 -5 -3 160.78 37.70 -15 5 2 31.40 33.80 15 5 -2 50.99 30.30 15 5 -2 25.30 29.30 -15 5 2 -5.30 39.20 15 5 -2 46.00 29.20 -15 -5 2 35.20 37.20 15 -5 -2 28.00 51.99 15 -5 -2 34.00 27.70 -15 -5 2 3.70 19.10 15 -5 -2 34.50 39.70 -15 -5 2 30.30 37.90 -15 5 1 138.99 36.80 -15 5 1 128.79 37.00 15 5 -1 123.39 38.80 15 5 -1 142.09 34.40 15 5 -1 164.08 41.00 -15 -5 1 131.89 21.10 15 -5 -1 140.89 41.80 15 -5 -1 142.79 41.60 -15 -5 1 166.08 42.20 -15 -5 1 231.18 48.00 15 6 -2 64.39 34.80 15 6 -2 88.49 42.80 15 6 -2 93.29 40.40 -15 -6 2 55.99 20.80 -15 -6 2 12.30 37.60 -15 -6 2 40.60 38.60 15 -6 -2 12.70 30.60 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 71616 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co1 Co 0.31756(3) 0.40262(2) 0.59184(5) 0.01728(14) Uani 1 1 d . . . . . O1 O 0.20829(19) 0.44643(13) 0.3783(3) 0.0230(5) Uani 1 1 d . . . . . O2 O 0.2740(2) 0.27807(13) 0.5287(3) 0.0254(5) Uani 1 1 d . . . . . H2A H 0.226571 0.276706 0.433829 0.038 Uiso 1 1 d R U . . . H2B H 0.237539 0.257657 0.602318 0.038 Uiso 1 1 d R U . . . O3 O 0.42499(19) 0.36096(14) 0.8133(3) 0.0233(5) Uani 1 1 d . . . . . H3A H 0.399388 0.377469 0.901381 0.035 Uiso 1 1 d R U . . . H3B H 0.489047 0.385585 0.821948 0.035 Uiso 1 1 d R U . . . O4 O -0.19314(19) 0.57471(16) 0.2678(3) 0.0274(5) Uani 1 1 d . . . . . O5 O -0.2889(2) 0.56776(17) 0.0014(3) 0.0327(6) Uani 1 1 d . . . . . O6 O 0.1692(2) 0.32976(14) 0.2242(3) 0.0308(5) Uani 1 1 d . . . . . N1 N 0.4489(2) 0.39701(15) 0.4402(3) 0.0192(5) Uani 1 1 d . . . . . N2 N 0.5995(2) 0.47575(15) 0.3659(3) 0.0201(5) Uani 1 1 d . . . . . C1 C -0.0954(3) 0.53308(19) 0.0519(4) 0.0194(6) Uani 1 1 d . . . . . C2 C 0.5584(3) 0.3402(2) 0.2495(5) 0.0319(8) Uani 1 1 d . . . . . H2 H 0.573853 0.296339 0.178589 0.038 Uiso 1 1 calc R U . . . C3 C 0.4724(3) 0.3339(2) 0.3395(4) 0.0271(7) Uani 1 1 d . . . . . H3 H 0.428892 0.284694 0.330723 0.033 Uiso 1 1 calc R U . . . C4 C 0.5134(3) 0.46475(17) 0.4464(4) 0.0178(6) Uani 1 1 d . . . . . C6 C 0.0816(3) 0.45721(18) 0.1176(4) 0.0199(6) Uani 1 1 d . . . . . C7 C 0.6213(3) 0.4129(2) 0.2664(4) 0.0275(7) Uani 1 1 d . . . . . H7 H 0.680981 0.418331 0.206536 0.033 Uiso 1 1 calc R U . . . C8 C -0.0135(3) 0.49118(19) 0.1662(4) 0.0208(6) Uani 1 1 d . . . . . H8 H -0.022578 0.485601 0.280115 0.025 Uiso 1 1 calc R U . . . C10 C -0.2005(3) 0.56200(19) 0.1106(4) 0.0204(6) Uani 1 1 d . . . . . C12 C 0.1615(3) 0.40695(19) 0.2483(4) 0.0198(6) Uani 1 1 d . . . . . O7 O 0.2816(6) 0.6768(4) 0.3595(9) 0.129(2) Uani 1 1 d . . . . . N3 N 0.1220(5) 0.7079(4) 0.4475(8) 0.0841(16) Uani 1 1 d . . . . . C9 C 0.1961(5) 0.6428(5) 0.3973(7) 0.0785(19) Uani 1 1 d . . . . . H9 H 0.181477 0.584856 0.394050 0.094 Uiso 1 1 calc R U . . . C11 C 0.0106(7) 0.6847(5) 0.4672(15) 0.128(4) Uani 1 1 d . . . . . H11A H -0.041330 0.694373 0.360856 0.192 Uiso 1 1 calc R U . . . H11B H -0.011654 0.718323 0.556700 0.192 Uiso 1 1 calc R U . . . H11C H 0.009521 0.625810 0.497264 0.192 Uiso 1 1 calc R U . . . C13 C 0.1543(10) 0.7977(8) 0.4501(16) 0.166(5) Uiso 1 1 d . . . . . H13A H 0.232265 0.802434 0.437626 0.249 Uiso 1 1 calc R U . . . H13B H 0.144941 0.822520 0.557590 0.249 Uiso 1 1 calc R U . . . H13C H 0.106727 0.826759 0.356887 0.249 Uiso 1 1 calc R U . . . O8 O 0.3687(3) 0.5775(3) 0.1644(5) 0.0630(9) Uani 1 1 d G . . . . H8A H 0.329707 0.599231 0.233204 0.094 Uiso 1 1 d G U . . . H8B H 0.332888 0.532644 0.127616 0.094 Uiso 1 1 d G U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Co1 0.0183(2) 0.0181(2) 0.0167(2) 0.00090(14) 0.00646(15) 0.00049(15) O1 0.0266(12) 0.0236(11) 0.0179(10) 0.0006(8) 0.0015(9) 0.0044(9) O2 0.0317(12) 0.0225(11) 0.0224(11) 0.0037(8) 0.0060(9) -0.0048(9) O3 0.0233(11) 0.0255(11) 0.0215(11) 0.0017(8) 0.0054(9) 0.0038(9) O4 0.0210(11) 0.0441(14) 0.0189(11) -0.0031(9) 0.0087(9) 0.0047(10) O5 0.0225(12) 0.0539(16) 0.0218(12) -0.0017(11) 0.0046(9) 0.0111(11) O6 0.0438(15) 0.0243(12) 0.0238(11) -0.0018(9) 0.0045(10) 0.0095(10) N1 0.0203(12) 0.0164(12) 0.0226(12) -0.0009(9) 0.0087(10) -0.0004(9) N2 0.0219(13) 0.0191(12) 0.0217(12) 0.0000(10) 0.0098(10) 0.0001(10) C1 0.0210(15) 0.0220(14) 0.0167(13) -0.0010(11) 0.0072(11) 0.0015(11) C2 0.041(2) 0.0242(16) 0.0349(18) -0.0097(14) 0.0190(16) 0.0002(14) C3 0.0318(18) 0.0196(14) 0.0313(17) -0.0051(13) 0.0092(14) -0.0021(13) C4 0.0215(14) 0.0163(13) 0.0167(13) 0.0013(11) 0.0059(11) 0.0008(11) C6 0.0225(15) 0.0202(14) 0.0175(13) -0.0007(11) 0.0055(11) 0.0021(11) C7 0.0318(18) 0.0264(16) 0.0283(16) -0.0038(13) 0.0163(14) 0.0007(13) C8 0.0244(15) 0.0254(15) 0.0140(13) 0.0012(11) 0.0075(11) 0.0042(12) C10 0.0221(15) 0.0215(14) 0.0190(14) 0.0024(11) 0.0076(12) 0.0021(12) C12 0.0201(14) 0.0258(15) 0.0154(13) 0.0025(11) 0.0084(11) 0.0039(12) O7 0.112(5) 0.130(5) 0.151(6) -0.011(4) 0.043(4) 0.015(4) N3 0.066(3) 0.082(4) 0.107(4) 0.015(3) 0.025(3) -0.002(3) C9 0.045(3) 0.124(6) 0.068(4) 0.001(3) 0.014(3) -0.022(3) C11 0.079(5) 0.091(5) 0.233(11) -0.002(6) 0.081(6) -0.013(4) O8 0.0405(18) 0.069(2) 0.080(3) -0.0151(19) 0.0127(17) -0.0197(17) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Co1 O2 91.58(9) . . ? O1 Co1 O3 177.93(9) . . ? O1 Co1 N1 88.68(9) . . ? O1 Co1 N2 91.89(9) . 3_666 ? O2 Co1 O3 89.54(9) . . ? O2 Co1 N1 90.26(9) . . ? O2 Co1 N2 165.82(9) . 3_666 ? O3 Co1 N1 93.06(9) . . ? O3 Co1 N2 87.44(9) . 3_666 ? O4 Co1 O1 88.22(9) 3_566 . ? O4 Co1 O2 96.89(10) 3_566 . ? O4 Co1 O3 89.91(9) 3_566 . ? O4 Co1 N1 172.28(10) 3_566 . ? O4 Co1 N2 96.96(10) 3_566 3_666 ? N1 Co1 N2 76.08(9) . 3_666 ? C12 O1 Co1 129.2(2) . . ? Co1 O2 H2A 109.4 . . ? Co1 O2 H2B 109.4 . . ? H2A O2 H2B 104.4 . . ? Co1 O3 H3A 109.3 . . ? Co1 O3 H3B 109.4 . . ? H3A O3 H3B 104.5 . . ? C10 O4 Co1 130.1(2) . 3_566 ? C3 N1 Co1 128.3(2) . . ? C4 N1 Co1 115.58(19) . . ? C4 N1 C3 116.2(3) . . ? C4 N2 Co1 114.89(19) . 3_666 ? C4 N2 C7 116.5(3) . . ? C7 N2 Co1 128.5(2) . 3_666 ? C6 C1 C10 121.6(3) 3_565 . ? C8 C1 C6 119.3(3) . 3_565 ? C8 C1 C10 118.9(3) . . ? C3 C2 H2 121.0 . . ? C3 C2 C7 117.9(3) . . ? C7 C2 H2 121.0 . . ? N1 C3 C2 121.4(3) . . ? N1 C3 H3 119.3 . . ? C2 C3 H3 119.3 . . ? N1 C4 N2 126.6(3) . . ? N1 C4 C4 116.6(3) . 3_666 ? N2 C4 C4 116.9(3) . 3_666 ? C1 C6 C12 123.3(3) 3_565 . ? C8 C6 C1 118.6(3) . 3_565 ? C8 C6 C12 118.0(3) . . ? N2 C7 C2 121.4(3) . . ? N2 C7 H7 119.3 . . ? C2 C7 H7 119.3 . . ? C1 C8 C6 122.1(3) . . ? C1 C8 H8 119.0 . . ? C6 C8 H8 119.0 . . ? O4 C10 C1 116.8(3) . . ? O5 C10 O4 125.2(3) . . ? O5 C10 C1 117.9(3) . . ? O1 C12 C6 115.9(3) . . ? O6 C12 O1 125.8(3) . . ? O6 C12 C6 118.1(3) . . ? C9 N3 C13 120.7(7) . . ? C11 N3 C9 118.6(6) . . ? C11 N3 C13 119.9(7) . . ? O7 C9 N3 109.4(7) . . ? O7 C9 H9 125.3 . . ? N3 C9 H9 125.3 . . ? N3 C11 H11A 109.5 . . ? N3 C11 H11B 109.5 . . ? N3 C11 H11C 109.5 . . ? H11A C11 H11B 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? N3 C13 H13A 109.5 . . ? N3 C13 H13B 109.5 . . ? N3 C13 H13C 109.5 . . ? H13A C13 H13B 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? H8A O8 H8B 104.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Co1 O1 2.074(2) . ? Co1 O2 2.091(2) . ? Co1 O3 2.098(2) . ? Co1 O4 2.067(2) 3_566 ? Co1 N1 2.170(3) . ? Co1 N2 2.180(3) 3_666 ? O1 C12 1.255(4) . ? O2 H2A 0.8609 . ? O2 H2B 0.8608 . ? O3 H3A 0.8600 . ? O3 H3B 0.8599 . ? O4 C10 1.257(4) . ? O5 C10 1.251(4) . ? O6 C12 1.251(4) . ? N1 C3 1.350(4) . ? N1 C4 1.328(4) . ? N2 C4 1.332(4) . ? N2 C7 1.334(4) . ? C1 C6 1.401(4) 3_565 ? C1 C8 1.387(4) . ? C1 C10 1.507(4) . ? C2 H2 0.9400 . ? C2 C3 1.373(5) . ? C2 C7 1.380(5) . ? C3 H3 0.9400 . ? C4 C4 1.484(6) 3_666 ? C6 C8 1.390(4) . ? C6 C12 1.514(4) . ? C7 H7 0.9400 . ? C8 H8 0.9400 . ? O7 C9 1.252(8) . ? N3 C9 1.475(9) . ? N3 C11 1.433(8) . ? N3 C13 1.481(14) . ? C9 H9 0.9400 . ? C11 H11A 0.9700 . ? C11 H11B 0.9700 . ? C11 H11C 0.9700 . ? C13 H13A 0.9700 . ? C13 H13B 0.9700 . ? C13 H13C 0.9700 . ? O8 H8A 0.8600 . ? O8 H8B 0.8597 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Co1 O1 C12 O6 2.7(5) . . . . ? Co1 O1 C12 C6 177.33(19) . . . . ? Co1 O4 C10 O5 6.5(5) 3_566 . . . ? Co1 O4 C10 C1 -170.0(2) 3_566 . . . ? Co1 N1 C3 C2 179.4(3) . . . . ? Co1 N1 C4 N2 179.4(2) . . . . ? Co1 N1 C4 C4 -0.7(4) . . . 3_666 ? Co1 N2 C4 N1 179.3(2) 3_666 . . . ? Co1 N2 C4 C4 -0.5(4) 3_666 . . 3_666 ? Co1 N2 C7 C2 -178.0(3) 3_666 . . . ? C1 C6 C8 C1 1.0(5) 3_565 . . . ? C1 C6 C12 O1 120.9(3) 3_565 . . . ? C1 C6 C12 O6 -64.0(4) 3_565 . . . ? C3 N1 C4 N2 -1.3(5) . . . . ? C3 N1 C4 C4 178.6(3) . . . 3_666 ? C3 C2 C7 N2 -0.5(5) . . . . ? C4 N1 C3 C2 0.1(5) . . . . ? C4 N2 C7 C2 -0.5(5) . . . . ? C6 C1 C8 C6 -1.0(5) 3_565 . . . ? C6 C1 C10 O4 -158.9(3) 3_565 . . . ? C6 C1 C10 O5 24.3(4) 3_565 . . . ? C7 N2 C4 N1 1.5(5) . . . . ? C7 N2 C4 C4 -178.4(3) . . . 3_666 ? C7 C2 C3 N1 0.7(5) . . . . ? C8 C1 C10 O4 25.1(4) . . . . ? C8 C1 C10 O5 -151.7(3) . . . . ? C8 C6 C12 O1 -62.9(4) . . . . ? C8 C6 C12 O6 112.2(3) . . . . ? C10 C1 C8 C6 175.1(3) . . . . ? C12 C6 C8 C1 -175.4(3) . . . . ? C11 N3 C9 O7 169.3(8) . . . . ? C13 N3 C9 O7 -0.8(10) . . . . ?