#------------------------------------------------------------------------------ #$Date: 2024-09-26 01:33:43 +0300 (Thu, 26 Sep 2024) $ #$Revision: 294892 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/93/7249385.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7249385 loop_ _publ_author_name 'Jeon, Ie-Rang' 'Jeannin, olivier' 'Robert, Antoine' 'Barriere, Frederic' 'Fourmigu\'e, Marc' _publ_section_title ; N-iodophtalimide as halogen bond donor, a comparison with N-iodosuccinimide and N-iodosaccharin† ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D4CE00654B _journal_year 2024 _chemical_formula_sum 'C20 H20 I2 N4 O4' _chemical_formula_weight 634.2 _chemical_name_common (NISucc)2(o-Me2bipy) _chemical_name_systematic Bis(N-iodosuccinimide)(5,5?-dimethyl-2,2?-bipyridine) _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _symmetry_cell_setting monoclinic _symmetry_Int_Tables_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _audit_conform_dict_location ftp://ftp.iucr.org/pub/cif_core.dic _audit_conform_dict_name cif_core.dic _audit_conform_dict_version 2.4.3 _audit_creation_date 2024-03-22T13:54:25-00:00 _audit_creation_method 'WinGX routine CIF_UPDATE' _audit_update_record ; 2024-06-27 deposited with the CCDC. 2024-09-25 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 94.164(4) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 8.4092(8) _cell_length_b 16.8459(18) _cell_length_c 15.5232(16) _cell_measurement_reflns_used 9970 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 27.5 _cell_measurement_theta_min 2.71 _cell_measurement_wavelength 0.71073 _cell_volume 2193.2(4) _computing_cell_refinement 'APEX3 (Bruker, 2015)' _computing_data_collection 'Bruker APEX3 (Bruker, 2015)' _computing_data_reduction 'SAINT (Bruker, 2014)' _computing_molecular_graphics 'Ortep for Windows (Farrugia, 2012)' _computing_publication_material 'WinGX publication routines (Farrugia, 2012)' _computing_structure_refinement 'SHELXL-2019/2 (Sheldrick, 2019)' _diffrn_ambient_temperature 150(2) _diffrn_detector CMOS-PHOTON70 _diffrn_detector_area_resol_mean 7.39 _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device_type 'D8 VENTURE Bruker AXS' _diffrn_measurement_method 'rotation images' _diffrn_orient_matrix_UB_11 0.00003 _diffrn_orient_matrix_UB_12 0.059337 _diffrn_orient_matrix_UB_13 0.001847 _diffrn_orient_matrix_UB_21 0.047621 _diffrn_orient_matrix_UB_22 0.001553 _diffrn_orient_matrix_UB_23 -0.057161 _diffrn_orient_matrix_UB_31 -0.109309 _diffrn_orient_matrix_UB_32 0.000693 _diffrn_orient_matrix_UB_33 -0.030018 _diffrn_radiation_monochromator 'multilayer monochromator' _diffrn_radiation_probe x-ray _diffrn_radiation_source 'Incoatec microfocus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0367 _diffrn_reflns_av_unetI/netI 0.0231 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 37649 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.508 _diffrn_reflns_theta_min 2.428 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 2.902 _exptl_absorpt_correction_T_max 0.944 _exptl_absorpt_correction_T_min 0.757 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; [Sheldrick, G.M. (2014). SADABS Bruker AXS Inc., Madison, Wisconsin, USA] ; _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.921 _exptl_crystal_density_method 'not measured' _exptl_crystal_description prism _exptl_crystal_F_000 1224 _exptl_crystal_size_max 0.19 _exptl_crystal_size_mid 0.08 _exptl_crystal_size_min 0.02 _refine_diff_density_max 0.664 _refine_diff_density_min -0.588 _refine_diff_density_rms 0.085 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.72 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_constraints 0 _refine_ls_number_parameters 273 _refine_ls_number_reflns 5000 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.72 _refine_ls_R_factor_all 0.0183 _refine_ls_R_factor_gt 0.0173 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0302P)^2^+5.4031P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0428 _refine_ls_wR_factor_ref 0.0439 _reflns_Friedel_coverage 0 _reflns_number_gt 4791 _reflns_number_total 5000 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4ce00654b1.cif _cod_data_source_block shelx_CCDC8 _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 7249385 _shelx_res_file ; TITL shelxt_a.res in P2(1)/c shelx.res created by SHELXL-2019/3 at 13:54:12 on 22-Mar-2024 CELL 0.71073 8.4092 16.8459 15.5232 90.000 94.164 90.000 ZERR 4.00 0.0008 0.0018 0.0016 0.000 0.004 0.000 LATT 1 SYMM - X, 1/2 + Y, 1/2 - Z SFAC C H I N O UNIT 80 80 8 16 16 MERG 2 FMAP 2 PLAN 20 BOND $H CONF ACTA LIST 4 L.S. 10 TEMP -123.00 WGHT 0.030200 5.403100 FVAR 0.30997 C1 1 0.614089 0.742297 0.612591 11.00000 0.01414 0.01641 = 0.01628 0.00106 0.00138 -0.00252 C2 1 0.477145 0.860887 0.598220 11.00000 0.01732 0.01923 = 0.02407 -0.00262 0.00118 0.00001 AFIX 43 H2 2 0.415210 0.896734 0.562434 11.00000 -1.20000 AFIX 0 C3 1 0.511804 0.881393 0.684446 11.00000 0.01884 0.02080 = 0.02609 -0.00788 0.00908 -0.00706 C4 1 0.601084 0.827536 0.735281 11.00000 0.02829 0.02782 = 0.01571 -0.00468 0.00358 -0.00837 AFIX 43 H4 2 0.627091 0.838848 0.794589 11.00000 -1.20000 AFIX 0 C5 1 0.652636 0.757220 0.700001 11.00000 0.02544 0.02277 = 0.01623 0.00126 0.00042 -0.00347 AFIX 43 H5 2 0.713024 0.719959 0.734714 11.00000 -1.20000 AFIX 0 C6 1 0.666464 0.667962 0.571748 11.00000 0.01536 0.01687 = 0.01514 0.00034 -0.00147 -0.00043 C7 1 0.798000 0.607774 0.463599 11.00000 0.01837 0.02091 = 0.01716 -0.00021 0.00135 0.00052 AFIX 43 H7 2 0.858740 0.612781 0.414619 11.00000 -1.20000 AFIX 0 C8 1 0.763196 0.532013 0.491787 11.00000 0.01954 0.01722 = 0.01858 -0.00120 -0.00366 0.00137 C9 1 0.677727 0.526471 0.564909 11.00000 0.03001 0.01549 = 0.02338 0.00369 0.00240 -0.00165 AFIX 43 H9 2 0.652250 0.475840 0.587076 11.00000 -1.20000 AFIX 0 C10 1 0.629627 0.594795 0.605520 11.00000 0.02703 0.01990 = 0.01839 0.00259 0.00435 -0.00137 AFIX 43 H10 2 0.572144 0.591402 0.655863 11.00000 -1.20000 AFIX 0 C11 1 0.450726 0.958122 0.719385 11.00000 0.03270 0.02662 = 0.03918 -0.01423 0.01483 -0.00459 AFIX 137 H11A 2 0.368832 0.946675 0.759448 11.00000 -1.50000 H11B 2 0.404610 0.990645 0.671537 11.00000 -1.50000 H11C 2 0.539000 0.986963 0.749900 11.00000 -1.50000 AFIX 0 C12 1 0.817025 0.459576 0.445810 11.00000 0.03016 0.01920 = 0.02775 -0.00577 -0.00099 0.00279 AFIX 137 H12A 2 0.731107 0.441279 0.404530 11.00000 -1.50000 H12B 2 0.843989 0.417523 0.487988 11.00000 -1.50000 H12C 2 0.911146 0.472602 0.414874 11.00000 -1.50000 AFIX 0 C13 1 0.257962 0.800583 0.232070 11.00000 0.01754 0.01756 = 0.01830 0.00147 0.00173 0.00296 C14 1 0.149502 0.684527 0.280714 11.00000 0.01807 0.01656 = 0.01879 -0.00306 0.00195 0.00194 C15 1 0.079164 0.694154 0.188319 11.00000 0.02238 0.02283 = 0.01912 -0.00293 -0.00235 -0.00177 AFIX 23 H15A 2 -0.038645 0.696860 0.186377 11.00000 -1.20000 H15B 2 0.110194 0.649156 0.152101 11.00000 -1.20000 AFIX 0 C16 1 0.148120 0.771812 0.156971 11.00000 0.02560 0.02367 = 0.01546 0.00065 -0.00125 0.00092 AFIX 23 H16A 2 0.208071 0.762819 0.105265 11.00000 -1.20000 H16B 2 0.062381 0.810894 0.142521 11.00000 -1.20000 AFIX 0 C17 1 0.991913 0.917825 0.313887 11.00000 0.02074 0.01876 = 0.02091 0.00158 0.00390 0.00281 C18 1 1.108801 0.941541 0.450455 11.00000 0.01394 0.01552 = 0.02492 -0.00126 0.00379 0.00162 C19 1 1.182043 1.001710 0.392973 11.00000 0.02352 0.01936 = 0.02676 -0.00086 0.00641 -0.00558 AFIX 23 H19A 2 1.297957 0.992293 0.391152 11.00000 -1.20000 H19B 2 1.165281 1.056312 0.414092 11.00000 -1.20000 AFIX 0 C20 1 1.096567 0.989768 0.304023 11.00000 0.02758 0.01754 = 0.02533 0.00424 0.00496 -0.00056 AFIX 23 H20A 2 1.031442 1.036866 0.286736 11.00000 -1.20000 H20B 2 1.174031 0.980131 0.260099 11.00000 -1.20000 AFIX 0 I1 3 0.383658 0.764433 0.418611 11.00000 0.01579 0.01625 = 0.01594 -0.00066 -0.00041 0.00160 I2 3 0.880408 0.797659 0.447015 11.00000 0.01593 0.01561 = 0.01671 -0.00019 0.00203 -0.00105 N1 4 0.526122 0.793614 0.562994 11.00000 0.01626 0.01678 = 0.01742 -0.00184 -0.00099 0.00046 N2 4 0.750753 0.674237 0.501580 11.00000 0.01665 0.01773 = 0.01675 0.00046 0.00080 0.00035 N3 4 0.250488 0.747707 0.300042 11.00000 0.01811 0.01776 = 0.01452 0.00025 -0.00130 -0.00009 N4 4 1.004288 0.894776 0.399814 11.00000 0.01765 0.01551 = 0.01837 0.00156 0.00206 -0.00205 O1 5 0.339350 0.860039 0.234833 11.00000 0.02684 0.02267 = 0.02835 0.00577 -0.00031 -0.00464 O2 5 0.124818 0.630671 0.329779 11.00000 0.03421 0.02048 = 0.02570 0.00286 0.00104 -0.00498 O3 5 0.910766 0.884263 0.257345 11.00000 0.03505 0.03304 = 0.02085 -0.00044 -0.00317 -0.00571 O4 5 1.136721 0.934005 0.527674 11.00000 0.02197 0.02416 = 0.02077 0.00003 -0.00109 0.00012 HKLF 4 REM shelxt_a.res in P2(1)/c REM wR2 = 0.0439, GooF = S = 0.720, Restrained GooF = 0.720 for all data REM R1 = 0.0173 for 4791 Fo > 4sig(Fo) and 0.0183 for all 5000 data REM 273 parameters refined using 0 restraints END WGHT 0.0177 1.6755 REM Highest difference peak 0.664, deepest hole -0.588, 1-sigma level 0.085 Q1 1 0.7802 0.8020 0.4419 11.00000 0.05 0.66 Q2 1 0.2808 0.7643 0.4341 11.00000 0.05 0.64 Q3 1 0.4862 0.7632 0.4029 11.00000 0.05 0.58 Q4 1 0.7665 0.5678 0.4778 11.00000 0.05 0.51 Q5 1 0.9802 0.7964 0.4212 11.00000 0.05 0.50 Q6 1 0.9212 0.7418 0.4147 11.00000 0.05 0.48 Q7 1 0.7239 0.5282 0.5217 11.00000 0.05 0.40 Q8 1 0.8267 0.8551 0.4784 11.00000 0.05 0.38 Q9 1 1.0213 0.9206 0.4263 11.00000 0.05 0.38 Q10 1 0.4205 0.7106 0.3941 11.00000 0.05 0.37 Q11 1 0.3425 0.7070 0.4484 11.00000 0.05 0.37 Q12 1 0.7807 0.5001 0.4672 11.00000 0.05 0.37 Q13 1 0.4804 0.9159 0.7023 11.00000 0.05 0.36 Q14 1 0.7639 0.6388 0.4805 11.00000 0.05 0.36 Q15 1 0.9680 0.8636 0.4171 11.00000 0.05 0.36 Q16 1 0.1135 0.6896 0.2370 11.00000 0.05 0.36 Q17 1 0.3308 0.8197 0.4511 11.00000 0.05 0.35 Q18 1 0.4306 0.8227 0.3911 11.00000 0.05 0.34 Q19 1 0.6109 0.7420 0.6582 11.00000 0.05 0.33 Q20 1 1.0425 0.9558 0.3070 11.00000 0.05 0.33 ; _shelx_res_checksum 31539 _shelx_hkl_file ; -1 0 0 105.089 7.76785 1 -1 0 0 100.621 7.81987 1 2 0 0 7.22343 2.20562 3 2 0 0 8.76356 1.03 4 -2 0 0 8.54932 1.02335 4 2 0 0 8.62419 0.57002 5 3 0 0 283.025 11.9594 4 3 0 0 244.064 15.7789 3 3 0 0 269.258 10.939 5 -3 0 0 272.912 11.8738 4 -4 0 0 9316.93 398.206 1 -4 0 0 9999.99 399.501 1 5 0 0 27.3408 5.79148 3 5 0 0 33.1358 2.97127 4 5 0 0 32.5511 2.05888 5 -5 0 0 30.6599 2.86568 4 6 0 0 112.484 13.5209 3 6 0 0 119.709 7.23069 4 6 0 0 115.739 5.83902 5 -6 0 0 123.204 7.19123 4 -7 0 0 0.73466 1.02705 4 7 0 0 0.92718 0.86157 5 7 0 0 0.83979 0.80372 2 7 0 0 3.60246 1.68659 4 7 0 0 4.79703 4.16542 3 8 0 0 4107.62 159.077 2 8 0 0 3911.12 161.537 4 8 0 0 4092.77 187.387 3 8 0 0 3895.27 159.282 5 9 0 0 11.7139 1.63684 2 9 0 0 9.21175 6.28393 3 9 0 0 8.10219 2.99316 4 9 0 0 10.7136 2.04576 5 10 0 0 257.465 14.8544 4 10 0 0 249.068 27.2905 3 1 -1 0 62.5252 2.60281 2 1 -1 0 60.5729 2.71522 5 -1 1 0 64.5879 2.69183 5 1 1 0 69.0601 2.78427 5 -1 1 0 62.6569 3.04541 4 -1 1 0 59.9363 2.68414 5 -2 -1 0 5085.27 207.63 1 2 -1 0 5349.14 210.113 1 2 1 0 5010.12 208.916 1 -2 1 0 4554.95 206.202 1 -3 -1 0 1.13013 0.65181 4 3 -1 0 0.91996 0.6365 4 3 -1 0 0.30706 0.28193 5 3 1 0 1.20621 0.36942 5 3 1 0 1.06854 0.55187 4 3 1 0 0.47105 1.15132 3 -3 1 0 1.88555 0.75238 4 4 -1 0 242.365 11.4572 4 4 -1 0 237.63 10.2061 5 -4 -1 0 247.19 11.2005 4 4 1 0 250.883 11.2488 4 4 1 0 214.945 16.0335 3 4 1 0 246.654 10.2061 5 -4 1 0 249.255 11.4006 4 5 -1 0 0.4315 1.76637 3 5 -1 0 0.79414 0.87912 4 5 -1 0 0.22853 0.46059 2 5 -1 0 1.62142 0.59375 5 -5 -1 0 1.64597 0.90088 4 -5 1 0 0.98064 0.92243 4 5 1 0 1.50145 0.83921 4 5 1 0 -0.1594 1.44919 3 5 1 0 0.64893 0.4845 5 6 -1 0 2918.24 113.549 5 6 -1 0 2778.35 127.171 3 6 -1 0 3040.25 113.406 2 6 1 0 2644.64 125.599 3 6 1 0 2874.58 113.515 5 7 -1 0 22.8313 3.35847 4 7 -1 0 22.4602 1.86896 2 7 -1 0 20.9715 7.3375 3 7 -1 0 22.1989 2.15682 5 -7 -1 0 21.0809 3.11405 4 7 1 0 21.415 3.25567 4 7 1 0 19.0979 2.08583 5 7 1 0 19.9794 7.04607 3 8 -1 0 520.653 21.9807 2 8 -1 0 510.083 22.6564 5 8 -1 0 549.414 25.0923 4 -8 -1 0 536.805 24.501 4 8 1 0 538.104 22.737 2 8 1 0 522.603 24.5609 4 8 1 0 519.857 22.6916 5 9 -1 0 1.11721 1.76328 4 9 -1 0 -0.2874 3.88515 3 9 -1 0 1.04243 0.84669 2 9 -1 0 1.31846 0.78601 2 9 -1 0 2.55333 1.33048 5 9 1 0 2.6665 4.5593 3 9 1 0 2.58673 1.19504 2 9 1 0 0.34025 1.95323 4 9 1 0 0.13849 1.0826 5 10 -1 0 1112.10 48.9862 4 10 -1 0 1074.73 66.8995 3 10 1 0 1121.85 67.3315 3 10 1 0 1105.18 48.6201 4 1 -2 0 1091.42 53.3838 1 -1 -2 0 1026.27 53.0592 1 1 2 0 1135.25 54.5935 1 2 -2 0 8.18051 0.55376 2 2 -2 0 8.04383 0.79105 5 -2 -2 0 10.4059 1.00554 4 -2 -2 0 5.70603 1.89597 3 -2 2 0 7.04695 1.10881 4 2 2 0 8.67803 0.90979 4 -2 2 0 7.75335 0.57325 2 -2 2 0 9.26718 0.68664 5 2 2 0 9.79194 0.89033 5 2 2 0 7.1465 2.04364 3 -2 2 0 9.27247 0.69489 5 3 -2 0 167.505 6.8637 2 -3 -2 0 156.754 7.60923 4 3 -2 0 161.646 7.14298 5 3 2 0 170.617 7.22096 5 -3 2 0 181.252 8.28268 4 3 2 0 159.888 7.60273 4 4 -2 0 6627.29 266.618 1 -4 -2 0 5765.11 256.60 1 -4 2 0 5711.85 255.533 1 4 2 0 6117.81 262.865 1 5 -2 0 24.6001 1.56138 2 -5 -2 0 26.3747 2.5791 4 5 -2 0 25.9603 2.81951 4 5 -2 0 23.4408 1.8181 5 5 2 0 21.5859 5.05109 3 -5 2 0 26.8713 2.78161 4 5 2 0 25.0944 1.8597 5 5 2 0 23.4724 2.40021 4 -6 -2 0 476.784 20.8072 4 6 -2 0 468.106 21.3955 4 6 -2 0 430.883 30.356 3 6 -2 0 447.835 19.6522 5 6 -2 0 465.884 18.958 2 6 2 0 463.872 29.9648 3 6 2 0 479.615 20.8685 4 7 -2 0 0.64293 1.29235 4 7 -2 0 2.06499 0.60499 2 7 -2 0 2.39237 3.82846 3 -7 -2 0 3.33535 1.57586 4 7 -2 0 2.97507 1.00133 5 7 2 0 -0.1976 2.49932 3 7 2 0 -0.3085 1.10382 4 7 2 0 1.91123 0.94756 5 8 -2 0 2458.87 101.428 2 8 -2 0 2561.53 105.25 4 8 -2 0 2586.69 102.67 5 -8 -2 0 2581.05 104.442 4 8 2 0 2647.55 104.655 4 8 2 0 2525.84 102.671 5 9 -2 0 107.202 6.3684 5 9 -2 0 102.793 16.0884 3 9 -2 0 114.778 8.44552 4 9 2 0 112.439 7.86853 4 9 2 0 111.637 6.4962 2 9 2 0 110.04 6.48962 5 9 2 0 117.103 16.5704 3 10 -2 0 91.1832 16.6992 3 10 -2 0 96.8386 8.29279 4 10 2 0 101.763 7.95996 4 10 2 0 79.4698 15.7631 3 0 -3 0 1.65845 0.46569 5 0 -3 0 2.37556 1.06681 3 0 3 0 1.57482 0.95714 3 0 3 0 1.69307 0.48093 5 1 -3 0 207.09 8.84741 5 -1 -3 0 207.723 11.3656 3 1 3 0 215.537 11.1291 3 -1 3 0 204.081 8.73849 2 -1 3 0 223.77 8.94279 5 1 3 0 212.876 9.12368 5 -2 -3 0 6063.92 251.121 1 2 -3 0 5719.09 250.243 1 2 3 0 6048.42 252.43 1 -2 3 0 5802.46 249.863 1 3 -3 0 23.4574 1.20922 2 3 -3 0 26.9194 2.38287 4 3 -3 0 23.7473 1.62243 5 -3 -3 0 25.5828 1.92852 4 -3 -3 0 20.6451 3.76301 3 3 3 0 19.6663 3.67636 3 -3 3 0 23.7408 1.29516 5 -3 3 0 26.9023 1.30317 5 3 3 0 22.7144 1.70128 5 3 3 0 25.3848 1.84344 4 -4 -3 0 82.6559 8.94621 3 4 -3 0 100.772 4.79541 5 -4 -3 0 101.801 5.45889 4 4 -3 0 99.9702 4.19876 2 4 -3 0 108.468 6.09793 4 4 3 0 102.83 5.30863 4 4 3 0 87.7912 9.19276 3 4 3 0 97.9108 4.8646 5 5 -3 0 39.878 2.02339 2 5 -3 0 39.2831 3.66439 4 5 -3 0 44.0929 2.67013 5 -5 -3 0 42.2474 3.28694 4 5 3 0 45.9566 2.76342 5 5 3 0 42.77 3.17354 4 5 3 0 32.807 6.13534 3 6 -3 0 3432.24 131.415 2 6 -3 0 3359.64 132.359 5 6 3 0 3187.03 144.145 3 7 -3 0 200.131 9.06371 5 7 -3 0 187.383 10.8886 4 7 -3 0 182.047 7.75726 2 7 -3 0 170.503 18.4054 3 -7 -3 0 185.609 10.0671 4 7 3 0 185.778 9.03586 5 7 3 0 197.958 10.234 4 7 3 0 183.454 17.7978 3 -8 -3 0 284.691 14.4094 4 8 -3 0 287.622 13.0737 5 8 -3 0 282.069 30.5086 3 8 -3 0 281.063 15.2843 4 8 3 0 258.257 24.9013 3 8 3 0 275.369 13.062 5 8 3 0 290.083 14.4985 4 9 -3 0 2.13806 1.21521 5 9 -3 0 3.44984 4.45303 3 9 -3 0 2.599 2.17734 4 9 3 0 6.2326 5.51702 3 9 3 0 0.42264 1.83226 4 9 3 0 1.8295 1.29033 5 10 -3 0 788.444 37.793 4 10 -3 0 730.605 53.4255 3 10 3 0 878.974 37.1401 4 10 3 0 862.414 54.9613 3 0 -4 0 5441.47 234.66 1 0 4 0 5309.65 234.863 1 -1 4 0 901.093 36.0873 2 2 -4 0 346.773 14.4631 5 -2 -4 0 307.802 18.0897 3 -2 -4 0 347.889 14.4508 4 2 -4 0 368.277 15.3769 4 2 4 0 353.861 14.8077 5 -2 4 0 350.064 14.4766 5 -2 4 0 349.774 14.1701 2 -2 4 0 355.993 14.6068 5 2 4 0 354.049 18.2441 3 -3 -4 0 98.1598 8.94494 3 3 -4 0 113.447 6.26098 4 3 -4 0 117.143 5.3075 5 -3 -4 0 111.111 5.45677 4 -3 4 0 115.99 5.09699 5 3 4 0 120.275 5.38066 4 -3 4 0 104.261 4.77266 2 3 4 0 108.574 8.98789 3 -3 4 0 112.215 5.06614 5 3 4 0 114.961 5.5319 5 -4 -4 0 3010.57 144.606 1 4 -4 0 3213.17 150.625 1 -4 4 0 3025.39 143.943 1 4 4 0 2911.89 149.031 1 5 -4 0 520.072 24.0945 4 5 -4 0 538.863 21.3461 2 -5 -4 0 538.689 23.0867 4 5 4 0 508.307 30.3394 3 5 4 0 568.574 22.6901 5 5 4 0 542.086 22.9626 4 6 -4 0 377.896 16.6518 5 -6 -4 0 374.461 17.5596 4 6 -4 0 394.493 18.7629 4 6 4 0 381.516 17.4582 4 6 4 0 382.799 26.1335 3 6 4 0 406.69 16.9269 5 7 -4 0 22.7719 2.31979 5 7 -4 0 23.9482 3.8403 4 -7 -4 0 18.3484 2.89229 4 7 4 0 25.8246 7.68024 3 7 4 0 24.911 2.46926 5 7 4 0 20.3088 2.93705 4 8 -4 0 752.246 34.979 4 8 -4 0 699.204 47.4784 3 -8 -4 0 770.75 33.52 4 8 -4 0 785.516 32.1614 5 8 4 0 791.757 33.5264 4 8 4 0 753.315 32.3042 5 8 4 0 791.477 47.0921 3 9 -4 0 260.523 12.3008 5 9 -4 0 246.153 25.3137 3 -9 -4 0 258.391 13.8334 4 9 -4 0 227.196 14.4076 4 9 4 0 265.748 13.7571 4 9 4 0 248.661 12.4626 5 9 4 0 274.835 25.2311 3 10 -4 0 54.8277 6.61797 4 10 -4 0 48.4138 13.894 3 10 4 0 66.8689 6.15803 4 10 4 0 60.6187 13.898 3 0 -5 0 1.70478 1.2717 3 0 5 0 2.27477 1.48213 3 0 5 0 3.12146 0.81115 5 0 5 0 2.78142 0.81548 5 1 -5 0 1599.51 92.2861 1 -1 -5 0 1816.46 95.4485 1 1 5 0 1761.87 95.7452 1 -1 5 0 1823.28 95.6706 1 2 -5 0 804.285 31.9613 5 -2 -5 0 749.389 36.952 3 2 -5 0 783.968 32.881 4 -2 -5 0 785.20 31.8579 4 -2 5 0 796.136 32.2171 5 2 5 0 788.007 32.4109 5 -2 5 0 781.062 31.6939 2 -2 5 0 824.126 32.0888 5 3 -5 0 782.739 31.7006 5 -3 -5 0 692.062 37.2796 3 -3 -5 0 814.323 31.8311 4 3 -5 0 817.639 33.0382 4 -3 5 0 784.207 31.1858 2 3 5 0 779.929 37.2702 3 -3 5 0 795.465 31.6529 5 -3 5 0 774.221 31.5574 5 3 5 0 799.248 31.5415 4 3 5 0 745.308 32.5625 5 4 -5 0 291.175 14.2275 4 -4 -5 0 292.38 13.0262 4 4 -5 0 303.502 12.7588 5 4 5 0 281.709 18.4784 3 -4 5 0 297.978 12.1313 5 -4 5 0 279.004 11.9416 2 4 5 0 300.588 12.8226 4 -4 5 0 294.862 12.149 5 4 5 0 297.558 13.0779 5 -5 -5 0 64.0906 8.75804 3 5 -5 0 59.9277 5.16215 4 -5 -5 0 73.57 4.57599 4 5 -5 0 70.9374 4.08554 5 5 5 0 82.6455 4.4864 5 5 5 0 78.5004 4.44309 4 5 5 0 70.2695 8.831 3 6 -5 0 672.357 27.6664 5 6 -5 0 660.675 29.8421 4 -6 -5 0 641.139 28.3807 4 6 5 0 640.787 37.4378 3 6 5 0 666.058 28.2108 4 6 5 0 688.859 28.0163 5 -7 -5 0 671.65 30.3743 4 7 -5 0 722.869 29.4996 5 7 -5 0 696.946 31.9675 4 7 5 0 724.646 29.8396 5 7 5 0 711.901 30.2667 4 7 5 0 681.01 41.133 3 -8 -5 0 149.747 9.19209 4 8 -5 0 166.731 8.3783 5 8 -5 0 156.114 10.5136 4 8 5 0 172.275 8.73687 5 8 5 0 152.169 9.00287 4 8 5 0 154.698 17.5472 3 9 -5 0 14.9789 2.27332 5 9 -5 0 10.9374 7.0484 3 9 -5 0 15.7433 3.65796 4 -9 -5 0 12.8651 2.9646 4 9 5 0 13.1327 6.9908 3 9 5 0 12.7471 2.44585 5 9 5 0 16.075 3.09905 4 10 -5 0 218.095 25.7228 3 10 -5 0 227.119 14.5652 4 10 5 0 249.468 26.1533 3 0 -6 0 1200.89 76.1826 1 0 6 0 1268.28 78.2996 1 -1 6 0 951.172 39.0189 5 -2 -6 0 175.38 7.59782 4 2 -6 0 156.541 7.61639 5 -2 -6 0 165.673 12.2521 3 2 -6 0 171.938 8.63104 4 -2 6 0 171.899 7.51577 2 2 6 0 175.517 11.441 3 2 6 0 170.437 8.23518 5 -2 6 0 173.232 8.05912 5 -2 6 0 165.924 7.83471 5 3 -6 0 1033.86 41.0754 4 -3 -6 0 882.567 45.9671 3 3 -6 0 964.766 39.503 5 -3 -6 0 1007.77 39.5904 4 -3 6 0 988.83 39.6559 5 3 6 0 951.503 40.0339 5 3 6 0 1004.94 45.5013 3 -3 6 0 976.641 39.0759 2 -3 6 0 966.56 39.51 5 4 -6 0 579.956 25.3815 4 -4 -6 0 574.691 23.8953 4 4 -6 0 571.474 23.6611 5 -4 6 0 538.593 23.2484 5 4 6 0 569.228 30.4383 3 -4 6 0 550.975 22.9061 2 -4 6 0 580.827 23.3226 5 4 6 0 571.893 23.5224 4 4 6 0 579.922 24.1933 5 -5 -6 0 1686.52 68.3033 4 5 -6 0 1732.09 67.8865 5 5 -6 0 1717.32 70.009 4 5 6 0 1688.20 67.9215 4 5 6 0 1645.03 76.9369 3 5 6 0 1650.02 68.2923 5 -6 -6 0 18.0362 5.97256 3 6 -6 0 28.0883 2.47761 5 -6 -6 0 21.1618 2.75857 4 6 -6 0 22.766 3.68682 4 6 6 0 28.234 2.63688 4 6 6 0 28.968 2.7915 5 6 6 0 19.9731 5.86006 3 7 -6 0 111.34 7.96849 4 -7 -6 0 82.9672 11.9707 3 7 -6 0 103.647 5.76966 5 -7 -6 0 104.736 6.49217 4 7 6 0 97.1305 6.03424 5 7 6 0 100.813 6.12596 4 7 6 0 101.881 12.9747 3 8 -6 0 455.416 23.1451 4 8 -6 0 454.039 20.2479 5 -8 -6 0 436.445 21.2284 4 8 6 0 472.504 20.8451 5 8 6 0 472.323 21.0288 4 8 6 0 473.567 33.1485 3 9 -6 0 386.391 33.7396 3 9 -6 0 480.327 20.0234 5 -9 -6 0 434.767 21.0318 4 9 -6 0 414.454 22.7443 4 9 6 0 429.615 20.3514 5 9 6 0 496.384 35.3709 3 9 6 0 462.094 20.9038 4 10 -6 0 82.8152 15.50 3 10 -6 0 79.1946 8.03024 4 10 6 0 86.2056 15.9108 3 0 -7 0 3.19161 1.93323 3 0 7 0 1.21364 0.7678 5 0 7 0 2.28785 0.98509 5 1 -7 0 1676.96 71.6479 3 2 -7 0 599.663 26.6501 5 -2 -7 0 648.699 26.5955 4 -2 -7 0 675.225 33.902 3 -2 7 0 628.304 26.57 2 -2 7 0 677.299 27.078 5 2 7 0 674.93 27.4917 5 -2 7 0 643.991 27.1925 5 -3 -7 0 528.31 22.1134 4 -3 -7 0 493.145 29.0139 3 3 -7 0 528.182 23.5311 4 3 -7 0 540.636 22.1515 5 3 7 0 551.079 22.8892 5 -3 7 0 529.836 22.3947 5 -3 7 0 499.418 22.6921 5 3 7 0 578.457 28.446 3 -3 7 0 523.024 21.7443 2 -4 -7 0 3.9643 1.05318 4 4 -7 0 5.8101 1.9179 4 -4 -7 0 5.4752 3.15659 3 4 -7 0 8.49464 1.40703 5 4 7 0 3.16838 2.55436 3 -4 7 0 4.07614 0.7735 2 -4 7 0 3.55957 0.96741 5 -4 7 0 4.73855 1.04988 5 4 7 0 1.99706 1.13247 5 5 -7 0 339.402 15.1234 5 5 -7 0 365.596 17.335 4 -5 -7 0 349.321 15.4926 4 -5 7 0 342.355 14.212 5 5 7 0 340.10 15.7347 5 5 7 0 331.735 22.4085 3 -5 7 0 337.372 14.2219 5 5 7 0 359.87 15.0363 4 -6 -7 0 40.3307 3.52051 4 6 -7 0 44.8981 4.84774 4 6 -7 0 37.2556 3.09793 5 6 7 0 46.164 8.15215 3 6 7 0 42.6637 3.21839 4 6 7 0 40.2618 3.57066 5 7 -7 0 1043.56 47.4348 4 7 -7 0 1112.39 44.3959 5 -7 -7 0 1053.96 45.0474 4 7 7 0 1076.64 57.0253 3 7 7 0 1080.76 45.0294 5 7 7 0 1082.45 44.5675 4 -8 -7 0 45.7331 4.54557 4 8 -7 0 50.6838 4.0418 5 8 -7 0 57.9498 6.51436 4 8 7 0 63.3731 4.74152 5 8 7 0 57.9962 10.8541 3 8 7 0 49.5433 4.28753 4 9 -7 0 206.947 10.5163 5 9 -7 0 202.681 13.3922 4 -9 -7 0 206.488 11.4972 4 9 7 0 213.305 11.1044 4 9 7 0 206.999 11.2244 5 9 7 0 205.167 21.9446 3 10 -7 0 3.84133 4.90604 3 10 -7 0 0.83853 2.61898 4 10 7 0 3.53088 5.62193 3 0 -8 0 164.832 11.8495 3 0 8 0 141.847 7.7359 5 0 8 0 146.001 7.43559 5 -1 -8 0 2705.93 152.901 1 1 -8 0 2830.17 154.565 1 1 8 0 3124.29 160.834 1 -1 8 0 2985.21 157.85 1 -2 -8 0 6.4647 3.20474 3 2 -8 0 4.75968 1.18699 5 2 8 0 6.24709 1.56938 5 -2 8 0 5.12837 1.36952 5 -2 8 0 2.90179 1.08157 5 2 8 0 8.78296 3.14883 3 -3 -8 0 1551.34 61.885 4 3 -8 0 1548.59 63.6421 4 -3 -8 0 1427.02 70.4274 3 3 -8 0 1582.51 61.9706 5 -3 8 0 1534.73 61.6159 2 -3 8 0 1557.71 62.2138 5 -3 8 0 1561.43 62.3508 5 -4 -8 0 3.98119 1.16503 4 -4 -8 0 2.57665 2.64502 3 4 -8 0 7.15541 1.34941 5 4 -8 0 1.78939 1.44798 4 -4 8 0 3.89836 1.13773 5 -4 8 0 5.26468 1.19676 5 4 8 0 0.73324 1.00332 5 -4 8 0 3.94942 0.84569 2 4 8 0 5.02413 3.03385 3 5 -8 0 1649.35 66.2692 5 -5 -8 0 1670.94 66.5613 4 5 -8 0 1627.30 68.6165 4 -5 8 0 1611.27 65.1908 2 5 8 0 1596.20 67.0369 5 5 8 0 1721.13 76.2399 3 -5 8 0 1619.53 65.6079 5 -5 8 0 1632.50 65.6085 5 6 -8 0 3.46947 1.37029 5 -6 -8 0 4.55687 3.83441 3 6 -8 0 2.88444 1.96664 4 -6 -8 0 2.63801 1.33417 4 6 8 0 4.97553 3.76457 3 6 8 0 2.87374 1.5072 5 -7 -8 0 629.435 28.2567 4 7 -8 0 646.144 30.7102 4 7 -8 0 665.491 27.7723 5 7 8 0 654.833 39.4774 3 7 8 0 645.523 28.5628 5 7 8 0 667.715 27.7172 4 -8 -8 0 0.35936 1.49114 4 8 -8 0 0.90276 1.2047 5 8 -8 0 2.48299 2.15532 4 -8 -8 0 1.44211 3.45774 3 8 8 0 1.52441 3.54243 3 8 8 0 0.56694 1.26787 4 8 8 0 2.63405 1.62704 5 9 -8 0 689.955 35.7441 4 9 -8 0 752.901 32.3976 5 9 8 0 774.476 33.538 5 9 8 0 818.618 49.336 3 10 -8 0 30.645 5.65721 4 0 -9 0 0.84909 1.89006 3 0 9 0 0.88768 1.10901 5 0 9 0 0.16043 0.82189 5 -1 -9 0 2329.38 138.732 1 1 -9 0 2435.70 140.784 1 -1 9 0 2644.65 145.228 1 1 9 0 2411.26 143.243 1 -2 -9 0 41.2829 6.92913 3 2 -9 0 35.8994 2.78124 5 -2 9 0 35.5043 3.1485 5 2 9 0 35.9729 3.23683 5 -2 9 0 32.0657 2.62098 2 -2 9 0 41.7927 3.20177 5 3 -9 0 2306.66 98.1175 4 -3 -9 0 2381.80 107.06 3 -3 -9 0 2470.57 96.5318 4 -3 9 0 2384.91 96.4066 2 -3 9 0 2504.57 97.0514 5 -3 9 0 2434.33 97.0975 5 4 -9 0 34.1811 2.73967 5 4 -9 0 30.1761 4.07194 4 -4 -9 0 28.6589 6.60802 3 -4 9 0 37.1811 2.37558 2 -4 9 0 33.1567 2.76869 5 4 9 0 38.2176 6.48515 3 4 9 0 30.6006 3.23244 5 -4 9 0 29.7377 2.81489 5 5 -9 0 699.558 28.9632 5 5 -9 0 692.763 31.4581 4 -5 -9 0 673.835 29.0888 4 -5 9 0 667.595 27.9688 2 5 9 0 727.705 38.2048 3 5 9 0 680.956 29.9024 5 -6 -9 0 75.7775 5.08977 4 6 -9 0 71.8123 6.62106 4 -6 -9 0 64.8866 10.5491 3 6 -9 0 83.9721 4.91426 5 6 9 0 79.0627 5.62211 5 6 9 0 78.3759 10.6256 3 7 -9 0 1004.01 46.1566 4 7 -9 0 1018.67 42.8885 5 -7 -9 0 990.499 43.2889 4 7 9 0 1048.10 44.0516 5 7 9 0 1117.48 56.4359 3 8 -9 0 5.51671 1.69039 5 8 -9 0 4.13764 2.70887 4 -8 -9 0 4.91966 4.7535 3 -8 -9 0 4.6918 1.8409 4 8 9 0 4.00719 4.37411 3 8 9 0 4.95343 2.05141 5 9 -9 0 242.128 12.6484 5 9 -9 0 226.418 15.2014 4 9 9 0 261.279 24.9399 3 0 -10 0 272.872 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530.771 25.6747 5 2 11 0 598.474 25.5604 5 2 11 0 612.68 26.375 5 -2 11 0 592.208 25.313 2 -3 -11 0 1613.17 77.0878 3 3 -11 0 1471.43 65.4915 4 -3 -11 0 1496.37 63.7288 4 3 -11 0 1453.45 63.845 5 3 11 0 1611.12 65.1797 5 -3 11 0 1648.14 64.7178 5 3 11 0 1767.29 72.8934 3 -3 11 0 1609.94 64.6648 5 -3 11 0 1515.92 63.7356 2 -4 -11 0 3.07978 3.71625 3 -4 -11 0 4.53928 1.38591 4 4 -11 0 6.3178 2.23418 4 4 -11 0 2.49344 1.22455 5 -4 11 0 4.48365 1.62779 5 -4 11 0 1.88952 1.20973 5 4 11 0 2.13277 1.52879 5 -4 11 0 3.7442 1.15794 2 4 11 0 3.03782 3.16423 3 -5 -11 0 487.485 34.1677 3 5 -11 0 508.926 22.2673 5 -5 -11 0 502.058 22.2763 4 5 -11 0 486.464 24.7091 4 -5 11 0 519.241 22.2537 5 5 11 0 579.789 32.0432 3 -5 11 0 503.806 22.2049 5 5 11 0 516.527 23.5378 5 6 -11 0 247.955 15.3039 4 -6 -11 0 258.859 12.8902 4 6 -11 0 296.483 13.0723 5 -6 11 0 273.628 11.4881 2 -6 11 0 251.241 12.492 5 -6 11 0 266.375 12.4931 5 6 11 0 306.771 22.4452 3 6 11 0 280.845 14.2002 5 -7 -11 0 710.699 47.7603 3 7 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2 -6 314.448 15.5961 4 7 2 -6 306.345 13.5546 2 6 -2 -6 125.581 15.3221 3 -6 -2 6 131.357 6.85645 5 6 -2 -6 119.137 7.45957 5 6 -2 -6 135.922 5.79848 2 6 -2 -6 128.133 8.30309 4 -6 -2 6 120.574 8.14886 4 6 2 -6 129.691 6.60162 2 -6 2 6 119.69 8.20376 4 6 2 -6 132.199 7.76531 5 -6 2 6 129.268 6.91531 5 6 2 -6 126.691 7.91825 4 6 2 -6 124.344 14.7055 3 5 -2 -6 1127.18 45.0572 2 -5 -2 6 1066.01 47.2984 4 -5 -2 6 1178.40 46.2125 5 5 -2 -6 1074.68 46.5715 5 5 -2 -6 1122.44 47.4367 4 5 2 -6 1053.07 56.0346 3 5 2 -6 1163.64 47.2221 4 -5 2 6 1133.61 47.5945 4 5 2 -6 1177.46 46.9613 5 -5 2 6 1090.69 46.1726 5 5 2 -6 1159.29 45.7769 2 -4 -2 6 4401.24 226.001 1 -4 -2 6 4154.22 219.781 1 -4 2 6 4325.33 222.855 1 3 -2 -6 169.184 8.22691 5 3 -2 -6 163.842 7.34426 2 -3 -2 6 165.787 8.11311 5 -3 -2 6 169.163 7.58093 2 3 -2 -6 163.363 8.45153 4 -3 -2 6 151.731 8.33196 4 3 2 -6 153.512 7.60145 2 -3 2 6 160.52 8.122 5 -3 2 6 156.807 7.23816 2 3 2 -6 140.343 11.8316 3 -3 2 6 151.272 8.39157 4 3 2 -6 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25.7227 3 -2 8 -6 455.11 19.2579 5 -2 8 -6 443.102 19.4033 5 -2 8 -6 448.308 19.9155 2 2 8 6 449.895 19.5974 5 3 -8 6 125.739 6.83984 2 -3 -8 -6 114.366 11.2773 3 3 -8 6 135.205 10.1667 3 3 -8 6 133.44 6.99158 5 -3 8 -6 126.567 7.15574 2 3 8 6 145.346 11.0562 3 3 8 6 123.747 6.71444 5 -3 8 -6 129.659 6.22507 5 -3 8 -6 127.354 6.28461 5 4 -8 6 287.924 13.0977 2 4 -8 6 292.567 13.2039 5 -4 8 -6 261.295 13.2779 2 4 8 6 294.542 12.9536 5 5 -8 6 1310.81 53.3294 5 5 -8 6 1283.41 53.1605 2 5 8 6 1355.49 53.0647 5 -5 8 -6 1258.30 53.5116 2 6 -8 6 184.317 12.1603 4 6 -8 6 214.181 10.1376 5 6 -8 6 204.481 9.82287 2 -6 -8 -6 171.851 16.4348 3 -6 8 -6 198.814 10.184 2 6 8 6 233.038 16.7813 3 6 8 6 203.317 9.69776 5 7 -8 6 8.62825 1.65584 2 -7 -8 -6 8.49933 4.60547 3 7 -8 6 7.04841 2.58382 4 7 8 6 8.46588 1.683 5 7 8 6 9.08179 4.5226 3 8 -8 6 117.231 9.79668 4 8 8 6 140.447 14.8091 3 9 -8 6 582.048 41.3564 3 9 -8 6 619.364 30.6677 4 9 8 6 638.977 29.1496 2 9 -9 -6 612.155 29.0327 5 -9 -9 6 624.522 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318.832 15.2383 2 7 -5 7 325.076 24.7771 3 7 5 7 308.692 14.0917 5 7 5 7 351.315 22.5153 3 8 -5 7 300.155 25.0961 3 8 -5 7 296.191 14.2702 2 8 -5 7 298.904 16.677 4 8 5 7 334.551 23.2215 3 8 5 7 286.279 15.678 2 9 -5 7 38.4713 5.77711 4 9 -5 7 32.3857 9.45367 3 9 5 7 39.321 4.91015 2 9 5 7 46.2034 9.31226 3 10 -6 -7 469.74 22.1643 5 10 -6 -7 392.925 37.3865 3 10 -6 -7 415.066 23.9313 4 -10 -6 7 430.342 23.56 4 -10 6 7 476.821 24.3246 4 10 6 -7 461.492 22.8445 5 10 6 -7 476.319 39.1037 3 10 6 -7 481.357 22.8939 4 9 -6 -7 650.728 49.353 3 -9 -6 7 791.136 35.4945 4 9 -6 -7 780.763 33.6222 5 9 -6 -7 756.005 35.7994 4 -9 6 7 757.087 35.4802 4 9 6 -7 715.659 34.0883 5 9 6 -7 724.557 32.7346 2 9 6 -7 785.558 50.3915 3 9 6 -7 779.487 34.1734 4 8 -6 -7 24.8774 3.71316 5 8 -6 -7 14.2014 3.86366 4 -8 -6 7 17.1533 3.93082 4 8 6 -7 19.9601 3.07091 2 -8 6 7 13.8139 3.48038 4 8 6 -7 23.9069 3.85192 4 8 6 -7 21.5119 3.74235 5 -8 6 7 18.2462 2.48842 5 8 6 -7 22.7892 8.10601 3 -7 -6 7 30.1609 6.92055 4 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9 2000.00 79.3153 2 0 5 9 1900.24 78.5961 4 0 5 -9 1960.90 79.0424 5 -1 -5 -9 1756.41 70.0798 5 -1 -5 -9 1864.00 74.0403 3 1 -5 9 1741.58 71.1198 2 1 -5 9 1567.19 72.7588 3 1 -5 9 1734.30 71.0171 5 1 5 9 1764.42 71.5646 2 1 5 9 1783.05 70.4139 4 -1 5 -9 1707.09 70.6138 5 -1 5 -9 1814.30 71.5413 2 2 -5 9 109.331 7.22805 3 -2 -5 -9 94.5228 7.3861 3 2 -5 9 96.0928 5.72902 5 2 -5 9 93.5191 5.89402 2 -2 5 -9 101.317 5.66203 5 2 5 9 93.1552 6.27755 2 -2 5 -9 94.0319 6.17057 2 2 5 9 96.2486 4.96269 4 2 5 9 93.7109 5.62626 5 -2 5 -9 95.8547 5.01159 5 3 -5 9 125.208 6.53747 5 -3 -5 -9 102.573 8.32373 3 3 -5 9 115.10 6.85666 2 3 5 9 118.889 5.46764 4 3 5 9 120.224 7.40884 2 3 5 9 113.853 6.27399 5 -3 5 -9 121.008 7.19672 2 4 -5 9 858.80 36.2348 5 4 -5 9 833.059 36.8674 2 4 5 9 863.658 35.1006 4 4 5 9 874.204 36.1024 5 4 5 9 923.535 39.7381 3 4 5 9 846.822 37.7491 2 4 5 9 960.143 35.3151 4 -4 5 -9 806.949 37.0626 2 5 -5 9 1005.94 42.9835 2 5 -5 9 1023.97 42.06 5 5 5 9 1140.71 41.355 4 -5 5 -9 988.148 43.1869 2 5 5 9 1014.55 41.8737 5 5 5 9 973.44 43.8773 2 5 5 9 1000.49 40.9676 4 6 -5 9 0.10129 2.21231 3 6 -5 9 3.25535 1.65939 2 6 -5 9 3.61946 1.27616 5 6 5 9 1.89818 1.01598 5 6 5 9 0.58188 1.59898 2 6 5 9 1.32337 0.8584 4 6 5 9 1.09594 2.34995 3 7 -5 9 6.10669 2.01953 2 7 -5 9 8.41608 1.5648 5 7 -5 9 5.77891 3.98577 3 7 -5 9 9.12329 2.76996 4 7 5 9 9.18303 1.54106 5 7 5 9 11.8753 2.71019 2 7 5 9 11.3946 4.26215 3 8 -5 9 610.373 27.1823 2 8 -5 9 616.05 29.3838 4 8 5 9 613.964 28.6853 2 9 -5 9 275.781 16.5233 4 9 5 9 303.612 16.1294 2 -9 -6 9 322.374 18.6024 4 9 -6 -9 323.729 16.941 5 9 6 -9 319.959 34.9965 3 9 6 -9 331.147 17.5314 4 9 6 -9 325.006 17.7412 5 -8 -6 9 226.44 14.2807 4 8 -6 -9 241.022 13.1459 5 8 -6 -9 242.723 14.7163 4 8 -6 -9 207.284 23.7768 3 8 6 -9 237.362 23.6394 3 8 6 -9 250.933 13.5821 4 -8 6 9 236.776 12.0979 5 8 6 -9 238.978 13.9017 5 -8 6 9 236.069 14.4164 4 8 6 -9 253.787 12.4925 2 -7 -6 9 52.5011 4.67193 5 7 -6 -9 49.4125 5.77577 4 7 -6 -9 56.0593 5.19146 5 -7 -6 9 58.2134 6.07337 4 7 6 -9 52.7629 5.65991 5 7 6 -9 59.62 4.7769 2 7 6 -9 68.5106 5.65333 4 -7 6 9 60.9879 6.23013 4 7 6 -9 50.0811 10.5714 3 -7 6 9 58.6875 4.93035 5 -6 -6 9 428.245 20.4818 5 -6 -6 9 447.611 22.4837 4 6 -6 -9 469.109 21.1659 5 6 -6 -9 426.283 22.016 4 -6 6 9 444.809 22.1486 4 -6 6 9 447.687 20.909 5 6 6 -9 457.393 20.6028 2 6 6 -9 482.811 21.9628 5 -6 6 9 435.096 18.5128 2 6 6 -9 422.258 30.8736 3 6 6 -9 490.176 23.1697 4 -5 -6 9 507.873 24.0008 4 5 -6 -9 510.55 22.9711 5 -5 -6 9 513.754 22.8454 5 5 -6 -9 488.723 23.8083 4 5 6 -9 503.452 23.5799 5 -5 6 9 518.62 23.1908 5 5 6 -9 484.737 31.122 3 -5 6 9 510.542 23.9818 4 5 6 -9 493.115 22.584 2 -5 6 9 512.03 21.2349 2 -4 -6 9 195.603 10.8999 4 -4 -6 9 189.496 10.1501 5 4 -6 -9 187.118 10.6364 4 -4 -6 9 190.957 9.64903 2 4 -6 -9 176.556 9.91424 5 -4 6 9 182.178 8.89311 2 4 6 -9 180.539 10.5128 5 -4 6 9 195.173 10.7846 4 -4 6 9 176.666 10.1991 5 4 6 -9 192.652 15.819 3 4 6 -9 187.656 9.90228 2 -3 -6 9 113.179 7.17146 4 -3 -6 9 97.4325 6.46402 5 -3 -6 9 84.5482 10.2682 3 3 -6 -9 106.67 6.81924 4 -3 -6 9 97.9362 6.08123 2 3 -6 -9 107.898 6.4597 5 -3 6 9 103.362 5.84578 2 3 6 -9 102.874 10.3799 3 -3 6 9 112.902 7.01111 4 3 6 -9 109.316 6.9857 5 3 6 -9 99.5568 6.36941 2 -3 6 9 109.149 6.9462 5 2 -6 -9 926.038 37.0278 5 -2 -6 9 863.431 37.7092 4 -2 -6 9 872.815 36.8947 2 -2 -6 9 866.189 37.2915 5 2 -6 -9 850.01 37.1398 4 2 6 -9 884.519 41.9241 3 -2 6 9 873.781 36.7566 2 2 6 -9 873.142 37.2503 2 -2 6 9 857.544 37.4782 5 2 6 -9 910.252 37.6866 5 -2 6 9 889.74 37.4133 4 -1 -6 9 1851.63 77.1685 5 -1 -6 9 1998.45 77.7401 4 1 -6 -9 1844.06 76.6881 4 1 -6 -9 1850.62 76.5512 5 -1 -6 9 1911.83 76.9366 2 1 6 -9 1947.66 77.4239 5 -1 6 9 1838.53 77.2911 5 1 6 -9 1919.54 77.3781 2 -1 6 9 1938.17 76.9999 4 -1 6 9 1855.77 76.9507 2 0 -6 -9 317.962 17.1264 3 0 -6 9 277.139 17.2844 3 0 -6 9 304.278 14.4583 5 0 -6 -9 317.617 13.8009 5 0 -6 -9 308.468 13.7175 4 0 -6 9 312.916 14.3771 2 0 6 9 289.107 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1016.37 43.7299 4 -7 0 10 982.618 41.2982 5 -6 0 10 484.221 22.0782 5 -6 0 10 491.344 23.5519 4 -6 0 10 518.946 21.0236 2 6 0 -10 427.473 31.8267 3 6 0 -10 475.942 22.9143 4 6 0 -10 493.406 21.1244 2 5 0 -10 957.02 41.2253 4 -5 0 10 955.245 40.7237 5 -5 0 10 961.714 41.7803 4 5 0 -10 898.943 50.5893 3 5 0 -10 984.728 41.2153 5 -5 0 10 948.144 39.402 2 5 0 -10 979.11 39.7992 2 4 0 -10 752.393 32.3653 5 -4 0 10 744.705 32.8103 4 4 0 -10 665.102 39.2272 3 4 0 -10 767.768 32.4501 4 -4 0 10 753.561 32.2206 5 4 0 -10 747.935 31.3536 2 -4 0 10 750.163 31.0352 2 3 0 -10 3297.01 125.26 5 3 0 -10 3251.94 125.143 4 3 0 -10 2766.36 130.996 3 2 0 -10 1525.45 62.3634 2 -2 0 10 1603.66 63.0023 5 2 0 -10 1505.67 62.6305 5 2 0 -10 1507.07 62.4351 4 -2 0 10 1538.13 62.205 2 -2 0 10 1470.44 62.8015 4 -1 0 10 121.285 6.71333 2 -1 0 10 114.507 6.93087 5 1 0 -10 119.699 6.79803 2 1 0 -10 113.825 6.65224 5 -1 0 10 103.529 6.55036 4 0 0 -10 146.718 7.91433 2 0 0 -10 133.514 7.21796 5 0 0 10 148.675 7.85651 2 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3081.76 126.537 2 3 1 10 3160.35 126.704 2 4 -1 10 1352.66 55.414 2 4 -1 10 1299.14 53.9423 5 4 1 10 1343.82 55.5656 2 4 1 10 1312.07 53.8898 5 5 -1 10 94.1012 6.56957 2 5 -1 10 87.9306 5.20647 5 5 -1 10 88.664 6.67637 3 5 1 10 95.4293 5.23473 5 5 1 10 100.687 6.87859 3 5 1 10 95.4222 6.70809 2 6 -1 10 784.918 32.7278 2 6 -1 10 758.505 30.5377 5 6 -1 10 754.556 32.3921 4 6 -1 10 685.90 34.5435 3 6 1 10 672.665 33.835 2 6 1 10 734.516 34.3993 3 6 1 10 747.985 30.3732 5 6 1 10 738.474 31.7222 4 7 -1 10 774.176 33.9325 2 7 -1 10 776.175 33.8606 4 7 -1 10 722.507 37.7208 3 7 1 10 778.317 34.207 2 7 1 10 747.40 37.3398 3 7 1 10 795.997 33.3857 4 8 -1 10 392.495 20.3747 4 8 -1 10 440.296 20.6426 2 8 1 10 436.879 20.9222 2 -9 -2 10 306.291 17.1293 4 9 -2 -10 254.49 28.3438 3 9 -2 -10 278.914 15.427 5 9 -2 -10 264.24 16.1091 4 9 2 -10 266.079 27.7185 3 9 2 -10 282.865 16.0153 4 -9 2 10 292.098 16.8364 4 9 2 -10 288.653 15.8796 5 8 -2 -10 3.82151 5.92389 3 -8 -2 10 2.39181 2.32905 4 8 -2 -10 3.35689 2.38074 4 8 -2 -10 4.70764 2.2671 5 -8 -2 10 3.973 1.94361 5 -8 2 10 3.91198 1.90528 5 8 2 -10 4.38761 5.92913 3 8 2 -10 1.36998 1.22128 2 8 2 -10 3.11559 2.24617 5 8 2 -10 0.16754 2.03158 4 7 -2 -10 862.668 39.5511 5 -7 -2 10 912.433 38.694 5 7 -2 -10 930.357 37.2957 2 -7 -2 10 920.555 40.956 4 7 -2 -10 932.098 40.5706 4 7 -2 -10 851.595 53.3877 3 -7 2 10 942.338 41.0885 4 -7 2 10 905.815 38.8099 5 7 2 -10 918.298 38.1372 2 7 2 -10 855.621 52.4402 3 7 2 -10 926.428 40.1349 4 7 2 -10 914.187 40.0576 5 6 -2 -10 755.848 30.5063 2 -6 -2 10 757.08 31.8256 5 6 -2 -10 703.164 32.7137 4 6 -2 -10 662.452 43.2248 3 6 -2 -10 727.041 33.7606 5 -6 -2 10 740.427 33.3429 4 6 2 -10 667.025 42.2852 3 -6 2 10 733.03 30.2477 2 -6 2 10 724.612 31.8161 5 6 2 -10 737.266 31.0953 2 6 2 -10 772.197 32.7818 4 6 2 -10 730.24 33.2639 5 -6 2 10 743.551 33.3767 4 -5 -2 10 433.006 20.3852 5 5 -2 -10 397.991 29.299 3 5 -2 -10 451.966 21.164 4 5 -2 -10 472.131 20.9576 5 -5 -2 10 442.291 21.4427 4 5 -2 -10 453.39 19.3725 2 -5 -2 10 448.795 19.487 2 5 2 -10 454.289 20.952 4 5 2 -10 465.075 19.9191 2 -5 2 10 434.65 19.0578 2 5 2 -10 451.128 21.0435 5 -5 2 10 448.318 21.5163 4 -5 2 10 463.048 20.7074 5 5 2 -10 381.283 27.9159 3 4 -2 -10 54.57 4.65056 4 -4 -2 10 46.0824 4.25071 5 4 -2 -10 51.0112 4.3822 5 -4 -2 10 53.8321 4.83983 4 4 -2 -10 50.8122 3.702 2 -4 -2 10 50.5903 3.72552 2 4 -2 -10 41.9046 8.10275 3 -4 2 10 47.3025 3.47125 2 -4 2 10 44.3456 4.29829 5 4 2 -10 51.3323 4.52152 5 4 2 -10 38.8136 7.24475 3 4 2 -10 52.6804 4.08666 2 -4 2 10 47.7153 4.64646 4 4 2 -10 53.8674 4.50466 4 -3 -2 10 2000.56 79.4234 4 3 -2 -10 1920.52 78.6602 5 -3 -2 10 1916.92 77.9091 2 -3 -2 10 1976.65 78.852 5 3 -2 -10 1899.29 78.6967 4 3 -2 -10 1905.74 77.9443 2 3 2 -10 1743.65 84.3907 3 -3 2 10 1907.52 78.8486 5 3 2 -10 2004.48 78.375 2 -3 2 10 1907.03 77.7856 2 3 2 -10 2018.15 79.0623 5 3 2 -10 1966.59 78.6339 4 -3 2 10 1881.81 79.0662 4 -2 -2 10 2188.28 90.3434 4 2 -2 -10 2183.57 89.911 5 2 -2 -10 2255.48 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52.2193 4 -3 7 10 1236.64 51.0625 2 3 7 -10 1250.30 52.4678 5 -2 -7 10 250.461 12.6207 5 -2 -7 10 276.053 13.3942 4 2 -7 -10 234.709 12.2365 4 2 -7 -10 228.174 11.8986 5 -2 -7 10 235.123 12.0366 2 2 7 -10 264.537 16.6528 3 -2 7 10 257.38 12.6081 4 2 7 -10 235.728 12.4454 2 -2 7 10 225.604 12.5846 5 2 7 -10 231.277 12.6326 5 -2 7 10 256.872 12.1348 2 -1 -7 10 320.529 14.9083 5 -1 -7 10 311.00 15.2689 4 1 -7 -10 287.255 13.9939 5 -1 -7 10 299.71 14.4701 2 1 -7 -10 287.476 14.1416 4 -1 7 10 314.072 14.4936 4 1 7 -10 305.446 14.9497 5 1 7 -10 315.636 15.0458 2 -1 7 10 313.416 14.6546 2 -1 7 10 288.774 14.8575 5 0 -7 10 545.553 25.5317 5 0 -7 -10 582.163 24.7451 4 0 -7 10 513.081 29.1765 3 0 -7 -10 579.913 24.7311 5 0 -7 -10 589.727 28.9727 3 0 -7 10 591.229 25.5829 2 0 7 10 568.834 25.7878 5 0 7 -10 550.58 25.508 5 0 7 -10 613.319 26.1027 2 0 7 10 615.441 26.0412 2 0 7 10 599.744 25.0593 4 0 7 -10 636.293 29.4823 3 -1 -7 -10 356.334 19.9848 3 1 -7 10 337.90 19.4155 3 1 -7 10 355.457 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28.6005 5 -4 13 -11 652.612 29.2218 2 4 13 11 615.882 30.0614 2 5 -13 11 157.831 9.32496 2 5 -13 11 162.141 9.8385 5 5 13 11 161.437 16.6683 2 5 13 11 146.576 9.59701 5 -5 13 -11 152.801 10.2092 2 -6 -14 11 467.467 25.8549 4 6 -14 -11 479.883 23.2185 5 -6 -14 11 499.324 23.8686 5 6 -14 -11 447.539 25.2368 4 6 14 -11 493.548 25.6518 5 6 14 -11 531.296 27.2726 2 -6 14 11 512.713 25.2611 5 5 -14 -11 211.186 12.696 5 5 -14 -11 188.617 12.9295 4 -5 -14 11 186.651 13.3718 4 -5 -14 11 203.909 12.2205 5 -5 14 11 209.525 13.4045 5 5 14 -11 201.264 12.7199 2 5 14 -11 182.05 14.2415 5 5 14 -11 222.233 20.1915 3 -4 -14 11 25.3402 9.29116 3 4 -14 -11 29.8968 4.83359 4 -4 -14 11 28.8135 4.39926 5 4 -14 -11 27.0776 3.94411 5 4 14 -11 37.8694 5.33459 2 -4 14 11 30.8213 5.28513 5 4 14 -11 26.7193 7.66991 3 -4 14 11 27.9808 3.71426 2 4 14 -11 26.9613 4.91408 5 3 -14 -11 96.1923 11.8371 3 -3 -14 11 95.4168 7.50368 5 -3 -14 11 85.7931 13.7369 3 -3 -14 11 89.6742 8.20383 4 3 -14 -11 98.1837 8.69788 4 3 14 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1 -14 11 301.889 23.6498 3 1 -14 11 308.743 16.4801 5 -1 14 -11 290.00 20.0163 5 1 14 11 320.181 17.4197 2 1 14 11 335.083 17.3547 5 -1 14 -11 331.176 17.3392 2 2 -14 11 1054.78 54.8906 3 2 -14 11 1066.33 45.7075 2 -2 -14 -11 1018.07 56.5435 3 2 -14 11 1113.89 46.4066 5 -2 14 -11 1096.59 47.0613 2 2 14 11 1050.37 46.6486 5 -2 14 -11 1073.65 45.654 5 3 -14 11 200.789 17.5305 3 3 -14 11 222.783 11.7981 2 3 -14 11 202.293 12.1181 5 -3 14 -11 223.785 13.0195 2 3 14 11 218.754 12.555 5 4 -14 11 74.1072 6.14142 5 4 -14 11 73.8036 5.78665 2 -4 -14 -11 67.9569 11.9176 3 -4 14 -11 56.2101 6.8815 2 4 14 11 70.7456 6.37619 5 5 -14 11 177.25 10.4601 2 5 -14 11 185.758 11.1973 5 5 14 11 201.225 13.0658 2 -5 14 -11 177.041 11.6428 2 5 14 11 179.087 11.0928 5 5 -15 -11 114.356 9.58485 4 5 -15 -11 110.776 7.79082 5 -5 -15 11 84.9693 15.4761 3 -5 -15 11 106.15 8.37253 5 -5 -15 11 87.6811 9.22559 4 5 15 -11 116.299 9.27677 2 5 15 -11 124.356 15.1408 3 5 15 -11 127.184 9.76729 5 -5 15 11 102.661 9.25774 5 -4 -15 11 1325.27 61.261 4 4 -15 -11 1346.10 58.4564 5 -4 -15 11 1380.38 59.5222 5 4 -15 -11 1288.15 59.9046 4 -4 15 11 1349.39 60.9231 5 4 15 -11 1452.08 60.8231 2 4 15 -11 1431.51 61.3707 5 4 15 -11 1542.18 71.2112 3 3 -15 -11 236.117 12.3889 5 -3 -15 11 217.356 15.8358 4 -3 -15 11 235.562 13.4388 5 3 -15 -11 231.46 13.4415 4 -3 -15 11 197.235 22.0908 3 3 -15 -11 227.13 19.099 3 3 15 -11 256.62 14.8094 5 -3 15 11 241.924 14.7404 5 3 15 -11 228.903 13.9011 2 3 15 -11 238.436 19.8403 3 2 -15 -11 23.0156 6.23583 3 -2 -15 11 26.6321 4.34434 5 2 -15 -11 25.0972 3.96168 4 -2 -15 11 26.1662 8.69412 3 2 15 -11 26.3097 7.14908 3 2 15 -11 29.5807 4.86139 2 -2 15 11 23.118 3.92018 2 -2 15 11 34.4294 5.20039 5 1 -15 -11 356.151 17.1726 4 -1 -15 11 369.302 18.4576 5 1 -15 -11 372.64 24.8196 3 1 -15 -11 343.849 17.0253 5 -1 -15 11 314.34 26.9973 3 1 15 -11 376.451 19.2497 2 -1 15 11 369.319 18.6357 2 -1 15 11 352.04 19.219 5 0 -15 -11 829.879 36.9977 5 0 -15 11 750.464 47.9451 3 0 -15 11 879.253 38.6459 5 0 -15 -11 969.29 47.8092 3 0 15 -11 879.13 39.0283 5 0 15 -11 887.121 37.383 5 0 15 11 854.285 39.09 2 0 15 11 878.061 39.5044 5 -1 -15 -11 99.5303 12.6343 3 1 -15 11 68.1006 11.3635 3 1 -15 11 82.2094 6.91576 5 -1 15 -11 83.8329 7.06233 5 1 15 11 79.8703 7.09791 5 -1 15 -11 98.5224 6.29308 5 2 -15 11 21.2005 6.93183 3 2 -15 11 22.304 3.88385 5 -2 -15 -11 24.2693 7.65539 3 -2 15 -11 36.0451 3.86093 5 -2 15 -11 32.583 5.43508 2 -2 15 -11 23.2737 3.79353 5 2 15 11 27.7275 4.54924 5 3 -15 11 450.199 21.4205 2 3 -15 11 464.467 22.1822 5 3 15 11 432.45 22.2133 5 4 -15 11 662.492 30.7708 5 4 -15 11 670.751 30.0813 2 4 15 11 669.658 31.0143 5 -4 -16 11 7.33098 3.61352 5 4 -16 -11 5.645 3.44891 4 -4 -16 11 5.77634 3.36937 4 4 -16 -11 8.15109 4.69152 3 -4 -16 11 7.16191 5.71284 3 4 -16 -11 3.02724 2.27992 5 4 16 -11 4.40477 4.49798 3 4 16 -11 7.70992 2.82183 2 -4 16 11 7.18055 3.70365 5 4 16 -11 9.52341 3.10508 5 -3 -16 11 116.483 8.7914 5 3 -16 -11 115.27 7.69037 5 3 -16 -11 122.812 8.71312 4 -3 -16 11 108.14 9.4709 4 3 -16 -11 106.645 13.048 3 3 16 -11 112.477 10.3978 2 3 16 -11 115.361 13.8138 3 -3 16 11 107.564 8.01007 2 3 16 -11 127.675 9.66627 5 -3 16 11 105.802 9.41774 5 2 -16 -11 852.783 39.7034 4 -2 -16 11 861.408 41.6006 4 -2 -16 11 886.091 40.5435 5 2 -16 -11 874.06 39.1467 5 2 -16 -11 913.194 48.6061 3 2 16 -11 940.63 41.6411 2 2 16 -11 954.841 41.992 5 -2 16 11 893.268 40.3643 2 -2 16 11 895.151 41.8468 5 2 16 -11 1011.46 50.4292 3 -1 -16 11 136.797 17.0626 3 1 -16 -11 164.911 15.8489 3 -1 -16 11 129.647 9.46968 5 -1 -16 11 147.319 10.4542 4 1 16 -11 144.848 8.91981 5 1 16 -11 150.859 10.5231 2 -1 16 11 138.448 9.99677 2 -1 16 11 138.784 10.3425 5 0 -16 -11 26.9803 7.4771 3 0 -16 11 22.8296 4.20445 5 0 -16 11 16.9174 7.16989 3 0 16 -11 29.5504 4.57382 5 0 16 11 18.6274 4.21083 5 0 16 -11 24.5678 3.35148 5 0 16 -11 28.5837 4.68329 2 1 -16 11 216.736 20.8755 3 -1 -16 -11 253.202 21.3562 3 1 -16 11 239.171 13.8552 5 1 16 11 232.606 14.3158 5 -1 16 -11 263.985 12.8509 5 -1 16 -11 245.915 14.052 5 -1 16 -11 254.142 14.7189 2 -2 -16 -11 784.207 49.0979 3 2 -16 11 917.372 39.5963 5 2 16 11 824.312 39.6163 5 -2 16 -11 988.496 38.2131 5 -2 16 -11 883.386 40.1277 2 3 -16 11 65.546 6.35667 5 3 -16 11 60.3891 12.986 3 -3 -16 -11 41.8652 9.87278 3 3 16 11 50.7903 5.86271 5 -3 16 -11 66.7103 6.69277 2 4 -16 11 68.8662 6.37066 5 4 16 11 57.9911 6.34218 5 -4 16 -11 72.7316 6.92186 2 3 -17 -11 89.2722 6.91313 5 -3 -17 11 83.9036 8.31659 4 3 -17 -11 88.1081 12.1897 3 -3 -17 11 79.8593 14.4378 3 -3 -17 11 88.249 7.87796 5 3 17 -11 79.0348 8.11758 5 3 17 -11 98.1275 8.3388 2 3 17 -11 85.0002 12.1765 3 -3 17 11 78.8332 8.36814 5 2 -17 -11 3.64911 4.21704 3 -2 -17 11 7.24698 3.65189 5 -2 -17 11 1.62168 2.36621 4 2 -17 -11 4.31671 2.1144 5 -2 -17 11 1.43628 4.39496 3 -2 17 11 0.33609 2.57001 2 -2 17 11 2.86577 3.00912 5 2 17 -11 9.04803 3.09179 2 2 17 -11 3.33473 2.12383 5 2 17 -11 0.04087 3.60231 3 1 -17 -11 113.063 7.96042 5 -1 -17 11 120.445 9.68299 4 -1 -17 11 125.699 16.5676 3 1 17 -11 123.757 8.15529 5 -1 17 11 139.063 9.60501 2 1 17 -11 132.586 9.71623 5 0 -17 -11 750.667 41.8753 3 0 -17 11 596.563 42.2785 3 0 17 -11 730.732 33.2585 2 -1 -17 -11 217.654 20.0323 3 1 -17 11 189.254 19.8294 3 -1 17 -11 204.053 13.1543 2 -1 17 -11 219.135 11.3743 5 -1 17 -11 193.792 12.4887 5 2 -17 11 16.3161 7.03832 3 -2 -17 -11 22.4314 8.27522 3 -2 17 -11 18.546 4.05726 2 -2 -18 11 617.859 30.1117 5 2 -18 -11 593.285 28.6178 5 -2 -18 11 624.113 31.2427 4 2 -18 -11 653.583 38.9788 3 2 18 -11 689.073 31.6473 2 -2 18 11 637.471 30.1312 2 -2 18 11 607.981 31.4182 5 2 18 -11 649.335 31.6373 5 2 18 -11 634.351 29.0648 5 -1 -18 11 168.515 11.6025 4 -1 -18 11 175.257 11.2683 5 1 -18 -11 171.273 17.0882 3 -1 -18 11 133.171 18.0247 3 1 -18 -11 148.886 10.652 5 1 18 -11 159.516 9.92811 5 -1 18 11 154.331 11.7213 5 1 18 -11 169.904 11.7896 2 -1 18 11 152.443 11.2294 2 1 18 -11 191.759 12.4771 5 0 -18 11 33.2853 5.07035 5 0 -18 11 39.4909 10.9578 3 0 -18 -11 32.7115 8.93119 3 0 18 -11 29.2731 5.27573 2 0 18 -11 38.6754 4.51495 5 0 18 11 35.8012 5.70826 5 1 -18 11 159.563 10.8778 5 -1 -18 -11 146.212 16.7444 3 -1 18 -11 132.478 11.9299 5 1 18 11 149.845 10.9322 5 -1 18 -11 141.095 10.6926 2 -1 18 -11 164.50 9.31949 5 9 0 -12 1007.59 43.8842 4 -9 0 12 1000.26 44.7455 4 9 0 -12 858.951 60.1848 3 -8 0 12 116.533 7.83113 5 -8 0 12 138.416 10.2056 4 8 0 -12 119.735 8.95428 5 8 0 -12 125.766 17.5554 3 8 0 -12 109.234 8.9186 4 7 0 -12 2.27582 2.1555 4 7 0 -12 3.9334 1.46965 2 7 0 -12 0.58256 1.98183 5 -7 0 12 3.54236 2.10464 4 7 0 -12 3.87934 5.41763 3 -7 0 12 0.47199 1.80356 5 6 0 -12 166.07 8.63312 2 -6 0 12 162.467 8.34435 2 -6 0 12 155.739 10.7039 5 -6 0 12 163.517 10.6214 4 6 0 -12 154.244 9.8682 5 6 0 -12 142.208 9.6343 4 6 0 -12 138.092 16.4769 3 -5 0 12 1906.15 78.6858 5 5 0 -12 1730.33 88.5805 3 -5 0 12 1930.03 79.7123 4 5 0 -12 1998.97 77.7283 2 -5 0 12 1975.17 77.2574 2 5 0 -12 1876.39 78.8306 4 5 0 -12 1903.64 78.971 5 -4 0 12 105.294 7.37809 5 4 0 -12 100.544 11.5758 3 -4 0 12 104.753 7.6192 4 4 0 -12 98.4144 7.12933 4 4 0 -12 105.021 6.56884 2 -4 0 12 109.357 6.39027 2 4 0 -12 128.302 7.77203 5 -3 0 12 438.471 19.9853 5 -3 0 12 426.555 20.1239 4 3 0 -12 418.034 19.174 2 3 0 -12 410.001 19.6388 5 3 0 -12 430.823 19.5416 4 -3 0 12 427.618 18.9285 2 3 0 -12 371.912 24.4244 3 2 0 -12 529.197 23.7054 2 -2 0 12 543.67 24.249 4 -2 0 12 562.998 23.629 2 2 0 -12 468.931 27.1798 3 -2 0 12 554.404 24.3211 5 2 0 -12 531.663 23.8335 5 1 0 -12 2773.46 121.052 3 1 0 -12 3136.18 118.993 5 0 0 -12 220.017 10.8473 5 0 0 12 217.977 11.4975 2 0 0 -12 239.036 11.8927 2 0 0 12 221.215 11.6039 5 0 0 12 212.502 11.2557 4 0 0 -12 223.549 10.4691 3 -1 0 -12 470.705 20.2266 5 1 0 12 468.773 21.6339 2 1 0 12 489.131 21.5286 5 -1 0 -12 470.601 21.7748 2 1 0 12 461.827 21.0444 4 -2 0 -12 891.332 34.9107 5 2 0 12 831.151 36.4836 2 -2 0 -12 812.548 36.4893 2 2 0 12 864.886 35.9197 5 2 0 12 803.597 35.4407 4 3 0 12 1904.90 76.9389 2 3 0 12 1819.79 75.7864 5 4 0 12 9.87679 2.09445 5 5 0 12 468.396 22.3047 2 5 0 12 466.577 20.6853 5 6 0 12 442.203 21.2652 2 6 0 12 425.602 19.143 5 7 0 12 873.394 39.9614 4 7 0 12 759.339 36.2488 2 8 0 12 13.5249 3.3046 2 9 -1 -12 14.9176 8.96979 3 9 -1 -12 21.7157 4.58677 4 9 -1 -12 12.9676 5.53273 5 -9 -1 12 12.3797 4.03202 4 9 1 -12 14.3933 8.75078 3 -9 1 12 14.0745 3.96901 4 9 1 -12 14.6104 4.02103 4 -8 -1 12 148.724 8.78536 5 8 -1 -12 129.482 9.87133 4 -8 -1 12 133.52 10.4459 4 8 -1 -12 144.883 9.8126 5 8 -1 -12 134.669 18.4751 3 8 1 -12 144.937 9.92198 5 8 1 -12 139.644 9.98527 4 8 1 -12 124.758 17.8858 3 -8 1 12 142.383 10.5598 4 7 -1 -12 951.896 57.6866 3 -7 -1 12 1001.07 43.1055 5 7 -1 -12 1010.95 44.4589 4 7 -1 -12 1051.74 41.9046 2 7 -1 -12 969.454 43.9514 5 -7 -1 12 1007.82 45.1972 4 7 1 -12 1029.35 42.2226 2 -7 1 12 1060.23 43.3898 5 7 1 -12 937.029 56.8807 3 7 1 -12 975.445 44.1026 4 -7 1 12 1031.25 45.3185 4 7 1 -12 995.873 44.2332 5 6 -1 -12 170.56 18.581 3 6 -1 -12 194.536 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3 6 14 123.007 6.529 4 4 -6 14 188.965 10.4927 5 4 -6 14 199.049 11.1376 2 4 6 14 179.891 11.499 2 -4 6 -14 189.303 11.2768 2 4 6 14 169.208 10.187 5 5 -6 14 44.947 4.59481 2 5 -6 14 34.2231 4.02412 5 5 6 14 32.973 5.10906 2 -5 6 -14 32.154 4.73398 2 5 6 14 44.9249 4.28645 5 6 -6 14 118.536 8.41088 2 6 6 14 117.248 9.24975 2 -7 -7 14 87.263 9.82638 4 7 -7 -14 88.4659 7.46991 5 -7 -7 14 92.8919 7.24575 5 7 -7 -14 73.7297 13.6511 3 7 7 -14 75.3752 13.2639 3 7 7 -14 77.7037 6.61226 2 7 7 -14 84.846 7.68629 5 -7 7 14 82.1428 12.9565 4 6 -7 -14 44.6342 5.99459 4 -6 -7 14 46.8978 5.1132 5 -6 -7 14 48.7949 6.67471 4 6 -7 -14 45.0348 5.03664 5 -6 7 14 35.6797 5.40502 5 6 7 -14 45.1801 9.70317 3 6 7 -14 61.8425 5.73776 2 6 7 -14 46.3764 6.31477 5 -6 7 14 47.3014 5.72363 4 5 -7 -14 2.27447 2.4338 4 -5 -7 14 6.83768 2.62239 5 -5 -7 14 3.62557 1.80628 2 5 -7 -14 4.29364 3.55 5 -5 7 14 2.69468 1.53487 2 -5 7 14 3.68187 2.58796 5 -5 7 14 1.69197 2.03838 4 5 7 -14 4.68787 4.28187 3 5 7 -14 6.75094 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0 -5 -18 41.5388 4.11939 5 0 -5 18 48.8561 5.59917 4 0 5 -18 32.4307 5.2971 2 0 5 -18 59.4357 5.15632 5 0 5 18 51.9415 5.76898 5 0 5 18 43.4431 5.4957 2 0 5 18 53.5811 5.24254 4 1 -5 18 102.079 8.32152 4 1 -5 18 110.054 8.06279 2 1 -5 18 107.316 8.26241 5 1 5 18 99.7333 8.28971 2 1 5 18 104.183 8.2503 5 -1 5 -18 96.0475 8.59684 2 2 -5 18 235.736 13.8748 4 2 -5 18 242.78 13.9356 5 2 5 18 238.92 14.0171 5 3 -5 18 408.573 19.809 5 3 -5 18 370.067 19.6886 2 3 -5 18 377.548 19.5961 4 3 5 18 376.344 19.6554 5 -3 5 -18 384.008 20.4072 2 3 5 18 356.543 20.171 2 -4 -6 18 269.938 16.9508 4 4 -6 -18 295.922 15.7681 4 -4 -6 18 257.759 14.7522 2 4 -6 -18 296.656 15.692 5 -4 -6 18 285.844 16.1857 5 -4 6 18 290.003 16.4361 4 4 6 -18 248.416 15.7305 2 -4 6 18 286.534 16.5522 5 -4 6 18 277.338 14.8812 2 4 6 -18 275.034 17.9225 5 3 -6 -18 15.0024 3.48551 5 -3 -6 18 18.3238 3.54679 2 -3 -6 18 8.27677 4.01574 5 -3 6 18 23.0407 5.65784 5 -3 6 18 18.5163 4.74704 4 3 6 -18 8.87101 3.38391 5 -3 6 18 18.5075 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-18 9.27895 3.39415 2 3 6 18 21.2393 4.3257 2 -4 -7 18 30.8423 5.0702 5 4 -7 -18 25.9001 4.7061 4 4 -7 -18 28.0474 4.53622 5 -4 -7 18 25.3844 5.16197 4 -4 7 18 24.1565 4.20902 2 -4 7 18 28.514 5.16673 5 4 7 -18 36.8751 5.52517 5 4 7 -18 33.6401 5.877 2 -4 7 18 25.0737 4.62464 4 -3 -7 18 6.66624 3.02729 4 3 -7 -18 6.77211 2.63211 5 -3 -7 18 2.73856 2.64295 5 -3 7 18 4.17093 2.64267 5 -3 7 18 6.40197 3.11976 4 -3 7 18 6.95539 2.98983 2 3 7 -18 7.2691 2.97831 5 2 -7 -18 601.682 28.5249 5 -2 -7 18 614.468 31.0162 2 -2 7 18 646.571 29.7698 2 -2 7 18 659.285 30.0837 4 2 7 -18 654.504 30.3201 5 -1 -7 18 21.9111 4.57321 4 1 -7 -18 18.4988 3.25529 5 -1 -7 18 21.3772 4.31553 5 -1 7 18 22.8374 3.78653 4 -1 7 18 19.2928 4.06917 5 -1 7 18 23.1572 4.40239 2 1 7 -18 21.2223 3.84368 5 0 -7 18 82.7429 7.51752 5 0 -7 -18 84.9254 5.96113 5 0 -7 18 99.1768 8.19515 4 0 7 18 80.4532 7.78851 5 0 7 -18 94.5665 7.02965 5 0 7 18 101.387 7.95657 2 1 -7 18 4.62979 2.16589 2 1 -7 18 3.211 2.2153 4 1 -7 18 3.31503 2.43791 5 1 7 18 8.54966 2.91747 5 -1 7 -18 1.48147 2.26317 2 2 -7 18 549.036 26.9011 2 2 -7 18 579.333 27.7441 4 2 -7 18 582.08 27.1652 5 -2 7 -18 553.98 27.7926 2 2 7 18 551.926 27.7044 2 2 7 18 561.33 27.3466 5 -3 -8 18 4.3318 2.925 4 -3 -8 18 4.43693 2.86738 5 -3 -8 18 1.13576 2.22644 2 3 -8 -18 0.93041 2.57346 5 3 8 -18 -0.7007 2.24864 2 -3 8 18 4.89689 2.64395 2 3 8 -18 9.16424 3.43231 5 -3 8 18 9.00732 3.30796 5 -2 -8 18 13.6149 3.40321 2 2 -8 -18 7.97761 2.79678 5 -2 -8 18 5.44655 3.21197 5 -2 -8 18 8.03047 3.21949 4 -2 8 18 8.12541 2.92091 2 2 8 -18 11.3336 3.59606 2 2 8 -18 9.58516 3.39778 5 -2 8 18 12.7103 3.95395 5 -2 8 18 10.6315 3.15156 4 -1 -8 18 8.62349 4.33242 4 -1 -8 18 5.18275 2.76447 2 1 -8 -18 10.3394 2.76195 5 1 8 -18 11.6215 3.2207 5 -1 8 18 2.39898 2.81821 5 -1 8 18 8.1753 2.86387 2 0 -8 18 812.353 35.4089 2 0 -8 -18 727.67 34.8304 5 0 -8 18 767.544 39.223 5 0 8 -18 785.371 36.2672 2 0 8 18 777.281 35.8707 2 1 -8 18 -2.7739 1.99586 5 1 -8 18 -0.629 1.75042 2 -1 8 -18 -0.5369 2.11697 2 1 8 18 0.02734 2.91318 2 1 8 18 1.39827 1.96783 5 2 -8 18 12.8194 3.46613 2 2 -8 18 14.2594 3.63617 5 2 -8 18 7.11387 3.26188 4 -2 8 -18 12.1454 3.67158 2 2 8 18 19.1753 4.19068 2 2 8 18 12.834 3.47718 5 2 -9 -18 738.82 33.4075 5 -2 -9 18 789.911 37.0322 4 -2 -9 18 768.729 35.3352 5 -2 -9 18 747.937 34.4768 2 2 9 -18 783.04 35.2291 5 -2 9 18 756.222 34.8862 2 -2 9 18 754.88 36.1246 5 2 9 -18 728.739 35.5407 2 -1 -9 18 16.3853 4.24534 4 1 -9 -18 9.51733 2.98022 5 -1 -9 18 14.7091 3.54949 2 -1 -9 18 15.2274 3.76464 5 1 9 -18 14.9537 3.85941 2 1 9 -18 8.91166 3.44929 5 -1 9 18 6.37171 3.00007 2 -1 9 18 9.49949 3.46272 5 0 -9 18 101.529 8.01527 2 0 -9 18 92.8446 8.58024 4 0 -9 18 106.591 8.42145 5 0 9 -18 108.082 8.94764 2 0 9 18 106.869 8.81131 5 1 -9 18 -0.1613 2.23871 4 1 -9 18 0.13838 1.69141 2 1 -9 18 1.04911 3.43517 5 -1 9 -18 -0.386 2.71711 2 1 9 18 2.65175 2.73376 2 1 9 18 0.5997 2.34168 5 -4 0 19 -0.3595 2.35246 5 -4 0 19 0.34868 2.06291 2 4 0 -19 3.7451 2.30807 5 -4 0 19 1.10956 2.32189 4 4 0 -19 -0.4609 2.01392 2 3 0 -19 0.52837 2.36569 5 -3 0 19 2.69364 2.31651 5 -3 0 19 0.37984 2.13413 4 -3 0 19 -0.1335 1.46249 2 3 0 -19 1.06762 2.10127 2 -2 0 19 1.70015 2.00757 2 2 0 -19 0.01483 2.37765 5 -2 0 19 -2.69 3.00103 5 2 0 -19 2.34101 2.34945 2 -1 0 19 1.0279 1.94422 2 -1 0 19 -0.0168 2.17646 5 1 0 -19 0.65059 1.87364 5 1 0 -19 -3.3119 1.73188 2 0 0 19 1.45157 1.92472 4 0 0 19 1.68397 1.86499 5 0 0 19 5.07696 2.48223 2 0 0 -19 3.08219 2.70996 5 1 0 19 0.01341 2.18584 5 1 0 19 0.27356 2.12859 4 2 0 19 -2.3662 1.96837 2 2 0 19 1.0659 2.24688 4 2 0 19 -1.5857 1.58227 5 4 -1 -19 4.21435 2.47025 5 -4 -1 19 3.12954 2.27378 2 -4 -1 19 2.44702 2.63727 4 -4 -1 19 10.3826 3.49058 5 4 -1 -19 0.58971 1.96304 2 -4 1 19 6.20436 3.15143 4 -4 1 19 6.23624 2.96345 5 4 1 -19 -0.0619 1.92393 2 -4 1 19 3.34391 2.45511 2 4 1 -19 5.91994 2.47478 5 -3 -1 19 2.13724 1.85809 2 3 -1 -19 4.08986 2.15833 2 3 -1 -19 2.98674 2.58677 5 -3 -1 19 3.94826 2.43407 4 -3 -1 19 1.08642 2.40611 5 3 1 -19 0.62595 1.75609 2 -3 1 19 0.57567 1.87108 2 -3 1 19 -1.3723 2.23967 5 3 1 -19 3.98952 2.77441 5 -3 1 19 7.07843 2.51578 4 2 -1 -19 0.07319 2.02065 2 2 -1 -19 -0.6476 2.4983 5 -2 -1 19 -2.1099 3.17518 5 -2 -1 19 -1.0599 1.94718 4 -2 -1 19 -0.6552 1.72814 2 2 1 -19 0.76375 2.20829 2 2 1 -19 0.99901 2.59639 5 -2 1 19 0.6256 1.90096 2 -2 1 19 -1.6171 1.72338 4 -1 -1 19 35.3631 5.24106 5 -1 -1 19 32.879 5.26016 4 1 -1 -19 36.3587 4.54388 5 -1 -1 19 39.3043 5.23886 2 1 1 -19 43.8718 5.83065 2 -1 1 19 44.1166 5.59242 2 1 1 -19 43.9151 4.82623 5 -1 1 19 39.9734 5.82544 5 -1 1 19 49.7323 5.46532 4 0 -1 19 -0.4142 1.92665 5 0 -1 19 1.21713 2.34659 2 0 -1 19 4.80194 2.28061 4 0 1 19 -1.4052 1.64571 5 0 1 -19 5.86847 2.69735 2 0 1 19 0.43047 1.9777 4 0 1 19 0.96587 1.92039 2 1 -1 19 1.53009 2.60165 5 1 -1 19 5.50349 2.42037 4 1 1 19 3.45233 2.28311 4 1 1 19 3.92919 2.61371 5 2 -1 19 -1.7811 2.00202 2 2 -1 19 -1.8488 1.76435 4 2 -1 19 0.67714 2.18698 5 2 1 19 -0.9088 2.05504 2 2 1 19 0.49768 1.95015 5 -4 -2 19 3.47208 2.38361 2 -4 -2 19 0.82595 2.34317 4 -4 -2 19 6.02804 2.81422 5 4 -2 -19 4.14292 2.22402 5 -4 2 19 2.46523 2.44452 5 -4 2 19 1.60929 2.2411 2 4 2 -19 1.60925 2.2279 2 4 2 -19 2.67186 2.36423 5 -3 -2 19 79.6093 12.1119 4 -3 -2 19 77.1451 7.38152 5 -3 -2 19 74.3206 6.52955 2 3 -2 -19 75.5131 6.94828 5 -3 2 19 72.4969 7.17134 4 3 2 -19 78.5133 7.08254 5 -3 2 19 77.9238 7.60426 5 -3 2 19 81.3132 6.85938 2 3 2 -19 85.8273 7.50428 2 2 -2 -19 188.265 15.2366 5 -2 -2 19 191.485 12.3906 4 -2 -2 19 172.719 11.2884 2 -2 2 19 186.322 11.541 2 2 2 -19 210.696 12.5196 2 -2 2 19 173.217 13.3726 4 -1 -2 19 83.1345 7.49304 5 -1 -2 19 76.3007 7.08569 4 -1 -2 19 75.8424 6.82812 2 1 -2 -19 84.7831 6.33353 5 1 2 -19 81.008 7.26575 2 1 2 -19 80.7375 6.53085 5 -1 2 19 84.5283 7.26159 2 -1 2 19 84.1888 7.33303 4 -1 2 19 71.5163 7.25931 5 0 -2 19 -0.2124 1.83315 2 0 -2 19 -1.4741 3.1812 4 0 -2 19 0.42877 2.0614 5 0 2 19 1.53207 2.15985 5 0 2 19 1.23209 2.1088 4 0 2 19 0.7766 2.07787 2 1 -2 19 26.1916 4.56762 2 1 -2 19 29.0796 4.87639 5 -1 2 -19 27.755 4.6872 2 1 2 19 20.5274 4.37735 5 1 2 19 33.2349 4.69249 4 1 2 19 24.99 5.47997 2 2 -2 19 50.2872 7.04658 4 2 -2 19 40.1732 5.60904 5 2 -2 19 40.707 5.73434 2 2 2 19 55.1132 5.83858 5 2 2 19 55.4296 6.55351 2 4 -3 -19 86.1775 7.20117 5 -4 -3 19 64.243 7.02864 5 -4 -3 19 71.9724 7.62583 4 -4 -3 19 81.553 6.9267 2 4 3 -19 73.5834 7.11816 2 -4 3 19 70.1886 6.51871 2 -4 3 19 85.3768 8.07168 5 4 3 -19 98.3386 7.77275 5 -3 -3 19 103.865 7.73403 2 3 -3 -19 80.7353 7.33058 5 -3 -3 19 82.7387 7.99961 5 -3 -3 19 113.136 13.1999 4 3 3 -19 93.8305 7.97276 5 -3 3 19 94.6395 7.51371 2 -3 3 19 105.966 8.44651 4 -3 3 19 86.1536 8.3712 5 3 3 -19 101.661 8.07 2 -2 -3 19 -1.688 1.75702 4 -2 -3 19 -0.8393 1.89733 2 -2 -3 19 6.64922 4.5073 5 -2 3 19 2.504 2.74381 5 2 3 -19 -4.4367 3.29274 5 2 3 -19 3.64764 2.37644 2 -2 3 19 0.52587 1.72085 2 -1 -3 19 236.012 14.4806 5 -1 -3 19 232.613 14.2611 4 1 -3 -19 262.814 12.8294 5 -1 -3 19 216.667 13.593 2 -1 3 19 248.273 14.1047 4 -1 3 19 235.402 13.8522 2 -1 3 19 206.918 14.2914 5 1 3 -19 200.872 15.0686 2 1 3 -19 263.779 13.2931 5 0 -3 19 58.6363 6.28988 5 0 -3 19 53.5173 5.85461 4 0 3 19 57.9905 5.9463 4 0 3 19 58.4549 6.12102 5 0 3 -19 53.2086 7.84016 2 0 3 19 50.7089 6.36362 2 1 -3 19 89.1738 7.55692 2 1 -3 19 96.1361 7.76429 4 1 -3 19 97.7672 8.03454 5 -1 3 -19 97.017 8.25538 2 1 3 19 91.3813 8.07911 5 1 3 19 98.0158 8.22588 2 2 -3 19 -0.9765 2.02601 2 2 -3 19 0.92122 2.02799 5 2 -3 19 2.165 2.15876 4 -2 3 -19 -1.7511 2.11386 2 2 3 19 0.30419 2.33494 2 2 3 19 0.69544 1.83906 5 -3 -4 19 360.765 20.4724 4 3 -4 -19 378.047 18.875 5 -3 -4 19 379.171 20.094 5 -3 4 19 381.752 20.0825 4 -3 4 19 348.404 20.0915 5 -3 4 19 368.921 18.9905 2 2 -4 -19 147.30 9.4213 5 -2 -4 19 139.757 11.9153 4 -2 -4 19 165.114 11.4956 2 -2 -4 19 143.874 10.4379 5 -2 4 19 142.914 9.78819 2 2 4 -19 139.965 9.8239 5 -2 4 19 132.546 10.3481 5 -2 4 19 148.652 11.7837 4 1 -4 -19 156.517 9.05085 5 -1 -4 19 144.894 10.5277 4 1 4 -19 143.989 12.0324 2 -1 4 19 134.584 9.84916 4 -1 4 19 143.897 10.1944 2 1 4 -19 154.13 9.59123 5 0 -4 19 0.00946 2.03448 5 0 -4 19 3.36059 2.23889 4 0 -4 19 -2.8654 2.16019 2 0 4 19 2.26575 1.92677 4 0 4 19 1.51916 2.26641 5 0 4 19 2.77727 2.85669 2 0 4 -19 1.01417 1.99131 2 1 -4 19 263.846 15.4411 2 1 -4 19 292.859 15.9149 5 1 -4 19 264.891 15.6284 4 1 4 19 282.445 15.989 2 -1 4 -19 268.754 15.9348 2 1 4 19 276.502 15.9435 5 2 -4 19 112.368 8.52033 5 2 -4 19 97.8513 8.22217 4 2 -4 19 112.776 8.57257 2 2 4 19 104.149 8.74551 2 -2 4 -19 112.35 9.04566 2 2 4 19 109.441 8.56903 5 -3 -5 19 100.923 8.71699 5 -3 -5 19 126.225 9.77717 4 3 -5 -19 107.008 8.2609 5 -3 -5 19 91.9152 7.73223 2 -3 5 19 103.711 9.23868 5 3 5 -19 100.245 8.3097 2 -3 5 19 105.971 8.6545 4 3 5 -19 112.003 8.75848 5 -3 5 19 116.774 8.50339 2 2 -5 -19 2.60874 2.11178 5 -2 -5 19 -1.044 2.47692 2 -2 -5 19 6.37751 2.91629 5 -2 -5 19 5.02748 3.1201 4 -2 5 19 0.22664 1.79632 4 -2 5 19 -2.1483 1.76684 2 -2 5 19 4.32056 2.55717 5 2 5 -19 0.20997 2.14557 2 2 5 -19 1.67918 2.25933 5 -1 -5 19 332.271 20.4194 4 -1 -5 19 306.228 17.4111 2 -1 -5 19 351.137 22.305 5 1 -5 -19 342.677 16.2956 5 1 5 -19 329.235 18.1861 2 1 5 -19 337.188 16.9502 5 -1 5 19 348.785 17.8825 4 -1 5 19 294.839 19.6662 5 -1 5 19 309.337 17.5675 2 0 -5 19 96.5522 8.20376 4 0 -5 19 105.45 8.0965 2 0 5 -19 94.2405 8.25341 2 1 -5 19 180.474 11.9271 2 1 -5 19 201.883 12.5921 4 1 -5 19 199.775 12.7836 5 1 5 19 198.204 12.7632 2 1 5 19 198.674 13.0295 5 -1 5 -19 196.343 12.9148 2 2 -6 -19 121.07 8.30691 5 -2 -6 19 116.347 9.87284 4 -2 -6 19 138.886 9.9402 5 -2 -6 19 130.98 9.27923 2 -2 6 19 133.793 10.2357 5 -2 6 19 128.31 9.18501 2 2 6 -19 130.834 9.78605 2 2 6 -19 127.362 9.19001 5 -2 6 19 129.268 9.31878 4 -1 -6 19 180.515 12.5782 4 -1 -6 19 167.461 11.1068 2 -1 -6 19 177.08 11.9117 5 1 -6 -19 181.249 10.1959 5 -1 6 19 190.287 12.4688 5 1 6 -19 191.316 12.288 2 -1 6 19 156.845 11.2026 2 0 -6 19 6.94339 3.17571 5 0 -6 19 2.76038 2.44168 2 0 6 19 3.86448 2.66021 5 0 6 -19 7.88462 3.17867 2 0 6 19 4.11472 2.6949 2 1 -6 19 527.148 25.992 2 -1 6 -19 555.962 27.1557 2 1 6 19 527.207 26.6221 2 -1 -7 19 317.513 17.4614 5 -1 -7 19 311.484 16.7244 2 -1 -7 19 322.253 18.2213 4 -1 7 19 293.68 17.6017 5 1 7 -19 293.458 17.3936 2 0 -7 19 0.7506 2.08655 2 0 -7 19 3.13137 2.31614 4 0 -7 19 -0.0173 2.09857 5 0 7 19 1.67197 2.10678 2 0 7 19 5.01077 2.78894 5 0 7 -19 -1.3974 2.20467 2 -2 0 20 42.9825 6.31308 4 2 0 -20 45.7129 5.99495 2 2 0 -20 45.2211 5.18333 5 -2 0 20 29.3211 4.71432 2 -2 0 20 49.6968 6.52914 5 1 0 -20 753.815 36.9809 5 -1 0 20 853.318 37.8933 2 -1 0 20 889.028 38.9609 5 0 0 20 62.5122 6.86613 2 0 0 20 72.4406 7.08126 5 0 0 20 63.2868 6.60318 4 -2 -1 20 26.9193 4.35029 2 2 -1 -20 25.6727 4.2791 5 2 1 -20 26.6992 4.58083 2 -2 1 20 30.817 5.09363 5 2 1 -20 28.1593 4.44763 5 -2 1 20 26.1143 5.20707 2 -1 -1 20 37.1876 5.45752 4 1 -1 -20 33.8461 5.56982 5 -1 -1 20 23.8839 4.36334 2 -1 -1 20 33.0027 5.54186 5 1 1 -20 27.8168 5.04343 5 1 1 -20 33.232 5.35982 2 -1 1 20 33.854 5.48231 5 -1 1 20 24.6712 4.36744 2 -1 1 20 24.5835 4.62675 4 0 -1 20 47.5226 6.0082 2 0 -1 20 46.6599 5.60154 4 0 -1 20 39.5647 5.82869 5 0 1 -20 45.8132 6.31209 2 0 1 20 51.8908 6.52783 2 0 1 20 44.7696 6.9191 4 0 1 20 55.1223 6.13217 5 -1 -2 20 695.845 32.2461 2 -1 -2 20 692.978 32.9592 5 -1 -2 20 646.473 32.9435 4 -1 2 20 696.852 32.6587 4 -1 2 20 732.539 33.4405 5 -1 2 20 669.106 32.1376 2 1 2 -20 692.161 32.8629 2 0 -2 20 3.34377 2.29936 5 0 -2 20 -1.7438 1.92582 4 0 -2 20 6.83491 2.96608 2 0 2 20 1.32589 1.98103 4 0 2 20 1.93901 2.28896 5 0 2 -20 3.83196 2.56621 2 0 2 20 -0.2685 2.6617 2 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 10843 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.6141(2) 0.74230(11) 0.61259(12) 0.0156(3) Uani 1 1 d . . . . . C2 C 0.4771(2) 0.86089(12) 0.59822(13) 0.0202(4) Uani 1 1 d . . . . . H2 H 0.41521 0.896734 0.562434 0.024 Uiso 1 1 calc R U . . . C3 C 0.5118(2) 0.88139(12) 0.68445(13) 0.0215(4) Uani 1 1 d . . . . . C4 C 0.6011(2) 0.82754(13) 0.73528(12) 0.0238(4) Uani 1 1 d . . . . . H4 H 0.627091 0.838848 0.794589 0.029 Uiso 1 1 calc R U . . . C5 C 0.6526(2) 0.75722(12) 0.70000(13) 0.0215(4) Uani 1 1 d . . . . . H5 H 0.713024 0.719959 0.734714 0.026 Uiso 1 1 calc R U . . . C6 C 0.6665(2) 0.66796(11) 0.57175(11) 0.0159(3) Uani 1 1 d . . . . . C7 C 0.7980(2) 0.60777(12) 0.46360(12) 0.0188(4) Uani 1 1 d . . . . . H7 H 0.85874 0.612781 0.414619 0.023 Uiso 1 1 calc R U . . . C8 C 0.7632(2) 0.53201(11) 0.49179(12) 0.0187(4) Uani 1 1 d . . . . . C9 C 0.6777(3) 0.52647(12) 0.56491(13) 0.0229(4) Uani 1 1 d . . . . . H9 H 0.65225 0.47584 0.587076 0.028 Uiso 1 1 calc R U . . . C10 C 0.6296(2) 0.59479(12) 0.60552(13) 0.0216(4) Uani 1 1 d . . . . . H10 H 0.572144 0.591402 0.655863 0.026 Uiso 1 1 calc R U . . . C11 C 0.4507(3) 0.95812(14) 0.71939(16) 0.0322(5) Uani 1 1 d . . . . . H11A H 0.368832 0.946675 0.759448 0.048 Uiso 1 1 calc R U . . . H11B H 0.40461 0.990645 0.671537 0.048 Uiso 1 1 calc R U . . . H11C H 0.539 0.986963 0.7499 0.048 Uiso 1 1 calc R U . . . C12 C 0.8170(3) 0.45958(12) 0.44581(14) 0.0259(4) Uani 1 1 d . . . . . H12A H 0.731107 0.441279 0.40453 0.039 Uiso 1 1 calc R U . . . H12B H 0.843989 0.417523 0.487988 0.039 Uiso 1 1 calc R U . . . H12C H 0.911146 0.472602 0.414874 0.039 Uiso 1 1 calc R U . . . C13 C 0.2580(2) 0.80058(11) 0.23207(12) 0.0178(4) Uani 1 1 d . . . . . C14 C 0.1495(2) 0.68453(11) 0.28071(12) 0.0178(3) Uani 1 1 d . . . . . C15 C 0.0792(2) 0.69415(12) 0.18832(13) 0.0216(4) Uani 1 1 d . . . . . H15A H -0.038645 0.69686 0.186377 0.026 Uiso 1 1 calc R U . . . H15B H 0.110194 0.649156 0.152101 0.026 Uiso 1 1 calc R U . . . C16 C 0.1481(2) 0.77181(12) 0.15697(12) 0.0217(4) Uani 1 1 d . . . . . H16A H 0.208071 0.762819 0.105265 0.026 Uiso 1 1 calc R U . . . H16B H 0.062381 0.810894 0.142521 0.026 Uiso 1 1 calc R U . . . C17 C 0.9919(2) 0.91783(11) 0.31389(12) 0.0200(4) Uani 1 1 d . . . . . C18 C 1.1088(2) 0.94154(11) 0.45045(12) 0.0180(3) Uani 1 1 d . . . . . C19 C 1.1820(2) 1.00171(12) 0.39297(13) 0.0230(4) Uani 1 1 d . . . . . H19A H 1.297957 0.992293 0.391152 0.028 Uiso 1 1 calc R U . . . H19B H 1.165281 1.056312 0.414092 0.028 Uiso 1 1 calc R U . . . C20 C 1.0966(3) 0.98977(12) 0.30402(13) 0.0233(4) Uani 1 1 d . . . . . H20A H 1.031442 1.036866 0.286736 0.028 Uiso 1 1 calc R U . . . H20B H 1.174031 0.980131 0.260099 0.028 Uiso 1 1 calc R U . . . I1 I 0.38366(2) 0.76443(2) 0.41861(2) 0.01607(4) Uani 1 1 d . . . . . I2 I 0.88041(2) 0.79766(2) 0.44702(2) 0.01604(4) Uani 1 1 d . . . . . N1 N 0.52612(19) 0.79361(9) 0.56299(10) 0.0169(3) Uani 1 1 d . . . . . N2 N 0.75075(19) 0.67424(9) 0.50158(10) 0.0171(3) Uani 1 1 d . . . . . N3 N 0.25049(19) 0.74771(9) 0.30004(10) 0.0169(3) Uani 1 1 d . . . . . N4 N 1.00429(18) 0.89478(9) 0.39981(10) 0.0171(3) Uani 1 1 d . . . . . O1 O 0.33935(18) 0.86004(9) 0.23483(10) 0.0261(3) Uani 1 1 d . . . . . O2 O 0.12482(19) 0.63067(9) 0.32978(9) 0.0269(3) Uani 1 1 d . . . . . O3 O 0.91077(19) 0.88426(10) 0.25735(10) 0.0299(3) Uani 1 1 d . . . . . O4 O 1.13672(17) 0.93400(9) 0.52767(9) 0.0224(3) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0141(8) 0.0164(8) 0.0163(8) 0.0011(7) 0.0014(6) -0.0025(6) C2 0.0173(9) 0.0192(9) 0.0241(9) -0.0026(7) 0.0012(7) 0.0000(7) C3 0.0188(9) 0.0208(9) 0.0261(9) -0.0079(7) 0.0091(7) -0.0071(7) C4 0.0283(10) 0.0278(10) 0.0157(8) -0.0047(8) 0.0036(7) -0.0084(8) C5 0.0254(10) 0.0228(9) 0.0162(8) 0.0013(7) 0.0004(7) -0.0035(8) C6 0.0154(8) 0.0169(8) 0.0151(8) 0.0003(7) -0.0015(6) -0.0004(7) C7 0.0184(9) 0.0209(9) 0.0172(8) -0.0002(7) 0.0013(7) 0.0005(7) C8 0.0195(9) 0.0172(8) 0.0186(8) -0.0012(7) -0.0037(7) 0.0014(7) C9 0.0300(10) 0.0155(9) 0.0234(9) 0.0037(7) 0.0024(8) -0.0016(8) C10 0.0270(10) 0.0199(9) 0.0184(8) 0.0026(7) 0.0044(7) -0.0014(8) C11 0.0327(12) 0.0266(11) 0.0392(12) -0.0142(9) 0.0148(10) -0.0046(9) C12 0.0302(11) 0.0192(9) 0.0278(10) -0.0058(8) -0.0010(8) 0.0028(8) C13 0.0175(9) 0.0176(9) 0.0183(8) 0.0015(7) 0.0017(7) 0.0030(7) C14 0.0181(9) 0.0166(8) 0.0188(8) -0.0031(7) 0.0019(7) 0.0019(7) C15 0.0224(10) 0.0228(9) 0.0191(9) -0.0029(7) -0.0024(7) -0.0018(7) C16 0.0256(10) 0.0237(10) 0.0155(8) 0.0007(7) -0.0012(7) 0.0009(8) C17 0.0207(9) 0.0188(9) 0.0209(9) 0.0016(7) 0.0039(7) 0.0028(7) C18 0.0139(8) 0.0155(8) 0.0249(9) -0.0013(7) 0.0038(7) 0.0016(7) C19 0.0235(10) 0.0194(9) 0.0268(10) -0.0009(8) 0.0064(8) -0.0056(7) C20 0.0276(10) 0.0175(9) 0.0253(9) 0.0042(7) 0.0050(8) -0.0006(8) I1 0.01579(6) 0.01625(6) 0.01594(6) -0.00066(4) -0.00041(4) 0.00160(4) I2 0.01593(6) 0.01561(6) 0.01671(6) -0.00019(4) 0.00203(4) -0.00105(4) N1 0.0163(7) 0.0168(7) 0.0174(7) -0.0018(6) -0.0010(6) 0.0005(6) N2 0.0166(7) 0.0177(7) 0.0168(7) 0.0005(6) 0.0008(6) 0.0003(6) N3 0.0181(8) 0.0178(7) 0.0145(7) 0.0003(6) -0.0013(6) -0.0001(6) N4 0.0177(7) 0.0155(7) 0.0184(7) 0.0016(6) 0.0021(6) -0.0021(6) O1 0.0268(7) 0.0227(7) 0.0283(7) 0.0058(6) -0.0003(6) -0.0046(6) O2 0.0342(8) 0.0205(7) 0.0257(7) 0.0029(6) 0.0010(6) -0.0050(6) O3 0.0350(8) 0.0330(8) 0.0209(7) -0.0004(6) -0.0032(6) -0.0057(7) O4 0.0220(7) 0.0242(7) 0.0208(7) 0.0000(5) -0.0011(5) 0.0001(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 C1 C5 121.40(17) . . ? N1 C1 C6 117.78(16) . . ? C5 C1 C6 120.81(17) . . ? N1 C2 C3 123.68(19) . . ? N1 C2 H2 118.2 . . ? C3 C2 H2 118.2 . . ? C4 C3 C2 116.84(18) . . ? C4 C3 C11 122.76(19) . . ? C2 C3 C11 120.4(2) . . ? C3 C4 C5 120.37(18) . . ? C3 C4 H4 119.8 . . ? C5 C4 H4 119.8 . . ? C4 C5 C1 118.72(19) . . ? C4 C5 H5 120.6 . . ? C1 C5 H5 120.6 . . ? N2 C6 C10 121.48(17) . . ? N2 C6 C1 117.98(16) . . ? C10 C6 C1 120.54(16) . . ? N2 C7 C8 123.66(17) . . ? N2 C7 H7 118.2 . . ? C8 C7 H7 118.2 . . ? C7 C8 C9 116.92(17) . . ? C7 C8 C12 121.36(17) . . ? C9 C8 C12 121.71(18) . . ? C10 C9 C8 120.05(18) . . ? C10 C9 H9 120 . . ? C8 C9 H9 120 . . ? C6 C10 C9 119.11(17) . . ? C6 C10 H10 120.4 . . ? C9 C10 H10 120.4 . . ? C3 C11 H11A 109.5 . . ? C3 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C3 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C8 C12 H12A 109.5 . . ? C8 C12 H12B 109.5 . . ? H12A C12 H12B 109.5 . . ? C8 C12 H12C 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? O1 C13 N3 124.12(18) . . ? O1 C13 C16 127.11(18) . . ? N3 C13 C16 108.77(16) . . ? O2 C14 N3 124.82(18) . . ? O2 C14 C15 126.88(18) . . ? N3 C14 C15 108.29(16) . . ? C14 C15 C16 105.17(15) . . ? C14 C15 H15A 110.7 . . ? C16 C15 H15A 110.7 . . ? C14 C15 H15B 110.7 . . ? C16 C15 H15B 110.7 . . ? H15A C15 H15B 108.8 . . ? C13 C16 C15 104.71(15) . . ? C13 C16 H16A 110.8 . . ? C15 C16 H16A 110.8 . . ? C13 C16 H16B 110.8 . . ? C15 C16 H16B 110.8 . . ? H16A C16 H16B 108.9 . . ? O3 C17 N4 124.43(18) . . ? O3 C17 C20 127.00(18) . . ? N4 C17 C20 108.57(17) . . ? O4 C18 N4 124.93(17) . . ? O4 C18 C19 126.64(18) . . ? N4 C18 C19 108.43(16) . . ? C18 C19 C20 105.13(16) . . ? C18 C19 H19A 110.7 . . ? C20 C19 H19A 110.7 . . ? C18 C19 H19B 110.7 . . ? C20 C19 H19B 110.7 . . ? H19A C19 H19B 108.8 . . ? C17 C20 C19 104.71(16) . . ? C17 C20 H20A 110.8 . . ? C19 C20 H20A 110.8 . . ? C17 C20 H20B 110.8 . . ? C19 C20 H20B 110.8 . . ? H20A C20 H20B 108.9 . . ? N3 I1 N1 175.09(6) . . ? N4 I2 N2 175.41(6) . . ? C2 N1 C1 118.98(17) . . ? C2 N1 I1 112.95(12) . . ? C1 N1 I1 126.34(12) . . ? C7 N2 C6 118.76(16) . . ? C7 N2 I2 113.08(12) . . ? C6 N2 I2 127.03(12) . . ? C14 N3 C13 113.03(16) . . ? C14 N3 I1 124.99(12) . . ? C13 N3 I1 121.98(13) . . ? C18 N4 C17 112.82(16) . . ? C18 N4 I2 123.82(12) . . ? C17 N4 I2 123.34(13) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 N1 1.343(2) . ? C1 C5 1.395(3) . ? C1 C6 1.485(2) . ? C2 N1 1.336(2) . ? C2 C3 1.393(3) . ? C2 H2 0.95 . ? C3 C4 1.387(3) . ? C3 C11 1.506(3) . ? C4 C5 1.388(3) . ? C4 H4 0.95 . ? C5 H5 0.95 . ? C6 N2 1.346(2) . ? C6 C10 1.383(3) . ? C7 N2 1.339(2) . ? C7 C8 1.387(3) . ? C7 H7 0.95 . ? C8 C9 1.390(3) . ? C8 C12 1.500(3) . ? C9 C10 1.387(3) . ? C9 H9 0.95 . ? C10 H10 0.95 . ? C11 H11A 0.98 . ? C11 H11B 0.98 . ? C11 H11C 0.98 . ? C12 H12A 0.98 . ? C12 H12B 0.98 . ? C12 H12C 0.98 . ? C13 O1 1.212(2) . ? C13 N3 1.386(2) . ? C13 C16 1.514(3) . ? C14 O2 1.212(2) . ? C14 N3 1.381(2) . ? C14 C15 1.520(3) . ? C15 C16 1.525(3) . ? C15 H15A 0.99 . ? C15 H15B 0.99 . ? C16 H16A 0.99 . ? C16 H16B 0.99 . ? C17 O3 1.212(3) . ? C17 N4 1.386(2) . ? C17 C20 1.512(3) . ? C18 O4 1.211(2) . ? C18 N4 1.382(2) . ? C18 C19 1.511(3) . ? C19 C20 1.523(3) . ? C19 H19A 0.99 . ? C19 H19B 0.99 . ? C20 H20A 0.99 . ? C20 H20B 0.99 . ? I1 N3 2.1028(16) . ? I1 N1 2.5120(16) . ? I2 N4 2.0999(15) . ? I2 N2 2.5225(16) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N1 C2 C3 C4 -0.6(3) . . . . ? N1 C2 C3 C11 -179.44(18) . . . . ? C2 C3 C4 C5 0.4(3) . . . . ? C11 C3 C4 C5 179.17(19) . . . . ? C3 C4 C5 C1 0.6(3) . . . . ? N1 C1 C5 C4 -1.3(3) . . . . ? C6 C1 C5 C4 179.98(18) . . . . ? N1 C1 C6 N2 56.4(2) . . . . ? C5 C1 C6 N2 -124.89(19) . . . . ? N1 C1 C6 C10 -123.9(2) . . . . ? C5 C1 C6 C10 54.9(3) . . . . ? N2 C7 C8 C9 -1.6(3) . . . . ? N2 C7 C8 C12 178.99(18) . . . . ? C7 C8 C9 C10 0.8(3) . . . . ? C12 C8 C9 C10 -179.82(19) . . . . ? N2 C6 C10 C9 -1.5(3) . . . . ? C1 C6 C10 C9 178.80(19) . . . . ? C8 C9 C10 C6 0.7(3) . . . . ? O2 C14 C15 C16 179.52(19) . . . . ? N3 C14 C15 C16 -1.5(2) . . . . ? O1 C13 C16 C15 178.99(19) . . . . ? N3 C13 C16 C15 -1.7(2) . . . . ? C14 C15 C16 C13 1.8(2) . . . . ? O4 C18 C19 C20 -175.64(18) . . . . ? N4 C18 C19 C20 5.2(2) . . . . ? O3 C17 C20 C19 -174.8(2) . . . . ? N4 C17 C20 C19 4.6(2) . . . . ? C18 C19 C20 C17 -5.7(2) . . . . ? C3 C2 N1 C1 -0.1(3) . . . . ? C3 C2 N1 I1 165.80(15) . . . . ? C5 C1 N1 C2 1.1(3) . . . . ? C6 C1 N1 C2 179.85(16) . . . . ? C5 C1 N1 I1 -162.74(14) . . . . ? C6 C1 N1 I1 16.0(2) . . . . ? C8 C7 N2 C6 0.9(3) . . . . ? C8 C7 N2 I2 169.59(15) . . . . ? C10 C6 N2 C7 0.7(3) . . . . ? C1 C6 N2 C7 -179.55(16) . . . . ? C10 C6 N2 I2 -166.25(14) . . . . ? C1 C6 N2 I2 13.5(2) . . . . ? O2 C14 N3 C13 179.47(18) . . . . ? C15 C14 N3 C13 0.4(2) . . . . ? O2 C14 N3 I1 0.0(3) . . . . ? C15 C14 N3 I1 -179.02(12) . . . . ? O1 C13 N3 C14 -179.82(18) . . . . ? C16 C13 N3 C14 0.8(2) . . . . ? O1 C13 N3 I1 -0.4(3) . . . . ? C16 C13 N3 I1 -179.71(12) . . . . ? O4 C18 N4 C17 178.35(18) . . . . ? C19 C18 N4 C17 -2.4(2) . . . . ? O4 C18 N4 I2 -2.8(3) . . . . ? C19 C18 N4 I2 176.43(12) . . . . ? O3 C17 N4 C18 177.97(19) . . . . ? C20 C17 N4 C18 -1.4(2) . . . . ? O3 C17 N4 I2 -0.9(3) . . . . ? C20 C17 N4 I2 179.70(12) . . . . ?