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Information card for entry 7249398
Preview
| Coordinates | 7249398.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C32 H28 B2 Li2 N12 |
|---|---|
| Calculated formula | C32 H28 B2 Li2 N12 |
| Title of publication | Optimised syntheses and purifications of 3-aryl/heterocyclic dihydrobis- and hydrotris-(pyrazolyl)borate ligands as their alkali salts |
| Authors of publication | Thomas, Jarrod R.; Mifsud, Jonathan T.; Sulway, Scott A. |
| Journal of publication | RSC Advances |
| Year of publication | 2024 |
| Journal volume | 14 |
| Journal issue | 42 |
| Pages of publication | 30713 - 30718 |
| a | 10.5827 ± 0.0005 Å |
| b | 21.2856 ± 0.0011 Å |
| c | 14.616 ± 0.0006 Å |
| α | 90° |
| β | 104.567 ± 0.002° |
| γ | 90° |
| Cell volume | 3186.6 ± 0.3 Å3 |
| Cell temperature | 100 K |
| Ambient diffraction temperature | 100 K |
| Number of distinct elements | 5 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.087 |
| Residual factor for significantly intense reflections | 0.061 |
| Weighted residual factors for significantly intense reflections | 0.1429 |
| Weighted residual factors for all reflections included in the refinement | 0.1817 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.157 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 294917 (current) | 2024-09-27 | cif/ Adding structures of 7249393, 7249394, 7249395, 7249396, 7249397, 7249398 via cif-deposit CGI script. |
7249398.cif |
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Users of the data should acknowledge the original authors of the
structural data.