#------------------------------------------------------------------------------ #$Date: 2024-10-02 01:37:02 +0300 (Wed, 02 Oct 2024) $ #$Revision: 294971 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/94/7249414.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7249414 loop_ _publ_author_name 'Chen, Zhe-Hong' 'Zhang, Xiao-Yue' 'Li, Dahuan' 'Li, Xin-Xiong' 'Sun, Yan-Qiong' 'Sun, Cai' 'Zheng, Shou-Tian' _publ_section_title ; Organic-Inorganic Hybrid Co-Containing Polyoxotungstates as Oxygen Evolution Catalyst ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D4CE00873A _journal_year 2024 _chemical_formula_moiety 'C10 H11 Ge K2 N2 O42 W9.001 Zn2, C10 H18 N2 O7 Zn, C5 H4 N O, 0.5(H6 O3 Zn), 2(H2 O)' _chemical_formula_sum 'C25 H42.5 Ge K2 N5 O53.5 W9 Zn3.5' _chemical_formula_weight 3303.37 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _audit_creation_date 2024-02-24 _audit_creation_method ; Olex2 1.5 (compiled 2021.08.20 svn.r13c46975 for OlexSys, GUI svn.r6396) ; _audit_update_record ; 2024-05-14 deposited with the CCDC. 2024-10-01 downloaded from the CCDC. ; _cell_angle_alpha 67.382(4) _cell_angle_beta 76.551(3) _cell_angle_gamma 87.841(2) _cell_formula_units_Z 2 _cell_length_a 11.7109(3) _cell_length_b 15.5844(6) _cell_length_c 19.2261(8) _cell_measurement_reflns_used 19127 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 29.3940 _cell_measurement_theta_min 1.7880 _cell_volume 3145.0(2) _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'multiwire proportional' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0614 _diffrn_reflns_av_unetI/netI 0.0688 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 31183 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.027 _diffrn_reflns_theta_max 25.027 _diffrn_reflns_theta_min 1.791 _exptl_absorpt_coefficient_mu 18.413 _exptl_absorpt_correction_type none _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 3.488 _exptl_crystal_description plate _exptl_crystal_F_000 2993 _exptl_crystal_size_max 1.5 _exptl_crystal_size_mid 1 _exptl_crystal_size_min 0.2 _refine_diff_density_max 3.930 _refine_diff_density_min -3.152 _refine_diff_density_rms 0.491 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.070 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 930 _refine_ls_number_reflns 11072 _refine_ls_number_restraints 169 _refine_ls_restrained_S_all 1.073 _refine_ls_R_factor_all 0.0875 _refine_ls_R_factor_gt 0.0620 _refine_ls_shift/su_max 0.004 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1374P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1792 _refine_ls_wR_factor_ref 0.2039 _reflns_Friedel_coverage 0.000 _reflns_number_gt 8084 _reflns_number_total 11072 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4ce00873a2.cif _cod_data_source_block a_sq _cod_original_formula_sum 'C25 H42.50 Ge K2 N5 O53.50 W9 Zn3.50' _cod_database_code 7249414 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All O(H,H) groups 2. Uiso/Uaniso restraints and constraints W12: within 2A with sigma of 0.02 and sigma for terminal atoms of 0.04 within 2A Uanis(O52) \\sim Ueq, Uanis(O55) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.0025 Uanis(O31) \\sim Ueq, Uanis(O37) \\sim Ueq, Uanis(O2) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.0025 Uanis(O8) \\sim Ueq, Uanis(O35) \\sim Ueq, Uanis(O39) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.0025 Uanis(O18) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.0025 Uanis(C24) \\sim Ueq, Uanis(C14) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.0025 Uanis(O20) \\sim Ueq, Uanis(O40) \\sim Ueq: with sigma of 0.05 and sigma for terminal atoms of 0.025 Uanis(O20) \\sim Ueq: with sigma of 0.002 and sigma for terminal atoms of 0.001 Uanis(C22) \\sim Ueq, Uanis(C15) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.0025 Uanis(N3) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.0025 Uanis(W7) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.0005 Uanis(W7A) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.0005 Uanis(O43) \\sim Ueq, Uanis(O42) \\sim Ueq, Uanis(O21) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.0025 Uanis(O22) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.0025 Uanis(O13) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.005 Uanis(O3) \\sim Ueq: with sigma of 0.005 and sigma for terminal atoms of 0.0025 Uanis(C8) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.005 Uanis(C16) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002 Uanis(O21) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002 Uanis(O38) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(O54) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 3. Others 1*[Sof(W10)+Sof(W12)]+1*[Sof(W1)+Sof(W2)]=1 with esd of 0.001 Sof(W10)=Sof(W12)=FVAR(1) Sof(W1)=Sof(W2)=FVAR(2) Fixed Sof: W7(0.93) W7A(0.07) W8(0.63) W8A(0.37) O43(0.5) H43A(0.5) H43B(0.5) O41(0.5) H41A(0.5) H41B(0.5) O42(0.5) H42A(0.5) H42B(0.5) 4.a Riding coordinates: O53(H53A,H53B), O55(H55A,H55B) 4.b Rotating group: O52(H52A,H52B), O35(H35A,H35B), O37(H37A,H37B), O36(H36A,H36B), O39(H39A, H39B), O40(H40A,H40B), O41(H41A,H41B), O42(H42A,H42B), O54(H54A,H54B) 4.c Aromatic/amide H refined with riding coordinates: C2(H2), C5(H5), C10(H10), C1(H1), C9(H9), C12(H12), C15(H15), C14(H14), C20(H20), C19(H19), C18(H18), C17(H17), C8(H8), C4(H4), C7(H7), C25(H25), C24(H24), C22(H22), C21(H21) 4.d Fitted hexagon refined as free rotating group: C13(C12,C11,N3,C15,C14), C16(C20,C19,N4,C18,C17) 4.e X=CH2 refined with riding coordinates: O43(H43A,H43B) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL a_a.res in P-1 a_sq.res created by SHELXL-2018/3 at 16:28:38 on 24-Feb-2024 REM Old TITL A in P-1 REM SHELXT solution in P-1: R1 0.285, Rweak 0.005, Alpha 0.042 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C66 N26 O81 W18 CELL 0.71073 11.7109 15.5844 19.2261 67.382 76.551 87.841 ZERR 2 0.0003 0.0006 0.0008 0.004 0.003 0.002 LATT 1 SFAC C H Ge K N O W Zn UNIT 50 85 2 4 10 107 18 7 ISOR 0.005 0.0025 O52 O55 ISOR 0.005 0.0025 O31 O37 O2 ISOR 0.005 0.0025 O8 O35 O39 ISOR 0.005 0.0025 O18 ISOR 0.005 0.0025 C24 C14 ISOR 0.05 0.025 O20 O40 ISOR 0.002 0.001 O20 ISOR 0.005 0.0025 C22 C15 ISOR 0.005 0.0025 N3 ISOR 0.001 0.0005 W7 ISOR 0.001 0.0005 W7A ISOR 0.005 0.0025 O43 O42 O21 ISOR 0.005 0.0025 O22 ISOR 0.01 0.005 O13 ISOR 0.005 0.0025 O3 ISOR 0.01 0.005 C8 ISOR 0.001 0.002 C16 ISOR 0.001 0.002 O21 SIMU 0.02 0.04 2 W12 ISOR 0.01 0.02 O38 ISOR 0.01 0.02 O54 SUMP 1 0.001 1 2 1 3 L.S. 10 0 14 PLAN 30 CONF MORE -1 BOND $H ABIN fmap 2 acta SHEL 999 0.84 OMIT -1 1 1 OMIT 1 0 1 REM REM REM WGHT 0.137400 FVAR 0.06902 0.25519 0.74540 W6 7 0.602310 0.221117 0.674631 11.00000 0.02488 0.01830 = 0.02247 0.00172 -0.00516 -0.00126 PART 2 W1 7 0.791245 0.406689 0.577805 31.00000 0.01435 0.01816 = 0.01494 0.00087 -0.00411 -0.00089 PART 0 W5 7 0.298280 0.245615 0.778318 11.00000 0.02723 0.02398 = 0.01944 0.00166 -0.00279 -0.00332 PART 2 W2 7 0.704410 0.641901 0.571525 31.00000 0.02338 0.01817 = 0.01542 -0.00099 -0.00632 -0.00053 PART 1 W7 7 0.711155 0.320182 0.774547 10.93000 0.02512 0.02508 = 0.02008 0.00102 -0.00901 0.00049 PART 2 W7A 7 0.674105 0.330580 0.791726 10.07000 0.00631 0.00638 = 0.00688 -0.00204 -0.00108 0.00137 PART 0 W4 7 0.217967 0.460402 0.760802 11.00000 0.03611 0.02825 = 0.01825 -0.00005 0.00010 0.00435 PART 1 W8 7 0.626711 0.553803 0.767742 10.63000 0.03476 0.02202 = 0.01439 -0.00183 -0.00983 -0.00052 PART 0 W8A 7 0.601832 0.557439 0.768907 10.37000 0.06532 0.01945 = 0.04301 0.00450 -0.03095 -0.00950 W9 7 0.405663 0.350819 0.873122 11.00000 0.04655 0.02470 = 0.01514 0.00029 -0.00567 -0.00162 W3 7 0.426925 0.665428 0.659600 11.00000 0.04706 0.02235 = 0.02184 -0.00175 -0.00664 0.00150 GE1 3 0.501875 0.443309 0.662660 11.00000 0.02526 0.01649 = 0.01512 0.00090 -0.00644 0.00063 ZN3 8 0.751538 0.834801 0.773812 11.00000 0.03150 0.03216 = 0.02606 -0.00852 -0.01133 -0.00019 O5 6 0.301881 0.292761 0.667347 11.00000 0.02399 0.01613 = 0.01664 0.00146 -0.00575 -0.00051 O3 6 0.385499 0.651474 0.581698 11.00000 0.02681 0.01039 = 0.02148 -0.01010 -0.00184 0.00587 O27 6 0.553121 0.304099 0.839496 11.00000 0.04479 0.01424 = 0.01491 -0.00780 -0.01787 -0.00098 O24 6 0.679579 0.213097 0.758252 11.00000 0.03890 0.00840 = 0.02039 -0.00216 -0.01558 0.00374 O51 6 0.110812 0.389527 0.594798 11.00000 0.02454 0.04471 = 0.03937 0.02184 -0.01833 -0.00089 O23 6 0.335124 0.239413 0.870743 11.00000 0.04268 0.00876 = 0.01932 -0.00897 -0.00107 -0.00278 O16 6 0.455592 0.210727 0.745653 11.00000 0.02087 0.02086 = 0.01784 -0.00442 -0.00248 -0.00123 O4 6 0.220456 0.484043 0.663674 11.00000 0.02729 0.03628 = 0.01590 0.00936 -0.00473 0.00763 O32 6 0.549276 0.547957 0.666749 11.00000 0.03269 0.01397 = 0.01841 0.00171 -0.00171 -0.00309 O1 6 0.701771 0.445861 0.510045 11.00000 0.01610 0.03257 = 0.01175 -0.00149 -0.00586 -0.00092 O19 6 0.830653 0.361974 0.684358 11.00000 0.02013 0.03163 = 0.02728 0.00480 -0.01358 -0.00584 O14 6 0.178676 0.324094 0.787921 11.00000 0.03138 0.02313 = 0.02798 -0.01345 -0.00470 0.00420 O8 6 0.783553 0.528981 0.586672 11.00000 0.02912 0.02988 = 0.02566 -0.00202 -0.01158 -0.00475 O20 6 0.729199 0.626765 0.676860 11.00000 0.03547 0.03313 = 0.03322 -0.01234 -0.00957 0.00100 O18 6 0.753762 0.277510 0.606908 11.00000 0.02527 0.02489 = 0.02360 -0.00361 -0.00469 -0.00077 O7 6 0.930858 0.413483 0.522314 11.00000 0.03157 0.01743 = 0.02303 0.00732 -0.00493 -0.00481 O33 6 0.388843 0.390202 0.744602 11.00000 0.04268 0.01499 = 0.02183 -0.01055 -0.00706 0.00140 O21 6 0.509496 0.648735 0.746827 11.00000 0.02690 0.02564 = 0.02587 -0.01089 -0.00593 0.00117 O10 6 0.581304 0.720699 0.592635 11.00000 0.04429 0.02855 = 0.02747 0.00112 -0.01451 -0.01256 O22 6 0.262018 0.408723 0.866674 11.00000 0.04137 0.03852 = 0.02777 -0.00397 -0.00538 0.00579 O38 6 0.676192 0.891435 0.851915 11.00000 0.02438 0.01194 = 0.03015 -0.01309 -0.00405 -0.00378 O17 6 0.620014 0.106829 0.682720 11.00000 0.02721 0.01939 = 0.04023 0.00775 -0.00774 -0.00032 O6 6 0.530232 0.273908 0.594736 11.00000 0.02913 0.02115 = 0.01795 0.00187 -0.01007 0.00378 O12 6 0.315381 0.567133 0.737129 11.00000 0.05106 0.02485 = 0.02170 -0.00645 -0.00284 0.00802 O26 6 0.488472 0.468779 0.834612 11.00000 0.06031 0.03079 = 0.01725 0.00058 -0.00743 -0.01093 O13 6 0.077734 0.491435 0.795228 11.00000 0.05531 0.04493 = 0.02593 -0.02828 0.00593 0.00620 O15 6 0.220071 0.140874 0.813435 11.00000 0.02624 0.04867 = 0.01520 0.00090 -0.00185 0.00174 O25 6 0.701995 0.447924 0.766193 11.00000 0.03791 0.03870 = 0.02053 0.00919 -0.01230 -0.00368 O30 6 0.390974 0.313906 0.972143 11.00000 0.06601 0.02094 = 0.01796 -0.00362 -0.00143 -0.00249 O9 6 0.817995 0.723272 0.514276 11.00000 0.06317 0.01801 = 0.03154 -0.00785 -0.02224 -0.00274 O34 6 0.616870 0.369026 0.670715 11.00000 0.01363 0.03256 = 0.02374 0.01123 -0.00709 -0.00271 O29 6 0.676879 0.578063 0.834464 11.00000 0.07681 0.02404 = 0.02969 -0.00608 -0.02349 -0.00398 N1 5 0.730648 0.937993 0.879990 11.00000 0.03168 0.01619 = 0.01611 -0.00691 0.00029 -0.01453 O28 6 0.790282 0.276325 0.843057 11.00000 0.05330 0.03291 = 0.04101 0.01036 -0.03007 -0.01394 O11 6 0.355732 0.761352 0.663675 11.00000 0.04819 0.06177 = 0.02832 0.00829 0.00161 -0.00466 O47 6 0.383817 0.845478 0.847673 11.00000 0.04939 0.03830 = 0.06049 -0.01334 -0.00177 0.01338 O44 6 1.057821 1.234102 1.068879 11.00000 0.06648 0.04600 = 0.05486 -0.02254 -0.03171 -0.01333 O46 6 0.140175 0.992076 0.538596 11.00000 0.02407 0.06310 = 0.05317 0.01061 -0.00632 -0.00151 C2 1 0.793519 0.945666 0.986888 11.00000 0.01762 0.01844 = 0.02211 -0.01104 -0.00821 0.00463 AFIX 43 H2 2 0.797150 0.917541 1.038582 11.00000 -1.20000 AFIX 0 C5 1 0.779794 1.026598 0.835112 11.00000 0.03246 0.02220 = 0.03251 -0.01892 -0.01664 0.00971 AFIX 43 H5 2 0.774554 1.054264 0.783707 11.00000 -1.20000 AFIX 0 O45 6 0.932876 0.957181 0.266241 11.00000 0.05899 0.07448 = 0.05581 0.02673 0.01332 0.03017 N2 5 1.002078 1.189093 1.038985 11.00000 0.01818 0.03056 = 0.03162 -0.00544 -0.00431 0.00592 C10 1 0.973307 1.171267 0.928687 11.00000 0.02397 0.02384 = 0.01386 -0.00241 -0.01395 -0.00030 AFIX 43 H10 2 0.987584 1.193563 0.874923 11.00000 -1.20000 AFIX 0 C3 1 0.841912 1.036378 0.941572 11.00000 0.02325 0.01957 = 0.01887 -0.00689 0.00034 -0.00862 C1 1 0.740685 0.898779 0.954110 11.00000 0.01907 0.01632 = 0.01709 -0.00458 0.01046 -0.00575 AFIX 43 H1 2 0.710783 0.837908 0.984002 11.00000 -1.20000 AFIX 0 C9 1 1.020920 1.215574 0.960762 11.00000 0.02565 0.03005 = 0.03495 0.00100 -0.00811 0.00981 AFIX 43 H9 2 1.070362 1.268012 0.928751 11.00000 -1.20000 AFIX 0 N5 5 0.411116 0.889215 0.890456 11.00000 0.03339 0.06195 = 0.03056 -0.00204 0.00784 0.01428 AFIX 66 C13 1 0.592804 0.965608 0.379898 11.00000 0.05408 0.02570 = 0.03073 -0.00521 -0.02417 0.01379 C12 1 0.648151 0.882008 0.399660 11.00000 0.05433 0.00825 = 0.07554 -0.01729 -0.02060 0.00253 AFIX 43 H12 2 0.609049 0.828839 0.439852 11.00000 -1.20000 AFIX 65 C11 1 0.761940 0.877875 0.359349 11.00000 0.06024 0.02001 = 0.05408 -0.01482 -0.01415 -0.00181 N3 5 0.820383 0.957342 0.299277 11.00000 0.04640 0.04498 = 0.04582 -0.01391 -0.00614 0.01115 C15 1 0.765038 1.040943 0.279515 11.00000 0.07603 0.07196 = 0.07156 -0.02463 -0.01152 0.01323 AFIX 43 H15 2 0.804140 1.094111 0.239322 11.00000 -1.20000 AFIX 65 C14 1 0.651248 1.045077 0.319825 11.00000 0.06391 0.06298 = 0.06263 -0.02100 -0.01214 0.00870 AFIX 43 H14 2 0.614218 1.101011 0.306602 11.00000 -1.20000 AFIX 66 C16 1 0.473270 0.972265 0.424217 11.00000 0.02640 0.02646 = 0.02629 -0.00989 -0.00658 0.00161 C20 1 0.431493 1.059318 0.416624 11.00000 0.03367 0.03825 = 0.02717 -0.00272 -0.01647 0.00396 AFIX 43 H20 2 0.479112 1.112854 0.384842 11.00000 -1.20000 AFIX 65 C19 1 0.318543 1.066354 0.456532 11.00000 0.02945 0.03020 = 0.03559 -0.00431 -0.01495 0.00079 AFIX 43 H19 2 0.290591 1.124598 0.451452 11.00000 -1.20000 AFIX 65 N4 5 0.247369 0.986337 0.504034 11.00000 0.03238 0.03469 = 0.04490 -0.01788 -0.01158 -0.00391 C18 1 0.289145 0.899284 0.511628 11.00000 0.04156 0.03004 = 0.03710 -0.00548 -0.00379 -0.00394 AFIX 43 H18 2 0.241525 0.845748 0.543410 11.00000 -1.20000 AFIX 65 C17 1 0.402095 0.892246 0.471720 11.00000 0.05133 0.02523 = 0.04172 -0.01528 -0.02388 0.01160 AFIX 43 H17 2 0.430046 0.834002 0.476801 11.00000 -1.20000 AFIX 0 C6 1 0.898105 1.087428 0.975511 11.00000 0.01603 0.01249 = 0.02462 -0.00063 -0.01244 -0.00053 C8 1 0.936692 1.110361 1.084123 11.00000 0.04095 0.04746 = 0.01855 -0.01347 -0.00401 -0.00064 AFIX 43 H8 2 0.927781 1.088663 1.137517 11.00000 -1.20000 AFIX 0 C4 1 0.835326 1.073764 0.864578 11.00000 0.02585 0.02499 = 0.01865 0.00981 -0.01161 -0.01948 AFIX 43 H4 2 0.870042 1.132722 0.832596 11.00000 -1.20000 AFIX 0 C7 1 0.882861 1.060963 1.054860 11.00000 0.03222 0.01968 = 0.01266 0.00055 -0.00395 -0.00779 AFIX 43 H7 2 0.834848 1.008382 1.088634 11.00000 -1.20000 AFIX 0 C25 1 0.443697 0.983413 0.860104 11.00000 0.04292 0.04915 = 0.03628 0.02269 0.01124 0.00786 AFIX 43 H25 2 0.440681 1.018204 0.809021 11.00000 -1.20000 AFIX 0 C24 1 0.478497 1.026640 0.898762 11.00000 0.03965 0.03987 = 0.03992 -0.01279 -0.00411 0.00667 AFIX 43 H24 2 0.500981 1.089789 0.874354 11.00000 -1.20000 AFIX 0 C22 1 0.443344 0.881790 1.010947 11.00000 0.03972 0.03847 = 0.03731 -0.01004 -0.01041 0.00734 AFIX 43 H22 2 0.440539 0.847640 1.063088 11.00000 -1.20000 AFIX 0 C23 1 0.482192 0.977663 0.977980 11.00000 0.02882 0.04193 = 0.03490 0.00998 0.00662 0.02626 C21 1 0.410695 0.839118 0.969380 11.00000 0.02998 0.04030 = 0.07379 0.02494 0.00692 0.00921 AFIX 43 H21 2 0.387585 0.776052 0.992660 11.00000 -1.20000 AFIX 0 O49 6 1.129650 0.681719 0.598387 11.00000 0.06257 0.03011 = 0.06421 0.00128 -0.00904 0.01294 O48 6 0.967936 0.870405 0.562019 11.00000 0.03990 0.05980 = 0.06230 -0.00702 -0.00668 0.00063 O50 6 -0.001255 0.224089 0.674042 11.00000 0.05488 0.05385 = 0.06303 -0.01301 -0.00406 0.02098 O52 6 0.975265 1.054230 0.628844 11.00000 0.09818 0.09875 = 0.09931 -0.03887 -0.02336 0.00399 AFIX 7 H52A 2 1.014899 1.045666 0.677706 11.00000 -1.50000 H52B 2 0.893820 1.011545 0.665316 11.00000 -1.50000 AFIX 0 ZN2 8 0.458821 0.602054 0.497743 11.00000 0.02160 0.01905 = 0.01519 0.00191 -0.00382 0.00061 ZN1 8 0.283484 0.424995 0.584964 11.00000 0.02064 0.02402 = 0.01746 0.00053 -0.00314 0.00253 O2 6 0.636690 0.627523 0.502093 11.00000 0.02300 0.01474 = 0.02010 -0.00247 -0.00661 0.00266 O31 6 0.456918 0.464947 0.577410 11.00000 0.01569 0.01976 = 0.02569 -0.00590 -0.00718 0.00066 O35 6 0.769099 0.961567 0.678327 11.00000 0.03668 0.03842 = 0.03534 -0.01432 -0.00916 0.00248 AFIX 7 H35A 2 0.717808 0.999861 0.688408 11.00000 -1.50000 H35B 2 0.750422 0.953676 0.639799 11.00000 -1.50000 AFIX 0 O37 6 0.582260 0.807513 0.764164 11.00000 0.03497 0.03686 = 0.03600 -0.01225 -0.00955 0.00223 AFIX 7 H37A 2 0.529462 0.836992 0.785788 11.00000 -1.50000 H37B 2 0.558387 0.748734 0.791156 11.00000 -1.50000 AFIX 0 O36 6 0.743295 0.707038 0.875093 11.00000 0.05145 0.03337 = 0.02746 -0.02467 -0.00248 0.00232 AFIX 7 H36A 2 0.714157 0.658082 0.869800 11.00000 -1.50000 H36B 2 0.691650 0.708695 0.917256 11.00000 -1.50000 AFIX 0 O39 6 0.923036 0.855190 0.782049 11.00000 0.04062 0.04100 = 0.03980 -0.01488 -0.01105 0.00009 AFIX 7 H39A 2 0.967468 0.898079 0.737045 11.00000 -1.50000 H39B 2 0.926675 0.883370 0.815726 11.00000 -1.50000 AFIX 0 O40 6 0.827388 0.766093 0.700990 11.00000 0.03287 0.04068 = 0.04031 -0.01366 -0.01159 -0.00064 AFIX 7 H40A 2 0.867409 0.805614 0.657716 11.00000 -1.50000 H40B 2 0.773274 0.743707 0.688331 11.00000 -1.50000 AFIX 0 O43 6 0.047422 0.566258 1.063448 10.50000 0.02892 0.02705 = 0.02669 -0.01288 -0.00456 0.00255 AFIX 93 H43A 2 -0.005055 0.603527 1.081529 10.50000 -1.50000 H43B 2 0.121445 0.559093 1.074194 10.50000 -1.50000 AFIX 0 O41 6 -0.068831 0.378481 1.099969 10.50000 0.09327 0.00354 = 0.01924 -0.00268 -0.00772 -0.00284 AFIX 7 H41A 2 -0.012862 0.315322 1.121539 10.50000 -1.50000 H41B 2 -0.143244 0.329240 1.103312 10.50000 -1.50000 AFIX 0 ZN4 8 0.000000 0.500000 1.000000 10.50000 0.09665 0.05516 = 0.05639 -0.01921 0.01766 0.00636 O42 6 -0.158076 0.556336 1.009813 10.50000 0.04680 0.04653 = 0.04542 -0.01856 -0.01018 0.00433 AFIX 7 H42A 2 -0.176369 0.604873 1.035117 10.50000 -1.50000 H42B 2 -0.229807 0.512165 1.045017 10.50000 -1.50000 AFIX 0 K2 4 1.042790 0.773648 0.469569 11.00000 0.05433 0.09531 = 0.06399 -0.03352 -0.01445 0.02140 K1 4 0.969393 0.522297 0.661895 11.00000 0.06812 0.07290 = 0.08707 -0.01362 -0.02998 -0.00960 O53 6 1.097242 0.746057 0.719299 11.00000 0.11628 0.07701 = 0.13439 -0.05682 -0.02271 0.02815 AFIX 3 H53A 2 1.101853 0.785477 0.673419 11.00000 -1.50000 H53B 2 1.093542 0.778767 0.746239 11.00000 -1.50000 AFIX 0 O54 6 -0.092510 0.601889 0.805895 11.00000 0.11107 0.10260 = 0.14775 -0.03644 -0.04598 0.02252 AFIX 7 H54A 2 -0.174611 0.591014 0.833287 11.00000 -1.50000 H54B 2 -0.083071 0.669255 0.786939 11.00000 -1.50000 AFIX 0 O55 6 -0.318896 0.354792 1.127510 11.00000 0.16013 0.16069 = 0.15969 -0.06238 -0.03773 0.00842 AFIX 3 H55A 2 -0.335326 0.297842 1.138040 11.00000 -1.50000 H55B 2 -0.385226 0.379052 1.130450 11.00000 -1.50000 AFIX 0 PART 1 W10 7 0.783803 0.415440 0.589077 21.00000 0.04547 0.02572 = 0.03269 0.00484 -0.02193 -0.00284 W12 7 0.683454 0.646699 0.576155 21.00000 0.05245 0.01937 = 0.04444 0.01496 -0.02273 -0.01429 HKLF 4 REM a_a.res in P-1 REM wR2 = 0.2039, GooF = S = 1.070, Restrained GooF = 1.073 for all data REM R1 = 0.0620 for 8084 Fo > 4sig(Fo) and 0.0875 for all 11072 data REM 930 parameters refined using 169 restraints END WGHT 0.1372 0.0000 REM Highest difference peak 3.930, deepest hole -3.152, 1-sigma level 0.491 Q1 1 0.0156 0.4892 1.0974 11.00000 0.05 3.93 Q2 1 0.3409 0.3748 0.8950 11.00000 0.05 3.41 Q3 1 0.3642 0.6971 0.6832 11.00000 0.05 3.07 Q4 1 0.2014 0.4227 0.7306 11.00000 0.05 2.76 Q5 1 0.4130 0.4513 0.5380 11.00000 0.05 2.63 Q6 1 0.2256 0.6351 1.0536 11.00000 0.05 2.57 Q7 1 0.6156 0.6573 0.4409 11.00000 0.05 2.55 Q8 1 0.2754 0.3805 0.8448 11.00000 0.05 2.50 Q9 1 0.5492 0.2494 0.6998 11.00000 0.05 2.45 Q10 1 0.3167 0.2189 0.7506 11.00000 0.05 2.40 Q11 1 0.7982 0.3671 0.5531 11.00000 0.05 2.38 Q12 1 0.1497 0.4465 0.6975 11.00000 0.05 2.32 Q13 1 0.6664 0.3021 0.7278 11.00000 0.05 2.32 Q14 1 0.6688 0.1616 0.6704 11.00000 0.05 2.30 Q15 1 -0.2354 0.2731 1.1664 11.00000 0.05 2.26 Q16 1 0.6849 0.4228 0.4410 11.00000 0.05 2.25 Q17 1 0.4005 0.6469 0.6175 11.00000 0.05 2.20 Q18 1 0.7375 0.4467 0.6003 11.00000 0.05 2.20 Q19 1 0.5388 0.2051 0.6213 11.00000 0.05 2.09 Q20 1 0.7197 0.4645 0.6530 11.00000 0.05 2.06 Q21 1 0.5822 0.2855 0.7088 11.00000 0.05 2.05 Q22 1 0.3642 0.3349 0.8318 11.00000 0.05 2.04 Q23 1 0.4531 0.6514 0.7593 11.00000 0.05 2.00 Q24 1 1.0000 1.0000 0.5000 10.50000 0.05 1.99 Q25 1 0.6443 0.2392 0.7067 11.00000 0.05 1.98 Q26 1 0.7359 0.4091 0.4945 11.00000 0.05 1.94 Q27 1 0.7214 0.3902 0.5091 11.00000 0.05 1.93 Q28 1 0.5632 0.5944 0.7880 11.00000 0.05 1.91 Q29 1 -0.1950 0.4991 1.0427 11.00000 0.05 1.90 Q30 1 0.7202 0.3776 0.5312 11.00000 0.05 1.89 ; _shelx_res_checksum 51637 _shelx_hkl_file ; 0 0 -2 1120.85 31.28 0 0 -3 11.50 1.08 0 0 4 78.28 8.41 0 0 -4 115.25 4.52 0 0 5 225.43 14.64 0 0 -5 282.72 9.47 0 0 6 158.16 12.11 0 0 -6 195.56 7.46 0 0 7 96.31 9.30 0 0 -7 128.17 5.82 0 0 8 29.90 5.99 0 0 -8 48.29 3.50 0 0 9 1875.59 74.34 0 0 -9 2606.06 69.00 0 0 10 75.53 8.76 0 0 -10 115.09 6.10 0 0 11 2225.07 81.72 0 0 -11 2803.09 76.05 0 0 12 501.15 24.45 0 0 -12 602.23 20.15 0 0 13 11.18 4.58 0 0 -13 13.16 2.90 0 0 14 83.81 9.14 0 0 -14 102.53 6.66 0 0 15 19.44 6.16 0 0 -15 32.02 4.19 0 0 16 25.75 6.51 0 0 -16 28.69 4.26 0 0 17 94.17 10.44 0 0 -17 119.11 7.67 0 0 18 118.62 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3.13 0 3 11 62.22 4.32 0 -3 -11 60.81 4.24 0 3 12 13.56 1.43 0 3 12 9.95 1.38 0 -3 -12 12.02 2.59 0 3 12 13.75 2.53 0 -3 -13 208.87 9.51 0 3 13 214.64 9.77 0 3 14 5.99 5.73 0 -3 -14 -0.22 2.31 0 3 15 20.90 7.48 0 -3 -15 25.72 3.61 0 3 16 7.24 6.59 0 -3 -16 9.23 3.07 0 3 17 102.60 12.00 0 -3 -17 119.12 7.35 0 3 18 22.76 7.85 0 -3 -18 31.09 4.37 0 3 19 78.99 11.22 0 -3 -19 91.68 6.81 0 3 20 37.57 8.73 0 3 20 56.49 13.17 0 3 21 4.28 10.68 0 3 21 -6.23 7.68 0 3 22 -4.45 7.41 0 3 23 -3.09 7.44 0 3 24 -4.35 7.33 0 -4 19 -3.42 12.60 0 -4 18 -12.43 14.27 0 4 -18 7.63 4.89 0 -4 17 1.60 12.04 0 4 -17 14.61 5.08 0 -4 16 24.36 4.13 0 4 -16 35.41 6.16 0 -4 15 2.21 10.74 0 -4 15 3.59 3.16 0 4 -15 6.18 4.37 0 -4 14 573.74 35.35 0 -4 14 552.47 20.21 0 -4 13 1142.64 37.07 0 4 -13 1396.93 42.37 0 -4 12 45.68 4.15 0 4 -12 32.45 1.90 0 4 -12 33.07 2.01 0 4 -12 51.38 6.03 0 4 -12 51.36 5.53 0 -4 11 294.44 11.46 0 4 -11 286.91 10.01 0 4 -11 350.32 15.30 0 4 -11 361.34 14.29 0 -4 10 3.68 2.25 0 4 -10 3.74 1.51 0 4 -10 5.12 2.62 0 -4 9 36.02 2.94 0 -4 9 33.55 2.47 0 -4 9 32.62 2.49 0 4 -9 38.35 4.15 0 -4 8 35.24 2.74 0 -4 8 35.99 2.61 0 -4 8 35.84 2.61 0 4 -8 38.50 3.96 0 -4 7 41.44 2.64 0 -4 7 42.70 3.03 0 -4 7 47.21 3.07 0 4 -7 45.10 4.06 0 -4 6 9.64 1.27 0 -4 6 17.01 2.21 0 -4 6 13.36 2.49 0 4 -6 13.84 2.38 0 -4 5 22.05 2.94 0 -4 5 15.78 2.53 0 4 -5 15.74 2.29 0 4 -4 636.21 21.40 0 -4 4 649.86 21.77 0 -4 3 1332.07 39.11 0 4 -3 1292.13 38.85 0 4 -2 3524.91 98.58 0 -4 2 3510.02 98.66 0 4 -1 196.98 7.76 0 -4 1 197.93 7.76 0 -4 0 48.16 2.31 0 4 0 49.70 2.68 0 -4 0 47.62 2.96 0 4 1 14.23 2.21 0 4 2 64.25 5.47 0 4 3 185.78 11.13 0 4 4 217.39 13.16 0 4 4 197.98 10.70 0 4 4 202.86 8.34 0 -4 -5 8.63 3.52 0 4 5 8.00 2.05 0 -4 -6 326.56 12.89 0 -4 -6 351.01 10.94 0 4 6 314.97 12.24 0 -4 -7 895.46 28.64 0 4 7 942.65 28.88 0 -4 -8 5.40 1.43 0 4 8 7.26 1.75 0 -4 -9 197.13 7.20 0 4 9 203.79 7.65 0 -4 -10 30.72 2.77 0 4 10 28.36 2.90 0 -4 -11 365.67 14.63 0 -4 -11 390.36 14.76 0 -4 -11 495.83 15.33 0 4 11 486.77 15.80 0 -4 -12 141.57 6.36 0 -4 -12 144.10 6.98 0 -4 -12 128.13 6.20 0 4 12 151.95 7.42 0 -4 -13 24.97 2.61 0 -4 -13 25.90 2.59 0 -4 -13 28.06 3.31 0 4 13 25.66 3.35 0 4 14 36.56 2.59 0 4 14 35.04 2.61 0 -4 -14 43.71 3.94 0 4 14 42.05 4.28 0 4 15 0.74 0.99 0 4 15 0.30 0.99 0 4 15 0.67 2.42 0 -4 -15 1.02 2.34 0 4 16 98.40 11.93 0 -4 -16 84.85 5.99 0 4 17 66.37 10.59 0 -4 -17 42.28 4.76 0 4 18 133.56 13.32 0 -4 -18 115.85 7.37 0 4 19 21.06 8.13 0 4 19 36.30 11.61 0 -4 -19 17.53 3.96 0 4 20 18.92 10.29 0 4 20 20.08 7.98 0 -4 -20 14.94 4.04 0 4 21 36.43 12.30 0 4 21 26.70 8.58 0 4 22 32.95 12.97 0 4 22 21.83 8.73 0 4 23 9.29 7.57 0 4 24 7.82 7.55 0 -5 18 -3.14 12.17 0 5 -18 9.27 5.38 0 -5 17 6.81 10.27 0 5 -17 0.52 5.10 0 -5 16 57.89 14.25 0 5 -16 66.76 8.04 0 -5 15 60.18 4.65 0 -5 15 55.23 13.86 0 -5 14 10.25 2.72 0 -5 14 -0.65 9.97 0 5 -14 7.57 4.69 0 -5 13 341.82 23.84 0 5 -13 339.81 15.95 0 -5 12 53.11 11.11 0 -5 12 36.94 3.31 0 5 -12 39.26 2.85 0 5 -12 40.69 3.03 0 5 -12 51.13 5.55 0 5 -12 44.23 6.36 0 -5 11 94.82 4.67 0 5 -11 97.78 4.86 0 5 -11 105.19 7.48 0 -5 10 42.05 2.85 0 -5 10 44.83 3.13 0 -5 10 42.70 3.07 0 -5 9 20.08 1.94 0 -5 9 20.41 2.42 0 -5 9 19.69 2.44 0 5 -9 27.59 3.72 0 -5 8 4.13 1.23 0 -5 8 4.89 1.95 0 -5 8 3.76 1.79 0 5 -8 6.23 2.59 0 -5 7 3.54 0.89 0 -5 7 6.44 1.97 0 -5 7 3.55 2.05 0 -5 7 5.51 2.38 0 5 -7 5.79 2.34 0 5 -6 134.68 7.42 0 -5 6 147.95 8.15 0 5 -5 168.53 8.41 0 -5 5 181.81 9.01 0 -5 4 37.49 3.61 0 5 -4 36.17 3.52 0 5 -3 24.04 2.79 0 -5 3 27.45 2.94 0 -5 2 1424.34 42.24 0 5 -2 1416.06 42.13 0 5 -1 1371.77 37.42 0 -5 1 1383.27 37.44 0 -5 0 137.73 5.08 0 -5 0 146.01 6.48 0 5 1 19.93 2.42 0 5 2 132.00 7.83 0 5 3 14.96 3.48 0 5 4 65.16 6.70 0 5 4 27.26 5.08 0 5 5 5.41 3.68 0 5 5 2.38 1.75 0 5 5 0.74 2.29 0 5 6 13.25 4.80 0 5 6 5.97 2.27 0 -5 -7 182.22 7.03 0 -5 -7 166.57 9.95 0 -5 -8 248.67 10.94 0 -5 -8 258.40 8.93 0 5 8 257.56 10.62 0 -5 -9 136.89 8.41 0 -5 -9 111.90 6.07 0 5 9 129.38 6.55 0 -5 -10 372.09 13.36 0 -5 -10 327.64 14.57 0 -5 -11 900.08 23.63 0 5 11 1016.58 25.03 0 5 12 230.84 15.50 0 -5 -12 75.86 5.58 0 -5 -12 159.39 6.83 0 5 12 173.33 7.44 0 5 13 8.04 6.31 0 -5 -13 -3.41 2.77 0 5 13 4.80 2.33 0 -5 -13 1.49 2.08 0 5 14 6.05 5.77 0 -5 -14 1.00 2.05 0 -5 -14 1.34 1.90 0 5 14 1.15 2.33 0 -5 -14 2.79 2.14 0 5 15 57.05 10.77 0 -5 -15 55.88 3.93 0 -5 -15 56.34 3.98 0 -5 -15 58.99 4.74 0 5 15 56.68 5.08 0 5 16 13.60 7.00 0 5 16 5.88 1.99 0 5 16 6.49 1.95 0 5 16 4.21 3.09 0 -5 -16 6.62 2.90 0 5 17 54.00 2.75 0 5 17 38.80 2.51 0 5 17 84.01 11.09 0 -5 -17 70.30 5.53 0 5 17 65.61 5.75 0 5 18 147.85 14.35 0 -5 -18 129.66 7.96 0 5 19 68.85 12.63 0 5 19 83.99 11.39 0 -5 -19 59.66 5.84 0 5 20 70.88 13.32 0 5 20 53.29 10.44 0 -5 -20 68.77 6.12 0 5 21 33.79 9.21 0 5 21 15.98 10.05 0 5 22 92.50 15.61 0 5 22 95.59 13.30 0 5 23 110.04 13.77 0 5 24 70.54 11.89 0 -6 18 3.61 10.90 0 6 -18 9.01 6.03 0 -6 17 -1.41 10.94 0 6 -17 0.28 5.58 0 -6 16 -1.34 10.05 0 6 -16 8.69 5.51 0 -6 15 46.00 12.15 0 6 -15 54.63 7.83 0 -6 14 24.13 2.70 0 -6 14 37.72 10.87 0 6 -14 41.98 6.70 0 -6 13 5.47 8.11 0 -6 13 2.16 1.88 0 6 -13 -0.26 4.67 0 -6 12 -1.02 8.15 0 -6 12 1.10 1.69 0 6 -12 0.78 1.94 0 6 -12 -0.48 4.06 0 6 -11 -0.07 1.75 0 -6 11 -4.65 7.54 0 -6 11 0.93 1.38 0 -6 11 0.60 1.88 0 6 -11 -0.52 3.29 0 -6 10 120.35 12.58 0 -6 10 93.39 4.86 0 -6 10 97.95 4.84 0 6 -10 124.91 7.70 0 -6 9 51.15 3.76 0 -6 9 44.86 3.59 0 -6 8 46.11 3.85 0 -6 8 48.55 3.89 0 6 -8 56.53 5.10 0 -6 7 4.37 2.34 0 -6 7 1.12 2.51 0 -6 7 1.90 2.38 0 6 -7 0.41 2.29 0 -6 6 227.10 9.92 0 6 -6 196.57 9.71 0 -6 6 205.18 10.38 0 6 -5 69.54 5.19 0 -6 5 69.54 5.47 0 -6 4 278.94 12.28 0 6 -4 296.19 12.13 0 6 -3 1.95 1.69 0 -6 3 -0.26 4.97 0 -6 3 1.41 1.64 0 6 -2 96.54 5.66 0 -6 2 91.90 5.53 0 -6 1 61.00 3.55 0 6 -1 64.68 2.70 0 -6 1 68.74 4.52 0 -6 0 9.55 1.12 0 6 0 11.65 1.67 0 -6 0 11.39 1.92 0 -6 -1 198.95 8.39 0 6 1 183.45 8.21 0 6 2 0.41 1.84 0 6 3 3.59 2.66 0 6 4 -0.37 1.28 0 6 4 4.88 3.14 0 6 5 134.87 9.79 0 6 5 103.35 8.48 0 6 6 8.30 4.04 0 6 6 5.88 2.14 0 6 6 7.48 2.96 0 6 7 9.62 4.56 0 6 7 1.73 2.16 0 6 8 2.07 4.97 0 -6 -8 -2.12 3.57 0 6 8 -0.84 1.90 0 -6 -9 123.85 8.99 0 -6 -9 146.25 6.35 0 6 9 140.82 7.74 0 6 10 69.65 10.74 0 -6 -10 48.03 3.14 0 -6 -10 70.30 6.31 0 -6 -10 43.97 4.52 0 6 10 55.12 4.52 0 -6 -11 223.49 10.77 0 -6 -11 197.68 7.50 0 6 11 204.14 9.56 0 -6 -12 160.41 8.00 0 -6 -12 146.50 8.47 0 6 13 28.43 7.57 0 -6 -13 2.92 2.92 0 -6 -13 18.50 2.94 0 -6 -13 -2.59 3.50 0 6 13 23.89 3.46 0 6 14 25.73 7.41 0 -6 -14 -0.89 2.55 0 -6 -14 18.16 2.94 0 -6 -14 -0.26 2.81 0 6 14 17.04 3.33 0 -6 -15 2.64 2.29 0 -6 -15 -1.17 2.34 0 -6 -15 0.22 2.27 0 6 15 1.56 2.57 0 -6 -16 44.34 4.15 0 -6 -16 39.47 4.13 0 6 16 54.13 5.43 0 6 17 -1.94 2.57 0 6 17 -2.47 2.42 0 6 17 3.50 6.23 0 -6 -17 2.36 2.33 0 -6 -17 1.27 2.77 0 6 17 -1.27 3.24 0 6 18 10.20 6.79 0 6 18 4.04 1.92 0 6 18 3.09 2.14 0 6 18 7.31 3.27 0 -6 -18 6.94 3.13 0 6 19 24.54 9.68 0 6 19 31.45 8.86 0 -6 -19 19.97 4.06 0 6 19 17.58 4.19 0 6 20 5.53 8.89 0 6 20 11.91 7.41 0 -6 -20 10.68 3.57 0 6 21 17.53 9.32 0 6 21 30.98 9.30 0 6 22 83.68 12.69 0 6 22 71.27 13.94 0 6 23 106.14 13.83 0 6 24 5.32 7.93 0 -7 17 3.81 9.99 0 7 -17 3.68 5.94 0 -7 16 46.59 12.36 0 7 -16 55.39 8.62 0 -7 15 -1.73 8.95 0 7 -15 -1.73 5.19 0 -7 14 23.11 9.73 0 7 -14 15.54 5.77 0 -7 13 80.53 12.37 0 7 -13 94.60 9.21 0 -7 12 5.47 7.24 0 7 -11 -0.28 2.14 0 -7 11 0.82 6.10 0 -7 11 1.40 2.27 0 -7 11 1.25 2.31 0 -7 10 167.06 13.43 0 -7 10 131.81 6.61 0 -7 10 137.10 6.72 0 7 -10 165.08 9.43 0 -7 9 360.89 19.18 0 -7 9 297.63 11.78 0 -7 9 295.22 11.83 0 7 -9 368.65 14.83 0 7 -8 14.10 3.42 0 -7 8 14.53 5.53 0 -7 8 13.56 3.11 0 -7 8 10.33 2.94 0 -7 8 16.04 3.94 0 7 -7 3.00 2.51 0 -7 7 4.37 4.04 0 -7 7 5.04 2.72 0 -7 7 3.20 2.57 0 -7 7 3.22 3.01 0 -7 6 102.92 8.32 0 -7 6 107.53 6.92 0 7 -6 97.17 6.61 0 -7 6 93.02 6.90 0 -7 5 148.39 9.53 0 7 -5 166.09 8.75 0 -7 5 163.11 9.10 0 -7 4 121.04 7.72 0 -7 4 133.45 7.80 0 7 -4 126.87 7.37 0 7 -3 13.86 2.85 0 -7 3 11.44 2.64 0 -7 3 11.82 4.97 0 -7 3 14.29 2.77 0 -7 2 257.45 10.09 0 -7 2 293.48 11.54 0 7 -1 25.14 1.71 0 -7 1 26.03 2.29 0 -7 1 29.90 3.26 0 -7 0 70.80 3.16 0 7 0 79.06 3.89 0 -7 0 72.16 4.89 0 -7 -1 73.02 4.93 0 7 1 73.05 4.73 0 7 2 154.11 8.28 0 7 3 191.64 10.38 0 7 4 197.48 11.48 0 7 5 282.46 10.85 0 7 5 185.94 13.25 0 7 6 274.83 14.16 0 7 6 274.42 11.80 0 7 7 262.59 15.80 0 7 7 253.38 12.60 0 7 7 254.46 10.23 0 7 8 133.01 10.81 0 7 8 95.77 7.00 0 7 9 114.96 11.09 0 -7 -9 100.52 8.13 0 7 10 92.09 9.49 0 -7 -10 80.20 7.03 0 -7 -10 46.74 6.94 0 7 10 32.79 4.06 0 7 11 21.99 5.95 0 -7 -11 6.87 1.97 0 -7 -11 21.04 4.34 0 -7 -11 -0.43 3.74 0 7 11 8.39 2.59 0 -7 -12 8.63 3.55 0 -7 -12 19.54 2.46 0 -7 -12 23.74 4.24 0 7 12 9.82 3.03 0 -7 -13 37.01 3.05 0 -7 -13 39.99 4.78 0 7 13 43.06 4.71 0 -7 -14 64.94 5.66 0 -7 -14 68.72 5.75 0 -7 -14 66.87 5.86 0 -7 -14 74.82 4.48 0 7 15 483.29 23.05 0 -7 -15 182.93 10.35 0 -7 -15 152.02 9.92 0 -7 -15 299.93 12.00 0 7 15 375.35 13.38 0 7 16 144.10 12.91 0 -7 -16 89.17 5.95 0 7 16 101.75 6.74 0 7 17 132.24 13.10 0 -7 -17 106.21 6.81 0 -7 -17 50.20 5.10 0 -7 -17 43.08 4.95 0 7 17 116.59 7.63 0 7 18 -1.88 2.42 0 -7 -18 0.84 2.40 0 -7 -18 0.15 2.85 0 7 18 -2.08 3.29 0 7 19 11.07 2.62 0 7 19 20.97 9.21 0 7 19 27.13 8.45 0 -7 -19 8.30 3.70 0 7 19 9.86 3.83 0 7 20 6.59 7.87 0 7 20 8.56 6.98 0 -7 -20 7.98 3.70 0 7 21 9.38 8.78 0 7 21 13.94 8.71 0 7 22 12.97 9.14 0 7 22 24.82 9.02 0 7 23 32.88 10.83 0 7 23 43.11 10.89 0 -8 17 62.07 13.34 0 8 -17 71.51 9.90 0 -8 16 184.90 18.94 0 8 -16 178.46 13.70 0 -8 15 66.54 12.62 0 8 -15 83.58 9.60 0 -8 14 90.80 12.86 0 8 -14 103.35 9.94 0 -8 13 31.15 9.51 0 8 -13 31.43 6.57 0 -8 12 337.56 20.90 0 -8 11 206.73 9.19 0 -8 11 225.24 9.34 0 -8 10 156.17 7.67 0 -8 10 153.55 7.67 0 -8 9 93.76 9.43 0 -8 9 81.67 5.66 0 -8 9 84.48 5.69 0 -8 8 275.59 15.80 0 -8 8 284.34 12.49 0 -8 8 294.22 12.45 0 -8 8 333.63 15.18 0 8 -8 326.41 14.14 0 -8 7 91.73 8.45 0 -8 7 100.76 6.92 0 -8 7 102.28 6.94 0 -8 7 101.15 7.91 0 8 -7 102.60 7.22 0 8 -6 16.95 3.50 0 -8 6 14.03 4.26 0 -8 6 17.86 4.15 0 -8 6 13.10 3.48 0 8 -5 111.68 7.18 0 -8 5 87.25 7.00 0 -8 5 107.31 7.42 0 8 -4 3.44 2.46 0 -8 4 1.49 2.59 0 -8 4 0.24 4.09 0 -8 4 3.29 2.44 0 -8 3 823.25 30.26 0 -8 3 732.52 24.67 0 -8 2 1016.21 31.65 0 -8 2 930.83 39.28 0 -8 1 46.95 3.09 0 8 -1 49.31 2.55 0 -8 1 42.70 7.96 0 -8 1 55.34 4.58 0 8 0 41.03 2.88 0 -8 0 37.03 2.23 0 -8 0 34.89 3.68 0 8 1 106.42 5.92 0 -8 -1 108.61 6.51 0 -8 -2 43.43 4.11 0 8 2 22.85 3.52 0 8 3 107.36 7.61 0 8 4 223.51 12.26 0 8 5 1.19 1.25 0 8 5 22.14 4.56 0 8 6 58.20 4.43 0 8 6 42.00 6.18 0 8 7 162.28 8.69 0 8 7 158.55 8.08 0 8 7 167.19 10.27 0 8 8 86.65 9.58 0 8 8 100.01 7.44 0 8 8 80.38 5.10 0 8 9 675.21 27.80 0 8 9 615.92 22.61 0 8 10 17.45 5.64 0 -8 -10 16.73 4.63 0 8 10 5.56 2.87 0 8 11 68.62 8.71 0 -8 -11 63.00 6.53 0 8 12 106.64 10.44 0 -8 -12 113.26 7.70 0 8 13 44.30 8.02 0 -8 -13 2.55 4.34 0 -8 -13 46.03 5.32 0 -8 -13 17.06 2.83 0 8 13 19.07 3.94 0 -8 -14 11.39 3.98 0 -8 -14 -1.60 4.02 0 -8 -14 4.21 2.21 0 8 14 4.76 2.96 0 -8 -15 265.84 10.22 0 -8 -15 282.22 12.84 0 -8 -15 312.53 13.29 0 8 15 293.22 13.10 0 8 16 8.21 6.35 0 -8 -16 1.66 2.75 0 -8 -16 -4.28 3.67 0 -8 -16 -0.32 2.66 0 -8 -16 1.47 2.33 0 8 16 2.49 2.68 0 8 17 53.96 9.62 0 -8 -17 28.19 5.02 0 -8 -17 18.40 3.85 0 -8 -17 22.11 4.04 0 8 17 49.89 5.40 0 8 18 45.44 9.36 0 -8 -18 28.73 5.04 0 8 18 41.72 5.19 0 8 19 1.86 2.75 0 8 19 2.23 7.61 0 -8 -19 0.37 3.89 0 8 19 5.88 3.61 0 8 20 -1.00 2.36 0 8 20 -5.56 7.63 0 -8 -20 -5.82 4.32 0 8 21 11.39 7.82 0 8 21 6.23 7.78 0 8 22 18.33 8.86 0 8 22 0.50 8.45 0 8 23 4.67 8.91 0 8 23 1.94 7.87 0 -9 16 56.60 11.76 0 9 -16 52.71 9.12 0 -9 15 100.20 13.53 0 9 -15 100.07 10.68 0 -9 14 45.96 10.23 0 9 -14 51.58 8.26 0 -9 13 69.76 10.62 0 9 -13 64.20 8.63 0 -9 12 124.86 12.52 0 -9 11 448.53 22.38 0 -9 11 405.44 15.24 0 -9 10 53.89 8.22 0 -9 10 45.46 4.58 0 -9 10 47.77 4.86 0 -9 9 93.48 9.21 0 -9 9 75.84 5.94 0 -9 9 80.55 6.23 0 -9 8 115.89 9.60 0 -9 8 121.38 7.80 0 -9 8 128.48 7.72 0 -9 8 135.33 9.47 0 9 -7 55.77 5.79 0 -9 7 50.93 6.38 0 -9 7 52.77 5.51 0 -9 7 56.55 6.10 0 -9 7 58.43 6.31 0 9 -6 -0.67 2.77 0 -9 6 -1.84 3.83 0 -9 6 0.73 3.24 0 -9 6 -1.54 4.39 0 -9 6 -1.36 3.16 0 9 -5 25.73 4.08 0 -9 5 26.11 4.24 0 -9 5 34.55 5.58 0 -9 5 32.04 4.67 0 -9 4 26.66 3.70 0 -9 4 34.24 5.99 0 -9 4 27.46 4.15 0 -9 3 600.09 24.43 0 -9 3 545.83 19.93 0 -9 2 1631.59 49.64 0 -9 2 1734.56 59.15 0 -9 1 16.75 2.16 0 9 -1 16.88 1.69 0 -9 1 9.42 6.03 0 -9 1 16.45 3.26 0 -9 0 862.53 25.51 0 9 0 873.75 26.33 0 -9 0 981.47 38.24 0 -9 0 962.23 29.83 0 -9 -1 0.58 1.86 0 -9 -1 0.39 5.47 0 9 1 1.88 1.95 0 -9 -2 14.85 2.90 0 9 2 10.77 2.92 0 9 3 10.01 3.27 0 9 4 43.67 5.62 0 9 5 97.19 8.15 0 9 6 7.35 1.94 0 9 6 6.14 4.11 0 9 7 381.40 14.27 0 9 7 359.18 17.16 0 9 8 78.45 6.29 0 9 8 104.61 9.45 0 9 8 86.54 5.82 0 9 8 94.45 7.57 0 -9 -8 69.29 8.13 0 9 9 2301.88 70.58 0 9 9 2002.49 64.51 0 -9 -9 1963.42 67.34 0 9 9 2324.62 65.83 0 9 10 468.16 22.57 0 9 10 410.80 18.64 0 9 10 484.33 18.92 0 -9 -10 451.47 20.17 0 9 11 27.56 6.46 0 -9 -11 28.95 5.40 0 9 11 20.90 3.98 0 9 12 9.21 5.32 0 -9 -12 6.90 3.68 0 9 12 -0.37 2.59 0 9 13 5.49 5.56 0 -9 -13 4.17 3.44 0 9 13 -1.71 3.14 0 9 14 2.27 5.88 0 -9 -14 8.80 4.04 0 9 14 -2.53 3.13 0 -9 -15 63.86 6.51 0 -9 -15 79.32 6.77 0 9 16 0.33 5.82 0 -9 -16 -1.02 2.53 0 -9 -16 9.14 3.65 0 -9 -16 -7.16 5.41 0 -9 -16 10.55 3.67 0 9 16 2.57 2.75 0 9 17 1.10 5.82 0 -9 -17 5.06 3.29 0 -9 -17 2.33 3.18 0 9 17 1.79 2.83 0 9 18 270.70 17.47 0 9 18 254.92 16.62 0 -9 -18 176.31 9.97 0 9 18 191.32 10.87 0 9 19 106.99 12.15 0 9 19 72.59 10.96 0 -9 -19 21.40 6.70 0 -9 -19 32.79 5.41 0 9 19 62.39 6.62 0 9 20 36.01 4.88 0 9 20 105.11 12.30 0 9 20 89.63 11.83 0 -9 -20 26.05 6.90 0 9 21 54.71 10.46 0 9 21 50.22 10.35 0 9 22 39.08 10.31 0 9 22 45.92 10.44 0 9 23 7.59 8.50 0 9 23 2.42 8.95 0 -10 16 6.05 8.26 0 -10 15 6.46 8.28 0 10 -15 0.32 6.08 0 -10 14 -0.39 7.50 0 10 -14 1.27 5.94 0 -10 13 7.00 6.48 0 -10 12 46.85 8.37 0 -10 11 49.74 8.52 0 -10 11 41.77 4.76 0 -10 10 1.12 5.38 0 -10 10 2.38 3.41 0 -10 9 62.95 7.85 0 -10 9 56.85 5.62 0 -10 9 72.94 6.29 0 -10 8 17.73 5.19 0 -10 8 22.65 4.69 0 -10 8 28.49 4.58 0 -10 8 27.24 5.36 0 -10 7 7.50 4.13 0 -10 7 17.51 4.73 0 -10 7 14.09 4.26 0 -10 7 14.50 4.45 0 -10 6 47.86 5.47 0 -10 6 58.89 6.92 0 -10 6 60.21 6.51 0 -10 6 61.16 6.42 0 -10 5 94.28 6.83 0 -10 5 120.72 9.25 0 -10 5 118.36 8.39 0 -10 4 18.96 3.50 0 -10 4 26.98 4.32 0 -10 3 1.14 2.21 0 -10 3 -0.87 4.82 0 -10 3 0.54 2.61 0 -10 2 553.70 18.81 0 -10 2 610.12 26.79 0 -10 2 632.65 22.40 0 -10 1 132.35 5.77 0 10 -1 124.13 4.89 0 -10 1 173.59 13.55 0 -10 1 156.13 8.69 0 10 0 507.14 15.54 0 -10 0 537.20 19.30 0 10 1 37.07 3.54 0 -10 -1 38.80 8.28 0 -10 -1 33.51 4.32 0 -10 -2 234.60 16.13 0 -10 -2 220.35 10.94 0 -10 -3 52.53 5.36 0 10 3 19.24 3.89 0 10 4 47.21 5.73 0 10 5 4.19 3.55 0 -10 -5 4.08 5.08 0 10 6 161.47 10.35 0 -10 -6 142.94 11.41 0 10 7 104.70 8.75 0 10 7 54.33 4.19 0 10 7 54.18 7.22 0 -10 -7 86.04 8.82 0 10 8 98.27 8.80 0 10 8 76.20 5.55 0 10 8 64.16 6.83 0 10 8 58.67 5.47 0 -10 -8 88.96 8.89 0 10 9 1136.15 38.44 0 10 9 1207.81 43.58 0 -10 -9 1169.10 42.37 0 10 9 1205.37 39.86 0 10 9 1250.51 36.92 0 10 10 773.62 30.40 0 -10 -10 746.19 28.32 0 10 10 707.53 25.73 0 10 11 282.39 16.47 0 10 11 232.76 12.93 0 10 11 279.84 13.34 0 -10 -11 287.43 14.72 0 10 12 8.80 5.56 0 10 12 3.80 3.80 0 -10 -12 10.44 4.34 0 10 12 6.66 3.26 0 10 13 15.72 5.08 0 10 13 23.17 6.75 0 -10 -13 22.89 5.23 0 10 13 11.26 3.94 0 10 14 20.28 6.61 0 10 14 10.42 5.08 0 -10 -14 18.46 4.60 0 10 14 7.41 3.70 0 10 15 45.57 7.63 0 10 15 56.40 9.29 0 -10 -15 56.34 6.46 0 10 15 40.06 5.47 0 10 16 0.93 5.25 0 10 16 17.27 6.74 0 -10 -16 10.14 3.93 0 -10 -16 13.86 4.26 0 10 16 2.38 2.96 0 10 17 80.79 9.49 0 -10 -17 82.58 7.20 0 -10 -17 95.07 7.50 0 10 18 168.14 13.34 0 -10 -18 185.85 10.35 0 10 19 275.52 18.03 0 10 19 256.48 16.82 0 -10 -19 229.86 12.06 0 10 20 190.78 16.02 0 10 20 268.32 18.44 0 10 21 174.15 15.91 0 10 21 226.06 17.60 0 10 22 15.54 8.97 0 10 22 10.38 8.48 0 10 23 2.72 8.56 0 -11 14 9.90 7.63 0 -11 13 41.48 8.71 0 -11 12 13.08 6.51 0 -11 11 123.05 11.31 0 -11 10 43.26 7.44 0 -11 10 37.66 5.28 0 -11 9 2.36 4.43 0 -11 9 1.30 3.93 0 -11 9 1.71 4.41 0 -11 8 88.83 8.26 0 -11 8 102.43 8.13 0 -11 8 115.44 9.43 0 -11 7 -0.37 3.70 0 -11 7 1.64 4.37 0 -11 7 -1.15 4.15 0 -11 6 93.69 7.41 0 -11 6 116.26 9.55 0 -11 6 115.11 8.82 0 -11 5 8.60 3.54 0 -11 5 8.62 5.28 0 -11 5 8.62 3.70 0 -11 4 2.83 2.75 0 -11 4 5.41 3.22 0 -11 3 12.82 3.05 0 -11 3 20.23 4.02 0 -11 2 107.10 5.75 0 -11 2 113.13 7.93 0 -11 1 -0.19 1.82 0 11 -1 1.41 1.23 0 -11 1 2.57 2.79 0 11 0 12.58 2.12 0 -11 0 12.04 3.24 0 11 1 117.39 6.12 0 -11 -1 114.60 8.06 0 11 2 162.63 8.73 0 -11 -2 173.01 10.09 0 -11 -3 147.05 9.01 0 11 3 75.04 6.59 0 -11 -4 31.26 4.58 0 11 4 4.09 3.27 0 11 5 1.90 3.46 0 11 6 66.84 7.13 0 11 6 21.01 5.99 0 11 7 95.23 8.50 0 11 7 34.89 6.51 0 11 8 50.54 4.11 0 11 8 44.90 6.20 0 11 8 45.98 5.12 0 11 9 5.27 4.11 0 11 9 2.05 2.72 0 11 9 0.84 2.53 0 11 9 1.21 2.98 0 11 10 86.38 8.88 0 11 10 68.51 6.07 0 11 10 77.16 6.83 0 11 10 73.00 5.10 0 11 11 192.07 10.98 0 11 11 229.65 14.36 0 11 11 209.69 11.18 0 11 12 0.80 3.42 0 11 12 5.25 4.95 0 11 12 1.77 2.96 0 11 13 128.82 9.84 0 11 13 162.81 12.80 0 11 13 161.07 9.95 0 11 14 0.24 4.09 0 11 14 7.35 5.64 0 11 14 -0.20 3.35 0 11 15 72.48 9.84 0 11 15 59.58 7.54 0 11 15 53.91 6.68 0 11 16 22.37 7.70 0 11 16 20.36 5.97 0 -11 -16 28.19 5.32 0 11 16 18.01 4.37 0 11 17 24.99 7.50 0 11 17 15.31 6.03 0 -11 -17 26.68 5.15 0 11 17 12.30 4.17 0 11 18 19.85 6.62 0 -11 -18 18.27 5.01 0 11 19 49.35 8.73 0 -11 -19 59.69 6.90 0 11 20 8.65 7.16 0 11 21 44.75 9.82 0 11 21 60.01 10.61 0 11 22 15.70 8.86 0 11 22 2.40 7.46 0 11 23 4.19 7.26 0 -12 11 85.95 9.69 0 -12 10 162.83 12.28 0 -12 10 190.76 10.46 0 -12 9 0.91 4.73 0 -12 9 -0.35 4.50 0 -12 9 2.31 4.30 0 -12 8 32.12 5.92 0 -12 8 31.39 5.97 0 -12 8 38.11 6.49 0 -12 7 0.19 3.98 0 -12 7 2.46 4.93 0 -12 7 0.73 4.21 0 -12 6 24.90 4.76 0 -12 6 25.31 6.46 0 -12 6 25.40 5.51 0 -12 5 469.73 21.34 0 -12 5 463.77 19.59 0 -12 4 136.56 7.83 0 -12 4 130.33 11.70 0 -12 3 111.94 6.46 0 -12 3 117.64 8.62 0 -12 2 23.48 3.26 0 -12 2 24.88 4.50 0 -12 1 128.28 5.51 0 -12 1 155.67 9.60 0 12 0 27.45 2.75 0 -12 0 28.10 4.67 0 12 1 186.32 8.41 0 -12 -1 192.49 11.05 0 12 2 118.92 7.16 0 -12 -2 117.06 8.71 0 -12 -3 13.60 3.83 0 12 3 8.71 3.14 0 -12 -4 47.04 5.77 0 12 4 -1.28 3.55 0 12 5 37.68 5.90 0 12 6 61.26 7.11 0 12 7 10.48 4.32 0 12 8 -0.39 1.17 0 12 8 4.08 3.52 0 12 9 90.60 5.58 0 12 9 79.32 6.18 0 12 10 55.62 5.32 0 12 10 54.91 4.95 0 12 11 54.26 7.70 0 12 11 38.65 5.28 0 12 12 -1.43 3.87 0 12 12 1.92 4.50 0 12 13 115.29 10.53 0 12 13 77.18 7.46 0 12 14 24.82 6.48 0 12 14 14.55 4.67 0 12 15 3.52 6.31 0 12 15 2.36 4.58 0 12 16 17.47 6.94 0 12 16 6.92 4.97 0 -12 -16 16.78 4.80 0 12 17 19.85 7.03 0 12 17 8.24 5.49 0 -12 -17 13.58 4.80 0 12 18 131.39 12.62 0 -12 -18 128.78 9.47 0 12 19 13.64 6.94 0 12 19 5.95 5.99 0 -12 -19 10.18 4.95 0 12 20 1.67 6.33 0 12 21 -3.52 6.98 0 12 22 25.34 8.32 0 12 23 28.23 8.76 0 -13 9 63.15 7.33 0 -13 9 74.34 8.35 0 -13 8 1.40 4.43 0 -13 8 -2.38 5.12 0 -13 8 -3.16 4.73 0 -13 7 1.62 4.17 0 -13 7 2.38 4.99 0 -13 7 4.91 4.67 0 -13 6 20.52 4.74 0 -13 6 18.77 6.20 0 -13 6 28.39 5.90 0 -13 5 388.45 15.87 0 -13 5 386.05 19.98 0 -13 5 420.49 18.98 0 -13 4 1084.07 34.89 0 -13 4 1037.06 41.12 0 -13 3 4.35 3.09 0 -13 3 -5.21 6.87 0 -13 3 3.18 3.72 0 -13 2 238.90 9.23 0 -13 2 267.43 13.81 0 -13 1 6.79 3.68 0 13 0 -1.60 1.84 0 -13 0 1.80 3.00 0 13 1 55.02 4.37 0 -13 -1 53.98 6.33 0 13 2 85.67 6.05 0 -13 -2 85.02 7.74 0 -13 -3 8.08 3.89 0 13 3 11.46 3.41 0 -13 -4 32.25 5.51 0 13 4 3.16 3.22 0 -13 -5 455.79 19.30 0 13 5 271.26 15.65 0 13 6 52.14 7.15 0 13 7 908.64 34.44 0 13 8 31.19 5.97 0 13 9 -1.58 1.32 0 13 9 0.15 3.35 0 13 10 32.77 3.93 0 13 10 33.34 4.32 0 13 11 10.59 3.83 0 13 11 12.41 3.09 0 13 12 17.84 5.60 0 13 12 9.66 4.22 0 13 13 33.27 6.64 0 13 13 20.04 4.73 0 13 14 35.34 7.35 0 13 14 14.83 4.93 0 13 15 14.09 6.31 0 13 15 -1.49 4.80 0 13 16 299.47 17.79 0 -13 -16 296.81 14.61 0 13 17 18.76 7.09 0 13 17 -1.73 5.14 0 -13 -17 13.90 5.34 0 13 18 8.76 6.68 0 13 18 -2.66 5.47 0 -13 -18 6.77 4.74 0 13 19 1.71 5.47 0 13 19 -1.58 6.33 0 -13 -19 6.49 4.80 0 13 20 21.79 8.91 0 13 20 4.26 6.10 0 -13 -20 14.05 5.79 0 13 21 9.40 7.00 0 13 22 12.71 7.48 0 13 23 15.57 7.67 0 -14 9 8.28 5.34 0 -14 8 -4.73 6.48 0 -14 8 -0.82 5.02 0 -14 7 24.23 6.46 0 -14 7 26.05 6.21 0 -14 6 1.97 5.51 0 -14 6 2.36 4.32 0 -14 5 -1.54 6.57 0 -14 5 6.12 4.69 0 -14 4 468.09 24.32 0 -14 4 571.17 23.26 0 -14 3 33.44 4.04 0 -14 3 26.03 7.26 0 -14 3 41.62 6.31 0 -14 2 233.80 16.41 0 -14 2 229.99 13.40 0 -14 1 18.01 4.88 0 -14 0 4.89 3.96 0 14 1 1.49 2.36 0 -14 -1 5.81 3.93 0 -14 -2 17.51 4.63 0 14 2 21.75 4.06 0 -14 -3 0.80 3.65 0 14 3 5.19 3.26 0 -14 -4 7.54 4.41 0 14 4 0.61 3.44 0 -14 -5 229.82 13.32 0 14 5 94.54 8.78 0 -14 -6 20.99 5.36 0 14 6 16.77 5.08 0 14 7 948.18 35.71 0 14 8 274.70 15.76 0 14 9 7.85 4.76 0 14 9 -3.78 4.06 0 14 10 6.10 4.76 0 14 10 -5.60 3.70 0 14 11 -1.69 2.87 0 14 11 6.79 5.30 0 14 11 2.96 3.05 0 14 12 30.85 6.66 0 14 12 23.80 4.19 0 14 13 22.18 6.12 0 14 13 9.47 4.24 0 14 14 52.27 8.41 0 14 14 42.74 6.03 0 14 15 67.47 9.60 0 14 15 62.60 7.11 0 14 16 311.79 18.50 0 14 16 274.03 14.70 0 -14 -16 331.03 16.02 0 14 17 135.18 12.71 0 -14 -17 136.84 10.10 0 14 18 22.46 6.16 0 14 18 40.06 8.69 0 -14 -18 37.62 6.55 0 14 19 20.15 6.21 0 14 19 27.02 8.11 0 -14 -19 26.55 6.27 0 14 20 14.31 8.08 0 14 20 22.96 6.81 0 -14 -20 22.46 6.18 0 14 21 33.98 7.91 0 -15 8 -1.77 5.79 0 -15 7 10.62 6.29 0 -15 7 6.85 5.32 0 -15 6 62.00 8.88 0 -15 6 53.55 7.70 0 -15 5 43.50 8.19 0 -15 5 58.30 7.50 0 -15 4 8.73 6.25 0 -15 4 31.76 6.20 0 -15 3 26.83 7.83 0 -15 3 47.06 6.85 0 -15 2 -5.75 7.42 0 -15 2 -0.26 4.34 0 -15 1 5.51 6.40 0 -15 1 4.17 4.37 0 -15 0 2.40 4.15 0 -15 -1 12.71 4.61 0 -15 -2 0.86 3.87 0 15 3 29.05 5.01 0 -15 -3 27.17 5.77 0 15 4 10.05 4.04 0 -15 -4 23.89 5.92 0 15 5 3.81 3.89 0 -15 -5 44.45 7.07 0 -15 -6 51.75 7.50 0 15 6 37.68 6.29 0 -15 -7 -3.39 5.19 0 15 7 3.41 4.47 0 15 8 101.02 9.95 0 15 9 13.32 5.58 0 15 9 -1.66 4.60 0 15 10 4.97 5.17 0 15 11 7.31 5.68 0 15 11 4.39 3.46 0 15 12 15.41 6.44 0 15 12 8.41 3.13 0 15 13 6.87 5.55 0 15 14 54.33 8.62 0 15 15 57.59 9.01 0 -15 -15 59.93 7.61 0 15 16 8.52 6.75 0 -15 -16 15.11 5.66 0 15 17 63.19 9.90 0 -15 -17 65.33 8.00 0 15 18 4.17 6.88 0 -15 -18 7.83 5.45 0 15 19 44.43 9.45 0 -15 -19 45.61 7.29 0 -15 -20 29.20 6.81 0 -16 7 31.89 7.24 0 -16 6 7.55 5.55 0 -16 6 16.71 6.08 0 -16 5 0.33 5.64 0 -16 5 0.87 5.12 0 -16 4 119.33 12.45 0 -16 4 200.92 13.01 0 -16 3 -3.05 6.64 0 -16 3 0.86 4.91 0 -16 2 15.80 7.48 0 -16 2 20.49 6.03 0 -16 1 64.53 10.59 0 -16 1 57.29 7.74 0 -16 0 74.17 10.94 0 -16 0 50.41 7.42 0 -16 -1 47.21 9.06 0 -16 -1 33.62 6.55 0 -16 -2 28.97 6.40 0 -16 -3 32.38 6.62 0 -16 -4 18.61 5.81 0 16 5 18.55 5.02 0 -16 -5 197.95 13.32 0 -16 -6 3.52 4.93 0 16 6 -5.55 4.99 0 -16 -7 82.93 9.79 0 16 7 100.78 9.66 0 -16 -8 12.63 5.32 0 16 8 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25 8.65 8.48 -5 -3 16 3.20 9.92 -5 -3 15 2.36 8.75 -5 -3 15 -0.19 4.19 -5 -3 14 22.87 9.92 -5 -3 14 30.61 5.49 -5 -3 13 -5.47 8.45 -5 -3 13 0.17 3.91 -5 -3 12 32.71 9.30 -5 -3 12 36.15 5.30 5 3 -12 30.93 4.08 5 3 -11 17.38 3.52 -5 -3 11 11.98 6.87 5 3 -11 20.84 6.62 -5 -3 11 10.81 4.09 5 3 -10 2.23 2.21 5 3 -10 5.47 2.74 5 3 -10 5.60 2.81 -5 -3 10 1.88 5.17 -5 -3 10 5.81 3.72 5 3 -10 10.51 4.28 5 3 -9 67.12 4.88 -5 -3 9 73.56 8.97 5 3 -9 66.45 4.99 5 3 -9 50.87 10.94 5 3 -9 73.70 5.01 5 3 -9 79.27 6.21 -5 -3 9 66.86 6.33 5 3 -8 52.19 4.41 -5 -3 8 63.02 8.02 5 3 -8 47.19 4.28 5 3 -8 53.12 4.30 -5 -3 8 53.59 5.36 5 3 -8 44.10 4.84 5 3 -7 32.97 3.89 5 3 -7 36.51 3.87 5 3 -7 24.32 7.11 5 3 -7 40.55 3.81 -5 -3 7 37.03 4.89 5 3 -7 34.85 3.93 -5 -3 7 32.84 6.23 -5 -3 6 157.88 11.20 5 3 -6 145.47 7.85 5 3 -6 187.43 12.19 5 3 -6 135.95 7.42 -5 -3 6 139.87 8.54 5 3 -6 168.10 11.44 5 3 -6 131.70 7.33 5 3 -6 143.65 7.18 5 3 -5 313.33 12.78 -5 -3 5 317.76 15.97 5 3 -5 284.90 12.02 5 3 -5 294.11 12.36 5 3 -5 310.02 12.11 5 3 -5 287.28 13.77 5 3 -4 2.81 2.40 5 3 -4 4.86 3.42 5 3 -4 2.53 2.21 -5 -3 4 3.20 3.13 5 3 -4 10.20 3.16 5 3 -4 4.80 2.64 5 3 -3 51.99 4.60 -5 -3 3 54.11 5.77 5 3 -3 49.85 4.39 5 3 -3 59.38 5.92 5 3 -3 50.72 4.86 -5 -3 2 54.22 4.71 5 3 -2 60.92 4.89 -5 -3 2 58.48 5.64 5 3 -2 58.76 4.82 5 3 -2 65.94 5.92 5 3 -2 72.40 5.04 5 3 -2 48.57 4.56 5 3 -1 18.46 3.00 -5 -3 1 19.71 3.59 -5 -3 1 20.90 3.14 5 3 -1 18.07 3.59 5 3 -1 18.63 3.24 5 3 -1 10.76 6.10 5 3 -1 21.85 2.94 5 3 -1 17.64 2.81 -5 -3 0 127.37 7.11 5 3 0 123.68 6.90 5 3 0 117.06 7.72 5 3 0 116.95 6.85 -5 -3 0 81.76 10.40 5 3 0 124.91 6.42 5 3 0 62.97 9.94 5 3 0 105.37 6.31 -5 -3 0 123.98 7.29 5 3 1 95.66 6.88 5 3 1 94.23 6.07 5 3 1 64.62 8.86 -5 -3 -1 125.95 8.97 -5 -3 -1 105.58 6.29 5 3 1 92.37 5.64 5 3 1 99.03 5.58 5 3 2 202.30 9.53 5 3 2 191.66 10.35 -5 -3 -2 219.79 9.60 5 3 2 205.98 9.02 5 3 2 203.64 9.12 -5 -3 -3 4.89 2.16 5 3 3 3.24 2.08 5 3 3 4.71 1.90 5 3 3 5.36 3.29 -5 -3 -3 5.90 2.23 5 3 3 7.03 2.05 -5 -3 -3 5.66 1.90 -5 -3 -4 555.52 19.52 -5 -3 -4 520.36 18.83 5 3 4 529.55 18.57 5 3 4 545.12 18.01 -5 -3 -4 547.30 18.31 -5 -3 -5 35.95 3.96 -5 -3 -5 40.97 5.43 -5 -3 -5 40.64 3.35 5 3 5 33.68 3.68 5 3 6 314.13 13.16 -5 -3 -6 353.99 13.83 -5 -3 -6 370.23 15.31 5 3 6 326.02 13.25 -5 -3 -6 324.25 12.17 5 3 7 52.66 4.41 -5 -3 -7 52.36 4.52 -5 -3 -7 56.44 5.34 5 3 7 50.93 4.52 -5 -3 -7 52.14 3.65 -5 -3 -8 45.25 4.28 5 3 8 43.37 4.00 -5 -3 -8 49.07 4.88 5 3 8 43.67 4.37 -5 -3 -8 37.40 3.13 -5 -3 -8 37.96 4.06 5 3 9 160.60 8.22 -5 -3 -9 173.33 8.60 -5 -3 -9 158.37 7.29 -5 -3 -9 164.81 8.99 -5 -3 -10 95.01 6.12 5 3 10 90.69 5.97 -5 -3 -10 96.14 6.88 5 3 11 35.32 3.78 5 3 11 32.84 3.74 5 3 11 33.38 3.63 -5 -3 -11 34.05 4.58 5 3 12 1.56 2.31 5 3 12 -0.39 2.38 5 3 12 0.45 2.46 -5 -3 -12 0.71 2.70 5 3 12 -2.10 3.14 5 3 13 558.76 19.76 5 3 13 558.07 19.46 5 3 13 566.30 19.00 -5 -3 -13 551.52 21.81 5 3 14 4.26 2.64 5 3 14 2.59 2.42 5 3 14 2.62 2.47 -5 -3 -14 2.49 3.14 5 3 15 346.02 13.97 5 3 15 371.24 13.71 5 3 15 373.71 13.32 -5 -3 -15 350.88 16.39 5 3 16 11.67 2.98 5 3 16 14.66 2.96 5 3 16 15.82 3.05 -5 -3 -16 10.77 4.21 5 3 17 0.54 2.23 5 3 17 2.57 2.36 -5 -3 -17 -1.28 3.83 5 3 18 -1.30 2.36 5 3 18 -1.51 2.49 -5 -3 -18 -0.22 3.94 -5 -3 -19 15.89 5.30 -5 -3 -20 34.29 6.35 -5 -3 -21 47.47 7.07 5 3 22 3.05 12.28 -5 -3 -22 54.13 7.33 5 3 23 2.55 12.91 -5 -3 -23 1.71 5.32 5 3 24 237.36 20.86 -5 -3 -24 250.42 14.64 5 3 25 13.49 8.93 -5 -4 16 10.53 9.88 -5 -4 15 7.42 9.15 -5 -4 14 36.73 10.72 -5 -4 14 36.86 5.62 -5 -4 13 70.48 11.42 -5 -4 13 66.11 6.55 -5 -4 12 133.10 8.67 -5 -4 12 150.96 14.38 5 4 -11 7.96 4.65 -5 -4 11 12.02 6.96 -5 -4 11 10.94 4.17 5 4 -10 16.11 3.20 5 4 -10 23.32 4.15 -5 -4 10 16.80 6.42 -5 -4 10 11.98 3.93 5 4 -10 19.78 5.81 5 4 -9 -0.22 2.51 5 4 -9 0.99 2.64 5 4 -9 0.37 2.61 -5 -4 9 -0.67 5.30 5 4 -9 4.06 3.41 -5 -4 9 0.30 3.14 -5 -4 8 148.93 11.61 5 4 -8 147.17 7.80 5 4 -8 158.65 7.61 5 4 -8 143.33 7.72 5 4 -8 136.35 8.04 5 4 -7 19.95 3.50 5 4 -7 25.45 3.39 5 4 -7 26.31 3.37 5 4 -7 18.03 3.41 -5 -4 7 16.26 5.14 5 4 -6 12.75 3.24 5 4 -6 10.53 2.70 5 4 -6 15.03 2.94 5 4 -6 2.79 6.77 5 4 -6 16.36 5.97 5 4 -6 12.99 2.92 -5 -4 6 18.14 4.71 5 4 -5 24.34 3.67 5 4 -5 25.31 3.26 5 4 -5 29.20 6.10 -5 -4 5 29.05 5.08 5 4 -5 24.52 3.44 5 4 -5 19.02 6.35 5 4 -5 29.44 3.42 -5 -4 4 166.46 10.27 5 4 -4 153.29 8.26 5 4 -4 178.82 11.31 5 4 -4 150.18 7.42 5 4 -4 171.63 12.11 5 4 -4 144.56 7.78 5 4 -4 153.59 7.55 5 4 -4 133.38 8.47 5 4 -3 117.73 6.94 -5 -4 3 103.40 7.95 5 4 -3 117.10 8.63 5 4 -3 102.40 6.18 5 4 -3 107.10 6.44 5 4 -3 107.92 6.25 5 4 -3 97.32 6.77 -5 -4 3 102.17 7.67 5 4 -2 268.58 11.78 -5 -4 2 261.69 13.06 5 4 -2 263.80 11.26 5 4 -2 301.79 13.97 5 4 -2 257.82 11.46 5 4 -2 268.56 11.15 5 4 -2 246.36 11.76 5 4 -1 30.55 3.74 -5 -4 1 31.00 4.34 5 4 -1 30.16 3.68 5 4 -1 31.67 4.48 5 4 -1 23.11 8.41 5 4 -1 24.77 3.52 5 4 -1 23.85 3.44 5 4 -1 43.26 4.76 5 4 -1 28.28 3.54 5 4 0 57.61 5.64 5 4 0 54.67 4.61 5 4 0 55.43 4.65 5 4 0 71.02 5.68 5 4 0 53.72 4.69 5 4 0 59.58 10.49 5 4 0 49.51 4.43 5 4 0 51.00 4.47 5 4 1 183.75 9.86 5 4 1 168.40 8.69 5 4 1 162.72 14.94 5 4 1 207.03 9.71 5 4 1 175.02 8.84 -5 -4 -1 175.93 9.19 5 4 1 175.75 8.62 5 4 2 17.73 3.05 5 4 2 20.51 3.68 -5 -4 -2 24.21 5.08 5 4 2 12.88 5.51 5 4 2 20.65 3.22 5 4 2 24.73 3.33 5 4 2 25.12 3.13 -5 -4 -2 21.77 3.22 5 4 3 181.29 9.10 5 4 3 193.20 9.47 -5 -4 -3 209.41 9.45 5 4 3 202.37 9.08 5 4 3 213.24 9.60 5 4 4 27.15 3.42 5 4 4 33.21 3.29 -5 -4 -4 34.00 6.94 -5 -4 -4 32.77 3.89 5 4 4 33.27 3.87 -5 -4 -4 35.24 3.54 5 4 4 34.54 3.70 -5 -4 -5 267.70 14.63 5 4 5 253.34 11.28 -5 -4 -5 251.18 10.57 -5 -4 -6 4.08 1.67 -5 -4 -6 4.00 3.27 5 4 6 4.04 2.27 5 4 7 108.74 6.75 5 4 7 126.77 6.94 5 4 7 120.22 7.11 -5 -4 -7 123.52 6.42 5 4 7 128.26 7.57 5 4 8 0.13 1.95 -5 -4 -8 -0.39 1.58 5 4 8 -3.14 2.55 -5 -4 -8 1.82 2.57 5 4 8 -2.12 2.51 -5 -4 -8 1.34 1.95 5 4 8 0.60 2.23 5 4 9 90.19 6.05 -5 -4 -9 104.82 6.03 -5 -4 -9 113.99 7.42 5 4 9 102.36 6.48 5 4 9 96.48 6.12 -5 -4 -9 106.16 6.77 5 4 10 60.96 4.97 -5 -4 -10 63.99 5.68 5 4 10 66.76 5.25 5 4 10 58.99 4.95 -5 -4 -10 55.80 5.19 5 4 11 38.80 4.04 5 4 11 43.69 4.24 5 4 11 37.62 3.91 -5 -4 -11 38.16 4.61 5 4 12 188.60 9.27 5 4 12 191.19 9.25 5 4 12 202.86 9.01 5 4 12 196.38 10.77 -5 -4 -12 191.77 10.48 5 4 13 12.82 3.09 5 4 13 19.17 3.33 5 4 13 12.04 2.98 -5 -4 -13 16.21 3.80 5 4 14 2.51 2.36 5 4 14 1.66 2.34 5 4 14 4.43 2.62 -5 -4 -14 0.19 3.20 5 4 15 38.89 4.24 5 4 15 43.04 4.11 5 4 15 46.63 4.43 -5 -4 -15 33.27 5.47 5 4 16 69.28 5.51 5 4 16 79.29 5.17 5 4 16 74.93 5.23 -5 -4 -16 63.69 6.79 5 4 17 0.60 2.53 5 4 17 2.27 2.57 -5 -4 -17 -2.31 4.02 5 4 18 7.39 2.87 5 4 18 4.13 3.03 -5 -4 -18 4.97 4.00 5 4 19 -0.95 2.77 -5 -4 -19 4.43 4.48 -5 -4 -20 0.89 4.58 -5 -4 -21 73.91 8.06 -5 -4 -22 22.65 6.08 5 4 23 14.72 14.48 -5 -4 -23 5.40 5.02 5 4 24 3.93 9.53 -5 -4 -24 6.87 5.71 -5 -4 -25 0.73 5.38 -5 -5 15 17.62 10.27 -5 -5 14 12.71 9.04 -5 -5 13 10.74 7.83 -5 -5 12 10.25 7.05 -5 -5 11 27.69 7.80 -5 -5 10 160.75 13.23 5 5 -10 156.36 11.48 5 5 -9 1.21 2.66 5 5 -9 0.33 3.55 -5 -5 9 3.59 4.89 5 5 -9 3.29 4.08 5 5 -8 39.93 4.67 5 5 -8 50.39 4.95 5 5 -8 46.76 4.89 -5 -5 8 36.06 7.03 5 5 -7 1.06 2.77 5 5 -7 0.33 2.94 5 5 -7 1.79 2.64 5 5 -7 -0.11 3.20 -5 -5 7 -0.56 4.61 -5 -5 6 71.42 7.91 5 5 -6 67.51 5.56 5 5 -6 70.54 5.06 5 5 -6 64.68 5.12 5 5 -6 64.27 4.69 5 5 -5 67.54 5.56 -5 -5 5 64.87 6.94 5 5 -5 64.57 4.47 5 5 -5 82.69 9.32 5 5 -5 68.38 5.15 5 5 -5 63.34 4.88 -5 -5 4 132.37 9.17 5 5 -4 123.59 7.44 5 5 -4 117.67 6.31 5 5 -4 119.89 6.94 5 5 -4 121.82 6.64 -5 -5 4 134.42 9.14 -5 -5 3 5.79 3.29 5 5 -3 5.25 2.77 5 5 -3 2.90 2.23 5 5 -3 7.76 3.87 5 5 -3 3.54 2.31 5 5 -3 0.39 4.60 5 5 -3 4.78 2.40 5 5 -3 5.32 2.70 -5 -5 3 3.87 3.00 5 5 -2 1.32 2.25 -5 -5 2 1.67 2.83 5 5 -2 -0.22 3.29 5 5 -2 0.52 2.23 5 5 -2 -0.20 2.42 5 5 -2 2.72 3.76 5 5 -2 1.34 2.25 5 5 -2 1.94 2.14 5 5 -1 68.12 5.40 -5 -5 1 68.33 6.20 5 5 -1 69.16 5.08 5 5 -1 83.14 6.90 5 5 -1 64.60 5.12 5 5 -1 69.24 7.67 5 5 -1 61.07 4.89 5 5 -1 65.07 5.38 5 5 0 9.86 2.66 5 5 0 10.61 3.41 5 5 0 8.28 2.66 5 5 0 10.12 3.61 5 5 0 10.35 2.61 5 5 0 13.70 6.83 5 5 0 9.55 2.62 5 5 0 8.97 2.75 5 5 1 88.42 6.03 5 5 1 101.71 7.28 5 5 1 88.07 6.07 5 5 1 95.44 7.78 5 5 1 76.92 5.55 5 5 1 90.06 6.05 5 5 2 88.12 6.85 5 5 2 80.51 5.77 -5 -5 -2 84.68 12.45 5 5 2 107.76 12.09 5 5 2 82.77 5.84 5 5 2 105.93 7.63 5 5 2 81.02 5.55 -5 -5 -2 87.10 6.20 5 5 2 81.33 5.73 5 5 3 192.87 9.60 5 5 3 206.43 10.83 -5 -5 -3 212.59 14.59 5 5 3 230.04 11.11 5 5 3 197.52 9.79 5 5 3 206.54 9.55 -5 -5 -3 210.52 10.07 5 5 3 212.38 9.79 5 5 4 335.36 13.90 5 5 4 357.21 13.90 -5 -5 -4 388.39 17.38 5 5 4 338.21 14.05 5 5 4 354.55 13.79 -5 -5 -4 340.85 13.96 5 5 4 377.69 15.22 -5 -5 -5 -0.33 5.10 5 5 5 5.10 2.49 -5 -5 -5 3.70 1.94 -5 -5 -6 -0.35 1.73 -5 -5 -6 -2.68 4.17 5 5 6 1.25 2.18 5 5 7 71.68 5.45 -5 -5 -7 80.35 7.57 5 5 7 78.80 5.69 5 5 7 81.61 5.51 5 5 7 84.57 6.33 -5 -5 -7 69.18 5.08 -5 -5 -8 2.25 1.84 5 5 8 -1.19 2.40 5 5 8 -0.11 2.33 -5 -5 -8 4.52 3.33 5 5 8 0.13 2.27 5 5 8 -0.50 2.61 -5 -5 -8 1.75 2.25 -5 -5 -9 31.99 3.68 5 5 9 26.05 3.68 -5 -5 -9 34.68 4.74 5 5 9 36.15 4.13 -5 -5 -9 28.06 3.83 5 5 9 31.15 3.76 5 5 10 53.89 4.89 5 5 10 52.75 4.88 -5 -5 -10 55.56 5.60 -5 -5 -10 52.40 5.23 5 5 10 56.85 4.82 5 5 11 150.83 8.30 5 5 11 158.80 8.30 -5 -5 -11 162.70 9.14 -5 -5 -11 132.99 8.47 5 5 11 158.31 7.93 5 5 12 54.89 4.97 5 5 12 48.64 4.67 -5 -5 -12 53.20 5.55 5 5 12 50.30 4.54 5 5 12 52.71 5.71 -5 -5 -12 49.92 5.40 5 5 13 330.56 13.92 5 5 13 358.38 13.92 5 5 13 345.73 13.25 -5 -5 -13 333.07 15.18 5 5 14 33.27 4.19 5 5 14 30.74 3.91 5 5 14 32.67 4.15 -5 -5 -14 33.46 4.97 5 5 15 170.93 9.04 5 5 15 189.42 8.71 5 5 15 185.29 8.97 -5 -5 -15 172.86 10.89 5 5 16 37.49 4.45 5 5 16 43.54 4.50 -5 -5 -16 38.63 5.60 5 5 17 41.90 4.76 5 5 17 61.52 5.08 -5 -5 -17 50.89 6.25 5 5 18 1.04 2.75 -5 -5 -18 -0.43 3.89 5 5 19 -0.87 3.09 -5 -5 -19 3.67 4.34 -5 -5 -20 97.91 8.78 -5 -5 -21 5.19 4.78 5 5 22 2.49 13.40 -5 -5 -22 123.18 9.66 5 5 23 -8.48 13.23 -5 -5 -23 -0.22 5.02 5 5 24 53.50 13.83 -5 -5 -24 52.36 7.96 -5 -5 -25 0.97 5.23 -5 -6 15 11.61 9.92 -5 -6 14 130.33 15.31 -5 -6 13 20.24 8.78 -5 -6 12 43.21 9.38 -5 -6 11 46.30 9.10 -5 -6 10 194.52 14.57 -5 -6 9 22.20 6.46 5 6 -8 144.65 8.52 -5 -6 8 143.63 11.93 5 6 -8 174.11 10.89 5 6 -8 173.23 9.81 -5 -6 7 206.21 13.66 5 6 -7 213.07 10.44 5 6 -7 236.41 11.41 5 6 -7 213.80 10.05 5 6 -6 351.31 14.16 -5 -6 6 320.85 17.06 5 6 -6 323.36 12.56 5 6 -6 360.56 14.20 5 6 -5 6.88 3.11 5 6 -5 7.03 2.42 -5 -6 5 7.85 4.26 5 6 -5 9.21 3.16 5 6 -5 9.01 2.90 5 6 -5 -2.55 8.95 -5 -6 5 6.27 3.78 5 6 -4 47.90 4.82 -5 -6 4 37.33 5.66 5 6 -4 50.57 8.02 5 6 -4 43.04 3.72 5 6 -4 44.53 10.23 5 6 -4 47.41 4.45 5 6 -4 48.08 4.65 -5 -6 4 48.32 6.01 5 6 -3 313.31 13.49 -5 -6 3 321.16 15.24 5 6 -3 291.73 11.85 5 6 -3 315.66 21.98 5 6 -3 335.57 12.82 5 6 -3 308.96 13.10 -5 -6 3 341.86 16.10 5 6 -2 253.67 11.76 -5 -6 2 270.74 13.43 5 6 -2 307.67 15.31 5 6 -2 266.12 10.79 5 6 -2 250.88 11.37 5 6 -2 219.16 17.25 5 6 -2 269.34 11.11 -5 -6 2 289.33 14.05 5 6 -2 247.42 12.17 5 6 -1 78.78 5.97 -5 -6 1 78.75 6.85 5 6 -1 86.54 5.56 5 6 -1 77.56 5.77 5 6 -1 77.98 5.43 5 6 -1 79.03 6.16 5 6 0 17.70 3.24 5 6 0 13.68 3.26 5 6 0 11.67 3.91 5 6 0 14.55 3.03 5 6 0 14.38 3.00 5 6 0 7.24 4.54 5 6 0 13.34 3.03 5 6 1 317.35 13.45 5 6 1 365.69 15.54 5 6 1 293.53 12.89 5 6 1 420.73 26.16 5 6 1 255.39 16.13 5 6 1 316.66 12.71 5 6 1 324.96 13.70 5 6 2 240.85 11.93 5 6 2 216.01 10.46 5 6 2 190.97 12.56 5 6 2 206.28 10.16 5 6 2 214.90 9.84 5 6 2 230.73 10.81 5 6 3 252.97 11.39 5 6 3 258.14 12.52 5 6 3 232.13 11.07 5 6 3 236.50 11.03 5 6 3 234.64 13.40 5 6 3 256.50 10.81 -5 -6 -3 235.27 11.41 5 6 4 6.59 2.59 5 6 4 5.30 2.51 5 6 4 -0.35 2.81 5 6 4 4.43 2.51 5 6 4 1.88 2.31 -5 -6 -4 -4.17 5.68 -5 -6 -4 5.14 2.20 5 6 4 2.75 3.07 5 6 5 420.21 16.65 5 6 5 408.34 16.49 -5 -6 -5 430.37 16.67 5 6 6 40.58 6.53 -5 -6 -6 35.21 3.87 5 6 6 40.94 4.95 5 6 7 5.60 2.66 -5 -6 -7 7.07 2.33 5 6 7 7.95 2.64 -5 -6 -7 3.16 4.15 5 6 7 2.07 3.94 5 6 7 9.81 3.16 5 6 8 46.76 4.69 5 6 8 54.87 4.95 -5 -6 -8 47.32 6.48 5 6 8 56.40 4.67 -5 -6 -8 50.72 4.97 -5 -6 -8 57.18 4.88 5 6 8 52.62 5.45 5 6 9 76.90 5.99 -5 -6 -9 78.69 5.92 -5 -6 -9 73.54 6.10 5 6 9 76.76 5.86 -5 -6 -9 81.17 7.31 5 6 9 77.28 5.51 5 6 10 205.05 10.64 5 6 10 229.17 10.70 -5 -6 -10 229.88 12.15 -5 -6 -10 228.82 11.46 5 6 10 234.12 10.25 5 6 11 31.95 4.24 5 6 11 34.91 4.24 -5 -6 -11 36.66 5.15 -5 -6 -11 36.97 4.88 5 6 11 36.49 4.15 5 6 12 -0.76 2.46 5 6 12 0.58 2.49 5 6 12 0.26 2.47 -5 -6 -12 0.69 3.03 5 6 12 -2.70 3.46 -5 -6 -12 -1.95 3.14 5 6 13 17.94 3.74 5 6 13 21.42 3.68 -5 -6 -13 19.09 4.19 5 6 13 21.75 3.76 -5 -6 -13 17.75 4.08 5 6 14 305.81 13.47 -5 -6 -14 289.75 13.81 5 6 14 306.93 12.88 -5 -6 -14 289.51 14.29 5 6 14 320.29 12.62 5 6 15 107.81 7.33 -5 -6 -15 106.10 8.00 -5 -6 -15 104.22 8.52 5 6 15 120.91 7.29 5 6 16 6.72 3.09 5 6 16 3.80 3.33 -5 -6 -16 0.61 3.70 5 6 17 7.50 3.13 5 6 17 5.10 3.68 -5 -6 -17 5.94 4.09 5 6 18 -0.89 2.94 -5 -6 -18 1.08 3.81 5 6 19 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187.47 11.35 -5 -7 1 58.58 6.21 5 7 -1 63.51 5.64 5 7 -1 75.01 7.67 5 7 -1 62.74 4.78 5 7 -1 68.51 5.28 5 7 -1 61.70 5.40 -5 -7 1 77.50 6.92 5 7 -1 53.42 5.55 5 7 0 79.21 6.10 5 7 0 71.94 5.17 5 7 0 91.70 7.72 5 7 0 90.04 10.81 5 7 0 68.36 5.36 5 7 0 66.00 5.49 5 7 0 72.18 5.99 5 7 1 112.15 7.33 5 7 1 119.40 8.86 5 7 1 99.14 10.62 5 7 1 117.06 6.74 5 7 1 105.63 6.92 5 7 1 114.66 7.54 5 7 2 201.61 10.22 5 7 2 237.84 12.04 5 7 2 198.86 9.88 5 7 2 229.32 9.88 5 7 2 232.72 10.85 5 7 3 139.28 8.11 5 7 3 156.95 9.27 5 7 3 132.06 7.93 5 7 3 138.12 7.68 5 7 3 133.88 7.31 5 7 4 28.49 4.54 5 7 4 27.59 4.04 5 7 4 24.38 3.63 5 7 4 26.44 3.68 -5 -7 -4 24.30 3.61 5 7 5 638.79 23.20 5 7 5 626.92 22.63 5 7 5 683.21 22.33 -5 -7 -5 640.28 23.24 5 7 6 288.04 15.70 -5 -7 -6 345.30 14.61 5 7 7 78.13 8.73 -5 -7 -7 62.69 5.43 5 7 7 60.66 6.42 5 7 8 9.49 3.18 -5 -7 -8 13.42 3.14 5 7 8 17.08 3.33 -5 -7 -8 10.03 5.01 5 7 8 18.74 3.37 -5 -7 -8 19.57 4.08 5 7 8 12.56 4.99 5 7 8 11.18 3.57 5 7 9 18.94 3.70 -5 -7 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104.42 6.66 5 8 2 86.84 6.53 5 8 3 10.90 3.33 5 8 3 6.36 2.98 5 8 3 5.75 3.59 5 8 3 10.42 3.13 5 8 3 6.75 4.74 5 8 3 11.18 3.20 5 8 4 121.90 8.04 5 8 4 121.30 8.41 5 8 4 136.45 13.45 5 8 4 126.75 7.18 5 8 4 104.61 7.13 -5 -8 -4 109.95 7.57 5 8 5 74.17 6.64 5 8 5 83.62 6.94 5 8 5 75.62 5.95 5 8 5 75.23 6.08 -5 -8 -5 79.30 6.40 5 8 6 449.70 17.75 5 8 6 452.25 16.90 -5 -8 -6 455.34 17.42 5 8 7 51.45 7.87 -5 -8 -7 35.52 4.58 -5 -8 -8 3.46 2.72 5 8 8 2.42 3.13 5 8 8 6.94 3.20 5 8 8 7.67 5.08 5 8 8 5.14 3.09 -5 -8 -8 2.23 4.30 5 8 8 0.26 3.09 5 8 9 269.58 13.32 -5 -8 -9 266.66 13.30 5 8 9 298.72 12.26 5 8 9 264.60 12.36 5 8 10 7.29 3.55 -5 -8 -10 4.50 3.20 -5 -8 -10 1.66 4.30 5 8 10 5.49 3.01 -5 -8 -10 6.23 3.57 5 8 10 7.13 3.22 5 8 11 22.50 4.47 -5 -8 -11 19.15 4.32 -5 -8 -11 11.35 4.84 5 8 11 24.38 4.09 5 8 12 64.85 6.59 -5 -8 -12 46.83 6.46 -5 -8 -12 55.04 6.36 5 8 12 68.72 5.97 5 8 13 112.74 8.39 -5 -8 -13 104.28 8.65 -5 -8 -13 115.18 8.67 5 8 13 130.42 8.17 5 8 14 -0.82 3.52 5 8 14 1.73 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9 1 320.29 14.22 -5 -9 -1 307.56 15.09 5 9 2 47.93 6.12 5 9 2 56.23 5.71 5 9 3 26.81 4.86 5 9 3 25.29 8.82 5 9 3 32.62 4.47 5 9 4 29.36 4.88 5 9 4 32.40 8.28 5 9 4 32.49 7.03 5 9 4 30.74 4.43 5 9 5 107.22 8.24 5 9 5 129.30 11.15 5 9 5 130.98 12.52 5 9 5 108.09 7.67 -5 -9 -5 110.25 8.02 5 9 6 30.66 4.99 5 9 6 51.64 8.48 5 9 6 35.00 4.80 -5 -9 -6 41.77 4.99 5 9 6 34.14 6.64 5 9 7 118.29 10.77 -5 -9 -7 90.88 7.22 -5 -9 -8 3.46 2.85 -5 -9 -8 -5.79 7.00 5 9 8 3.26 4.76 5 9 9 149.75 8.97 -5 -9 -9 150.03 9.77 -5 -9 -10 124.93 9.15 5 9 10 132.60 8.45 -5 -9 -11 102.25 8.60 5 9 11 108.85 7.82 -5 -9 -12 19.26 5.79 -5 -9 -12 27.39 5.53 5 9 12 33.74 5.14 -5 -9 -13 -1.00 5.34 -5 -9 -13 4.48 3.85 5 9 13 2.81 3.83 -5 -9 -14 91.59 8.71 -5 -9 -14 108.74 8.91 5 9 14 105.43 8.75 -5 -9 -15 7.76 4.34 -5 -9 -15 3.27 4.61 5 9 15 -3.35 5.36 -5 -9 -16 9.27 4.58 -5 -9 -17 23.05 5.56 -5 -9 -18 80.94 8.48 -5 -9 -19 12.52 5.21 -5 -9 -20 97.95 9.36 -5 -9 -21 6.03 5.27 -5 -9 -22 16.39 6.20 5 9 22 -18.20 14.59 -5 -9 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28.62 -5 -11 -3 1054.72 29.62 5 11 4 93.52 11.98 5 11 4 76.89 8.17 5 11 5 49.94 6.08 5 11 5 77.63 8.24 5 11 6 -4.00 4.22 5 11 6 -2.10 5.41 5 11 6 -5.38 5.08 5 11 7 69.00 7.28 5 11 7 160.19 12.24 5 11 7 99.87 9.29 -5 -11 -7 161.55 10.90 -5 -11 -7 142.18 9.68 5 11 8 50.02 7.74 -5 -11 -8 42.61 6.53 -5 -11 -8 35.50 5.71 -5 -11 -9 0.78 3.37 -5 -11 -9 8.97 4.65 5 11 9 -0.56 4.74 5 11 10 284.88 14.89 -5 -11 -10 239.64 14.14 -5 -11 -11 151.15 11.22 5 11 11 107.18 10.10 -5 -11 -12 723.38 27.91 -5 -11 -12 453.69 28.26 -5 -11 -13 181.78 16.11 -5 -11 -14 58.33 9.92 -5 -11 -15 -9.02 7.41 -5 -11 -16 17.36 6.75 -5 -11 -17 -3.96 5.99 -5 -11 -18 28.19 7.48 -5 -11 -19 1.41 5.71 -5 -11 -20 1.79 6.18 -5 -11 -21 146.59 13.64 -5 -11 -22 201.43 15.67 -5 -11 -23 18.44 7.95 -5 -11 -24 31.30 8.89 -5 -11 -25 2.62 7.15 -5 -12 9 16.64 7.07 -5 -12 8 36.69 7.89 -5 -12 7 60.72 8.82 -5 -12 7 58.61 9.23 -5 -12 6 59.39 8.39 -5 -12 6 60.88 8.84 -5 -12 5 17.42 6.12 -5 -12 5 14.94 6.21 -5 -12 4 73.24 8.69 -5 -12 4 81.78 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3.39 2.46 -6 -5 0 4.61 2.88 6 5 0 1.45 3.22 6 5 1 135.03 9.14 6 5 1 112.80 7.52 6 5 1 137.36 15.33 6 5 1 118.14 7.74 6 5 1 148.64 8.75 6 5 1 119.91 7.33 6 5 1 120.09 7.50 -6 -5 -1 129.62 8.47 6 5 2 144.82 9.40 6 5 2 128.99 7.93 -6 -5 -2 103.46 13.49 6 5 2 146.35 14.50 6 5 2 121.32 7.93 6 5 2 153.14 8.63 6 5 2 136.65 7.85 -6 -5 -2 133.14 8.45 6 5 2 134.62 7.89 6 5 3 52.27 5.92 6 5 3 46.93 4.93 -6 -5 -3 54.67 7.78 6 5 3 59.47 9.21 6 5 3 46.76 4.97 6 5 3 52.68 4.88 6 5 3 47.71 4.71 -6 -5 -3 52.70 5.10 6 5 3 54.30 5.19 6 5 4 24.64 3.83 6 5 4 25.75 4.76 -6 -5 -4 29.06 5.01 6 5 4 26.55 3.96 6 5 4 20.54 5.95 6 5 4 26.79 4.09 6 5 4 27.86 3.80 -6 -5 -4 23.61 3.55 6 5 4 28.53 4.02 6 5 5 78.90 6.14 6 5 5 91.64 5.97 -6 -5 -5 75.56 10.38 -6 -5 -5 97.73 7.41 6 5 5 75.38 6.35 -6 -5 -5 83.71 6.01 6 5 5 89.93 6.55 -6 -5 -6 -0.33 5.21 -6 -5 -6 4.09 2.68 6 5 6 4.11 2.68 -6 -5 -6 5.51 2.34 6 5 7 87.32 6.23 -6 -5 -7 89.76 8.80 6 5 7 81.71 6.35 6 5 7 83.44 6.01 6 5 7 81.09 6.55 -6 -5 -7 83.73 5.75 6 5 8 57.35 5.27 -6 -5 -8 62.63 7.05 6 5 8 65.37 5.62 6 5 8 67.08 5.40 6 5 8 63.73 6.03 -6 -5 -8 62.33 4.91 6 5 9 98.79 6.88 -6 -5 -9 121.71 9.02 -6 -5 -9 95.10 7.16 6 5 9 102.66 7.05 6 5 9 105.37 6.77 -6 -5 -9 109.11 6.59 6 5 9 113.77 7.98 6 5 10 43.71 4.74 -6 -5 -10 41.55 4.99 -6 -5 -10 45.77 5.66 6 5 10 42.33 4.82 6 5 10 46.80 4.84 -6 -5 -10 42.65 4.28 6 5 10 44.77 5.40 -6 -5 -11 56.62 4.97 6 5 11 48.49 5.10 -6 -5 -11 51.60 5.86 6 5 11 60.06 5.47 -6 -5 -11 57.87 5.90 6 5 11 51.02 5.06 6 5 12 1.53 2.57 -6 -5 -12 -0.30 2.49 6 5 12 2.12 2.96 -6 -5 -12 3.01 3.48 6 5 12 3.03 3.00 -6 -5 -12 0.37 2.98 6 5 13 234.34 11.65 6 5 13 246.31 11.61 6 5 13 276.45 11.50 -6 -5 -13 241.86 12.80 6 5 14 5.43 3.22 6 5 14 4.43 3.11 6 5 14 4.73 3.11 -6 -5 -14 5.40 3.52 6 5 15 1.10 2.55 6 5 15 2.36 3.00 6 5 15 4.09 3.16 -6 -5 -15 -1.86 4.24 6 5 16 68.20 6.01 6 5 16 79.97 5.77 6 5 16 70.47 5.84 -6 -5 -16 60.62 7.03 6 5 17 32.75 4.60 6 5 17 34.55 4.52 6 5 17 42.11 4.71 -6 -5 -17 22.74 5.58 6 5 18 38.78 5.01 6 5 18 47.49 4.97 -6 -5 -18 37.61 6.38 6 5 19 -1.64 3.24 6 5 19 -3.91 3.93 -6 -5 -19 -7.42 5.51 6 5 20 -2.57 5.04 -6 -5 -20 7.61 5.10 -6 -5 -21 12.37 5.40 -6 -5 -22 37.46 7.05 -6 -5 -23 23.11 6.38 6 5 24 -6.68 14.40 -6 -5 -24 25.77 6.75 -6 -6 14 75.55 13.14 -6 -6 13 111.10 14.50 -6 -6 12 212.16 17.40 -6 -6 11 5.81 7.03 -6 -6 10 108.02 12.04 -6 -6 9 120.67 12.04 6 6 -9 168.90 10.62 6 6 -8 31.35 4.95 -6 -6 8 18.38 6.23 -6 -6 7 131.41 11.07 6 6 -7 130.81 8.43 6 6 -7 145.92 8.28 6 6 -7 137.77 8.34 6 6 -7 114.77 7.72 6 6 -6 531.33 20.08 -6 -6 6 518.94 23.39 6 6 -6 539.34 19.04 6 6 -6 538.01 19.63 6 6 -6 477.41 17.94 6 6 -5 61.14 5.99 -6 -6 5 58.30 7.72 6 6 -5 52.32 4.71 6 6 -5 56.81 5.36 6 6 -5 39.22 8.56 6 6 -5 52.60 5.45 6 6 -4 932.90 30.81 -6 -6 4 902.12 33.47 6 6 -4 845.05 28.34 6 6 -4 872.30 29.81 6 6 -4 863.01 36.30 6 6 -4 927.08 29.20 -6 -6 4 940.19 33.88 6 6 -3 31.99 4.52 -6 -6 3 36.36 5.84 6 6 -3 36.21 6.88 6 6 -3 29.40 3.87 6 6 -3 28.90 4.17 6 6 -3 21.31 5.75 6 6 -3 32.97 4.13 -6 -6 3 30.70 5.47 6 6 -2 20.97 4.00 -6 -6 2 21.75 4.78 6 6 -2 19.56 3.61 6 6 -2 23.65 3.67 6 6 -2 27.07 5.77 6 6 -2 27.07 5.75 6 6 -2 19.00 3.54 6 6 -1 497.67 19.72 6 6 -1 487.64 18.64 6 6 -1 582.04 23.11 6 6 -1 555.10 35.58 6 6 -1 505.41 19.46 6 6 -1 576.53 23.76 6 6 -1 522.46 18.87 6 6 0 182.15 9.82 6 6 0 168.66 9.15 6 6 0 200.89 11.91 6 6 0 210.86 12.73 6 6 0 229.60 21.73 6 6 0 167.15 9.49 6 6 0 177.20 9.08 6 6 0 175.60 9.66 6 6 1 21.58 3.80 6 6 1 22.76 4.80 6 6 1 19.54 3.55 6 6 1 28.66 9.29 6 6 1 19.24 3.61 -6 -6 -1 27.20 4.26 6 6 1 23.30 3.80 6 6 1 21.45 5.01 6 6 2 25.60 4.00 6 6 2 33.55 5.15 6 6 2 27.45 4.11 6 6 2 31.91 4.09 6 6 2 28.08 4.04 -6 -6 -2 27.86 4.19 6 6 2 30.29 5.08 6 6 3 5.97 2.74 6 6 3 12.26 3.94 6 6 3 5.73 2.81 6 6 3 6.81 3.11 6 6 3 14.70 6.55 6 6 3 7.20 2.81 -6 -6 -3 5.88 2.79 6 6 3 4.67 3.26 6 6 4 75.36 7.20 6 6 4 77.07 6.12 6 6 4 77.91 6.03 -6 -6 -4 63.77 9.43 6 6 4 75.32 6.31 6 6 4 82.60 6.10 -6 -6 -4 76.09 6.20 6 6 4 92.20 7.22 6 6 5 1300.73 43.58 6 6 5 1387.33 43.37 -6 -6 -5 1438.18 48.38 6 6 5 1342.39 44.03 6 6 5 1460.07 43.43 6 6 5 1545.75 45.87 -6 -6 -5 1329.81 43.58 -6 -6 -6 106.42 8.48 -6 -6 -6 96.11 6.72 6 6 6 114.96 8.00 6 6 7 98.51 6.75 -6 -6 -7 94.32 6.51 6 6 7 110.75 7.96 6 6 8 89.74 6.62 -6 -6 -8 89.63 8.97 6 6 8 99.53 7.01 6 6 8 96.94 6.59 -6 -6 -8 89.58 6.35 6 6 8 96.57 7.70 6 6 9 3.68 2.68 -6 -6 -9 4.24 2.47 6 6 9 3.48 2.87 -6 -6 -9 1.95 4.04 6 6 9 5.62 3.01 6 6 9 -0.61 3.33 -6 -6 -9 2.31 3.01 6 6 10 207.81 10.92 -6 -6 -10 241.52 13.12 6 6 10 222.21 11.13 -6 -6 -10 203.92 11.31 6 6 10 225.13 10.53 6 6 10 238.30 12.63 -6 -6 -10 219.38 10.83 -6 -6 -11 79.01 6.31 6 6 11 77.87 6.40 6 6 11 78.86 6.38 -6 -6 -11 81.31 7.57 -6 -6 -11 70.69 6.61 6 6 11 84.94 6.23 6 6 12 2.81 2.94 -6 -6 -12 4.15 2.98 6 6 12 4.39 3.11 6 6 12 3.78 2.92 -6 -6 -12 2.90 3.68 -6 -6 -12 2.72 3.31 6 6 13 9.69 3.33 6 6 13 9.86 3.37 6 6 13 11.22 3.63 -6 -6 -13 8.11 3.80 6 6 14 25.16 4.58 6 6 14 34.14 4.67 6 6 14 30.22 4.41 -6 -6 -14 24.71 4.93 6 6 15 -1.36 3.07 6 6 15 2.79 3.22 6 6 15 3.37 3.13 -6 -6 -15 -4.89 4.39 6 6 16 173.16 9.99 6 6 16 195.92 9.42 6 6 16 187.58 9.73 6 6 17 17.83 4.13 6 6 17 22.20 4.37 -6 -6 -17 8.39 5.10 6 6 18 22.40 4.41 6 6 18 29.68 4.71 -6 -6 -18 23.78 5.81 6 6 19 123.39 8.47 -6 -6 -19 112.15 9.90 6 6 19 140.30 8.95 -6 -6 -20 -0.24 5.06 -6 -6 -21 -1.23 5.04 -6 -6 -22 28.34 6.75 -6 -6 -23 9.90 5.73 -6 -6 -24 0.76 5.73 -6 -7 13 219.81 18.50 -6 -7 12 -2.62 8.06 -6 -7 11 86.58 11.80 -6 -7 10 36.47 8.11 -6 -7 9 189.22 14.35 -6 -7 8 69.74 9.27 6 7 -8 90.12 8.93 6 7 -7 52.21 5.88 -6 -7 7 53.91 7.93 6 7 -7 64.83 6.90 -6 -7 6 293.48 16.30 6 7 -6 333.13 13.94 6 7 -6 331.40 13.88 6 7 -5 73.54 6.64 -6 -7 5 69.41 8.06 6 7 -5 65.68 5.04 6 7 -5 74.73 6.31 6 7 -5 85.71 6.70 6 7 -4 1057.57 34.00 -6 -7 4 1087.51 37.21 6 7 -4 1134.98 33.10 6 7 -4 1053.46 33.47 -6 -7 4 1115.42 38.01 6 7 -3 315.38 13.96 -6 -7 3 311.93 16.02 6 7 -3 292.92 12.00 6 7 -3 322.58 13.06 6 7 -3 302.50 13.47 -6 -7 3 313.27 16.47 6 7 -2 371.09 15.39 -6 -7 2 356.22 17.06 6 7 -2 335.38 13.55 6 7 -2 353.00 14.79 6 7 -2 378.23 14.35 -6 -7 2 377.66 17.77 6 7 -1 -0.17 2.90 6 7 -1 3.05 2.98 6 7 -1 0.78 2.70 6 7 -1 -2.61 4.22 6 7 -1 1.38 4.04 6 7 -1 0.11 2.74 6 7 0 416.64 17.32 6 7 0 432.70 16.58 6 7 0 519.52 21.03 6 7 0 416.84 17.14 6 7 0 595.08 34.57 6 7 0 309.87 19.72 6 7 0 450.69 16.69 6 7 1 9.69 3.27 6 7 1 12.62 4.41 6 7 1 11.07 3.26 6 7 1 18.72 9.14 6 7 1 13.21 3.55 6 7 1 5.41 4.17 6 7 2 136.65 10.03 6 7 2 112.15 7.80 6 7 2 118.25 7.85 6 7 2 96.72 9.43 6 7 2 117.00 7.28 6 7 2 123.76 7.98 -6 -7 -2 113.84 8.28 6 7 3 2.79 2.79 6 7 3 9.51 3.16 6 7 3 5.68 3.72 6 7 3 6.05 3.01 6 7 3 5.71 2.92 -6 -7 -3 5.23 2.88 6 7 3 1.34 3.91 6 7 4 1.82 2.77 6 7 4 -0.65 3.42 6 7 4 -0.50 2.47 6 7 4 2.46 2.81 -6 -7 -4 -3.70 9.10 6 7 4 2.74 2.98 -6 -7 -4 0.71 2.53 6 7 4 -3.22 3.93 6 7 5 1897.19 59.04 6 7 5 2022.42 61.44 6 7 5 1952.21 61.68 6 7 5 1933.81 59.12 6 7 5 2114.94 58.69 -6 -7 -5 1903.78 59.19 -6 -7 -6 937.91 39.97 -6 -7 -6 1009.27 35.22 -6 -7 -7 559.82 22.24 6 7 7 631.26 24.58 6 7 8 300.79 13.96 6 7 8 306.04 13.88 6 7 8 330.11 13.47 -6 -7 -8 303.00 13.75 6 7 8 334.95 15.82 6 7 9 123.01 8.19 6 7 9 121.15 7.98 -6 -7 -9 120.65 10.76 -6 -7 -9 119.70 8.76 6 7 9 130.27 7.78 -6 -7 -9 116.58 7.78 6 7 9 135.11 9.60 6 7 10 26.20 4.52 6 7 10 31.67 4.48 -6 -7 -10 16.86 5.49 -6 -7 -10 36.53 4.95 6 7 10 29.88 4.37 -6 -7 -10 30.61 4.35 6 7 11 249.62 12.76 -6 -7 -11 262.81 12.99 6 7 11 266.72 12.60 -6 -7 -11 265.92 14.51 -6 -7 -11 252.87 13.21 6 7 11 295.97 12.32 6 7 12 18.59 4.13 -6 -7 -12 20.49 4.19 6 7 12 20.58 3.96 6 7 12 24.77 4.26 -6 -7 -12 15.30 4.91 -6 -7 -12 21.85 4.48 6 7 13 61.57 6.23 -6 -7 -13 55.39 6.42 6 7 13 72.90 5.94 6 7 13 65.61 6.03 6 7 14 112.44 8.19 -6 -7 -14 112.15 8.97 6 7 14 131.48 7.91 6 7 14 120.00 7.96 6 7 15 259.46 13.17 -6 -7 -15 244.02 13.94 6 7 15 283.52 12.28 6 7 15 271.09 12.69 6 7 16 567.71 23.00 -6 -7 -16 594.64 24.77 6 7 17 593.45 23.76 -6 -7 -17 605.50 25.62 6 7 18 -2.23 3.46 6 7 18 -1.06 4.04 -6 -7 -18 1.47 4.35 6 7 19 2.81 3.48 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-6 -8 -5 144.08 8.99 -6 -8 -6 502.73 32.41 6 8 6 779.43 26.29 6 8 6 595.79 27.45 -6 -8 -6 721.59 26.24 6 8 7 35.09 7.83 -6 -8 -7 26.11 4.19 6 8 8 512.11 23.46 -6 -8 -8 386.55 17.40 -6 -8 -9 10.64 3.31 -6 -8 -9 12.08 4.58 6 8 9 11.65 3.63 -6 -8 -10 8.35 3.26 6 8 10 7.41 3.46 -6 -8 -10 2.20 4.84 -6 -8 -10 9.15 3.89 -6 -8 -11 159.54 10.55 6 8 11 178.22 9.90 -6 -8 -11 167.24 10.25 -6 -8 -12 36.12 5.55 -6 -8 -12 41.33 5.84 6 8 12 42.74 5.23 -6 -8 -13 36.69 5.73 -6 -8 -13 36.56 5.55 6 8 13 44.08 5.40 6 8 14 8.02 3.83 -6 -8 -14 6.33 3.93 -6 -8 -15 200.33 12.39 6 8 15 242.36 11.96 -6 -8 -16 69.26 7.93 6 8 16 88.66 7.61 -6 -8 -17 849.93 33.62 6 8 17 983.94 32.79 6 8 18 1.10 4.95 -6 -8 -18 5.69 5.04 -6 -8 -19 16.97 6.36 -6 -8 -20 8.89 5.77 -6 -8 -21 7.37 5.94 -6 -8 -22 27.63 7.24 -6 -8 -23 2.79 6.01 -6 -8 -24 13.77 6.88 -6 -9 12 31.93 9.38 -6 -9 11 -0.39 7.09 -6 -9 10 24.12 7.63 -6 -9 9 5.51 6.25 -6 -9 8 23.37 7.00 -6 -9 7 12.32 6.03 -6 -9 6 66.32 8.43 -6 -9 5 5.28 4.82 6 9 -5 0.60 6.48 -6 -9 5 6.51 4.95 -6 -9 4 194.58 13.01 6 9 -4 178.43 11.98 -6 -9 4 199.17 13.55 -6 -9 3 76.16 8.34 6 9 -3 101.02 8.50 -6 -9 3 102.99 9.51 6 9 -2 5.90 2.83 6 9 -2 0.41 5.02 6 9 -2 5.73 3.81 -6 -9 2 4.11 4.28 6 9 -1 20.54 5.99 6 9 -1 20.80 3.59 6 9 -1 31.26 5.04 -6 -9 1 23.54 5.43 6 9 0 19.57 5.40 6 9 0 16.23 3.61 6 9 0 25.06 4.47 -6 -9 0 21.98 5.06 6 9 1 3.63 3.27 6 9 1 3.63 3.72 6 9 2 2.94 3.14 6 9 2 4.39 4.06 6 9 3 80.72 8.19 6 9 3 81.05 6.81 6 9 4 27.99 5.36 6 9 4 31.97 8.99 6 9 4 35.95 4.93 -6 -9 -4 35.09 5.02 6 9 5 224.91 13.38 6 9 5 254.77 12.63 -6 -9 -5 243.63 12.91 6 9 6 1.66 3.50 6 9 6 1.25 3.13 6 9 6 0.41 5.77 -6 -9 -6 2.01 2.79 6 9 7 79.73 9.92 -6 -9 -7 49.16 5.64 -6 -9 -8 9.69 3.46 6 9 8 5.69 5.21 -6 -9 -9 18.94 4.21 6 9 9 21.03 4.39 6 9 9 24.60 6.53 -6 -9 -9 10.23 6.18 -6 -9 -10 1.79 2.87 -6 -9 -10 -1.64 4.50 6 9 10 5.28 3.59 -6 -9 -11 4.47 3.41 6 9 11 3.11 3.52 -6 -9 -11 -0.87 3.98 -6 -9 -12 51.49 6.49 -6 -9 -12 43.02 6.75 6 9 12 64.34 6.55 -6 -9 -13 17.40 4.91 -6 -9 -13 16.95 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6.57 4.11 6 10 5 13.99 4.28 6 10 5 15.78 7.52 -6 -10 -5 10.53 3.57 6 10 6 207.29 13.16 6 10 6 249.34 12.95 -6 -10 -6 243.03 13.21 6 10 7 -0.97 4.00 6 10 7 8.52 3.98 6 10 7 4.06 5.34 -6 -10 -7 9.01 3.74 6 10 8 120.76 11.26 -6 -10 -8 79.92 7.44 6 10 9 146.51 11.69 -6 -10 -9 101.41 8.60 -6 -10 -10 12.45 4.35 6 10 10 19.95 4.80 6 10 10 19.22 6.14 -6 -10 -11 -0.26 3.50 6 10 11 1.43 3.94 -6 -10 -11 -8.06 6.62 -6 -10 -12 6.88 4.19 6 10 12 -1.92 4.84 -6 -10 -12 -1.41 5.27 -6 -10 -13 51.91 7.33 -6 -10 -13 33.51 7.18 6 10 13 47.88 6.55 -6 -10 -14 2.18 4.41 -6 -10 -14 -2.20 5.12 6 10 14 -4.86 5.01 -6 -10 -15 96.46 9.88 6 10 15 120.61 10.14 -6 -10 -16 28.82 6.35 6 10 16 13.40 6.27 -6 -10 -17 94.36 9.84 -6 -10 -18 10.77 5.58 -6 -10 -19 6.33 5.45 -6 -10 -20 20.65 6.57 -6 -10 -21 27.17 7.15 -6 -10 -22 19.30 7.18 -6 -10 -23 7.39 6.75 -6 -10 -24 69.54 10.07 -6 -11 11 13.68 8.15 -6 -11 10 37.08 8.75 -6 -11 9 47.19 9.02 -6 -11 8 252.86 16.62 -6 -11 7 17.73 7.37 -6 -11 6 396.52 20.45 -6 -11 6 389.14 21.21 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3.24 7 5 3 14.61 3.37 7 5 4 72.77 6.35 7 5 4 76.44 7.41 -7 -5 -4 88.18 8.02 7 5 4 71.49 6.68 7 5 4 83.68 6.14 -7 -5 -4 77.52 6.35 7 5 4 81.11 6.21 7 5 5 -1.97 3.20 7 5 5 -1.73 2.29 -7 -5 -5 -5.01 7.46 -7 -5 -5 3.81 3.13 7 5 5 -0.39 4.21 7 5 5 -2.85 3.96 7 5 5 1.49 2.64 -7 -5 -5 -0.63 2.33 -7 -5 -6 1.64 2.61 -7 -5 -6 -1.95 6.03 7 5 6 1.02 2.61 -7 -5 -6 1.34 2.12 -7 -5 -7 195.40 14.18 -7 -5 -7 199.42 10.90 7 5 7 198.49 10.81 -7 -5 -7 194.02 9.82 7 5 8 70.84 6.12 -7 -5 -8 62.65 8.76 7 5 8 71.94 6.36 7 5 8 75.47 6.14 7 5 8 76.53 6.74 -7 -5 -8 70.32 5.51 7 5 9 262.70 12.82 -7 -5 -9 281.21 15.46 7 5 9 282.94 13.25 7 5 9 288.75 12.65 -7 -5 -9 268.99 11.95 7 5 10 30.81 4.56 7 5 10 36.34 4.91 7 5 10 33.87 4.61 -7 -5 -10 34.01 3.98 7 5 11 3.20 2.92 -7 -5 -11 3.14 2.42 7 5 11 2.25 3.03 7 5 11 8.60 3.41 -7 -5 -11 2.47 3.39 7 5 12 10.25 3.41 -7 -5 -12 9.06 2.92 7 5 12 8.91 3.52 7 5 12 10.81 3.70 -7 -5 -12 13.94 4.15 7 5 13 11.61 3.59 -7 -5 -13 8.06 3.07 7 5 13 9.73 3.59 7 5 13 6.48 3.50 -7 -5 -13 7.24 3.78 7 5 14 4.86 3.42 -7 -5 -14 6.92 3.05 7 5 14 4.34 3.50 7 5 14 6.36 3.61 -7 -5 -14 3.22 3.81 7 5 15 6.42 3.35 -7 -5 -15 2.46 3.09 7 5 15 7.82 3.55 7 5 15 7.09 3.52 -7 -5 -15 2.68 3.68 7 5 16 46.87 5.68 7 5 16 64.38 6.03 7 5 16 60.47 5.69 -7 -5 -16 56.64 7.07 7 5 17 52.88 5.99 7 5 17 63.86 6.01 7 5 17 60.92 5.69 -7 -5 -17 58.76 7.57 7 5 18 135.78 9.19 7 5 18 166.44 8.78 7 5 18 162.35 9.06 -7 -5 -18 130.51 10.42 7 5 19 36.04 5.21 7 5 19 44.94 5.45 -7 -5 -19 27.20 6.44 7 5 20 41.40 5.19 -7 -5 -20 28.06 6.57 -7 -5 -21 -7.00 6.64 -7 -5 -22 -3.41 5.58 -7 -5 -23 2.92 5.68 -7 -6 12 -4.17 8.67 -7 -6 11 -1.30 7.65 -7 -6 10 30.55 8.37 7 6 -9 20.24 5.08 -7 -6 9 14.29 7.16 7 6 -8 10.64 4.13 -7 -6 8 5.64 6.01 -7 -6 7 24.32 6.85 7 6 -7 26.50 4.71 -7 -6 6 0.32 5.08 7 6 -6 10.74 4.32 7 6 -6 2.25 3.33 7 6 -6 2.18 3.03 -7 -6 5 7.44 5.23 7 6 -5 14.55 4.41 7 6 -5 3.22 3.33 7 6 -5 6.62 3.00 -7 -6 4 289.48 16.65 7 6 -4 289.72 12.60 7 6 -4 268.95 13.23 -7 -6 3 6.27 4.84 7 6 -3 9.40 3.41 7 6 -3 1.99 9.36 7 6 -3 11.39 3.72 7 6 -3 6.61 4.15 7 6 -2 46.44 4.99 7 6 -2 44.29 5.41 7 6 -2 63.25 14.96 7 6 -2 50.93 6.36 7 6 -1 5.69 4.35 7 6 -1 1.30 2.98 7 6 -1 8.80 8.26 7 6 -1 2.21 3.11 -7 -6 1 4.41 3.67 7 6 -1 2.94 3.39 7 6 0 52.60 5.53 7 6 0 68.10 7.89 7 6 0 48.19 5.60 7 6 0 63.21 6.40 7 6 0 75.23 13.88 -7 -6 0 63.99 6.77 7 6 1 106.19 7.80 7 6 1 116.00 9.56 7 6 1 107.74 7.54 7 6 1 98.01 7.70 7 6 1 116.22 8.32 -7 -6 -1 105.21 8.41 7 6 2 146.33 9.23 7 6 2 170.41 11.41 7 6 2 182.04 17.49 7 6 2 154.50 9.53 7 6 2 175.13 9.99 7 6 2 148.97 8.82 7 6 2 142.18 8.84 -7 -6 -2 153.83 9.94 7 6 3 37.48 4.89 7 6 3 41.57 6.35 7 6 3 37.42 5.30 -7 -6 -3 24.00 9.58 7 6 3 49.91 10.03 7 6 3 45.20 5.14 -7 -6 -3 39.35 4.97 7 6 3 41.20 4.89 7 6 3 46.83 5.40 7 6 4 9.73 4.39 7 6 4 9.21 3.29 7 6 4 10.92 3.35 7 6 4 9.64 3.57 7 6 4 20.47 7.11 7 6 4 9.27 3.59 -7 -6 -4 2.10 5.10 7 6 4 13.86 3.67 -7 -6 -4 12.17 3.46 7 6 5 70.76 6.44 7 6 5 71.81 7.63 7 6 5 75.08 6.14 -7 -6 -5 88.89 8.78 7 6 5 75.81 6.96 7 6 5 74.13 6.53 7 6 5 86.51 7.07 -7 -6 -5 79.92 6.51 -7 -6 -6 16.13 4.37 7 6 6 10.40 3.55 -7 -6 -6 11.41 3.20 -7 -6 -7 80.64 7.35 -7 -6 -7 59.04 9.94 -7 -6 -7 79.34 6.18 7 6 7 82.97 7.24 7 6 8 12.30 3.41 7 6 8 7.85 3.42 -7 -6 -8 19.35 5.90 7 6 8 13.45 3.96 -7 -6 -8 12.23 3.18 7 6 9 62.09 6.14 7 6 9 64.87 6.05 -7 -6 -9 70.73 5.77 7 6 10 310.97 14.40 7 6 10 328.42 13.83 -7 -6 -10 291.62 13.32 -7 -6 -11 9.86 3.05 7 6 11 4.97 3.41 7 6 11 3.98 3.29 -7 -6 -11 5.94 3.80 -7 -6 -12 2.42 2.53 7 6 12 1.71 3.11 -7 -6 -12 2.51 3.27 7 6 13 29.85 4.82 -7 -6 -13 33.79 5.53 -7 -6 -13 31.89 4.54 -7 -6 -14 20.62 4.30 7 6 14 30.24 4.80 -7 -6 -14 27.48 5.25 -7 -6 -15 1.94 3.41 7 6 15 1.64 3.41 -7 -6 -15 0.22 3.78 -7 -6 -16 26.63 5.04 7 6 16 30.80 5.08 -7 -6 -16 21.03 5.66 7 6 17 12.50 4.30 -7 -6 -17 2.68 5.08 7 6 18 0.47 3.55 -7 -6 -18 0.24 4.58 -7 -6 -19 120.46 10.59 7 6 19 151.87 9.01 7 6 20 4.30 4.06 -7 -6 -20 0.52 4.93 7 6 21 65.91 7.61 -7 -6 -21 57.33 8.56 -7 -6 -22 20.32 6.55 -7 -6 -23 16.21 6.46 -7 -7 12 52.32 11.22 -7 -7 11 16.06 8.21 -7 -7 10 5.15 7.03 -7 -7 9 -2.98 6.79 -7 -7 8 14.79 6.59 7 7 -8 24.15 5.88 -7 -7 7 15.70 6.38 7 7 -7 18.10 4.71 -7 -7 6 8.21 5.62 7 7 -6 8.41 4.11 -7 -7 5 39.58 7.01 7 7 -5 55.56 7.82 7 7 -5 41.29 5.55 -7 -7 4 385.41 19.84 7 7 -4 387.35 16.58 7 7 -4 377.43 15.03 -7 -7 3 109.10 10.12 7 7 -3 103.66 7.01 7 7 -3 114.83 8.09 7 7 -3 119.96 10.36 7 7 -2 176.10 9.49 7 7 -2 190.00 10.46 7 7 -2 195.21 12.99 7 7 -1 122.75 7.83 7 7 -1 123.20 8.50 7 7 -1 141.40 11.03 7 7 0 58.93 5.69 7 7 0 59.23 7.83 7 7 0 58.09 5.99 7 7 0 58.97 7.70 -7 -7 0 61.37 6.90 7 7 1 61.05 7.65 7 7 1 44.99 5.19 7 7 1 51.02 6.94 7 7 1 47.65 5.56 7 7 1 72.96 13.53 -7 -7 -1 54.93 6.42 7 7 2 11.31 4.80 7 7 2 23.32 8.69 7 7 2 9.62 3.59 -7 -7 -2 11.16 3.91 7 7 2 9.14 4.21 7 7 3 24.95 5.64 7 7 3 40.51 9.81 7 7 3 26.96 4.65 7 7 3 31.89 5.51 -7 -7 -3 34.09 4.84 7 7 4 54.91 5.69 7 7 4 56.25 7.22 7 7 4 58.65 6.03 -7 -7 -4 40.06 11.67 -7 -7 -4 53.98 5.77 7 7 4 63.02 6.70 7 7 5 142.20 10.77 7 7 5 152.77 9.02 -7 -7 -5 126.57 13.81 7 7 5 148.90 9.49 7 7 5 154.40 10.16 -7 -7 -5 143.30 9.21 -7 -7 -6 55.64 8.11 7 7 6 57.65 6.18 -7 -7 -6 57.79 5.79 -7 -7 -7 481.73 22.16 -7 -7 -7 480.72 19.22 -7 -7 -8 204.33 10.85 7 7 9 6.27 3.68 -7 -7 -9 9.71 3.22 7 7 10 44.66 5.49 -7 -7 -10 49.87 5.14 7 7 11 36.47 5.23 -7 -7 -11 37.35 5.15 -7 -7 -11 29.75 4.47 7 7 12 138.68 8.95 -7 -7 -12 126.49 9.42 -7 -7 -12 121.66 8.43 -7 -7 -13 16.52 4.21 7 7 13 19.24 4.24 -7 -7 -13 17.90 4.74 -7 -7 -14 1.04 3.29 7 7 14 -0.87 3.39 -7 -7 -14 0.93 3.85 -7 -7 -15 -0.89 3.70 7 7 15 2.81 3.91 -7 -7 -15 2.44 3.94 -7 -7 -16 207.23 12.65 7 7 16 230.69 11.89 -7 -7 -16 218.10 13.60 -7 -7 -17 91.47 9.21 7 7 17 101.15 7.91 7 7 18 42.50 5.71 -7 -7 -18 31.61 6.62 7 7 19 4.06 4.06 -7 -7 -19 -3.18 5.84 7 7 20 -3.83 4.89 -7 -7 -20 0.54 5.14 -7 -7 -21 158.59 12.47 7 7 21 141.55 10.85 -7 -7 -22 20.51 6.75 -7 -7 -23 -1.97 5.99 -7 -8 11 0.41 6.70 -7 -8 10 7.85 7.01 -7 -8 9 5.94 6.70 -7 -8 8 -2.12 6.38 7 8 -8 -4.88 8.06 -7 -8 7 27.80 7.18 7 8 -7 28.15 6.49 -7 -8 6 14.42 6.46 7 8 -6 21.16 5.30 -7 -8 5 20.75 6.53 7 8 -5 22.46 4.84 -7 -8 4 7.13 5.47 7 8 -4 12.19 4.02 -7 -8 4 5.51 4.86 -7 -8 3 72.75 8.76 7 8 -3 76.07 5.92 7 8 -3 73.74 6.87 -7 -8 3 85.07 8.89 7 8 -2 2.31 3.22 7 8 -2 10.74 4.17 7 8 -1 52.77 5.45 7 8 -1 59.06 15.37 7 8 -1 63.54 6.36 7 8 0 146.64 8.54 7 8 0 155.67 12.43 7 8 0 141.94 9.30 7 8 1 103.61 7.37 7 8 1 107.18 10.18 7 8 1 94.93 7.68 -7 -8 -1 114.23 9.17 7 8 2 20.32 5.71 7 8 2 38.68 10.98 7 8 2 20.26 4.67 -7 -8 -2 25.90 4.74 7 8 3 7.41 4.86 7 8 3 2.61 3.41 -7 -8 -3 4.91 3.41 7 8 4 130.61 10.36 7 8 4 118.21 8.67 -7 -8 -4 136.06 9.29 7 8 5 9.25 4.45 7 8 5 6.46 3.70 -7 -8 -5 6.94 3.24 7 8 6 26.44 5.82 7 8 6 38.93 5.32 -7 -8 -6 24.73 4.48 7 8 7 117.32 12.09 -7 -8 -7 88.87 7.18 -7 -8 -8 224.61 15.28 -7 -8 -8 237.97 12.63 7 8 9 107.57 8.19 -7 -8 -9 113.24 8.11 -7 -8 -10 19.59 4.11 7 8 10 15.18 4.32 7 8 11 144.93 9.38 -7 -8 -11 124.19 9.81 -7 -8 -11 128.52 8.99 7 8 12 245.88 12.45 -7 -8 -12 212.12 12.93 -7 -8 -12 214.23 12.34 -7 -8 -13 -2.92 4.21 -7 -8 -13 7.46 3.93 7 8 13 6.40 3.89 -7 -8 -14 0.71 4.08 7 8 14 6.20 3.96 -7 -8 -14 8.69 4.37 -7 -8 -15 18.09 5.56 7 8 15 23.37 4.73 -7 -8 -15 28.08 5.86 -7 -8 -16 42.35 6.79 -7 -8 -16 45.35 7.37 7 8 16 53.11 6.33 -7 -8 -17 124.61 10.81 7 8 17 190.34 10.74 7 8 18 1.17 4.09 -7 -8 -18 -0.54 5.45 7 8 19 10.70 5.04 -7 -8 -19 4.21 5.43 -7 -8 -20 67.79 8.75 7 8 20 42.83 7.65 -7 -8 -21 158.65 12.99 -7 -8 -22 2.05 5.97 -7 -8 -23 33.53 8.02 -7 -9 11 2.88 7.22 -7 -9 10 5.10 7.07 -7 -9 9 23.18 7.98 -7 -9 8 0.35 6.21 -7 -9 7 0.33 6.05 -7 -9 6 6.87 6.03 7 9 -6 0.30 7.13 -7 -9 5 0.63 5.40 7 9 -5 1.21 5.28 -7 -9 4 134.33 11.35 7 9 -4 128.02 9.69 -7 -9 4 120.24 11.00 7 9 -3 5.77 4.24 -7 -9 3 2.47 4.56 7 9 -2 2.68 3.85 -7 -9 2 1.80 4.28 7 9 -1 5.84 3.03 7 9 -1 3.96 3.61 7 9 -1 -8.28 12.69 7 9 0 4.11 3.24 7 9 0 1.90 3.70 7 9 0 -7.09 12.52 7 9 1 16.86 5.51 7 9 1 10.23 3.76 7 9 1 11.42 4.41 7 9 1 9.51 10.40 7 9 2 14.53 5.66 7 9 2 15.46 4.76 -7 -9 -2 20.23 4.69 7 9 3 0.28 4.28 7 9 3 -0.19 4.04 -7 -9 -3 -0.24 3.35 7 9 4 0.84 4.35 7 9 4 5.08 3.94 -7 -9 -4 6.12 3.41 7 9 5 12.63 5.14 7 9 5 16.60 4.63 -7 -9 -5 10.61 3.98 7 9 6 42.52 6.79 7 9 6 54.22 6.31 -7 -9 -6 49.91 6.07 7 9 7 21.23 5.56 -7 -9 -7 10.62 8.22 7 9 7 39.86 8.84 7 9 7 29.34 5.14 -7 -9 -7 22.33 4.52 -7 -9 -8 -8.30 7.68 7 9 8 5.75 5.81 -7 -9 -8 2.34 3.14 7 9 9 6.98 5.95 -7 -9 -9 3.70 3.26 -7 -9 -10 9.12 3.70 7 9 10 9.25 4.19 -7 -9 -11 2.29 3.31 7 9 11 -3.22 4.48 -7 -9 -11 -5.17 4.74 -7 -9 -12 70.37 8.13 7 9 12 73.46 7.67 -7 -9 -12 74.75 7.48 -7 -9 -13 -5.38 4.73 -7 -9 -13 7.20 4.63 7 9 13 2.40 4.17 -7 -9 -14 3.76 4.52 7 9 14 20.15 5.10 -7 -9 -14 18.42 5.32 -7 -9 -15 48.73 7.42 -7 -9 -15 57.85 7.76 7 9 15 58.33 6.75 -7 -9 -16 -0.91 5.15 7 9 16 8.02 4.74 -7 -9 -16 9.04 5.15 -7 -9 -17 2.20 4.50 7 9 17 3.00 4.73 -7 -9 -17 6.79 5.06 -7 -9 -18 9.97 5.27 7 9 18 4.82 5.14 -7 -9 -19 8.97 5.36 7 9 19 -7.39 6.27 -7 -9 -20 6.20 5.25 -7 -9 -21 56.68 8.48 -7 -9 -22 12.47 6.48 -7 -9 -23 37.96 8.04 -7 -10 10 51.56 10.16 -7 -10 9 18.96 7.65 -7 -10 8 13.96 7.42 -7 -10 7 1.38 6.35 -7 -10 6 3.00 6.27 -7 -10 5 4.50 5.97 7 10 -5 -6.57 8.43 -7 -10 5 2.75 5.75 -7 -10 4 83.79 9.81 7 10 -4 72.96 9.53 -7 -10 4 96.14 10.14 7 10 -3 7.85 5.10 -7 -10 3 12.62 6.07 7 10 -2 9.14 4.97 -7 -10 2 16.24 6.07 7 10 -1 3.01 4.43 -7 -10 1 -1.19 4.37 7 10 0 58.58 5.64 7 10 0 73.54 15.22 7 10 0 64.16 6.98 7 10 1 97.19 7.05 7 10 1 109.15 8.50 7 10 2 4.39 4.09 7 10 2 1.00 3.89 7 10 3 -2.38 4.63 7 10 3 -3.03 4.39 -7 -10 -3 4.28 3.85 7 10 4 59.06 7.82 7 10 4 68.81 7.07 -7 -10 -4 65.48 7.03 7 10 5 13.29 5.38 7 10 5 19.30 4.99 7 10 5 25.42 8.71 -7 -10 -5 16.39 4.69 7 10 6 10.20 5.02 7 10 6 15.59 4.61 7 10 6 21.51 8.17 -7 -10 -6 14.66 4.65 7 10 7 44.06 7.11 7 10 7 62.95 6.98 -7 -10 -7 56.19 6.61 7 10 8 98.08 9.71 -7 -10 -8 124.35 9.34 7 10 9 47.39 8.35 -7 -10 -9 49.29 6.29 -7 -10 -10 1.73 3.33 7 10 10 4.45 3.94 7 10 11 64.38 6.85 -7 -10 -11 51.62 6.46 -7 -10 -12 7.59 4.34 -7 -10 -12 -0.37 5.66 7 10 12 3.85 4.74 -7 -10 -13 35.19 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12.30 4.24 -8 -5 5 101.73 10.48 8 5 -5 117.51 8.39 8 5 -5 119.25 7.09 -8 -5 4 -1.90 5.14 8 5 -4 1.41 3.31 8 5 -4 -6.77 10.92 8 5 -4 -0.91 3.78 8 5 -4 0.39 2.53 8 5 -3 -1.28 3.35 8 5 -3 0.56 3.61 8 5 -3 1.71 2.59 8 5 -2 26.79 4.80 8 5 -2 24.25 4.89 8 5 -2 26.33 3.87 8 5 -1 22.79 4.58 8 5 -1 23.37 4.78 -8 -5 1 22.76 4.89 8 5 -1 28.06 3.91 8 5 0 12.24 4.00 8 5 0 9.12 7.37 8 5 0 14.85 4.48 8 5 0 13.73 3.37 -8 -5 0 19.35 4.52 8 5 1 2.18 3.41 8 5 1 -2.57 6.61 8 5 1 -0.41 3.57 8 5 1 -0.60 2.51 -8 -5 -1 -0.67 2.98 8 5 2 5.99 3.22 8 5 2 3.89 3.59 8 5 2 0.58 5.28 8 5 2 6.48 3.68 8 5 2 6.77 2.85 -8 -5 -2 7.11 3.54 8 5 3 4.13 4.15 8 5 3 3.59 2.98 -8 -5 -3 1.56 5.41 8 5 3 -0.50 5.45 8 5 3 8.91 3.22 -8 -5 -3 4.61 3.26 8 5 4 104.87 9.19 -8 -5 -4 126.79 10.14 8 5 4 105.39 7.44 -8 -5 -4 107.68 7.89 8 5 4 115.92 7.63 8 5 5 69.78 7.83 -8 -5 -5 89.20 7.85 8 5 5 76.66 6.53 -8 -5 -5 80.57 6.55 8 5 5 77.93 6.18 8 5 6 81.35 6.36 -8 -5 -6 94.47 7.46 8 5 6 86.28 7.07 -8 -5 -6 82.90 6.61 -8 -5 -7 6.10 3.31 -8 -5 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6 -4 54.11 5.62 8 6 -4 60.70 6.31 8 6 -4 58.46 6.01 8 6 -3 7.87 3.54 8 6 -3 -4.06 10.42 8 6 -3 4.86 3.78 8 6 -3 6.05 3.35 8 6 -2 -0.48 3.70 8 6 -2 -3.70 10.18 8 6 -2 0.37 3.65 8 6 -2 -0.69 3.13 8 6 -1 3.14 3.67 8 6 -1 2.57 8.71 8 6 -1 -0.78 3.72 8 6 -1 -0.69 2.94 -8 -6 1 0.52 4.28 8 6 0 58.33 6.21 8 6 0 63.71 6.81 8 6 0 62.65 13.51 -8 -6 0 78.73 7.87 8 6 0 69.16 6.33 8 6 1 1.77 3.74 8 6 1 -4.34 7.80 8 6 1 3.61 3.83 8 6 1 5.75 3.33 -8 -6 -1 1.95 3.65 8 6 2 62.22 6.44 8 6 2 66.99 6.87 8 6 2 56.29 11.63 -8 -6 -2 71.84 7.13 8 6 2 72.89 6.44 8 6 3 1.19 6.31 8 6 3 1.23 3.55 8 6 3 4.97 3.27 -8 -6 -3 5.19 3.48 8 6 4 156.51 11.63 -8 -6 -4 131.80 13.62 8 6 4 147.76 10.03 -8 -6 -4 164.51 10.14 8 6 4 162.26 9.43 8 6 4 176.45 9.95 8 6 5 159.91 11.65 8 6 5 163.43 9.45 -8 -6 -5 167.19 12.69 8 6 5 160.32 10.40 -8 -6 -5 174.24 10.18 8 6 6 2.96 2.92 8 6 6 -0.26 4.09 8 6 6 3.26 3.76 -8 -6 -6 2.88 3.91 -8 -6 -6 2.96 2.88 -8 -6 -7 16.32 4.50 -8 -6 -7 10.27 3.24 8 6 8 54.02 6.36 -8 -6 -8 51.91 5.92 -8 -6 -8 50.80 5.27 8 6 9 -1.17 3.55 -8 -6 -9 -3.54 3.05 -8 -6 -9 2.33 3.33 8 6 10 57.03 6.31 -8 -6 -10 63.88 5.66 8 6 11 17.62 4.69 -8 -6 -11 15.20 3.48 8 6 12 9.64 4.21 -8 -6 -12 9.73 3.24 8 6 13 30.07 5.04 -8 -6 -13 30.74 4.43 -8 -6 -13 30.81 5.68 -8 -6 -14 18.16 3.98 8 6 14 25.01 4.89 -8 -6 -14 16.99 5.21 -8 -6 -15 24.08 4.24 8 6 15 24.36 4.91 -8 -6 -15 24.00 5.56 -8 -6 -16 6.05 3.54 8 6 16 2.49 4.09 -8 -6 -16 7.05 4.99 -8 -6 -17 9.32 3.87 8 6 17 18.27 5.04 -8 -6 -17 11.67 5.64 -8 -6 -18 14.12 4.37 8 6 18 20.97 4.82 -8 -6 -18 16.43 6.01 -8 -6 -19 75.66 7.48 -8 -6 -19 80.12 9.17 8 6 19 98.45 7.98 -8 -6 -20 11.29 4.54 8 6 20 16.11 4.86 -8 -6 -20 9.14 5.64 8 6 21 34.16 5.69 -8 -6 -21 30.11 7.26 -8 -6 -22 11.95 6.36 -8 -7 11 -3.16 7.98 -8 -7 10 73.56 11.57 -8 -7 9 327.69 20.62 -8 -7 8 4.99 6.83 8 7 -8 5.17 4.89 -8 -7 7 204.18 15.61 8 7 -7 232.00 12.45 -8 -7 6 113.52 11.76 8 7 -6 129.32 9.06 -8 -7 5 137.94 12.24 8 7 -5 148.10 9.64 -8 -7 4 74.56 9.29 8 7 -4 78.99 7.46 8 7 -4 69.80 16.65 8 7 -3 158.00 9.34 8 7 -3 175.52 10.53 8 7 -2 48.90 5.64 8 7 -2 50.80 6.33 8 7 -1 84.09 7.05 8 7 -1 88.31 7.67 8 7 -1 111.63 17.77 -8 -7 1 117.19 9.94 8 7 0 414.33 17.32 8 7 0 397.79 18.12 -8 -7 0 419.32 20.15 8 7 1 13.29 4.71 8 7 1 27.43 10.66 8 7 1 20.32 4.97 -8 -7 -1 15.43 5.17 8 7 2 722.51 27.13 8 7 2 742.97 28.26 -8 -7 -2 771.00 29.53 8 7 3 30.96 10.33 8 7 3 29.49 5.43 -8 -7 -3 30.72 5.28 8 7 4 116.80 8.95 -8 -7 -4 118.66 8.78 8 7 5 105.95 8.43 -8 -7 -5 99.57 8.04 -8 -7 -6 321.22 19.59 8 7 6 340.53 16.08 -8 -7 -6 328.42 15.46 -8 -7 -7 1.51 4.13 -8 -7 -7 2.66 3.03 -8 -7 -8 39.76 6.12 -8 -7 -8 32.00 4.56 -8 -7 -9 4.02 3.70 8 7 9 -0.61 3.42 -8 -7 -9 -1.08 2.74 8 7 10 2.01 3.65 -8 -7 -10 -0.35 2.85 8 7 11 562.26 22.46 -8 -7 -11 546.28 21.29 8 7 12 209.82 11.87 -8 -7 -12 197.70 10.89 8 7 13 91.81 7.80 -8 -7 -13 79.81 8.28 -8 -7 -13 84.57 6.92 -8 -7 -14 1.73 3.31 8 7 14 -0.58 3.87 -8 -7 -14 4.24 4.61 -8 -7 -15 20.77 4.54 8 7 15 24.56 5.38 -8 -7 -15 24.79 5.95 -8 -7 -16 29.27 5.21 8 7 16 23.52 5.56 -8 -7 -16 29.94 6.40 -8 -7 -17 69.68 8.52 8 7 17 52.70 7.18 -8 -7 -17 56.99 6.92 -8 -7 -18 23.95 5.40 8 7 18 22.57 5.45 -8 -7 -18 28.12 6.94 -8 -7 -19 9.04 4.73 8 7 19 22.81 5.38 -8 -7 -19 18.42 6.51 -8 -7 -20 -1.53 4.58 8 7 20 5.34 4.73 -8 -7 -20 0.86 5.45 -8 -7 -21 18.05 5.64 8 7 21 32.06 6.21 -8 -7 -21 18.91 6.96 -8 -7 -22 41.33 8.04 -8 -8 10 7.16 7.20 -8 -8 9 174.76 15.26 -8 -8 8 50.22 9.49 -8 -8 7 192.79 15.80 8 8 -7 260.15 13.94 -8 -8 6 3.93 6.05 8 8 -6 6.64 4.86 -8 -8 5 158.33 13.19 8 8 -5 133.34 23.43 8 8 -5 174.33 10.79 8 8 -4 1.38 4.11 8 8 -4 -6.70 11.93 8 8 -3 207.32 25.88 8 8 -3 164.08 10.64 8 8 -2 75.40 6.53 8 8 -2 79.03 7.50 8 8 -2 96.57 18.81 8 8 -1 74.06 6.75 8 8 -1 76.59 7.20 -8 -8 1 90.84 9.17 8 8 0 274.29 13.40 8 8 0 297.18 14.64 -8 -8 0 296.66 16.49 8 8 1 131.20 9.01 8 8 1 151.17 10.14 -8 -8 -1 144.39 10.94 8 8 2 546.65 22.07 8 8 2 573.18 23.35 -8 -8 -2 601.41 24.93 8 8 3 375.93 17.88 -8 -8 -3 397.36 18.87 8 8 4 154.93 10.53 -8 -8 -4 147.18 10.48 -8 -8 -5 4.89 9.94 8 8 5 18.61 4.93 -8 -8 -5 15.48 4.32 8 8 6 256.84 13.40 -8 -8 -6 243.63 13.04 8 8 7 81.46 7.80 -8 -8 -7 80.42 7.33 -8 -8 -8 18.03 5.81 -8 -8 -8 20.15 4.30 -8 -8 -9 9.49 4.84 8 8 9 6.75 4.17 -8 -8 -9 8.97 3.70 8 8 10 4.39 4.04 -8 -8 -10 -1.80 3.41 8 8 11 713.46 26.66 -8 -8 -11 682.84 26.12 8 8 12 786.96 28.71 -8 -8 -12 761.99 28.45 8 8 13 115.40 8.76 -8 -8 -13 118.19 9.73 -8 -8 -13 106.77 8.52 8 8 14 162.70 10.31 -8 -8 -14 141.64 9.84 -8 -8 -15 16.47 4.93 8 8 15 18.33 4.89 -8 -8 -15 25.73 6.03 -8 -8 -16 0.24 4.04 8 8 16 2.42 4.32 -8 -8 -16 0.82 5.06 8 8 17 57.03 6.85 -8 -8 -17 43.86 6.68 -8 -8 -17 36.54 7.24 -8 -8 -18 19.95 5.56 8 8 18 25.21 5.43 -8 -8 -18 19.46 6.40 -8 -8 -19 -2.81 4.82 8 8 19 3.20 4.54 -8 -8 -19 -3.85 5.95 -8 -8 -20 21.08 6.40 8 8 20 42.72 6.83 -8 -8 -20 28.02 7.54 -8 -8 -21 61.50 8.76 -8 -8 -21 78.36 10.23 -8 -8 -22 61.85 9.47 8 8 22 45.57 8.63 -8 -9 9 16.15 7.80 -8 -9 8 42.87 9.25 -8 -9 7 6.75 6.55 -8 -9 6 6.12 6.48 8 9 -6 7.00 5.75 -8 -9 5 5.90 6.07 8 9 -5 11.96 5.40 8 9 -4 5.12 4.76 8 9 -4 8.69 12.58 8 9 -3 60.06 17.03 8 9 -3 56.36 6.96 8 9 -2 22.29 5.15 8 9 -2 16.88 12.84 8 9 -1 1.43 4.09 8 9 -1 -2.75 11.11 8 9 0 2.92 3.44 8 9 0 4.74 4.17 8 9 0 2.51 9.75 -8 -9 0 2.08 4.50 8 9 1 156.54 9.49 8 9 1 164.60 10.74 -8 -9 -1 152.21 11.57 8 9 2 25.47 4.86 8 9 2 18.81 5.25 8 9 2 27.89 12.08 -8 -9 -2 20.24 5.45 8 9 3 306.07 15.65 -8 -9 -3 298.74 16.24 8 9 4 2.38 4.24 -8 -9 -4 -2.49 4.06 8 9 5 25.96 5.58 -8 -9 -5 24.90 5.34 8 9 6 50.31 6.48 -8 -9 -6 38.28 5.84 8 9 7 9.66 4.50 -8 -9 -7 -3.13 9.17 8 9 7 14.59 7.41 -8 -9 -7 9.77 3.85 -8 -9 -8 12.00 7.57 8 9 8 34.85 8.71 -8 -9 -8 26.92 5.06 -8 -9 -9 69.33 10.07 -8 -9 -9 97.28 8.02 8 9 10 8.09 4.45 -8 -9 -10 1.79 3.48 8 9 11 5.88 4.41 -8 -9 -11 4.84 3.83 8 9 12 571.12 22.91 -8 -9 -12 531.48 22.85 -8 -9 -13 46.72 7.54 8 9 13 66.86 7.22 -8 -9 -13 52.66 6.83 -8 -9 -14 269.16 16.17 -8 -9 -14 289.23 15.61 -8 -9 -15 4.04 4.48 8 9 15 6.18 4.65 -8 -9 -15 6.29 5.04 -8 -9 -16 0.86 4.67 8 9 16 2.75 4.43 -8 -9 -16 5.08 4.88 -8 -9 -17 29.79 6.36 8 9 17 34.27 6.20 -8 -9 -17 40.66 7.24 -8 -9 -18 39.78 7.28 -8 -9 -18 40.56 7.41 -8 -9 -19 2.23 5.01 8 9 19 5.01 5.14 -8 -9 -19 5.19 5.06 -8 -9 -20 6.27 5.77 8 9 20 12.19 6.03 -8 -9 -20 14.90 6.55 -8 -9 -21 48.86 8.58 -8 -9 -21 67.15 9.29 8 9 21 46.00 8.58 -8 -9 -22 -3.70 5.95 -8 -9 -22 7.67 6.66 -8 -10 9 58.95 10.61 -8 -10 8 50.13 9.64 -8 -10 7 19.98 7.78 -8 -10 6 45.90 8.82 8 10 -6 20.65 8.58 8 10 -5 7.48 6.75 8 10 -4 10.46 13.06 8 10 -4 29.38 6.72 -8 -10 4 19.11 7.09 8 10 -3 5.51 5.28 8 10 -3 -5.97 13.45 -8 -10 3 1.71 5.64 8 10 -2 21.90 5.79 8 10 -2 32.17 14.46 8 10 -1 4.15 4.39 8 10 -1 -8.88 12.84 8 10 0 20.62 5.27 8 10 0 26.20 12.32 8 10 1 2.61 4.26 8 10 1 5.90 10.49 -8 -10 -1 2.66 4.58 8 10 2 70.91 6.74 8 10 2 103.25 16.21 8 10 2 87.90 8.21 -8 -10 -2 85.85 8.80 8 10 3 80.44 8.02 -8 -10 -3 78.80 8.17 8 10 4 0.89 4.34 -8 -10 -4 -3.16 4.43 8 10 5 15.13 5.28 -8 -10 -5 16.37 4.97 8 10 6 53.63 10.76 8 10 6 48.90 6.81 -8 -10 -6 41.68 6.18 8 10 7 5.51 4.52 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7.15 10 9 6 132.82 10.76 -10 -9 -6 113.34 9.79 10 9 7 204.64 13.10 -10 -9 -7 186.80 12.08 10 9 8 119.03 10.33 -10 -9 -8 94.86 8.69 -10 -9 -9 308.60 22.27 -10 -9 -9 405.60 18.53 -10 -9 -10 3.41 6.72 10 9 10 12.15 5.68 -10 -9 -10 10.12 4.67 10 9 11 46.18 7.22 -10 -9 -11 37.07 8.11 -10 -9 -11 48.64 6.72 10 9 12 96.26 9.21 -10 -9 -12 99.16 10.74 -10 -9 -12 89.84 8.34 -10 -9 -13 38.41 7.72 10 9 13 35.24 6.66 -10 -9 -13 31.02 5.75 10 9 14 8.91 5.40 -10 -9 -14 14.89 4.86 10 9 15 35.02 6.64 -10 -9 -15 29.86 5.92 -10 -9 -16 9.86 5.95 10 9 16 1.90 4.88 -10 -9 -16 -3.13 4.60 -10 -9 -17 124.32 11.91 10 9 17 120.22 10.42 -10 -9 -17 120.09 9.94 -10 -9 -18 451.01 23.05 -10 -9 -18 420.90 20.26 10 9 19 8.88 5.90 -10 -9 -19 9.86 6.44 -10 -9 -19 3.63 4.76 10 9 20 140.41 10.89 10 9 21 10.22 5.88 10 9 22 0.50 5.77 10 10 -4 15.39 6.31 10 10 -3 20.08 6.20 10 10 -2 36.75 7.15 10 10 -2 41.90 16.02 10 10 -1 13.25 5.99 10 10 -1 15.17 13.49 -10 -10 1 12.60 6.49 10 10 0 5.04 5.66 -10 -10 0 1.75 5.84 10 10 1 15.13 5.94 10 10 1 17.94 13.75 -10 -10 -1 6.14 5.68 10 10 2 16.13 6.10 10 10 2 26.61 13.53 -10 -10 -2 19.00 6.75 10 10 3 110.51 10.36 -10 -10 -3 126.38 11.35 10 10 4 6.07 5.51 10 10 4 4.93 11.35 -10 -10 -4 8.28 5.41 10 10 5 0.26 5.19 -10 -10 -5 -2.68 4.78 10 10 6 0.26 5.41 -10 -10 -6 -5.71 4.54 10 10 7 82.43 9.14 -10 -10 -7 61.76 7.93 10 10 8 20.41 6.49 10 10 8 35.11 10.70 -10 -10 -8 20.06 5.49 -10 -10 -9 26.96 12.26 -10 -10 -9 90.84 8.84 -10 -10 -10 7.91 4.86 10 10 11 15.65 6.03 -10 -10 -11 -4.47 8.48 -10 -10 -11 0.78 4.78 10 10 12 58.35 7.95 -10 -10 -12 33.64 9.02 -10 -10 -12 37.40 6.74 -10 -10 -13 -0.41 6.46 10 10 13 5.90 5.40 -10 -10 -13 0.26 4.73 10 10 14 36.40 7.20 -10 -10 -14 32.30 6.33 10 10 15 32.23 7.11 -10 -10 -15 38.05 6.77 -10 -10 -16 -0.37 5.95 10 10 16 0.24 4.99 -10 -10 -16 -0.56 4.58 -10 -10 -17 0.37 6.66 10 10 17 1.73 5.01 -10 -10 -17 3.74 4.86 -10 -10 -18 171.75 14.66 10 10 18 174.18 12.09 -10 -10 -18 133.01 11.78 10 10 19 36.08 7.18 -10 -10 -19 30.70 6.90 10 10 20 67.19 8.80 10 10 21 7.70 6.40 10 10 22 2.29 6.70 10 11 -4 -0.97 6.83 10 11 -3 58.26 9.04 10 11 -2 98.12 10.07 10 11 -1 15.67 6.46 10 11 0 42.74 8.06 10 11 0 66.50 16.99 -10 -11 0 55.41 8.84 10 11 1 3.70 5.77 10 11 1 21.27 14.03 -10 -11 -1 3.93 5.86 10 11 2 6.94 5.68 10 11 2 3.89 11.87 -10 -11 -2 -1.38 5.82 10 11 3 25.31 6.81 10 11 3 27.82 12.84 -10 -11 -3 13.96 6.10 10 11 4 8.48 5.92 -10 -11 -4 2.59 5.08 10 11 5 3.59 5.45 -10 -11 -5 -1.25 4.76 10 11 6 13.12 6.18 -10 -11 -6 5.47 4.82 10 11 7 36.28 7.29 10 11 7 46.16 11.18 -10 -11 -7 24.52 6.07 10 11 8 108.78 14.20 10 11 8 87.53 9.55 -10 -11 -8 76.96 8.71 10 11 9 80.64 9.49 -10 -11 -9 73.85 8.58 -10 -11 -10 -17.53 12.34 -10 -11 -10 -0.28 4.28 10 11 11 -3.31 5.66 -10 -11 -11 -4.91 5.08 10 11 12 10.92 6.03 -10 -11 -12 9.94 5.28 10 11 13 1.62 5.36 -10 -11 -13 -5.79 8.86 -10 -11 -13 3.48 4.89 10 11 14 9.06 5.90 -10 -11 -14 6.27 5.19 10 11 15 15.93 6.27 -10 -11 -15 16.56 6.07 10 11 16 25.83 6.62 -10 -11 -16 14.42 7.65 -10 -11 -16 17.17 6.20 -10 -11 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0.00 8 8 21 1.04 0.00 -2 9 21 -0.03 0.00 -1 9 21 -0.11 0.00 0 9 21 -0.08 0.00 1 9 21 0.58 0.00 2 9 21 -0.67 0.00 3 9 21 -0.03 0.00 4 9 21 1.01 0.00 5 9 21 -1.34 0.00 6 9 21 0.65 0.00 7 9 21 0.58 0.00 -1 10 21 0.08 0.00 0 10 21 -0.24 0.00 1 10 21 -0.42 0.00 2 10 21 1.20 0.00 3 10 21 -0.91 0.00 4 10 21 -0.42 0.00 5 10 21 1.46 0.00 6 10 21 -1.14 0.00 7 10 21 -0.16 0.00 -1 11 21 0.20 0.00 0 11 21 0.59 0.00 1 11 21 -0.32 0.00 2 11 21 -1.05 0.00 3 11 21 1.82 0.00 4 11 21 -0.85 0.00 5 11 21 -0.81 0.00 6 11 21 1.37 0.00 0 12 21 -0.49 0.00 1 12 21 1.11 0.00 4 12 21 2.28 0.00 5 12 21 -0.58 0.00 1 13 21 -1.43 0.00 2 13 21 0.89 0.00 3 13 21 1.51 0.00 4 13 21 -3.06 0.00 2 3 22 -0.21 0.00 3 3 22 0.05 0.00 4 3 22 0.62 0.00 5 3 22 -1.05 0.00 1 4 22 1.16 0.00 2 4 22 -0.13 0.00 3 4 22 -0.22 0.00 4 4 22 -0.48 0.00 5 4 22 1.37 0.00 6 4 22 -1.66 0.00 0 5 22 1.83 0.00 1 5 22 -1.68 0.00 2 5 22 0.67 0.00 3 5 22 0.11 0.00 4 5 22 0.26 0.00 5 5 22 -1.28 0.00 6 5 22 1.83 0.00 0 6 22 -1.33 0.00 1 6 22 1.59 0.00 2 6 22 -1.05 0.00 3 6 22 0.26 0.00 4 6 22 -0.21 0.00 5 6 22 0.93 0.00 6 6 22 -1.46 0.00 0 7 22 0.53 0.00 1 7 22 -0.93 0.00 2 7 22 0.95 0.00 3 7 22 -0.62 0.00 4 7 22 0.45 0.00 5 7 22 -0.69 0.00 6 7 22 0.86 0.00 0 8 22 0.09 0.00 1 8 22 0.10 0.00 2 8 22 -0.39 0.00 3 8 22 0.66 0.00 4 8 22 -0.82 0.00 5 8 22 0.81 0.00 6 8 22 -0.51 0.00 0 9 22 -0.22 0.00 1 9 22 0.37 0.00 2 9 22 -0.32 0.00 3 9 22 -0.21 0.00 4 9 22 0.90 0.00 5 9 22 -1.14 0.00 6 9 22 0.63 0.00 1 10 22 -0.24 0.00 2 10 22 0.70 0.00 3 10 22 -0.56 0.00 4 10 22 -0.36 0.00 5 10 22 1.18 0.00 2 11 22 -0.50 0.00 3 11 22 1.20 0.00 4 11 22 -0.70 0.00 0 1 0 -26.62 0.00 13 4 0 0.32 0.00 -13 6 0 1.11 0.00 -12 9 0 -0.45 0.00 -11 11 0 1.51 0.00 10 11 0 -0.75 0.00 6 15 0 0.93 0.00 -3 17 0 0.20 0.00 1 17 0 0.03 0.00 5 -16 1 -0.54 0.00 7 -15 1 -0.65 0.00 12 -9 1 -0.61 0.00 13 -6 1 1.22 0.00 -13 -3 1 0.58 0.00 0 0 1 30.51 0.00 -1 1 1 8.29 0.00 0 1 1 -24.45 0.00 13 5 1 -0.79 0.00 -12 9 1 -0.19 0.00 -11 11 1 1.30 0.00 -6 16 1 0.43 0.00 5 16 1 -0.43 0.00 -4 17 1 -1.12 0.00 -2 -16 2 0.31 0.00 -6 -14 2 -0.83 0.00 8 -14 2 -0.64 0.00 10 -12 2 0.93 0.00 -11 -8 2 -0.31 0.00 -13 -2 2 -1.33 0.00 -13 5 2 -0.98 0.00 -11 11 2 0.96 0.00 9 13 2 -0.56 0.00 8 14 2 0.04 0.00 7 15 2 -0.37 0.00 0 -16 3 -0.64 0.00 3 -16 3 -0.83 0.00 6 -15 3 0.02 0.00 13 -6 3 1.33 0.00 -13 0 3 -0.60 0.00 -13 1 3 -0.28 0.00 -13 3 3 -1.15 0.00 -13 4 3 0.99 0.00 6 16 3 0.08 0.00 -1 18 3 1.34 0.00 0 18 3 -1.22 0.00 5 -15 4 0.92 0.00 7 -14 4 0.36 0.00 -6 -13 4 0.34 0.00 -9 -10 4 -0.50 0.00 13 -6 4 1.29 0.00 14 0 4 0.60 0.00 14 1 4 -0.67 0.00 -12 8 4 -0.97 0.00 11 11 4 0.19 0.00 -5 17 4 2.06 0.00 -2 18 4 0.44 0.00 2 18 4 0.44 0.00 -1 -15 5 -0.25 0.00 8 -13 5 0.44 0.00 10 -11 5 0.35 0.00 12 -8 5 -0.59 0.00 14 0 5 0.46 0.00 14 1 5 -0.24 0.00 14 2 5 0.18 0.00 13 7 5 -1.14 0.00 9 14 5 -0.42 0.00 8 15 5 -0.34 0.00 -12 -1 6 -0.97 0.00 14 0 6 0.25 0.00 14 1 6 0.23 0.00 14 2 6 -0.35 0.00 -12 6 6 -0.84 0.00 -11 10 6 0.44 0.00 -10 12 6 0.05 0.00 -1 12 6 -4.39 0.00 -1 13 6 4.44 0.00 10 13 6 0.49 0.00 7 16 6 -0.06 0.00 -3 18 6 -2.66 0.00 3 18 6 -0.75 0.00 0 -14 7 -0.45 0.00 4 -14 7 -0.13 0.00 8 -12 7 0.16 0.00 -6 -11 7 0.19 0.00 -8 -9 7 0.03 0.00 11 -9 7 -0.25 0.00 13 -5 7 -0.12 0.00 -11 -3 7 0.17 0.00 14 1 7 0.67 0.00 -12 2 7 -0.89 0.00 14 2 7 -0.82 0.00 -12 3 7 1.32 0.00 -12 4 7 -1.24 0.00 12 10 7 0.35 0.00 -3 18 7 -2.78 0.00 -2 18 7 2.51 0.00 -1 18 7 -1.35 0.00 -8 -8 8 0.51 0.00 -2 11 8 -5.28 0.00 11 12 8 1.15 0.00 -9 13 8 -0.10 0.00 -3 14 8 1.64 0.00 -3 16 8 -0.34 0.00 -2 16 8 0.01 0.00 -5 17 8 0.89 0.00 6 17 8 0.36 0.00 -3 18 8 -2.69 0.00 4 18 8 0.35 0.00 1 -13 9 -0.18 0.00 2 -13 9 0.44 0.00 3 -13 9 -0.45 0.00 8 -11 9 -0.18 0.00 12 -6 9 0.92 0.00 -11 7 9 -0.15 0.00 11 12 9 1.07 0.00 -8 14 9 -0.45 0.00 -3 15 9 -1.21 0.00 -4 16 9 -0.33 0.00 -3 16 9 -0.34 0.00 -5 17 9 0.31 0.00 -4 17 9 -0.99 0.00 -3 18 9 -2.41 0.00 4 18 9 0.52 0.00 3 -12 10 0.04 0.00 5 -12 10 0.50 0.00 -3 -11 10 -0.75 0.00 7 -11 10 -0.30 0.00 -8 -6 10 0.37 0.00 13 -3 10 0.34 0.00 12 10 10 -0.03 0.00 -9 12 10 -0.01 0.00 11 12 10 0.88 0.00 -4 14 10 -2.09 0.00 -7 15 10 -1.00 0.00 -6 16 10 -1.02 0.00 4 18 10 0.80 0.00 9 -9 11 0.12 0.00 -8 -5 11 0.26 0.00 -9 -3 11 -0.16 0.00 13 -2 11 0.76 0.00 13 7 11 -0.68 0.00 -10 8 11 0.07 0.00 12 10 11 -0.16 0.00 11 12 11 0.64 0.00 -6 15 11 2.19 0.00 -2 18 11 3.16 0.00 4 18 11 1.10 0.00 2 -11 12 -0.17 0.00 8 -9 12 0.27 0.00 10 -7 12 -0.01 0.00 -9 -1 12 0.54 0.00 13 6 12 0.75 0.00 -9 10 12 -0.48 0.00 -7 14 12 1.26 0.00 -4 17 12 0.81 0.00 6 17 12 1.11 0.00 4 18 12 1.32 0.00 1 -10 13 0.67 0.00 4 -10 13 0.21 0.00 -2 -9 13 0.53 0.00 -7 -4 13 0.53 0.00 -8 -2 13 -0.20 0.00 -9 1 13 0.97 0.00 13 2 13 -0.30 0.00 13 3 13 0.35 0.00 13 4 13 0.04 0.00 13 5 13 -0.54 0.00 4 13 13 1.54 0.00 -1 18 13 -3.84 0.00 3 18 13 -0.45 0.00 5 -9 14 0.09 0.00 -2 -8 14 -0.09 0.00 7 -8 14 0.40 0.00 -8 0 14 0.51 0.00 10 13 14 0.88 0.00 -6 14 14 -1.35 0.00 7 16 14 0.18 0.00 1 18 14 -1.07 0.00 2 18 14 -0.76 0.00 5 -8 15 -0.01 0.00 -2 -7 15 -0.19 0.00 12 0 15 0.65 0.00 -8 3 15 -0.44 0.00 -8 8 15 -1.47 0.00 12 8 15 0.09 0.00 5 13 15 -1.11 0.00 9 14 15 0.34 0.00 8 15 15 -0.96 0.00 -2 17 15 -1.42 0.00 5 17 15 1.39 0.00 5 -7 16 0.22 0.00 -3 -5 16 0.66 0.00 -4 -4 16 0.17 0.00 10 -3 16 0.50 0.00 -6 -1 16 0.75 0.00 11 -1 16 0.10 0.00 -7 2 16 -0.46 0.00 12 3 16 0.76 0.00 12 4 16 -1.06 0.00 12 5 16 0.93 0.00 12 6 16 -0.54 0.00 11 10 16 -0.21 0.00 -6 12 16 0.67 0.00 5 12 16 1.72 0.00 10 12 16 -0.75 0.00 5 13 16 -0.65 0.00 5 14 16 -0.43 0.00 -4 15 16 0.69 0.00 6 16 16 -0.04 0.00 4 17 16 -0.96 0.00 1 -6 17 -0.18 0.00 5 -6 17 -0.57 0.00 7 -5 17 0.21 0.00 -5 -1 17 -0.81 0.00 4 12 17 0.96 0.00 -4 14 17 0.90 0.00 5 14 17 -1.44 0.00 8 14 17 0.33 0.00 -3 15 17 1.11 0.00 7 15 17 -0.49 0.00 2 -5 18 0.10 0.00 3 -5 18 -0.15 0.00 4 -5 18 -0.13 0.00 -2 -3 18 -1.43 0.00 8 -3 18 0.11 0.00 -3 -2 18 -0.41 0.00 10 0 18 -0.66 0.00 11 4 18 0.05 0.00 11 5 18 0.10 0.00 -6 6 18 -0.02 0.00 11 6 18 -0.12 0.00 10 10 18 0.69 0.00 -5 11 18 0.67 0.00 9 12 18 0.14 0.00 -4 13 18 -1.67 0.00 5 13 18 0.83 0.00 6 13 18 1.10 0.00 -3 14 18 -2.31 0.00 -2 15 18 -2.56 0.00 6 15 18 -0.65 0.00 0 16 18 1.15 0.00 4 16 18 1.53 0.00 0 -3 19 -0.86 0.00 6 -3 19 -0.46 0.00 -3 0 19 0.20 0.00 9 0 19 0.09 0.00 -5 6 19 -0.10 0.00 -5 7 19 0.05 0.00 10 8 19 0.40 0.00 -4 11 19 -0.83 0.00 2 11 19 -2.39 0.00 9 11 19 0.72 0.00 -2 14 19 2.94 0.00 6 14 19 0.35 0.00 5 15 19 3.33 0.00 2 -2 20 -0.90 0.00 5 -2 20 0.38 0.00 9 9 20 1.53 0.00 -3 11 20 0.84 0.00 2 11 20 -1.72 0.00 6 13 20 0.32 0.00 0 14 20 0.46 0.00 5 14 20 -3.17 0.00 1 0 21 -0.31 0.00 5 0 21 0.15 0.00 0 1 21 -0.65 0.00 -1 2 21 0.50 0.00 8 3 21 1.42 0.00 -2 4 21 -1.57 0.00 8 9 21 -1.40 0.00 -2 10 21 0.25 0.00 7 11 21 -0.46 0.00 2 12 21 0.22 0.00 3 12 21 -2.11 0.00 6 12 21 -0.93 0.00 5 13 21 2.12 0.00 2 2 22 0.19 0.00 3 2 22 0.24 0.00 4 2 22 -0.57 0.00 1 3 22 -0.41 0.00 6 3 22 1.09 0.00 0 4 22 -1.70 0.00 7 5 22 -1.65 0.00 7 6 22 1.29 0.00 -1 7 22 -0.17 0.00 7 7 22 -0.58 0.00 7 8 22 -0.09 0.00 0 10 22 -0.01 0.00 6 10 22 -1.00 0.00 1 11 22 -0.30 0.00 5 11 22 -0.54 0.00 3 12 22 -1.30 0.00 3 6 23 0.30 0.00 3 7 23 -0.67 0.00 4 7 23 0.35 0.00 3 8 23 0.70 0.00 4 8 23 -0.74 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 140621) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.500 0.500 0.000 62 25 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 0 1 0 1.418 0 0 1 1.181 -1 1 1 2.455 0 1 1 1.453 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL a P -1 R = 0.06 CELL 11.7109 15.5844 19.2261 67.38 76.55 87.84 SPGR P-1 # Solvent Accessible Volume = 62 # Electrons Found in S.A.V. = 24 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others Q101 0.013 0.490 0.097 ! 4.70 eA-3 Q102 0.654 0.633 0.097 ! 4.18 eA-3 Q103 0.250 0.645 0.042 ! 3.76 eA-3 Q104 0.580 0.657 0.123 ! 3.64 eA-3 Q105 0.631 0.319 0.307 ! 3.50 eA-3 Q106 0.781 0.586 0.267 ! 3.40 eA-3 Q107 0.448 0.757 0.300 ! 3.19 eA-3 Q108 1.000 0.500 0.000 ! 3.16 eA-3 Q109 0.578 0.537 0.467 ! 3.07 eA-3 Q110 0.732 0.623 0.153 ! 3.06 eA-3 Q111 0.615 0.664 0.443 ! 2.97 eA-3 Q112 0.685 0.778 0.247 ! 2.91 eA-3 Q113 0.763 0.287 0.157 ! 2.89 eA-3 C114 0.563 0.439-0.007 ! 2.87 eA-3 Q115 0.217 0.597 0.422 ! 2.78 eA-3 Q116 0.762 0.737 0.203 ! 2.77 eA-3 Q117 0.329 0.687 0.284 ! 2.75 eA-3 Q118 0.702 0.755 0.219 ! 2.74 eA-3 Q119 0.563 0.341 0.340 ! 2.67 eA-3 Q120 0.595 0.361 0.370 ! 2.61 eA-3 Q121 1.000 1.000 0.500 ! 2.57 eA-3 Q122 0.343 0.840 0.323 ! 2.56 eA-3 Q123 0.655 0.594 0.181 ! 2.53 eA-3 Q124 0.858 0.543 0.312 ! 2.51 eA-3 Q125 0.486 0.368 0.368 ! 2.47 eA-3 Q126 0.408 0.702 0.297 ! 2.46 eA-3 Q127 0.364 0.766 0.293 ! 2.44 eA-3 Q128 0.686 0.422 0.441 ! 2.41 eA-3 Q129 0.456 0.803 0.375 ! 2.38 eA-3 Q130 0.625 0.720 0.190 ! 2.37 eA-3 Q131 0.437 0.422 0.345 ! 2.35 eA-3 Q132 0.282 0.548 0.338 ! 2.32 eA-3 Q133 0.095 0.880 0.362 ! 2.31 eA-3 Q134 0.904 0.944 0.259 ! 2.29 eA-3 Q135 0.294 0.694 0.218 ! 2.29 eA-3 Q136 0.403 0.773 0.329 ! 2.28 eA-3 Q137 0.468 0.688 0.341 ! 2.28 eA-3 Q138 0.673 0.416 0.125 ! 2.27 eA-3 Q139 1.003 0.571 0.045 ! 2.26 eA-3 Q140 0.282 0.623 0.468 ! 2.25 eA-3 Q141 0.388 0.546 0.345 ! 2.24 eA-3 Q142 0.689 0.621 0.433 ! 2.22 eA-3 Q143 0.906 0.673 0.377 ! 2.22 eA-3 Q144 0.655 0.644 0.221 ! 2.22 eA-3 Q145 0.203 0.632 0.444 ! 2.19 eA-3 Q146 0.421 0.674 0.365 ! 2.18 eA-3 Q147 0.300 0.368 0.418 ! 2.16 eA-3 Q148 0.264 0.816 0.175 ! 2.14 eA-3 Q149 0.407 0.645 0.270 ! 2.13 eA-3 Q150 0.092 0.409 0.185 ! 2.13 eA-3 Q151 0.091 0.613 0.408 ! 2.09 eA-3 Q152 0.049 0.763 0.476 ! 2.09 eA-3 Q153 0.811 0.493 0.045 ! 2.09 eA-3 Q154 0.203 0.236 0.472 ! 2.07 eA-3 Q155 0.531 0.313 0.300 ! 2.06 eA-3 Q156 0.688 0.626 0.235 ! 2.06 eA-3 Q157 0.640 0.660 0.180 ! 2.04 eA-3 Q158 0.749 0.417 0.479 ! 2.03 eA-3 Q159 0.751 0.520 0.437 ! 2.03 eA-3 Q160 0.734 0.513 0.206 ! 2.02 eA-3 Q161 0.453 0.327 0.265 ! 2.01 eA-3 Q162 0.798 0.047 0.302 ! 2.00 eA-3 Q163 0.716 0.303 0.295 ! 1.99 eA-3 Q164 0.688 0.326 0.462 ! 1.98 eA-3 Q165 0.278 0.562 0.382 ! 1.98 eA-3 Q166 0.329 0.368 0.466 ! 1.97 eA-3 Q167 0.561 0.790 0.413 ! 1.97 eA-3 Q168 0.534 0.743 0.286 ! 1.97 eA-3 Q169 0.826 0.733 0.172 ! 1.97 eA-3 Q170 0.285 0.340 0.443 ! 1.97 eA-3 Q171 0.778 0.797 0.249 ! 1.97 eA-3 Q172 0.172 0.580 0.380 ! 1.96 eA-3 Q173 0.156 0.690 0.286 ! 1.95 eA-3 Q174 0.531 0.640 0.449 ! 1.94 eA-3 Q175 0.122 0.589 0.077 ! 1.94 eA-3 Q176 0.253 0.411 0.435 ! 1.93 eA-3 Q177 0.186 0.408 0.455 ! 1.93 eA-3 Q178 0.097 0.589 0.045 ! 1.93 eA-3 Q179 0.156 0.419-0.009 ! 1.93 eA-3 Q180 0.765 0.484 0.500 ! 1.92 eA-3 Q181 0.265 0.419 0.363 ! 1.91 eA-3 Q182 0.705 0.393 0.501 ! 1.91 eA-3 Q183 0.609 0.817 0.238 ! 1.89 eA-3 Q184 0.561 0.347 0.240 ! 1.89 eA-3 Q185 0.452 0.392 0.225 ! 1.89 eA-3 Q186 0.845 0.755 0.221 ! 1.89 eA-3 Q187 0.593 0.669 0.158 ! 1.88 eA-3 Q188 0.983 0.826 0.285 ! 1.88 eA-3 Q189 0.205 0.547 0.406 ! 1.88 eA-3 Q190 0.878 0.296 0.422 ! 1.88 eA-3 Q191 0.420 0.458 0.288 ! 1.87 eA-3 Q192 0.921 0.601 0.256 ! 1.87 eA-3 Q193 0.669 0.364 0.103 ! 1.86 eA-3 Q194 0.171 0.665 0.340 ! 1.86 eA-3 Q195 0.907 0.501 0.155 ! 1.86 eA-3 Q196 0.157 0.223 0.295 ! 1.86 eA-3 Q197 0.065 0.434 0.297 ! 1.86 eA-3 Q198 0.376 0.449 0.238 ! 1.86 eA-3 Q199 0.675 0.343 0.417 ! 1.84 eA-3 ) ; _shelx_fab_checksum 881 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group W6 W 0.60231(6) 0.22112(5) 0.67463(4) 0.0249(2) Uani 1 1 d . . . . . W1 W 0.7912(5) 0.4067(5) 0.5778(4) 0.0179(7) Uani 0.75(2) 1 d . . P A 2 W5 W 0.29828(6) 0.24562(5) 0.77832(4) 0.0270(2) Uani 1 1 d . . . . . W2 W 0.7044(5) 0.6419(4) 0.5715(3) 0.0203(7) Uani 0.75(2) 1 d . . P A 2 W7 W 0.71115(10) 0.32018(7) 0.77455(6) 0.0258(3) Uani 0.93 1 d . U P A 1 W7A W 0.6741(10) 0.3306(8) 0.7917(6) 0.007(3) Uani 0.07 1 d . U P A 2 W4 W 0.21797(7) 0.46040(6) 0.76080(4) 0.0315(2) Uani 1 1 d . . . . . W8 W 0.6267(7) 0.5538(6) 0.7677(3) 0.0246(8) Uani 0.63 1 d . . P A 1 W8A W 0.6018(13) 0.5574(10) 0.7689(7) 0.044(3) Uani 0.37 1 d . . P A . W9 W 0.40566(7) 0.35082(5) 0.87312(4) 0.0315(2) Uani 1 1 d . . . . . W3 W 0.42693(7) 0.66543(5) 0.65960(4) 0.0328(2) Uani 1 1 d . . . . . Ge1 Ge 0.50187(15) 0.44331(12) 0.66266(10) 0.0208(4) Uani 1 1 d . . . . . Zn3 Zn 0.75154(18) 0.83480(15) 0.77381(12) 0.0299(5) Uani 1 1 d . . . . . O5 O 0.3019(9) 0.2928(8) 0.6673(6) 0.021(3) Uani 1 1 d . . . . . O3 O 0.3855(10) 0.6515(7) 0.5817(6) 0.019(2) Uani 1 1 d . U . . . O27 O 0.5531(10) 0.3041(8) 0.8395(6) 0.022(3) Uani 1 1 d . . . . . O24 O 0.6796(10) 0.2131(7) 0.7583(6) 0.022(3) Uani 1 1 d . . . . . O51 O 0.1108(11) 0.3895(10) 0.5948(8) 0.046(4) Uani 1 1 d . . . . . O23 O 0.3351(11) 0.2394(7) 0.8707(6) 0.023(3) Uani 1 1 d . . . . . O16 O 0.4556(9) 0.2107(8) 0.7457(6) 0.021(3) Uani 1 1 d . . . . . O4 O 0.2205(10) 0.4840(9) 0.6637(6) 0.033(3) Uani 1 1 d . . . . . O32 O 0.5493(10) 0.5480(8) 0.6667(6) 0.025(3) Uani 1 1 d . . . . . O1 O 0.7018(9) 0.4459(8) 0.5100(6) 0.022(3) Uani 1 1 d . . . . . O19 O 0.8307(10) 0.3620(9) 0.6844(7) 0.030(3) Uani 1 1 d . . . . . O14 O 0.1787(10) 0.3241(8) 0.7879(7) 0.027(3) Uani 1 1 d . . . . . O8 O 0.7836(10) 0.5290(9) 0.5867(7) 0.030(3) Uani 1 1 d . U . . . O20 O 0.7292(11) 0.6268(9) 0.6769(7) 0.034(3) Uani 1 1 d . U . . . O18 O 0.7538(10) 0.2775(8) 0.6069(6) 0.027(3) Uani 1 1 d . U . . . O7 O 0.9309(10) 0.4135(8) 0.5223(7) 0.029(3) Uani 1 1 d . . . . . O33 O 0.3888(11) 0.3902(8) 0.7446(6) 0.026(3) Uani 1 1 d . . . . . O21 O 0.5095(10) 0.6487(8) 0.7468(7) 0.026(3) Uani 1 1 d . U . . . O10 O 0.5813(11) 0.7207(9) 0.5926(7) 0.036(3) Uani 1 1 d . . . . . O22 O 0.2620(12) 0.4087(10) 0.8667(7) 0.039(3) Uani 1 1 d . U . . . O38 O 0.6762(10) 0.8914(7) 0.8519(6) 0.021(3) Uani 1 1 d . U . . . O17 O 0.6200(11) 0.1068(8) 0.6827(7) 0.035(3) Uani 1 1 d . . . . . O6 O 0.5302(10) 0.2739(8) 0.5947(6) 0.025(3) Uani 1 1 d . . . . . O12 O 0.3154(12) 0.5671(9) 0.7371(7) 0.035(3) Uani 1 1 d . . . . . O26 O 0.4885(12) 0.4688(9) 0.8346(7) 0.039(3) Uani 1 1 d . . . . . O13 O 0.0777(12) 0.4914(10) 0.7952(7) 0.040(3) Uani 1 1 d . U . . . O15 O 0.2201(10) 0.1409(9) 0.8134(6) 0.035(3) Uani 1 1 d . . . . . O25 O 0.7020(11) 0.4479(9) 0.7662(7) 0.038(3) Uani 1 1 d . . . . . O30 O 0.3910(12) 0.3139(9) 0.9721(7) 0.038(3) Uani 1 1 d . . . . . O9 O 0.8180(12) 0.7233(9) 0.5143(7) 0.036(3) Uani 1 1 d . . . . . O34 O 0.6169(9) 0.3690(9) 0.6707(7) 0.030(3) Uani 1 1 d . . . . . O29 O 0.6769(13) 0.5781(9) 0.8345(7) 0.043(4) Uani 1 1 d . . . . . N1 N 0.7306(12) 0.9380(10) 0.8800(7) 0.022(3) Uani 1 1 d . . . . . O28 O 0.7903(13) 0.2763(10) 0.8431(8) 0.046(4) Uani 1 1 d . . . . . O11 O 0.3557(13) 0.7614(11) 0.6637(8) 0.056(5) Uani 1 1 d . . . . . O47 O 0.3838(13) 0.8455(11) 0.8477(10) 0.053(4) Uani 1 1 d . . . . . O44 O 1.0578(14) 1.2341(11) 1.0689(8) 0.051(4) Uani 1 1 d . . . . . O46 O 0.1402(12) 0.9921(11) 0.5386(9) 0.057(5) Uani 1 1 d . . . . . C2 C 0.7935(13) 0.9457(11) 0.9869(9) 0.018(4) Uani 1 1 d . . . . . H2 H 0.797150 0.917541 1.038582 0.021 Uiso 1 1 calc R U . . . C5 C 0.7798(15) 1.0266(12) 0.8351(10) 0.025(4) Uani 1 1 d . . . . . H5 H 0.774554 1.054264 0.783707 0.030 Uiso 1 1 calc R U . . . O45 O 0.9329(15) 0.9572(13) 0.2662(10) 0.085(7) Uani 1 1 d . . . . . N2 N 1.0021(12) 1.1891(11) 1.0390(8) 0.029(4) Uani 1 1 d . . . . . C10 C 0.9733(14) 1.1713(12) 0.9287(9) 0.020(4) Uani 1 1 d . . . . . H10 H 0.987584 1.193563 0.874923 0.024 Uiso 1 1 calc R U . . . C3 C 0.8419(14) 1.0364(12) 0.9416(9) 0.021(4) Uani 1 1 d . . . . . C1 C 0.7407(14) 0.8988(12) 0.9541(9) 0.021(4) Uani 1 1 d . . . . . H1 H 0.710783 0.837908 0.984002 0.025 Uiso 1 1 calc R U . . . C9 C 1.0209(16) 1.2156(14) 0.9608(11) 0.034(5) Uani 1 1 d . . . . . H9 H 1.070362 1.268012 0.928751 0.041 Uiso 1 1 calc R U . . . N5 N 0.4111(15) 0.8892(14) 0.8905(10) 0.050(5) Uani 1 1 d . . . . . C13 C 0.5928(9) 0.9656(9) 0.3799(7) 0.036(5) Uani 1 1 d G . . . . C12 C 0.6482(11) 0.8820(7) 0.3997(7) 0.045(6) Uani 1 1 d G . . . . H12 H 0.609049 0.828839 0.439852 0.054 Uiso 1 1 calc R U . . . C11 C 0.7619(11) 0.8779(7) 0.3593(8) 0.044(5) Uani 1 1 d G . . . . N3 N 0.8204(9) 0.9573(9) 0.2993(7) 0.048(5) Uani 1 1 d G U . . . C15 C 0.7650(12) 1.0409(8) 0.2795(7) 0.075(8) Uani 1 1 d G U . . . H15 H 0.804140 1.094111 0.239322 0.091 Uiso 1 1 calc R U . . . C14 C 0.6512(12) 1.0451(7) 0.3198(8) 0.065(7) Uani 1 1 d G U . . . H14 H 0.614218 1.101011 0.306602 0.078 Uiso 1 1 calc R U . . . C16 C 0.4733(8) 0.9723(8) 0.4242(6) 0.026(4) Uani 1 1 d G U . . . C20 C 0.4315(9) 1.0593(6) 0.4166(6) 0.035(5) Uani 1 1 d G . . . . H20 H 0.479112 1.112854 0.384842 0.041 Uiso 1 1 calc R U . . . C19 C 0.3185(9) 1.0664(6) 0.4565(7) 0.033(5) Uani 1 1 d G . . . . H19 H 0.290591 1.124598 0.451452 0.040 Uiso 1 1 calc R U . . . N4 N 0.2474(7) 0.9863(8) 0.5040(6) 0.036(4) Uani 1 1 d G . . . . C18 C 0.2891(9) 0.8993(6) 0.5116(6) 0.039(5) Uani 1 1 d G . . . . H18 H 0.241525 0.845748 0.543410 0.047 Uiso 1 1 calc R U . . . C17 C 0.4021(10) 0.8922(6) 0.4717(7) 0.037(5) Uani 1 1 d G . . . . H17 H 0.430046 0.834002 0.476801 0.044 Uiso 1 1 calc R U . . . C6 C 0.8981(13) 1.0874(11) 0.9755(9) 0.018(4) Uani 1 1 d . . . . . C8 C 0.9367(17) 1.1104(15) 1.0841(11) 0.036(5) Uani 1 1 d . U . . . H8 H 0.927781 1.088663 1.137517 0.043 Uiso 1 1 calc R U . . . C4 C 0.8353(15) 1.0738(12) 0.8646(9) 0.027(4) Uani 1 1 d . . . . . H4 H 0.870042 1.132722 0.832596 0.033 Uiso 1 1 calc R U . . . C7 C 0.8829(15) 1.0610(12) 1.0549(9) 0.024(4) Uani 1 1 d . . . . . H7 H 0.834848 1.008382 1.088634 0.028 Uiso 1 1 calc R U . . . C25 C 0.4437(19) 0.9834(17) 0.8601(13) 0.059(8) Uani 1 1 d . . . . . H25 H 0.440681 1.018204 0.809021 0.071 Uiso 1 1 calc R U . . . C24 C 0.4785(18) 1.0266(16) 0.8988(12) 0.042(5) Uani 1 1 d . U . . . H24 H 0.500981 1.089789 0.874354 0.050 Uiso 1 1 calc R U . . . C22 C 0.4433(18) 0.8818(15) 1.0109(12) 0.040(5) Uani 1 1 d . U . . . H22 H 0.440539 0.847640 1.063088 0.048 Uiso 1 1 calc R U . . . C23 C 0.4822(17) 0.9777(15) 0.9780(11) 0.046(6) Uani 1 1 d . . . . . C21 C 0.4107(19) 0.8391(17) 0.9694(15) 0.066(9) Uani 1 1 d . . . . . H21 H 0.387585 0.776052 0.992660 0.079 Uiso 1 1 calc R U . . . O49 O 1.1297(14) 0.6817(10) 0.5984(10) 0.060(5) Uani 1 1 d . . . . . O48 O 0.9679(13) 0.8704(12) 0.5620(9) 0.060(5) Uani 1 1 d . . . . . O50 O -0.0013(14) 0.2241(11) 0.6740(10) 0.062(5) Uani 1 1 d . . . . . O52 O 0.975(2) 1.0542(16) 0.6288(13) 0.099(7) Uani 1 1 d . U . . . H52A H 1.014899 1.045666 0.677706 0.148 Uiso 1 1 d R U . . . H52B H 0.893820 1.011545 0.665316 0.148 Uiso 1 1 d R U . . . Zn2 Zn 0.45882(16) 0.60205(14) 0.49774(10) 0.0213(5) Uani 1 1 d . . . . . Zn1 Zn 0.28348(17) 0.42499(14) 0.58496(11) 0.0236(5) Uani 1 1 d . . . . . O2 O 0.6367(9) 0.6275(8) 0.5021(6) 0.020(3) Uani 1 1 d . U . . . O31 O 0.4569(9) 0.4649(8) 0.5774(6) 0.021(3) Uani 1 1 d . U . . . O35 O 0.7691(11) 0.9616(9) 0.6783(7) 0.037(3) Uani 1 1 d . U . . . H35A H 0.717808 0.999861 0.688408 0.055 Uiso 1 1 d R U . . . H35B H 0.750422 0.953676 0.639799 0.055 Uiso 1 1 d R U . . . O37 O 0.5823(11) 0.8075(10) 0.7642(7) 0.036(3) Uani 1 1 d . U . . . H37A H 0.529462 0.836992 0.785788 0.054 Uiso 1 1 d R U . . . H37B H 0.558387 0.748734 0.791156 0.054 Uiso 1 1 d R U . . . O36 O 0.7433(12) 0.7070(9) 0.8751(7) 0.035(3) Uani 1 1 d . . . . . H36A H 0.714157 0.658082 0.869800 0.052 Uiso 1 1 d R U . . . H36B H 0.691650 0.708695 0.917256 0.052 Uiso 1 1 d R U . . . O39 O 0.9230(12) 0.8552(10) 0.7820(8) 0.040(3) Uani 1 1 d . U . . . H39A H 0.967468 0.898079 0.737045 0.061 Uiso 1 1 d R U . . . H39B H 0.926675 0.883370 0.815726 0.061 Uiso 1 1 d R U . . . O40 O 0.8274(11) 0.7661(10) 0.7010(8) 0.038(3) Uani 1 1 d . U . . . H40A H 0.867409 0.805614 0.657716 0.057 Uiso 1 1 d R U . . . H40B H 0.773274 0.743707 0.688331 0.057 Uiso 1 1 d R U . . . O43 O 0.047(2) 0.5663(17) 1.0634(13) 0.027(6) Uani 0.5 1 d . U P . . H43A H -0.005055 0.603527 1.081529 0.041 Uiso 0.5 1 calc R U P . . H43B H 0.121445 0.559093 1.074194 0.041 Uiso 0.5 1 calc R U P . . O41 O -0.069(3) 0.3785(16) 1.1000(13) 0.040(7) Uani 0.5 1 d . . P . . H41A H -0.012862 0.315322 1.121539 0.060 Uiso 0.5 1 d R U P . . H41B H -0.143244 0.329240 1.103312 0.060 Uiso 0.5 1 d R U P . . Zn4 Zn 0.000000 0.500000 1.000000 0.0765(15) Uani 1 2 d S . P . . O42 O -0.158(2) 0.556(2) 1.0098(16) 0.046(7) Uani 0.5 1 d . U P . . H42A H -0.176369 0.604873 1.035117 0.069 Uiso 0.5 1 d R U P . . H42B H -0.229807 0.512165 1.045017 0.069 Uiso 0.5 1 d R U P . . K2 K 1.0428(5) 0.7736(5) 0.4696(3) 0.0708(18) Uani 1 1 d . . . . . K1 K 0.9694(6) 0.5223(5) 0.6619(4) 0.079(2) Uani 1 1 d . . . . . O53 O 1.097(2) 0.7461(15) 0.7193(14) 0.106(8) Uani 1 1 d . . . . . H53A H 1.101853 0.785477 0.673419 0.159 Uiso 1 1 d R U . . . H53B H 1.093542 0.778767 0.746239 0.159 Uiso 1 1 d R U . . . O54 O -0.093(2) 0.6019(19) 0.8059(16) 0.122(9) Uani 1 1 d . U . . . H54A H -0.174611 0.591014 0.833287 0.183 Uiso 1 1 d R U . . . H54B H -0.083071 0.669255 0.786939 0.183 Uiso 1 1 d R U . . . O55 O -0.319(3) 0.355(2) 1.1275(17) 0.160(12) Uani 1 1 d . U . . . H55A H -0.335326 0.297842 1.138040 0.240 Uiso 1 1 d R U . . . H55B H -0.385226 0.379052 1.130450 0.240 Uiso 1 1 d R U . . . W10 W 0.7838(19) 0.4154(18) 0.5891(15) 0.037(5) Uani 0.26(2) 1 d . . P A 1 W12 W 0.683(2) 0.6467(13) 0.5762(10) 0.045(5) Uani 0.26(2) 1 d . . P A 1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 W6 0.0249(4) 0.0183(4) 0.0225(4) 0.0017(3) -0.0052(3) -0.0013(3) W1 0.0144(11) 0.0182(12) 0.0149(12) 0.0009(9) -0.0041(7) -0.0009(7) W5 0.0272(4) 0.0240(4) 0.0194(4) 0.0017(3) -0.0028(3) -0.0033(3) W2 0.0234(12) 0.0182(11) 0.0154(10) -0.0010(8) -0.0063(7) -0.0005(8) W7 0.0251(5) 0.0251(5) 0.0201(5) 0.0010(4) -0.0090(4) 0.0005(4) W7A 0.006(3) 0.006(3) 0.007(3) -0.0020(14) -0.0011(12) 0.0014(10) W4 0.0361(5) 0.0283(5) 0.0182(4) -0.0001(3) 0.0001(3) 0.0043(3) W8 0.0348(19) 0.0220(13) 0.0144(12) -0.0018(9) -0.0098(10) -0.0005(11) W8A 0.065(8) 0.019(3) 0.043(3) 0.004(2) -0.031(4) -0.009(4) W9 0.0465(5) 0.0247(4) 0.0151(4) 0.0003(3) -0.0057(3) -0.0016(4) W3 0.0471(5) 0.0223(4) 0.0218(4) -0.0018(3) -0.0066(3) 0.0015(4) Ge1 0.0253(10) 0.0165(10) 0.0151(9) 0.0009(7) -0.0064(7) 0.0006(8) Zn3 0.0315(12) 0.0322(13) 0.0261(11) -0.0085(10) -0.0113(9) -0.0002(10) O5 0.024(6) 0.016(6) 0.017(6) 0.001(5) -0.006(5) -0.001(5) O3 0.027(4) 0.010(4) 0.021(4) -0.010(3) -0.002(3) 0.006(3) O27 0.045(7) 0.014(6) 0.015(6) -0.008(5) -0.018(5) -0.001(5) O24 0.039(7) 0.008(6) 0.020(6) -0.002(5) -0.016(5) 0.004(5) O51 0.025(7) 0.045(9) 0.039(8) 0.022(7) -0.018(6) -0.001(6) O23 0.043(7) 0.009(6) 0.019(6) -0.009(5) -0.001(5) -0.003(5) O16 0.021(6) 0.021(6) 0.018(6) -0.004(5) -0.002(5) -0.001(5) O4 0.027(7) 0.036(8) 0.016(6) 0.009(6) -0.005(5) 0.008(6) O32 0.033(7) 0.014(6) 0.018(6) 0.002(5) -0.002(5) -0.003(5) O1 0.016(6) 0.033(7) 0.012(6) -0.001(5) -0.006(4) -0.001(5) O19 0.020(6) 0.032(7) 0.027(7) 0.005(6) -0.014(5) -0.006(5) O14 0.031(7) 0.023(7) 0.028(7) -0.013(5) -0.005(5) 0.004(5) O8 0.029(5) 0.030(5) 0.026(4) -0.002(4) -0.012(4) -0.005(4) O20 0.035(4) 0.033(4) 0.033(3) -0.012(2) -0.010(2) 0.001(2) O18 0.025(4) 0.025(5) 0.024(4) -0.004(4) -0.005(4) -0.001(4) O7 0.032(7) 0.017(6) 0.023(6) 0.007(5) -0.005(5) -0.005(5) O33 0.043(7) 0.015(6) 0.022(6) -0.011(5) -0.007(5) 0.001(5) O21 0.027(3) 0.026(3) 0.026(3) -0.0109(14) -0.0059(12) 0.0012(10) O10 0.044(8) 0.029(8) 0.027(7) 0.001(6) -0.015(6) -0.013(6) O22 0.041(5) 0.039(5) 0.028(5) -0.004(4) -0.005(4) 0.006(4) O38 0.024(5) 0.012(5) 0.030(6) -0.013(4) -0.004(4) -0.004(4) O17 0.027(7) 0.019(7) 0.040(8) 0.008(6) -0.008(6) 0.000(5) O6 0.029(7) 0.021(7) 0.018(6) 0.002(5) -0.010(5) 0.004(5) O12 0.051(9) 0.025(7) 0.022(7) -0.006(6) -0.003(6) 0.008(6) O26 0.060(9) 0.031(8) 0.017(7) 0.001(6) -0.007(6) -0.011(7) O13 0.055(7) 0.045(7) 0.026(6) -0.028(5) 0.006(5) 0.006(6) O15 0.026(7) 0.049(9) 0.015(6) 0.001(6) -0.002(5) 0.002(6) O25 0.038(8) 0.039(8) 0.021(7) 0.009(6) -0.012(6) -0.004(6) O30 0.066(10) 0.021(7) 0.018(6) -0.004(5) -0.001(6) -0.002(7) O9 0.063(9) 0.018(7) 0.032(7) -0.008(6) -0.022(7) -0.003(6) O34 0.014(6) 0.033(7) 0.024(7) 0.011(6) -0.007(5) -0.003(5) O29 0.077(10) 0.024(7) 0.030(7) -0.006(6) -0.023(7) -0.004(7) N1 0.032(8) 0.016(7) 0.016(7) -0.007(6) 0.000(6) -0.015(6) O28 0.053(9) 0.033(8) 0.041(8) 0.010(7) -0.030(7) -0.014(7) O11 0.048(9) 0.062(11) 0.028(8) 0.008(7) 0.002(7) -0.005(8) O47 0.049(10) 0.038(9) 0.060(10) -0.013(8) -0.002(8) 0.013(7) O44 0.066(10) 0.046(9) 0.055(10) -0.023(8) -0.032(8) -0.013(8) O46 0.024(8) 0.063(11) 0.053(10) 0.011(8) -0.006(7) -0.002(7) C2 0.018(8) 0.018(9) 0.022(9) -0.011(7) -0.008(7) 0.005(7) C5 0.032(10) 0.022(10) 0.033(10) -0.019(8) -0.017(8) 0.010(8) O45 0.059(11) 0.074(13) 0.056(11) 0.027(9) 0.013(9) 0.030(10) N2 0.018(8) 0.031(9) 0.032(9) -0.005(7) -0.004(6) 0.006(7) C10 0.024(9) 0.024(9) 0.014(8) -0.002(7) -0.014(7) 0.000(7) C3 0.023(9) 0.020(9) 0.019(9) -0.007(7) 0.000(7) -0.009(7) C1 0.019(9) 0.016(9) 0.017(9) -0.005(7) 0.010(7) -0.006(7) C9 0.026(10) 0.030(11) 0.035(11) 0.001(9) -0.008(8) 0.010(8) N5 0.033(10) 0.062(14) 0.031(10) -0.002(10) 0.008(8) 0.014(9) C13 0.054(13) 0.026(11) 0.031(11) -0.005(9) -0.024(9) 0.014(10) C12 0.054(14) 0.008(9) 0.076(16) -0.017(10) -0.021(12) 0.003(9) C11 0.060(15) 0.020(11) 0.054(14) -0.015(10) -0.014(11) -0.002(10) N3 0.046(6) 0.045(6) 0.046(6) -0.014(4) -0.006(4) 0.011(4) C15 0.076(9) 0.072(9) 0.072(9) -0.025(5) -0.012(5) 0.013(5) C14 0.064(8) 0.063(8) 0.063(8) -0.021(5) -0.012(5) 0.009(5) C16 0.026(4) 0.026(4) 0.026(4) -0.0099(18) -0.0066(14) 0.0016(11) C20 0.034(11) 0.038(12) 0.027(10) -0.003(9) -0.016(8) 0.004(9) C19 0.029(11) 0.030(11) 0.036(11) -0.004(9) -0.015(9) 0.001(9) N4 0.032(10) 0.035(10) 0.045(10) -0.018(8) -0.012(8) -0.004(8) C18 0.042(12) 0.030(12) 0.037(12) -0.005(9) -0.004(9) -0.004(9) C17 0.051(13) 0.025(11) 0.042(12) -0.015(9) -0.024(10) 0.012(9) C6 0.016(8) 0.012(8) 0.025(9) -0.001(7) -0.012(7) -0.001(7) C8 0.041(8) 0.047(9) 0.019(7) -0.013(7) -0.004(6) -0.001(7) C4 0.026(10) 0.025(10) 0.019(9) 0.010(8) -0.012(7) -0.019(8) C7 0.032(10) 0.020(9) 0.013(8) 0.001(7) -0.004(7) -0.008(8) C25 0.043(13) 0.049(15) 0.036(13) 0.023(12) 0.011(10) 0.008(11) C24 0.040(7) 0.040(7) 0.040(7) -0.013(5) -0.004(5) 0.007(5) C22 0.040(6) 0.038(7) 0.037(6) -0.010(5) -0.010(5) 0.007(5) C23 0.029(11) 0.042(14) 0.035(13) 0.010(9) 0.007(9) 0.026(10) C21 0.030(12) 0.040(14) 0.074(18) 0.025(13) 0.007(12) 0.009(10) O49 0.063(11) 0.030(9) 0.064(11) 0.001(8) -0.009(8) 0.013(8) O48 0.040(9) 0.060(11) 0.062(11) -0.007(9) -0.007(8) 0.001(8) O50 0.055(10) 0.054(11) 0.063(11) -0.013(9) -0.004(8) 0.021(8) O52 0.098(7) 0.099(7) 0.099(7) -0.039(3) -0.023(3) 0.004(3) Zn2 0.0216(10) 0.0191(10) 0.0152(10) 0.0019(8) -0.0038(8) 0.0006(8) Zn1 0.0206(10) 0.0240(11) 0.0175(10) 0.0005(8) -0.0031(8) 0.0025(8) O2 0.023(4) 0.015(4) 0.020(4) -0.002(3) -0.007(3) 0.003(3) O31 0.016(4) 0.020(4) 0.026(4) -0.006(3) -0.007(3) 0.001(3) O35 0.037(4) 0.038(4) 0.035(4) -0.014(2) -0.009(2) 0.002(2) O37 0.035(4) 0.037(4) 0.036(4) -0.012(2) -0.010(2) 0.002(2) O36 0.051(8) 0.033(8) 0.027(7) -0.025(6) -0.002(6) 0.002(6) O39 0.041(4) 0.041(4) 0.040(4) -0.015(3) -0.011(2) 0.000(2) O40 0.033(7) 0.041(8) 0.040(8) -0.014(6) -0.012(6) -0.001(6) O43 0.029(6) 0.027(6) 0.027(6) -0.013(3) -0.005(3) 0.003(3) O41 0.09(2) 0.004(12) 0.019(13) -0.003(10) -0.008(14) -0.003(13) Zn4 0.097(4) 0.055(3) 0.056(3) -0.019(2) 0.018(2) 0.006(3) O42 0.047(8) 0.047(8) 0.045(8) -0.019(4) -0.010(3) 0.004(3) K2 0.054(3) 0.095(5) 0.064(4) -0.034(3) -0.014(3) 0.021(3) K1 0.068(4) 0.073(4) 0.087(5) -0.014(4) -0.030(4) -0.010(3) O53 0.116(19) 0.077(16) 0.13(2) -0.057(15) -0.023(15) 0.028(14) O54 0.111(15) 0.103(15) 0.148(16) -0.036(12) -0.046(13) 0.023(12) O55 0.160(12) 0.161(12) 0.160(12) -0.062(5) -0.038(4) 0.008(3) W10 0.045(6) 0.026(5) 0.033(8) 0.005(4) -0.022(5) -0.003(4) W12 0.052(9) 0.019(5) 0.044(6) 0.015(4) -0.023(5) -0.014(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O24 W6 O34 73.4(4) . . ? O16 W6 O24 87.8(5) . . ? O16 W6 O18 157.6(5) . . ? O16 W6 O34 85.0(5) . . ? O18 W6 O24 83.8(5) . . ? O18 W6 O34 72.7(5) . . ? O17 W6 O24 96.7(5) . . ? O17 W6 O16 102.0(5) . . ? O17 W6 O18 99.7(6) . . ? O17 W6 O6 105.0(6) . . ? O17 W6 O34 167.8(5) . . ? O6 W6 O24 158.3(5) . . ? O6 W6 O16 89.3(5) . . ? O6 W6 O18 90.9(5) . . ? O6 W6 O34 84.9(5) . . ? O1 W1 O19 157.0(6) . . ? O1 W1 O8 89.5(6) . . ? O1 W1 O18 94.9(6) . . ? O1 W1 O34 85.4(5) . . ? O1 W1 K2 104.2(5) . 2_766 ? O1 W1 K1 135.3(5) . . ? O19 W1 O34 72.2(5) . . ? O19 W1 K2 91.9(5) . 2_766 ? O19 W1 K1 48.4(4) . . ? O8 W1 O19 83.7(6) . . ? O8 W1 O34 85.2(6) . . ? O8 W1 K2 151.2(4) . 2_766 ? O8 W1 K1 47.8(4) . . ? O18 W1 O19 83.6(6) . . ? O18 W1 O8 157.3(6) . . ? O18 W1 O34 73.0(5) . . ? O18 W1 K2 48.1(4) . 2_766 ? O18 W1 K1 129.4(5) . . ? O7 W1 O1 104.6(6) . . ? O7 W1 O19 98.4(6) . . ? O7 W1 O8 101.9(6) . . ? O7 W1 O18 98.5(6) . . ? O7 W1 O34 167.6(6) . . ? O7 W1 K2 50.4(5) . 2_766 ? O7 W1 K1 77.3(5) . . ? O34 W1 K2 120.6(4) . 2_766 ? O34 W1 K1 100.9(4) . . ? K2 W1 K1 109.8(2) 2_766 . ? O5 W5 O33 83.0(4) . . ? O23 W5 O5 158.4(5) . . ? O23 W5 O16 89.0(5) . . ? O23 W5 O33 76.0(4) . . ? O16 W5 O5 83.7(5) . . ? O16 W5 O33 84.5(5) . . ? O14 W5 O5 87.6(5) . . ? O14 W5 O23 91.7(5) . . ? O14 W5 O16 157.5(5) . . ? O14 W5 O33 73.8(5) . . ? O15 W5 O5 102.3(5) . . ? O15 W5 O23 99.1(5) . . ? O15 W5 O16 101.2(5) . . ? O15 W5 O14 101.0(6) . . ? O15 W5 O33 172.5(5) . . ? O32 W2 K1 99.2(3) . . ? O8 W2 O32 85.3(5) . . ? O8 W2 O20 85.5(6) . . ? O8 W2 O10 156.7(6) . . ? O8 W2 K1 42.4(4) . . ? O20 W2 O32 71.6(5) . . ? O20 W2 K1 53.6(4) . . ? O10 W2 O32 71.7(5) . . ? O10 W2 O20 84.0(5) . . ? O10 W2 K1 136.7(4) . . ? O9 W2 O32 167.8(6) . . ? O9 W2 O8 100.9(6) . . ? O9 W2 O20 98.2(6) . . ? O9 W2 O10 101.1(7) . . ? O9 W2 O2 102.9(6) . . ? O9 W2 K1 79.1(5) . . ? O2 W2 O32 87.2(5) . . ? O2 W2 O8 92.5(5) . . ? O2 W2 O20 158.8(6) . . ? O2 W2 O10 89.8(6) . . ? O2 W2 K1 132.8(4) . . ? O27 W7 O34 84.8(4) . . ? O27 W7 K1 138.1(3) . . ? O27 W7 W10 126.2(5) . . ? O24 W7 O27 88.6(5) . . ? O24 W7 O25 158.0(5) . . ? O24 W7 O34 73.4(4) . . ? O24 W7 K1 131.0(4) . . ? O24 W7 W10 84.2(6) . . ? O19 W7 O27 157.9(4) . . ? O19 W7 O24 91.3(6) . . ? O19 W7 O25 87.6(6) . . ? O19 W7 O34 74.0(4) . . ? O19 W7 K1 40.2(4) . . ? O19 W7 W10 32.0(5) . . ? O25 W7 O27 84.3(5) . . ? O25 W7 O34 85.2(5) . . ? O25 W7 K1 53.8(4) . . ? O25 W7 W10 83.2(6) . . ? O34 W7 K1 93.4(3) . . ? O34 W7 W10 42.1(5) . . ? O28 W7 O27 100.7(6) . . ? O28 W7 O24 101.0(6) . . ? O28 W7 O19 101.0(6) . . ? O28 W7 O25 100.8(6) . . ? O28 W7 O34 172.2(7) . . ? O28 W7 K1 86.2(4) . . ? O28 W7 W10 133.0(6) . . ? W10 W7 K1 58.4(4) . . ? O27 W7A W9 20.1(5) . . ? O27 W7A O24 92.7(8) . . ? O27 W7A O19 158.3(9) . . ? O27 W7A O25 108.7(9) . . ? O27 W7A O34 94.1(7) . . ? O27 W7A O28 114.6(9) . . ? O24 W7A W9 108.9(5) . . ? O24 W7A O19 73.1(6) . . ? O24 W7A O34 67.9(5) . . ? O19 W7A W9 152.5(5) . . ? O19 W7A O34 65.7(5) . . ? O25 W7A W9 89.1(6) . . ? O25 W7A O24 149.2(8) . . ? O25 W7A O19 79.5(7) . . ? O25 W7A O34 88.2(7) . . ? O25 W7A O28 103.2(8) . . ? O34 W7A W9 89.2(4) . . ? O28 W7A W9 125.7(7) . . ? O28 W7A O24 86.7(7) . . ? O28 W7A O19 81.5(7) . . ? O28 W7A O34 142.8(8) . . ? O4 W4 O14 89.6(5) . . ? O4 W4 O33 88.1(5) . . ? O4 W4 O22 161.1(5) . . ? O4 W4 O12 94.2(6) . . ? O4 W4 K1 51.6(4) . 1_455 ? O14 W4 O33 72.1(4) . . ? O14 W4 O22 82.7(5) . . ? O14 W4 K1 89.1(4) . 1_455 ? O33 W4 K1 136.1(3) . 1_455 ? O22 W4 O33 73.2(5) . . ? O22 W4 K1 144.9(4) . 1_455 ? O12 W4 O14 156.5(5) . . ? O12 W4 O33 84.9(5) . . ? O12 W4 O22 86.4(5) . . ? O12 W4 K1 111.3(4) . 1_455 ? O13 W4 O4 102.5(6) . . ? O13 W4 O14 98.4(6) . . ? O13 W4 O33 165.9(5) . . ? O13 W4 O22 95.7(6) . . ? O13 W4 O12 103.3(6) . . ? O13 W4 K1 51.7(4) . 1_455 ? O20 W8 O32 74.0(5) . . ? O20 W8 O21 89.7(6) . . ? O20 W8 O26 157.2(7) . . ? O20 W8 O25 91.2(6) . . ? O21 W8 O32 71.7(5) . . ? O21 W8 O26 84.1(6) . . ? O26 W8 O32 83.3(5) . . ? O25 W8 O32 86.0(5) . . ? O25 W8 O21 156.5(7) . . ? O25 W8 O26 86.1(7) . . ? O29 W8 O32 169.9(7) . . ? O29 W8 O20 101.8(7) . . ? O29 W8 O21 99.4(7) . . ? O29 W8 O26 100.8(7) . . ? O29 W8 O25 103.4(7) . . ? O32 W8A W3 44.4(4) . . ? O20 W8A W3 84.7(6) . . ? O20 W8A O32 74.1(6) . . ? O20 W8A O25 81.7(7) . . ? O21 W8A W3 34.4(5) . . ? O21 W8A O32 78.7(7) . . ? O21 W8A O20 92.3(8) . . ? O21 W8A O26 96.4(9) . . ? O21 W8A O25 163.2(9) . . ? O21 W8A O29 103.9(9) . . ? O26 W8A W3 92.5(7) . . ? O26 W8A O32 90.3(8) . . ? O26 W8A O20 160.4(10) . . ? O26 W8A O25 85.1(8) . . ? O26 W8A O29 102.7(8) . . ? O25 W8A W3 129.0(7) . . ? O25 W8A O32 84.6(7) . . ? O29 W8A W3 137.6(8) . . ? O29 W8A O32 166.2(9) . . ? O29 W8A O20 92.2(9) . . ? O29 W8A O25 91.9(8) . . ? O27 W9 W7A 15.3(4) . . ? O27 W9 O23 85.0(5) . . ? O27 W9 O33 84.5(4) . . ? O23 W9 W7A 97.7(4) . . ? O23 W9 O33 73.5(4) . . ? O33 W9 W7A 80.0(4) . . ? O22 W9 W7A 149.6(4) . . ? O22 W9 O27 158.4(5) . . ? O22 W9 O23 89.7(6) . . ? O22 W9 O33 73.9(5) . . ? O22 W9 O26 90.8(6) . . ? O26 W9 W7A 71.8(5) . . ? O26 W9 O27 86.6(6) . . ? O26 W9 O23 158.3(5) . . ? O26 W9 O33 85.8(5) . . ? O30 W9 W7A 109.1(5) . . ? O30 W9 O27 102.9(6) . . ? O30 W9 O23 99.1(5) . . ? O30 W9 O33 169.3(6) . . ? O30 W9 O22 98.6(6) . . ? O30 W9 O26 102.2(6) . . ? O3 W3 W8A 133.3(4) . . ? O3 W3 O32 89.3(5) . . ? O3 W3 O21 161.7(5) . . ? O3 W3 O10 90.7(5) . . ? O3 W3 O12 93.0(5) . . ? O3 W3 W12 85.6(5) . . ? O32 W3 W8A 44.0(4) . . ? O32 W3 W12 44.1(4) . . ? O21 W3 W8A 28.5(4) . . ? O21 W3 O32 72.4(4) . . ? O21 W3 W12 80.7(5) . . ? O10 W3 W8A 78.2(4) . . ? O10 W3 O32 72.5(5) . . ? O10 W3 O21 83.2(5) . . ? O10 W3 W12 28.9(5) . . ? O12 W3 W8A 82.0(5) . . ? O12 W3 O32 83.9(5) . . ? O12 W3 O21 86.0(5) . . ? O12 W3 O10 156.0(5) . . ? O12 W3 W12 127.9(5) . . ? O11 W3 W8A 124.3(6) . . ? O11 W3 O3 102.4(6) . . ? O11 W3 O32 167.1(6) . . ? O11 W3 O21 95.8(6) . . ? O11 W3 O10 101.7(6) . . ? O11 W3 O12 100.7(6) . . ? O11 W3 W12 130.5(6) . . ? W12 W3 W8A 63.1(4) . . ? O33 Ge1 O32 107.2(5) . . ? O33 Ge1 O31 111.8(5) . . ? O34 Ge1 O32 108.2(6) . . ? O34 Ge1 O33 106.7(5) . . ? O34 Ge1 O31 111.2(6) . . ? O31 Ge1 O32 111.5(5) . . ? O38 Zn3 O35 93.9(5) . . ? O38 Zn3 O37 88.9(5) . . ? O38 Zn3 O36 84.9(5) . . ? O38 Zn3 O39 93.9(5) . . ? O38 Zn3 O40 175.4(5) . . ? O35 Zn3 O37 90.8(5) . . ? O35 Zn3 O36 175.9(5) . . ? O35 Zn3 O39 90.7(5) . . ? O35 Zn3 O40 90.8(5) . . ? O37 Zn3 O36 93.0(5) . . ? O39 Zn3 O37 176.7(6) . . ? O39 Zn3 O36 85.6(5) . . ? O39 Zn3 O40 86.2(5) . . ? O40 Zn3 O37 90.9(5) . . ? O40 Zn3 O36 90.5(5) . . ? W5 O5 Zn1 133.4(6) . . ? W3 O3 Zn2 136.8(6) . . ? W7A O27 W9 144.5(9) . . ? W9 O27 W7 152.2(6) . . ? W6 O24 W7A 118.2(6) . . ? W7 O24 W6 120.8(5) . . ? Zn1 O51 K1 103.9(6) . 1_455 ? W5 O23 W9 119.3(5) . . ? W6 O16 W5 154.9(6) . . ? W4 O4 Zn1 137.3(7) . . ? W4 O4 K1 101.0(5) . 1_455 ? Zn1 O4 K1 107.7(5) . 1_455 ? W8A O32 W2 97.1(6) . . ? W8A O32 W8 6.7(5) . . ? W8A O32 W3 91.6(6) . . ? W3 O32 W2 94.8(4) . . ? W3 O32 W8 97.1(5) . . ? Ge1 O32 W2 120.4(6) . . ? Ge1 O32 W8 124.1(6) . . ? Ge1 O32 W8A 124.8(7) . . ? Ge1 O32 W3 120.7(6) . . ? Ge1 O32 W12 123.5(8) . . ? W12 O32 W8 93.7(7) . . ? W12 O32 W8A 97.7(8) . . ? W12 O32 W3 89.4(7) . . ? Zn2 O1 Zn1 96.4(4) 2_666 2_666 ? W10 O1 Zn2 134.5(9) . 2_666 ? W10 O1 Zn1 125.9(9) . 2_666 ? W1 O19 W7A 117.1(6) . . ? W1 O19 K1 99.2(5) . . ? W7 O19 K1 115.0(6) . . ? W7 O19 W10 116.8(9) . . ? W7A O19 K1 109.9(6) . . ? W10 O19 K1 95.8(9) . . ? W5 O14 W4 119.8(6) . . ? W1 O8 K1 101.4(5) . . ? W2 O8 W1 147.6(7) . . ? W2 O8 K1 110.8(6) . . ? W10 O8 K1 99.8(9) . . ? W10 O8 W12 144.9(11) . . ? W12 O8 K1 112.9(8) . . ? W2 O20 K1 95.6(5) . . ? W8 O20 W8A 7.6(7) . . ? W8 O20 K1 108.0(6) . . ? W8 O20 W12 117.1(9) . . ? W8A O20 W2 116.8(8) . . ? W8A O20 K1 115.1(7) . . ? W8A O20 W12 111.7(10) . . ? W12 O20 K1 102.8(9) . . ? W6 O18 K2 138.9(6) . 2_766 ? W6 O18 W10 114.6(9) . . ? W1 O18 W6 120.2(7) . . ? W10 O18 K2 106.4(8) . 2_766 ? K2 O7 K1 86.3(4) 2_766 2_766 ? W10 O7 K2 107.5(9) . 2_766 ? W10 O7 K1 135.6(9) . 2_766 ? W5 O33 W9 90.9(4) . . ? W4 O33 W5 94.3(4) . . ? W4 O33 W9 94.4(4) . . ? Ge1 O33 W5 124.4(6) . . ? Ge1 O33 W4 120.2(6) . . ? Ge1 O33 W9 124.3(6) . . ? W8 O21 W3 118.8(6) . . ? W8A O21 W8 5.3(7) . . ? W8A O21 W3 117.1(8) . . ? W2 O10 W3 120.2(7) . . ? W12 O10 W3 117.1(10) . . ? W9 O22 W4 118.3(7) . . ? N1 O38 Zn3 126.7(10) . . ? W6 O6 Zn2 137.6(7) . 2_666 ? W4 O12 W3 147.7(7) . . ? W8A O26 W8 7.3(7) . . ? W8A O26 W9 154.2(10) . . ? W9 O26 W8 150.1(9) . . ? W4 O13 K1 101.0(5) . 1_455 ? W7 O25 W8A 149.1(8) . . ? W7 O25 K1 97.7(5) . . ? W7A O25 W8A 135.3(9) . . ? W7A O25 K1 113.1(7) . . ? W8 O25 W7 155.5(8) . . ? W8 O25 W8A 6.4(7) . . ? W8 O25 K1 105.1(6) . . ? W8A O25 K1 110.6(6) . . ? W2 O9 K2 150.3(7) . . ? W12 O9 K2 155.9(9) . . ? W6 O34 W1 93.4(5) . . ? W6 O34 W7 92.4(4) . . ? W6 O34 W7A 98.0(5) . . ? W1 O34 W7A 104.7(5) . . ? Ge1 O34 W6 123.4(6) . . ? Ge1 O34 W1 121.3(6) . . ? Ge1 O34 W7 124.5(7) . . ? Ge1 O34 W7A 112.1(7) . . ? Ge1 O34 W10 119.3(9) . . ? W10 O34 W6 99.2(9) . . ? W10 O34 W7 90.4(8) . . ? W8 O29 W8A 8.6(7) . . ? O38 N1 C5 121.5(13) . . ? O38 N1 C1 120.0(13) . . ? C1 N1 C5 118.5(14) . . ? C3 C2 H2 120.4 . . ? C1 C2 H2 120.4 . . ? C1 C2 C3 119.2(15) . . ? N1 C5 H5 119.5 . . ? C4 C5 N1 120.9(16) . . ? C4 C5 H5 119.5 . . ? O44 N2 C9 120.8(16) . . ? O44 N2 C8 121.2(16) . . ? C8 N2 C9 117.6(17) . . ? C9 C10 H10 119.5 . . ? C9 C10 C6 121.0(16) . . ? C6 C10 H10 119.5 . . ? C2 C3 C6 120.0(15) . . ? C4 C3 C2 117.6(15) . . ? C4 C3 C6 122.4(15) . . ? N1 C1 C2 122.2(15) . . ? N1 C1 H1 118.9 . . ? C2 C1 H1 118.9 . . ? N2 C9 H9 118.4 . . ? C10 C9 N2 123.3(18) . . ? C10 C9 H9 118.4 . . ? O47 N5 C25 122.8(19) . . ? O47 N5 C21 121(2) . . ? C25 N5 C21 117(2) . . ? C12 C13 C14 120.0 . . ? C12 C13 C16 120.8(9) . . ? C14 C13 C16 119.2(9) . . ? C13 C12 H12 120.0 . . ? C13 C12 C11 120.0 . . ? C11 C12 H12 120.0 . . ? N3 C11 C12 120.0 . . ? O45 N3 C11 120.6(11) . . ? O45 N3 C15 118.9(12) . . ? C15 N3 C11 120.0 . . ? N3 C15 H15 120.0 . . ? N3 C15 C14 120.0 . . ? C14 C15 H15 120.0 . . ? C13 C14 H14 120.0 . . ? C15 C14 C13 120.0 . . ? C15 C14 H14 120.0 . . ? C20 C16 C13 119.6(9) . . ? C20 C16 C17 120.0 . . ? C17 C16 C13 120.4(9) . . ? C16 C20 H20 120.0 . . ? C16 C20 C19 120.0 . . ? C19 C20 H20 120.0 . . ? C20 C19 H19 120.0 . . ? C20 C19 N4 120.0 . . ? N4 C19 H19 120.0 . . ? O46 N4 C19 120.6(11) . . ? O46 N4 C18 119.3(11) . . ? C18 N4 C19 120.0 . . ? N4 C18 H18 120.0 . . ? N4 C18 C17 120.0 . . ? C17 C18 H18 120.0 . . ? C16 C17 H17 120.0 . . ? C18 C17 C16 120.0 . . ? C18 C17 H17 120.0 . . ? C10 C6 C3 122.5(14) . . ? C7 C6 C10 114.4(15) . . ? C7 C6 C3 123.0(14) . . ? N2 C8 H8 118.8 . . ? N2 C8 C7 122.4(17) . . ? C7 C8 H8 118.8 . . ? C5 C4 C3 121.5(16) . . ? C5 C4 H4 119.3 . . ? C3 C4 H4 119.3 . . ? C6 C7 H7 119.4 . . ? C8 C7 C6 121.2(16) . . ? C8 C7 H7 119.4 . . ? N5 C25 H25 117.9 . . ? C24 C25 N5 124(2) . . ? C24 C25 H25 117.9 . . ? C25 C24 H24 119.7 . . ? C25 C24 C23 121(2) . . ? C23 C24 H24 119.7 . . ? C23 C22 H22 118.9 . . ? C21 C22 H22 118.9 . . ? C21 C22 C23 122(2) . . ? C22 C23 C24 116(2) . . ? C23 C23 C24 122(2) 2_677 . ? C23 C23 C22 122(2) 2_677 . ? N5 C21 H21 119.7 . . ? C22 C21 N5 121(2) . . ? C22 C21 H21 119.7 . . ? K2 O49 K1 96.2(6) . . ? H52A O52 H52B 95.2 . . ? K2 O52 H52A 117.9 2_776 . ? K2 O52 H52B 118.6 2_776 . ? O3 Zn2 O1 95.5(5) . 2_666 ? O3 Zn2 Zn1 89.5(3) . . ? O3 Zn2 O2 93.4(4) . . ? O3 Zn2 O31 172.1(4) . 2_666 ? O3 Zn2 O31 93.6(4) . . ? O1 Zn2 Zn1 41.9(3) 2_666 . ? O1 Zn2 O2 168.9(5) 2_666 . ? O1 Zn2 O31 86.7(4) 2_666 2_666 ? O6 Zn2 O3 96.5(5) 2_666 . ? O6 Zn2 O1 95.1(4) 2_666 2_666 ? O6 Zn2 Zn1 137.0(3) 2_666 . ? O6 Zn2 O2 90.4(4) 2_666 . ? O6 Zn2 O31 169.8(5) 2_666 . ? O6 Zn2 O31 90.9(5) 2_666 2_666 ? O2 Zn2 Zn1 131.9(3) . . ? O31 Zn2 O1 82.5(4) . 2_666 ? O31 Zn2 Zn1 41.5(3) . . ? O31 Zn2 Zn1 87.1(3) 2_666 . ? O31 Zn2 O2 90.4(4) . . ? O31 Zn2 O2 83.6(4) 2_666 . ? O31 Zn2 O31 79.1(5) . 2_666 ? O5 Zn1 O1 168.6(4) . 2_666 ? O5 Zn1 Zn2 131.2(3) . . ? O5 Zn1 O2 86.9(4) . 2_666 ? O5 Zn1 O31 89.9(4) . . ? O5 Zn1 K1 109.0(3) . 1_455 ? O51 Zn1 O5 90.9(5) . . ? O51 Zn1 O1 97.4(4) . 2_666 ? O51 Zn1 Zn2 137.8(4) . . ? O51 Zn1 O2 97.6(6) . 2_666 ? O51 Zn1 O31 177.6(6) . . ? O51 Zn1 K1 46.9(5) . 1_455 ? O4 Zn1 O5 95.7(5) . . ? O4 Zn1 O51 87.1(6) . . ? O4 Zn1 O1 92.5(5) . 2_666 ? O4 Zn1 Zn2 85.5(4) . . ? O4 Zn1 O2 174.6(5) . 2_666 ? O4 Zn1 O31 90.6(5) . . ? O4 Zn1 K1 43.9(3) . 1_455 ? O1 Zn1 Zn2 41.7(3) 2_666 . ? O1 Zn1 O2 84.3(4) 2_666 2_666 ? O1 Zn1 K1 82.4(3) 2_666 1_455 ? Zn2 Zn1 K1 105.20(11) . 1_455 ? O2 Zn1 Zn2 89.2(3) 2_666 . ? O2 Zn1 K1 139.3(3) 2_666 1_455 ? O31 Zn1 O1 82.1(4) . 2_666 ? O31 Zn1 Zn2 41.3(3) . . ? O31 Zn1 O2 84.7(4) . 2_666 ? O31 Zn1 K1 130.7(3) . 1_455 ? W2 O2 Zn2 135.5(6) . . ? Zn1 O2 Zn2 94.4(4) 2_666 . ? W12 O2 Zn2 127.8(10) . . ? W12 O2 Zn1 134.7(10) . 2_666 ? Ge1 O31 Zn2 118.9(6) . 2_666 ? Ge1 O31 Zn2 119.7(6) . . ? Ge1 O31 Zn1 119.0(6) . . ? Zn2 O31 Zn2 100.9(5) . 2_666 ? Zn2 O31 Zn1 97.2(4) . . ? Zn1 O31 Zn2 96.4(5) . 2_666 ? Zn3 O35 H35A 110.9 . . ? Zn3 O35 H35B 110.4 . . ? H35A O35 H35B 103.2 . . ? Zn3 O37 H37A 111.0 . . ? Zn3 O37 H37B 111.3 . . ? H37A O37 H37B 102.9 . . ? Zn3 O36 H36A 112.2 . . ? Zn3 O36 H36B 112.2 . . ? H36A O36 H36B 102.0 . . ? Zn3 O39 H39A 112.3 . . ? Zn3 O39 H39B 113.6 . . ? H39A O39 H39B 99.9 . . ? Zn3 O40 H40A 109.8 . . ? Zn3 O40 H40B 109.8 . . ? H40A O40 H40B 104.2 . . ? H43A O43 H43B 120.0 . . ? Zn4 O43 H43A 120.0 . . ? Zn4 O43 H43B 120.0 . . ? H41A O41 H41B 89.9 . . ? Zn4 O41 H41A 122.0 . . ? Zn4 O41 H41B 123.2 . . ? O43 Zn4 O43 180.0(12) . 2_567 ? O43 Zn4 O41 93.1(9) . . ? O43 Zn4 O41 93.1(9) 2_567 2_567 ? O43 Zn4 O41 86.9(9) 2_567 . ? O43 Zn4 O41 86.9(9) . 2_567 ? O41 Zn4 O41 180.0 2_567 . ? O42 Zn4 O43 90.6(11) . 2_567 ? O42 Zn4 O43 89.4(11) . . ? O42 Zn4 O43 90.6(11) 2_567 . ? O42 Zn4 O43 89.4(11) 2_567 2_567 ? O42 Zn4 O41 90.7(12) 2_567 2_567 ? O42 Zn4 O41 89.3(12) . 2_567 ? O42 Zn4 O41 90.7(12) . . ? O42 Zn4 O41 89.3(12) 2_567 . ? O42 Zn4 O42 180.0 . 2_567 ? Zn4 O42 H42A 121.4 . . ? Zn4 O42 H42B 117.2 . . ? H42A O42 H42B 94.9 . . ? W1 K2 K1 70.75(19) 2_766 . ? W1 K2 W10 2.4(5) 2_766 2_766 ? O18 K2 W1 31.0(3) 2_766 2_766 ? O18 K2 O7 58.4(4) 2_766 2_766 ? O18 K2 O50 72.9(4) 2_766 2_666 ? O18 K2 K1 96.3(3) 2_766 . ? O18 K2 W10 30.8(4) 2_766 2_766 ? O7 K2 W1 27.4(3) 2_766 2_766 ? O7 K2 O50 74.3(4) 2_766 2_666 ? O7 K2 K1 50.3(3) 2_766 . ? O7 K2 W10 27.8(4) 2_766 2_766 ? O9 K2 W1 109.5(4) . 2_766 ? O9 K2 O18 137.7(5) . 2_766 ? O9 K2 O7 83.5(4) . 2_766 ? O9 K2 O49 104.9(5) . . ? O9 K2 O48 80.1(5) . . ? O9 K2 O50 79.9(5) . 2_666 ? O9 K2 O52 97.1(6) . 2_776 ? O9 K2 K1 68.1(3) . . ? O9 K2 W10 108.9(5) . 2_766 ? O49 K2 W1 76.9(4) . 2_766 ? O49 K2 O18 83.6(4) . 2_766 ? O49 K2 O7 74.5(5) . 2_766 ? O49 K2 O50 147.7(5) . 2_666 ? O49 K2 K1 42.8(4) . . ? O49 K2 W10 79.3(5) . 2_766 ? O48 K2 W1 152.7(4) . 2_766 ? O48 K2 O18 141.1(5) . 2_766 ? O48 K2 O7 141.0(5) . 2_766 ? O48 K2 O49 75.9(5) . . ? O48 K2 O50 135.8(5) . 2_666 ? O48 K2 K1 90.7(4) . . ? O48 K2 W10 155.0(5) . 2_766 ? O50 K2 W1 71.5(4) 2_666 2_766 ? O50 K2 K1 117.1(4) 2_666 . ? O50 K2 W10 69.1(5) 2_666 2_766 ? O52 K2 W1 126.2(5) 2_776 2_766 ? O52 K2 O18 102.0(6) 2_776 2_766 ? O52 K2 O7 141.8(6) 2_776 2_766 ? O52 K2 O49 140.1(7) 2_776 . ? O52 K2 O48 75.6(6) 2_776 . ? O52 K2 O50 68.3(6) 2_776 2_666 ? O52 K2 K1 161.6(5) 2_776 . ? O52 K2 W10 124.3(6) 2_776 2_766 ? W10 K2 K1 72.4(4) 2_766 . ? O51 K1 W4 75.4(3) 1_655 1_655 ? O51 K1 O20 145.7(4) 1_655 . ? O51 K1 O7 59.6(3) 1_655 2_766 ? O51 K1 O25 116.6(4) 1_655 . ? O51 K1 O54 147.3(5) 1_655 1_655 ? O51 K1 W10 70.1(5) 1_655 . ? O4 K1 W4 27.4(2) 1_655 1_655 ? O4 K1 O51 55.6(4) 1_655 1_655 ? O4 K1 O20 157.8(4) 1_655 . ? O4 K1 O7 82.7(3) 1_655 2_766 ? O4 K1 O13 54.4(4) 1_655 1_655 ? O4 K1 O25 141.4(4) 1_655 . ? O4 K1 O54 97.7(5) 1_655 1_655 ? O4 K1 W10 125.7(5) 1_655 . ? O19 K1 W4 112.7(3) . 1_655 ? O19 K1 O51 67.1(4) . 1_655 ? O19 K1 O4 113.2(4) . 1_655 ? O19 K1 O20 87.5(4) . . ? O19 K1 O7 96.7(4) . 2_766 ? O19 K1 O13 112.1(4) . 1_655 ? O19 K1 O25 50.1(4) . . ? O19 K1 O54 116.5(6) . 1_655 ? O19 K1 W10 31.7(4) . . ? O8 K1 W4 167.3(4) . 1_655 ? O8 K1 O51 93.8(4) . 1_655 ? O8 K1 O4 146.7(5) . 1_655 ? O8 K1 O19 56.0(3) . . ? O8 K1 O20 52.0(4) . . ? O8 K1 O7 68.9(4) . 2_766 ? O8 K1 O13 156.4(4) . 1_655 ? O8 K1 O25 60.3(3) . . ? O8 K1 O54 115.4(5) . 1_655 ? O8 K1 W10 28.7(5) . . ? O20 K1 W4 137.9(3) . 1_655 ? O20 K1 O7 103.6(4) . 2_766 ? O20 K1 O25 48.0(3) . . ? O20 K1 O54 64.3(5) . 1_655 ? O20 K1 W10 76.2(5) . . ? O7 K1 W4 109.8(3) 2_766 1_655 ? O7 K1 O25 128.9(4) 2_766 . ? O7 K1 O54 143.0(6) 2_766 1_655 ? O7 K1 W10 71.2(5) 2_766 . ? O13 K1 W4 27.3(3) 1_655 1_655 ? O13 K1 O51 99.6(4) 1_655 1_655 ? O13 K1 O20 111.6(4) 1_655 . ? O13 K1 O7 134.7(4) 1_655 2_766 ? O13 K1 O25 96.2(4) 1_655 . ? O13 K1 O54 48.0(5) 1_655 1_655 ? O13 K1 W10 143.8(5) 1_655 . ? O25 K1 W4 118.4(3) . 1_655 ? O25 K1 O54 70.8(5) . 1_655 ? O25 K1 W10 61.8(5) . . ? O49 K1 W4 72.4(3) . 1_655 ? O49 K1 O51 101.4(5) . 1_655 ? O49 K1 O4 64.1(4) . 1_655 ? O49 K1 O19 164.4(5) . . ? O49 K1 O8 117.0(5) . . ? O49 K1 O20 98.2(4) . . ? O49 K1 O7 67.9(4) . 2_766 ? O49 K1 O13 79.4(5) . 1_655 ? O49 K1 O25 141.9(5) . . ? O49 K1 O54 79.0(6) . 1_655 ? O49 K1 W10 136.0(6) . . ? O54 K1 W4 73.6(4) 1_655 1_655 ? O54 K1 W10 131.4(6) 1_655 . ? W10 K1 W4 138.7(5) . 1_655 ? H53A O53 H53B 104.5 . . ? K1 O54 H54A 112.8 1_455 . ? K1 O54 H54B 112.8 1_455 . ? H54A O54 H54B 101.2 . . ? H55A O55 H55B 104.5 . . ? W7 W10 K2 103.4(7) . 2_766 ? W7 W10 K1 72.3(5) . . ? O1 W10 W7 134.7(10) . . ? O1 W10 O19 164.5(14) . . ? O1 W10 O18 86.5(12) . . ? O1 W10 O7 93.6(13) . . ? O1 W10 O34 87.3(9) . . ? O1 W10 K2 93.5(11) . 2_766 ? O1 W10 K1 140.7(12) . . ? O19 W10 W7 31.2(5) . . ? O19 W10 O18 83.3(11) . . ? O19 W10 O7 97.6(11) . . ? O19 W10 O34 78.6(10) . . ? O19 W10 K2 87.0(10) . 2_766 ? O19 W10 K1 52.5(7) . . ? O8 W10 W7 93.9(11) . . ? O8 W10 O1 93.2(12) . . ? O8 W10 O19 94.6(14) . . ? O8 W10 O18 169.1(15) . . ? O8 W10 O7 103.5(12) . . ? O8 W10 O34 95.7(13) . . ? O8 W10 K2 147.9(11) . 2_766 ? O8 W10 K1 51.5(7) . . ? O18 W10 W7 78.7(8) . . ? O18 W10 O34 73.4(9) . . ? O18 W10 K2 42.9(6) . 2_766 ? O18 W10 K1 131.5(10) . . ? O7 W10 W7 127.7(11) . . ? O7 W10 O18 87.4(12) . . ? O7 W10 O34 160.7(16) . . ? O7 W10 K2 44.7(7) . 2_766 ? O7 W10 K1 81.0(8) . . ? O34 W10 W7 47.5(6) . . ? O34 W10 K2 116.0(10) . 2_766 ? O34 W10 K1 110.2(10) . . ? K1 W10 K2 108.4(6) . 2_766 ? O32 W12 W3 46.5(6) . . ? O8 W12 W3 131.1(9) . . ? O8 W12 O32 84.7(8) . . ? O20 W12 W3 87.1(8) . . ? O20 W12 O32 74.9(8) . . ? O20 W12 O8 80.6(9) . . ? O10 W12 W3 34.0(6) . . ? O10 W12 O32 79.9(11) . . ? O10 W12 O8 163.8(13) . . ? O10 W12 O20 90.4(10) . . ? O10 W12 O9 104.8(11) . . ? O10 W12 O2 98.9(13) . . ? O9 W12 W3 138.8(11) . . ? O9 W12 O32 167.7(12) . . ? O9 W12 O8 89.4(12) . . ? O9 W12 O20 93.5(10) . . ? O2 W12 W3 92.6(10) . . ? O2 W12 O32 92.5(10) . . ? O2 W12 O8 86.8(10) . . ? O2 W12 O20 162.9(12) . . ? O2 W12 O9 97.9(10) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag W6 O24 1.983(11) . ? W6 O16 1.898(11) . ? W6 O18 1.943(11) . ? W6 O17 1.736(13) . ? W6 O6 1.824(10) . ? W6 O34 2.289(13) . ? W1 O1 1.773(12) . ? W1 O19 2.053(13) . ? W1 O8 1.975(15) . ? W1 O18 1.909(14) . ? W1 O7 1.714(13) . ? W1 O34 2.301(13) . ? W1 K2 3.639(10) 2_766 ? W1 K1 3.782(10) . ? W5 O5 1.962(10) . ? W5 O23 1.891(11) . ? W5 O16 1.932(11) . ? W5 O14 1.848(12) . ? W5 O33 2.315(12) . ? W5 O15 1.714(13) . ? W2 O32 2.321(12) . ? W2 O8 1.910(14) . ? W2 O20 2.035(13) . ? W2 O10 1.931(15) . ? W2 O9 1.721(15) . ? W2 O2 1.788(12) . ? W2 K1 3.963(9) . ? W7 O27 1.941(12) . ? W7 O24 1.877(11) . ? W7 O19 1.860(12) . ? W7 O25 1.936(14) . ? W7 O34 2.362(11) . ? W7 O28 1.700(12) . ? W7 K1 4.023(6) . ? W7 W10 3.20(3) . ? W7A W9 3.232(11) . ? W7A O27 1.473(17) . ? W7A O24 2.156(16) . ? W7A O19 2.322(16) . ? W7A O25 1.724(18) . ? W7A O34 2.417(16) . ? W7A O28 1.854(17) . ? W4 O4 1.752(12) . ? W4 O14 2.026(12) . ? W4 O33 2.260(12) . ? W4 O22 2.063(13) . ? W4 O12 1.896(13) . ? W4 O13 1.746(13) . ? W4 K1 3.738(6) 1_455 ? W8 O32 2.358(14) . ? W8 O20 1.840(14) . ? W8 O21 1.970(14) . ? W8 O26 1.978(15) . ? W8 O25 1.848(16) . ? W8 O29 1.695(14) . ? W8A W3 3.235(14) . ? W8A O32 2.247(18) . ? W8A O20 1.987(18) . ? W8A O21 1.734(18) . ? W8A O26 1.812(19) . ? W8A O25 2.04(2) . ? W8A O29 1.820(19) . ? W9 O27 1.918(12) . ? W9 O23 1.971(11) . ? W9 O33 2.360(11) . ? W9 O22 1.886(13) . ? W9 O26 1.903(13) . ? W9 O30 1.731(12) . ? W3 O3 1.767(11) . ? W3 O32 2.264(12) . ? W3 O21 2.053(11) . ? W3 O10 1.962(13) . ? W3 O12 1.940(13) . ? W3 O11 1.703(17) . ? W3 W12 3.12(3) . ? Ge1 O32 1.778(12) . ? Ge1 O33 1.740(12) . ? Ge1 O34 1.738(12) . ? Ge1 O31 1.744(11) . ? Zn3 O38 2.039(11) . ? Zn3 O35 2.093(13) . ? Zn3 O37 2.107(13) . ? Zn3 O36 2.170(13) . ? Zn3 O39 2.096(13) . ? Zn3 O40 2.097(14) . ? O5 Zn1 2.102(10) . ? O3 Zn2 2.049(11) . ? O51 Zn1 2.063(12) . ? O51 K1 3.080(18) 1_455 ? O4 Zn1 2.045(14) . ? O4 K1 2.983(13) 1_455 ? O32 W12 2.17(2) . ? O1 Zn2 2.107(11) 2_666 ? O1 Zn1 2.114(11) 2_666 ? O1 W10 1.88(3) . ? O19 K1 2.867(14) . ? O19 W10 1.90(3) . ? O8 K1 2.858(13) . ? O8 W10 1.75(3) . ? O8 W12 2.11(3) . ? O20 K1 3.207(15) . ? O20 W12 2.03(2) . ? O18 K2 2.757(13) 2_766 ? O18 W10 2.07(3) . ? O7 K2 2.869(14) 2_766 ? O7 K1 3.217(13) 2_766 ? O7 W10 1.90(3) . ? O10 W12 1.69(3) . ? O38 N1 1.312(17) . ? O6 Zn2 2.045(11) 2_666 ? O13 K1 2.989(15) 1_455 ? O25 K1 3.276(14) . ? O9 K2 2.621(15) . ? O9 W12 1.87(3) . ? O34 W10 2.15(2) . ? N1 C5 1.38(2) . ? N1 C1 1.35(2) . ? O47 N5 1.35(3) . ? O44 N2 1.33(2) . ? O46 N4 1.294(16) . ? C2 H2 0.9300 . ? C2 C3 1.40(2) . ? C2 C1 1.37(2) . ? C5 H5 0.9300 . ? C5 C4 1.35(2) . ? O45 N3 1.323(18) . ? N2 C9 1.36(2) . ? N2 C8 1.34(2) . ? C10 H10 0.9300 . ? C10 C9 1.30(3) . ? C10 C6 1.45(2) . ? C3 C6 1.46(2) . ? C3 C4 1.39(2) . ? C1 H1 0.9300 . ? C9 H9 0.9300 . ? N5 C25 1.39(3) . ? N5 C21 1.41(3) . ? C13 C12 1.3900 . ? C13 C14 1.3900 . ? C13 C16 1.483(12) . ? C12 H12 0.9300 . ? C12 C11 1.3900 . ? C11 N3 1.3900 . ? N3 C15 1.3900 . ? C15 H15 0.9300 . ? C15 C14 1.3900 . ? C14 H14 0.9300 . ? C16 C20 1.3900 . ? C16 C17 1.3900 . ? C20 H20 0.9300 . ? C20 C19 1.3900 . ? C19 H19 0.9300 . ? C19 N4 1.3900 . ? N4 C18 1.3900 . ? C18 H18 0.9300 . ? C18 C17 1.3900 . ? C17 H17 0.9300 . ? C6 C7 1.39(2) . ? C8 H8 0.9300 . ? C8 C7 1.36(3) . ? C4 H4 0.9300 . ? C7 H7 0.9300 . ? C25 H25 0.9300 . ? C25 C24 1.31(3) . ? C24 H24 0.9300 . ? C24 C23 1.43(3) . ? C22 H22 0.9300 . ? C22 C23 1.42(3) . ? C22 C21 1.34(4) . ? C23 C23 1.42(5) 2_677 ? C21 H21 0.9300 . ? O49 K2 2.748(17) . ? O49 K1 2.853(17) . ? O48 K2 2.727(19) . ? O50 K2 2.900(19) 2_666 ? O52 H52A 1.1034 . ? O52 H52B 1.1054 . ? O52 K2 2.66(2) 2_776 ? Zn2 Zn1 3.148(3) . ? Zn2 O2 2.162(11) . ? Zn2 O31 2.093(11) . ? Zn2 O31 2.138(12) 2_666 ? Zn1 O2 2.148(12) 2_666 ? Zn1 O31 2.103(11) . ? Zn1 K1 4.098(8) 1_455 ? O2 W12 1.77(2) . ? O35 H35A 0.8731 . ? O35 H35B 0.8713 . ? O37 H37A 0.8787 . ? O37 H37B 0.8791 . ? O36 H36A 0.8969 . ? O36 H36B 0.9002 . ? O39 H39A 0.9155 . ? O39 H39B 0.9202 . ? O40 H40A 0.8587 . ? O40 H40B 0.8581 . ? O43 H43A 0.9300 . ? O43 H43B 0.9300 . ? O43 Zn4 2.05(2) . ? O41 H41A 1.1551 . ? O41 H41B 1.1571 . ? O41 Zn4 2.13(2) . ? Zn4 O42 2.02(3) 2_567 ? Zn4 O42 2.02(3) . ? O42 H42A 1.0378 . ? O42 H42B 1.0288 . ? K2 K1 4.170(9) . ? K2 W10 3.89(3) 2_766 ? K1 O54 3.37(3) 1_655 ? K1 W10 3.60(3) . ? O53 H53A 0.8497 . ? O53 H53B 0.8491 . ? O54 H54A 0.9688 . ? O54 H54B 0.9711 . ? O55 H55A 0.8499 . ? O55 H55B 0.8505 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag W7A W9 O22 W4 28.8(15) . . . . ? W8A W3 O3 Zn2 -27.6(12) . . . . ? W9 W7A O25 W8A -9.5(12) . . . . ? W9 W7A O25 K1 -176.7(4) . . . . ? W3 W8A O21 W8 -110(6) . . . . ? W3 W8A O26 W8 157(5) . . . . ? W3 W8A O26 W9 95(2) . . . . ? W3 W8A O29 W8 -133(5) . . . . ? W3 O10 W12 O32 -9.6(9) . . . . ? W3 O10 W12 O8 -28(5) . . . . ? W3 O10 W12 O20 -84.2(10) . . . . ? W3 O10 W12 O9 -177.9(7) . . . . ? W3 O10 W12 O2 81.4(11) . . . . ? Zn3 O38 N1 C5 71.6(19) . . . . ? Zn3 O38 N1 C1 -107.6(15) . . . . ? O5 W5 O23 W9 18.6(17) . . . . ? O5 W5 O14 W4 -81.6(7) . . . . ? O27 W7 O24 W6 86.0(7) . . . . ? O27 W7 O19 K1 98.7(13) . . . . ? O27 W7 O19 W10 -12(2) . . . . ? O27 W7A O25 W8A -13.9(16) . . . . ? O27 W7A O25 K1 178.9(7) . . . . ? O27 W9 O22 W4 0(2) . . . . ? O24 W6 O16 W5 131.7(16) . . . . ? O24 W6 O6 Zn2 36(2) . . . 2_666 ? O24 W7 O19 K1 -171.9(5) . . . . ? O24 W7 O19 W10 77.0(12) . . . . ? O24 W7A O27 W9 -144.4(12) . . . . ? O24 W7A O25 W8A 117.8(16) . . . . ? O24 W7A O25 K1 -49.4(18) . . . . ? O23 W5 O14 W4 76.7(7) . . . . ? O23 W9 O22 W4 -76.1(8) . . . . ? O16 W6 O6 Zn2 118.4(10) . . . 2_666 ? O16 W5 O23 W9 88.5(7) . . . . ? O16 W5 O14 W4 -14.6(17) . . . . ? O4 W4 O12 W3 -17.5(14) . . . . ? O4 W4 O13 K1 9.3(7) . . . 1_455 ? O32 W2 O9 K2 92(3) . . . . ? O32 W2 O2 Zn2 28.3(9) . . . . ? O32 W2 O2 Zn1 -123.8(7) . . . 2_666 ? O32 W8 O20 W8A 50(5) . . . . ? O32 W8 O20 K1 -110.5(6) . . . . ? O32 W8 O20 W12 4.8(10) . . . . ? O32 W8 O25 W7 -59.9(17) . . . . ? O32 W8 O25 W8A -52(5) . . . . ? O32 W8 O25 K1 97.9(5) . . . . ? O32 W8 O29 W8A 60(5) . . . . ? O32 W8A O21 W8 -106(6) . . . . ? O32 W8A O21 W3 4.0(7) . . . . ? O32 W8A O26 W8 112(5) . . . . ? O32 W8A O26 W9 51(2) . . . . ? O32 W8A O29 W8 -42(4) . . . . ? O32 W3 O3 Zn2 -25.7(9) . . . . ? O32 Ge1 O33 W5 -175.3(6) . . . . ? O32 Ge1 O33 W4 64.5(7) . . . . ? O32 Ge1 O33 W9 -55.9(8) . . . . ? O32 Ge1 O34 W6 177.1(6) . . . . ? O32 Ge1 O34 W1 -64.0(9) . . . . ? O32 Ge1 O34 W7 56.2(8) . . . . ? O32 Ge1 O34 W7A 60.5(7) . . . . ? O32 Ge1 O34 W10 -56.9(12) . . . . ? O32 Ge1 O31 Zn2 -1.9(8) . . . . ? O32 Ge1 O31 Zn2 122.5(6) . . . 2_666 ? O32 Ge1 O31 Zn1 -120.7(6) . . . . ? O1 W1 O7 K2 -96.6(6) . . . 2_766 ? O1 W1 O7 K1 -0.6(11) . . . 2_766 ? O19 W1 O1 Zn2 -52(2) . . . 2_666 ? O19 W1 O1 Zn1 117.3(16) . . . 2_666 ? O19 W1 O7 K2 85.6(6) . . . 2_766 ? O19 W1 O7 K1 -178.5(7) . . . 2_766 ? O19 W7 O24 W6 -71.9(7) . . . . ? O19 W7A O27 W9 -96(3) . . . . ? O19 W7A O25 W8A 145.3(11) . . . . ? O19 W7A O25 K1 -21.9(6) . . . . ? O14 W5 O23 W9 -69.0(7) . . . . ? O14 W4 O4 Zn1 -42.7(10) . . . . ? O14 W4 O4 K1 89.2(5) . . . 1_455 ? O14 W4 O12 W3 81.3(18) . . . . ? O14 W4 O13 K1 -82.2(5) . . . 1_455 ? O8 W1 O1 Zn2 -124.5(9) . . . 2_666 ? O8 W1 O1 Zn1 44.9(8) . . . 2_666 ? O8 W1 O7 K2 170.8(5) . . . 2_766 ? O8 W1 O7 K1 -93.2(8) . . . 2_766 ? O8 W2 O9 K2 -28.2(15) . . . . ? O8 W2 O2 Zn2 113.5(9) . . . . ? O8 W2 O2 Zn1 -38.7(8) . . . 2_666 ? O20 W2 O9 K2 58.8(15) . . . . ? O20 W2 O2 Zn2 30(2) . . . . ? O20 W2 O2 Zn1 -122.6(16) . . . 2_666 ? O20 W8 O25 W7 -133.7(17) . . . . ? O20 W8 O25 W8A -126(5) . . . . ? O20 W8 O25 K1 24.1(6) . . . . ? O20 W8 O29 W8A 124(5) . . . . ? O20 W8A O21 W8 -33(6) . . . . ? O20 W8A O21 W3 77.3(9) . . . . ? O20 W8A O26 W8 75(5) . . . . ? O20 W8A O26 W9 14(5) . . . . ? O20 W8A O29 W8 -49(4) . . . . ? O18 W6 O16 W5 64(2) . . . . ? O18 W6 O6 Zn2 -39.1(10) . . . 2_666 ? O18 W1 O1 Zn2 33.2(10) . . . 2_666 ? O18 W1 O1 Zn1 -157.4(8) . . . 2_666 ? O18 W1 O7 K2 0.9(6) . . . 2_766 ? O18 W1 O7 K1 96.8(8) . . . 2_766 ? O7 W1 O1 Zn2 133.3(9) . . . 2_666 ? O7 W1 O1 Zn1 -57.3(10) . . . 2_666 ? O33 W5 O23 W9 3.9(6) . . . . ? O33 W5 O14 W4 1.8(6) . . . . ? O33 W4 O4 Zn1 29.4(10) . . . . ? O33 W4 O4 K1 161.3(5) . . . 1_455 ? O33 W4 O12 W3 70.2(13) . . . . ? O33 W4 O13 K1 -129(2) . . . 1_455 ? O33 W9 O22 W4 -3.2(6) . . . . ? O33 Ge1 O32 W2 177.9(6) . . . . ? O33 Ge1 O32 W8 60.4(8) . . . . ? O33 Ge1 O32 W8A 52.3(9) . . . . ? O33 Ge1 O32 W3 -64.7(7) . . . . ? O33 Ge1 O32 W12 -176.9(9) . . . . ? O33 Ge1 O34 W6 62.0(8) . . . . ? O33 Ge1 O34 W1 -179.1(7) . . . . ? O33 Ge1 O34 W7 -58.8(8) . . . . ? O33 Ge1 O34 W7A -54.6(7) . . . . ? O33 Ge1 O34 W10 -172.0(10) . . . . ? O33 Ge1 O31 Zn2 118.1(6) . . . . ? O33 Ge1 O31 Zn2 -117.5(6) . . . 2_666 ? O33 Ge1 O31 Zn1 -0.6(8) . . . . ? O21 W8 O20 W8A -21(5) . . . . ? O21 W8 O20 K1 178.4(5) . . . . ? O21 W8 O20 W12 -66.3(11) . . . . ? O21 W8 O25 W7 -42(3) . . . . ? O21 W8 O25 W8A -34(4) . . . . ? O21 W8 O25 K1 116.1(15) . . . . ? O21 W8 O29 W8A 33(4) . . . . ? O21 W8A O26 W8 -169(5) . . . . ? O21 W8A O26 W9 129.7(19) . . . . ? O21 W8A O29 W8 -141(5) . . . . ? O21 W3 O3 Zn2 -23(2) . . . . ? O10 W2 O9 K2 144.3(13) . . . . ? O10 W2 O2 Zn2 -43.3(9) . . . . ? O10 W2 O2 Zn1 164.5(7) . . . 2_666 ? O10 W3 O3 Zn2 46.8(9) . . . . ? O22 W4 O4 Zn1 23(2) . . . . ? O22 W4 O4 K1 155.0(15) . . . 1_455 ? O22 W4 O12 W3 143.6(14) . . . . ? O22 W4 O13 K1 -165.7(5) . . . 1_455 ? O38 N1 C5 C4 179.9(16) . . . . ? O38 N1 C1 C2 -177.9(15) . . . . ? O17 W6 O16 W5 -131.9(15) . . . . ? O17 W6 O6 Zn2 -139.4(10) . . . 2_666 ? O6 W6 O16 W5 -26.7(16) . . . . ? O12 W4 O4 Zn1 114.1(10) . . . . ? O12 W4 O4 K1 -114.0(5) . . . 1_455 ? O12 W4 O13 K1 106.8(5) . . . 1_455 ? O12 W3 O3 Zn2 -109.5(9) . . . . ? O26 W8 O20 W8A 53(4) . . . . ? O26 W8 O20 K1 -107.8(18) . . . . ? O26 W8 O20 W12 8(2) . . . . ? O26 W8 O25 W7 23.7(18) . . . . ? O26 W8 O25 W8A 31(5) . . . . ? O26 W8 O25 K1 -178.6(5) . . . . ? O26 W8 O29 W8A -53(4) . . . . ? O26 W8A O21 W8 165(7) . . . . ? O26 W8A O21 W3 -85.1(9) . . . . ? O26 W8A O29 W8 119(5) . . . . ? O26 W9 O22 W4 82.2(8) . . . . ? O13 W4 O4 Zn1 -141.2(10) . . . . ? O13 W4 O4 K1 -9.3(7) . . . 1_455 ? O13 W4 O12 W3 -121.4(13) . . . . ? O15 W5 O23 W9 -170.4(7) . . . . ? O15 W5 O14 W4 176.3(6) . . . . ? O25 W7 O24 W6 14.8(18) . . . . ? O25 W7 O19 K1 30.1(5) . . . . ? O25 W7 O19 W10 -81.1(12) . . . . ? O25 W7A O27 W9 13.1(17) . . . . ? O25 W8 O20 W8A 135(5) . . . . ? O25 W8 O20 K1 -25.0(6) . . . . ? O25 W8 O20 W12 90.3(11) . . . . ? O25 W8 O29 W8A -142(5) . . . . ? O25 W8A O21 W8 -101(7) . . . . ? O25 W8A O21 W3 9(4) . . . . ? O25 W8A O26 W8 28(4) . . . . ? O25 W8A O26 W9 -33(2) . . . . ? O25 W8A O29 W8 33(4) . . . . ? O30 W9 O22 W4 -175.3(7) . . . . ? O9 W2 O2 Zn2 -144.7(8) . . . . ? O9 W2 O2 Zn1 63.1(9) . . . 2_666 ? O34 W6 O16 W5 58.2(15) . . . . ? O34 W6 O6 Zn2 33.4(10) . . . 2_666 ? O34 W1 O1 Zn2 -39.3(10) . . . 2_666 ? O34 W1 O1 Zn1 130.1(8) . . . 2_666 ? O34 W1 O7 K2 46(3) . . . 2_766 ? O34 W1 O7 K1 142(3) . . . 2_766 ? O34 W7 O24 W6 1.0(6) . . . . ? O34 W7 O19 K1 115.8(6) . . . . ? O34 W7 O19 W10 4.6(11) . . . . ? O34 W7A O27 W9 -76.4(14) . . . . ? O34 W7A O25 W8A 79.7(12) . . . . ? O34 W7A O25 K1 -87.5(6) . . . . ? O34 Ge1 O32 W2 63.1(7) . . . . ? O34 Ge1 O32 W8 -54.4(8) . . . . ? O34 Ge1 O32 W8A -62.5(9) . . . . ? O34 Ge1 O32 W3 -179.4(6) . . . . ? O34 Ge1 O32 W12 68.4(11) . . . . ? O34 Ge1 O33 W5 -59.6(8) . . . . ? O34 Ge1 O33 W4 -179.8(6) . . . . ? O34 Ge1 O33 W9 59.9(8) . . . . ? O34 Ge1 O31 Zn2 -122.7(6) . . . . ? O34 Ge1 O31 Zn2 1.7(8) . . . 2_666 ? O34 Ge1 O31 Zn1 118.5(6) . . . . ? O29 W8 O20 W8A -121(5) . . . . ? O29 W8 O20 K1 79.0(8) . . . . ? O29 W8 O20 W12 -165.8(11) . . . . ? O29 W8 O25 W7 123.8(17) . . . . ? O29 W8 O25 W8A 132(5) . . . . ? O29 W8 O25 K1 -78.4(7) . . . . ? O29 W8A O21 W8 60(6) . . . . ? O29 W8A O21 W3 170.1(7) . . . . ? O29 W8A O26 W8 -63(4) . . . . ? O29 W8A O26 W9 -124.4(19) . . . . ? N1 C5 C4 C3 -2(3) . . . . ? O28 W7 O24 W6 -173.4(7) . . . . ? O28 W7 O19 K1 -70.4(7) . . . . ? O28 W7 O19 W10 178.4(12) . . . . ? O28 W7A O27 W9 128.0(12) . . . . ? O28 W7A O25 W8A -136.1(11) . . . . ? O28 W7A O25 K1 56.7(9) . . . . ? O11 W3 O3 Zn2 148.9(9) . . . . ? O47 N5 C25 C24 -175(2) . . . . ? O47 N5 C21 C22 176.8(19) . . . . ? O44 N2 C9 C10 176.5(18) . . . . ? O44 N2 C8 C7 -177.2(18) . . . . ? O46 N4 C18 C17 176.8(13) . . . . ? C2 C3 C6 C10 165.1(16) . . . . ? C2 C3 C6 C7 -16(3) . . . . ? C2 C3 C4 C5 3(3) . . . . ? C5 N1 C1 C2 3(2) . . . . ? O45 N3 C15 C14 -172.5(17) . . . . ? N2 C8 C7 C6 3(3) . . . . ? C10 C6 C7 C8 -1(3) . . . . ? C3 C2 C1 N1 -2(2) . . . . ? C3 C6 C7 C8 -180.0(18) . . . . ? C1 N1 C5 C4 -1(3) . . . . ? C1 C2 C3 C6 179.8(15) . . . . ? C1 C2 C3 C4 -1(2) . . . . ? C9 N2 C8 C7 -5(3) . . . . ? C9 C10 C6 C3 179.2(17) . . . . ? C9 C10 C6 C7 0(2) . . . . ? N5 C25 C24 C23 -2(3) . . . . ? C13 C12 C11 N3 0.0 . . . . ? C13 C16 C20 C19 178.5(12) . . . . ? C13 C16 C17 C18 -178.5(12) . . . . ? C12 C13 C14 C15 0.0 . . . . ? C12 C13 C16 C20 164.2(8) . . . . ? C12 C13 C16 C17 -17.3(14) . . . . ? C12 C11 N3 O45 172.3(18) . . . . ? C12 C11 N3 C15 0.0 . . . . ? C11 N3 C15 C14 0.0 . . . . ? N3 C15 C14 C13 0.0 . . . . ? C14 C13 C12 C11 0.0 . . . . ? C14 C13 C16 C20 -13.4(13) . . . . ? C14 C13 C16 C17 165.1(8) . . . . ? C16 C13 C12 C11 -177.6(13) . . . . ? C16 C13 C14 C15 177.6(13) . . . . ? C16 C20 C19 N4 0.0 . . . . ? C20 C16 C17 C18 0.0 . . . . ? C20 C19 N4 O46 -176.7(14) . . . . ? C20 C19 N4 C18 0.0 . . . . ? C19 N4 C18 C17 0.0 . . . . ? N4 C18 C17 C16 0.0 . . . . ? C17 C16 C20 C19 0.0 . . . . ? C6 C10 C9 N2 -2(3) . . . . ? C6 C3 C4 C5 -177.8(17) . . . . ? C8 N2 C9 C10 4(3) . . . . ? C4 C3 C6 C10 -14(3) . . . . ? C4 C3 C6 C7 164.9(18) . . . . ? C25 N5 C21 C22 -2(3) . . . . ? C25 C24 C23 C22 -2(3) . . . . ? C25 C24 C23 C23 -179(2) . . . 2_677 ? C23 C22 C21 N5 -1(3) . . . . ? C21 N5 C25 C24 3(3) . . . . ? C21 C22 C23 C24 3(3) . . . . ? C21 C22 C23 C23 -179(2) . . . 2_677 ? Zn2 O1 W10 W7 -22(3) 2_666 . . . ? Zn2 O1 W10 O19 -1(8) 2_666 . . . ? Zn2 O1 W10 O8 -121.1(12) 2_666 . . . ? Zn2 O1 W10 O18 48.0(16) 2_666 . . . ? Zn2 O1 W10 O7 135.2(10) 2_666 . . . ? Zn2 O1 W10 O34 -25.5(17) 2_666 . . . ? Zn2 O1 W10 K2 90.4(12) 2_666 . . 2_766 ? Zn2 O1 W10 K1 -144.7(11) 2_666 . . . ? Zn2 O2 W12 W3 -10.0(11) . . . . ? Zn2 O2 W12 O32 36.5(13) . . . . ? Zn2 O2 W12 O8 121.0(10) . . . . ? Zn2 O2 W12 O20 79(6) . . . . ? Zn2 O2 W12 O10 -43.7(14) . . . . ? Zn2 O2 W12 O9 -150.0(9) . . . . ? Zn1 O1 W10 W7 132.3(12) 2_666 . . . ? Zn1 O1 W10 O19 154(6) 2_666 . . . ? Zn1 O1 W10 O8 33.6(15) 2_666 . . . ? Zn1 O1 W10 O18 -157.3(8) 2_666 . . . ? Zn1 O1 W10 O7 -70.2(15) 2_666 . . . ? Zn1 O1 W10 O34 129.2(9) 2_666 . . . ? Zn1 O1 W10 K2 -115.0(9) 2_666 . . 2_766 ? Zn1 O1 W10 K1 10(2) 2_666 . . . ? Zn1 O2 W12 W3 -164.5(8) 2_666 . . . ? Zn1 O2 W12 O32 -117.9(11) 2_666 . . . ? Zn1 O2 W12 O8 -33.4(13) 2_666 . . . ? Zn1 O2 W12 O20 -76(6) 2_666 . . . ? Zn1 O2 W12 O10 161.9(9) 2_666 . . . ? Zn1 O2 W12 O9 55.5(15) 2_666 . . . ? O2 W2 O9 K2 -123.3(13) . . . . ? O31 Ge1 O32 W2 -59.4(8) . . . . ? O31 Ge1 O32 W8 -176.9(6) . . . . ? O31 Ge1 O32 W8A 175.0(7) . . . . ? O31 Ge1 O32 W3 58.0(7) . . . . ? O31 Ge1 O32 W12 -54.2(11) . . . . ? O31 Ge1 O33 W5 62.2(8) . . . . ? O31 Ge1 O33 W4 -58.0(8) . . . . ? O31 Ge1 O33 W9 -178.4(6) . . . . ? O31 Ge1 O34 W6 -60.2(8) . . . . ? O31 Ge1 O34 W1 58.7(9) . . . . ? O31 Ge1 O34 W7 179.0(6) . . . . ? O31 Ge1 O34 W7A -176.8(6) . . . . ? O31 Ge1 O34 W10 65.8(12) . . . . ? K2 W1 O1 Zn2 81.1(9) 2_766 . . 2_666 ? K2 W1 O1 Zn1 -109.5(7) 2_766 . . 2_666 ? K2 W1 O7 K1 96.0(9) 2_766 . . 2_766 ? K2 O9 W12 W3 134.2(18) . . . . ? K2 O9 W12 O32 25(8) . . . . ? K2 O9 W12 O8 -36(2) . . . . ? K2 O9 W12 O20 45(3) . . . . ? K2 O9 W12 O10 135.9(19) . . . . ? K2 O9 W12 O2 -122.6(19) . . . . ? K1 W1 O1 Zn2 -140.1(7) . . . 2_666 ? K1 W1 O1 Zn1 29.3(11) . . . 2_666 ? K1 W1 O7 K2 129.5(4) . . . 2_766 ? K1 W1 O7 K1 -134.5(8) . . . 2_766 ? K1 W2 O9 K2 8.4(13) . . . . ? K1 W2 O2 Zn2 128.3(7) . . . . ? K1 W2 O2 Zn1 -23.9(10) . . . 2_666 ? K1 W7 O24 W6 -78.9(7) . . . . ? K1 W7 O19 W10 -111.2(13) . . . . ? K1 W4 O4 Zn1 -131.9(12) 1_455 . . . ? K1 W4 O12 W3 -67.6(14) 1_455 . . . ? K1 O8 W10 W7 63.6(6) . . . . ? K1 O8 W10 O1 -161.1(8) . . . . ? K1 O8 W10 O19 32.3(10) . . . . ? K1 O8 W10 O18 111(8) . . . . ? K1 O8 W10 O7 -66.6(12) . . . . ? K1 O8 W10 O34 111.3(8) . . . . ? K1 O8 W10 K2 -59(2) . . . 2_766 ? W10 W7 O24 W6 -40.7(7) . . . . ? W10 W7 O19 K1 111.2(13) . . . . ? W12 W3 O3 Zn2 18.3(9) . . . . ? W12 O8 W10 W7 -95(2) . . . . ? W12 O8 W10 O1 40(2) . . . . ? W12 O8 W10 O19 -126.7(18) . . . . ? W12 O8 W10 O18 -48(9) . . . . ? W12 O8 W10 O7 134.4(17) . . . . ? W12 O8 W10 O34 -48(2) . . . . ? W12 O8 W10 K2 141.6(16) . . . 2_766 ? W12 O8 W10 K1 -159(2) . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.500 0.500 0.000 69.7 24.9 ?