#------------------------------------------------------------------------------ #$Date: 2024-12-06 22:01:22 +0200 (Fri, 06 Dec 2024) $ #$Revision: 296614 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/94/7249418.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7249418 loop_ _publ_author_name 'Chiu, Wei-Jung' 'Sun, Chung-Ming' _publ_section_title ; Electrochemistry-enabled Rh-catalyzed regioselective [4 + 1] and [4 + 2] cycloaddition of benzoic acid with alkynyl esters/amides ; _journal_issue 21 _journal_name_full 'Green Chemistry' _journal_page_first 10996 _journal_page_last 11002 _journal_paper_doi 10.1039/D4GC03753G _journal_volume 26 _journal_year 2024 _chemical_formula_moiety 'C20 H22 O4' _chemical_formula_sum 'C20 H22 O4' _chemical_formula_weight 326.37 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2024-03-25 _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _audit_update_record ; 2024-03-27 deposited with the CCDC. 2024-10-02 downloaded from the CCDC. ; _cell_angle_alpha 83.847(2) _cell_angle_beta 78.595(2) _cell_angle_gamma 81.772(2) _cell_formula_units_Z 2 _cell_length_a 7.4776(2) _cell_length_b 9.1826(2) _cell_length_c 12.9115(3) _cell_measurement_reflns_used 7485 _cell_measurement_temperature 99.98(10) _cell_measurement_theta_max 72.0950 _cell_measurement_theta_min 3.4880 _cell_volume 857.25(4) _computing_cell_refinement 'CrysAlisPro 1.171.42.96a (Rigaku OD, 2023)' _computing_data_collection 'CrysAlisPro 1.171.42.96a (Rigaku OD, 2023)' _computing_data_reduction 'CrysAlisPro 1.171.42.96a (Rigaku OD, 2023)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 99.98(10) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type 'HyPix-Arc 150' _diffrn_measured_fraction_theta_full 0.989 _diffrn_measured_fraction_theta_max 0.989 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 59.00 120.00 0.50 0.05 -- 69.38 15.00-180.00 122 2 \w 39.00 117.00 0.50 0.05 -- 69.38 15.00 -90.00 156 3 \w 37.00 106.00 0.50 0.05 -- 56.15 15.00 30.00 138 4 \w 46.00 126.00 0.50 0.05 -- 80.61 15.00 -60.00 160 5 \w 46.00 71.00 0.50 0.05 -- 80.61 15.00 30.00 50 6 \w 74.00 110.00 0.50 0.05 -- 80.61 15.00 30.00 72 7 \w 73.00 121.00 0.50 0.05 -- 80.61 15.00 60.00 96 8 \w 66.00 107.00 0.50 0.05 -- 80.61 15.00 150.00 82 9 \w 39.00 74.00 0.50 0.05 -- 80.61-111.00 30.00 70 10 \w 68.00 93.00 0.50 0.05 -- 80.00-105.00-121.25 50 11 \w 41.00 67.00 0.50 0.05 -- 80.00-105.00-121.25 52 12 \w 60.00 86.00 0.50 0.05 -- 80.61-100.00-146.00 52 13 \w 54.00 80.00 0.50 0.05 -- 69.38-100.00-146.00 52 14 \w 14.00 53.00 0.50 0.05 -- 56.15-100.00-146.00 78 15 \w 39.00 64.00 0.50 0.05 -- 80.61 -95.00-120.00 50 16 \w 40.00 65.00 0.50 0.05 -- 80.61 -95.00 -30.00 50 17 \w 18.00 51.00 0.50 0.05 -- 56.15 -95.00 30.00 66 18 \w 13.00 41.00 0.50 0.05 -- 56.15 -95.00 90.00 56 19 \w 38.00 66.00 0.50 0.05 -- 80.61 -95.00 90.00 56 20 \w 43.00 88.00 0.50 0.05 -- 80.61 -95.00 60.00 90 21 \w 27.00 57.00 0.50 0.05 -- 69.38 -95.00 -90.00 60 22 \w -56.00 -30.00 0.50 0.05 -- -59.22 100.00 -42.00 52 23 \w -97.00 -70.00 0.50 0.05 -- -81.00 114.00-123.49 54 24 \w -97.00 -72.00 0.50 0.05 -- -81.00 116.00 -52.33 50 25 \w -66.00 -35.00 0.50 0.05 -- -81.00 114.00-123.49 62 26 \w -97.00 -35.00 0.50 0.05 -- -81.00 115.00 -17.34 124 27 \w -95.00 -36.00 0.50 0.05 -- -81.00 114.00 70.98 118 28 \w -97.00 -39.00 0.50 0.05 -- -81.00 116.00 133.85 116 29 \w -98.00 -42.00 0.50 0.05 -- -81.00 118.00 98.49 112 30 \w -90.00 -50.00 0.50 0.05 -- -76.67 111.00 150.00 80 31 \w -92.00 -43.00 0.50 0.05 -- -76.67 111.00 90.00 98 32 \w -79.00 -54.00 0.50 0.05 -- -71.82 100.00 -42.00 50 33 \w -77.00 -51.00 0.50 0.05 -- -76.67 100.00 -42.00 52 34 \w -88.00 -32.00 0.50 0.05 -- -76.67 111.00 -90.00 112 35 \w -126.00 -44.00 0.50 0.05 -- -76.67 -15.00 90.00 164 36 \w -115.00 -41.00 0.50 0.05 -- -76.67 -15.00 0.00 148 37 \w -112.00 -87.00 0.50 0.05 -- -76.67 -15.00-120.00 50 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy R, DW system, HyPix-Arc 150' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.1178349000 _diffrn_orient_matrix_UB_12 -0.1516670000 _diffrn_orient_matrix_UB_13 -0.0093659000 _diffrn_orient_matrix_UB_21 -0.0244194000 _diffrn_orient_matrix_UB_22 0.0019977000 _diffrn_orient_matrix_UB_23 -0.1158774000 _diffrn_orient_matrix_UB_31 0.1743382000 _diffrn_orient_matrix_UB_32 0.0769395000 _diffrn_orient_matrix_UB_33 -0.0374070000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0318 _diffrn_reflns_av_unetI/netI 0.0226 _diffrn_reflns_Laue_measured_fraction_full 0.989 _diffrn_reflns_Laue_measured_fraction_max 0.989 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 10200 _diffrn_reflns_point_group_measured_fraction_full 0.989 _diffrn_reflns_point_group_measured_fraction_max 0.989 _diffrn_reflns_theta_full 67.068 _diffrn_reflns_theta_max 67.068 _diffrn_reflns_theta_min 3.504 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'Rigaku (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.707 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.91784 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.96a (Rigaku Oxford Diffraction, 2023) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.264 _exptl_crystal_description block _exptl_crystal_F_000 348 _exptl_crystal_size_max 0.21 _exptl_crystal_size_mid 0.13 _exptl_crystal_size_min 0.1 _refine_diff_density_max 0.275 _refine_diff_density_min -0.240 _refine_diff_density_rms 0.059 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.069 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 219 _refine_ls_number_reflns 3011 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.069 _refine_ls_R_factor_all 0.0426 _refine_ls_R_factor_gt 0.0352 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0438P)^2^+0.3614P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0892 _refine_ls_wR_factor_ref 0.0943 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2797 _reflns_number_total 3011 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4gc03753g2.cif _cod_data_source_block 240370lt_auto _cod_depositor_comments 'Adding full bibliography for 7249417--7249418.cif.' _cod_database_code 7249418 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.933 _shelx_estimated_absorpt_t_min 0.866 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Secondary CH2 refined with riding coordinates: C14(H14A,H14B), C20(H20A,H20B), C21(H21A,H21B), C22(H22A,H22B), C23(H23A,H23B) 2.b Aromatic/amide H refined with riding coordinates: C5(H5), C6(H6), C7(H7), C8(H8), C10(H10), C11(H11) 2.c Idealised Me refined as rotating group: C17(H17A,H17B,H17C), C24(H24A,H24B,H24C) ; _shelx_res_file ; TITL 240370lt_auto_a.res in P-1 240370lt_auto.res created by SHELXL-2018/3 at 16:01:04 on 25-Mar-2024 REM Old TITL 240370lt_auto in P-1 REM SHELXT solution in P-1: R1 0.776, Rweak 0.280, Alpha 0.037 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C20 O18 CELL 1.54184 7.4776 9.1826 12.9115 83.847 78.595 81.772 ZERR 2 0.0002 0.0002 0.0003 0.002 0.002 0.002 LATT 1 SFAC C H O UNIT 40 44 8 L.S. 4 PLAN 5 SIZE 0.21 0.13 0.1 TEMP -173.17(10) CONF fmap 2 MORE -1 BOND $H ACTA SHEL 99 0.837 OMIT -3 0 9 OMIT -3 6 0 OMIT -2 5 1 OMIT -2 5 2 OMIT 0 2 8 OMIT 0 5 9 OMIT 1 2 10 OMIT 1 4 11 OMIT 1 6 1 OMIT 1 7 0 OMIT 2 -2 7 OMIT 2 0 8 OMIT 2 7 0 OMIT 2 7 1 OMIT 3 -3 9 OMIT 3 -2 10 REM REM REM WGHT 0.043800 0.361400 FVAR 1.01280 O1 3 0.448666 0.478565 0.626252 11.00000 0.01480 0.02259 = 0.01533 -0.00448 -0.00422 -0.00169 O16 3 0.153568 0.111196 0.718912 11.00000 0.03326 0.01867 = 0.02679 0.00341 -0.01338 -0.00844 O18 3 0.344627 0.234257 0.778912 11.00000 0.04508 0.02474 = 0.03160 0.00299 -0.02458 -0.00880 O19 3 0.676023 0.521559 0.704363 11.00000 0.01473 0.03346 = 0.02170 -0.00872 -0.00417 -0.00174 C2 1 0.512633 0.526778 0.706693 11.00000 0.01736 0.01820 = 0.01510 -0.00186 -0.00493 -0.00240 C3 1 0.353667 0.580193 0.786590 11.00000 0.01639 0.01492 = 0.01537 0.00038 -0.00345 -0.00274 C4 1 0.347277 0.639469 0.884693 11.00000 0.01881 0.01493 = 0.01507 0.00031 -0.00364 -0.00233 C5 1 0.502477 0.668397 0.922403 11.00000 0.01679 0.03224 = 0.02156 -0.00738 -0.00465 -0.00196 AFIX 43 H5 2 0.621898 0.647462 0.881179 11.00000 -1.20000 AFIX 0 C6 1 0.481834 0.726535 1.018184 11.00000 0.02418 0.03709 = 0.02419 -0.00927 -0.00942 -0.00400 AFIX 43 H6 2 0.587232 0.746697 1.042216 11.00000 -1.20000 AFIX 0 C7 1 0.306597 0.756737 1.081366 11.00000 0.03098 0.02882 = 0.01753 -0.00745 -0.00454 -0.00451 AFIX 43 H7 2 0.294282 0.795647 1.148045 11.00000 -1.20000 AFIX 0 C8 1 0.154558 0.730002 1.046617 11.00000 0.02361 0.02584 = 0.01776 -0.00384 0.00116 -0.00348 AFIX 43 H8 2 0.036676 0.750498 1.089662 11.00000 -1.20000 AFIX 0 C9 1 0.169357 0.672182 0.947422 11.00000 0.01978 0.01718 = 0.01679 0.00050 -0.00204 -0.00398 C10 1 0.011008 0.647026 0.909670 11.00000 0.01590 0.02613 = 0.02066 -0.00222 0.00131 -0.00458 AFIX 43 H10 2 -0.106601 0.668161 0.952866 11.00000 -1.20000 AFIX 0 C11 1 0.021927 0.593403 0.813240 11.00000 0.01505 0.02362 = 0.01991 -0.00090 -0.00418 -0.00528 AFIX 43 H11 2 -0.085487 0.579562 0.788516 11.00000 -1.20000 AFIX 0 C12 1 0.197963 0.559706 0.752391 11.00000 0.01793 0.01385 = 0.01542 0.00159 -0.00427 -0.00373 C13 1 0.248185 0.499487 0.645243 11.00000 0.01371 0.01984 = 0.01635 -0.00113 -0.00493 -0.00267 C14 1 0.181015 0.350829 0.641190 11.00000 0.02199 0.02011 = 0.01757 -0.00182 -0.00780 -0.00417 AFIX 23 H14A 2 0.045039 0.365913 0.652083 11.00000 -1.20000 H14B 2 0.227084 0.317201 0.569301 11.00000 -1.20000 AFIX 0 C15 1 0.238398 0.229639 0.721089 11.00000 0.02263 0.01918 = 0.01707 -0.00367 -0.00472 -0.00305 C17 1 0.201240 -0.014564 0.790675 11.00000 0.04302 0.01933 = 0.02809 0.00461 -0.01254 -0.00683 AFIX 137 H17A 2 0.332207 -0.050539 0.770734 11.00000 -1.50000 H17B 2 0.127924 -0.093330 0.786456 11.00000 -1.50000 H17C 2 0.175808 0.015184 0.863334 11.00000 -1.50000 AFIX 0 C20 1 0.184561 0.608252 0.556547 11.00000 0.01650 0.02187 = 0.01671 -0.00060 -0.00529 -0.00265 AFIX 23 H20A 2 0.214801 0.558778 0.489692 11.00000 -1.20000 H20B 2 0.049121 0.631456 0.573971 11.00000 -1.20000 AFIX 0 C21 1 0.268553 0.752452 0.537887 11.00000 0.02130 0.02209 = 0.01944 0.00043 -0.00547 -0.00343 AFIX 23 H21A 2 0.404054 0.730328 0.528309 11.00000 -1.20000 H21B 2 0.225529 0.809100 0.601129 11.00000 -1.20000 AFIX 0 C22 1 0.217660 0.846447 0.440863 11.00000 0.02260 0.02113 = 0.01883 -0.00027 -0.00579 -0.00257 AFIX 23 H22A 2 0.082208 0.869620 0.451036 11.00000 -1.20000 H22B 2 0.258781 0.788946 0.377939 11.00000 -1.20000 AFIX 0 C23 1 0.303557 0.990491 0.420168 11.00000 0.02492 0.02202 = 0.02453 0.00009 -0.00622 -0.00372 AFIX 23 H23A 2 0.263547 1.047394 0.483444 11.00000 -1.20000 H23B 2 0.439052 0.967210 0.409271 11.00000 -1.20000 AFIX 0 C24 1 0.251415 1.085624 0.323933 11.00000 0.03738 0.02508 = 0.03284 0.00665 -0.01119 -0.00738 AFIX 137 H24A 2 0.295740 1.031716 0.260398 11.00000 -1.50000 H24B 2 0.307586 1.177313 0.315362 11.00000 -1.50000 H24C 2 0.117373 1.109046 0.334129 11.00000 -1.50000 AFIX 0 HKLF 4 REM 240370lt_auto_a.res in P-1 REM wR2 = 0.0943, GooF = S = 1.069, Restrained GooF = 1.069 for all data REM R1 = 0.0352 for 2797 Fo > 4sig(Fo) and 0.0426 for all 3011 data REM 219 parameters refined using 0 restraints END WGHT 0.0438 0.3616 REM Highest difference peak 0.275, deepest hole -0.240, 1-sigma level 0.059 Q1 1 0.2174 0.4284 0.6496 11.00000 0.05 0.27 Q2 1 0.2555 0.6452 0.9255 11.00000 0.05 0.22 Q3 1 0.4465 0.5782 0.7445 11.00000 0.05 0.21 Q4 1 0.3643 0.6186 0.8246 11.00000 0.05 0.20 Q5 1 0.2326 0.6825 0.5444 11.00000 0.05 0.20 ; _shelx_res_checksum 62564 _shelx_hkl_file ; 0 0 1 80.00 1.77 0 0 -1 79.19 1.82 0 0 -1 79.92 1.77 0 0 2 717.49 15.31 0 0 -2 705.00 15.21 0 0 -2 693.87 15.31 0 0 -3 950.51 20.55 0 0 3 950.79 20.56 0 0 -3 960.39 20.56 0 0 3 921.16 20.54 0 0 4 219.07 5.14 0 0 -4 220.63 5.15 0 0 -4 220.13 5.17 0 0 4 220.84 5.18 0 0 -5 86.57 2.35 0 0 -5 81.70 2.35 0 0 5 86.48 2.40 0 0 -6 904.57 20.00 0 0 -6 898.91 20.04 0 0 6 902.13 20.10 0 0 7 164.00 4.46 0 0 -7 167.15 4.36 0 0 -8 305.45 7.69 0 0 -8 329.46 8.01 0 0 8 312.14 7.86 0 0 -8 311.73 7.75 0 0 -9 22.63 1.23 0 0 -9 22.82 1.38 0 0 9 24.18 1.37 0 0 -9 24.54 1.30 0 0 -10 4.68 0.59 0 0 -10 3.81 0.58 0 0 -10 4.99 0.70 0 0 10 3.62 0.61 0 0 -11 193.04 5.56 0 0 -11 182.11 5.30 0 0 -11 179.23 5.17 0 0 -12 309.31 7.91 0 0 12 293.83 7.99 0 0 -13 0.98 0.37 0 0 13 0.23 0.35 0 0 -14 169.99 4.55 0 0 14 174.20 4.65 0 0 14 174.11 4.80 0 0 15 49.11 1.66 0 0 15 52.33 1.73 0 -1 15 0.84 0.22 0 -1 15 1.03 0.26 0 1 -14 14.10 0.82 0 -1 14 15.14 0.89 0 -1 14 14.95 0.96 0 1 -13 4.91 0.60 0 -1 13 6.06 0.66 0 -1 13 4.98 0.65 0 -1 12 14.44 1.01 0 -1 11 144.68 4.54 0 1 -11 140.57 4.26 0 1 -11 139.85 4.19 0 1 -10 1.34 0.41 0 -1 10 1.72 0.47 0 1 -10 1.41 0.44 0 1 -10 2.03 0.43 0 1 -9 8.11 0.74 0 -1 9 7.06 0.75 0 1 -9 8.02 0.80 0 1 -9 7.56 0.70 0 -1 8 496.66 11.76 0 1 -8 491.54 11.47 0 1 -8 483.10 11.54 0 1 -7 480.94 11.11 0 -1 6 252.97 6.12 0 1 -6 244.63 5.77 0 1 -6 249.29 5.98 0 1 -5 1.33 0.20 0 -1 5 1.05 0.26 0 1 -5 1.53 0.26 0 -1 4 40.18 1.04 0 1 -4 44.07 1.19 0 1 -4 46.40 1.21 0 -1 4 47.76 1.39 0 1 -4 42.56 1.32 0 1 -4 42.02 1.03 0 1 -4 46.59 1.33 0 -1 3 9.46 0.47 0 1 -3 10.20 0.46 0 1 -3 9.86 0.40 0 1 -3 10.41 0.40 0 -1 2 773.67 16.79 0 1 -2 771.81 16.75 0 1 -1 416.08 9.04 0 -1 -1 37.14 0.98 0 1 1 37.51 0.99 0 1 1 38.50 0.96 0 -1 -1 37.64 0.99 0 -1 -2 129.66 3.06 0 -1 -2 128.09 3.03 0 1 2 127.74 3.02 0 1 3 1346.72 29.67 0 1 3 1365.43 29.66 0 -1 -3 1389.06 29.68 0 -1 -3 1374.94 29.70 0 1 4 728.73 15.84 0 -1 -4 725.64 15.55 0 1 4 735.50 15.84 0 1 4 691.73 15.49 0 -1 -4 719.29 15.84 0 -1 -4 731.95 15.90 0 -1 -5 159.26 3.68 0 -1 -5 159.54 4.03 0 -1 -5 156.83 4.09 0 -1 -5 160.84 4.02 0 1 5 153.46 3.99 0 1 5 159.61 4.01 0 -1 -6 151.97 4.04 0 -1 -6 153.85 4.01 0 -1 -6 154.49 4.14 0 1 6 151.90 4.01 0 1 6 152.43 4.04 0 -1 -7 229.27 5.71 0 1 7 224.97 5.68 0 -1 -7 217.34 5.84 0 -1 -8 59.94 2.14 0 -1 -8 60.51 2.30 0 1 8 58.38 2.21 0 -1 -8 58.81 2.16 0 -1 -9 175.90 4.91 0 -1 -9 174.10 4.94 0 -1 -9 178.64 5.14 0 1 9 172.22 5.03 0 -1 -10 0.40 0.37 0 -1 -10 1.20 0.36 0 -1 -10 1.05 0.38 0 -1 -11 123.13 3.84 0 -1 -11 122.11 4.10 0 1 11 113.82 3.89 0 -1 -11 117.87 3.86 0 -1 -12 272.45 7.27 0 -1 -12 266.66 7.08 0 1 12 269.02 7.29 0 1 13 92.12 3.20 0 -1 -13 95.79 3.19 0 1 14 -0.04 0.30 0 1 14 0.58 0.31 0 -1 -14 -0.04 0.20 0 1 15 364.06 8.23 0 1 15 368.28 8.29 0 -2 14 10.13 0.73 0 -2 14 8.80 0.66 0 2 -14 9.37 0.67 0 -2 14 9.77 0.68 0 2 -13 17.63 1.10 0 -2 13 15.12 0.97 0 -2 13 18.39 1.15 0 -2 12 83.41 3.06 0 -2 12 83.88 2.85 0 -2 11 3.03 0.61 0 -2 11 3.27 0.53 0 -2 10 158.72 4.88 0 -2 10 159.26 4.59 0 2 -10 164.09 4.61 0 -2 9 151.54 4.56 0 2 -9 146.46 4.23 0 -2 9 153.80 4.26 0 2 -9 147.33 4.23 0 2 -8 8.78 0.71 0 -2 8 10.26 0.84 0 2 -7 169.00 4.36 0 2 -7 165.29 4.36 0 -2 7 161.09 4.55 0 2 -6 1028.78 22.26 0 -2 6 1007.65 22.42 0 2 -6 1016.62 22.25 0 2 -6 981.22 22.01 0 2 -5 939.43 20.92 0 2 -5 944.39 20.96 0 -2 5 981.00 21.23 0 2 -5 967.94 21.08 0 2 -5 961.65 20.92 0 2 -5 961.60 21.08 0 -2 4 36.19 1.26 0 2 -4 36.52 1.12 0 2 -4 36.15 1.18 0 2 -4 36.78 1.20 0 2 -3 6.43 0.40 0 -2 3 5.49 0.39 0 2 -3 6.03 0.37 0 2 -3 5.66 0.33 0 -2 3 7.04 0.38 0 2 -2 8336.92 179.55 0 2 -2 8439.36 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788.96 17.63 0 5 3 139.68 3.90 0 5 3 131.34 3.83 0 5 3 128.73 3.75 0 -5 -4 487.78 11.66 0 5 4 485.98 11.18 0 5 4 483.67 11.54 0 -5 -5 747.26 17.61 0 5 5 764.65 17.11 0 -5 -6 21.22 1.32 0 5 6 21.32 1.09 0 5 6 20.96 1.25 0 -5 -7 187.55 5.45 0 5 7 178.42 5.30 0 5 7 187.31 5.00 0 5 8 10.66 0.96 0 5 8 11.80 0.83 0 5 9 -0.07 0.00 0 -5 -9 -0.07 0.00 0 -5 -10 2.50 0.59 0 5 10 -0.07 0.00 0 5 10 2.24 0.47 0 -5 -10 -0.07 0.15 0 -5 -11 11.23 1.03 0 -5 -11 11.70 1.04 0 5 12 20.15 1.13 0 -5 -12 19.74 1.25 0 5 13 0.07 0.22 0 -5 -13 0.04 0.25 0 -5 -13 0.21 0.25 0 5 14 3.71 0.38 0 6 -12 34.72 1.25 0 6 -12 32.36 1.29 0 6 -11 25.93 1.31 0 6 -11 27.23 1.27 0 6 -11 27.99 1.26 0 -6 10 -0.04 0.26 0 6 -10 0.11 0.30 0 6 -10 0.87 0.33 0 -6 9 5.62 0.65 0 -6 8 0.32 0.28 0 -6 7 1.43 0.38 0 -6 7 0.70 0.38 0 -6 6 8.79 0.81 0 -6 6 9.61 0.90 0 -6 5 1.77 0.41 0 -6 5 1.05 0.41 0 -6 4 916.70 20.89 0 6 -4 929.62 21.58 0 -6 4 908.88 21.02 0 -6 3 828.75 19.07 0 -6 3 842.14 19.18 0 -6 2 260.21 6.68 0 6 -1 59.72 2.12 0 -6 1 62.00 2.25 0 -6 0 0.45 0.29 0 6 0 0.34 0.24 0 6 0 0.73 0.27 0 -6 -1 20.92 1.18 0 6 1 18.62 1.11 0 6 1 20.90 1.15 0 6 2 39.03 1.72 0 6 2 36.79 1.45 0 6 3 29.37 1.53 0 -6 -3 29.79 1.58 0 6 3 32.15 1.33 0 6 4 440.30 10.90 0 -6 -4 437.74 11.09 0 6 4 459.43 10.54 0 6 5 32.53 1.65 0 -6 -5 31.85 1.74 0 6 5 31.20 1.39 0 6 6 23.09 1.40 0 -6 -6 22.62 1.47 0 6 6 21.02 1.15 0 6 7 8.86 0.90 0 -6 -7 6.22 0.79 0 6 7 7.94 0.72 0 6 8 18.15 1.03 0 6 8 17.22 1.21 0 -6 -9 -0.07 0.00 0 6 9 63.49 1.91 0 6 9 61.75 2.22 0 -6 -9 22.18 1.54 0 -6 -10 2.34 0.58 0 -6 -10 3.08 0.56 0 -6 -11 0.25 0.33 0 -6 -11 0.12 0.35 0 6 11 0.17 0.26 0 -6 -12 79.68 2.75 0 -6 -12 84.76 2.81 0 6 12 80.57 2.52 0 -6 -13 6.03 0.53 0 6 13 5.93 0.47 0 -6 -13 5.67 0.54 0 7 -11 11.41 0.66 0 7 -11 11.46 0.69 0 7 -10 24.21 1.22 0 7 -10 24.84 1.22 0 7 -9 14.34 1.03 0 7 -8 3.37 0.59 0 -7 7 4.23 0.64 0 -7 6 9.24 0.92 0 7 -6 8.01 0.80 0 -7 5 911.81 21.14 0 -7 5 934.11 21.30 0 7 -5 911.50 21.21 0 -7 4 1631.22 36.38 0 -7 4 1620.11 36.24 0 -7 3 750.79 17.88 0 -7 3 790.55 18.02 0 7 -3 768.86 18.75 0 -7 2 325.04 8.34 0 -7 1 219.52 6.04 0 -7 0 89.95 3.13 0 7 1 138.55 4.23 0 7 1 137.94 4.20 0 7 2 69.91 2.66 0 7 3 0.46 0.24 0 7 3 0.17 0.29 0 -7 -3 0.42 0.33 0 -7 -4 85.41 3.31 0 7 4 94.41 3.21 0 7 4 87.70 2.83 0 -7 -5 12.20 1.12 0 7 5 14.67 1.12 0 7 5 14.49 0.94 0 -7 -6 1.71 0.51 0 7 6 2.03 0.46 0 7 6 1.93 0.39 0 -7 -7 97.89 3.65 0 7 7 95.07 3.10 0 7 7 101.26 3.50 0 7 8 263.30 7.20 0 7 9 120.64 2.95 0 7 9 115.44 2.43 0 7 10 6.12 0.59 0 -7 -10 5.46 0.72 0 -7 -10 6.02 0.75 0 7 11 141.10 3.84 0 -7 -11 140.88 4.19 0 -7 -11 146.15 4.23 0 -7 -12 73.43 2.35 0 -7 -12 71.73 2.35 0 8 -9 49.68 1.75 0 8 -9 52.24 1.86 0 8 -8 45.03 1.84 0 8 -8 41.26 1.67 0 8 -7 2.56 0.46 0 8 -7 2.58 0.54 0 -8 6 73.11 2.69 0 8 -6 75.16 2.80 0 8 -6 73.16 2.64 0 -8 5 60.26 2.44 0 8 -4 328.33 8.56 0 8 -3 119.23 4.42 0 -8 3 118.13 3.91 0 8 -2 9.20 1.13 0 -8 2 11.27 0.96 0 8 -1 2.28 0.72 0 -8 1 2.17 0.49 0 8 0 484.61 12.88 0 8 1 138.57 5.08 0 -8 -2 31.45 1.84 0 8 2 36.21 2.26 0 -8 -3 256.67 7.26 0 8 3 253.24 7.75 0 -8 -4 145.59 4.76 0 8 4 139.82 5.07 0 8 5 17.44 1.07 0 8 5 18.54 1.51 0 8 5 18.88 1.25 0 8 6 184.03 5.35 0 -8 -6 185.49 5.68 0 8 7 81.70 2.92 0 -8 -7 78.34 3.09 0 8 7 77.65 2.59 0 8 8 28.11 1.48 0 8 8 26.38 1.26 0 -8 -8 28.60 1.63 0 8 9 6.99 0.68 0 -8 -9 5.38 0.67 0 -8 -9 5.59 0.72 0 8 9 6.17 0.56 0 -8 -10 82.33 2.75 0 -8 -10 78.00 2.71 0 -8 -11 49.63 1.78 0 -8 -11 48.07 1.77 0 9 -8 11.51 0.68 0 9 -7 17.51 0.97 0 9 -6 523.47 12.22 0 9 -6 534.19 12.41 0 9 -5 15.33 1.01 0 -9 5 15.07 0.97 0 9 -5 15.47 1.02 0 9 -4 81.23 2.86 0 -9 4 81.11 2.82 0 9 -4 83.72 2.83 0 9 -4 82.81 2.73 0 -9 3 7.48 0.75 0 9 -3 7.15 0.78 0 9 -3 7.26 0.88 0 9 -3 6.95 0.72 0 9 -2 30.42 1.97 0 -9 2 35.25 1.71 0 9 -1 2.78 0.69 0 -9 1 4.44 0.64 0 -9 0 79.97 3.15 0 9 0 89.40 3.73 0 -9 0 90.05 3.12 0 -9 -1 126.72 4.27 0 9 1 136.56 4.88 0 -9 -2 222.01 6.38 0 9 2 221.60 6.97 0 9 3 2.78 0.66 0 -9 -3 1.85 0.50 0 9 4 1.98 0.60 0 -9 -4 2.32 0.57 0 9 5 29.53 1.81 0 -9 -5 30.75 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257.80 7.14 -1 -1 -11 241.03 6.71 1 1 12 427.76 11.10 -1 -1 -12 462.47 11.48 -1 -1 -12 434.82 10.93 -1 -1 -12 459.80 11.07 1 1 13 2.07 0.48 -1 -1 -14 26.74 1.33 1 1 14 26.49 1.32 1 1 14 30.31 1.48 1 1 15 5.97 0.53 1 1 15 5.80 0.55 1 2 -14 2.78 0.34 -1 -2 14 0.03 0.12 1 2 -13 0.04 0.27 -1 -2 13 0.08 0.18 -1 -2 13 0.52 0.25 1 2 -13 0.23 0.24 1 2 -12 2.51 0.49 -1 -2 12 0.60 0.26 1 2 -11 152.14 4.58 -1 -2 11 150.65 4.37 1 2 -11 153.47 4.55 1 2 -11 152.46 4.53 1 2 -10 26.10 1.41 -1 -2 10 22.54 1.26 1 2 -10 25.29 1.41 1 2 -9 30.56 1.53 1 2 -8 37.15 1.59 -1 -2 8 35.71 1.63 1 2 -8 36.06 1.62 1 2 -7 19.53 0.96 1 2 -7 18.35 1.04 1 2 -6 198.89 4.91 1 2 -6 195.68 5.08 1 2 -6 199.05 5.00 1 2 -6 197.45 4.84 -1 -2 6 200.77 5.05 1 2 -6 194.48 4.92 1 2 -5 428.21 10.04 1 2 -5 440.65 10.19 1 2 -5 446.61 9.96 1 2 -5 442.17 10.11 -1 -2 5 441.34 10.13 1 2 -5 449.04 10.10 1 2 -4 6.28 0.39 1 2 -4 6.43 0.42 1 2 -4 7.03 0.41 1 2 -4 6.63 0.45 1 2 -4 6.55 0.49 1 2 -4 6.66 0.48 -1 -2 4 7.53 0.47 1 2 -3 1036.00 23.08 1 2 -3 1068.14 22.91 1 2 -3 1065.05 23.02 1 2 -3 1050.06 22.82 1 2 -3 1068.00 22.99 1 2 -3 1059.53 23.00 -1 -2 3 1066.69 22.92 1 2 -3 1000.70 22.99 1 2 -3 1052.42 22.94 1 2 -3 1049.90 22.90 1 2 -2 2.22 0.27 1 2 -2 2.94 0.33 1 2 -2 2.02 0.23 1 2 -2 2.02 0.31 1 2 -2 2.12 0.34 1 2 -2 3.28 0.16 -1 -2 2 1.99 0.18 1 2 -2 1.71 0.22 1 2 -2 1.60 0.24 1 2 -2 1.69 0.24 -1 -2 2 2.07 0.21 1 2 -2 1.66 0.24 1 2 -1 56.90 1.42 1 2 -1 55.93 1.65 1 2 -1 56.58 1.67 1 2 -1 57.24 1.49 1 2 -1 52.99 1.51 1 2 -1 53.53 1.28 1 2 -1 57.43 1.66 1 2 -1 54.35 1.53 1 2 -1 55.96 1.69 1 2 0 1703.27 36.71 1 2 0 1698.60 36.90 1 2 0 1697.40 36.97 1 2 0 1770.46 36.87 1 2 0 1665.73 36.75 1 2 0 1717.68 36.64 -1 -2 0 1704.04 36.64 1 2 0 1670.78 36.97 1 2 0 1696.36 36.82 1 2 0 1741.01 37.02 1 2 1 92.23 2.43 -1 -2 -1 93.27 2.24 1 2 1 95.20 2.16 1 2 1 91.06 2.37 1 2 1 103.68 2.49 1 2 1 93.96 2.46 1 2 1 92.40 2.25 1 2 1 93.61 2.21 1 2 1 94.77 2.52 1 2 2 1958.07 41.36 1 2 2 1915.27 41.22 -1 -2 -2 1927.44 41.28 1 2 2 1937.56 41.45 1 2 2 1901.24 41.33 1 2 2 1906.18 41.03 -1 -2 -2 1884.89 41.26 1 2 2 1905.25 41.14 -1 -2 -3 128.04 3.22 1 2 3 131.69 3.17 1 2 3 131.06 3.18 1 2 3 125.07 3.26 1 2 3 129.26 3.09 -1 -2 -3 126.79 3.23 -1 -2 -4 57.12 1.76 1 2 4 57.95 1.70 1 2 4 55.93 1.60 1 2 4 53.69 1.65 -1 -2 -4 56.35 1.72 -1 -2 -5 544.95 12.42 -1 -2 -5 548.80 12.36 1 2 5 555.18 12.31 1 2 5 523.20 12.09 1 2 5 560.55 12.36 -1 -2 -5 540.39 12.37 -1 -2 -6 1325.63 29.02 1 2 6 1319.27 28.93 -1 -2 -6 1277.77 29.09 1 2 6 1325.89 29.01 -1 -2 -6 1320.77 29.02 -1 -2 -7 80.19 2.63 1 2 7 85.75 2.62 -1 -2 -7 80.43 2.63 -1 -2 -8 -0.06 0.00 -1 -2 -8 0.19 0.28 -1 -2 -9 388.62 4.99 -1 -2 -9 395.83 5.00 -1 -2 -10 -0.06 0.00 1 2 10 0.29 0.41 -1 -2 -11 17.12 1.17 1 2 11 16.04 1.13 -1 -2 -11 17.18 1.31 -1 -2 -12 487.00 11.90 1 2 12 468.51 11.86 -1 -2 -12 494.11 12.28 1 2 13 32.92 1.68 -1 -2 -13 33.11 1.65 1 2 14 27.08 1.37 1 2 14 27.78 1.32 -1 -2 -14 27.70 1.36 1 2 15 8.46 0.62 1 2 15 8.80 0.64 1 3 -14 1.60 0.26 -1 -3 13 -0.03 0.17 1 3 -13 70.70 1.77 1 3 -12 39.37 1.45 1 3 -12 39.14 1.54 1 3 -11 89.99 3.16 1 3 -11 90.25 3.01 1 3 -10 34.58 1.69 -1 -3 10 35.46 1.59 1 3 -9 106.62 3.48 -1 -3 9 105.29 3.31 1 3 -9 115.87 3.58 1 3 -8 59.39 2.27 -1 -3 8 60.73 2.14 1 3 -8 63.88 2.37 -1 -3 7 248.75 6.44 1 3 -7 250.66 6.43 1 3 -7 253.02 6.44 1 3 -6 10.68 0.73 1 3 -6 12.11 0.79 1 3 -6 11.01 0.77 1 3 -6 10.52 0.72 1 3 -6 10.22 0.72 -1 -3 6 10.70 0.66 -1 -3 5 257.92 6.16 1 3 -5 261.17 6.24 -1 -3 5 261.68 6.35 1 3 -5 272.10 6.39 1 3 -5 252.42 6.13 1 3 -5 257.84 6.32 1 3 -5 260.05 6.35 -1 -3 4 24.39 1.03 1 3 -4 26.49 1.08 1 3 -4 23.64 1.00 1 3 -4 27.11 1.11 1 3 -4 25.26 1.04 1 3 -4 26.11 1.09 -1 -3 4 24.95 0.94 1 3 -3 67.08 2.02 -1 -3 3 70.04 1.92 1 3 -3 71.01 2.05 1 3 -3 77.78 1.85 -1 -3 3 71.18 2.04 1 3 -3 80.22 2.10 1 3 -3 73.72 2.26 1 3 -3 69.83 2.10 1 3 -2 1782.18 38.27 1 3 -2 1682.54 38.57 1 3 -2 1737.94 38.35 -1 -3 2 1713.86 38.15 1 3 -2 1759.02 38.61 -1 -3 2 1768.08 38.11 1 3 -2 1763.11 38.03 1 3 -1 463.30 10.55 -1 -3 1 475.05 10.59 -1 -3 1 492.02 10.65 1 3 -1 475.41 11.00 1 3 -1 487.78 10.75 1 3 -1 479.54 10.59 1 3 0 326.31 7.28 1 3 0 320.01 7.57 1 3 0 324.76 7.17 1 3 0 319.97 7.17 1 3 0 320.45 7.16 -1 -3 0 314.97 7.19 1 3 1 63.63 1.58 1 3 1 67.76 1.88 1 3 1 65.34 1.62 1 3 1 61.63 1.63 1 3 1 60.79 1.91 1 3 1 66.39 1.70 1 3 1 64.12 1.74 -1 -3 -1 63.27 1.71 1 3 1 66.13 1.75 1 3 2 483.37 10.79 1 3 2 493.56 10.70 1 3 2 480.01 11.09 1 3 2 499.29 10.82 1 3 2 491.90 11.03 1 3 2 500.21 10.96 -1 -3 -3 406.93 9.40 1 3 3 386.94 9.55 1 3 3 410.25 9.17 -1 -3 -3 421.15 9.37 1 3 3 422.28 9.33 1 3 3 408.96 9.32 -1 -3 -4 457.29 10.44 1 3 4 442.43 10.47 1 3 4 468.81 10.21 -1 -3 -4 445.86 10.40 1 3 4 464.81 10.36 1 3 4 438.46 10.19 1 3 5 1340.92 28.96 -1 -3 -5 1329.51 29.19 1 3 5 1336.53 29.10 1 3 5 1277.24 29.07 -1 -3 -5 1333.12 29.19 -1 -3 -6 639.16 14.66 1 3 6 646.92 14.40 1 3 6 618.71 14.53 -1 -3 -7 0.51 0.31 -1 -3 -7 0.47 0.35 -1 -3 -7 0.64 0.34 1 3 7 0.68 0.31 1 3 8 5.11 0.62 -1 -3 -8 5.72 0.67 -1 -3 -8 4.63 0.64 1 3 8 5.60 0.60 -1 -3 -8 5.85 0.67 -1 -3 -9 0.93 0.43 1 3 9 0.56 0.31 -1 -3 -9 0.54 0.35 -1 -3 -9 1.63 0.45 1 3 10 169.36 3.33 -1 -3 -10 163.41 3.78 -1 -3 -10 167.84 3.55 1 3 11 78.44 2.36 -1 -3 -11 76.38 2.45 1 3 12 132.64 4.13 -1 -3 -12 132.32 4.25 1 3 13 104.52 3.36 1 3 14 140.13 3.86 -1 -3 -14 136.94 3.89 1 3 15 16.62 0.82 1 3 15 15.16 0.80 1 4 -13 43.18 1.58 1 4 -12 9.59 0.75 1 4 -12 9.37 0.78 1 4 -11 82.34 2.87 1 4 -11 78.94 2.85 1 4 -10 21.31 1.34 1 4 -10 19.32 1.26 1 4 -9 248.37 6.91 1 4 -9 264.30 6.81 1 4 -8 271.34 7.21 1 4 -8 264.05 6.96 1 4 -7 11.62 0.87 1 4 -7 12.37 0.93 -1 -4 6 149.61 4.21 1 4 -6 147.47 4.19 1 4 -6 149.03 4.18 1 4 -5 39.09 1.52 1 4 -5 40.39 1.59 -1 -4 4 374.97 8.52 1 4 -4 373.83 8.64 -1 -4 4 367.26 8.72 -1 -4 4 357.03 8.56 1 4 -4 373.18 8.75 1 4 -4 363.84 8.80 1 4 -4 372.45 8.98 1 4 -3 3.24 0.43 1 4 -3 2.75 0.42 -1 -4 3 3.63 0.41 1 4 -3 3.15 0.47 -1 -4 3 3.52 0.36 -1 -4 2 261.09 6.04 1 4 -2 272.41 6.63 1 4 -2 256.54 6.12 1 4 -1 697.79 15.58 1 4 -1 709.57 15.65 -1 -4 1 741.18 15.71 1 4 -1 710.47 16.08 1 4 -1 696.14 15.57 1 4 0 2689.70 57.99 1 4 0 2703.96 57.87 -1 -4 0 2712.34 58.03 1 4 0 2658.67 58.31 1 4 0 2670.19 57.98 -1 -4 -1 1113.64 25.20 1 4 1 1156.15 25.22 1 4 1 1173.06 25.24 1 4 1 1167.06 25.05 1 4 2 19.07 0.83 1 4 2 20.50 0.89 1 4 2 18.46 0.72 1 4 3 439.43 9.79 1 4 3 434.35 9.98 -1 -4 -3 437.99 10.14 1 4 3 437.58 10.04 1 4 3 426.33 9.95 1 4 4 811.91 18.95 1 4 4 835.39 18.41 -1 -4 -4 834.57 18.79 1 4 4 833.01 18.54 1 4 4 849.41 18.66 -1 -4 -5 368.68 8.97 1 4 5 372.79 8.62 1 4 5 361.53 9.00 1 4 5 378.57 8.88 -1 -4 -6 231.33 6.19 1 4 6 239.84 6.08 1 4 7 25.38 1.19 -1 -4 -7 23.26 1.33 -1 -4 -8 480.91 11.80 1 4 8 479.21 11.42 1 4 8 489.67 11.68 -1 -4 -8 475.88 11.79 -1 -4 -9 68.52 2.76 1 4 9 72.16 2.55 1 4 9 73.12 2.73 -1 -4 -9 71.75 2.81 1 4 10 19.72 1.15 -1 -4 -10 9.95 0.93 -1 -4 -11 -0.07 0.00 -1 -4 -11 -0.07 0.00 -1 -4 -12 11.77 1.02 1 4 12 13.04 0.98 -1 -4 -12 13.88 1.10 -1 -4 -13 18.17 1.19 1 4 13 17.15 1.05 -1 -4 -13 19.90 1.23 1 4 14 11.87 0.76 -1 -4 -14 13.34 0.86 1 4 15 4.36 0.38 1 5 -13 51.31 1.59 1 5 -12 73.79 2.36 1 5 -12 74.78 2.37 1 5 -11 12.71 0.92 1 5 -11 11.75 0.85 1 5 -11 12.39 0.93 1 5 -10 46.88 2.03 1 5 -10 44.52 2.04 1 5 -9 36.11 1.79 1 5 -9 37.25 1.86 1 5 -8 25.63 1.48 1 5 -8 29.47 1.66 1 5 -7 478.55 11.54 1 5 -6 203.06 5.59 1 5 -6 205.40 5.56 1 5 -5 3.91 0.52 -1 -5 5 3.56 0.51 1 5 -5 2.87 0.49 1 5 -4 12.94 0.91 -1 -5 4 14.32 0.90 1 5 -4 14.33 1.05 1 5 -3 307.70 7.84 1 5 -3 290.81 7.14 1 5 -2 32.49 1.65 -1 -5 2 30.59 1.24 1 5 -2 30.67 1.19 -1 -5 1 22.41 1.01 1 5 -1 25.72 1.43 1 5 -1 23.86 1.23 -1 -5 0 121.96 3.29 1 5 0 121.04 3.51 1 5 1 2.14 0.27 1 5 1 2.49 0.37 1 5 1 1.80 0.31 1 5 1 2.46 0.34 1 5 2 254.78 6.33 1 5 2 268.38 6.17 1 5 3 264.09 6.56 -1 -5 -3 263.20 6.75 1 5 3 278.91 7.17 1 5 3 270.18 6.33 1 5 4 4.34 0.62 -1 -5 -4 3.97 0.53 1 5 4 4.95 0.53 1 5 4 4.86 0.43 1 5 5 399.14 9.48 -1 -5 -5 384.57 9.64 1 5 5 390.53 9.83 1 5 6 44.53 1.65 -1 -5 -6 47.88 2.05 1 5 7 3.05 0.51 -1 -5 -7 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617.93 14.62 2 3 -11 633.84 14.73 2 3 -10 42.23 1.91 2 3 -10 38.47 1.87 2 3 -10 44.11 1.97 2 3 -9 0.65 0.33 2 3 -9 0.50 0.71 2 3 -9 0.24 0.36 2 3 -9 0.50 0.34 2 3 -9 0.53 0.37 2 3 -8 36.82 1.74 2 3 -8 36.61 1.73 2 3 -8 34.82 1.71 2 3 -8 31.79 1.57 2 3 -8 34.02 1.67 2 3 -7 167.53 4.78 2 3 -7 166.06 4.76 2 3 -7 162.31 4.75 2 3 -7 171.66 4.60 2 3 -7 169.82 4.81 2 3 -6 475.55 7.15 2 3 -6 474.61 7.06 2 3 -6 479.06 6.76 2 3 -6 482.82 7.07 2 3 -6 472.02 6.98 2 3 -5 415.68 9.99 2 3 -5 429.33 9.87 2 3 -5 416.32 9.99 2 3 -4 23.20 1.08 2 3 -4 22.04 1.01 2 3 -4 21.55 1.05 2 3 -4 22.65 1.03 2 3 -4 21.33 1.07 2 3 -4 22.55 1.11 2 3 -4 21.19 1.07 2 3 -3 99.49 2.83 2 3 -3 99.03 2.80 2 3 -3 85.51 2.99 2 3 -3 101.83 2.80 2 3 -3 97.51 2.70 2 3 -3 97.48 2.74 2 3 -3 96.42 2.96 2 3 -3 94.50 2.74 2 3 -3 99.33 2.84 2 3 -3 97.24 2.80 2 3 -3 101.22 2.93 2 3 -2 1014.44 22.34 2 3 -2 1022.02 22.39 2 3 -2 987.19 22.32 2 3 -2 1009.62 22.61 2 3 -2 1005.14 22.67 2 3 -2 1034.92 22.32 2 3 -2 1011.30 22.22 2 3 -2 1003.71 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1.66 2 4 -12 41.49 1.58 2 4 -11 227.42 5.94 2 4 -11 217.18 5.88 2 4 -11 223.47 5.93 2 4 -10 173.85 5.11 2 4 -10 183.29 5.13 2 4 -9 122.36 3.91 2 4 -9 123.39 3.92 2 4 -9 119.70 3.93 2 4 -9 119.06 3.86 2 4 -8 12.21 1.01 2 4 -8 12.29 1.04 2 4 -8 10.83 0.93 2 4 -8 8.92 1.15 2 4 -8 11.74 0.98 2 4 -7 39.83 1.59 2 4 -7 40.87 1.63 2 4 -7 38.12 1.67 2 4 -6 396.44 4.76 2 4 -6 390.39 4.77 2 4 -6 405.06 4.48 2 4 -6 397.21 5.04 2 4 -6 396.87 4.83 2 4 -5 170.03 4.74 2 4 -5 173.76 4.78 2 4 -5 173.21 4.85 2 4 -5 163.26 4.61 2 4 -5 175.93 4.73 2 4 -5 176.65 4.81 2 4 -4 9.36 0.74 2 4 -3 183.24 4.88 2 4 -3 183.77 4.83 2 4 -3 187.49 4.76 2 4 -3 197.41 4.91 2 4 -3 175.67 4.71 2 4 -3 200.61 4.97 2 4 -3 178.89 5.02 2 4 -3 175.63 4.86 2 4 -2 19.94 1.03 2 4 -2 19.65 1.07 2 4 -2 20.48 1.03 2 4 -2 18.44 1.15 2 4 -2 25.84 1.13 2 4 -2 19.13 0.90 2 4 -2 27.34 1.26 2 4 -2 19.92 1.02 2 4 -2 17.83 0.94 2 4 -2 19.59 1.14 2 4 -1 192.55 4.77 2 4 -1 164.96 4.85 2 4 -1 174.46 4.35 2 4 -1 180.28 4.33 2 4 -1 173.51 4.82 2 4 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2.22 2 5 -3 185.87 3.15 2 5 -3 185.92 2.89 2 5 -3 179.90 3.51 2 5 -2 83.70 2.81 2 5 -2 81.53 2.99 2 5 -2 89.33 2.54 2 5 -2 81.17 2.73 2 5 -1 5.85 0.73 2 5 -1 6.15 0.69 2 5 -1 6.92 0.60 2 5 -1 5.81 0.46 2 5 0 17.56 0.93 2 5 0 15.46 0.81 2 5 0 18.28 1.12 2 5 0 16.86 1.19 2 5 1 7.19 0.84 -2 -5 -1 7.06 0.56 2 5 1 7.20 0.54 2 5 1 7.54 0.70 2 5 1 7.68 0.56 -2 -5 -2 1486.87 32.91 2 5 2 1506.95 33.34 2 5 2 1524.81 33.60 2 5 2 1483.18 33.12 2 5 3 1910.76 41.52 2 5 3 1846.83 41.83 2 5 3 1881.58 41.37 -2 -5 -4 298.53 7.48 2 5 4 302.90 7.86 2 5 4 300.59 7.49 2 5 5 101.11 3.47 2 5 5 109.36 3.13 2 5 5 99.99 3.20 -2 -5 -5 109.28 3.33 -2 -5 -6 535.96 12.79 2 5 7 39.52 1.69 -2 -5 -7 34.01 1.73 -2 -5 -7 35.72 1.77 -2 -5 -8 58.15 2.43 -2 -5 -8 58.95 2.46 -2 -5 -9 40.39 2.00 2 5 9 38.71 1.65 -2 -5 -9 40.22 2.00 -2 -5 -10 11.77 1.05 2 5 10 12.98 0.91 -2 -5 -10 10.92 1.03 -2 -5 -11 131.46 4.31 -2 -5 -11 137.22 4.38 -2 -5 -12 0.48 0.32 2 5 12 1.09 0.33 -2 -5 -13 1.36 0.40 -2 -5 -13 0.85 0.36 -2 -5 -14 16.31 0.93 -2 -5 -15 72.66 2.07 2 6 -11 0.25 0.21 2 6 -11 0.50 0.26 2 6 -11 0.60 0.25 2 6 -10 20.43 1.13 2 6 -10 19.83 1.13 2 6 -10 20.44 1.06 2 6 -9 25.16 1.41 2 6 -9 22.71 1.34 2 6 -9 25.16 1.30 2 6 -8 0.30 0.38 2 6 -7 125.34 4.10 2 6 -7 123.88 3.93 2 6 -7 122.78 3.99 2 6 -7 118.02 3.78 2 6 -6 131.29 4.24 2 6 -6 133.45 4.24 2 6 -6 131.75 4.20 2 6 -6 139.24 4.39 2 6 -6 137.94 4.09 2 6 -5 360.95 9.32 2 6 -5 383.57 9.49 2 6 -5 366.74 9.49 2 6 -5 373.06 9.37 2 6 -5 361.32 9.09 2 6 -4 302.46 4.34 2 6 -4 308.91 4.66 2 6 -4 314.57 4.00 2 6 -4 307.61 4.54 2 6 -3 -0.29 0.40 2 6 -3 0.63 0.32 2 6 -3 0.22 0.33 2 6 -3 0.28 0.36 2 6 -3 0.34 0.36 2 6 -2 80.32 2.77 2 6 -2 79.21 2.61 2 6 -2 77.62 2.79 2 6 -2 76.48 3.09 2 6 -1 4.20 0.71 2 6 -1 3.99 0.59 2 6 -1 4.16 0.56 2 6 -1 4.39 0.50 2 6 0 1.64 0.34 2 6 0 1.03 0.37 2 6 1 -0.08 0.00 -2 -6 -2 23.38 1.24 2 6 2 26.13 1.62 -2 -6 -3 91.75 3.04 2 6 3 101.33 3.59 -2 -6 -4 62.94 2.39 2 6 4 65.50 2.74 -2 -6 -5 30.55 1.60 2 6 5 32.92 1.84 -2 -6 -6 59.20 2.40 2 6 6 55.37 2.46 2 6 7 96.81 3.15 -2 -6 -7 94.06 3.37 -2 -6 -7 91.62 3.35 -2 -6 -8 46.01 2.17 -2 -6 -8 43.33 2.12 -2 -6 -9 34.65 1.86 -2 -6 -9 33.76 1.83 -2 -6 -10 203.33 5.94 -2 -6 -11 46.36 2.10 -2 -6 -12 29.82 1.53 -2 -6 -12 30.18 1.53 -2 -6 -13 3.64 0.50 -2 -6 -13 3.30 0.47 -2 -6 -14 34.61 1.30 2 7 -10 8.59 0.61 2 7 -10 9.88 0.65 2 7 -9 55.63 2.06 2 7 -9 55.22 2.02 2 7 -8 0.16 0.34 2 7 -8 0.58 0.29 2 7 -8 0.89 0.36 2 7 -7 151.85 4.60 2 7 -7 164.52 4.44 2 7 -7 158.48 4.67 2 7 -6 7.65 0.83 2 7 -6 8.22 0.86 2 7 -5 61.62 2.55 2 7 -5 59.86 2.55 2 7 -5 60.43 2.43 2 7 -5 61.97 2.52 2 7 -4 11.87 1.06 2 7 -4 12.93 1.07 2 7 -4 13.45 1.01 2 7 -4 12.96 1.06 2 7 -3 719.83 16.49 2 7 -3 689.16 16.36 2 7 -3 674.37 16.08 2 7 -3 690.88 16.39 2 7 -2 290.24 7.78 2 7 -2 288.42 8.23 2 7 -2 296.53 7.68 2 7 -1 59.32 2.51 2 7 -1 58.90 1.92 2 7 0 -0.06 0.00 2 7 0 8.82 1.09 2 7 1 -0.09 0.00 2 7 2 14.87 1.37 2 7 3 23.21 1.66 -2 -7 -4 3.54 0.59 2 7 4 2.81 0.71 2 7 5 270.73 7.88 -2 -7 -5 281.30 7.49 -2 -7 -6 458.63 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1 2 122.40 3.29 3 1 2 126.92 3.42 3 1 2 119.36 3.37 3 1 2 115.01 2.96 3 1 2 122.49 2.85 3 1 3 578.72 12.97 3 1 3 587.45 13.21 3 1 3 578.82 12.97 3 1 3 570.05 13.21 3 1 3 570.05 13.22 3 1 3 567.40 13.07 3 1 3 546.95 12.74 -3 -1 -3 588.20 12.79 3 1 3 571.51 13.07 3 1 3 599.04 12.64 3 1 3 568.85 12.64 3 1 4 13.89 0.72 3 1 4 13.87 0.84 3 1 4 12.70 0.80 3 1 4 13.75 0.76 3 1 4 12.26 0.74 -3 -1 -4 13.32 0.68 -3 -1 -4 14.32 0.67 3 1 4 13.20 0.67 3 1 4 13.76 0.59 3 1 5 521.49 11.99 -3 -1 -5 524.68 11.77 -3 -1 -5 526.23 11.81 3 1 5 513.49 11.82 3 1 5 505.58 11.85 3 1 5 517.33 11.59 3 1 5 523.21 11.82 3 1 5 509.45 11.96 3 1 6 0.10 0.22 -3 -1 -6 0.07 0.22 3 1 6 0.22 0.20 -3 -1 -7 5.31 0.55 -3 -1 -7 5.85 0.57 3 1 7 6.31 0.61 -3 -1 -8 3.37 0.49 3 1 8 3.83 0.52 -3 -1 -9 184.24 5.13 3 1 9 176.85 5.19 -3 -1 -10 16.09 1.14 3 1 10 16.79 1.23 3 1 10 16.13 1.02 -3 -1 -11 687.28 16.07 3 1 11 674.78 16.30 -3 -1 -11 676.97 16.55 3 1 11 669.75 15.73 -3 -1 -12 10.38 1.09 3 1 12 7.59 0.74 -3 -1 -12 8.57 0.84 3 1 13 2.34 0.46 -3 -1 -13 2.30 0.56 -3 -1 -14 3.25 0.57 3 1 14 2.73 0.44 -3 -1 -14 3.39 0.50 3 1 14 3.17 0.45 3 1 15 2.07 0.32 -3 -1 -15 2.25 0.36 3 1 15 2.42 0.34 3 2 -13 58.13 1.88 3 2 -12 0.71 0.34 3 2 -12 0.53 0.25 3 2 -11 497.88 11.72 3 2 -11 488.41 11.46 3 2 -11 470.90 11.33 3 2 -10 10.17 0.94 3 2 -10 11.29 0.97 3 2 -9 57.30 2.23 3 2 -9 55.12 2.21 3 2 -9 55.35 2.34 3 2 -9 50.96 2.13 3 2 -8 14.94 1.06 3 2 -8 13.97 1.00 3 2 -8 12.71 1.03 3 2 -8 13.29 0.98 3 2 -7 68.23 2.03 3 2 -7 71.07 2.00 3 2 -7 73.43 2.06 3 2 -7 69.57 2.11 3 2 -7 68.00 1.99 3 2 -6 1.39 0.36 3 2 -6 1.10 0.33 3 2 -6 1.75 0.41 3 2 -6 1.71 0.38 3 2 -6 2.22 0.44 3 2 -5 222.50 3.27 3 2 -5 231.19 3.67 3 2 -5 226.94 3.36 3 2 -5 227.41 3.22 3 2 -4 137.42 3.91 3 2 -4 134.75 3.76 3 2 -4 140.39 3.87 3 2 -4 141.77 4.01 3 2 -4 138.72 3.83 3 2 -4 146.44 4.03 3 2 -4 136.24 3.92 3 2 -4 135.58 3.85 3 2 -4 140.90 3.89 3 2 -4 138.87 4.03 3 2 -3 174.14 4.61 3 2 -3 173.81 4.90 3 2 -3 174.06 4.50 3 2 -3 185.71 4.59 3 2 -3 181.19 4.58 3 2 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234.90 6.19 -3 -3 -9 512.43 12.61 -3 -3 -9 503.62 12.33 -3 -3 -9 508.57 12.28 -3 -3 -10 202.01 6.11 -3 -3 -10 207.22 5.88 -3 -3 -10 209.61 5.86 3 3 11 65.63 2.46 -3 -3 -11 65.17 2.85 -3 -3 -11 69.56 2.68 -3 -3 -11 65.46 2.64 3 3 12 62.65 2.26 -3 -3 -12 64.31 2.57 3 3 13 103.35 3.11 -3 -3 -14 208.44 5.54 3 3 15 6.47 0.53 -3 -3 -15 8.03 0.59 3 4 -12 139.98 3.61 3 4 -11 8.17 0.66 3 4 -11 7.86 0.85 3 4 -11 9.29 0.70 3 4 -10 65.99 2.49 3 4 -10 57.52 2.24 3 4 -10 65.45 2.37 3 4 -10 62.90 2.32 3 4 -9 156.28 4.60 3 4 -9 153.45 4.48 3 4 -9 148.47 4.38 3 4 -9 140.74 4.44 3 4 -8 49.69 2.18 3 4 -8 46.77 2.05 3 4 -8 46.23 2.09 3 4 -8 44.23 2.20 3 4 -8 46.24 2.09 3 4 -7 27.73 1.55 3 4 -7 25.69 1.44 3 4 -7 24.87 1.48 3 4 -7 28.31 1.57 3 4 -7 25.64 1.65 3 4 -7 26.15 1.49 3 4 -6 513.02 5.91 3 4 -6 499.36 5.92 3 4 -6 510.66 5.95 3 4 -6 495.58 5.39 3 4 -6 506.31 6.13 3 4 -6 495.26 5.76 3 4 -5 -0.05 0.00 3 4 -5 2.55 0.53 3 4 -5 2.47 0.51 3 4 -5 -0.11 0.25 3 4 -5 2.32 0.51 3 4 -5 2.04 0.77 3 4 -5 2.24 0.47 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4 -6 9 4.30 0.55 4 -6 10 10.84 0.78 4 -6 10 11.38 0.76 -4 5 10 0.82 0.22 -4 5 9 97.15 3.02 -4 5 9 94.55 2.82 -4 5 8 4.11 0.51 -4 5 8 5.42 0.65 4 -5 -7 0.37 0.28 -4 5 7 0.73 0.31 -4 5 6 0.43 0.38 4 -5 -6 0.06 0.27 4 -5 -5 1.15 0.42 -4 5 5 0.67 0.39 -4 5 5 0.76 0.33 -4 5 4 74.92 2.61 -4 5 4 74.69 3.05 -4 5 4 74.20 3.03 -4 5 3 3.47 0.67 -4 5 3 3.22 0.63 -4 5 3 3.76 0.52 -4 5 2 53.70 2.44 -4 5 1 4.44 0.71 4 -5 0 0.55 0.37 -4 5 0 0.28 0.37 4 -5 1 140.79 4.49 -4 5 -1 134.08 4.46 -4 5 -1 142.45 4.57 4 -5 1 142.75 4.23 4 -5 2 208.38 5.76 4 -5 2 207.39 5.98 4 -5 3 55.65 2.29 4 -5 3 56.92 2.41 -4 5 -3 52.91 2.38 4 -5 4 108.90 2.79 -4 5 -4 105.71 2.95 4 -5 4 110.19 2.93 4 -5 5 26.42 1.45 -4 5 -5 28.43 1.56 4 -5 5 31.27 1.58 4 -5 6 13.82 1.08 -4 5 -6 14.25 1.12 4 -5 6 13.32 1.04 -4 5 -7 121.46 3.98 -4 5 -7 111.70 3.87 4 -5 8 15.27 1.13 -4 5 -8 13.96 1.10 -4 5 -8 16.23 1.16 4 -5 8 12.43 1.08 4 -5 9 6.89 0.72 -4 5 -9 6.35 0.71 -4 5 -9 6.69 0.72 4 -5 9 5.09 0.70 4 -5 10 6.95 0.69 -4 5 -10 5.41 0.63 4 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3.57 4 3 -10 125.17 3.71 4 3 -10 128.29 3.85 4 3 -10 126.88 3.61 4 3 -9 78.70 2.69 4 3 -9 79.27 2.72 4 3 -8 23.19 1.24 4 3 -8 21.91 1.20 4 3 -7 1.22 0.41 4 3 -7 0.98 0.42 4 3 -7 -0.06 0.00 4 3 -7 0.92 0.63 4 3 -7 0.81 0.38 4 3 -6 0.88 0.40 4 3 -6 1.03 0.40 4 3 -6 0.71 0.39 4 3 -6 0.58 0.52 4 3 -6 0.79 0.36 4 3 -6 1.32 0.45 4 3 -5 120.77 3.75 4 3 -5 116.98 3.61 4 3 -5 117.32 3.68 4 3 -5 115.79 3.85 4 3 -5 116.84 3.74 4 3 -5 119.30 3.62 4 3 -5 112.72 3.73 4 3 -4 10.04 0.83 4 3 -4 8.56 0.75 4 3 -4 8.25 0.89 4 3 -4 8.30 0.77 4 3 -4 9.23 0.90 4 3 -4 9.00 0.85 4 3 -4 8.33 0.80 4 3 -4 9.01 0.76 4 3 -4 7.91 0.81 4 3 -4 8.41 0.94 4 3 -3 8.82 0.91 4 3 -3 8.58 0.81 4 3 -3 8.80 0.89 4 3 -3 10.84 0.81 4 3 -3 8.54 0.71 4 3 -3 -0.05 0.17 4 3 -3 8.10 0.77 4 3 -3 8.42 0.82 4 3 -3 7.18 0.79 4 3 -3 9.65 0.84 4 3 -3 8.69 0.75 4 3 -3 7.91 0.79 4 3 -3 8.08 0.78 4 3 -3 -0.04 0.01 4 3 -2 79.23 2.49 4 3 -2 -0.04 0.00 4 3 -2 -0.05 0.00 4 3 -2 -0.04 0.00 4 3 -2 -0.05 0.00 4 3 -2 87.18 2.49 4 3 -2 32.80 1.33 4 3 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4 3 3 7.18 0.74 4 3 3 7.18 0.78 4 3 3 6.65 0.77 4 3 3 7.25 0.74 4 3 3 6.00 0.72 4 3 3 9.20 0.87 4 3 3 6.14 0.74 4 3 4 33.73 1.49 4 3 4 29.70 1.52 4 3 4 31.63 1.61 4 3 4 33.36 1.58 4 3 4 29.99 1.58 4 3 4 27.54 1.58 4 3 4 33.17 1.69 4 3 4 32.17 1.63 4 3 4 31.50 1.61 4 3 5 50.31 1.95 4 3 5 47.37 2.10 4 3 5 47.01 2.08 4 3 5 50.58 2.19 4 3 5 53.51 2.26 4 3 5 50.18 2.08 4 3 6 12.64 0.99 4 3 6 11.98 0.99 4 3 6 12.04 0.99 4 3 6 12.75 1.00 4 3 6 11.43 1.01 -4 -3 -7 355.14 8.96 4 3 7 367.90 9.31 4 3 7 342.21 8.92 -4 -3 -7 355.48 8.72 -4 -3 -8 82.50 2.78 4 3 8 73.89 2.98 -4 -3 -8 75.48 2.90 -4 -3 -8 79.71 2.68 -4 -3 -9 32.80 1.65 -4 -3 -9 33.08 1.83 -4 -3 -9 32.37 1.59 -4 -3 -10 193.21 5.53 -4 -3 -10 194.27 5.84 -4 -3 -11 38.42 1.84 -4 -3 -11 36.82 2.02 -4 -3 -12 84.34 2.94 -4 -3 -12 84.41 3.20 4 3 12 81.88 2.84 -4 -3 -13 1.07 0.37 -4 -3 -13 0.68 0.39 4 3 14 63.32 2.32 -4 -3 -14 65.27 2.20 -4 -3 -15 10.54 0.63 4 4 -11 67.84 2.02 4 4 -10 17.21 0.95 4 4 -10 17.56 1.23 4 4 -10 15.62 0.92 4 4 -9 57.90 2.13 4 4 -9 58.85 2.37 4 4 -9 56.26 2.34 4 4 -9 57.39 2.18 4 4 -9 56.54 2.13 4 4 -8 24.09 1.49 4 4 -8 19.80 1.62 4 4 -8 20.55 1.28 4 4 -7 22.75 1.38 4 4 -7 20.83 1.29 4 4 -7 22.54 1.26 4 4 -7 19.89 1.66 4 4 -7 22.84 1.34 4 4 -6 11.47 0.90 4 4 -6 12.29 1.38 4 4 -6 12.14 0.97 4 4 -6 12.09 0.99 4 4 -6 14.21 1.12 4 4 -5 158.24 4.90 4 4 -5 153.92 4.73 4 4 -5 168.05 4.82 4 4 -5 151.39 4.51 4 4 -5 156.93 4.67 4 4 -5 157.29 4.94 4 4 -5 154.82 4.61 4 4 -4 60.51 2.04 4 4 -4 71.82 2.27 4 4 -4 65.53 2.24 4 4 -4 65.02 2.15 4 4 -4 64.10 2.41 4 4 -4 67.96 2.30 4 4 -3 197.78 3.32 4 4 -3 -0.08 0.00 4 4 -3 216.80 3.68 4 4 -3 87.27 2.36 4 4 -3 202.10 3.75 4 4 -3 196.56 3.86 4 4 -3 199.45 3.81 4 4 -3 198.36 4.02 4 4 -3 -0.04 0.00 4 4 -3 202.29 3.76 4 4 -3 -0.05 0.00 4 4 -3 199.05 3.73 4 4 -3 208.92 4.21 4 4 -2 136.52 2.67 4 4 -2 -0.08 0.00 4 4 -2 -0.06 0.00 4 4 -2 140.67 2.72 4 4 -2 141.28 3.31 4 4 -2 144.65 3.39 4 4 -2 -0.05 0.00 4 4 -2 142.50 2.58 4 4 -2 -0.06 0.00 4 4 -2 136.80 3.17 4 4 -2 139.81 3.44 4 4 -2 135.69 3.11 4 4 -1 14.54 1.11 4 4 -1 -0.07 0.00 4 4 -1 -0.08 0.00 4 4 -1 14.62 0.82 4 4 -1 -0.05 0.00 4 4 -1 13.88 1.09 4 4 -1 13.44 1.06 4 4 -1 13.47 1.02 4 4 -1 -0.07 0.00 4 4 -1 13.10 1.41 4 4 -1 9.56 0.74 4 4 -1 -0.05 0.00 4 4 -1 14.76 0.88 4 4 0 -0.07 0.00 4 4 0 -0.07 0.00 4 4 0 280.99 4.54 4 4 0 291.06 3.39 4 4 0 287.45 4.46 4 4 0 287.48 4.73 4 4 0 283.77 3.54 4 4 0 297.24 4.00 4 4 0 -0.07 0.00 4 4 0 -0.05 0.00 4 4 0 284.16 3.94 4 4 0 284.57 3.75 4 4 1 1101.76 7.06 4 4 1 1205.11 9.56 4 4 1 1180.31 9.12 4 4 1 1158.70 6.54 4 4 1 1222.12 7.73 4 4 1 1174.37 9.53 4 4 1 1194.83 9.69 4 4 1 1171.89 6.85 4 4 1 1205.82 7.68 4 4 2 106.87 3.10 4 4 2 105.63 3.68 4 4 2 105.03 3.62 4 4 2 107.22 3.62 4 4 2 115.20 3.79 4 4 2 111.03 3.70 4 4 2 104.09 3.58 4 4 2 115.79 3.32 4 4 2 102.30 3.02 4 4 2 105.84 3.17 4 4 2 102.82 3.63 4 4 3 8.94 0.75 4 4 3 7.49 0.81 4 4 3 9.05 0.91 4 4 3 7.91 0.87 4 4 3 7.84 0.86 4 4 3 7.16 0.84 4 4 3 8.72 0.64 4 4 3 7.22 0.62 4 4 3 7.90 0.85 4 4 3 10.02 0.90 4 4 4 -0.07 0.34 4 4 4 0.64 0.38 4 4 4 0.33 0.36 4 4 4 0.06 0.29 4 4 4 -0.07 0.39 4 4 4 -0.12 0.35 4 4 4 -0.31 0.38 4 4 4 0.28 0.30 4 4 4 0.24 0.36 4 4 5 35.10 1.89 4 4 5 40.73 1.98 4 4 5 41.41 1.92 4 4 5 38.76 1.94 4 4 5 39.48 1.89 4 4 5 40.39 1.91 4 4 5 38.53 1.74 4 4 5 41.07 1.93 4 4 6 0.47 0.37 4 4 6 0.49 0.34 4 4 6 0.78 0.37 4 4 6 0.95 0.40 4 4 6 0.90 0.37 -4 -4 -7 803.44 18.26 4 4 7 825.32 18.87 4 4 7 782.84 18.54 4 4 7 791.66 18.78 4 4 7 776.02 18.64 -4 -4 -8 398.08 9.78 -4 -4 -8 401.85 9.96 4 4 8 381.19 9.98 -4 -4 -9 424.80 10.64 -4 -4 -9 412.04 10.37 -4 -4 -9 421.02 10.32 -4 -4 -10 15.18 1.20 -4 -4 -10 15.54 1.10 -4 -4 -10 17.48 1.18 -4 -4 -11 102.19 3.42 4 4 12 9.49 0.94 4 4 12 9.43 0.85 -4 -4 -13 10.09 0.78 4 4 13 9.54 0.85 4 4 13 8.21 0.70 -4 -4 -14 3.27 0.43 4 4 14 2.86 0.43 -4 -4 -15 64.40 1.87 4 5 -10 100.68 2.90 4 5 -10 105.30 2.89 4 5 -9 47.55 1.84 4 5 -9 46.13 1.80 4 5 -9 48.20 1.80 4 5 -8 139.68 4.15 4 5 -8 139.68 4.13 4 5 -8 129.39 4.02 4 5 -8 141.72 4.04 4 5 -7 181.58 5.15 4 5 -7 173.28 5.07 4 5 -6 109.82 3.79 4 5 -6 111.56 3.72 4 5 -6 110.15 3.83 4 5 -6 107.33 3.59 4 5 -6 105.16 3.67 4 5 -6 106.11 3.46 4 5 -5 67.25 2.75 4 5 -5 67.75 2.72 4 5 -5 68.30 2.84 4 5 -5 67.24 2.61 4 5 -5 66.57 2.77 4 5 -5 64.82 2.46 4 5 -4 160.38 4.83 4 5 -4 158.73 4.92 4 5 -4 159.25 4.54 4 5 -4 160.29 4.96 4 5 -4 160.01 4.71 4 5 -4 148.96 4.64 4 5 -3 2.60 1.19 4 5 -3 1.40 0.38 4 5 -3 1.18 0.49 4 5 -3 2.64 1.61 4 5 -3 1.37 0.48 4 5 -3 2.06 0.50 4 5 -3 0.92 0.46 4 5 -3 2.53 0.50 4 5 -3 -0.06 0.00 4 5 -2 102.72 2.55 4 5 -2 94.91 3.08 4 5 -2 -0.06 0.00 4 5 -2 103.18 2.45 4 5 -2 94.06 2.92 4 5 -2 104.48 3.13 4 5 -2 96.63 2.21 4 5 -2 -0.06 0.00 4 5 -2 106.02 3.42 4 5 -2 105.33 2.92 4 5 -2 0.40 0.41 4 5 -1 71.40 1.84 4 5 -1 -0.06 0.00 4 5 -1 72.52 2.06 4 5 -1 73.72 2.66 4 5 -1 73.15 2.27 4 5 -1 -0.08 0.00 4 5 -1 75.23 2.95 4 5 -1 76.79 2.48 4 5 -1 73.89 2.63 4 5 -1 77.08 2.18 4 5 -1 -0.06 0.00 4 5 -1 74.22 1.99 4 5 0 46.75 1.43 4 5 0 43.47 1.56 4 5 0 47.17 2.09 4 5 0 46.52 2.16 4 5 0 44.70 1.83 4 5 0 48.96 2.48 4 5 0 43.82 1.91 4 5 0 44.92 2.05 4 5 0 45.84 1.71 4 5 0 46.26 1.62 4 5 0 44.15 1.46 4 5 0 44.91 1.68 4 5 1 13.04 0.86 4 5 1 14.50 1.20 4 5 1 13.80 1.33 4 5 1 14.31 1.23 4 5 1 13.60 1.08 4 5 1 14.13 0.96 4 5 1 12.85 1.11 4 5 1 13.95 1.19 4 5 1 13.19 0.94 4 5 1 13.51 0.90 4 5 1 11.60 0.80 4 5 1 14.35 0.99 4 5 2 160.18 5.06 4 5 2 150.66 5.00 4 5 2 164.79 4.86 4 5 2 157.47 4.48 4 5 2 152.40 4.99 4 5 2 151.38 4.85 4 5 2 156.35 4.45 4 5 2 160.36 4.33 4 5 2 158.41 4.44 4 5 3 207.20 6.05 4 5 3 198.34 5.89 4 5 3 204.87 6.06 4 5 3 206.33 5.88 4 5 3 210.64 5.57 4 5 3 202.61 5.92 4 5 3 202.85 6.07 4 5 3 195.40 5.35 4 5 3 203.37 5.38 4 5 4 293.85 8.21 4 5 4 327.58 7.95 4 5 4 315.76 8.28 4 5 4 306.30 8.42 4 5 4 308.64 8.29 4 5 4 301.61 8.36 4 5 5 113.11 3.82 4 5 5 112.00 3.56 4 5 5 112.46 3.83 4 5 5 104.63 3.77 4 5 5 109.16 3.89 4 5 5 106.00 3.83 4 5 6 5.38 0.74 4 5 6 4.89 0.69 4 5 6 5.71 0.77 4 5 6 4.73 0.72 4 5 6 3.97 0.67 4 5 6 5.39 0.76 4 5 7 0.56 0.40 4 5 7 2.10 0.57 4 5 7 1.23 0.49 -4 -5 -8 93.04 3.20 4 5 8 97.21 3.54 4 5 8 100.62 3.60 -4 -5 -9 406.89 10.18 4 5 9 406.66 10.42 4 5 9 410.83 10.56 4 5 10 324.15 8.69 -4 -5 -10 326.84 8.40 4 5 11 194.95 5.69 4 5 12 1.04 0.38 4 5 12 0.84 0.36 -4 -5 -12 0.91 0.35 4 5 13 2.32 0.41 -4 -5 -13 3.90 0.48 -4 -5 -14 4.18 0.42 4 6 -9 4.48 0.47 4 6 -9 4.39 0.47 4 6 -9 4.22 0.43 4 6 -8 29.42 1.40 4 6 -8 27.79 1.35 4 6 -8 28.11 1.28 4 6 -7 1.69 0.47 4 6 -7 1.27 0.41 4 6 -7 0.95 0.35 4 6 -6 163.44 4.99 4 6 -6 159.57 4.71 4 6 -5 20.05 1.38 4 6 -5 19.09 1.34 4 6 -5 19.58 1.17 4 6 -4 141.66 4.38 4 6 -4 134.41 4.41 4 6 -4 133.26 3.99 4 6 -4 139.23 4.47 4 6 -4 129.24 4.13 4 6 -3 37.75 2.10 4 6 -3 38.62 2.00 4 6 -3 42.46 2.00 4 6 -3 41.41 1.75 4 6 -3 41.62 2.07 4 6 -3 42.32 1.88 4 6 -2 6.34 0.64 4 6 -2 5.45 0.85 4 6 -2 5.86 0.86 4 6 -2 6.66 0.83 4 6 -2 4.38 0.70 4 6 -2 4.57 0.60 4 6 -2 5.33 0.68 4 6 -2 8.22 0.87 4 6 -1 154.25 3.56 4 6 -1 151.06 3.95 4 6 -1 158.65 4.30 4 6 -1 156.36 3.74 4 6 -1 156.51 3.31 4 6 -1 154.10 4.30 4 6 -1 151.57 3.08 4 6 0 122.57 3.89 4 6 0 120.63 3.73 4 6 0 118.57 4.37 4 6 0 113.34 4.09 4 6 0 120.75 4.01 4 6 0 119.87 3.55 4 6 0 120.03 3.86 4 6 0 118.87 4.31 4 6 1 1.92 0.54 4 6 1 1.59 0.51 4 6 1 2.06 0.40 4 6 1 1.54 0.56 4 6 1 1.95 0.46 4 6 1 1.41 0.45 4 6 2 5.35 0.62 4 6 2 5.71 0.80 4 6 2 5.74 0.88 4 6 2 4.89 0.76 4 6 2 4.04 0.73 4 6 2 4.41 0.60 4 6 2 4.57 0.61 4 6 3 4.83 0.79 4 6 3 5.99 0.82 4 6 3 4.96 0.64 4 6 3 4.48 0.78 4 6 3 5.57 0.63 4 6 3 4.98 0.60 4 6 4 96.52 3.59 4 6 4 97.38 3.25 4 6 4 99.72 3.65 4 6 4 93.81 3.62 4 6 4 95.96 3.75 4 6 4 102.32 3.78 4 6 5 11.88 1.12 4 6 5 11.19 0.95 4 6 5 13.48 1.20 4 6 5 8.90 1.08 4 6 5 12.23 1.17 4 6 5 10.73 1.07 4 6 6 1464.07 33.42 4 6 6 1456.21 33.49 4 6 6 1449.77 33.57 4 6 6 1506.03 33.10 4 6 7 316.50 8.53 4 6 7 320.72 8.61 4 6 7 305.60 8.48 4 6 7 311.08 8.52 4 6 7 313.67 8.24 4 6 8 51.27 2.13 4 6 8 48.86 2.11 4 6 8 48.15 2.05 4 6 9 0.49 0.34 4 6 9 0.93 0.42 4 6 9 0.88 0.44 4 6 10 49.95 2.17 4 6 11 84.90 2.95 -4 -6 -11 86.50 2.86 4 6 12 60.82 2.22 -4 -6 -12 62.67 2.15 4 6 13 8.79 0.64 -4 -6 -13 7.94 0.58 4 7 -8 17.42 0.89 4 7 -8 17.52 0.93 4 7 -7 40.46 1.51 4 7 -7 41.75 1.65 4 7 -7 38.55 1.67 4 7 -7 43.20 1.74 4 7 -6 7.57 0.64 4 7 -6 7.13 0.71 4 7 -6 8.73 0.83 4 7 -6 8.97 0.83 4 7 -5 214.36 5.63 4 7 -5 213.13 6.14 4 7 -5 220.68 5.88 4 7 -5 218.32 6.13 4 7 -5 224.10 6.07 4 7 -4 24.87 1.52 4 7 -4 22.58 1.31 4 7 -3 137.67 4.44 4 7 -3 135.81 4.42 4 7 -3 133.61 4.26 4 7 -2 269.92 7.75 4 7 -2 274.07 7.42 4 7 -2 256.84 6.90 4 7 -2 278.54 7.45 4 7 -2 270.74 7.20 4 7 -1 49.04 2.35 4 7 -1 44.53 2.45 4 7 -1 45.86 2.19 4 7 -1 47.27 2.08 4 7 -1 50.39 2.26 4 7 0 139.48 4.34 4 7 0 133.17 4.58 4 7 0 140.74 4.89 4 7 0 136.07 4.40 4 7 0 130.88 4.71 4 7 0 138.11 4.35 4 7 0 130.71 4.07 4 7 1 1.92 0.49 4 7 1 1.81 0.49 4 7 1 1.09 0.52 4 7 1 1.78 0.55 4 7 1 1.90 0.56 4 7 2 0.88 0.35 4 7 2 0.53 0.41 4 7 2 0.59 0.36 4 7 2 0.09 0.35 4 7 2 -0.08 0.22 4 7 3 3.92 0.60 4 7 3 5.61 0.80 4 7 3 5.11 0.75 4 7 3 5.77 0.68 4 7 4 9.02 0.78 4 7 4 8.91 1.07 4 7 4 9.74 1.08 4 7 4 9.13 0.83 4 7 4 8.49 0.94 4 7 5 218.15 4.51 4 7 5 234.26 3.92 4 7 5 222.38 4.71 4 7 5 230.75 4.99 4 7 6 77.39 2.86 4 7 6 77.58 3.20 4 7 6 76.78 3.21 4 7 6 79.45 3.31 4 7 7 337.16 9.01 4 7 7 319.99 8.92 4 7 7 336.56 8.97 4 7 8 104.73 3.86 4 7 8 107.76 3.83 4 7 9 274.08 7.23 4 7 10 79.98 2.94 4 7 10 88.73 2.92 4 7 11 8.49 0.73 4 7 11 7.18 0.67 -4 -7 -11 8.28 0.65 -4 -7 -12 1.16 0.27 4 7 12 1.43 0.31 4 8 -7 12.02 0.71 4 8 -6 27.60 1.25 4 8 -6 24.30 1.22 4 8 -6 25.00 1.11 4 8 -5 3.51 0.57 4 8 -5 3.46 0.49 4 8 -5 3.38 0.56 4 8 -4 -0.17 0.36 4 8 -4 0.10 0.25 4 8 -4 -0.29 0.40 4 8 -3 0.68 0.41 4 8 -3 1.48 0.47 4 8 -3 0.58 0.33 4 8 -2 24.46 1.48 4 8 -2 21.83 1.56 4 8 -2 24.40 1.35 4 8 -1 0.59 0.40 4 8 -1 0.09 0.39 4 8 0 39.32 1.92 4 8 0 38.19 2.05 4 8 0 38.31 2.23 4 8 1 5.54 0.76 4 8 1 6.41 0.86 4 8 1 6.35 0.93 4 8 1 6.07 0.76 4 8 2 0.56 0.36 4 8 2 1.31 0.51 4 8 2 1.23 0.41 4 8 2 1.08 0.49 4 8 3 32.14 1.92 4 8 3 32.91 1.75 4 8 4 87.66 3.10 4 8 4 81.05 2.75 4 8 5 129.11 3.54 4 8 5 123.31 3.56 4 8 6 8.80 0.97 4 8 6 8.75 0.99 4 8 6 7.71 0.73 4 8 7 3.99 0.68 4 8 7 3.62 0.60 4 8 7 3.86 0.55 4 8 8 126.13 4.16 4 8 8 128.49 4.21 4 8 8 134.78 3.89 4 8 9 15.08 1.05 4 8 9 15.06 0.96 4 8 9 15.17 1.09 4 8 10 105.43 3.09 4 8 10 101.76 3.23 4 8 11 40.92 1.50 4 8 11 40.50 1.50 4 9 -5 7.30 0.54 4 9 -5 8.39 0.62 4 9 -4 30.63 1.42 4 9 -4 31.62 1.29 4 9 -4 33.06 1.46 4 9 -3 0.51 0.33 4 9 -3 0.33 0.33 4 9 -2 113.52 3.57 4 9 -2 110.09 3.51 4 9 -1 56.45 2.23 4 9 -1 51.52 2.34 4 9 -1 51.19 2.35 4 9 -1 52.24 2.15 4 9 0 1.07 0.45 4 9 0 0.15 0.40 4 9 0 0.67 0.36 4 9 0 0.97 0.37 4 9 1 45.93 1.98 4 9 1 45.81 2.13 4 9 1 44.13 2.29 4 9 1 42.28 1.90 4 9 2 36.25 1.91 4 9 2 36.18 2.08 4 9 2 35.31 1.76 4 9 2 40.10 1.79 4 9 2 36.76 1.68 4 9 3 17.70 1.22 4 9 3 14.87 1.23 4 9 3 16.40 1.37 4 9 3 16.19 1.06 4 9 4 139.86 4.44 4 9 4 143.45 4.62 4 9 4 145.01 4.76 4 9 5 474.79 11.49 4 9 5 457.75 11.57 4 9 5 457.25 11.65 4 9 5 452.60 11.66 4 9 6 219.41 6.10 4 9 6 221.63 6.18 4 9 6 210.55 6.09 4 9 6 217.83 6.18 4 9 7 7.23 0.77 4 9 7 7.26 0.80 4 9 7 8.39 0.79 4 9 7 8.85 0.81 4 9 8 9.99 0.84 4 9 8 9.03 0.79 4 9 9 38.48 1.59 4 9 9 35.65 1.48 4 9 10 1.10 0.28 4 10 -3 63.82 1.98 4 10 -2 3.38 0.44 4 10 -2 2.79 0.41 4 10 -1 0.04 0.24 4 10 -1 0.21 0.27 4 10 0 -0.31 0.37 4 10 0 0.25 0.34 4 10 0 0.39 0.26 4 10 0 0.36 0.27 4 10 1 3.53 0.47 4 10 1 2.93 0.56 4 10 1 3.07 0.54 4 10 2 1.22 0.34 4 10 2 1.06 0.42 4 10 2 0.40 0.37 4 10 2 0.42 0.32 4 10 3 11.63 0.91 4 10 3 11.84 0.97 4 10 3 11.17 0.97 4 10 4 44.66 1.90 4 10 4 45.90 2.00 4 10 4 47.03 2.03 4 10 5 7.73 0.67 4 10 5 6.95 0.70 4 10 5 5.13 0.62 4 10 5 7.53 0.75 4 10 6 146.27 3.97 4 10 6 147.15 4.05 4 10 7 12.35 0.80 4 10 7 12.01 0.79 4 10 8 4.97 0.47 -5 8 3 3.07 0.39 -5 8 2 23.90 1.13 -5 8 1 70.48 2.33 -5 8 0 29.93 1.35 -5 8 -1 93.89 2.94 -5 8 -1 98.64 2.99 -5 8 -2 63.42 2.18 -5 8 -2 66.27 2.24 -5 8 -3 13.22 0.83 -5 8 -4 16.87 0.90 -5 8 -5 0.86 0.24 5 -7 -6 7.31 0.57 -5 7 6 6.33 0.50 5 -7 -5 4.53 0.52 -5 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5 2 -2 64.18 1.82 5 2 -2 64.21 1.98 5 2 -2 63.22 2.24 5 2 -2 65.28 2.27 5 2 -2 65.70 2.37 5 2 -2 65.28 2.08 5 2 -1 0.41 0.36 5 2 -1 0.48 0.38 5 2 -1 0.22 0.37 5 2 -1 0.21 0.43 5 2 -1 -0.06 0.00 5 2 -1 -0.06 0.00 5 2 -1 0.68 0.34 5 2 -1 0.15 0.26 5 2 -1 0.17 0.30 5 2 -1 0.64 0.34 5 2 -1 0.13 0.24 5 2 -1 0.21 0.26 5 2 -1 0.60 0.40 5 2 0 190.58 3.43 5 2 0 182.34 3.52 5 2 0 175.47 2.90 5 2 0 184.04 3.75 5 2 0 175.04 3.71 5 2 0 173.93 3.67 5 2 0 178.47 3.74 5 2 0 178.45 3.87 5 2 0 178.82 3.29 5 2 0 180.35 3.21 5 2 0 186.87 3.87 5 2 1 575.28 6.36 5 2 1 577.08 6.10 5 2 1 571.21 6.70 5 2 1 586.94 6.97 5 2 1 587.73 5.72 5 2 1 559.42 5.49 5 2 1 581.47 6.60 5 2 1 570.73 6.73 5 2 2 0.05 0.43 5 2 2 0.06 0.33 5 2 2 0.07 0.30 5 2 2 -0.07 0.00 5 2 2 0.13 0.33 5 2 2 -0.05 0.22 5 2 2 0.25 0.36 5 2 2 0.55 0.44 5 2 3 71.80 2.38 5 2 3 72.44 2.26 5 2 3 67.74 2.15 5 2 3 68.47 2.33 5 2 3 68.52 2.04 5 2 3 68.95 2.36 5 2 3 68.79 2.24 5 2 4 3.17 0.59 5 2 4 2.20 0.52 5 2 4 2.71 0.63 5 2 4 3.99 0.59 5 2 4 2.88 0.98 5 2 4 2.92 0.56 5 2 4 2.50 0.46 5 2 5 34.25 1.84 5 2 5 34.04 1.83 5 2 5 33.47 1.71 5 2 5 32.48 1.92 5 2 5 34.60 1.63 5 2 5 35.21 1.82 5 2 5 35.06 1.95 5 2 6 0.16 0.37 5 2 6 0.28 0.34 5 2 6 0.21 0.35 5 2 6 0.05 0.31 5 2 7 200.73 6.17 5 2 7 201.77 5.57 5 2 8 2.39 0.49 5 2 8 3.31 0.71 -5 -2 -9 146.82 4.34 5 2 9 146.25 4.39 5 2 9 150.10 4.99 5 2 10 0.32 0.43 -5 -2 -10 0.21 0.29 -5 -2 -10 0.30 0.39 -5 -2 -11 2.41 0.50 -5 -2 -11 3.07 0.61 -5 -2 -12 4.73 0.58 -5 -2 -12 4.96 0.72 -5 -2 -13 3.38 0.46 -5 -2 -13 4.17 0.59 5 2 14 57.50 2.12 -5 -2 -14 57.94 1.89 -5 -2 -14 61.88 2.13 5 3 -10 0.43 0.86 5 3 -10 0.02 0.37 5 3 -9 42.93 1.95 5 3 -9 42.92 1.84 5 3 -9 42.63 1.65 5 3 -9 43.33 1.65 5 3 -8 89.72 3.08 5 3 -8 87.25 2.84 5 3 -8 86.56 2.88 5 3 -8 94.25 3.14 5 3 -7 0.58 0.36 5 3 -7 0.47 0.47 5 3 -7 0.31 0.86 5 3 -6 41.26 1.60 5 3 -6 41.70 1.69 5 3 -6 44.10 1.76 5 3 -6 46.26 1.85 5 3 -5 262.68 4.30 5 3 -5 256.23 3.92 5 3 -5 264.45 4.19 5 3 -5 268.39 4.38 5 3 -4 3.59 0.59 5 3 -4 3.37 0.78 5 3 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4.10 0.57 5 3 0 3.57 0.64 5 3 0 6.22 0.80 5 3 0 3.65 0.68 5 3 0 5.80 0.77 5 3 1 13.58 1.24 5 3 1 -0.08 0.00 5 3 1 -0.07 0.00 5 3 1 -0.07 0.00 5 3 1 14.74 0.96 5 3 1 12.69 0.92 5 3 1 13.15 0.90 5 3 1 14.18 1.15 5 3 1 14.98 1.19 5 3 1 -0.04 0.00 5 3 1 14.52 0.97 5 3 1 12.83 0.88 5 3 1 12.88 1.08 5 3 2 15.13 0.95 5 3 2 17.15 1.21 5 3 2 13.99 0.87 5 3 2 13.84 0.90 5 3 2 15.29 1.47 5 3 2 17.15 1.19 5 3 2 15.78 1.20 5 3 2 14.31 1.16 5 3 2 16.95 1.05 5 3 2 13.88 0.89 5 3 2 12.98 1.08 5 3 2 14.38 1.14 5 3 3 11.96 0.90 5 3 3 12.22 1.04 5 3 3 13.21 0.86 5 3 3 12.43 1.02 5 3 3 11.39 1.04 5 3 3 12.32 1.08 5 3 3 14.30 1.60 5 3 3 13.95 1.15 5 3 3 12.46 1.10 5 3 3 11.82 1.10 5 3 3 13.30 1.10 5 3 4 15.76 1.02 5 3 4 16.64 1.17 5 3 4 14.33 1.09 5 3 4 14.99 1.19 5 3 4 15.69 1.24 5 3 4 13.83 1.62 5 3 4 14.86 1.18 5 3 4 14.57 1.18 5 3 4 16.41 1.29 5 3 4 14.75 1.17 5 3 5 132.70 2.89 5 3 5 136.45 3.25 5 3 5 129.27 3.14 5 3 5 128.87 3.29 5 3 5 135.41 3.31 5 3 5 128.51 3.30 5 3 5 134.44 3.57 5 3 5 129.20 3.30 5 3 6 2.29 0.49 5 3 6 1.89 0.48 5 3 6 1.58 0.55 5 3 6 1.37 0.50 5 3 6 2.39 0.54 5 3 6 1.86 0.55 5 3 6 1.97 0.48 5 3 6 -0.07 0.00 5 3 7 91.78 2.67 5 3 7 90.58 2.75 5 3 7 90.30 2.73 5 3 7 94.34 3.06 5 3 7 91.03 2.49 5 3 8 9.47 1.04 5 3 8 8.68 0.86 5 3 9 1008.52 23.56 5 3 9 999.04 22.99 -5 -3 -10 90.96 3.04 -5 -3 -10 89.14 3.31 5 3 11 90.23 3.03 -5 -3 -11 90.66 3.29 -5 -3 -12 174.68 4.86 -5 -3 -12 180.19 5.18 5 3 12 180.85 5.35 -5 -3 -13 17.62 0.97 -5 -3 -13 16.32 1.06 5 3 13 16.27 1.11 5 3 14 52.66 1.92 -5 -3 -14 52.45 1.73 5 4 -10 53.90 1.68 5 4 -9 106.69 3.01 5 4 -9 101.58 3.11 5 4 -9 106.40 3.02 5 4 -8 274.89 6.83 5 4 -8 278.27 6.91 5 4 -8 262.64 6.91 5 4 -8 270.64 6.87 5 4 -7 11.68 0.93 5 4 -7 12.46 0.90 5 4 -7 11.01 0.91 5 4 -6 7.49 1.04 5 4 -6 6.17 0.67 5 4 -6 5.81 0.72 5 4 -5 25.69 1.29 5 4 -5 25.22 1.40 5 4 -5 29.58 1.61 5 4 -5 25.40 1.55 5 4 -5 24.97 1.36 5 4 -4 16.80 1.31 5 4 -4 20.17 1.33 5 4 -4 19.55 1.19 5 4 -4 20.33 1.69 5 4 -4 16.89 1.97 5 4 -4 19.04 1.25 5 4 -3 61.55 2.41 5 4 -3 63.62 2.68 5 4 -3 61.15 2.69 5 4 -3 65.95 2.84 5 4 -3 61.49 2.63 5 4 -3 56.39 2.42 5 4 -3 62.75 2.33 5 4 -3 60.53 2.85 5 4 -3 57.54 2.94 5 4 -3 59.96 2.56 5 4 -2 -0.14 1.39 5 4 -2 0.78 0.69 5 4 -2 0.45 0.50 5 4 -2 -0.52 1.00 5 4 -2 -0.05 0.00 5 4 -2 -0.07 0.00 5 4 -2 0.61 0.42 5 4 -2 1.25 0.47 5 4 -2 -0.06 0.00 5 4 -2 0.53 0.34 5 4 -2 0.28 0.42 5 4 -1 316.52 4.13 5 4 -1 294.02 5.46 5 4 -1 329.86 5.90 5 4 -1 326.11 4.14 5 4 -1 -0.06 0.00 5 4 -1 -0.34 0.38 5 4 -1 327.12 5.18 5 4 -1 348.09 5.77 5 4 -1 326.46 5.36 5 4 -1 327.13 5.48 5 4 -1 332.03 4.38 5 4 -1 329.20 4.95 5 4 -1 -0.06 0.00 5 4 0 544.80 5.74 5 4 0 568.33 6.31 5 4 0 560.85 7.18 5 4 0 573.72 7.42 5 4 0 -0.07 0.00 5 4 0 -0.08 0.00 5 4 0 526.83 5.03 5 4 0 -0.08 0.00 5 4 0 530.22 6.92 5 4 0 551.42 7.05 5 4 0 -0.09 0.00 5 4 0 546.22 5.28 5 4 0 552.46 5.48 5 4 0 560.41 6.15 5 4 0 562.59 7.04 5 4 1 467.12 5.16 5 4 1 469.38 5.58 5 4 1 469.04 6.56 5 4 1 150.96 3.83 5 4 1 370.06 5.44 5 4 1 469.02 6.69 5 4 1 444.30 4.39 5 4 1 -0.09 0.01 5 4 1 -0.08 0.01 5 4 1 453.82 6.39 5 4 1 460.50 5.25 5 4 1 459.70 4.77 5 4 1 462.38 4.86 5 4 1 473.38 5.45 5 4 1 473.55 6.44 5 4 2 540.20 6.93 5 4 2 488.27 6.74 5 4 2 479.23 6.57 5 4 2 494.15 6.96 5 4 2 513.57 6.39 5 4 2 489.69 5.30 5 4 2 528.76 5.85 5 4 2 490.03 6.74 5 4 2 492.40 6.96 5 4 2 490.57 5.32 5 4 2 497.58 5.19 5 4 2 509.83 5.55 5 4 3 43.71 2.56 5 4 3 38.83 1.92 5 4 3 36.00 1.78 5 4 3 33.86 1.36 5 4 3 38.01 1.91 5 4 3 36.59 1.94 5 4 3 35.59 1.83 5 4 3 35.99 1.85 5 4 3 40.36 2.03 5 4 3 35.56 1.76 5 4 4 -0.06 0.00 5 4 4 90.41 2.87 5 4 4 -0.08 0.00 5 4 4 76.94 2.56 5 4 4 84.41 2.80 5 4 4 84.03 2.79 5 4 4 88.13 2.94 5 4 4 85.53 2.87 5 4 4 77.50 2.69 5 4 4 79.81 2.61 5 4 5 44.36 1.99 5 4 5 45.19 2.02 5 4 5 41.71 1.90 5 4 5 39.21 2.00 5 4 5 45.29 2.07 5 4 5 43.52 2.01 5 4 5 42.45 2.03 5 4 5 43.83 1.93 5 4 6 -0.12 0.33 5 4 6 -0.08 0.39 5 4 6 0.29 0.41 5 4 6 0.09 0.42 5 4 6 0.16 0.40 5 4 6 0.08 0.40 5 4 6 0.07 0.36 5 4 7 125.77 4.02 5 4 7 127.24 4.36 5 4 7 124.88 4.19 5 4 7 122.80 4.40 5 4 7 125.26 4.22 5 4 8 170.93 5.05 5 4 8 168.56 5.41 5 4 8 178.55 5.46 5 4 8 160.90 5.12 5 4 9 37.55 2.05 5 4 9 31.91 1.71 5 4 10 145.44 4.69 5 4 10 135.26 4.27 5 4 11 34.90 1.87 5 4 11 34.51 1.66 -5 -4 -11 34.95 1.58 5 4 12 25.19 1.46 5 4 12 22.42 1.21 -5 -4 -12 22.29 1.16 5 4 13 66.49 2.34 -5 -4 -13 64.43 2.05 5 4 14 0.83 0.27 -5 -4 -14 0.48 0.20 5 5 -9 149.36 3.77 5 5 -9 143.14 3.77 5 5 -8 173.91 4.59 5 5 -8 178.02 4.68 5 5 -8 174.32 4.66 5 5 -7 18.00 1.05 5 5 -7 17.20 1.39 5 5 -7 17.30 1.09 5 5 -7 16.49 1.05 5 5 -6 270.53 7.15 5 5 -6 271.07 7.07 5 5 -6 269.01 6.93 5 5 -5 15.55 1.18 5 5 -5 16.80 1.13 5 5 -5 15.58 1.00 5 5 -4 4.12 0.60 5 5 -4 4.24 0.72 5 5 -4 3.62 0.58 5 5 -4 3.19 0.64 5 5 -4 3.73 0.60 5 5 -3 0.74 0.39 5 5 -3 3.28 0.65 5 5 -3 1.34 1.28 5 5 -3 1.15 0.43 5 5 -3 1.18 0.47 5 5 -3 1.86 2.07 5 5 -3 1.63 0.52 5 5 -3 0.95 0.43 5 5 -2 22.70 1.32 5 5 -2 23.05 1.51 5 5 -2 19.62 1.47 5 5 -2 21.35 1.56 5 5 -2 23.92 1.65 5 5 -2 22.47 1.29 5 5 -2 26.71 2.76 5 5 -2 24.57 1.53 5 5 -2 22.24 1.38 5 5 -2 24.19 1.66 5 5 -2 20.57 1.62 5 5 -1 124.45 4.59 5 5 -1 118.46 3.83 5 5 -1 127.45 3.87 5 5 -1 132.33 4.20 5 5 -1 126.64 4.46 5 5 -1 131.79 4.58 5 5 -1 127.33 3.77 5 5 -1 129.58 5.00 5 5 -1 122.35 4.57 5 5 -1 124.37 4.35 5 5 -1 123.32 4.13 5 5 -1 121.18 3.93 5 5 0 60.84 2.27 5 5 0 65.75 2.48 5 5 0 63.17 2.79 5 5 0 66.29 2.89 5 5 0 17.90 1.85 5 5 0 63.31 2.21 5 5 0 19.83 1.85 5 5 0 63.07 2.89 5 5 0 65.14 2.25 5 5 0 63.45 2.20 5 5 0 67.33 2.50 5 5 0 63.67 2.72 5 5 1 2.83 0.92 5 5 1 2.34 0.49 5 5 1 0.80 0.43 5 5 1 1.52 0.57 5 5 1 1.18 0.50 5 5 1 0.97 0.84 5 5 1 -0.09 0.01 5 5 1 0.69 0.51 5 5 1 1.04 0.40 5 5 1 0.95 0.37 5 5 1 0.86 0.47 5 5 2 1.46 0.40 5 5 2 -0.26 0.80 5 5 2 0.37 0.46 5 5 2 0.45 0.43 5 5 2 1.59 0.45 5 5 2 -0.09 0.00 5 5 2 0.43 0.45 5 5 2 0.24 0.45 5 5 2 1.07 0.37 5 5 2 0.33 0.33 5 5 3 374.41 9.96 5 5 3 364.75 9.99 5 5 3 383.55 9.46 5 5 3 373.57 9.83 5 5 3 378.01 9.90 5 5 3 363.51 10.00 5 5 3 366.84 10.11 5 5 3 366.88 10.10 5 5 4 441.14 11.38 5 5 4 437.69 11.39 5 5 4 465.91 10.93 5 5 4 425.51 11.20 5 5 4 425.99 11.26 5 5 4 424.82 11.38 5 5 4 437.41 11.54 5 5 4 426.10 11.46 5 5 5 3.15 0.71 5 5 5 2.31 0.62 5 5 5 2.59 0.65 5 5 5 2.74 0.62 5 5 5 2.52 0.65 5 5 5 2.92 0.67 5 5 6 303.74 5.39 5 5 6 286.43 5.08 5 5 6 294.62 5.12 5 5 6 270.74 5.09 5 5 6 288.85 5.34 5 5 6 279.31 5.31 5 5 7 128.87 3.38 5 5 7 124.61 3.36 5 5 7 133.69 3.55 5 5 7 128.44 3.33 5 5 7 124.04 3.49 5 5 8 131.02 4.45 5 5 8 136.07 4.64 5 5 8 144.69 4.38 5 5 9 0.40 0.35 5 5 9 0.23 0.36 5 5 9 0.25 0.35 5 5 10 0.23 0.32 5 5 11 56.68 2.40 5 5 11 56.08 2.20 5 5 12 40.30 1.83 5 5 12 42.60 1.72 -5 -5 -12 41.97 1.57 5 5 13 76.15 2.42 5 5 13 71.77 2.25 -5 -5 -13 73.09 2.14 5 6 -8 29.45 1.18 5 6 -8 29.93 1.21 5 6 -8 30.42 1.22 5 6 -7 100.74 2.94 5 6 -7 104.10 3.05 5 6 -7 99.75 3.06 5 6 -6 37.14 1.57 5 6 -6 36.58 1.63 5 6 -6 39.58 1.74 5 6 -6 40.05 1.84 5 6 -5 273.64 7.05 5 6 -5 285.33 7.24 5 6 -5 278.75 7.53 5 6 -5 284.24 7.39 5 6 -4 51.75 2.13 5 6 -4 53.67 2.42 5 6 -3 124.12 4.11 5 6 -3 116.65 3.86 5 6 -3 114.54 3.57 5 6 -2 265.66 7.54 5 6 -2 269.53 7.71 5 6 -2 266.46 6.93 5 6 -2 277.34 7.51 5 6 -2 273.17 7.27 5 6 -2 267.53 7.06 5 6 -2 275.19 7.51 5 6 -1 0.21 0.37 5 6 -1 0.30 0.33 5 6 -1 0.19 0.45 5 6 -1 0.44 0.42 5 6 -1 0.06 0.38 5 6 -1 -0.10 0.55 5 6 -1 1.73 0.75 5 6 -1 -0.07 0.33 5 6 -1 -0.16 0.43 5 6 0 1.34 0.52 5 6 0 1.14 0.41 5 6 0 1.61 0.60 5 6 0 1.46 0.57 5 6 0 1.30 0.40 5 6 0 1.17 0.52 5 6 0 1.79 0.92 5 6 0 1.18 0.54 5 6 1 57.95 2.31 5 6 1 60.07 2.11 5 6 1 57.34 1.89 5 6 1 -0.10 0.01 5 6 1 -0.09 0.01 5 6 1 59.77 2.46 5 6 1 54.30 2.49 5 6 1 61.61 2.14 5 6 2 3.14 0.72 5 6 2 1.80 0.52 5 6 2 4.08 0.77 5 6 2 -0.09 0.00 5 6 2 -0.10 0.00 5 6 2 -0.09 0.00 5 6 2 3.27 0.54 5 6 2 2.67 0.52 5 6 3 161.75 4.26 5 6 3 154.41 3.88 5 6 3 166.45 4.23 5 6 3 163.78 4.25 5 6 3 157.20 4.10 5 6 3 163.99 3.43 5 6 3 150.88 3.11 5 6 4 48.50 2.24 5 6 4 51.65 2.36 5 6 4 50.10 2.36 5 6 4 54.65 2.46 5 6 4 53.42 1.97 5 6 5 18.98 1.53 5 6 5 22.91 1.60 5 6 5 18.85 1.48 5 6 5 20.30 1.56 5 6 5 21.00 1.61 5 6 5 20.49 1.54 5 6 5 19.99 1.32 5 6 6 280.83 8.13 5 6 6 291.93 8.10 5 6 6 289.13 8.16 5 6 6 299.32 7.76 5 6 6 282.51 8.04 5 6 6 289.48 8.16 5 6 6 290.17 8.31 5 6 7 1004.78 23.37 5 6 7 1004.44 23.27 5 6 7 979.24 23.19 5 6 7 987.20 23.23 5 6 8 5.19 0.76 5 6 8 6.46 0.82 5 6 8 4.81 0.68 5 6 8 5.09 0.73 5 6 9 267.11 7.54 5 6 9 279.81 7.30 5 6 10 0.13 0.32 5 6 10 0.21 0.34 5 6 10 0.38 0.29 5 6 11 0.57 0.32 5 6 11 0.67 0.33 5 6 12 16.30 0.95 5 6 12 18.30 0.97 5 7 -7 3.21 0.40 5 7 -7 4.09 0.44 5 7 -6 7.90 0.66 5 7 -6 6.80 0.59 5 7 -5 1.92 0.44 5 7 -5 1.92 0.57 5 7 -5 2.51 0.49 5 7 -5 2.15 0.44 5 7 -4 0.81 0.38 5 7 -4 1.20 0.59 5 7 -4 0.84 0.44 5 7 -4 0.69 0.35 5 7 -4 1.55 0.48 5 7 -3 84.40 3.11 5 7 -3 79.33 2.85 5 7 -3 76.90 2.60 5 7 -3 79.59 2.70 5 7 -3 88.15 3.15 5 7 -2 139.75 4.66 5 7 -2 133.59 3.99 5 7 -2 146.62 4.53 5 7 -1 3.46 0.63 5 7 -1 3.41 0.72 5 7 -1 2.19 0.60 5 7 -1 2.91 0.54 5 7 -1 2.94 0.58 5 7 0 4.70 0.78 5 7 0 4.80 0.62 5 7 0 5.27 0.82 5 7 0 5.72 0.76 5 7 0 5.76 0.89 5 7 0 5.48 0.90 5 7 1 8.14 0.91 5 7 1 9.05 0.89 5 7 1 9.89 1.04 5 7 1 8.15 1.02 5 7 1 8.93 0.89 5 7 2 -0.08 0.00 5 7 2 -0.09 0.00 5 7 2 0.24 0.36 5 7 2 0.15 0.37 5 7 2 -0.09 0.39 5 7 2 0.06 0.29 5 7 3 0.32 0.45 5 7 3 0.36 0.41 5 7 3 -0.09 0.00 5 7 3 0.28 0.43 5 7 3 0.28 0.31 5 7 4 70.47 2.71 5 7 4 75.43 2.75 5 7 4 72.05 2.80 5 7 5 30.74 1.77 5 7 5 32.55 1.51 5 7 5 27.78 1.67 5 7 5 31.80 1.85 5 7 5 31.48 1.88 5 7 6 22.72 1.36 5 7 6 22.02 1.57 5 7 6 25.94 1.66 5 7 6 20.18 1.52 5 7 6 22.12 1.60 5 7 7 56.48 2.30 5 7 7 54.03 2.52 5 7 8 85.94 2.96 5 7 8 87.80 3.21 5 7 8 82.09 3.11 5 7 9 19.16 1.27 5 7 9 20.96 1.22 5 7 10 4.69 0.61 5 7 10 6.52 0.64 5 7 11 28.63 1.28 5 8 -6 0.23 0.21 5 8 -5 6.54 0.55 5 8 -5 6.12 0.58 5 8 -4 99.21 3.18 5 8 -4 103.60 3.03 5 8 -3 38.11 1.61 5 8 -3 37.51 1.77 5 8 -3 41.78 1.86 5 8 -2 3.16 0.48 5 8 -2 4.70 0.68 5 8 -2 4.22 0.62 5 8 -1 22.28 1.50 5 8 -1 25.01 1.60 5 8 -1 26.54 1.49 5 8 -1 23.76 1.41 5 8 0 8.18 0.95 5 8 0 7.65 0.94 5 8 0 7.72 0.86 5 8 0 6.91 0.79 5 8 0 9.08 0.86 5 8 1 21.67 1.60 5 8 1 20.18 1.44 5 8 1 21.02 1.29 5 8 1 21.33 1.33 5 8 2 5.52 0.69 5 8 2 9.14 1.07 5 8 2 7.38 0.75 5 8 2 7.51 0.91 5 8 3 82.60 2.91 5 8 3 89.32 3.59 5 8 3 90.08 3.41 5 8 4 47.23 2.40 5 8 4 42.77 2.19 5 8 5 0.73 0.45 5 8 5 0.47 0.45 5 8 5 0.91 0.47 5 8 5 0.56 0.37 5 8 6 132.53 4.36 5 8 6 129.54 4.33 5 8 6 140.89 4.52 5 8 6 135.29 4.34 5 8 6 123.72 4.17 5 8 6 136.70 3.94 5 8 7 0.94 0.40 5 8 7 0.50 0.32 5 8 7 0.06 0.30 5 8 7 0.25 0.36 5 8 7 0.04 0.27 5 8 8 27.77 1.47 5 8 8 27.32 1.31 5 8 8 27.67 1.51 5 8 9 15.27 0.90 5 8 9 13.12 0.89 5 8 9 13.98 0.97 5 8 10 1.92 0.35 5 8 10 1.88 0.35 5 9 -3 29.80 1.28 5 9 -2 4.03 0.52 5 9 -2 4.89 0.56 5 9 -1 20.42 1.15 5 9 -1 20.24 1.12 5 9 0 15.18 1.00 5 9 0 15.28 1.10 5 9 0 15.14 1.13 5 9 0 13.68 0.95 5 9 1 4.32 0.59 5 9 1 4.96 0.64 5 9 1 4.28 0.68 5 9 1 4.65 0.68 5 9 2 200.75 5.39 5 9 2 194.49 5.81 5 9 2 206.68 5.97 5 9 2 206.40 5.74 5 9 3 2.31 0.57 5 9 3 2.20 0.52 5 9 4 33.64 1.64 5 9 4 34.30 1.78 5 9 4 33.48 1.83 5 9 4 34.11 1.75 5 9 5 1.32 0.44 5 9 5 1.39 0.46 5 9 5 1.48 0.44 5 9 5 1.32 0.47 5 9 6 81.51 2.82 5 9 6 80.10 2.83 5 9 6 80.26 2.87 5 9 6 88.76 2.94 5 9 7 0.18 0.29 5 9 7 0.08 0.26 5 9 8 61.92 2.13 5 9 8 58.83 2.06 5 10 1 15.58 0.93 5 10 2 0.33 0.30 5 10 3 8.87 0.69 5 10 3 10.15 0.78 5 10 4 12.89 0.84 5 10 4 14.32 0.90 5 10 5 45.62 1.71 5 10 5 45.17 1.68 5 10 6 83.42 2.50 -6 7 2 7.96 0.58 6 -7 -2 8.09 0.53 -6 7 1 103.30 2.92 6 -7 -1 97.23 2.79 -6 7 0 18.41 0.98 -6 7 -1 29.26 1.32 -6 7 -1 30.60 1.33 -6 7 -2 4.05 0.49 -6 7 -2 4.59 0.50 -6 7 -3 4.01 0.47 -6 7 -4 54.37 1.85 -6 7 -5 180.53 4.53 6 -6 -5 116.62 3.19 -6 6 4 5.32 0.50 6 -6 -4 5.89 0.48 -6 6 3 6.74 0.61 6 -6 -3 7.45 0.63 6 -6 -3 7.21 0.60 -6 6 2 40.80 1.71 6 -6 -2 42.57 1.66 6 -6 -1 0.72 0.30 -6 6 1 0.94 0.35 -6 6 1 1.24 0.38 -6 6 0 49.74 2.07 -6 6 0 52.93 2.11 -6 6 0 51.14 2.06 6 -6 0 46.53 1.92 -6 6 -1 57.88 2.28 -6 6 -1 59.37 2.31 6 -6 1 58.94 2.17 -6 6 -2 0.83 0.36 -6 6 -2 0.31 0.29 6 -6 2 0.51 0.27 -6 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3.19 0.62 6 1 -4 3.71 0.68 6 1 -4 3.21 0.68 6 1 -4 2.85 0.50 6 1 -3 44.81 1.85 6 1 -3 42.81 2.20 6 1 -3 44.31 2.08 6 1 -3 41.73 2.06 6 1 -2 93.31 2.23 6 1 -2 92.46 2.94 6 1 -2 94.00 2.92 6 1 -2 93.95 2.91 6 1 -1 1.28 0.46 6 1 -1 0.33 0.46 6 1 -1 0.73 0.44 6 1 0 203.71 5.83 6 1 0 197.59 5.90 6 1 0 200.06 6.17 6 1 0 195.62 5.55 6 1 0 206.93 5.76 6 1 0 201.66 6.14 6 1 1 284.71 7.59 6 1 1 283.68 7.71 6 1 1 276.98 7.27 6 1 1 286.31 7.49 6 1 1 286.86 8.06 6 1 1 290.34 8.10 6 1 2 140.62 4.88 6 1 2 147.00 4.48 6 1 2 147.81 5.00 6 1 2 144.16 4.57 6 1 2 148.12 4.38 6 1 3 10.73 1.10 6 1 3 11.56 1.03 6 1 3 11.80 0.90 6 1 3 12.37 1.19 6 1 3 11.96 1.19 6 1 4 94.28 3.73 6 1 4 103.15 3.90 6 1 4 95.82 3.45 6 1 4 99.48 3.52 6 1 5 1.75 0.47 6 1 5 1.06 0.50 6 1 5 1.85 0.62 6 1 6 183.28 5.42 6 1 6 183.87 5.82 6 1 6 167.17 5.45 6 1 6 169.12 5.44 6 1 7 0.44 0.42 6 1 7 1.52 0.58 6 1 7 0.91 0.42 6 1 7 0.30 0.37 6 1 8 33.57 2.09 6 1 8 32.90 1.88 6 1 9 70.62 2.91 6 1 10 0.74 0.46 -6 -1 -11 34.15 1.77 6 1 11 36.15 1.83 6 1 11 39.72 1.98 6 1 12 17.28 1.14 6 1 12 16.49 1.13 -6 -1 -13 13.26 0.86 6 1 13 15.11 0.92 6 2 -9 58.91 2.01 6 2 -8 1.10 0.87 6 2 -7 180.59 4.91 6 2 -7 176.23 4.79 6 2 -7 182.72 4.94 6 2 -6 112.53 3.91 6 2 -6 119.63 3.64 6 2 -5 260.19 7.33 6 2 -5 266.25 6.91 6 2 -5 273.79 7.00 6 2 -4 153.93 4.93 6 2 -4 148.22 4.99 6 2 -4 153.17 4.50 6 2 -4 156.37 4.49 6 2 -3 14.50 1.33 6 2 -3 13.76 1.20 6 2 -3 12.28 1.08 6 2 -3 13.63 1.31 6 2 -3 12.67 1.01 6 2 -2 170.41 3.05 6 2 -2 159.53 3.77 6 2 -2 160.92 3.21 6 2 -2 155.18 3.84 6 2 -2 161.50 3.90 6 2 -1 1061.47 23.99 6 2 -1 1053.55 24.46 6 2 -1 1035.67 24.44 6 2 -1 1021.58 24.47 6 2 -1 1059.27 24.24 6 2 -1 1028.16 24.30 6 2 0 72.77 3.08 6 2 0 80.76 2.93 6 2 0 80.79 3.02 6 2 0 82.87 3.16 6 2 0 80.35 3.28 6 2 0 76.22 3.23 6 2 0 75.50 3.27 6 2 1 8.06 0.91 6 2 1 6.43 0.91 6 2 1 6.30 0.73 6 2 1 6.57 0.91 6 2 1 5.98 0.93 6 2 1 8.06 0.98 6 2 1 5.91 0.75 6 2 1 7.05 1.02 6 2 2 3.48 0.53 6 2 2 4.08 0.76 6 2 2 4.47 0.80 6 2 2 4.88 0.81 6 2 2 4.29 0.72 6 2 2 3.17 0.96 6 2 2 4.02 0.60 6 2 3 24.02 1.40 6 2 3 24.85 1.33 6 2 3 25.99 1.71 6 2 3 21.05 1.57 6 2 3 23.25 1.64 6 2 3 27.19 1.83 6 2 3 22.81 1.81 6 2 3 24.26 1.57 6 2 4 36.02 2.02 6 2 4 32.40 1.85 6 2 4 29.89 2.22 6 2 4 32.68 1.96 6 2 4 33.20 1.95 6 2 5 6.02 0.82 6 2 5 6.14 0.83 6 2 5 5.08 0.87 6 2 5 4.83 0.79 6 2 5 3.41 0.69 6 2 6 169.30 4.96 6 2 6 178.19 5.32 6 2 6 157.77 5.25 6 2 6 158.21 5.27 6 2 6 164.70 5.55 6 2 7 778.03 17.89 6 2 7 796.38 18.37 6 2 7 726.52 18.19 6 2 7 757.92 18.27 6 2 7 755.37 18.69 6 2 8 86.24 3.34 6 2 8 82.32 3.51 6 2 9 519.94 12.80 6 2 9 497.62 12.18 6 2 10 69.76 2.97 -6 -2 -11 17.04 1.15 6 2 11 17.19 1.26 6 2 11 19.13 1.31 6 2 12 47.25 2.02 -6 -2 -12 45.19 1.86 6 2 13 7.66 0.67 -6 -2 -13 6.96 0.59 6 3 -9 10.78 0.94 6 3 -8 13.48 1.21 6 3 -8 14.20 1.04 6 3 -7 53.86 2.25 6 3 -7 53.17 2.01 6 3 -6 54.11 2.30 6 3 -6 55.13 2.15 6 3 -5 108.30 3.51 6 3 -5 101.48 3.39 6 3 -4 36.36 2.15 6 3 -4 36.16 2.08 6 3 -4 35.45 1.86 6 3 -4 36.15 1.77 6 3 -3 50.76 2.21 6 3 -3 51.57 2.24 6 3 -3 50.87 2.60 6 3 -3 55.01 2.65 6 3 -3 51.90 2.23 6 3 -2 417.52 10.25 6 3 -2 416.82 10.89 6 3 -2 425.45 11.12 6 3 -2 415.19 10.87 6 3 -2 421.03 10.84 6 3 -2 426.63 11.19 6 3 -2 427.23 10.18 6 3 -2 385.19 10.77 6 3 -1 50.36 2.34 6 3 -1 50.36 2.62 6 3 -1 48.59 2.57 6 3 -1 51.33 2.17 6 3 -1 54.94 2.62 6 3 -1 55.70 2.72 6 3 -1 51.61 2.56 6 3 -1 51.02 2.52 6 3 0 1456.27 29.35 6 3 0 1472.96 29.37 6 3 0 1493.66 29.60 6 3 0 1500.76 29.71 6 3 0 1480.16 29.05 6 3 0 1442.19 28.64 6 3 0 1485.50 29.42 6 3 1 39.10 2.17 6 3 1 37.48 2.17 6 3 1 36.32 2.18 6 3 1 38.10 1.91 6 3 1 37.33 2.24 6 3 1 39.27 2.37 6 3 1 37.07 1.80 6 3 1 40.39 2.19 6 3 1 38.28 2.16 6 3 2 14.23 1.08 6 3 2 12.80 1.85 6 3 2 14.55 1.37 6 3 2 13.73 1.02 6 3 2 10.86 1.17 6 3 2 12.96 1.27 6 3 2 13.23 1.25 6 3 2 13.46 1.30 6 3 3 49.52 2.18 6 3 3 53.04 2.53 6 3 3 56.74 2.67 6 3 3 50.50 2.64 6 3 3 51.47 2.59 6 3 3 54.32 2.71 6 3 3 56.05 2.59 6 3 3 56.51 3.02 6 3 4 9.25 0.86 6 3 4 11.98 2.19 6 3 4 13.95 1.29 6 3 4 10.86 1.10 6 3 4 13.09 1.20 6 3 4 11.43 1.15 6 3 4 11.58 1.25 6 3 4 13.15 1.24 6 3 5 4.13 0.58 6 3 5 5.62 0.79 6 3 5 5.96 0.75 6 3 5 4.91 0.84 6 3 5 4.46 0.78 6 3 5 5.47 0.88 6 3 5 5.81 0.83 6 3 5 6.47 0.88 6 3 6 72.06 2.99 6 3 6 79.59 2.96 6 3 6 74.07 3.17 6 3 6 80.09 3.43 6 3 6 79.13 3.25 6 3 6 78.55 3.22 6 3 7 396.45 10.02 6 3 7 389.64 10.36 6 3 7 386.76 10.36 6 3 7 396.90 10.73 6 3 7 413.11 10.53 6 3 8 22.80 1.71 6 3 8 28.57 1.76 6 3 9 54.90 2.28 6 3 9 55.49 2.66 6 3 9 58.44 2.63 6 3 10 154.34 4.47 6 3 10 147.31 4.85 6 3 10 157.86 4.92 6 3 11 34.61 1.57 6 3 11 39.27 1.92 6 3 12 27.53 1.47 6 3 13 32.47 1.45 6 4 -8 165.36 4.33 6 4 -8 171.85 4.29 6 4 -7 0.03 0.99 6 4 -7 0.40 0.71 6 4 -6 46.94 1.90 6 4 -6 44.69 1.86 6 4 -6 41.89 2.05 6 4 -5 82.18 2.80 6 4 -5 84.43 2.88 6 4 -5 80.52 3.50 6 4 -5 81.81 2.92 6 4 -4 10.01 1.40 6 4 -4 10.57 0.98 6 4 -3 244.01 7.27 6 4 -3 252.56 7.30 6 4 -3 246.31 6.54 6 4 -3 247.78 6.75 6 4 -3 242.46 6.57 6 4 -2 94.67 3.76 6 4 -2 97.33 3.39 6 4 -2 104.82 3.40 6 4 -2 102.69 4.01 6 4 -2 94.62 4.07 6 4 -2 100.31 3.39 6 4 -2 103.69 3.49 6 4 -1 16.54 1.44 6 4 -1 15.16 1.51 6 4 -1 15.27 2.25 6 4 -1 12.51 1.34 6 4 -1 14.25 1.33 6 4 -1 13.13 1.11 6 4 -1 14.16 1.19 6 4 -1 13.12 1.44 6 4 -1 14.59 1.42 6 4 0 353.76 6.24 6 4 0 363.49 6.35 6 4 0 360.93 6.03 6 4 0 358.38 6.43 6 4 0 350.99 6.02 6 4 0 375.45 5.47 6 4 1 485.66 7.20 6 4 1 -0.09 0.00 6 4 1 476.07 7.06 6 4 1 472.05 7.05 6 4 1 483.17 7.43 6 4 1 482.58 7.17 6 4 1 486.33 7.31 6 4 1 -0.09 0.00 6 4 1 492.50 6.08 6 4 2 97.11 3.14 6 4 2 100.17 3.29 6 4 2 96.83 3.34 6 4 2 99.13 3.28 6 4 2 102.71 3.35 6 4 2 110.23 3.91 6 4 2 101.28 3.35 6 4 2 97.11 2.63 6 4 3 199.43 6.25 6 4 3 200.20 6.16 6 4 3 201.54 6.30 6 4 3 195.10 6.36 6 4 3 202.81 6.29 6 4 3 198.31 6.27 6 4 3 209.22 6.59 6 4 3 193.82 5.58 6 4 4 128.38 4.56 6 4 4 127.73 4.44 6 4 4 125.82 4.58 6 4 4 121.62 4.53 6 4 4 129.41 4.74 6 4 4 126.75 4.55 6 4 4 134.22 4.58 6 4 4 129.60 3.97 6 4 5 35.35 1.99 6 4 5 36.04 2.10 6 4 5 35.54 2.07 6 4 5 36.12 2.13 6 4 5 35.83 2.20 6 4 5 37.89 1.93 6 4 6 30.16 1.79 6 4 6 31.99 1.95 6 4 6 32.22 2.03 6 4 6 32.50 1.76 6 4 7 106.59 4.11 6 4 7 106.03 3.76 6 4 7 111.89 4.04 6 4 8 50.33 2.20 6 4 8 49.42 2.44 6 4 9 30.69 1.84 6 4 9 32.52 1.66 6 4 10 240.91 6.43 6 4 10 244.64 6.88 6 4 11 156.32 4.41 6 4 11 163.35 4.83 6 4 12 62.32 2.06 6 4 12 63.86 2.38 6 4 13 5.74 0.56 6 5 -7 103.71 2.95 6 5 -6 2.97 0.78 6 5 -6 3.77 0.65 6 5 -5 20.00 1.23 6 5 -5 23.62 1.38 6 5 -5 22.26 1.44 6 5 -5 23.05 1.28 6 5 -4 1.71 0.50 6 5 -4 0.25 0.49 6 5 -4 0.67 0.96 6 5 -4 1.44 0.81 6 5 -3 372.70 9.31 6 5 -3 386.44 9.44 6 5 -2 514.87 12.36 6 5 -2 447.80 11.33 6 5 -2 493.24 12.44 6 5 -2 467.51 11.42 6 5 -2 474.06 11.67 6 5 -2 486.92 11.97 6 5 -1 333.35 9.13 6 5 -1 320.32 9.01 6 5 -1 323.76 9.23 6 5 -1 350.46 9.42 6 5 -1 321.51 9.19 6 5 -1 318.75 8.26 6 5 -1 326.85 8.45 6 5 -1 328.62 8.70 6 5 0 4.99 0.71 6 5 0 5.25 0.88 6 5 0 5.31 0.76 6 5 0 4.56 0.81 6 5 0 5.33 1.22 6 5 0 3.97 0.72 6 5 0 6.70 0.80 6 5 1 0.72 0.41 6 5 1 0.92 0.42 6 5 1 0.83 0.59 6 5 1 0.78 0.53 6 5 1 0.19 0.93 6 5 1 -0.09 0.00 6 5 1 -0.09 0.00 6 5 2 -0.09 0.00 6 5 2 1.53 0.60 6 5 2 0.19 0.44 6 5 2 0.94 0.97 6 5 2 -0.09 0.00 6 5 2 1.47 0.41 6 5 3 130.15 4.79 6 5 3 135.26 4.81 6 5 3 129.58 4.61 6 5 3 132.40 4.72 6 5 3 137.21 4.84 6 5 3 131.48 4.85 6 5 4 429.88 11.45 6 5 4 448.28 11.40 6 5 4 418.51 11.41 6 5 4 434.00 11.61 6 5 5 763.38 18.42 6 5 5 767.41 18.30 6 5 5 734.20 18.33 6 5 5 760.52 18.61 6 5 6 270.41 7.65 6 5 6 264.49 7.46 6 5 6 252.17 7.48 6 5 6 260.18 7.70 6 5 7 335.88 9.18 6 5 7 325.80 8.88 6 5 7 345.59 8.77 6 5 8 21.46 1.36 6 5 8 20.66 1.48 6 5 9 34.01 1.68 6 5 9 32.88 1.85 6 5 10 2.75 0.52 6 5 10 2.82 0.58 6 5 11 24.32 1.23 6 5 11 24.73 1.39 6 5 12 3.73 0.41 6 5 12 3.51 0.51 6 6 -6 6.11 0.86 6 6 -5 35.99 1.54 6 6 -5 33.60 1.56 6 6 -4 27.39 1.37 6 6 -4 27.68 1.41 6 6 -4 24.02 1.44 6 6 -3 5.57 0.75 6 6 -3 5.49 0.68 6 6 -3 4.64 1.11 6 6 -3 5.15 0.74 6 6 -2 259.64 6.95 6 6 -2 265.99 7.23 6 6 -2 267.08 7.37 6 6 -1 91.52 3.33 6 6 0 9.63 0.95 6 6 0 8.59 1.02 6 6 0 7.67 0.93 6 6 0 8.90 1.10 6 6 1 15.28 1.34 6 6 1 16.46 1.36 6 6 1 15.87 1.44 6 6 1 17.06 1.23 6 6 1 18.95 1.54 6 6 2 3.24 0.72 6 6 2 3.19 0.55 6 6 2 2.17 0.70 6 6 2 -0.09 0.00 6 6 2 -0.09 0.00 6 6 3 13.10 1.23 6 6 3 9.43 1.13 6 6 3 13.09 1.28 6 6 3 10.32 1.16 6 6 4 4.73 0.80 6 6 4 6.18 0.94 6 6 4 4.89 0.82 6 6 4 5.71 0.89 6 6 5 343.16 9.39 6 6 5 356.37 8.99 6 6 5 340.95 9.45 6 6 6 0.76 0.47 6 6 6 1.73 0.50 6 6 6 1.93 0.58 6 6 6 1.45 0.56 6 6 6 1.27 0.50 6 6 7 15.32 1.13 6 6 7 17.02 1.33 6 6 7 15.84 1.24 6 6 7 17.14 1.33 6 6 8 78.75 2.80 6 6 8 81.42 3.10 6 6 8 72.39 2.80 6 6 9 7.71 0.85 6 6 9 8.33 0.78 6 6 10 15.92 1.11 6 6 10 16.63 1.01 6 6 11 2.32 0.42 6 6 11 2.35 0.38 6 7 -4 422.22 9.96 6 7 -3 104.00 3.14 6 7 -3 100.91 3.30 6 7 -2 3.97 0.59 6 7 -2 4.35 0.65 6 7 -1 10.94 0.87 6 7 -1 9.89 0.90 6 7 -1 11.73 1.05 6 7 -1 11.12 1.03 6 7 -1 11.80 0.99 6 7 0 71.27 2.72 6 7 0 70.54 2.98 6 7 0 77.66 2.99 6 7 0 78.48 2.84 6 7 1 85.98 3.28 6 7 1 89.70 3.48 6 7 1 86.63 3.05 6 7 1 82.14 2.96 6 7 1 78.82 3.32 6 7 2 4.39 0.80 6 7 2 3.80 0.72 6 7 2 3.88 0.58 6 7 3 14.78 1.30 6 7 3 12.75 1.24 6 7 4 135.42 4.72 6 7 4 149.47 4.88 6 7 5 -0.07 0.38 6 7 5 -0.08 0.40 6 7 5 0.48 0.45 6 7 5 0.15 0.44 6 7 6 173.19 5.30 6 7 6 178.25 5.45 6 7 6 175.77 5.34 6 7 7 38.61 1.88 6 7 7 37.06 1.91 6 7 7 35.52 1.66 6 7 8 9.20 0.83 6 7 8 9.39 0.87 6 7 8 9.27 0.79 6 7 9 0.24 0.28 6 7 9 0.50 0.30 6 7 10 5.93 0.60 6 7 10 6.65 0.57 6 8 -2 88.48 2.79 6 8 -1 0.91 0.35 6 8 0 13.81 1.05 6 8 0 12.15 0.96 6 8 0 11.18 0.86 6 8 0 11.80 0.91 6 8 1 0.09 0.29 6 8 1 0.06 0.32 6 8 1 -0.26 0.35 6 8 2 7.84 0.88 6 8 2 8.32 0.86 6 8 2 7.87 0.88 6 8 3 2.61 0.56 6 8 3 1.74 0.51 6 8 3 3.55 0.65 6 8 3 2.73 0.61 6 8 4 271.04 7.18 6 8 4 257.84 7.13 6 8 4 258.65 7.18 6 8 4 263.04 7.26 6 8 5 40.42 1.93 6 8 5 39.04 1.89 6 8 5 40.81 1.96 6 8 6 34.16 1.69 6 8 6 32.98 1.65 6 8 6 33.86 1.65 6 8 7 0.77 0.33 6 8 7 0.86 0.33 6 8 8 1.61 0.36 6 8 8 1.48 0.34 6 9 1 2.25 0.42 6 9 2 3.64 0.50 6 9 2 3.60 0.54 6 9 3 32.35 1.52 6 9 3 29.97 1.43 6 9 4 311.78 7.84 6 9 4 314.67 7.79 6 9 5 6.03 0.60 6 9 5 6.41 0.63 6 9 6 63.47 2.15 6 9 7 75.56 2.29 7 -6 0 44.04 1.46 7 -6 1 19.21 0.88 7 -6 2 1.50 0.26 7 -5 -3 2.73 0.33 7 -5 -2 6.19 0.53 7 -5 -1 0.85 0.29 7 -5 0 15.89 0.89 -7 5 0 5.61 0.54 7 -5 1 0.31 0.25 -7 5 -1 0.15 0.23 -7 5 -1 -0.03 0.20 7 -5 2 79.65 2.51 -7 5 -2 75.32 2.45 7 -5 3 14.92 0.88 -7 5 -3 17.82 0.97 7 -5 4 45.09 1.62 -7 5 -4 45.91 1.71 -7 5 -5 36.68 1.45 -7 5 -6 2.56 0.35 7 -4 -5 51.50 1.75 7 -4 -4 -0.07 0.24 7 -4 -4 -0.09 0.19 7 -4 -3 0.21 0.27 7 -4 -3 0.04 0.23 7 -4 -2 14.96 0.96 7 -4 -2 13.49 0.91 7 -4 -1 18.76 1.28 7 -4 -1 18.28 1.12 7 -4 -1 19.89 1.12 7 -4 0 0.40 0.32 7 -4 0 0.88 0.40 7 -4 0 0.63 0.32 7 -4 1 215.75 6.09 7 -4 1 211.24 5.64 7 -4 1 197.23 5.44 7 -4 2 101.51 3.60 7 -4 2 97.31 3.18 7 -4 3 268.49 6.73 -7 4 -3 206.17 5.89 7 -4 4 119.90 3.96 7 -4 4 121.09 3.54 -7 4 -4 119.53 3.62 -7 4 -5 0.98 0.33 7 -4 6 28.85 1.20 -7 4 -6 30.60 1.40 7 -4 7 75.12 2.26 -7 4 -7 84.88 2.55 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0.56 7 -2 -2 2.30 0.51 7 -2 -1 2.71 0.49 7 -2 -1 2.00 0.50 7 -2 -1 1.68 0.55 7 -2 0 15.88 1.13 7 -2 0 16.54 1.08 7 -2 0 15.75 1.31 7 -2 1 39.49 1.90 7 -2 1 35.88 1.74 7 -2 1 43.75 2.29 7 -2 1 41.14 1.96 7 -2 2 76.65 2.85 7 -2 2 75.10 3.25 7 -2 2 75.44 2.81 7 -2 3 2.40 0.51 7 -2 3 1.92 0.58 7 -2 3 2.49 0.51 7 -2 4 41.17 2.25 7 -2 4 44.22 2.23 7 -2 5 215.51 6.42 7 -2 5 217.47 6.46 -7 2 -6 22.34 1.27 7 -2 6 26.34 1.59 -7 2 -6 21.00 1.27 7 -2 6 26.77 1.70 -7 2 -7 7.90 0.75 -7 2 -7 9.89 0.82 7 -2 7 9.35 0.98 -7 2 -8 34.69 1.58 -7 2 -8 35.21 1.56 7 -2 8 35.89 1.89 -7 2 -9 43.10 1.71 7 -2 9 46.72 2.07 7 -2 10 2.09 0.46 -7 2 -10 1.95 0.33 -7 2 -11 6.45 0.47 7 -1 -7 13.81 0.85 7 -1 -6 50.34 1.96 7 -1 -5 1.19 0.37 7 -1 -5 1.41 0.43 7 -1 -4 0.79 0.34 7 -1 -4 0.43 0.40 7 -1 -3 69.85 2.67 7 -1 -3 71.48 2.82 7 -1 -2 2.17 0.55 7 -1 -2 2.04 0.47 7 -1 -2 1.56 0.48 7 -1 -1 72.27 2.67 7 -1 -1 79.20 2.33 7 -1 0 2.31 0.54 7 -1 0 1.19 0.39 7 -1 0 1.67 0.60 7 -1 0 1.51 0.48 7 -1 1 111.10 4.09 7 -1 1 102.35 3.59 7 -1 1 108.52 3.63 7 -1 1 99.21 3.35 7 -1 1 105.45 3.63 7 -1 2 249.65 6.86 7 -1 2 251.87 6.81 7 -1 2 246.14 7.40 7 -1 3 96.93 3.37 7 -1 3 93.19 3.24 7 -1 3 99.34 3.86 7 -1 4 41.02 1.95 7 -1 4 39.75 2.22 7 -1 4 39.42 1.81 7 -1 5 27.46 1.76 7 -1 5 26.92 1.80 7 -1 6 60.15 2.66 7 -1 6 59.56 2.68 7 -1 6 61.41 2.84 7 -1 7 206.61 6.15 7 -1 7 201.54 5.74 7 -1 8 20.75 1.49 -7 1 -8 17.68 1.09 -7 1 -8 18.55 1.11 7 -1 9 0.49 0.42 -7 1 -9 0.51 0.28 -7 1 -10 24.86 1.18 7 -1 10 25.83 1.46 -7 1 -11 11.86 0.69 -7 1 -11 10.26 0.71 7 -1 11 12.57 0.90 7 0 -7 0.90 0.52 7 0 -6 38.03 1.46 7 0 -6 37.56 1.68 7 0 -5 2.68 0.47 7 0 -5 2.92 0.58 7 0 -4 1.17 0.43 7 0 -4 0.90 0.46 7 0 -3 0.69 0.44 7 0 -2 24.55 1.53 7 0 -2 27.57 1.61 7 0 -1 25.87 1.60 7 0 -1 25.97 1.65 7 0 -1 26.63 1.55 7 0 0 34.30 1.88 7 0 0 32.86 2.02 7 0 0 31.66 1.73 7 0 0 32.79 1.64 7 0 0 31.24 1.97 7 0 0 32.66 1.81 7 0 1 14.15 1.10 7 0 1 9.78 0.99 7 0 1 13.04 1.15 7 0 1 13.63 1.31 7 0 2 114.73 4.27 7 0 2 113.24 3.73 7 0 2 113.57 3.87 7 0 2 108.59 4.10 7 0 2 116.32 3.89 7 0 3 30.79 1.98 7 0 3 33.14 1.75 7 0 3 33.27 2.06 7 0 3 31.04 1.61 7 0 4 248.21 7.50 7 0 4 264.32 7.66 7 0 4 256.08 7.00 7 0 5 29.59 1.88 7 0 6 152.61 5.00 7 0 6 155.13 5.01 7 0 7 10.57 1.03 7 0 7 9.07 0.95 7 0 7 10.04 1.12 7 0 8 107.92 3.99 7 0 9 80.36 3.17 -7 0 -10 0.15 0.21 7 0 10 0.26 0.37 -7 0 -11 0.76 0.25 7 0 11 1.01 0.34 -7 0 -11 1.36 0.33 7 1 -7 16.99 1.06 7 1 -6 7.20 0.83 7 1 -6 7.17 0.96 7 1 -5 3.97 0.69 7 1 -5 5.12 0.87 7 1 -4 61.73 2.20 7 1 -4 62.69 2.61 7 1 -3 114.49 4.05 7 1 -3 105.23 3.78 7 1 -2 8.38 0.94 7 1 -2 7.31 0.88 7 1 -1 45.15 2.14 7 1 -1 48.86 2.10 7 1 0 203.49 5.89 7 1 0 200.84 6.31 7 1 0 207.92 6.04 7 1 0 209.91 6.14 7 1 1 131.67 4.12 7 1 1 122.73 4.48 7 1 1 134.06 4.29 7 1 1 129.08 4.31 7 1 2 0.48 0.30 7 1 2 0.45 0.54 7 1 2 0.18 0.44 7 1 2 -0.07 0.00 7 1 2 -0.14 0.98 7 1 3 21.95 1.22 7 1 3 20.61 1.54 7 1 3 22.05 1.63 7 1 3 23.58 1.79 7 1 4 591.80 7.85 7 1 4 621.66 8.32 7 1 5 161.75 4.28 7 1 5 154.09 3.92 7 1 6 198.56 6.08 7 1 7 97.22 3.60 7 1 7 100.86 3.92 7 1 7 97.21 3.59 7 1 8 0.26 0.45 7 1 8 0.06 0.33 7 1 9 67.91 2.91 7 1 9 66.85 2.60 7 1 10 1.60 0.51 7 1 10 3.37 0.53 7 1 11 0.26 0.26 7 2 -7 1.04 0.77 7 2 -6 2.29 0.90 7 2 -5 2.31 0.87 7 2 -5 4.00 1.23 7 2 -4 65.39 2.38 7 2 -4 66.37 2.80 7 2 -3 70.61 2.99 7 2 -3 73.92 3.04 7 2 -2 36.62 2.00 7 2 -2 38.61 2.05 7 2 -1 25.74 1.53 7 2 -1 27.35 1.87 7 2 -1 24.66 1.85 7 2 -1 25.17 1.71 7 2 0 46.55 2.17 7 2 0 48.64 2.51 7 2 0 48.95 2.52 7 2 0 49.48 2.64 7 2 0 51.72 2.64 7 2 1 132.28 3.07 7 2 1 132.03 3.77 7 2 1 137.66 3.86 7 2 1 134.15 3.64 7 2 2 2.36 0.49 7 2 2 2.59 0.67 7 2 2 2.58 0.65 7 2 2 4.07 1.62 7 2 3 89.75 3.68 7 2 3 89.49 3.76 7 2 3 90.25 3.28 7 2 3 89.97 3.50 7 2 3 97.71 3.85 7 2 4 80.16 3.48 7 2 4 76.35 3.31 7 2 4 74.79 2.88 7 2 4 79.85 3.51 7 2 5 23.29 1.69 7 2 5 24.01 1.77 7 2 5 22.84 1.65 7 2 5 23.61 1.42 7 2 5 25.11 1.75 7 2 5 20.68 1.48 7 2 6 81.00 3.29 7 2 6 81.32 2.93 7 2 6 82.86 3.24 7 2 7 0.65 0.49 7 2 7 1.34 0.54 7 2 7 1.04 0.45 7 2 7 0.94 0.37 7 2 8 153.33 4.84 7 2 8 154.55 5.17 7 2 9 11.01 0.98 7 2 9 8.97 1.02 7 2 10 44.67 1.99 7 2 10 44.80 2.10 7 2 11 9.99 0.81 7 2 11 9.24 0.81 7 2 12 52.60 1.89 7 3 -7 0.32 0.64 7 3 -6 7.20 0.95 7 3 -5 -0.93 1.55 7 3 -5 -0.33 0.98 7 3 -4 -1.23 1.67 7 3 -4 -0.58 1.07 7 3 -3 3.05 0.84 7 3 -3 2.65 1.69 7 3 -3 3.05 1.02 7 3 -2 14.79 1.38 7 3 -1 593.39 14.85 7 3 -1 597.90 14.80 7 3 0 8.72 1.07 7 3 0 9.89 1.06 7 3 0 9.83 2.02 7 3 0 12.13 1.30 7 3 1 96.18 3.83 7 3 1 98.47 3.75 7 3 1 96.07 3.92 7 3 1 99.90 4.10 7 3 2 20.83 1.65 7 3 2 21.32 1.63 7 3 2 19.75 1.52 7 3 2 21.75 1.38 7 3 2 17.54 2.47 7 3 2 18.45 1.56 7 3 3 467.08 12.42 7 3 3 456.83 12.21 7 3 3 465.51 12.10 7 3 3 463.46 12.26 7 3 3 502.24 12.26 7 3 3 462.70 11.65 7 3 4 99.75 3.86 7 3 4 99.15 4.00 7 3 4 97.52 3.83 7 3 4 94.49 3.80 7 3 4 97.19 3.38 7 3 5 86.81 3.53 7 3 5 89.29 3.44 7 3 5 87.26 3.47 7 3 5 84.10 3.03 7 3 6 63.57 2.87 7 3 6 62.20 2.83 7 3 6 63.14 2.43 7 3 7 14.47 1.35 7 3 8 204.49 6.20 7 3 8 215.31 6.08 7 3 8 195.30 5.40 7 3 9 188.31 5.72 7 3 9 193.52 5.64 7 3 10 22.27 1.36 7 3 10 21.48 1.34 7 3 11 8.42 0.74 7 3 11 11.28 0.87 7 3 12 59.22 2.04 7 4 -5 14.33 1.01 7 4 -4 4.14 1.91 7 4 -4 0.03 0.77 7 4 -3 14.76 1.15 7 4 -3 15.64 2.35 7 4 -2 77.81 3.26 7 4 -2 81.07 3.79 7 4 -1 174.09 5.65 7 4 -1 177.32 5.90 7 4 0 27.24 1.85 7 4 1 306.50 9.17 7 4 1 327.21 9.23 7 4 2 578.90 14.90 7 4 2 601.19 14.95 7 4 2 605.39 14.93 7 4 2 582.19 14.81 7 4 3 0.18 0.64 7 4 3 0.64 0.49 7 4 3 0.62 0.48 7 4 4 388.10 10.59 7 4 4 412.01 10.72 7 4 4 428.79 10.79 7 4 4 381.12 9.88 7 4 5 26.08 1.74 7 4 5 25.34 1.80 7 4 6 23.57 1.72 7 4 7 46.75 2.41 7 4 7 50.15 2.39 7 4 8 30.93 1.84 7 4 8 35.03 1.87 7 4 9 2.78 0.58 7 4 9 2.12 0.53 7 4 10 7.63 0.75 7 4 10 7.11 0.75 7 4 11 79.62 2.67 7 4 12 137.35 3.73 7 5 0 21.45 1.52 7 5 1 85.44 3.48 7 5 1 88.41 3.67 7 5 2 7.33 0.94 7 5 2 7.49 0.99 7 5 2 7.29 1.35 7 5 3 8.37 1.07 7 5 3 10.20 1.41 7 5 4 32.45 1.96 7 5 4 31.42 1.99 7 5 5 14.10 1.18 7 5 5 13.50 1.29 7 5 5 12.99 1.21 7 5 6 50.59 2.34 7 5 6 53.33 2.55 7 5 7 44.82 2.11 7 5 7 46.35 2.25 7 5 8 14.54 1.15 7 5 8 16.67 1.23 7 5 9 17.53 1.15 7 5 9 21.04 1.29 7 5 10 0.29 0.33 7 6 1 219.95 6.61 7 6 1 244.96 6.75 7 6 2 0.08 0.43 7 6 2 0.15 0.39 7 6 3 245.65 7.20 7 6 3 258.16 7.16 7 6 4 3.82 0.70 7 6 4 2.65 0.60 7 6 4 2.95 0.65 7 6 5 6.11 0.87 7 6 5 5.76 0.77 7 6 5 5.42 0.76 7 6 6 0.64 0.41 7 6 6 0.43 0.40 7 6 6 0.74 0.38 7 6 7 14.73 1.11 7 6 7 16.23 1.11 7 6 7 15.27 1.18 7 6 8 0.23 0.31 7 6 9 41.38 1.80 7 6 10 90.12 2.80 7 7 1 83.49 2.98 7 7 2 0.12 0.32 7 7 2 0.06 0.34 7 7 3 176.16 5.41 7 7 3 195.95 5.47 7 7 4 7.49 0.83 7 7 4 6.05 0.72 7 7 5 1.54 0.46 7 7 5 1.90 0.47 7 7 6 11.77 0.96 7 7 6 11.77 0.91 7 7 7 1.02 0.36 7 7 7 0.86 0.32 7 7 8 0.34 0.26 7 8 2 10.00 0.77 7 8 3 0.50 0.34 7 8 4 36.57 1.59 7 8 5 12.35 0.82 7 8 5 13.97 0.91 7 8 6 17.65 0.94 7 8 6 18.18 1.00 8 -4 0 3.01 0.33 8 -4 1 48.08 1.57 8 -4 2 2.58 0.32 8 -3 -2 3.08 0.35 8 -3 -1 21.60 1.02 8 -3 0 34.18 1.55 8 -3 0 37.04 1.61 8 -3 0 36.11 1.43 8 -3 1 46.33 1.91 8 -3 1 44.78 1.68 8 -3 2 0.55 0.32 8 -3 2 0.80 0.27 8 -3 3 14.37 1.00 8 -3 4 83.03 2.76 8 -3 5 167.92 4.45 8 -3 5 157.74 4.07 8 -2 -3 61.38 1.93 8 -2 -3 58.11 2.00 8 -2 -2 9.50 0.68 8 -2 -2 7.31 0.72 8 -2 -1 8.25 0.67 8 -2 -1 7.14 0.73 8 -2 0 5.92 0.59 8 -2 0 4.84 0.73 8 -2 0 4.96 0.64 8 -2 0 6.07 0.68 8 -2 1 0.38 0.28 8 -2 1 0.35 0.34 8 -2 2 0.04 0.22 8 -2 2 0.12 0.29 8 -2 2 0.24 0.36 8 -2 3 23.34 1.40 8 -2 3 24.63 1.44 8 -2 3 20.32 1.08 8 -2 3 21.99 1.16 8 -2 4 0.46 0.35 8 -2 4 0.12 0.25 8 -2 5 1.23 0.40 8 -2 5 0.97 0.37 8 -2 5 0.38 0.27 8 -2 6 11.14 0.84 8 -2 6 10.19 0.79 8 -2 6 10.44 0.73 8 -2 7 1.79 0.32 8 -2 8 4.44 0.40 8 -1 -4 1.28 0.58 8 -1 -3 5.79 0.57 8 -1 -3 6.83 0.78 8 -1 -2 22.64 1.18 8 -1 -2 22.72 1.35 8 -1 -2 24.23 1.32 8 -1 -1 91.19 2.90 8 -1 -1 88.24 3.07 8 -1 -1 88.44 3.05 8 -1 -1 88.72 2.95 8 -1 0 7.69 0.72 8 -1 0 9.41 0.89 8 -1 0 8.48 0.86 8 -1 0 7.97 0.93 8 -1 1 20.32 1.15 8 -1 1 16.17 1.24 8 -1 1 17.13 1.26 8 -1 1 18.02 1.31 8 -1 2 1.09 0.47 8 -1 2 0.34 0.36 8 -1 2 0.90 0.31 8 -1 2 1.16 0.37 8 -1 3 137.52 4.44 8 -1 3 142.27 4.48 8 -1 3 136.41 3.93 8 -1 3 139.02 4.12 8 -1 4 0.06 0.42 8 -1 4 0.58 0.40 8 -1 4 0.10 0.27 8 -1 5 26.91 1.55 8 -1 5 28.51 1.58 8 -1 5 30.53 1.62 8 -1 5 29.76 1.43 8 -1 6 14.62 1.08 8 -1 6 15.43 1.07 8 -1 6 14.46 1.03 8 -1 6 12.94 0.89 8 -1 7 4.09 0.60 8 -1 7 3.86 0.52 8 -1 7 4.18 0.49 8 -1 8 9.63 0.81 8 -1 8 9.45 0.65 8 -1 9 15.21 0.94 8 -1 9 16.01 0.79 8 0 -4 1.23 0.79 8 0 -3 4.38 0.90 8 0 -2 4.54 0.57 8 0 -2 4.75 0.90 8 0 -2 4.07 0.63 8 0 -1 49.30 2.00 8 0 -1 51.63 2.20 8 0 -1 51.91 2.21 8 0 -1 55.31 2.42 8 0 -1 50.16 2.20 8 0 0 0.29 0.32 8 0 0 0.20 0.42 8 0 0 0.27 0.34 8 0 0 -0.42 0.85 8 0 1 31.04 1.50 8 0 1 31.33 1.78 8 0 1 28.79 1.72 8 0 1 28.99 1.76 8 0 2 18.34 1.34 8 0 2 15.64 1.26 8 0 2 16.63 1.05 8 0 2 18.70 1.61 8 0 2 16.83 1.15 8 0 3 4.11 0.72 8 0 3 3.67 0.70 8 0 3 4.80 0.63 8 0 4 25.51 1.58 8 0 4 24.62 1.54 8 0 4 22.33 1.49 8 0 4 24.61 1.36 8 0 5 8.02 0.90 8 0 5 7.98 0.90 8 0 5 7.56 0.85 8 0 5 8.75 0.79 8 0 6 14.00 1.09 8 0 6 16.39 1.23 8 0 6 15.76 1.14 8 0 6 15.27 1.10 8 0 6 15.33 1.00 8 0 7 84.65 2.89 8 0 7 90.85 3.21 8 0 7 87.99 2.92 8 0 7 85.41 2.78 8 0 8 19.78 1.27 8 0 8 22.67 1.10 8 0 9 2.48 0.47 8 0 9 2.11 0.33 8 0 10 6.15 0.46 8 1 -4 45.98 2.03 8 1 -3 89.75 3.08 8 1 -2 21.42 1.62 8 1 -2 20.36 1.33 8 1 -1 0.60 0.39 8 1 -1 -0.06 0.38 8 1 -1 0.66 1.18 8 1 -1 -0.28 0.42 8 1 0 14.70 1.03 8 1 0 15.50 1.20 8 1 0 16.81 1.24 8 1 0 16.81 1.34 8 1 0 14.20 1.62 8 1 1 26.14 1.38 8 1 1 23.83 1.58 8 1 1 24.63 1.60 8 1 1 25.51 2.01 8 1 2 18.66 1.12 8 1 2 20.71 1.53 8 1 2 17.27 1.94 8 1 2 16.82 1.35 8 1 2 21.71 1.51 8 1 3 4.12 0.77 8 1 3 3.20 1.70 8 1 3 3.51 0.69 8 1 3 4.37 0.70 8 1 3 3.59 0.69 8 1 3 4.26 0.61 8 1 4 0.08 0.40 8 1 4 0.44 0.45 8 1 4 0.08 0.42 8 1 4 0.07 0.41 8 1 4 0.22 0.30 8 1 5 2.57 0.59 8 1 5 3.55 0.63 8 1 5 3.09 0.63 8 1 5 2.79 0.62 8 1 5 2.68 0.47 8 1 6 5.02 0.69 8 1 6 5.62 0.79 8 1 6 5.73 0.73 8 1 6 6.58 0.78 8 1 6 6.07 0.66 8 1 7 53.54 2.20 8 1 7 53.08 2.18 8 1 7 57.27 2.46 8 1 7 56.24 2.07 8 1 8 31.73 1.66 8 1 8 28.23 1.32 8 1 9 16.26 1.07 8 1 9 13.92 0.81 8 1 10 1.74 0.27 8 2 -4 161.08 4.57 8 2 -3 2.86 1.51 8 2 -2 82.29 3.00 8 2 -2 81.72 3.17 8 2 -1 0.39 1.61 8 2 -1 0.34 0.53 8 2 -1 0.53 0.42 8 2 0 137.85 4.60 8 2 0 143.37 4.64 8 2 0 142.78 4.49 8 2 0 136.30 4.46 8 2 1 79.39 3.12 8 2 1 72.97 3.35 8 2 1 71.56 2.95 8 2 1 71.83 2.95 8 2 2 22.75 1.62 8 2 2 25.48 2.44 8 2 2 26.29 1.64 8 2 2 24.62 1.61 8 2 2 25.64 1.60 8 2 3 37.66 2.07 8 2 3 42.08 2.69 8 2 3 36.14 2.02 8 2 3 38.75 2.07 8 2 3 38.83 2.06 8 2 3 35.20 1.75 8 2 4 3.37 0.64 8 2 4 2.99 0.64 8 2 4 2.90 0.64 8 2 4 3.93 0.71 8 2 4 2.28 0.46 8 2 5 32.37 1.79 8 2 5 32.98 1.84 8 2 5 34.74 1.88 8 2 5 33.37 1.92 8 2 5 32.28 1.60 8 2 6 49.43 2.15 8 2 6 47.32 2.19 8 2 6 53.84 2.43 8 2 6 51.84 2.26 8 2 6 49.36 1.99 8 2 7 195.29 5.73 8 2 7 191.43 5.15 8 2 8 44.24 2.05 8 2 8 43.86 1.67 8 2 9 0.10 0.25 8 3 -3 12.14 1.82 8 3 -2 2.87 1.95 8 3 -2 2.28 0.79 8 3 -1 117.62 3.97 8 3 -1 124.99 4.36 8 3 0 72.42 2.97 8 3 0 76.51 3.62 8 3 1 5.44 2.15 8 3 1 5.45 0.89 8 3 1 5.56 0.76 8 3 2 39.01 2.09 8 3 2 35.85 1.99 8 3 2 39.17 2.04 8 3 3 24.18 1.63 8 3 3 23.81 1.57 8 3 3 21.15 1.50 8 3 4 46.35 2.29 8 3 4 49.42 2.33 8 3 4 53.28 2.47 8 3 5 3.43 0.73 8 3 5 4.73 0.74 8 3 5 3.54 0.51 8 3 6 70.27 2.83 8 3 6 62.36 2.27 8 3 7 0.67 0.40 8 3 8 27.56 1.53 8 3 9 0.24 0.30 8 4 0 6.74 1.11 8 4 1 170.57 5.23 8 4 2 99.73 3.65 8 4 2 106.97 3.75 8 4 3 0.08 0.43 8 4 3 -0.55 0.73 8 4 3 0.31 0.37 8 4 4 8.48 0.96 8 4 4 8.92 1.10 8 4 4 7.76 0.82 8 4 5 11.33 1.06 8 4 5 10.77 0.95 8 4 6 -0.07 0.40 8 4 6 0.23 0.30 8 4 7 17.84 1.22 8 4 7 17.67 1.16 8 4 8 8.89 0.83 8 4 8 10.65 0.84 8 4 9 44.67 1.74 8 5 2 2.74 0.50 8 5 3 0.35 0.33 8 5 4 0.26 0.38 8 5 4 0.12 0.29 8 5 5 86.03 3.11 8 5 5 83.96 2.99 8 5 6 17.09 1.17 8 5 6 14.94 1.07 8 5 7 0.51 0.36 8 5 7 0.48 0.31 8 5 8 2.09 0.40 8 5 9 1.96 0.34 8 6 3 27.50 1.37 8 6 4 20.34 1.19 8 6 5 2.28 0.44 8 6 6 42.25 1.74 8 6 7 -0.08 0.25 9 0 1 13.01 0.85 9 0 2 33.64 1.48 9 0 3 5.56 0.57 9 0 3 5.76 0.59 9 0 4 44.68 1.66 9 1 0 6.49 0.62 9 1 1 1.07 0.41 9 1 2 5.18 0.63 9 1 3 1.13 0.40 9 1 4 7.27 0.69 9 2 0 0.43 0.43 9 2 1 0.32 0.45 9 2 2 32.49 1.50 9 2 3 76.77 2.57 9 2 4 2.95 0.54 0 0 0 0.00 0.00 TITL 240370lt_auto in P-1 REM P-1 (#2 in standard setting) CELL 1.54184 7.477592 9.182590 12.911458 83.8466 78.5954 81.7720 ZERR 4.00 0.000147 0.000197 0.000268 0.0017 0.0017 0.0017 LATT 1 SFAC C H N O UNIT 44.00 40.00 4.00 4.00 REM CrysAlisPro recorded range (K): Min=100.0; max=100.0; aver:100.0 TEMP -173 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 28228 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.482 _oxdiff_exptl_absorpt_empirical_full_min 0.683 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.44867(11) 0.47857(9) 0.62625(6) 0.0172(2) Uani 1 1 d . . . . . O16 O 0.15357(13) 0.11120(10) 0.71891(7) 0.0250(2) Uani 1 1 d . . . . . O18 O 0.34463(15) 0.23426(11) 0.77891(8) 0.0313(3) Uani 1 1 d . . . . . O19 O 0.67602(11) 0.52156(10) 0.70436(7) 0.0228(2) Uani 1 1 d . . . . . C2 C 0.51263(16) 0.52678(13) 0.70669(9) 0.0166(3) Uani 1 1 d . . . . . C3 C 0.35367(16) 0.58019(13) 0.78659(9) 0.0155(3) Uani 1 1 d . . . . . C4 C 0.34728(16) 0.63947(13) 0.88469(9) 0.0163(3) Uani 1 1 d . . . . . C5 C 0.50248(17) 0.66840(15) 0.92240(10) 0.0231(3) Uani 1 1 d . . . . . H5 H 0.621898 0.647462 0.881179 0.028 Uiso 1 1 calc R U . . . C6 C 0.48183(19) 0.72653(16) 1.01818(11) 0.0273(3) Uani 1 1 d . . . . . H6 H 0.587232 0.746697 1.042216 0.033 Uiso 1 1 calc R U . . . C7 C 0.30660(19) 0.75674(15) 1.08137(10) 0.0253(3) Uani 1 1 d . . . . . H7 H 0.294282 0.795647 1.148045 0.030 Uiso 1 1 calc R U . . . C8 C 0.15456(18) 0.73000(15) 1.04662(10) 0.0229(3) Uani 1 1 d . . . . . H8 H 0.036676 0.750498 1.089662 0.027 Uiso 1 1 calc R U . . . C9 C 0.16936(17) 0.67218(13) 0.94742(9) 0.0181(3) Uani 1 1 d . . . . . C10 C 0.01101(17) 0.64703(14) 0.90967(10) 0.0213(3) Uani 1 1 d . . . . . H10 H -0.106601 0.668161 0.952866 0.026 Uiso 1 1 calc R U . . . C11 C 0.02193(17) 0.59340(14) 0.81324(10) 0.0192(3) Uani 1 1 d . . . . . H11 H -0.085487 0.579562 0.788516 0.023 Uiso 1 1 calc R U . . . C12 C 0.19796(16) 0.55971(13) 0.75239(9) 0.0156(3) Uani 1 1 d . . . . . C13 C 0.24818(16) 0.49949(13) 0.64524(9) 0.0163(3) Uani 1 1 d . . . . . C14 C 0.18101(17) 0.35083(13) 0.64119(10) 0.0191(3) Uani 1 1 d . . . . . H14A H 0.045039 0.365913 0.652083 0.023 Uiso 1 1 calc R U . . . H14B H 0.227084 0.317201 0.569301 0.023 Uiso 1 1 calc R U . . . C15 C 0.23840(17) 0.22964(14) 0.72109(9) 0.0193(3) Uani 1 1 d . . . . . C17 C 0.2012(2) -0.01456(15) 0.79067(11) 0.0295(3) Uani 1 1 d . . . . . H17A H 0.332207 -0.050539 0.770734 0.044 Uiso 1 1 calc R U . . . H17B H 0.127924 -0.093330 0.786456 0.044 Uiso 1 1 calc R U . . . H17C H 0.175808 0.015184 0.863334 0.044 Uiso 1 1 calc R U . . . C20 C 0.18456(16) 0.60825(14) 0.55655(9) 0.0181(3) Uani 1 1 d . . . . . H20A H 0.214801 0.558778 0.489692 0.022 Uiso 1 1 calc R U . . . H20B H 0.049121 0.631456 0.573971 0.022 Uiso 1 1 calc R U . . . C21 C 0.26855(17) 0.75245(14) 0.53789(10) 0.0208(3) Uani 1 1 d . . . . . H21A H 0.404054 0.730328 0.528309 0.025 Uiso 1 1 calc R U . . . H21B H 0.225529 0.809100 0.601129 0.025 Uiso 1 1 calc R U . . . C22 C 0.21766(17) 0.84645(14) 0.44086(10) 0.0207(3) Uani 1 1 d . . . . . H22A H 0.082208 0.869620 0.451036 0.025 Uiso 1 1 calc R U . . . H22B H 0.258781 0.788946 0.377939 0.025 Uiso 1 1 calc R U . . . C23 C 0.30356(19) 0.99049(14) 0.42017(10) 0.0237(3) Uani 1 1 d . . . . . H23A H 0.263547 1.047394 0.483444 0.028 Uiso 1 1 calc R U . . . H23B H 0.439052 0.967210 0.409271 0.028 Uiso 1 1 calc R U . . . C24 C 0.2514(2) 1.08562(16) 0.32393(12) 0.0314(3) Uani 1 1 d . . . . . H24A H 0.295740 1.031716 0.260398 0.047 Uiso 1 1 calc R U . . . H24B H 0.307586 1.177313 0.315362 0.047 Uiso 1 1 calc R U . . . H24C H 0.117373 1.109046 0.334129 0.047 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0148(4) 0.0226(4) 0.0153(4) -0.0045(3) -0.0042(3) -0.0017(3) O16 0.0333(5) 0.0187(5) 0.0268(5) 0.0034(4) -0.0134(4) -0.0084(4) O18 0.0451(6) 0.0247(5) 0.0316(5) 0.0030(4) -0.0246(5) -0.0088(4) O19 0.0147(5) 0.0335(5) 0.0217(5) -0.0087(4) -0.0042(3) -0.0017(4) C2 0.0174(6) 0.0182(6) 0.0151(6) -0.0019(4) -0.0049(5) -0.0024(5) C3 0.0164(6) 0.0149(6) 0.0154(6) 0.0004(4) -0.0034(5) -0.0027(4) C4 0.0188(6) 0.0149(6) 0.0151(6) 0.0003(4) -0.0036(5) -0.0023(5) C5 0.0168(6) 0.0322(7) 0.0216(7) -0.0074(5) -0.0046(5) -0.0020(5) C6 0.0242(7) 0.0371(8) 0.0242(7) -0.0093(6) -0.0094(5) -0.0040(6) C7 0.0310(7) 0.0288(7) 0.0175(6) -0.0075(5) -0.0045(5) -0.0045(6) C8 0.0236(7) 0.0258(7) 0.0178(6) -0.0038(5) 0.0012(5) -0.0035(5) C9 0.0198(6) 0.0172(6) 0.0168(6) 0.0005(5) -0.0020(5) -0.0040(5) C10 0.0159(6) 0.0261(7) 0.0207(6) -0.0022(5) 0.0013(5) -0.0046(5) C11 0.0151(6) 0.0236(6) 0.0199(6) -0.0009(5) -0.0042(5) -0.0053(5) C12 0.0179(6) 0.0138(6) 0.0154(6) 0.0016(4) -0.0043(5) -0.0037(4) C13 0.0137(6) 0.0198(6) 0.0164(6) -0.0011(5) -0.0049(4) -0.0027(5) C14 0.0220(6) 0.0201(6) 0.0176(6) -0.0018(5) -0.0078(5) -0.0042(5) C15 0.0226(6) 0.0192(6) 0.0171(6) -0.0037(5) -0.0047(5) -0.0031(5) C17 0.0430(8) 0.0193(7) 0.0281(7) 0.0046(5) -0.0125(6) -0.0068(6) C20 0.0165(6) 0.0219(6) 0.0167(6) -0.0006(5) -0.0053(5) -0.0026(5) C21 0.0213(6) 0.0221(6) 0.0194(6) 0.0004(5) -0.0055(5) -0.0034(5) C22 0.0226(6) 0.0211(6) 0.0188(6) -0.0003(5) -0.0058(5) -0.0026(5) C23 0.0249(7) 0.0220(7) 0.0245(7) 0.0001(5) -0.0062(5) -0.0037(5) C24 0.0374(8) 0.0251(7) 0.0328(8) 0.0067(6) -0.0112(6) -0.0074(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 O1 C13 110.95(9) . . ? C15 O16 C17 115.29(10) . . ? O1 C2 C3 108.42(10) . . ? O19 C2 O1 120.89(11) . . ? O19 C2 C3 130.69(11) . . ? C4 C3 C2 130.25(11) . . ? C12 C3 C2 107.57(10) . . ? C12 C3 C4 122.16(11) . . ? C3 C4 C9 116.23(11) . . ? C5 C4 C3 124.79(11) . . ? C5 C4 C9 118.97(11) . . ? C4 C5 H5 119.8 . . ? C6 C5 C4 120.39(12) . . ? C6 C5 H5 119.8 . . ? C5 C6 H6 119.6 . . ? C5 C6 C7 120.89(12) . . ? C7 C6 H6 119.6 . . ? C6 C7 H7 120.1 . . ? C8 C7 C6 119.83(12) . . ? C8 C7 H7 120.1 . . ? C7 C8 H8 119.4 . . ? C7 C8 C9 121.14(12) . . ? C9 C8 H8 119.4 . . ? C8 C9 C4 118.76(11) . . ? C8 C9 C10 121.43(11) . . ? C10 C9 C4 119.81(11) . . ? C9 C10 H10 118.8 . . ? C11 C10 C9 122.40(11) . . ? C11 C10 H10 118.8 . . ? C10 C11 H11 121.3 . . ? C10 C11 C12 117.46(11) . . ? C12 C11 H11 121.3 . . ? C3 C12 C11 121.90(11) . . ? C3 C12 C13 109.89(10) . . ? C11 C12 C13 128.20(11) . . ? O1 C13 C12 103.03(9) . . ? O1 C13 C14 108.59(10) . . ? O1 C13 C20 108.60(9) . . ? C12 C13 C14 114.24(10) . . ? C12 C13 C20 113.15(10) . . ? C14 C13 C20 108.90(9) . . ? C13 C14 H14A 108.4 . . ? C13 C14 H14B 108.4 . . ? H14A C14 H14B 107.5 . . ? C15 C14 C13 115.50(10) . . ? C15 C14 H14A 108.4 . . ? C15 C14 H14B 108.4 . . ? O16 C15 C14 110.08(10) . . ? O18 C15 O16 123.31(12) . . ? O18 C15 C14 126.62(12) . . ? O16 C17 H17A 109.5 . . ? O16 C17 H17B 109.5 . . ? O16 C17 H17C 109.5 . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C20 H20A 108.5 . . ? C13 C20 H20B 108.5 . . ? H20A C20 H20B 107.5 . . ? C21 C20 C13 115.04(10) . . ? C21 C20 H20A 108.5 . . ? C21 C20 H20B 108.5 . . ? C20 C21 H21A 109.2 . . ? C20 C21 H21B 109.2 . . ? C20 C21 C22 112.13(10) . . ? H21A C21 H21B 107.9 . . ? C22 C21 H21A 109.2 . . ? C22 C21 H21B 109.2 . . ? C21 C22 H22A 109.1 . . ? C21 C22 H22B 109.1 . . ? C21 C22 C23 112.69(10) . . ? H22A C22 H22B 107.8 . . ? C23 C22 H22A 109.1 . . ? C23 C22 H22B 109.1 . . ? C22 C23 H23A 109.0 . . ? C22 C23 H23B 109.0 . . ? H23A C23 H23B 107.8 . . ? C24 C23 C22 112.89(11) . . ? C24 C23 H23A 109.0 . . ? C24 C23 H23B 109.0 . . ? C23 C24 H24A 109.5 . . ? C23 C24 H24B 109.5 . . ? C23 C24 H24C 109.5 . . ? H24A C24 H24B 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C2 1.3635(14) . ? O1 C13 1.4583(14) . ? O16 C15 1.3406(15) . ? O16 C17 1.4500(15) . ? O18 C15 1.2005(16) . ? O19 C2 1.2103(15) . ? C2 C3 1.4746(16) . ? C3 C4 1.4211(16) . ? C3 C12 1.3674(17) . ? C4 C5 1.4120(17) . ? C4 C9 1.4240(17) . ? C5 H5 0.9500 . ? C5 C6 1.3714(18) . ? C6 H6 0.9500 . ? C6 C7 1.4075(19) . ? C7 H7 0.9500 . ? C7 C8 1.3636(19) . ? C8 H8 0.9500 . ? C8 C9 1.4168(17) . ? C9 C10 1.4226(18) . ? C10 H10 0.9500 . ? C10 C11 1.3708(18) . ? C11 H11 0.9500 . ? C11 C12 1.4044(17) . ? C12 C13 1.5033(16) . ? C13 C14 1.5298(17) . ? C13 C20 1.5394(16) . ? C14 H14A 0.9900 . ? C14 H14B 0.9900 . ? C14 C15 1.5097(17) . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C20 H20A 0.9900 . ? C20 H20B 0.9900 . ? C20 C21 1.5217(17) . ? C21 H21A 0.9900 . ? C21 H21B 0.9900 . ? C21 C22 1.5238(17) . ? C22 H22A 0.9900 . ? C22 H22B 0.9900 . ? C22 C23 1.5274(18) . ? C23 H23A 0.9900 . ? C23 H23B 0.9900 . ? C23 C24 1.5233(18) . ? C24 H24A 0.9800 . ? C24 H24B 0.9800 . ? C24 H24C 0.9800 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C2 C3 C4 179.31(11) . . . . ? O1 C2 C3 C12 1.13(13) . . . . ? O1 C13 C14 C15 59.76(13) . . . . ? O1 C13 C20 C21 -51.71(13) . . . . ? O19 C2 C3 C4 -0.8(2) . . . . ? O19 C2 C3 C12 -179.02(13) . . . . ? C2 O1 C13 C12 -3.13(12) . . . . ? C2 O1 C13 C14 -124.62(10) . . . . ? C2 O1 C13 C20 117.10(10) . . . . ? C2 C3 C4 C5 4.6(2) . . . . ? C2 C3 C4 C9 -176.01(11) . . . . ? C2 C3 C12 C11 177.10(11) . . . . ? C2 C3 C12 C13 -3.13(13) . . . . ? C3 C4 C5 C6 179.68(12) . . . . ? C3 C4 C9 C8 179.31(11) . . . . ? C3 C4 C9 C10 -0.92(17) . . . . ? C3 C12 C13 O1 3.84(12) . . . . ? C3 C12 C13 C14 121.42(11) . . . . ? C3 C12 C13 C20 -113.22(11) . . . . ? C4 C3 C12 C11 -1.27(18) . . . . ? C4 C3 C12 C13 178.50(10) . . . . ? C4 C5 C6 C7 0.8(2) . . . . ? C4 C9 C10 C11 -0.83(19) . . . . ? C5 C4 C9 C8 -1.23(17) . . . . ? C5 C4 C9 C10 178.55(11) . . . . ? C5 C6 C7 C8 -0.9(2) . . . . ? C6 C7 C8 C9 -0.1(2) . . . . ? C7 C8 C9 C4 1.15(19) . . . . ? C7 C8 C9 C10 -178.62(12) . . . . ? C8 C9 C10 C11 178.94(12) . . . . ? C9 C4 C5 C6 0.26(19) . . . . ? C9 C10 C11 C12 1.57(19) . . . . ? C10 C11 C12 C3 -0.54(18) . . . . ? C10 C11 C12 C13 179.73(12) . . . . ? C11 C12 C13 O1 -176.41(11) . . . . ? C11 C12 C13 C14 -58.83(16) . . . . ? C11 C12 C13 C20 66.53(15) . . . . ? C12 C3 C4 C5 -177.48(12) . . . . ? C12 C3 C4 C9 1.95(17) . . . . ? C12 C13 C14 C15 -54.59(14) . . . . ? C12 C13 C20 C21 62.03(13) . . . . ? C13 O1 C2 O19 -178.46(11) . . . . ? C13 O1 C2 C3 1.42(13) . . . . ? C13 C14 C15 O16 172.40(10) . . . . ? C13 C14 C15 O18 -8.00(19) . . . . ? C13 C20 C21 C22 173.15(10) . . . . ? C14 C13 C20 C21 -169.79(10) . . . . ? C17 O16 C15 O18 -1.09(18) . . . . ? C17 O16 C15 C14 178.52(11) . . . . ? C20 C13 C14 C15 177.84(10) . . . . ? C20 C21 C22 C23 -179.10(10) . . . . ? C21 C22 C23 C24 -179.38(11) . . . . ?