#------------------------------------------------------------------------------ #$Date: 2025-01-06 13:48:52 +0200 (Mon, 06 Jan 2025) $ #$Revision: 297106 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/96/7249619.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7249619 loop_ _publ_author_name 'Shen, Yue' 'Jin, Jiu-Zeng' 'Yang, Zhen-Yu' 'Zhao, Jie' 'Liu, Bin-Qiu' 'Zhang, Ju-Wen' _publ_section_title ; Syntheses and properties of two pH-directed types of cobalt--lanthanoid heterometallic complexes constructed from 2,5-dichlorobenzoate and 1,10-phenanthroline ; _journal_issue 48 _journal_name_full CrystEngComm _journal_page_first 6873 _journal_page_last 6882 _journal_paper_doi 10.1039/D4CE00886C _journal_volume 26 _journal_year 2024 _chemical_formula_moiety 'C94 H46 Cl20 Co2 Er2 N4 O20' _chemical_formula_sum 'C94 H46 Cl20 Co2 Er2 N4 O20' _chemical_formula_weight 2712.73 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _audit_creation_date 2022-01-25 _audit_creation_method ; Olex2 1.3-alpha (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6403) ; _audit_update_record ; 2022-07-08 deposited with the CCDC. 2024-11-14 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 107.346(2) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 13.7158(15) _cell_length_b 27.325(3) _cell_length_c 14.1709(16) _cell_measurement_reflns_used 9877 _cell_measurement_temperature 273.15 _cell_measurement_theta_max 28.57 _cell_measurement_theta_min 2.35 _cell_volume 5069.5(10) _computing_cell_refinement 'SAINT V8.18C (?, 2016)' _computing_data_reduction 'SAINT V8.18C (?, 2016)' _computing_molecular_graphics 'Olex2 1.3-alpha (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3-alpha (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 273.15 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.992 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0421 _diffrn_reflns_av_unetI/netI 0.0415 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.992 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 29 _diffrn_reflns_limit_k_min -36 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 37057 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.992 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.596 _diffrn_reflns_theta_min 1.680 _diffrn_source_current 30.0 _diffrn_source_power 1.2 _diffrn_source_voltage 40.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 2.557 _exptl_absorpt_correction_type none _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.777 _exptl_crystal_description block _exptl_crystal_F_000 2656 _refine_diff_density_max 0.983 _refine_diff_density_min -1.701 _refine_diff_density_rms 0.113 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.159 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 640 _refine_ls_number_reflns 12863 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.159 _refine_ls_R_factor_all 0.0524 _refine_ls_R_factor_gt 0.0416 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0271P)^2^+8.3604P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0869 _refine_ls_wR_factor_ref 0.0912 _reflns_Friedel_coverage 0.000 _reflns_number_gt 11031 _reflns_number_total 12863 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4ce00886c2.cif _cod_data_source_block 1_CCDC8 _cod_depositor_comments 'Adding full bibliography for 7249611--7249621.cif.' _cod_database_code 7249619 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Aromatic/amide H refined with riding coordinates: C14(H14), C18(H18), C30(H30), C34(H34), C38(H38), C46(H46), C47(H47), C3(H3), C25(H25), C7(H7), C29(H29), C15(H15), C2(H2), C33(H33), C35(H35), C37(H37), C19(H19), C5(H5), C21(H21), C43(H43), C11(H11), C45(H45), C23(H23) ; _shelx_res_file ; TITL 1_a.res in P2(1)/n 1.res created by SHELXL-2018/3 at 12:16:54 on 25-Jan-2022 REM Old TITL 1 in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.120, Rweak 0.009, Alpha 0.047, Orientation as input REM Formula found by SHELXT: C45 N5 O9 Cl10 Co Er CELL 0.71073 13.7158 27.3248 14.1709 90 107.346 90 ZERR 2 0.0015 0.003 0.0016 0 0.002 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Cl Co Er N O UNIT 188 92 40 4 4 8 40 EQIV $1 1-X,1-Y,1-Z L.S. 5 0 0 PLAN 5 TEMP 0 CONF FREE Er1 Er1_$1 FREE Er1 C4_$1 list 4 MORE -1 BOND $H fmap 2 53 acta REM REM REM WGHT 0.027100 8.360400 FVAR 0.20813 ER1 5 0.577405 0.437972 0.521787 11.00000 0.02109 0.02104 = 0.01921 -0.00091 0.00446 -0.00046 CO1 4 0.741128 0.315913 0.613504 11.00000 0.03559 0.03044 = 0.04460 0.00048 0.01215 0.00841 CL03 3 0.458433 0.516083 0.838979 11.00000 0.06158 0.11353 = 0.05063 0.00651 0.02526 -0.01745 CL04 3 0.805805 0.409739 0.935470 11.00000 0.04941 0.07464 = 0.05331 -0.01627 0.00773 -0.00813 CL05 3 0.890671 0.504614 0.580448 11.00000 0.04807 0.06784 = 0.08771 0.01390 -0.00451 0.00481 CL06 3 0.167550 0.347969 0.290658 11.00000 0.04537 0.09908 = 0.06918 -0.01716 -0.00835 0.01033 CL07 3 0.800184 0.517991 0.241224 11.00000 0.09739 0.09757 = 0.06544 0.03304 0.02847 -0.02669 CL08 3 0.479691 0.200178 0.549683 11.00000 0.09458 0.05024 = 0.11469 0.03587 0.00839 -0.01795 CL09 3 0.803302 0.705686 0.369518 11.00000 0.12700 0.05591 = 0.09481 0.01439 0.05547 -0.03033 CL0A 3 0.868053 0.296330 0.341773 11.00000 0.08651 0.07198 = 0.13166 -0.04291 0.06195 0.00309 CL0B 3 0.920724 0.545344 0.897420 11.00000 0.04271 0.20341 = 0.09771 0.03558 -0.00957 -0.00026 CL0C 3 0.348200 0.363193 0.872536 11.00000 0.06875 0.27262 = 0.11583 -0.05373 0.05536 -0.04966 O1 7 0.550411 0.507802 0.604668 11.00000 0.04633 0.03205 = 0.02038 -0.00832 0.00697 0.00153 O4 7 0.671186 0.500946 0.484441 11.00000 0.03361 0.02848 = 0.06172 -0.00411 0.02680 -0.00328 O6 7 0.584812 0.571171 0.463082 11.00000 0.03269 0.02897 = 0.07362 0.00172 0.02824 -0.00282 O8 7 0.650089 0.416847 0.681763 11.00000 0.05583 0.04407 = 0.02346 0.00642 0.00527 0.00466 O10 7 0.691462 0.339756 0.725584 11.00000 0.05802 0.05413 = 0.03473 0.01201 0.01915 0.02548 O5 7 0.542718 0.356484 0.511151 11.00000 0.03686 0.02322 = 0.08854 -0.00253 0.00248 -0.00545 O3 7 0.488283 0.572918 0.652683 11.00000 0.06591 0.04028 = 0.02602 -0.00920 -0.00374 0.02046 O7 7 0.606481 0.283424 0.545622 11.00000 0.04143 0.03773 = 0.05972 -0.00005 0.00492 0.00482 O2 7 0.719523 0.403113 0.495543 11.00000 0.04754 0.03983 = 0.04470 0.00655 0.02960 0.00946 O9 7 0.786992 0.330744 0.494064 11.00000 0.05979 0.04280 = 0.05540 0.00946 0.02579 0.01890 N1 6 0.820499 0.250509 0.649910 11.00000 0.04895 0.03584 = 0.03428 0.00564 0.01354 0.01162 C1 1 0.620771 0.532172 0.772916 11.00000 0.04317 0.02880 = 0.01659 -0.00100 0.00392 0.00179 C4 1 0.547750 0.537352 0.671064 11.00000 0.03838 0.02544 = 0.01905 -0.00480 0.00761 -0.00398 N2 6 0.887259 0.340973 0.705522 11.00000 0.04230 0.05173 = 0.05257 -0.00798 0.01956 -0.00464 C6 1 0.587229 0.525891 0.854548 11.00000 0.05198 0.04293 = 0.02681 -0.00131 0.00791 -0.00275 C8 1 0.664201 0.546144 0.474670 11.00000 0.02726 0.02823 = 0.03977 -0.00445 0.01796 -0.00575 C10 1 0.759047 0.574550 0.473279 11.00000 0.02678 0.03337 = 0.03343 -0.00685 0.01471 -0.00842 C12 1 0.656329 0.380422 0.736748 11.00000 0.03201 0.04358 = 0.02128 0.00481 0.00320 0.00744 C14 1 0.744174 0.620312 0.429065 11.00000 0.03956 0.03947 = 0.03671 -0.00592 0.01909 -0.01139 AFIX 43 H14 2 0.678129 0.632293 0.402915 11.00000 -1.20000 AFIX 0 C16 1 0.764869 0.372445 0.458849 11.00000 0.01932 0.03472 = 0.03125 -0.00483 0.00721 -0.00242 C18 1 0.783979 0.436997 0.344982 11.00000 0.03204 0.05710 = 0.03094 0.00260 0.01073 -0.00822 AFIX 43 H18 2 0.750679 0.457393 0.377960 11.00000 -1.20000 AFIX 0 C20 1 0.859100 0.558516 0.513911 11.00000 0.03269 0.04815 = 0.04568 -0.00860 0.01047 -0.00807 C22 1 0.798181 0.388012 0.371662 11.00000 0.02321 0.05213 = 0.02986 -0.00988 0.01070 -0.00595 C24 1 0.532792 0.311557 0.511673 11.00000 0.03182 0.02561 = 0.03586 -0.00264 0.01247 -0.00326 C26 1 0.677929 0.396628 0.917714 11.00000 0.04561 0.04398 = 0.03039 -0.00033 0.00863 0.00126 C28 1 0.616382 0.384907 0.823866 11.00000 0.04298 0.04460 = 0.02460 0.00524 0.00916 0.00878 C30 1 0.723991 0.537082 0.786011 11.00000 0.04199 0.05679 = 0.02881 0.00595 0.00801 0.00877 AFIX 43 H30 2 0.748188 0.539808 0.731515 11.00000 -1.20000 AFIX 0 C32 1 0.818161 0.455848 0.270887 11.00000 0.04332 0.08766 = 0.03432 0.00689 0.01141 -0.01768 C34 1 0.354517 0.322645 0.407254 11.00000 0.03339 0.04138 = 0.03526 -0.01059 0.00756 -0.00410 AFIX 43 H34 2 0.372369 0.354877 0.399286 11.00000 -1.20000 AFIX 0 C36 1 0.918848 0.255572 0.708227 11.00000 0.04249 0.05932 = 0.03222 0.01584 0.01748 0.02006 C38 1 0.655356 0.526065 0.949389 11.00000 0.07996 0.06390 = 0.01833 0.00451 0.00997 -0.00035 AFIX 43 H38 2 0.631909 0.521821 1.004029 11.00000 -1.20000 AFIX 0 C40 1 0.825743 0.648332 0.423256 11.00000 0.06354 0.04657 = 0.04827 -0.00484 0.03163 -0.02495 C42 1 0.427524 0.290895 0.465107 11.00000 0.03919 0.03017 = 0.03365 -0.00842 0.01573 -0.00826 C44 1 0.397840 0.243403 0.476363 11.00000 0.05969 0.04072 = 0.05165 -0.00036 0.01323 -0.01697 C46 1 0.757518 0.532557 0.961592 11.00000 0.07146 0.05971 = 0.02473 0.00663 -0.01133 0.00318 AFIX 43 H46 2 0.803652 0.533303 1.024788 11.00000 -1.20000 AFIX 0 C47 1 0.514473 0.374917 0.811872 11.00000 0.04370 0.11155 = 0.03807 -0.00802 0.01051 -0.00124 AFIX 43 H47 2 0.471285 0.367463 0.749326 11.00000 -1.20000 AFIX 0 C3 1 0.786024 0.206499 0.618656 11.00000 0.07227 0.03415 = 0.05037 0.00554 0.02206 0.01017 AFIX 43 H3 2 0.718832 0.203165 0.578964 11.00000 -1.20000 AFIX 0 C25 1 0.638936 0.397271 0.997168 11.00000 0.07366 0.08520 = 0.02776 -0.01285 0.01277 -0.00281 AFIX 43 H25 2 0.681317 0.405105 1.059852 11.00000 -1.20000 AFIX 0 C13 1 0.791485 0.537935 0.880724 11.00000 0.04579 0.06483 = 0.04093 0.00837 -0.00373 0.00261 C27 1 0.952691 0.303558 0.739963 11.00000 0.03610 0.07456 = 0.03565 0.00583 0.01711 0.00222 C7 1 0.916077 0.385893 0.735122 11.00000 0.05830 0.06561 = 0.08898 -0.01929 0.02976 -0.01719 AFIX 43 H7 2 0.871001 0.411545 0.710888 11.00000 -1.20000 AFIX 0 C29 1 0.924190 0.630991 0.459545 11.00000 0.04911 0.07149 = 0.07614 -0.01433 0.03145 -0.03407 AFIX 43 H29 2 0.978906 0.649264 0.452749 11.00000 -1.20000 AFIX 0 C15 1 0.847848 0.164274 0.643517 11.00000 0.11180 0.03722 = 0.07350 0.00985 0.04707 0.01986 AFIX 43 H15 2 0.822208 0.133695 0.619713 11.00000 -1.20000 AFIX 0 C31 1 0.984366 0.215238 0.737464 11.00000 0.06339 0.08037 = 0.04876 0.03927 0.03398 0.03835 C2 1 0.940078 0.586695 0.505494 11.00000 0.02656 0.08221 = 0.07078 -0.01565 0.01296 -0.01668 AFIX 43 H2 2 1.006452 0.575135 0.531704 11.00000 -1.20000 AFIX 0 C33 1 0.945968 0.169202 0.703162 11.00000 0.10232 0.06855 = 0.07171 0.04558 0.05277 0.05359 AFIX 43 H33 2 0.987365 0.141712 0.720979 11.00000 -1.20000 AFIX 0 C17 1 1.051894 0.311068 0.805408 11.00000 0.03836 0.11787 = 0.04647 0.00830 0.01482 -0.00310 C35 1 0.228737 0.259608 0.371361 11.00000 0.05442 0.08214 = 0.08233 -0.02315 0.00282 -0.03668 AFIX 43 H35 2 0.162883 0.248921 0.338914 11.00000 -1.20000 AFIX 0 C9 1 0.256221 0.307032 0.361628 11.00000 0.04074 0.06205 = 0.04089 -0.01897 0.00701 -0.00540 C37 1 0.298966 0.227976 0.429272 11.00000 0.07903 0.05730 = 0.10033 -0.00368 0.00721 -0.04221 AFIX 43 H37 2 0.280157 0.195879 0.437064 11.00000 -1.20000 AFIX 0 C19 1 1.078117 0.359251 0.836129 11.00000 0.05172 0.14976 = 0.07085 -0.02081 0.01877 -0.04090 AFIX 43 H19 2 1.141766 0.365788 0.880768 11.00000 -1.20000 AFIX 0 C39 1 0.476194 0.375865 0.891225 11.00000 0.05596 0.10967 = 0.05643 -0.01264 0.02943 -0.01306 C5 1 1.084994 0.224330 0.802213 11.00000 0.05544 0.13134 = 0.06562 0.05549 0.02650 0.04560 AFIX 43 H5 2 1.130158 0.198250 0.821325 11.00000 -1.20000 AFIX 0 C41 1 0.845742 0.358135 0.318476 11.00000 0.03760 0.07458 = 0.05148 -0.02935 0.02124 -0.00892 C21 1 1.115922 0.269053 0.835943 11.00000 0.04211 0.17024 = 0.05257 0.04183 0.01064 0.01762 AFIX 43 H21 2 1.180719 0.273030 0.880418 11.00000 -1.20000 AFIX 0 C43 1 0.538401 0.386451 0.984065 11.00000 0.07855 0.10623 = 0.04545 -0.00998 0.03793 -0.01156 AFIX 43 H43 2 0.512554 0.386289 1.037734 11.00000 -1.20000 AFIX 0 C11 1 0.865872 0.426947 0.219767 11.00000 0.06007 0.12877 = 0.03797 -0.00898 0.02488 -0.02576 AFIX 43 H11 2 0.888902 0.440240 0.169869 11.00000 -1.20000 AFIX 0 C45 1 0.879638 0.378264 0.242372 11.00000 0.05623 0.12170 = 0.05592 -0.03815 0.03496 -0.01057 AFIX 43 H45 2 0.911564 0.358365 0.207259 11.00000 -1.20000 AFIX 0 C23 1 1.011900 0.396440 0.801611 11.00000 0.06603 0.10619 = 0.10523 -0.03705 0.03512 -0.03811 AFIX 43 H23 2 1.029754 0.428456 0.821721 11.00000 -1.20000 AFIX 0 HKLF 4 REM 1_a.res in P2(1)/n REM wR2 = 0.0912, GooF = S = 1.159, Restrained GooF = 1.159 for all data REM R1 = 0.0416 for 11031 Fo > 4sig(Fo) and 0.0524 for all 12863 data REM 640 parameters refined using 0 restraints END WGHT 0.0271 8.3652 REM Highest difference peak 0.983, deepest hole -1.701, 1-sigma level 0.113 Q1 1 0.4377 0.2216 0.5849 11.00000 0.05 0.98 Q2 1 0.5176 0.4391 0.5338 11.00000 0.05 0.94 Q3 1 0.6416 0.4385 0.5130 11.00000 0.05 0.91 Q4 1 0.8113 0.4879 0.2081 11.00000 0.05 0.82 Q5 1 0.3980 0.3324 0.9201 11.00000 0.05 0.66 ; _shelx_res_checksum 75374 _shelx_hkl_file ; 2 0 0 131.39 4.80 -2 0 0 144.69 4.80 -2 0 0 142.89 5.00 3 0 0 -0.80 0.40 -3 0 0 0.00 0.40 -3 0 0 0.50 0.70 4 0 0 418.46 14.90 -4 0 0 447.56 16.50 -4 0 0 471.85 15.50 5 0 0 5.20 0.70 -5 0 0 2.60 1.40 -5 0 0 3.10 1.10 6 0 0 1605.64 56.99 -6 0 0 1808.22 58.19 -6 0 0 1773.72 60.89 7 0 0 -0.30 0.80 -7 0 0 -0.80 2.00 8 0 0 696.73 25.40 -8 0 0 794.42 26.60 -8 0 0 787.22 28.40 9 0 0 1.50 1.00 -9 0 0 2.20 2.00 -9 0 0 -3.30 2.50 -10 0 0 2.10 3.00 -10 0 0 8.00 2.20 -11 0 0 -5.60 3.10 -11 0 0 -1.30 2.50 -12 0 0 679.83 27.60 -12 0 0 711.43 25.40 -13 0 0 14.50 4.90 -13 0 0 6.30 3.70 -14 0 0 120.09 9.60 -15 0 0 -11.10 4.80 -16 0 0 -3.50 5.30 -17 0 0 -8.50 5.70 -17 0 1 13.20 6.80 -16 0 1 -3.30 5.10 -15 0 1 48.00 7.40 -14 0 1 1.10 3.20 -14 0 1 3.70 4.50 -13 0 1 1019.30 36.90 -13 0 1 1047.00 39.80 -12 0 1 4.80 2.80 -12 0 1 -3.40 3.80 -11 0 1 66.99 6.50 -11 0 1 78.29 5.00 -10 0 1 -1.00 2.60 -10 0 1 -0.90 1.90 -9 0 1 249.38 9.90 -9 0 1 246.88 11.20 9 0 -1 235.38 8.80 -8 0 1 4.00 2.10 -8 0 1 2.60 1.70 8 0 -1 1.10 1.10 -7 0 1 4923.91 158.78 -7 0 1 4804.72 165.18 7 0 -1 4586.34 157.18 -6 0 1 8.30 1.60 6 0 -1 1.80 0.80 -5 0 1 234.48 8.30 5 0 -1 211.68 7.70 -4 0 1 1.90 0.90 4 0 -1 3.40 0.60 -3 0 1 1832.02 58.89 3 0 -1 1704.03 58.19 -2 0 1 0.30 0.30 -2 0 1 0.80 0.40 1 0 -1 4404.26 145.89 0 0 -1 4.50 0.70 1 0 1 601.64 19.40 -1 0 -1 580.54 20.30 -1 0 -1 561.74 19.60 3 0 1 962.40 31.90 -3 0 -1 947.61 33.90 -3 0 -1 957.10 32.40 4 0 1 1.10 0.60 -4 0 -1 0.20 0.80 -4 0 -1 2.90 1.20 5 0 1 1732.83 57.49 -5 0 -1 1736.63 60.99 -5 0 -1 1751.02 58.39 -6 0 -1 5.10 2.30 -6 0 -1 2.20 1.60 7 0 1 1376.96 48.10 -7 0 -1 1527.85 49.30 -7 0 -1 1446.46 51.69 8 0 1 0.90 0.90 -8 0 -1 -0.40 2.30 -8 0 -1 -0.10 1.70 9 0 1 13.30 1.60 -9 0 -1 19.50 2.70 -9 0 -1 15.50 3.30 -10 0 -1 1.50 2.30 -10 0 -1 -6.20 2.80 -11 0 -1 928.31 33.10 -11 0 -1 947.41 35.60 -12 0 -1 7.60 4.20 -12 0 -1 2.20 3.40 -13 0 -1 303.57 13.00 -13 0 -1 300.47 15.00 -14 0 -1 -2.10 4.80 -15 0 -1 68.09 8.70 -16 0 -1 -3.10 5.30 -17 0 -1 43.10 7.90 -18 0 2 105.29 11.60 -17 0 2 -4.60 5.60 -16 0 2 47.90 7.70 -15 0 2 -1.90 4.80 -14 0 2 313.87 15.60 -14 0 2 292.37 13.20 -13 0 2 7.40 4.60 -13 0 2 4.90 3.30 -12 0 2 99.39 8.10 -12 0 2 106.49 6.20 -11 0 2 0.60 2.40 -11 0 2 -4.10 3.10 -10 0 2 -2.90 1.90 -10 0 2 0.40 2.70 10 0 -2 1.60 1.30 -9 0 2 0.80 2.20 -9 0 2 -3.50 1.80 9 0 -2 -0.10 1.20 -8 0 2 913.41 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5.50 3.70 -13 0 3 202.58 11.90 -13 0 3 208.38 9.70 -12 0 3 -1.40 2.60 -12 0 3 -5.00 3.70 -11 0 3 148.49 7.30 -11 0 3 141.09 8.50 -10 0 3 -1.90 2.60 -10 0 3 -2.50 1.90 10 0 -3 2.90 1.50 -9 0 3 1264.47 42.20 9 0 -3 1171.98 41.20 -8 0 3 -0.80 1.80 8 0 -3 2.40 1.40 -7 0 3 2896.61 94.59 7 0 -3 2748.32 93.39 -6 0 3 6.30 1.40 6 0 -3 3.60 1.30 -5 0 3 77.19 3.70 5 0 -3 74.79 3.60 4 0 -3 0.30 1.00 3 0 -3 329.27 11.80 2 0 -3 1.00 0.90 -1 0 3 9999.00 332.57 0 0 -3 7.90 1.60 1 0 3 1540.15 49.00 -1 0 -3 1470.55 50.99 -1 0 -3 1375.36 49.60 2 0 3 1.20 1.20 -2 0 -3 3.90 1.50 -2 0 -3 3.40 1.30 3 0 3 1085.09 36.40 -3 0 -3 1073.29 38.10 -3 0 -3 1076.09 36.80 4 0 3 0.90 1.20 -4 0 -3 0.40 1.60 -4 0 -3 2.30 1.50 5 0 3 1629.54 52.89 -5 0 -3 1561.44 55.59 -5 0 -3 1551.04 53.49 6 0 3 4.90 1.70 -6 0 -3 2.50 2.10 -6 0 -3 3.20 2.30 7 0 3 46.50 3.10 -7 0 -3 54.09 3.60 -7 0 -3 47.30 4.40 8 0 3 3.20 1.60 -8 0 -3 -6.30 2.70 -8 0 -3 2.80 2.50 -9 0 -3 12.00 3.40 -10 0 -3 -3.10 2.70 -10 0 -3 -3.60 3.10 -11 0 -3 530.95 21.70 -11 0 -3 526.45 20.10 -12 0 -3 3.80 4.00 -12 0 -3 11.40 4.70 -13 0 -3 165.68 9.00 -13 0 -3 183.08 11.00 -14 0 -3 -1.40 4.80 -15 0 -3 1.40 5.20 -16 0 -3 -7.40 5.30 -18 0 4 2.70 6.20 -17 0 4 -5.70 5.20 -16 0 4 63.29 8.50 -15 0 4 0.40 4.20 -14 0 4 486.65 19.40 -14 0 4 492.55 22.10 -13 0 4 -6.40 4.00 -13 0 4 5.90 3.20 -12 0 4 155.08 7.70 -12 0 4 146.99 9.80 -11 0 4 3.50 2.40 -11 0 4 -3.40 2.80 -10 0 4 54.79 4.40 10 0 -4 56.99 3.80 -9 0 4 -1.80 1.90 9 0 -4 -2.80 1.70 -8 0 4 4086.59 135.39 8 0 -4 4014.50 133.99 7 0 -4 5.70 2.00 -6 0 4 64.49 3.60 6 0 -4 64.49 3.60 5 0 -4 -0.90 1.10 4 0 -4 28.30 2.30 3 0 -4 2.50 1.30 -2 0 4 7435.16 253.37 2 0 -4 7792.32 252.67 -1 0 4 1.60 1.10 0 0 4 1521.75 51.89 0 0 -4 1562.64 52.79 -1 0 -4 3.00 1.30 -1 0 -4 2.50 1.60 2 0 4 11.00 1.90 -2 0 -4 13.30 1.90 -2 0 -4 15.50 2.10 3 0 4 -1.60 1.50 -3 0 -4 -0.80 1.40 -3 0 -4 4.60 2.00 4 0 4 2276.37 74.99 -4 0 -4 2243.38 78.29 -4 0 -4 2212.48 75.69 5 0 4 0.10 1.70 -5 0 -4 -1.00 2.00 -5 0 -4 4.90 2.10 6 0 4 843.22 29.10 -6 0 -4 830.92 29.30 -6 0 -4 830.72 30.50 7 0 4 0.90 1.60 -7 0 -4 -2.10 2.10 -7 0 -4 -5.60 2.40 8 0 4 22.50 2.80 -8 0 -4 22.80 3.70 -8 0 -4 24.80 3.30 -9 0 -4 -4.30 2.90 -9 0 -4 -0.30 2.70 -10 0 -4 488.65 18.50 -10 0 -4 484.55 19.90 -11 0 -4 -3.20 3.20 -11 0 -4 1.00 3.80 -12 0 -4 295.17 14.40 -12 0 -4 290.57 13.00 -13 0 -4 12.50 4.40 -13 0 -4 2.50 4.70 -14 0 -4 45.90 6.90 -15 0 -4 -5.30 5.00 -18 0 5 0.20 6.00 -17 0 5 1.80 4.70 -16 0 5 2.80 5.30 -15 0 5 326.07 14.10 -15 0 5 319.77 17.00 -14 0 5 8.30 4.00 -14 0 5 20.10 5.50 -13 0 5 7.80 4.50 -13 0 5 18.40 3.70 -12 0 5 -6.60 4.10 -12 0 5 6.50 3.10 -11 0 5 292.07 12.10 11 0 -5 289.97 11.90 -10 0 5 1.00 2.70 10 0 -5 -1.30 2.00 -9 0 5 855.11 30.60 9 0 -5 873.11 30.30 -8 0 5 6.80 2.20 8 0 -5 1.30 2.00 -7 0 5 164.98 7.20 7 0 -5 158.98 7.20 6 0 -5 -1.40 1.30 5 0 -5 327.97 12.50 4 0 -5 1.20 1.50 -3 0 5 3227.38 109.79 3 0 -5 3394.96 109.99 -2 0 5 0.00 1.40 -1 0 5 2672.43 89.09 0 0 5 -1.40 1.40 0 0 -5 3.80 2.10 1 0 5 5.30 1.90 -1 0 -5 2.20 2.00 -1 0 -5 5.30 1.40 2 0 5 9.70 2.20 -2 0 -5 1.60 1.60 -2 0 -5 -1.30 2.00 3 0 5 2324.67 76.89 -3 0 -5 2251.77 77.49 -3 0 -5 2286.97 79.79 4 0 5 -1.30 1.90 -4 0 -5 3.20 2.20 -4 0 -5 0.50 2.30 5 0 5 642.64 23.20 -5 0 -5 647.84 23.90 -5 0 -5 638.34 23.40 6 0 5 3.00 2.00 -6 0 -5 0.60 2.70 -6 0 -5 -1.30 2.40 7 0 5 375.36 14.60 -7 0 -5 373.36 15.40 -7 0 -5 381.76 14.80 8 0 5 1.40 2.30 -8 0 -5 -2.50 3.20 -8 0 -5 6.20 3.00 -9 0 -5 143.09 8.30 -9 0 -5 143.39 7.60 -10 0 -5 -1.10 3.40 -10 0 -5 -0.70 3.40 -11 0 -5 282.87 13.60 -11 0 -5 275.47 12.40 -12 0 -5 16.70 4.40 -12 0 -5 17.20 5.20 -13 0 -5 92.39 9.00 -14 0 -5 -2.60 5.40 -15 0 -5 -0.10 5.30 -18 0 6 0.90 6.00 -17 0 6 -3.90 5.20 -16 0 6 75.69 9.30 -15 0 6 5.70 3.90 -15 0 6 7.90 4.60 -14 0 6 284.37 12.80 -14 0 6 276.67 15.20 -13 0 6 -0.60 3.00 -13 0 6 -7.80 3.80 -12 0 6 37.00 4.60 -11 0 6 -2.10 2.60 11 0 -6 -4.70 2.40 -10 0 6 1243.38 44.00 10 0 -6 1280.67 43.80 -9 0 6 18.40 3.20 9 0 -6 7.90 3.00 -8 0 6 1462.75 50.19 8 0 -6 1452.25 49.90 7 0 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-11 0 7 90.09 5.80 11 0 -7 100.49 6.60 -10 0 7 0.70 2.60 10 0 -7 1.40 2.70 -9 0 7 1348.97 47.40 9 0 -7 1366.76 47.10 8 0 -7 0.60 2.40 7 0 -7 120.99 6.50 -6 0 7 -4.60 1.90 6 0 -7 -2.00 2.00 -5 0 7 1461.35 50.09 -4 0 7 -4.60 2.60 -3 0 7 2905.81 97.39 -2 0 7 3.70 2.20 -1 0 7 243.98 10.60 0 0 7 3.00 2.50 0 0 -7 1.00 3.00 1 0 7 268.37 11.20 -1 0 -7 237.38 11.30 2 0 7 -4.40 2.40 -2 0 -7 1.00 1.80 -2 0 -7 2.70 2.80 3 0 7 441.16 17.30 -3 0 -7 437.56 17.20 -3 0 -7 434.36 17.00 4 0 7 3.80 2.70 -4 0 -7 4.90 2.60 -4 0 -7 10.80 3.20 5 0 7 377.56 15.40 -5 0 -7 365.96 15.10 -5 0 -7 365.66 15.00 6 0 7 -5.70 2.50 7 0 7 123.69 8.00 -7 0 -7 162.28 8.30 -7 0 -7 157.88 8.60 -8 0 -7 -3.70 3.30 -8 0 -7 -6.30 3.10 -9 0 -7 348.37 14.80 -9 0 -7 337.57 15.20 -10 0 -7 3.40 4.30 -10 0 -7 9.70 4.40 -11 0 -7 218.98 12.00 -11 0 -7 221.28 11.70 -12 0 -7 -2.40 4.80 -12 0 -7 9.70 5.10 -13 0 -7 122.49 9.70 -14 0 -7 -3.60 5.40 -18 0 8 -0.50 5.90 -17 0 8 9.90 6.10 -16 0 8 129.19 10.60 -15 0 8 1.60 3.80 -15 0 8 1.10 4.80 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453.85 17.40 -6 -20 5 437.96 18.20 -7 -20 5 166.58 8.60 -7 -20 5 174.08 9.80 -8 -20 5 17.00 4.90 -9 -20 5 1.60 4.50 -10 -20 5 301.87 14.80 -11 -20 5 6.60 4.70 -12 -20 5 493.85 21.80 -13 -20 5 4.20 5.30 -14 -20 5 -1.70 5.30 -15 -20 5 -0.50 5.30 -13 20 -4 82.49 10.20 -12 20 -4 6.00 6.00 -11 20 -4 47.30 7.90 11 -20 4 54.59 6.90 -10 20 -4 14.60 6.50 10 -20 4 17.00 5.30 -9 20 -4 154.28 12.10 9 -20 4 159.08 9.90 -8 20 -4 -1.30 4.50 8 -20 4 6.50 4.10 -7 20 -4 291.87 16.60 7 -20 4 272.17 13.50 -6 20 -4 -5.20 5.00 6 -20 4 -1.20 2.80 5 -20 4 4.20 3.40 4 -20 4 7.00 3.50 3 -20 4 195.98 10.20 2 -20 4 43.90 4.80 1 -20 4 858.01 30.00 1 -20 4 855.61 31.20 0 -20 4 7.50 3.20 0 -20 4 9.30 2.60 -1 -20 4 55.69 4.50 -1 -20 4 56.79 4.70 -2 -20 4 4.50 2.80 -2 -20 4 8.60 3.00 -3 -20 4 235.68 10.60 -3 -20 4 234.98 10.80 -4 -20 4 11.30 3.60 -4 -20 4 9.30 3.20 -5 -20 4 1521.95 51.79 -5 -20 4 1483.75 52.79 -6 -20 4 9.60 3.10 -6 -20 4 8.30 3.90 -7 -20 4 45.80 4.40 -7 -20 4 42.90 5.60 -8 -20 4 -5.90 3.80 -9 -20 4 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-22 8 79.89 6.40 -1 -22 8 80.49 6.70 -2 -22 8 212.88 10.30 -2 -22 8 206.58 11.10 -3 -22 8 16.60 4.10 -3 -22 8 14.00 3.90 -4 -22 8 3.20 3.60 -4 -22 8 4.80 3.70 -5 -22 8 334.27 15.00 -5 -22 8 318.67 14.60 -6 -22 8 0.20 3.40 -6 -22 8 -4.50 3.80 -7 -22 8 135.29 9.20 -7 -22 8 138.39 8.80 -8 -22 8 387.06 16.30 -8 -22 8 385.66 17.80 -9 -22 8 5.30 5.10 -10 -22 8 1.40 4.90 -11 -22 8 75.39 8.70 -12 -22 8 64.79 8.70 -13 -22 8 50.69 8.10 -14 -22 8 83.19 9.80 -10 22 -7 38.40 8.50 10 -22 7 23.20 7.20 9 -22 7 17.00 6.30 8 -22 7 190.98 12.60 7 -22 7 1.50 5.10 6 -22 7 64.79 8.20 5 -22 7 229.88 13.50 4 -22 7 29.70 5.20 3 -22 7 17.50 4.50 2 -22 7 335.17 15.40 1 -22 7 113.99 8.50 0 -22 7 91.39 7.50 0 -22 7 90.39 6.10 -1 -22 7 258.27 11.70 -1 -22 7 262.27 12.40 -2 -22 7 3.80 3.00 -2 -22 7 -0.20 3.30 -3 -22 7 141.59 8.60 -3 -22 7 140.69 8.10 -4 -22 7 204.38 10.60 -4 -22 7 211.28 10.60 -5 -22 7 4.20 3.90 -5 -22 7 0.40 3.20 -6 -22 7 417.06 18.00 -6 -22 7 414.46 17.20 -7 -22 7 190.38 10.90 -7 -22 7 188.28 9.80 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-23 5 260.37 12.20 -1 -23 5 35.90 4.80 -1 -23 5 34.80 4.40 -2 -23 5 510.55 20.20 -2 -23 5 512.55 19.90 -3 -23 5 211.08 10.50 -3 -23 5 199.78 10.10 -4 -23 5 7.90 3.50 -4 -23 5 6.40 3.90 -5 -23 5 297.27 13.30 -5 -23 5 308.37 13.80 -6 -23 5 109.29 7.40 -6 -23 5 112.09 7.10 -7 -23 5 43.20 6.10 -7 -23 5 43.60 5.00 -8 -23 5 98.29 8.00 -9 -23 5 47.00 6.70 -10 -23 5 85.09 7.60 -11 -23 5 -0.50 4.90 -12 -23 5 54.19 7.90 -13 -23 5 31.60 7.20 -14 -23 5 109.99 10.40 -11 23 -4 77.79 9.90 -10 23 -4 26.70 7.20 10 -23 4 34.40 6.40 -9 23 -4 -0.10 5.80 9 -23 4 1.50 4.30 -8 23 -4 53.29 9.10 8 -23 4 59.69 6.90 7 -23 4 207.18 12.10 6 -23 4 11.40 4.40 5 -23 4 341.17 15.90 4 -23 4 66.49 6.00 3 -23 4 23.60 4.40 2 -23 4 68.39 5.70 1 -23 4 54.99 5.60 0 -23 4 23.60 4.20 0 -23 4 19.20 3.50 -1 -23 4 327.97 13.30 -1 -23 4 315.17 13.70 -2 -23 4 126.39 7.70 -2 -23 4 117.79 7.10 -3 -23 4 123.19 7.60 -3 -23 4 116.79 7.00 -4 -23 4 220.08 10.60 -4 -23 4 218.08 10.30 -5 -23 4 57.19 5.80 -5 -23 4 68.09 6.10 -6 -23 4 134.59 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5 -24 -7 15.20 4.20 4 -24 -7 4.00 3.70 3 -24 -7 255.87 12.70 2 -24 -7 46.30 6.10 2 -24 -7 41.10 5.90 1 -24 -7 320.27 14.80 1 -24 -7 295.77 14.40 0 -24 -7 15.50 4.70 0 -24 -7 17.80 4.90 -1 -24 -7 43.50 5.60 -1 -24 -7 46.60 6.40 -2 -24 -7 48.40 5.90 -2 -24 -7 51.29 6.90 -3 -24 -7 319.87 15.70 -3 -24 -7 332.07 15.00 -4 -24 -7 25.90 6.10 -5 -24 -7 109.49 9.30 -6 -24 -7 16.60 5.50 -7 -24 -7 66.79 8.20 -8 -24 -7 2.50 5.70 -9 -24 -7 45.40 7.50 13 -24 -8 3.30 5.70 12 -24 -8 12.10 5.90 11 -24 -8 6.10 5.70 10 -24 -8 420.16 19.70 9 -24 -8 31.80 6.50 8 -24 -8 67.39 7.20 7 -24 -8 36.00 5.70 6 -24 -8 70.49 7.80 5 -24 -8 -5.30 4.60 4 -24 -8 218.98 11.70 3 -24 -8 16.00 4.50 2 -24 -8 385.46 16.80 2 -24 -8 374.66 17.10 1 -24 -8 13.60 5.00 1 -24 -8 16.70 5.30 0 -24 -8 199.28 11.40 0 -24 -8 201.18 11.60 -1 -24 -8 19.00 5.10 -1 -24 -8 24.20 6.60 -2 -24 -8 83.19 8.20 -2 -24 -8 90.89 8.40 -3 -24 -8 3.50 5.70 -3 -24 -8 6.20 4.40 -4 -24 -8 121.79 10.20 -5 -24 -8 37.20 7.30 -6 -24 -8 241.78 14.10 -7 -24 -8 13.50 6.80 -8 -24 -8 11.10 5.90 11 -24 -9 165.18 12.50 10 -24 -9 24.10 6.80 9 -24 -9 162.88 11.70 8 -24 -9 0.20 5.10 7 -24 -9 274.47 14.80 6 -24 -9 17.50 5.80 5 -24 -9 95.89 8.90 4 -24 -9 25.20 6.00 3 -24 -9 455.15 19.80 2 -24 -9 37.40 5.90 2 -24 -9 36.50 6.10 1 -24 -9 366.96 17.80 1 -24 -9 403.56 17.90 0 -24 -9 16.60 5.90 0 -24 -9 11.40 5.00 -1 -24 -9 -1.60 4.70 -1 -24 -9 10.60 6.10 -2 -24 -9 2.60 5.80 -2 -24 -9 -2.70 4.60 -3 -24 -9 279.27 15.50 -4 -24 -9 7.00 6.50 -5 -24 -9 139.49 11.50 -6 -24 -9 11.00 7.10 -7 -24 -9 10.30 7.10 11 -24 -10 2.40 6.10 9 -24 -10 11.00 5.30 8 -24 -10 72.59 8.00 7 -24 -10 2.10 5.60 6 -24 -10 1.10 5.50 5 -24 -10 1.90 4.50 4 -24 -10 228.58 13.00 3 -24 -10 12.40 5.90 3 -24 -10 11.80 5.10 2 -24 -10 219.88 12.30 2 -24 -10 194.28 12.40 1 -24 -10 11.00 5.90 0 -24 -10 25.60 6.00 0 -24 -10 37.00 6.90 -1 -24 -10 7.90 5.80 -1 -24 -10 -3.30 4.80 -2 -24 -10 154.38 11.60 -2 -24 -10 162.78 11.00 -3 -24 -10 16.10 6.90 -4 -24 -10 224.78 14.90 -5 -24 -10 6.60 7.40 -6 -24 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130.99 10.10 -9 -26 8 14.90 6.00 -10 -26 8 46.20 7.80 -11 -26 8 157.68 11.90 -12 -26 8 11.80 6.30 8 -26 7 59.39 8.80 7 -26 7 9.10 5.10 6 -26 7 5.70 5.50 5 -26 7 144.09 10.50 4 -26 7 3.80 4.90 3 -26 7 40.10 6.50 2 -26 7 273.27 14.60 1 -26 7 34.20 5.80 0 -26 7 54.19 6.30 -1 -26 7 126.99 8.60 -2 -26 7 38.90 5.80 -2 -26 7 45.80 5.70 -3 -26 7 224.18 11.60 -3 -26 7 236.18 12.20 -4 -26 7 246.28 12.70 -4 -26 7 259.27 13.10 -5 -26 7 2.50 3.80 -5 -26 7 3.60 4.40 -6 -26 7 66.59 7.20 -6 -26 7 67.29 6.70 -7 -26 7 132.29 9.00 -7 -26 7 123.79 9.70 -8 -26 7 44.80 6.90 -9 -26 7 191.78 12.30 -10 -26 7 65.09 8.80 -11 -26 7 6.90 6.30 -12 -26 7 34.70 7.70 9 -26 6 54.59 8.50 8 -26 6 3.90 5.60 7 -26 6 6.60 4.70 6 -26 6 179.08 12.10 5 -26 6 31.10 6.30 4 -26 6 156.68 10.70 3 -26 6 183.38 11.30 2 -26 6 75.89 7.70 1 -26 6 154.28 10.00 0 -26 6 110.79 8.40 -1 -26 6 44.50 5.80 -2 -26 6 244.58 12.50 -2 -26 6 247.88 11.60 -3 -26 6 8.70 4.40 -3 -26 6 9.90 4.10 -4 -26 6 32.50 5.10 -4 -26 6 32.30 5.30 -5 -26 6 219.38 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255.57 11.90 -2 -26 4 258.97 12.50 -3 -26 4 216.18 11.10 -3 -26 4 223.48 10.90 -4 -26 4 48.30 5.30 -4 -26 4 47.40 5.80 -5 -26 4 57.39 6.00 -5 -26 4 67.39 6.20 -6 -26 4 225.28 12.10 -6 -26 4 240.78 11.50 -7 -26 4 32.00 5.70 -8 -26 4 158.28 10.40 -9 -26 4 58.59 7.40 -10 -26 4 27.70 6.60 -11 -26 4 64.29 8.40 -12 -26 4 39.40 7.50 -11 26 -3 61.39 9.80 11 -26 3 62.79 8.40 -10 26 -3 93.29 11.60 10 -26 3 98.49 9.70 9 -26 3 5.40 4.90 8 -26 3 20.80 5.30 7 -26 3 222.58 12.70 6 -26 3 23.70 4.70 5 -26 3 95.89 8.10 4 -26 3 70.49 7.10 3 -26 3 16.80 4.10 2 -26 3 189.48 10.40 1 -26 3 82.89 6.30 0 -26 3 295.07 13.80 -1 -26 3 420.76 17.10 -1 -26 3 428.96 17.70 -2 -26 3 97.49 6.90 -2 -26 3 73.19 6.30 -3 -26 3 68.49 6.30 -3 -26 3 85.29 6.40 -4 -26 3 27.60 4.70 -4 -26 3 30.80 4.20 -5 -26 3 82.49 6.50 -5 -26 3 78.19 6.50 -6 -26 3 207.78 11.10 -7 -26 3 247.48 12.80 -8 -26 3 62.89 7.10 -9 -26 3 91.59 8.60 -10 -26 3 79.19 7.50 -11 -26 3 6.70 5.40 -12 -26 3 96.79 9.50 -11 26 -2 34.70 8.50 11 -26 2 33.30 6.80 -10 26 -2 16.30 7.50 10 -26 2 15.70 5.50 -9 26 -2 67.49 10.00 9 -26 2 68.39 8.20 8 -26 2 43.60 6.50 7 -26 2 52.79 7.00 6 -26 2 102.79 7.70 5 -26 2 31.30 4.90 4 -26 2 179.18 9.90 3 -26 2 372.96 16.10 2 -26 2 5.20 3.10 1 -26 2 181.98 10.00 0 -26 2 330.77 14.90 -1 -26 2 40.80 4.70 -1 -26 2 44.90 5.70 -2 -26 2 162.28 8.50 -2 -26 2 178.48 9.50 -3 -26 2 176.38 9.10 -3 -26 2 150.38 8.70 -4 -26 2 20.50 4.00 -4 -26 2 16.50 3.40 -5 -26 2 78.59 5.90 -5 -26 2 71.39 6.80 -6 -26 2 315.87 14.70 -7 -26 2 28.50 5.50 -8 -26 2 148.29 9.80 -9 -26 2 68.59 7.60 -10 -26 2 -1.20 5.10 -11 -26 2 102.69 9.40 -12 -26 2 69.49 8.90 -12 26 -1 12.70 7.10 12 -26 1 17.60 6.10 -11 26 -1 69.59 9.90 11 -26 1 65.69 8.00 -10 26 -1 91.59 11.40 10 -26 1 103.59 9.10 -9 26 -1 1.00 6.10 9 -26 1 7.60 4.70 8 -26 1 17.90 5.10 7 -26 1 147.79 9.30 6 -26 1 11.60 4.40 5 -26 1 257.27 13.20 4 -26 1 258.67 12.70 3 -26 1 3.20 3.60 2 -26 1 110.89 7.30 1 -26 1 254.67 12.20 0 -26 1 26.30 4.50 -1 -26 1 49.80 4.90 -1 -26 1 51.09 5.60 -2 -26 1 130.59 7.90 -2 -26 1 122.69 7.40 -3 -26 1 23.50 4.30 -3 -26 1 29.30 4.20 -4 -26 1 94.79 6.40 -4 -26 1 93.59 6.40 -5 -26 1 273.07 12.30 -5 -26 1 268.17 12.70 -6 -26 1 115.59 8.30 -7 -26 1 172.98 10.30 -8 -26 1 114.29 8.80 -9 -26 1 46.10 6.80 -10 -26 1 36.00 6.60 -11 -26 1 39.40 7.20 -12 -26 1 70.39 9.00 -12 26 0 52.79 9.00 12 -26 0 55.59 7.60 -11 26 0 100.69 11.20 11 -26 0 96.89 9.30 -10 26 0 0.80 6.00 10 -26 0 8.10 4.60 -9 26 0 50.89 8.80 9 -26 0 61.29 7.00 -8 26 0 143.69 12.70 8 -26 0 139.09 9.10 7 -26 0 37.60 5.60 6 -26 0 200.38 11.30 5 -26 0 228.18 11.60 4 -26 0 46.30 5.20 3 -26 0 67.59 6.20 2 -26 0 57.49 5.20 1 -26 0 137.69 8.50 0 -26 0 169.28 9.40 -1 -26 0 133.89 7.40 -1 -26 0 135.09 8.30 -2 -26 0 53.39 4.90 -2 -26 0 59.89 5.40 -3 -26 0 68.69 6.00 -3 -26 0 69.79 5.80 -4 -26 0 53.29 5.50 -4 -26 0 57.69 6.00 -5 -26 0 248.18 11.30 -5 -26 0 249.97 12.20 -6 -26 0 213.88 11.40 -7 -26 0 33.90 5.10 -8 -26 0 164.88 10.30 -9 -26 0 64.19 7.30 -10 -26 0 4.60 5.30 -11 -26 0 123.49 10.20 -12 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4 -26 -2 12.50 4.10 3 -26 -2 165.08 9.40 2 -26 -2 175.58 9.40 1 -26 -2 59.29 6.10 0 -26 -2 368.06 14.90 0 -26 -2 333.57 15.20 -1 -26 -2 192.28 9.90 -1 -26 -2 198.18 9.40 -2 -26 -2 5.70 3.40 -2 -26 -2 5.90 3.30 -3 -26 -2 423.36 17.50 -3 -26 -2 418.36 17.00 -4 -26 -2 192.58 10.40 -4 -26 -2 199.08 10.00 -5 -26 -2 37.10 5.60 -6 -26 -2 123.79 8.50 -7 -26 -2 62.79 7.00 -8 -26 -2 52.59 6.60 -9 -26 -2 77.69 8.00 -10 -26 -2 20.90 6.40 -11 -26 -2 32.20 7.10 -12 26 3 80.09 10.10 12 -26 -3 84.09 8.70 -11 26 3 -1.20 5.50 11 -26 -3 0.50 4.60 -10 26 3 74.49 9.10 10 -26 -3 74.09 7.70 -9 26 3 72.29 9.80 9 -26 -3 82.49 7.80 -8 26 3 46.10 7.50 8 -26 -3 60.19 7.10 7 -26 -3 241.98 12.70 6 -26 -3 194.38 11.50 5 -26 -3 66.99 6.20 4 -26 -3 24.60 4.40 3 -26 -3 78.59 7.00 2 -26 -3 99.39 7.70 1 -26 -3 427.66 17.70 0 -26 -3 282.27 13.50 0 -26 -3 314.27 13.50 -1 -26 -3 91.69 6.80 -1 -26 -3 91.59 6.90 -2 -26 -3 196.38 10.20 -2 -26 -3 193.88 10.00 -3 -26 -3 15.80 4.00 -3 -26 -3 21.30 4.80 -4 -26 -3 71.09 6.80 -4 -26 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26.70 6.10 -4 -27 11 32.50 6.30 -5 -27 11 173.78 11.20 -5 -27 11 183.48 11.80 -6 -27 11 11.80 5.80 -6 -27 11 7.70 5.00 -7 -27 11 108.29 9.50 -7 -27 11 100.89 9.10 -8 -27 11 10.30 5.80 -9 -27 11 0.10 5.40 4 -27 10 -4.60 4.80 3 -27 10 36.40 6.90 2 -27 10 52.29 8.00 1 -27 10 4.40 5.40 0 -27 10 149.19 11.30 -1 -27 10 21.00 5.30 -2 -27 10 7.40 5.10 -3 -27 10 54.09 6.90 -4 -27 10 13.10 5.20 -4 -27 10 17.40 5.10 -5 -27 10 14.50 5.10 -5 -27 10 17.70 5.50 -6 -27 10 198.38 12.30 -6 -27 10 224.58 12.50 -7 -27 10 6.10 5.30 -7 -27 10 5.30 4.50 -8 -27 10 55.19 7.90 -9 -27 10 32.70 7.10 -10 -27 10 23.20 6.90 6 -27 9 1.20 6.10 5 -27 9 31.70 7.60 4 -27 9 35.20 7.40 3 -27 9 29.80 6.20 2 -27 9 -4.50 4.80 1 -27 9 116.39 9.90 0 -27 9 3.90 4.80 -1 -27 9 84.29 8.60 -2 -27 9 178.88 11.40 -3 -27 9 14.60 4.70 -3 -27 9 17.00 4.90 -4 -27 9 -2.50 4.50 -4 -27 9 -1.50 4.20 -5 -27 9 297.67 15.10 -5 -27 9 313.77 15.20 -6 -27 9 26.60 6.20 -6 -27 9 24.70 5.50 -7 -27 9 51.29 7.80 -7 -27 9 54.89 6.80 -8 -27 9 106.19 9.50 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-29 4 57.89 6.80 -1 -29 4 109.29 8.10 -2 -29 4 16.10 4.40 -3 -29 4 -0.80 3.50 -3 -29 4 0.60 3.80 -4 -29 4 264.77 12.70 -4 -29 4 238.98 12.10 -5 -29 4 4.40 4.30 -5 -29 4 2.40 4.20 -6 -29 4 61.89 6.90 -7 -29 4 15.20 5.30 -8 -29 4 67.09 7.80 -9 -29 4 3.30 5.20 -10 -29 4 163.38 11.80 -11 -29 4 5.20 6.00 9 -29 3 195.78 13.80 8 -29 3 9.60 4.80 7 -29 3 71.29 8.50 6 -29 3 49.10 6.70 5 -29 3 48.10 6.50 4 -29 3 3.80 3.60 3 -29 3 135.39 9.60 1 -29 3 283.97 14.00 0 -29 3 31.90 5.20 -1 -29 3 11.00 4.10 -2 -29 3 4.30 3.70 -3 -29 3 41.00 5.20 -3 -29 3 35.70 5.20 -4 -29 3 14.40 4.20 -4 -29 3 11.30 4.80 -5 -29 3 205.48 11.40 -5 -29 3 231.28 11.70 -6 -29 3 9.40 4.60 -7 -29 3 -0.80 4.40 -8 -29 3 7.70 5.00 -9 -29 3 106.89 9.50 -10 -29 3 9.70 6.00 -11 -29 3 211.68 13.70 9 -29 2 3.10 5.40 8 -29 2 168.38 11.80 7 -29 2 22.10 5.70 6 -29 2 -2.80 4.00 5 -29 2 8.60 4.40 4 -29 2 71.89 6.60 3 -29 2 34.10 5.10 2 -29 2 548.75 22.80 1 -29 2 98.69 7.80 0 -29 2 11.60 4.10 -1 -29 2 -0.60 3.30 -2 -29 2 20.40 4.20 -3 -29 2 23.60 4.60 -3 -29 2 21.70 4.90 -4 -29 2 504.25 20.40 -4 -29 2 466.05 19.90 -5 -29 2 18.30 4.20 -5 -29 2 15.50 4.70 -6 -29 2 0.60 4.10 -7 -29 2 10.30 4.90 -8 -29 2 10.80 5.30 -9 -29 2 60.09 7.80 -10 -29 2 312.07 16.70 -11 -29 2 19.80 7.10 10 -29 1 17.30 6.10 9 -29 1 199.88 13.10 8 -29 1 51.39 7.10 7 -29 1 25.60 5.80 6 -29 1 13.50 4.70 5 -29 1 50.39 5.90 4 -29 1 35.30 5.50 3 -29 1 484.45 20.20 2 -29 1 11.80 4.60 1 -29 1 108.59 7.90 0 -29 1 54.19 6.10 -1 -29 1 32.40 4.90 -2 -29 1 55.79 5.80 -3 -29 1 280.47 12.80 -3 -29 1 272.87 13.30 -4 -29 1 21.70 4.40 -4 -29 1 12.90 5.10 -5 -29 1 78.59 7.00 -6 -29 1 5.10 4.50 -7 -29 1 12.80 4.90 -8 -29 1 23.30 5.80 -9 -29 1 191.58 12.20 -10 -29 1 18.90 6.70 -11 -29 1 154.98 11.90 10 -29 0 273.57 15.80 9 -29 0 22.00 5.50 8 -29 0 67.79 7.70 7 -29 0 14.80 5.00 6 -29 0 9.50 3.90 5 -29 0 17.60 4.80 4 -29 0 230.98 12.40 3 -29 0 10.80 4.10 2 -29 0 130.99 8.40 1 -29 0 27.40 4.80 0 -29 0 -1.20 3.40 -1 -29 0 33.70 5.00 -2 -29 0 149.69 8.60 -2 -29 0 146.09 8.80 -3 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-1 -29 -4 6.60 4.60 -2 -29 -4 485.85 20.40 -2 -29 -4 500.45 20.70 -3 -29 -4 25.00 5.10 -3 -29 -4 26.70 5.40 -4 -29 -4 60.09 6.80 -5 -29 -4 6.90 4.80 -6 -29 -4 25.50 6.10 -7 -29 -4 32.50 6.70 -8 -29 -4 214.18 13.20 11 -29 -5 171.88 12.40 10 -29 -5 5.40 5.50 9 -29 -5 39.70 6.60 8 -29 -5 8.50 5.00 7 -29 -5 4.40 4.00 6 -29 -5 30.60 5.80 5 -29 -5 305.57 15.10 4 -29 -5 64.19 7.30 3 -29 -5 23.90 5.40 2 -29 -5 2.70 3.60 1 -29 -5 5.80 4.30 0 -29 -5 29.40 5.40 -1 -29 -5 396.46 18.00 -1 -29 -5 430.06 18.60 -2 -29 -5 1.50 4.80 -2 -29 -5 5.60 4.90 -3 -29 -5 95.39 8.00 -4 -29 -5 0.90 4.60 -5 -29 -5 11.40 5.30 -6 -29 -5 52.19 7.30 -7 -29 -5 152.38 11.20 -8 -29 -5 3.90 6.40 11 -29 -6 2.70 5.80 10 -29 -6 106.69 9.90 9 -29 -6 10.80 5.50 8 -29 -6 1.00 4.80 7 -29 -6 9.10 4.60 6 -29 -6 213.08 12.10 5 -29 -6 9.60 5.10 4 -29 -6 66.89 7.70 3 -29 -6 20.10 5.20 1 -29 -6 49.20 6.60 0 -29 -6 188.38 11.30 -1 -29 -6 11.30 5.30 -1 -29 -6 7.50 4.80 -2 -29 -6 236.78 12.70 -2 -29 -6 227.88 13.40 -3 -29 -6 5.10 5.00 -4 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25.90 5.80 -2 -30 8 103.59 8.90 -3 -30 8 2.70 4.60 -4 -30 8 -2.60 4.50 -5 -30 8 146.59 10.00 -5 -30 8 139.09 10.00 -6 -30 8 1.50 4.30 -6 -30 8 -2.10 4.80 -7 -30 8 100.69 10.40 -8 -30 8 147.89 11.30 -9 -30 8 -2.70 5.60 5 -30 7 132.29 11.60 4 -30 7 8.30 5.60 3 -30 7 11.70 5.50 2 -30 7 131.59 10.30 1 -30 7 1.50 4.70 0 -30 7 23.30 5.60 -1 -30 7 85.49 8.20 -2 -30 7 -0.40 4.20 -3 -30 7 14.30 4.80 -4 -30 7 168.18 10.70 -5 -30 7 16.70 5.50 -5 -30 7 17.80 5.40 -6 -30 7 55.49 7.40 -6 -30 7 56.79 7.60 -7 -30 7 108.29 9.50 -8 -30 7 27.20 6.90 -9 -30 7 47.10 7.80 6 -30 6 62.69 8.40 5 -30 6 -0.50 4.20 4 -30 6 21.40 5.20 3 -30 6 28.40 5.50 2 -30 6 21.10 5.80 1 -30 6 72.29 7.10 0 -30 6 108.59 9.00 -1 -30 6 18.10 4.60 -2 -30 6 22.40 4.70 -3 -30 6 31.20 5.50 -4 -30 6 30.50 6.00 -5 -30 6 237.28 12.70 -5 -30 6 253.27 13.60 -6 -30 6 15.00 6.10 -7 -30 6 24.10 6.10 -8 -30 6 129.59 10.30 -9 -30 6 16.80 6.50 -10 -30 6 31.60 7.40 7 -30 5 13.00 5.90 6 -30 5 28.30 5.80 5 -30 5 47.20 7.20 4 -30 5 25.80 5.90 3 -30 5 10.80 4.90 2 -30 5 121.49 9.50 1 -30 5 9.50 4.80 0 -30 5 71.09 7.60 -1 -30 5 193.68 11.30 -2 -30 5 46.40 6.10 -3 -30 5 17.20 4.80 -4 -30 5 142.49 9.50 -4 -30 5 132.39 9.30 -5 -30 5 8.30 5.20 -5 -30 5 10.20 4.40 -6 -30 5 100.59 8.50 -7 -30 5 146.79 10.40 -8 -30 5 10.80 5.60 -9 -30 5 58.09 8.10 -10 -30 5 143.69 11.40 8 -30 4 -0.80 5.40 7 -30 4 60.19 8.20 6 -30 4 144.69 11.10 5 -30 4 12.90 5.20 4 -30 4 19.70 5.40 3 -30 4 92.89 7.80 2 -30 4 7.40 4.00 1 -30 4 92.59 8.20 0 -30 4 167.08 9.90 -1 -30 4 6.10 4.20 -2 -30 4 6.20 4.00 -3 -30 4 173.38 10.30 -4 -30 4 66.09 7.00 -4 -30 4 61.49 6.70 -5 -30 4 78.89 7.00 -5 -30 4 72.49 7.20 -6 -30 4 141.19 9.70 -7 -30 4 12.50 5.40 -8 -30 4 43.40 7.30 -9 -30 4 26.10 6.50 -10 -30 4 41.50 7.80 8 -30 3 105.29 9.90 7 -30 3 64.89 7.40 6 -30 3 5.50 4.70 5 -30 3 24.20 5.40 4 -30 3 44.90 5.90 3 -30 3 41.10 5.60 2 -30 3 173.18 10.20 1 -30 3 115.29 8.80 0 -30 3 43.90 6.00 -1 -30 3 80.79 7.30 -2 -30 3 45.80 5.80 -3 -30 3 41.10 5.50 -4 -30 3 146.29 9.10 -4 -30 3 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181.78 11.30 -4 -32 5 -2.30 4.20 -5 -32 5 22.30 5.40 -5 -32 5 21.90 5.00 -6 -32 5 14.40 5.40 -7 -32 5 139.89 11.10 -8 -32 5 11.00 6.20 6 -32 4 87.59 9.40 5 -32 4 5.40 5.10 4 -32 4 150.88 10.30 3 -32 4 3.10 4.60 2 -32 4 -3.00 4.00 1 -32 4 4.10 4.40 0 -32 4 157.18 9.90 -1 -32 4 19.50 5.40 -2 -32 4 349.87 17.00 -3 -32 4 7.10 4.70 -4 -32 4 2.30 4.30 -5 -32 4 -3.30 4.00 -6 -32 4 44.50 6.70 -7 -32 4 5.60 5.50 -8 -32 4 182.78 12.90 7 -32 3 78.29 9.10 6 -32 3 14.20 5.70 5 -32 3 212.98 12.30 4 -32 3 29.50 6.00 3 -32 3 10.30 4.80 2 -32 3 -5.20 3.80 1 -32 3 34.60 5.90 0 -32 3 16.50 5.20 -1 -32 3 290.87 14.00 -2 -32 3 9.20 4.90 -3 -32 3 38.20 6.20 -4 -32 3 5.80 4.20 -5 -32 3 25.10 5.30 -6 -32 3 2.80 4.60 -7 -32 3 193.88 12.00 -8 -32 3 6.00 6.00 7 -32 2 5.80 4.60 6 -32 2 241.68 13.50 5 -32 2 16.10 5.40 4 -32 2 96.19 8.10 3 -32 2 1.80 4.30 2 -32 2 21.50 5.10 1 -32 2 6.60 4.40 0 -32 2 274.47 14.40 -1 -32 2 6.60 4.80 -2 -32 2 77.89 7.50 -3 -32 2 -3.30 3.70 -4 -32 2 -1.60 3.70 -5 -32 2 2.60 4.70 -6 -32 2 122.49 9.30 -7 -32 2 9.00 6.10 -8 -32 2 201.38 13.50 8 -32 1 1.90 5.10 7 -32 1 201.98 12.90 6 -32 1 9.70 5.50 5 -32 1 101.79 8.30 4 -32 1 1.70 3.70 3 -32 1 9.10 4.50 2 -32 1 3.00 4.30 1 -32 1 52.29 7.00 0 -32 1 27.10 5.80 -1 -32 1 401.76 18.20 -2 -32 1 23.80 5.10 -3 -32 1 1.90 3.80 -4 -32 1 2.40 4.00 -4 -32 1 0.20 3.70 -5 -32 1 59.69 6.60 -6 -32 1 21.70 5.70 -7 -32 1 301.57 16.10 -8 -32 1 10.20 5.90 8 -32 0 45.10 7.30 7 -32 0 19.30 5.80 6 -32 0 313.17 16.20 5 -32 0 12.30 5.00 4 -32 0 16.90 4.90 3 -32 0 7.80 3.80 2 -32 0 19.80 5.10 1 -32 0 11.40 4.70 0 -32 0 343.27 15.60 -1 -32 0 11.20 4.70 -2 -32 0 21.40 5.30 -3 -32 0 6.10 4.40 -4 -32 0 23.70 5.30 -5 -32 0 13.00 5.30 -6 -32 0 342.27 16.40 -7 -32 0 25.30 6.90 -8 -32 0 60.69 8.20 8 -32 -1 8.70 5.50 7 -32 -1 272.57 15.30 6 -32 -1 23.50 5.90 5 -32 -1 60.19 7.40 4 -32 -1 3.10 4.20 3 -32 -1 2.80 3.70 2 -32 -1 24.00 5.20 1 -32 -1 401.96 18.30 0 -32 -1 31.80 5.80 -1 -32 -1 54.49 6.80 -2 -32 -1 3.90 4.10 -3 -32 -1 6.70 4.40 -4 -32 -1 10.70 4.90 -5 -32 -1 109.39 8.70 -7 -32 -1 212.88 13.30 -8 -32 -1 -3.90 5.10 9 -32 -2 3.80 5.20 8 -32 -2 177.38 12.30 7 -32 -2 5.40 4.70 6 -32 -2 112.89 8.80 5 -32 -2 1.70 4.40 4 -32 -2 3.50 3.60 3 -32 -2 0.60 4.20 2 -32 -2 67.39 6.70 1 -32 -2 2.20 5.10 0 -32 -2 268.17 13.90 -1 -32 -2 7.00 4.50 -2 -32 -2 20.00 4.90 -3 -32 -2 9.00 4.20 -4 -32 -2 110.39 8.50 -5 -32 -2 6.40 5.20 -6 -32 -2 267.57 14.40 -7 -32 -2 4.60 6.10 9 -32 -3 42.60 6.70 8 -32 -3 10.90 5.80 7 -32 -3 185.08 12.50 6 -32 -3 -0.90 4.70 5 -32 -3 24.00 5.80 4 -32 -3 7.90 4.80 3 -32 -3 42.80 5.90 2 -32 -3 7.40 4.40 1 -32 -3 310.57 15.60 0 -32 -3 10.90 5.10 -1 -32 -3 43.30 6.10 -2 -32 -3 0.10 3.90 -4 -32 -3 19.70 5.90 -5 -32 -3 228.68 13.00 -6 -32 -3 5.30 5.80 -7 -32 -3 77.39 9.50 8 -32 -4 170.78 12.10 7 -32 -4 1.90 4.50 6 -32 -4 41.50 6.80 5 -32 -4 7.70 5.00 4 -32 -4 9.80 4.80 3 -32 -4 13.60 5.30 2 -32 -4 344.17 16.80 1 -32 -4 6.60 5.20 0 -32 -4 161.98 10.70 -1 -32 -4 2.20 4.30 -2 -32 -4 -0.40 4.30 -3 -32 -4 12.70 5.40 -4 -32 -4 175.88 11.20 -5 -32 -4 0.00 5.50 -6 -32 -4 100.59 9.50 8 -32 -5 9.30 6.10 7 -32 -5 115.29 10.10 6 -32 -5 13.70 5.50 5 -32 -5 27.80 5.70 4 -32 -5 6.70 4.30 3 -32 -5 194.38 12.30 2 -32 -5 6.70 5.30 1 -32 -5 219.48 12.80 0 -32 -5 -3.10 4.20 -1 -32 -5 45.60 6.60 -2 -32 -5 4.90 4.80 -3 -32 -5 75.09 8.70 -4 -32 -5 2.70 5.50 -5 -32 -5 155.78 11.30 8 -32 -6 165.18 12.20 7 -32 -6 2.50 5.60 6 -32 -6 22.10 6.10 5 -32 -6 6.10 4.90 4 -32 -6 46.80 7.00 3 -32 -6 3.00 4.60 2 -32 -6 287.67 15.30 1 -32 -6 -1.80 4.90 0 -32 -6 59.49 7.30 -1 -32 -6 1.80 4.50 -3 -32 -6 5.50 6.20 -4 -32 -6 159.38 11.60 7 -32 -7 81.29 9.40 6 -32 -7 5.40 5.60 5 -32 -7 1.20 4.30 4 -32 -7 16.90 5.90 3 -32 -7 231.08 14.00 2 -32 -7 16.20 6.10 1 -32 -7 191.88 12.60 0 -32 -7 -1.20 4.60 -1 -32 -7 18.60 5.70 -3 -32 -7 207.78 14.20 6 -32 -8 21.30 6.60 5 -32 -8 -0.80 5.40 4 -32 -8 146.49 11.20 3 -32 -8 8.40 5.80 2 -32 -8 199.58 13.10 1 -32 -8 9.60 5.90 0 -32 -8 67.59 8.40 -1 -32 -8 10.00 5.70 5 -32 -9 64.99 8.90 4 -32 -9 10.40 6.30 3 -32 -9 178.18 12.80 0 -33 8 12.50 5.60 -1 -33 8 83.59 9.10 -2 -33 8 4.50 4.40 -3 -33 8 119.39 10.10 -4 -33 8 17.80 5.50 2 -33 7 5.70 4.70 1 -33 7 -1.70 4.80 0 -33 7 48.50 6.60 -1 -33 7 4.00 5.10 -2 -33 7 115.09 9.80 -3 -33 7 4.10 5.00 -4 -33 7 56.49 7.40 -5 -33 7 26.50 5.70 3 -33 6 111.49 10.30 2 -33 6 10.90 5.60 1 -33 6 19.00 5.80 0 -33 6 5.20 4.90 -1 -33 6 121.49 9.90 -2 -33 6 8.80 5.10 -3 -33 6 175.88 11.40 -4 -33 6 22.20 5.30 -5 -33 6 9.10 5.30 -6 -33 6 14.30 5.90 -7 -33 6 102.39 9.30 4 -33 5 146.79 11.60 3 -33 5 11.30 4.80 2 -33 5 7.50 4.30 1 -33 5 14.30 5.20 0 -33 5 50.79 6.40 -1 -33 5 12.70 4.60 -2 -33 5 324.07 16.40 -3 -33 5 43.60 6.40 -4 -33 5 11.70 4.80 -6 -33 5 54.29 7.10 -7 -33 5 13.00 5.80 5 -33 4 112.39 9.40 4 -33 4 13.20 5.70 3 -33 4 26.10 5.40 2 -33 4 17.00 5.30 1 -33 4 63.99 7.60 0 -33 4 5.80 4.60 -1 -33 4 245.38 12.90 -2 -33 4 14.00 5.00 -3 -33 4 87.19 8.20 -4 -33 4 10.80 4.70 -6 -33 4 30.00 6.50 -7 -33 4 204.88 13.30 6 -33 3 113.79 10.50 5 -33 3 1.90 4.20 4 -33 3 93.89 9.10 3 -33 3 9.10 5.00 2 -33 3 32.30 5.70 1 -33 3 11.30 4.80 0 -33 3 149.79 10.50 -1 -33 3 7.80 5.00 -2 -33 3 265.17 13.90 -3 -33 3 69.09 7.60 -4 -33 3 3.20 4.60 -6 -33 3 47.30 7.20 -7 -33 3 7.80 5.70 -8 -33 3 166.68 11.80 6 -33 2 7.30 5.40 5 -33 2 127.79 10.50 4 -33 2 2.70 4.00 3 -33 2 1.50 4.30 2 -33 2 14.50 4.80 1 -33 2 64.59 7.40 0 -33 2 13.60 5.10 -1 -33 2 311.37 15.70 -2 -33 2 46.40 6.30 -3 -33 2 43.40 6.00 -4 -33 2 16.00 5.00 -5 -33 2 21.60 5.60 -6 -33 2 22.40 6.40 -7 -33 2 259.97 14.30 -8 -33 2 34.90 7.20 7 -33 1 18.40 5.90 6 -33 1 166.38 10.90 5 -33 1 16.30 5.50 4 -33 1 18.80 4.70 3 -33 1 3.10 4.40 2 -33 1 30.30 5.80 1 -33 1 11.20 4.90 0 -33 1 379.46 18.00 -1 -33 1 36.40 6.10 -2 -33 1 64.09 7.30 -3 -33 1 8.50 4.40 -5 -33 1 13.50 5.20 -6 -33 1 185.58 12.10 -7 -33 1 4.10 5.60 7 -33 0 139.69 11.30 6 -33 0 8.90 4.70 5 -33 0 87.59 8.60 4 -33 0 17.00 4.50 3 -33 0 8.60 4.30 2 -33 0 10.90 4.00 1 -33 0 179.18 11.30 0 -33 0 8.90 5.00 -1 -33 0 183.88 11.20 -2 -33 0 12.70 4.70 -3 -33 0 9.30 4.20 -5 -33 0 87.69 7.70 -6 -33 0 8.90 6.00 -7 -33 0 153.88 11.70 7 -33 -1 9.20 4.80 6 -33 -1 138.49 9.90 5 -33 -1 8.80 4.20 4 -33 -1 3.50 4.30 3 -33 -1 13.70 4.80 2 -33 -1 64.59 6.70 1 -33 -1 28.80 5.40 0 -33 -1 375.66 17.60 -1 -33 -1 12.80 4.90 -2 -33 -1 24.80 5.30 -3 -33 -1 0.50 3.80 -5 -33 -1 22.10 5.60 -6 -33 -1 217.68 13.40 -7 -33 -1 20.00 6.80 7 -33 -2 211.68 12.60 6 -33 -2 10.40 4.80 5 -33 -2 21.30 5.50 4 -33 -2 16.40 5.00 3 -33 -2 40.40 6.30 2 -33 -2 52.29 7.00 1 -33 -2 321.67 16.20 0 -33 -2 10.00 5.30 -1 -33 -2 69.09 7.50 -2 -33 -2 11.10 4.50 -5 -33 -2 136.19 10.40 -6 -33 -2 4.00 5.60 7 -33 -3 7.10 5.80 6 -33 -3 35.30 6.60 5 -33 -3 21.90 5.80 4 -33 -3 6.10 4.80 3 -33 -3 69.19 7.30 2 -33 -3 240.98 13.20 1 -33 -3 6.30 5.20 0 -33 -3 154.48 10.80 -1 -33 -3 10.40 4.80 -2 -33 -3 39.90 5.90 -4 -33 -3 128.49 9.90 -5 -33 -3 3.00 5.80 -6 -33 -3 128.39 10.60 7 -33 -4 172.48 12.20 6 -33 -4 26.60 6.30 5 -33 -4 1.80 4.80 4 -33 -4 13.10 5.10 3 -33 -4 94.49 8.90 2 -33 -4 12.60 5.70 1 -33 -4 257.57 14.20 0 -33 -4 3.00 4.60 -1 -33 -4 73.59 8.40 -2 -33 -4 8.90 4.50 -4 -33 -4 22.90 6.50 -5 -33 -4 139.39 10.60 7 -33 -5 5.80 5.70 6 -33 -5 48.80 6.80 5 -33 -5 27.70 6.10 4 -33 -5 11.90 4.80 3 -33 -5 35.90 6.00 2 -33 -5 337.57 16.70 1 -33 -5 21.20 5.80 0 -33 -5 58.79 7.70 -1 -33 -5 22.50 5.40 -4 -33 -5 181.68 12.50 6 -33 -6 15.20 5.20 5 -33 -6 4.70 5.20 4 -33 -6 24.40 6.20 3 -33 -6 191.98 12.40 2 -33 -6 11.00 5.80 1 -33 -6 134.19 10.60 0 -33 -6 13.00 5.50 -1 -33 -6 23.30 6.00 6 -33 -7 23.70 6.00 5 -33 -7 34.40 7.10 4 -33 -7 68.09 8.90 3 -33 -7 11.50 5.80 2 -33 -7 131.29 10.60 1 -33 -7 6.90 5.60 0 -33 -7 66.59 8.30 -1 -33 -7 -1.60 4.90 4 -33 -8 18.90 5.90 3 -33 -8 153.98 11.90 2 -33 -8 16.30 5.40 1 -33 -8 101.79 9.90 0 -33 -8 15.30 6.30 -1 -34 7 69.59 8.50 -2 -34 7 21.20 6.10 -3 -34 7 60.99 7.90 2 -34 6 6.60 5.20 1 -34 6 64.09 7.40 0 -34 6 24.20 6.20 -1 -34 6 31.60 6.40 -2 -34 6 76.89 8.50 -3 -34 6 24.40 5.90 -4 -34 6 23.00 6.30 3 -34 5 34.10 7.10 2 -34 5 118.89 10.30 1 -34 5 3.60 4.80 0 -34 5 27.00 6.10 -1 -34 5 163.38 11.30 -2 -34 5 7.70 5.30 -3 -34 5 45.10 6.80 -4 -34 5 69.09 7.90 4 -34 4 50.99 7.60 3 -34 4 95.49 9.70 2 -34 4 5.40 4.90 1 -34 4 70.19 8.10 0 -34 4 63.49 8.00 -1 -34 4 24.30 5.80 -2 -34 4 115.19 9.40 -3 -34 4 81.39 9.00 -4 -34 4 -2.30 4.60 5 -34 3 57.89 7.60 4 -34 3 81.19 8.70 3 -34 3 22.30 5.80 2 -34 3 37.60 5.80 1 -34 3 70.49 7.90 0 -34 3 50.49 7.00 -1 -34 3 123.39 9.70 -2 -34 3 78.49 8.20 -3 -34 3 22.80 5.30 -4 -34 3 29.50 5.50 -6 -34 3 46.50 6.90 5 -34 2 8.80 4.70 4 -34 2 11.40 4.80 3 -34 2 51.89 7.00 2 -34 2 5.60 4.10 1 -34 2 42.40 5.80 0 -34 2 121.39 9.60 -1 -34 2 10.00 5.20 -2 -34 2 101.49 8.90 -3 -34 2 79.09 7.90 -6 -34 2 69.89 7.70 6 -34 1 0.40 4.90 5 -34 1 75.59 8.50 4 -34 1 48.90 6.90 3 -34 1 -0.80 4.30 2 -34 1 44.50 6.50 1 -34 1 77.39 8.00 0 -34 1 13.00 5.40 -1 -34 1 88.89 8.50 -2 -34 1 83.29 8.10 -3 -34 1 24.50 5.40 -6 -34 1 28.50 6.60 6 -34 0 85.69 9.20 5 -34 0 48.00 7.40 4 -34 0 27.90 5.70 3 -34 0 19.80 5.40 2 -34 0 20.60 5.40 1 -34 0 48.00 6.90 0 -34 0 195.68 12.10 -1 -34 0 47.50 6.70 -2 -34 0 22.00 5.50 -3 -34 0 20.90 5.00 -6 -34 0 93.59 9.30 6 -34 -1 16.00 5.80 5 -34 -1 40.00 6.90 4 -34 -1 21.10 5.00 3 -34 -1 21.80 5.50 2 -34 -1 89.29 8.60 1 -34 -1 81.89 8.40 0 -34 -1 14.00 5.30 -1 -34 -1 78.79 8.10 -2 -34 -1 53.59 7.10 -5 -34 -1 79.29 8.50 -6 -34 -1 -0.30 5.60 6 -34 -2 67.39 8.50 5 -34 -2 24.80 5.50 4 -34 -2 7.60 4.90 3 -34 -2 59.79 6.80 2 -34 -2 127.19 9.90 1 -34 -2 14.10 5.40 0 -34 -2 142.19 10.20 -2 -34 -2 6.50 4.60 -5 -34 -2 13.70 6.00 6 -34 -3 35.90 6.60 5 -34 -3 -0.60 4.90 4 -34 -3 30.30 6.10 3 -34 -3 30.20 6.20 2 -34 -3 70.19 8.40 1 -34 -3 117.89 9.80 0 -34 -3 62.69 7.90 -1 -34 -3 68.89 7.80 -2 -34 -3 42.60 6.10 -5 -34 -3 80.49 9.00 6 -34 -4 42.40 7.30 5 -34 -4 42.40 7.10 4 -34 -4 3.20 5.00 3 -34 -4 69.69 8.20 2 -34 -4 124.09 10.10 1 -34 -4 31.40 6.30 0 -34 -4 82.39 8.50 -1 -34 -4 72.59 7.90 6 -34 -5 6.90 4.90 5 -34 -5 4.00 4.70 4 -34 -5 60.99 8.10 3 -34 -5 44.10 7.00 2 -34 -5 9.80 5.50 1 -34 -5 190.78 12.20 0 -34 -5 32.90 6.30 -1 -34 -5 1.70 4.90 5 -34 -6 49.10 7.00 4 -34 -6 16.60 5.60 3 -34 -6 22.40 6.20 2 -34 -6 78.49 7.80 1 -34 -6 37.00 6.90 0 -34 -6 36.60 6.90 -1 -34 -6 73.79 8.50 3 -34 -7 70.79 8.90 2 -34 -7 33.70 6.80 1 -34 -7 86.29 9.30 1 -35 5 91.39 9.40 0 -35 5 46.30 7.20 -1 -35 5 5.90 5.40 -2 -35 5 0.10 4.70 -3 -35 5 63.59 8.10 -4 -35 5 31.00 6.60 2 -35 4 99.19 8.70 1 -35 4 11.50 5.30 0 -35 4 44.50 7.00 -1 -35 4 60.29 8.00 -2 -35 4 27.40 6.00 -3 -35 4 21.40 5.70 3 -35 3 144.79 11.10 2 -35 3 5.00 5.20 1 -35 3 89.99 8.90 0 -35 3 44.20 7.00 -1 -35 3 7.70 5.20 -2 -35 3 15.70 5.50 -3 -35 3 89.79 8.60 4 -35 2 101.99 8.90 3 -35 2 13.10 5.60 2 -35 2 65.59 7.00 1 -35 2 41.60 6.70 0 -35 2 4.50 5.00 -1 -35 2 -2.20 4.40 -2 -35 2 124.19 9.80 -3 -35 2 36.30 6.20 4 -35 1 56.49 7.80 3 -35 1 57.49 6.90 2 -35 1 11.00 4.40 1 -35 1 34.70 6.40 0 -35 1 6.10 4.90 -1 -35 1 12.10 4.90 -2 -35 1 55.29 7.10 -3 -35 1 95.09 8.50 5 -35 0 47.30 6.80 3 -35 0 -2.60 4.80 2 -35 0 104.89 9.30 1 -35 0 9.10 5.10 0 -35 0 4.40 4.80 -1 -35 0 14.90 5.40 -2 -35 0 108.29 9.20 5 -35 -1 85.79 8.40 4 -35 -1 24.40 6.20 3 -35 -1 95.09 9.00 2 -35 -1 47.10 6.90 1 -35 -1 10.20 5.00 0 -35 -1 8.80 4.80 -1 -35 -1 49.70 6.80 -2 -35 -1 8.80 5.10 5 -35 -2 21.40 6.40 4 -35 -2 49.60 6.80 3 -35 -2 33.50 6.60 2 -35 -2 115.69 9.80 1 -35 -2 2.30 5.00 0 -35 -2 7.40 5.00 -1 -35 -2 44.40 6.50 -2 -35 -2 83.39 8.50 4 -35 -3 4.10 5.20 3 -35 -3 97.79 9.40 2 -35 -3 11.70 5.40 1 -35 -3 12.50 5.10 0 -35 -3 53.29 7.10 -1 -35 -3 86.89 8.70 4 -35 -4 136.09 10.90 3 -35 -4 23.80 6.50 2 -35 -4 26.60 6.00 1 -35 -4 62.29 7.80 0 -35 -4 39.60 6.60 -1 -35 -4 14.20 5.50 4 -35 -5 24.40 6.80 3 -35 -5 51.49 7.60 2 -35 -5 3.00 5.00 1 -35 -5 13.80 5.50 0 -35 -5 51.49 7.30 -1 -35 -5 85.49 9.80 1 -36 3 9.30 5.60 0 -36 3 5.80 5.00 -1 -36 3 1.80 4.80 -2 -36 3 63.99 8.00 -3 -36 3 7.50 5.20 2 -36 2 16.40 5.20 1 -36 2 51.29 7.40 0 -36 2 -0.70 4.40 -1 -36 2 8.50 4.80 -2 -36 2 3.80 4.90 -3 -36 2 151.88 10.60 3 -36 1 6.50 4.60 2 -36 1 153.18 10.40 1 -36 1 2.00 4.90 0 -36 1 3.50 4.60 -1 -36 1 0.20 4.40 -2 -36 1 84.59 8.60 3 -36 0 160.28 10.90 2 -36 0 12.70 5.80 1 -36 0 14.70 4.90 0 -36 0 0.20 4.60 -1 -36 0 14.60 5.20 3 -36 -1 12.90 5.90 2 -36 -1 83.89 8.90 1 -36 -1 2.60 4.70 0 -36 -1 3.70 4.80 -1 -36 -1 1.30 4.90 -2 -36 -1 176.38 12.50 3 -36 -2 136.39 10.10 2 -36 -2 3.10 5.20 1 -36 -2 11.30 4.70 0 -36 -2 0.20 4.70 -1 -36 -2 68.99 8.90 3 -36 -3 10.00 5.70 2 -36 -3 73.09 8.50 1 -36 -3 9.50 5.30 -1 -36 -3 9.10 5.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 88294 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Er1 Er 0.57740(2) 0.43797(2) 0.52179(2) 0.02078(5) Uani 1 1 d . . . . . Co1 Co 0.74113(4) 0.31591(2) 0.61350(4) 0.03683(13) Uani 1 1 d . . . . . Cl03 Cl 0.45843(11) 0.51608(7) 0.83898(11) 0.0734(4) Uani 1 1 d . . . . . Cl04 Cl 0.80581(10) 0.40974(5) 0.93547(10) 0.0608(3) Uani 1 1 d . . . . . Cl05 Cl 0.89067(10) 0.50461(5) 0.58045(13) 0.0733(4) Uani 1 1 d . . . . . Cl06 Cl 0.16755(10) 0.34797(6) 0.29066(12) 0.0768(4) Uani 1 1 d . . . . . Cl07 Cl 0.80018(14) 0.51799(7) 0.24122(12) 0.0859(5) Uani 1 1 d . . . . . Cl08 Cl 0.47969(14) 0.20018(5) 0.54968(15) 0.0915(6) Uani 1 1 d . . . . . Cl09 Cl 0.80330(15) 0.70569(6) 0.36952(14) 0.0877(5) Uani 1 1 d . . . . . Cl0A Cl 0.86805(13) 0.29633(6) 0.34177(16) 0.0903(6) Uani 1 1 d . . . . . Cl0B Cl 0.92072(12) 0.54534(10) 0.89742(16) 0.1213(8) Uani 1 1 d . . . . . Cl0C Cl 0.34820(15) 0.36319(13) 0.87254(19) 0.1463(12) Uani 1 1 d . . . . . O1 O 0.5504(2) 0.50780(9) 0.60467(19) 0.0336(6) Uani 1 1 d . . . . . O4 O 0.6712(2) 0.50095(9) 0.4844(2) 0.0385(7) Uani 1 1 d . . . . . O6 O 0.5848(2) 0.57117(10) 0.4631(3) 0.0424(7) Uani 1 1 d . . . . . O8 O 0.6501(2) 0.41685(11) 0.6818(2) 0.0426(7) Uani 1 1 d . . . . . O10 O 0.6915(2) 0.33976(12) 0.7256(2) 0.0478(8) Uani 1 1 d . . . . . O5 O 0.5427(2) 0.35648(10) 0.5112(3) 0.0531(9) Uani 1 1 d . . . . . O3 O 0.4883(3) 0.57292(11) 0.6527(2) 0.0479(8) Uani 1 1 d . . . . . O7 O 0.6065(2) 0.28342(11) 0.5456(3) 0.0485(8) Uani 1 1 d . . . . . O2 O 0.7195(2) 0.40311(10) 0.4955(2) 0.0406(7) Uani 1 1 d . . . . . O9 O 0.7870(2) 0.33074(11) 0.4941(3) 0.0508(8) Uani 1 1 d . . . . . N1 N 0.8205(3) 0.25051(13) 0.6499(3) 0.0394(8) Uani 1 1 d . . . . . C1 C 0.6208(3) 0.53217(13) 0.7729(3) 0.0306(8) Uani 1 1 d . . . . . C4 C 0.5478(3) 0.53735(13) 0.6711(3) 0.0278(7) Uani 1 1 d . . . . . N2 N 0.8873(3) 0.34097(15) 0.7055(3) 0.0477(9) Uani 1 1 d . . . . . C6 C 0.5872(3) 0.52589(16) 0.8545(3) 0.0414(10) Uani 1 1 d . . . . . C8 C 0.6642(3) 0.54614(13) 0.4747(3) 0.0300(8) Uani 1 1 d . . . . . C10 C 0.7590(3) 0.57455(14) 0.4733(3) 0.0299(8) Uani 1 1 d . . . . . C12 C 0.6563(3) 0.38042(15) 0.7367(3) 0.0333(8) Uani 1 1 d . . . . . C14 C 0.7442(3) 0.62031(15) 0.4291(3) 0.0369(9) Uani 1 1 d . . . . . H14 H 0.678129 0.632293 0.402915 0.044 Uiso 1 1 calc R U . . . C16 C 0.7649(3) 0.37245(14) 0.4588(3) 0.0285(8) Uani 1 1 d . . . . . C18 C 0.7840(3) 0.43700(17) 0.3450(3) 0.0397(9) Uani 1 1 d . . . . . H18 H 0.750679 0.457393 0.377960 0.048 Uiso 1 1 calc R U . . . C20 C 0.8591(3) 0.55852(16) 0.5139(3) 0.0424(10) Uani 1 1 d . . . . . C22 C 0.7982(3) 0.38801(16) 0.3717(3) 0.0345(9) Uani 1 1 d . . . . . C24 C 0.5328(3) 0.31156(13) 0.5117(3) 0.0306(8) Uani 1 1 d . . . . . C26 C 0.6779(3) 0.39663(16) 0.9177(3) 0.0406(9) Uani 1 1 d . . . . . C28 C 0.6164(3) 0.38491(16) 0.8239(3) 0.0376(9) Uani 1 1 d . . . . . C30 C 0.7240(3) 0.53708(17) 0.7860(3) 0.0431(10) Uani 1 1 d . . . . . H30 H 0.748188 0.539808 0.731515 0.052 Uiso 1 1 calc R U . . . C32 C 0.8182(4) 0.4558(2) 0.2709(4) 0.0551(13) Uani 1 1 d . . . . . C34 C 0.3545(3) 0.32264(16) 0.4073(3) 0.0373(9) Uani 1 1 d . . . . . H34 H 0.372369 0.354877 0.399286 0.045 Uiso 1 1 calc R U . . . C36 C 0.9188(3) 0.25557(18) 0.7082(3) 0.0433(10) Uani 1 1 d . . . . . C38 C 0.6554(4) 0.52606(19) 0.9494(3) 0.0551(13) Uani 1 1 d . . . . . H38 H 0.631909 0.521821 1.004029 0.066 Uiso 1 1 calc R U . . . C40 C 0.8257(4) 0.64833(17) 0.4233(4) 0.0495(12) Uani 1 1 d . . . . . C42 C 0.4275(3) 0.29089(14) 0.4651(3) 0.0333(8) Uani 1 1 d . . . . . C44 C 0.3978(4) 0.24340(17) 0.4764(4) 0.0514(12) Uani 1 1 d . . . . . C46 C 0.7575(4) 0.53256(19) 0.9616(3) 0.0576(14) Uani 1 1 d . . . . . H46 H 0.803652 0.533303 1.024788 0.069 Uiso 1 1 calc R U . . . C47 C 0.5145(4) 0.3749(2) 0.8119(4) 0.0648(15) Uani 1 1 d . . . . . H47 H 0.471285 0.367463 0.749326 0.078 Uiso 1 1 calc R U . . . C3 C 0.7860(4) 0.20650(16) 0.6187(4) 0.0514(12) Uani 1 1 d . . . . . H3 H 0.718832 0.203165 0.578964 0.062 Uiso 1 1 calc R U . . . C25 C 0.6389(4) 0.3973(2) 0.9972(4) 0.0627(14) Uani 1 1 d . . . . . H25 H 0.681317 0.405105 1.059852 0.075 Uiso 1 1 calc R U . . . C13 C 0.7915(4) 0.5379(2) 0.8807(4) 0.0541(12) Uani 1 1 d . . . . . C27 C 0.9527(3) 0.3036(2) 0.7400(3) 0.0474(11) Uani 1 1 d . . . . . C7 C 0.9161(4) 0.3859(2) 0.7351(5) 0.0693(16) Uani 1 1 d . . . . . H7 H 0.871001 0.411545 0.710888 0.083 Uiso 1 1 calc R U . . . C29 C 0.9242(4) 0.6310(2) 0.4595(4) 0.0628(15) Uani 1 1 d . . . . . H29 H 0.978906 0.649264 0.452749 0.075 Uiso 1 1 calc R U . . . C15 C 0.8478(5) 0.16427(19) 0.6435(5) 0.0699(17) Uani 1 1 d . . . . . H15 H 0.822208 0.133695 0.619713 0.084 Uiso 1 1 calc R U . . . C31 C 0.9844(4) 0.2152(2) 0.7375(4) 0.0604(15) Uani 1 1 d . . . . . C2 C 0.9401(3) 0.5867(2) 0.5055(4) 0.0602(14) Uani 1 1 d . . . . . H2 H 1.006452 0.575135 0.531704 0.072 Uiso 1 1 calc R U . . . C33 C 0.9460(5) 0.1692(2) 0.7032(5) 0.075(2) Uani 1 1 d . . . . . H33 H 0.987365 0.141712 0.720979 0.090 Uiso 1 1 calc R U . . . C17 C 1.0519(4) 0.3111(3) 0.8054(4) 0.0671(16) Uani 1 1 d . . . . . C35 C 0.2287(4) 0.2596(2) 0.3714(5) 0.0768(19) Uani 1 1 d . . . . . H35 H 0.162883 0.248921 0.338914 0.092 Uiso 1 1 calc R U . . . C9 C 0.2562(3) 0.30703(19) 0.3616(4) 0.0490(11) Uani 1 1 d . . . . . C37 C 0.2990(5) 0.2280(2) 0.4293(5) 0.083(2) Uani 1 1 d . . . . . H37 H 0.280157 0.195879 0.437064 0.100 Uiso 1 1 calc R U . . . C19 C 1.0781(5) 0.3593(3) 0.8361(5) 0.091(2) Uani 1 1 d . . . . . H19 H 1.141766 0.365788 0.880768 0.109 Uiso 1 1 calc R U . . . C39 C 0.4762(4) 0.3759(3) 0.8912(5) 0.0713(17) Uani 1 1 d . . . . . C5 C 1.0850(5) 0.2243(3) 0.8022(5) 0.082(2) Uani 1 1 d . . . . . H5 H 1.130158 0.198250 0.821325 0.099 Uiso 1 1 calc R U . . . C41 C 0.8457(3) 0.3581(2) 0.3185(4) 0.0528(13) Uani 1 1 d . . . . . C21 C 1.1159(4) 0.2691(4) 0.8359(5) 0.089(2) Uani 1 1 d . . . . . H21 H 1.180719 0.273030 0.880418 0.107 Uiso 1 1 calc R U . . . C43 C 0.5384(5) 0.3865(2) 0.9841(4) 0.0725(17) Uani 1 1 d . . . . . H43 H 0.512554 0.386289 1.037734 0.087 Uiso 1 1 calc R U . . . C11 C 0.8659(4) 0.4269(3) 0.2198(4) 0.0734(18) Uani 1 1 d . . . . . H11 H 0.888902 0.440240 0.169869 0.088 Uiso 1 1 calc R U . . . C45 C 0.8796(4) 0.3783(3) 0.2424(4) 0.0740(19) Uani 1 1 d . . . . . H45 H 0.911564 0.358365 0.207259 0.089 Uiso 1 1 calc R U . . . C23 C 1.0119(5) 0.3964(3) 0.8016(6) 0.090(2) Uani 1 1 d . . . . . H23 H 1.029754 0.428456 0.821721 0.108 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Er1 0.02109(7) 0.02104(7) 0.01921(8) -0.00091(6) 0.00446(5) -0.00046(6) Co1 0.0356(3) 0.0304(3) 0.0446(3) 0.0005(2) 0.0122(2) 0.0084(2) Cl03 0.0616(8) 0.1135(12) 0.0506(8) 0.0065(8) 0.0253(6) -0.0175(8) Cl04 0.0494(6) 0.0746(9) 0.0533(8) -0.0163(7) 0.0077(5) -0.0081(6) Cl05 0.0481(7) 0.0678(9) 0.0877(11) 0.0139(8) -0.0045(7) 0.0048(6) Cl06 0.0454(7) 0.0991(11) 0.0692(10) -0.0172(8) -0.0084(6) 0.0103(7) Cl07 0.0974(12) 0.0976(12) 0.0654(10) 0.0330(9) 0.0285(8) -0.0267(9) Cl08 0.0946(11) 0.0502(8) 0.1147(15) 0.0359(9) 0.0084(10) -0.0180(8) Cl09 0.1270(14) 0.0559(8) 0.0948(13) 0.0144(8) 0.0555(11) -0.0303(9) Cl0A 0.0865(11) 0.0720(10) 0.1317(16) -0.0429(10) 0.0620(11) 0.0031(8) Cl0B 0.0427(8) 0.203(2) 0.0977(15) 0.0356(15) -0.0096(8) -0.0003(11) Cl0C 0.0687(11) 0.273(3) 0.1158(18) -0.054(2) 0.0554(12) -0.0497(16) O1 0.0463(15) 0.0320(13) 0.0204(13) -0.0083(11) 0.0070(11) 0.0015(12) O4 0.0336(14) 0.0285(13) 0.062(2) -0.0041(13) 0.0268(13) -0.0033(11) O6 0.0327(14) 0.0290(14) 0.074(2) 0.0017(14) 0.0282(14) -0.0028(11) O8 0.0558(18) 0.0441(16) 0.0235(14) 0.0064(12) 0.0053(13) 0.0047(14) O10 0.0580(19) 0.0541(19) 0.0347(17) 0.0120(14) 0.0192(14) 0.0255(15) O5 0.0369(15) 0.0232(14) 0.089(3) -0.0025(15) 0.0025(15) -0.0055(12) O3 0.066(2) 0.0403(16) 0.0260(15) -0.0092(13) -0.0037(14) 0.0205(14) O7 0.0414(16) 0.0377(16) 0.060(2) 0.0000(15) 0.0049(14) 0.0048(13) O2 0.0475(16) 0.0398(15) 0.0447(18) 0.0065(13) 0.0296(14) 0.0095(13) O9 0.060(2) 0.0428(17) 0.055(2) 0.0095(15) 0.0258(16) 0.0189(15) N1 0.049(2) 0.0358(18) 0.0343(19) 0.0056(15) 0.0135(16) 0.0116(15) C1 0.043(2) 0.0288(18) 0.0166(17) -0.0010(14) 0.0039(15) 0.0018(15) C4 0.0384(19) 0.0254(17) 0.0191(17) -0.0048(14) 0.0076(14) -0.0040(14) N2 0.042(2) 0.052(2) 0.053(2) -0.0080(19) 0.0196(18) -0.0046(17) C6 0.052(2) 0.043(2) 0.027(2) -0.0013(18) 0.0079(18) -0.0028(19) C8 0.0273(17) 0.0282(17) 0.040(2) -0.0045(16) 0.0180(16) -0.0058(14) C10 0.0268(17) 0.0334(18) 0.033(2) -0.0068(15) 0.0147(15) -0.0084(14) C12 0.0320(19) 0.044(2) 0.0213(18) 0.0048(16) 0.0032(14) 0.0074(16) C14 0.040(2) 0.039(2) 0.037(2) -0.0059(18) 0.0191(17) -0.0114(17) C16 0.0193(15) 0.0347(19) 0.031(2) -0.0048(16) 0.0072(14) -0.0024(14) C18 0.0320(19) 0.057(3) 0.031(2) 0.003(2) 0.0107(16) -0.0082(19) C20 0.033(2) 0.048(2) 0.046(3) -0.009(2) 0.0105(17) -0.0081(18) C22 0.0232(17) 0.052(2) 0.030(2) -0.0099(18) 0.0107(15) -0.0060(16) C24 0.0318(18) 0.0256(17) 0.036(2) -0.0026(15) 0.0125(15) -0.0033(15) C26 0.046(2) 0.044(2) 0.030(2) -0.0003(18) 0.0086(18) 0.0013(19) C28 0.043(2) 0.045(2) 0.025(2) 0.0052(17) 0.0092(16) 0.0088(18) C30 0.042(2) 0.057(3) 0.029(2) 0.006(2) 0.0080(17) 0.009(2) C32 0.043(2) 0.088(4) 0.034(2) 0.007(2) 0.011(2) -0.018(2) C34 0.033(2) 0.041(2) 0.035(2) -0.0106(18) 0.0076(16) -0.0041(17) C36 0.042(2) 0.059(3) 0.032(2) 0.016(2) 0.0175(18) 0.020(2) C38 0.080(4) 0.064(3) 0.018(2) 0.005(2) 0.010(2) 0.000(3) C40 0.064(3) 0.047(2) 0.048(3) -0.005(2) 0.032(2) -0.025(2) C42 0.039(2) 0.0302(18) 0.034(2) -0.0084(16) 0.0157(17) -0.0083(16) C44 0.060(3) 0.041(2) 0.052(3) 0.000(2) 0.013(2) -0.017(2) C46 0.071(3) 0.060(3) 0.025(2) 0.007(2) -0.011(2) 0.003(3) C47 0.044(3) 0.112(5) 0.038(3) -0.008(3) 0.011(2) -0.001(3) C3 0.072(3) 0.034(2) 0.050(3) 0.006(2) 0.022(2) 0.010(2) C25 0.074(4) 0.085(4) 0.028(2) -0.013(3) 0.013(2) -0.003(3) C13 0.046(3) 0.065(3) 0.041(3) 0.008(2) -0.004(2) 0.003(2) C27 0.036(2) 0.075(3) 0.036(2) 0.006(2) 0.0171(18) 0.002(2) C7 0.058(3) 0.066(3) 0.089(5) -0.019(3) 0.030(3) -0.017(3) C29 0.049(3) 0.071(4) 0.076(4) -0.014(3) 0.031(3) -0.034(3) C15 0.112(5) 0.037(3) 0.073(4) 0.010(3) 0.047(4) 0.020(3) C31 0.063(3) 0.080(4) 0.049(3) 0.039(3) 0.034(2) 0.038(3) C2 0.027(2) 0.082(4) 0.071(4) -0.016(3) 0.013(2) -0.017(2) C33 0.102(5) 0.069(4) 0.072(4) 0.046(3) 0.053(4) 0.054(4) C17 0.038(3) 0.118(5) 0.046(3) 0.008(3) 0.015(2) -0.003(3) C35 0.054(3) 0.082(4) 0.082(5) -0.023(4) 0.003(3) -0.037(3) C9 0.041(2) 0.062(3) 0.041(3) -0.019(2) 0.0070(19) -0.005(2) C37 0.079(4) 0.057(3) 0.100(5) -0.004(3) 0.007(4) -0.042(3) C19 0.052(4) 0.150(7) 0.071(4) -0.021(5) 0.019(3) -0.041(4) C39 0.056(3) 0.110(5) 0.056(4) -0.013(3) 0.029(3) -0.013(3) C5 0.055(4) 0.131(6) 0.066(4) 0.055(4) 0.027(3) 0.046(4) C41 0.038(2) 0.075(3) 0.051(3) -0.029(3) 0.021(2) -0.009(2) C21 0.042(3) 0.170(8) 0.053(4) 0.042(5) 0.011(3) 0.018(4) C43 0.079(4) 0.106(5) 0.045(3) -0.010(3) 0.038(3) -0.012(4) C11 0.060(3) 0.129(6) 0.038(3) -0.009(3) 0.025(2) -0.026(4) C45 0.056(3) 0.122(6) 0.056(4) -0.038(4) 0.035(3) -0.011(3) C23 0.066(4) 0.106(6) 0.105(6) -0.037(5) 0.035(4) -0.038(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Er Er -0.2586 4.9576 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Er1 O1 72.61(9) . 3_666 ? O1 Er1 O3 123.91(9) . 3_666 ? O4 Er1 O1 73.77(10) . 3_666 ? O4 Er1 O1 71.77(10) . . ? O4 Er1 O6 136.15(9) . 3_666 ? O4 Er1 O3 85.37(12) . 3_666 ? O6 Er1 O1 74.90(10) 3_666 . ? O6 Er1 O1 69.62(10) 3_666 3_666 ? O6 Er1 O3 90.35(12) 3_666 3_666 ? O8 Er1 O1 148.30(10) . 3_666 ? O8 Er1 O1 78.02(10) . . ? O8 Er1 O4 108.15(11) . . ? O8 Er1 O6 91.62(12) . 3_666 ? O8 Er1 O5 80.65(12) . . ? O8 Er1 O3 157.61(11) . 3_666 ? O8 Er1 O2 85.11(11) . . ? O5 Er1 O1 140.82(12) . . ? O5 Er1 O1 115.65(10) . 3_666 ? O5 Er1 O4 146.85(11) . . ? O5 Er1 O6 73.26(11) . 3_666 ? O5 Er1 O3 78.58(12) . 3_666 ? O5 Er1 O2 75.76(11) . . ? O3 Er1 O1 51.74(9) 3_666 3_666 ? O2 Er1 O1 133.79(10) . . ? O2 Er1 O1 124.15(9) . 3_666 ? O2 Er1 O4 73.35(9) . . ? O2 Er1 O6 148.97(10) . 3_666 ? O2 Er1 O3 81.77(11) . 3_666 ? O10 Co1 O7 92.39(14) . . ? O10 Co1 O9 149.44(13) . . ? O10 Co1 N1 110.98(13) . . ? O10 Co1 N2 83.80(14) . . ? O7 Co1 N1 94.44(13) . . ? O7 Co1 N2 169.97(15) . . ? O9 Co1 O7 99.13(15) . . ? O9 Co1 N1 96.31(13) . . ? O9 Co1 N2 88.70(15) . . ? N1 Co1 N2 78.38(15) . . ? Er1 O1 Er1 107.39(9) . 3_666 ? C4 O1 Er1 89.2(2) . 3_666 ? C4 O1 Er1 162.8(3) . . ? C8 O4 Er1 137.6(2) . . ? C8 O6 Er1 138.7(2) . 3_666 ? C12 O8 Er1 139.0(3) . . ? C12 O10 Co1 128.8(3) . . ? C24 O5 Er1 174.0(3) . . ? C4 O3 Er1 98.1(2) . 3_666 ? C24 O7 Co1 115.8(3) . . ? C16 O2 Er1 154.1(3) . . ? C16 O9 Co1 114.9(3) . . ? C36 N1 Co1 114.5(3) . . ? C3 N1 Co1 126.3(3) . . ? C3 N1 C36 119.1(4) . . ? C6 C1 C4 121.8(4) . . ? C6 C1 C30 119.1(4) . . ? C30 C1 C4 119.0(3) . . ? O1 C4 Er1 64.76(19) . 3_666 ? O1 C4 C1 120.2(3) . . ? O3 C4 Er1 56.18(19) . 3_666 ? O3 C4 O1 120.8(3) . . ? O3 C4 C1 118.9(3) . . ? C1 C4 Er1 171.0(2) . 3_666 ? C27 N2 Co1 112.1(3) . . ? C7 N2 Co1 128.7(4) . . ? C7 N2 C27 119.0(5) . . ? C1 C6 Cl03 119.7(3) . . ? C1 C6 C38 121.0(4) . . ? C38 C6 Cl03 119.3(4) . . ? O4 C8 O6 126.2(3) . . ? O4 C8 C10 118.1(3) . . ? O6 C8 C10 115.6(3) . . ? C14 C10 C8 117.1(3) . . ? C14 C10 C20 117.7(3) . . ? C20 C10 C8 125.2(4) . . ? O8 C12 C28 118.3(4) . . ? O10 C12 O8 126.2(4) . . ? O10 C12 C28 115.5(4) . . ? C10 C14 H14 119.5 . . ? C40 C14 C10 121.0(4) . . ? C40 C14 H14 119.5 . . ? O2 C16 C22 117.7(3) . . ? O9 C16 O2 122.7(4) . . ? O9 C16 C22 119.5(3) . . ? C22 C18 H18 119.4 . . ? C32 C18 H18 119.4 . . ? C32 C18 C22 121.2(5) . . ? C10 C20 Cl05 123.3(3) . . ? C2 C20 Cl05 116.3(4) . . ? C2 C20 C10 120.4(4) . . ? C18 C22 C16 116.4(3) . . ? C18 C22 C41 117.8(4) . . ? C41 C22 C16 125.7(4) . . ? O5 C24 O7 122.5(4) . . ? O5 C24 C42 117.6(3) . . ? O7 C24 C42 119.9(3) . . ? C28 C26 Cl04 119.2(3) . . ? C25 C26 Cl04 120.0(4) . . ? C25 C26 C28 120.8(4) . . ? C26 C28 C12 122.9(4) . . ? C26 C28 C47 117.9(4) . . ? C47 C28 C12 119.1(4) . . ? C1 C30 H30 120.2 . . ? C1 C30 C13 119.7(4) . . ? C13 C30 H30 120.2 . . ? C18 C32 Cl07 119.5(4) . . ? C11 C32 Cl07 119.4(4) . . ? C11 C32 C18 121.1(6) . . ? C42 C34 H34 119.5 . . ? C9 C34 H34 119.5 . . ? C9 C34 C42 121.0(4) . . ? N1 C36 C27 117.2(4) . . ? N1 C36 C31 122.0(5) . . ? C31 C36 C27 120.8(5) . . ? C6 C38 H38 120.3 . . ? C46 C38 C6 119.3(5) . . ? C46 C38 H38 120.3 . . ? C14 C40 Cl09 119.3(4) . . ? C29 C40 Cl09 120.1(4) . . ? C29 C40 C14 120.6(5) . . ? C34 C42 C24 116.8(3) . . ? C44 C42 C24 125.3(4) . . ? C44 C42 C34 117.9(4) . . ? C42 C44 Cl08 123.0(4) . . ? C42 C44 C37 120.6(5) . . ? C37 C44 Cl08 116.4(4) . . ? C38 C46 H46 120.0 . . ? C13 C46 C38 119.9(4) . . ? C13 C46 H46 120.0 . . ? C28 C47 H47 119.6 . . ? C39 C47 C28 120.9(5) . . ? C39 C47 H47 119.6 . . ? N1 C3 H3 118.9 . . ? N1 C3 C15 122.2(5) . . ? C15 C3 H3 118.9 . . ? C26 C25 H25 119.8 . . ? C43 C25 C26 120.4(5) . . ? C43 C25 H25 119.8 . . ? C30 C13 Cl0B 119.8(4) . . ? C46 C13 Cl0B 119.3(4) . . ? C46 C13 C30 120.9(5) . . ? N2 C27 C36 117.7(4) . . ? N2 C27 C17 122.2(5) . . ? C17 C27 C36 120.1(5) . . ? N2 C7 H7 118.7 . . ? N2 C7 C23 122.5(6) . . ? C23 C7 H7 118.7 . . ? C40 C29 H29 120.5 . . ? C2 C29 C40 118.9(4) . . ? C2 C29 H29 120.5 . . ? C3 C15 H15 120.6 . . ? C33 C15 C3 118.8(6) . . ? C33 C15 H15 120.6 . . ? C36 C31 C5 117.5(6) . . ? C33 C31 C36 117.6(5) . . ? C33 C31 C5 124.8(5) . . ? C20 C2 H2 119.4 . . ? C29 C2 C20 121.2(5) . . ? C29 C2 H2 119.4 . . ? C15 C33 C31 120.3(5) . . ? C15 C33 H33 119.8 . . ? C31 C33 H33 119.8 . . ? C27 C17 C21 117.7(6) . . ? C19 C17 C27 116.6(6) . . ? C19 C17 C21 125.6(6) . . ? C9 C35 H35 120.3 . . ? C9 C35 C37 119.5(5) . . ? C37 C35 H35 120.3 . . ? C34 C9 Cl06 119.4(4) . . ? C35 C9 Cl06 120.2(4) . . ? C35 C9 C34 120.4(5) . . ? C44 C37 H37 119.7 . . ? C35 C37 C44 120.6(5) . . ? C35 C37 H37 119.7 . . ? C17 C19 H19 119.6 . . ? C23 C19 C17 120.8(6) . . ? C23 C19 H19 119.6 . . ? C47 C39 Cl0C 119.2(5) . . ? C43 C39 Cl0C 120.2(4) . . ? C43 C39 C47 120.6(5) . . ? C31 C5 H5 119.0 . . ? C21 C5 C31 122.1(6) . . ? C21 C5 H5 119.0 . . ? C22 C41 Cl0A 123.5(4) . . ? C22 C41 C45 119.9(5) . . ? C45 C41 Cl0A 116.6(4) . . ? C17 C21 H21 119.2 . . ? C5 C21 C17 121.7(6) . . ? C5 C21 H21 119.2 . . ? C25 C43 C39 119.4(5) . . ? C25 C43 H43 120.3 . . ? C39 C43 H43 120.3 . . ? C32 C11 H11 120.2 . . ? C32 C11 C45 119.6(5) . . ? C45 C11 H11 120.2 . . ? C41 C45 H45 119.8 . . ? C11 C45 C41 120.4(5) . . ? C11 C45 H45 119.8 . . ? C7 C23 H23 120.6 . . ? C19 C23 C7 118.9(7) . . ? C19 C23 H23 120.6 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Er1 O1 2.570(3) 3_666 ? Er1 O1 2.327(2) . ? Er1 O4 2.302(3) . ? Er1 O6 2.311(3) 3_666 ? Er1 O8 2.262(3) . ? Er1 O5 2.272(3) . ? Er1 O3 2.384(3) 3_666 ? Er1 O2 2.297(3) . ? Co1 O10 2.014(3) . ? Co1 O7 2.016(3) . ? Co1 O9 2.015(3) . ? Co1 N1 2.076(3) . ? Co1 N2 2.151(4) . ? Cl03 C6 1.735(5) . ? Cl04 C26 1.733(5) . ? Cl05 C20 1.733(5) . ? Cl06 C9 1.736(5) . ? Cl07 C32 1.749(6) . ? Cl08 C44 1.743(5) . ? Cl09 C40 1.729(5) . ? Cl0A C41 1.730(6) . ? Cl0B C13 1.729(5) . ? Cl0C C39 1.731(6) . ? O1 C4 1.249(4) . ? O4 C8 1.243(4) . ? O6 C8 1.254(4) . ? O8 C12 1.251(5) . ? O10 C12 1.240(5) . ? O5 C24 1.235(4) . ? O3 C4 1.245(4) . ? O7 C24 1.247(5) . ? O2 C16 1.246(4) . ? O9 C16 1.245(5) . ? N1 C36 1.363(6) . ? N1 C3 1.319(6) . ? C1 C4 1.498(5) . ? C1 C6 1.377(6) . ? C1 C30 1.378(6) . ? N2 C27 1.352(6) . ? N2 C7 1.319(7) . ? C6 C38 1.389(6) . ? C8 C10 1.520(5) . ? C10 C14 1.386(6) . ? C10 C20 1.391(6) . ? C12 C28 1.498(6) . ? C14 H14 0.9300 . ? C14 C40 1.378(5) . ? C16 C22 1.501(5) . ? C18 H18 0.9300 . ? C18 C22 1.389(6) . ? C18 C32 1.372(6) . ? C20 C2 1.386(6) . ? C22 C41 1.398(6) . ? C24 C42 1.507(5) . ? C26 C28 1.384(6) . ? C26 C25 1.383(7) . ? C28 C47 1.384(6) . ? C30 H30 0.9300 . ? C30 C13 1.385(6) . ? C32 C11 1.364(8) . ? C34 H34 0.9300 . ? C34 C42 1.392(6) . ? C34 C9 1.378(6) . ? C36 C27 1.419(7) . ? C36 C31 1.404(6) . ? C38 H38 0.9300 . ? C38 C46 1.371(7) . ? C40 C29 1.378(7) . ? C42 C44 1.383(6) . ? C44 C37 1.387(7) . ? C46 H46 0.9300 . ? C46 C13 1.368(7) . ? C47 H47 0.9300 . ? C47 C39 1.376(7) . ? C3 H3 0.9300 . ? C3 C15 1.413(7) . ? C25 H25 0.9300 . ? C25 C43 1.368(8) . ? C27 C17 1.415(7) . ? C7 H7 0.9300 . ? C7 C23 1.400(9) . ? C29 H29 0.9300 . ? C29 C2 1.361(8) . ? C15 H15 0.9300 . ? C15 C33 1.366(9) . ? C31 C33 1.394(9) . ? C31 C5 1.433(9) . ? C2 H2 0.9300 . ? C33 H33 0.9300 . ? C17 C19 1.400(10) . ? C17 C21 1.432(10) . ? C35 H35 0.9300 . ? C35 C9 1.368(8) . ? C35 C37 1.370(9) . ? C37 H37 0.9300 . ? C19 H19 0.9300 . ? C19 C23 1.353(10) . ? C39 C43 1.369(8) . ? C5 H5 0.9300 . ? C5 C21 1.335(10) . ? C41 C45 1.407(8) . ? C21 H21 0.9300 . ? C43 H43 0.9300 . ? C11 H11 0.9300 . ? C11 C45 1.368(9) . ? C45 H45 0.9300 . ? C23 H23 0.9300 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Er1 O1 C4 Er1 -164.4(9) . . . 3_666 ? Er1 O1 C4 O3 4.7(4) 3_666 . . . ? Er1 O1 C4 O3 -159.7(7) . . . . ? Er1 O1 C4 C1 -171.6(3) 3_666 . . . ? Er1 O1 C4 C1 24.0(11) . . . . ? Er1 O4 C8 O6 -16.6(7) . . . . ? Er1 O4 C8 C10 165.4(3) . . . . ? Er1 O6 C8 O4 13.8(7) 3_666 . . . ? Er1 O6 C8 C10 -168.1(3) 3_666 . . . ? Er1 O8 C12 O10 58.9(6) . . . . ? Er1 O8 C12 C28 -119.8(4) . . . . ? Er1 O3 C4 O1 -5.1(4) 3_666 . . . ? Er1 O3 C4 C1 171.2(3) 3_666 . . . ? Er1 O2 C16 O9 -81.4(7) . . . . ? Er1 O2 C16 C22 101.7(6) . . . . ? Co1 O10 C12 O8 -4.7(6) . . . . ? Co1 O10 C12 C28 174.1(3) . . . . ? Co1 O7 C24 O5 6.5(6) . . . . ? Co1 O7 C24 C42 -176.2(3) . . . . ? Co1 O9 C16 O2 1.3(5) . . . . ? Co1 O9 C16 C22 178.1(3) . . . . ? Co1 N1 C36 C27 2.8(5) . . . . ? Co1 N1 C36 C31 -178.1(3) . . . . ? Co1 N1 C3 C15 176.6(4) . . . . ? Co1 N2 C27 C36 2.8(5) . . . . ? Co1 N2 C27 C17 -177.2(4) . . . . ? Co1 N2 C7 C23 174.9(5) . . . . ? Cl03 C6 C38 C46 178.3(4) . . . . ? Cl04 C26 C28 C12 3.3(6) . . . . ? Cl04 C26 C28 C47 -179.6(4) . . . . ? Cl04 C26 C25 C43 -179.3(5) . . . . ? Cl05 C20 C2 C29 -176.3(4) . . . . ? Cl07 C32 C11 C45 -179.7(4) . . . . ? Cl08 C44 C37 C35 179.0(6) . . . . ? Cl09 C40 C29 C2 177.0(4) . . . . ? Cl0A C41 C45 C11 -179.4(5) . . . . ? Cl0C C39 C43 C25 -178.8(5) . . . . ? O4 C8 C10 C14 158.0(4) . . . . ? O4 C8 C10 C20 -22.9(6) . . . . ? O6 C8 C10 C14 -20.3(5) . . . . ? O6 C8 C10 C20 158.8(4) . . . . ? O8 C12 C28 C26 -95.1(5) . . . . ? O8 C12 C28 C47 87.8(6) . . . . ? O10 C12 C28 C26 86.0(5) . . . . ? O10 C12 C28 C47 -91.1(5) . . . . ? O5 C24 C42 C34 13.1(6) . . . . ? O5 C24 C42 C44 -166.0(4) . . . . ? O7 C24 C42 C34 -164.3(4) . . . . ? O7 C24 C42 C44 16.6(6) . . . . ? O2 C16 C22 C18 5.9(5) . . . . ? O2 C16 C22 C41 -177.0(4) . . . . ? O9 C16 C22 C18 -171.1(4) . . . . ? O9 C16 C22 C41 6.0(6) . . . . ? N1 C36 C27 N2 -3.8(6) . . . . ? N1 C36 C27 C17 176.2(4) . . . . ? N1 C36 C31 C33 1.1(7) . . . . ? N1 C36 C31 C5 -177.4(4) . . . . ? N1 C3 C15 C33 1.1(8) . . . . ? C1 C6 C38 C46 -0.1(7) . . . . ? C1 C30 C13 Cl0B -178.7(4) . . . . ? C1 C30 C13 C46 1.9(8) . . . . ? C4 C1 C6 Cl03 8.1(5) . . . . ? C4 C1 C6 C38 -173.5(4) . . . . ? C4 C1 C30 C13 172.7(4) . . . . ? N2 C27 C17 C19 2.4(7) . . . . ? N2 C27 C17 C21 -178.8(5) . . . . ? N2 C7 C23 C19 0.8(10) . . . . ? C6 C1 C4 O1 -121.1(4) . . . . ? C6 C1 C4 O3 62.5(5) . . . . ? C6 C1 C30 C13 -3.0(7) . . . . ? C6 C38 C46 C13 -1.1(8) . . . . ? C8 C10 C14 C40 -179.1(4) . . . . ? C8 C10 C20 Cl05 -4.6(6) . . . . ? C8 C10 C20 C2 177.8(4) . . . . ? C10 C14 C40 Cl09 -178.7(3) . . . . ? C10 C14 C40 C29 1.4(7) . . . . ? C10 C20 C2 C29 1.5(8) . . . . ? C12 C28 C47 C39 176.2(5) . . . . ? C14 C10 C20 Cl05 174.5(3) . . . . ? C14 C10 C20 C2 -3.1(6) . . . . ? C14 C40 C29 C2 -3.1(8) . . . . ? C16 C22 C41 Cl0A 3.5(6) . . . . ? C16 C22 C41 C45 -175.5(4) . . . . ? C18 C22 C41 Cl0A -179.4(3) . . . . ? C18 C22 C41 C45 1.5(6) . . . . ? C18 C32 C11 C45 0.2(8) . . . . ? C20 C10 C14 C40 1.7(6) . . . . ? C22 C18 C32 Cl07 -179.0(3) . . . . ? C22 C18 C32 C11 1.1(7) . . . . ? C22 C41 C45 C11 -0.3(8) . . . . ? C24 C42 C44 Cl08 1.2(7) . . . . ? C24 C42 C44 C37 -179.4(5) . . . . ? C26 C28 C47 C39 -1.0(9) . . . . ? C26 C25 C43 C39 -1.2(10) . . . . ? C28 C26 C25 C43 -0.2(8) . . . . ? C28 C47 C39 Cl0C 179.9(5) . . . . ? C28 C47 C39 C43 -0.4(11) . . . . ? C30 C1 C4 O1 63.3(5) . . . . ? C30 C1 C4 O3 -113.1(5) . . . . ? C30 C1 C6 Cl03 -176.2(3) . . . . ? C30 C1 C6 C38 2.1(7) . . . . ? C32 C18 C22 C16 175.4(4) . . . . ? C32 C18 C22 C41 -1.9(6) . . . . ? C32 C11 C45 C41 -0.6(9) . . . . ? C34 C42 C44 Cl08 -177.9(3) . . . . ? C34 C42 C44 C37 1.5(7) . . . . ? C36 N1 C3 C15 -0.1(7) . . . . ? C36 C27 C17 C19 -177.7(5) . . . . ? C36 C27 C17 C21 1.2(7) . . . . ? C36 C31 C33 C15 -0.2(8) . . . . ? C36 C31 C5 C21 1.4(8) . . . . ? C38 C46 C13 Cl0B -179.2(4) . . . . ? C38 C46 C13 C30 0.2(8) . . . . ? C40 C29 C2 C20 1.7(8) . . . . ? C42 C34 C9 Cl06 179.7(3) . . . . ? C42 C34 C9 C35 -0.8(7) . . . . ? C42 C44 C37 C35 -0.5(10) . . . . ? C47 C39 C43 C25 1.5(11) . . . . ? C3 N1 C36 C27 179.9(4) . . . . ? C3 N1 C36 C31 -1.0(6) . . . . ? C3 C15 C33 C31 -0.9(8) . . . . ? C25 C26 C28 C12 -175.8(4) . . . . ? C25 C26 C28 C47 1.3(7) . . . . ? C27 N2 C7 C23 -0.4(9) . . . . ? C27 C36 C31 C33 -179.8(4) . . . . ? C27 C36 C31 C5 1.6(7) . . . . ? C27 C17 C19 C23 -2.0(9) . . . . ? C27 C17 C21 C5 1.8(9) . . . . ? C7 N2 C27 C36 178.9(5) . . . . ? C7 N2 C27 C17 -1.2(7) . . . . ? C31 C36 C27 N2 177.1(4) . . . . ? C31 C36 C27 C17 -2.9(7) . . . . ? C31 C5 C21 C17 -3.2(10) . . . . ? C33 C31 C5 C21 -177.1(6) . . . . ? C17 C19 C23 C7 0.6(11) . . . . ? C9 C34 C42 C24 179.9(4) . . . . ? C9 C34 C42 C44 -0.9(6) . . . . ? C9 C35 C37 C44 -1.2(11) . . . . ? C37 C35 C9 Cl06 -178.7(5) . . . . ? C37 C35 C9 C34 1.9(9) . . . . ? C19 C17 C21 C5 -179.4(6) . . . . ? C5 C31 C33 C15 178.3(5) . . . . ? C21 C17 C19 C23 179.2(6) . . . . ?