#------------------------------------------------------------------------------ #$Date: 2024-11-21 01:40:17 +0200 (Thu, 21 Nov 2024) $ #$Revision: 296028 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/96/7249622.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7249622 loop_ _publ_author_name 'Khotchasanthong, Kenika' 'Pootaeng-On, Yupa' 'Rayanil, Kanok-on' 'Sukwattanasinitt, Mongkol' 'Laksee, Sakchai' 'Chainok, Kittipong' _publ_section_title ; Structure features of a supramolecular organic framework self-assembled from a chiral natural compound ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D4CE01008F _journal_year 2024 _chemical_absolute_configuration unk _chemical_formula_moiety 'C32 H54 O2, 0.175[C6H14]' _chemical_formula_sum 'C33.05 H56.45 O2' _chemical_formula_weight 485.83 _space_group_crystal_system hexagonal _space_group_IT_number 172 _space_group_name_Hall 'P 64' _space_group_name_H-M_alt 'P 64' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2024-10-01 _audit_creation_method ; Olex2 1.5 (compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928) ; _audit_update_record ; 2024-10-01 deposited with the CCDC. 2024-11-20 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 6 _cell_length_a 32.3290(19) _cell_length_b 32.3290(19) _cell_length_c 7.1254(5) _cell_measurement_reflns_used 8559 _cell_measurement_temperature 296 _cell_measurement_theta_max 24.93 _cell_measurement_theta_min 2.91 _cell_volume 6449.5(7) _computing_cell_refinement 'SAINT V8.40B (Bruker, 2021)' _computing_data_collection 'APEX4 (Bruker, 2021)' _computing_data_reduction 'SAINT V8.40B (Bruker, 2021)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT (Sheldrick, 2018)' _diffrn_ambient_temperature 296 _diffrn_detector 'Bruker PHOTON 200 area detector' _diffrn_detector_area_resol_mean 7.39 _diffrn_detector_type 'PHOTON II area detector' _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device 'four-circle KAPPA diffractometer' _diffrn_measurement_device_type 'Bruker D8 QUEST CMOS PHOTON II' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_collimation '0.5 mm' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_xray_symbol K-L~3~ _diffrn_reflns_av_R_equivalents 0.0789 _diffrn_reflns_av_unetI/netI 0.0572 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 38 _diffrn_reflns_limit_h_min -38 _diffrn_reflns_limit_k_max 36 _diffrn_reflns_limit_k_min -39 _diffrn_reflns_limit_l_max 8 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_number 41699 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.508 _diffrn_reflns_theta_min 2.910 _diffrn_source 'sealed x-ray tube' _diffrn_source_current 30.0 _diffrn_source_power 1.5 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.045 _exptl_absorpt_correction_T_max 0.7452 _exptl_absorpt_correction_T_min 0.6666 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0817 before and 0.0712 after correction. The Ratio of minimum to maximum transmission is 0.8945. The \l/2 correction factor is Not present. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 0.751 _exptl_crystal_description block _exptl_crystal_F_000 1624 _exptl_crystal_size_max 0.32 _exptl_crystal_size_mid 0.24 _exptl_crystal_size_min 0.11 _refine_diff_density_max 0.104 _refine_diff_density_min -0.097 _refine_diff_density_rms 0.020 _refine_ls_abs_structure_details ; Refined as an inversion twin. ; _refine_ls_abs_structure_Flack -0.8(15) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.978 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 422 _refine_ls_number_reflns 7994 _refine_ls_number_restraints 307 _refine_ls_restrained_S_all 0.990 _refine_ls_R_factor_all 0.0646 _refine_ls_R_factor_gt 0.0426 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0516P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0958 _refine_ls_wR_factor_ref 0.1042 _reflns_Friedel_coverage 0.842 _reflns_Friedel_fraction_full 0.998 _reflns_Friedel_fraction_max 0.998 _reflns_number_gt 5799 _reflns_number_total 7994 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL ypms4_0m_a_a.res in P6(4) 1.res created by SHELXL-2018/3 at 15:59:50 on 01-Oct-2024 REM Old TITL YPMS4_0m_a.res in P6(4) REM SHELXT solution in P6(4): R1 0.208, Rweak 0.101, Alpha 0.014 REM 0.751 for 5 systematic absences, Orientation as input REM Flack x = 0.276 ( 0.747 ) from 2092 Parsons' quotients REM Formula found by SHELXT: C31 O2 CELL 0.71073 32.329 32.329 7.1254 90 90 120 ZERR 6 0.0019 0.0019 0.0005 0 0 0 LATT -1 SYMM -Y+X,+X,0.667+Z SYMM -Y,+X-Y,0.333+Z SYMM -X,-Y,+Z SYMM +Y-X,-X,0.667+Z SYMM +Y,-X+Y,0.333+Z SFAC C H O UNIT 198.3 338.7 12 SADI O2 C27 O2A C27A SADI C17 C23 C17 C23A SADI C23 C24 C23A C24A SADI C23 C25 C23A C25A SADI C25 C26 C25A C26A SADI C26 C28 C26A C28A SADI C28 C29 C28A C29A SADI C28 C30 C28A C30A SADI C30 C31 C30A C31A SADI C30 C32 C30A C32A SADI 0.04 O2 C25 O2A C25A SADI 0.04 O2 C28 O2A C28A SADI 0.04 C17 C24 C17 C24A SADI 0.04 C17 C25 C17 C25A SADI 0.04 C23 C26 C23A C26A SADI 0.04 C24 C25 C24A C25A SADI 0.04 C25 C28 C25A C28A SADI 0.04 C26 C27 C26A C27A SADI 0.04 C26 C29 C26A C29A SADI 0.04 C26 C30 C26A C30A SADI 0.04 C28 C31 C28A C31A SADI 0.04 C28 C32 C28A C32A SADI 0.04 C29 C30 C29A C30A SADI 0.04 C31 C32 C31A C32A RIGU 0.001 0.001 O2 C23 C24 C25 C26 C27 C28 C29 C30 C31 C32 C17 ISOR 0.01 0.02 O2 C23 C24 C25 C26 C27 C28 C29 C30 C31 C32 RIGU 0.001 0.001 C17 O2A C23A C24A C25A C26A C27A C28A C29A C30A C31A C32A ISOR 0.01 0.02 O2A C23A C24A C25A C26A C27A C28A C29A C30A C31A C32A L.S. 4 PLAN 5 SIZE 0.32 0.24 0.11 TEMP 22.85 CONF list 4 MORE -1 ABIN BOND $H fmap 2 acta TWIN -1 0 0 0 -1 0 0 0 -1 2 OMIT -2 5 0 REM REM REM WGHT 0.051600 BASF -0.76292 FVAR 0.82422 0.32528 O1 3 0.340090 0.642855 0.451143 11.00000 0.09184 0.06741 = 0.04445 -0.00997 -0.01018 0.05763 AFIX 147 H1 2 0.328542 0.646008 0.353451 11.00000 -1.50000 AFIX 0 PART 1 O2 3 0.459843 0.286387 0.761782 21.00000 0.11077 0.11103 = 0.11534 0.03267 -0.01590 0.03679 PART 0 C1 1 0.386894 0.607600 0.327855 11.00000 0.06145 0.06159 = 0.03808 -0.00101 0.00074 0.04221 C2 1 0.343005 0.599934 0.441619 11.00000 0.06379 0.04886 = 0.04228 -0.01196 -0.00726 0.03564 AFIX 13 H2 2 0.314180 0.575152 0.379374 11.00000 -1.20000 AFIX 0 C3 1 0.343317 0.584447 0.640131 11.00000 0.07912 0.06922 = 0.03825 -0.00352 0.00852 0.05278 AFIX 23 H3A 2 0.315351 0.580792 0.705413 11.00000 -1.20000 H3B 2 0.371398 0.608934 0.704248 11.00000 -1.20000 AFIX 0 C4 1 0.343459 0.537384 0.646901 11.00000 0.08160 0.07395 = 0.03006 0.00063 0.01052 0.05226 AFIX 23 H4A 2 0.313956 0.512450 0.592502 11.00000 -1.20000 H4B 2 0.344389 0.529022 0.776958 11.00000 -1.20000 AFIX 0 C5 1 0.386356 0.539188 0.540605 11.00000 0.06151 0.06370 = 0.02912 -0.00368 0.00295 0.04334 C6 1 0.389063 0.560194 0.340809 11.00000 0.05215 0.05820 = 0.02893 -0.00277 -0.00454 0.03595 AFIX 13 H6 2 0.359928 0.536195 0.277727 11.00000 -1.20000 AFIX 0 C7 1 0.429082 0.560573 0.231559 11.00000 0.07439 0.08422 = 0.03532 0.01017 0.00419 0.05484 AFIX 23 H7A 2 0.458889 0.578703 0.299388 11.00000 -1.20000 H7B 2 0.432331 0.575786 0.110860 11.00000 -1.20000 AFIX 0 C8 1 0.418730 0.510010 0.202721 11.00000 0.08783 0.09146 = 0.03803 0.00705 0.01176 0.06615 AFIX 23 H8A 2 0.444449 0.510566 0.130586 11.00000 -1.20000 H8B 2 0.389495 0.492482 0.130871 11.00000 -1.20000 AFIX 0 C9 1 0.413524 0.484291 0.387321 11.00000 0.07234 0.07297 = 0.03646 -0.00349 -0.00186 0.05377 AFIX 13 H9 2 0.445205 0.500640 0.445760 11.00000 -1.20000 AFIX 0 C10 1 0.380987 0.489310 0.521653 11.00000 0.05967 0.06057 = 0.03416 -0.00156 -0.00310 0.04059 C11 1 0.351279 0.452820 0.633375 11.00000 0.07670 0.07459 = 0.06096 0.00165 0.01146 0.05099 AFIX 43 H11 2 0.330259 0.457313 0.708079 11.00000 -1.20000 AFIX 0 C12 1 0.349241 0.405025 0.647524 11.00000 0.08637 0.06630 = 0.05457 0.00956 0.01275 0.04891 AFIX 23 H12A 2 0.320976 0.380833 0.583378 11.00000 -1.20000 H12B 2 0.346993 0.395857 0.778375 11.00000 -1.20000 AFIX 0 C13 1 0.393682 0.407701 0.560137 11.00000 0.06715 0.06150 = 0.04392 -0.00738 -0.00565 0.04453 C14 1 0.400525 0.431415 0.364707 11.00000 0.07797 0.07030 = 0.04299 -0.01151 -0.00680 0.05333 C15 1 0.439640 0.424426 0.279788 11.00000 0.11048 0.09458 = 0.04427 -0.00588 0.00195 0.07618 AFIX 23 H15A 2 0.470845 0.448760 0.323701 11.00000 -1.20000 H15B 2 0.438995 0.425587 0.143846 11.00000 -1.20000 AFIX 0 C16 1 0.428053 0.374463 0.348111 11.00000 0.10775 0.09603 = 0.06417 -0.01169 -0.00275 0.08062 AFIX 23 H16A 2 0.456880 0.375168 0.390924 11.00000 -1.20000 H16B 2 0.414295 0.351433 0.246920 11.00000 -1.20000 AFIX 0 C17 1 0.392046 0.360661 0.511043 11.00000 0.07854 0.06665 = 0.05644 -0.01573 -0.01659 0.04833 PART 1 AFIX 13 H17 2 0.361056 0.342107 0.448627 21.00000 -1.20000 AFIX 13 PART 2 H17A 2 0.360131 0.338364 0.462436 -21.00000 -1.20000 AFIX 0 PART 0 C18 1 0.432159 0.651945 0.389796 11.00000 0.06965 0.06231 = 0.07661 -0.00483 -0.00575 0.03389 AFIX 137 H18A 2 0.429417 0.679662 0.364934 11.00000 -1.50000 H18B 2 0.458893 0.654278 0.321891 11.00000 -1.50000 H18C 2 0.436860 0.650005 0.521826 11.00000 -1.50000 AFIX 0 C19 1 0.377845 0.614169 0.119369 11.00000 0.09176 0.07630 = 0.04301 0.00672 -0.00030 0.05778 AFIX 137 H19A 2 0.348978 0.586629 0.077527 11.00000 -1.50000 H19B 2 0.404178 0.617870 0.044525 11.00000 -1.50000 H19C 2 0.374771 0.642078 0.106852 11.00000 -1.50000 AFIX 0 C20 1 0.431350 0.568573 0.659876 11.00000 0.08609 0.07529 = 0.04574 -0.00796 -0.01472 0.05279 AFIX 137 H20A 2 0.434183 0.598815 0.690262 11.00000 -1.50000 H20B 2 0.458974 0.573707 0.590457 11.00000 -1.50000 H20C 2 0.429015 0.551565 0.773464 11.00000 -1.50000 AFIX 0 C21 1 0.436114 0.437204 0.688195 11.00000 0.10406 0.07296 = 0.04505 -0.00441 -0.01756 0.05775 AFIX 137 H21A 2 0.439741 0.468297 0.705526 11.00000 -1.50000 H21B 2 0.464568 0.440357 0.632279 11.00000 -1.50000 H21C 2 0.430800 0.421570 0.807565 11.00000 -1.50000 AFIX 0 C22 1 0.355977 0.405484 0.245283 11.00000 0.11024 0.09309 = 0.06104 -0.02575 -0.03374 0.07472 AFIX 137 H22A 2 0.331789 0.411597 0.293182 11.00000 -1.50000 H22B 2 0.344546 0.371783 0.248828 11.00000 -1.50000 H22C 2 0.363358 0.416634 0.118140 11.00000 -1.50000 AFIX 0 PART 1 C23 1 0.390879 0.324983 0.667631 21.00000 0.07179 0.07172 = 0.05999 -0.01082 -0.02141 0.04007 AFIX 13 H23 2 0.420881 0.343405 0.736758 21.00000 -1.20000 AFIX 0 C24 1 0.353577 0.311422 0.808783 21.00000 0.08788 0.07011 = 0.09375 0.00835 0.00482 0.04946 AFIX 137 H24A 2 0.354240 0.339558 0.856001 21.00000 -1.50000 H24B 2 0.358967 0.295096 0.910053 21.00000 -1.50000 H24C 2 0.322985 0.290690 0.753156 21.00000 -1.50000 AFIX 0 C25 1 0.393919 0.282591 0.582149 21.00000 0.09873 0.07608 = 0.09785 0.00585 0.00668 0.05734 AFIX 23 H25A 2 0.362667 0.259669 0.533601 21.00000 -1.20000 H25B 2 0.415763 0.294368 0.476556 21.00000 -1.20000 AFIX 0 C26 1 0.410138 0.256537 0.714731 21.00000 0.09642 0.08388 = 0.09867 0.01021 0.00577 0.05681 AFIX 13 H26 2 0.391743 0.250160 0.831041 21.00000 -1.20000 AFIX 0 C27 1 0.472920 0.280671 0.949440 21.00000 0.13967 0.15261 = 0.11965 0.02896 -0.02274 0.07341 AFIX 137 H27A 2 0.500391 0.276670 0.944468 21.00000 -1.50000 H27B 2 0.446788 0.253046 1.006410 21.00000 -1.50000 H27C 2 0.480287 0.308491 1.022388 21.00000 -1.50000 AFIX 0 C28 1 0.398084 0.207624 0.629361 21.00000 0.10154 0.08294 = 0.10965 0.01909 0.01620 0.06105 C29 1 0.378854 0.166109 0.741305 21.00000 0.14290 0.08917 = 0.12533 0.02846 0.02349 0.06036 AFIX 93 H29A 2 0.378852 0.138997 0.697664 21.00000 -1.20000 H29B 2 0.366178 0.165849 0.858751 21.00000 -1.20000 AFIX 0 C30 1 0.418273 0.209408 0.444523 21.00000 0.08157 0.07088 = 0.10427 0.00868 0.00436 0.05007 AFIX 13 H30 2 0.416080 0.233187 0.366398 21.00000 -1.20000 AFIX 0 C31 1 0.467956 0.224795 0.481865 21.00000 0.08438 0.19885 = 0.17064 0.01688 0.00354 0.07621 AFIX 137 H31A 2 0.485241 0.258664 0.502823 21.00000 -1.50000 H31B 2 0.481381 0.217222 0.376185 21.00000 -1.50000 H31C 2 0.470167 0.208695 0.591331 21.00000 -1.50000 AFIX 0 C32 1 0.385176 0.155919 0.353830 21.00000 0.18180 0.09279 = 0.14356 -0.02018 -0.02509 0.05422 AFIX 137 H32A 2 0.368989 0.133294 0.452623 21.00000 -1.50000 H32B 2 0.405137 0.146976 0.285786 21.00000 -1.50000 H32C 2 0.362076 0.156249 0.270119 21.00000 -1.50000 AFIX 0 PART 2 O2A 3 0.467860 0.297763 0.722231 -21.00000 0.08181 0.05940 = 0.10600 0.01182 -0.01533 0.03453 C23A 1 0.403713 0.334932 0.670658 -21.00000 0.08222 0.05480 = 0.06594 -0.01118 -0.01853 0.04320 AFIX 13 H23A 2 0.436740 0.355529 0.712282 -21.00000 -1.20000 AFIX 0 C24A 1 0.371283 0.322747 0.833641 -21.00000 0.11434 0.07930 = 0.06636 -0.00382 -0.00807 0.05735 AFIX 137 H24D 2 0.379188 0.351267 0.902652 -21.00000 -1.50000 H24E 2 0.374751 0.300770 0.913594 -21.00000 -1.50000 H24F 2 0.338872 0.308299 0.790403 -21.00000 -1.50000 AFIX 0 C25A 1 0.398557 0.288439 0.585588 -21.00000 0.10586 0.06211 = 0.06462 -0.01191 -0.02667 0.05568 AFIX 23 H25C 2 0.364952 0.265991 0.564592 -21.00000 -1.20000 H25D 2 0.414443 0.295784 0.464640 -21.00000 -1.20000 AFIX 0 C26A 1 0.419136 0.264962 0.707805 -21.00000 0.08137 0.05156 = 0.07647 0.00553 -0.01336 0.03842 AFIX 13 H26A 2 0.404645 0.259332 0.832787 -21.00000 -1.20000 AFIX 0 C27A 1 0.491770 0.289983 0.873568 -21.00000 0.11109 0.11910 = 0.12638 0.00897 -0.03910 0.06156 AFIX 137 H27D 2 0.489008 0.259147 0.860392 -21.00000 -1.50000 H27E 2 0.477566 0.291327 0.990052 -21.00000 -1.50000 H27F 2 0.524893 0.314217 0.872532 -21.00000 -1.50000 AFIX 0 C28A 1 0.411717 0.218359 0.629624 -21.00000 0.10041 0.06601 = 0.10162 -0.00288 -0.01072 0.05463 C29A 1 0.380326 0.177783 0.726985 -21.00000 0.18430 0.06422 = 0.19664 0.01987 0.06264 0.06593 AFIX 93 H29C 2 0.372229 0.147823 0.680058 -21.00000 -1.20000 H29D 2 0.367248 0.180371 0.839589 -21.00000 -1.20000 AFIX 0 C30A 1 0.434914 0.220195 0.453645 -21.00000 0.11015 0.11519 = 0.11348 -0.01490 -0.00155 0.06535 AFIX 13 H30A 2 0.453152 0.253762 0.415222 -21.00000 -1.20000 AFIX 0 C31A 1 0.467802 0.202825 0.467739 -21.00000 0.18374 0.16980 = 0.17945 0.02249 0.04305 0.13647 AFIX 137 H31D 2 0.493916 0.223578 0.547768 -21.00000 -1.50000 H31E 2 0.479760 0.202073 0.345218 -21.00000 -1.50000 H31F 2 0.451767 0.171188 0.519675 -21.00000 -1.50000 AFIX 0 C32A 1 0.393429 0.191302 0.292346 -21.00000 0.18630 0.22673 = 0.12076 -0.03305 -0.03415 0.05381 AFIX 137 H32D 2 0.377248 0.208710 0.265402 -21.00000 -1.50000 H32E 2 0.370837 0.160076 0.338112 -21.00000 -1.50000 H32F 2 0.408140 0.188363 0.179966 -21.00000 -1.50000 AFIX 0 HKLF 4 REM ypms4_0m_a_a.res in P6(4) REM wR2 = 0.104174, GooF = S = 0.97778, Restrained GooF = 0.98980 for all data REM R1 = 0.042572 for 5799 Fo > 4sig(Fo) and 0.064599 for all 7994 data REM 422 parameters refined using 307 restraints END WGHT 0.0516 0.0000 REM Highest difference peak 0.104, deepest hole -0.097, 1-sigma level 0.020 Q1 1 0.4843 0.4863 0.6147 11.00000 0.05 0.10 Q2 1 0.2827 0.5687 0.2538 11.00000 0.05 0.10 Q3 1 0.5000 0.5000 0.4501 10.50000 0.05 0.10 Q4 1 0.5351 0.2848 0.6344 11.00000 0.05 0.10 Q5 1 0.3836 0.2763 0.4582 11.00000 0.05 0.09 REM The information below was added by Olex2. REM REM R1 = 0.042572 for 5799 Fo > 4sig(Fo) and 0.064599 for all 41710 data REM 422 parameters refined using n/a restraints REM Highest difference peak 0.10, deepest hole -0.10 REM Mean Shift 0, Max Shift -0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.064599 REM R1_gt = 0.042572 REM wR_ref = 0.104174 REM GOOF = 0.97778 REM Shift_max = -0.001 REM Shift_mean = 0 REM Reflections_all = 41710 REM Reflections_gt = 5799 REM Parameters = 422 REM Hole = -0.10 REM Peak = 0.10 REM Flack = n/a ; _cod_data_source_file d4ce01008f2.cif _cod_data_source_block 1 _cod_original_cell_volume 6449.5(9) _cod_database_code 7249622 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.995 _shelx_estimated_absorpt_t_min 0.986 _olex2_refinement_description ; 1. Twinned data refinement Scales: 1.8(15) -0.8(15) 2. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 3. Restrained distances O2-C27 \\sim O2A-C27A with sigma of 0.02 C17-C23 \\sim C17-C23A with sigma of 0.02 C23-C24 \\sim C23A-C24A with sigma of 0.02 C23-C25 \\sim C23A-C25A with sigma of 0.02 C25-C26 \\sim C25A-C26A with sigma of 0.02 C26-C28 \\sim C26A-C28A with sigma of 0.02 C28-C29 \\sim C28A-C29A with sigma of 0.02 C28-C30 \\sim C28A-C30A with sigma of 0.02 C30-C31 \\sim C30A-C31A with sigma of 0.02 C30-C32 \\sim C30A-C32A with sigma of 0.02 O2-C25 \\sim O2A-C25A with sigma of 0.04 O2-C28 \\sim O2A-C28A with sigma of 0.04 C17-C24 \\sim C17-C24A with sigma of 0.04 C17-C25 \\sim C17-C25A with sigma of 0.04 C23-C26 \\sim C23A-C26A with sigma of 0.04 C24-C25 \\sim C24A-C25A with sigma of 0.04 C25-C28 \\sim C25A-C28A with sigma of 0.04 C26-C27 \\sim C26A-C27A with sigma of 0.04 C26-C29 \\sim C26A-C29A with sigma of 0.04 C26-C30 \\sim C26A-C30A with sigma of 0.04 C28-C31 \\sim C28A-C31A with sigma of 0.04 C28-C32 \\sim C28A-C32A with sigma of 0.04 C29-C30 \\sim C29A-C30A with sigma of 0.04 C31-C32 \\sim C31A-C32A with sigma of 0.04 4. Uiso/Uaniso restraints and constraints Uanis(O2) \\sim Ueq, Uanis(C23) \\sim Ueq, Uanis(C24) \\sim Ueq, Uanis(C25) \\sim Ueq, Uanis(C26) \\sim Ueq, Uanis(C27) \\sim Ueq, Uanis(C28) \\sim Ueq, Uanis(C29) \\sim Ueq, Uanis(C30) \\sim Ueq, Uanis(C31) \\sim Ueq, Uanis(C32) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 Uanis(O2A) \\sim Ueq, Uanis(C23A) \\sim Ueq, Uanis(C24A) \\sim Ueq, Uanis(C25A) \\sim Ueq, Uanis(C26A) \\sim Ueq, Uanis(C27A) \\sim Ueq, Uanis(C28A) \\sim Ueq, Uanis(C29A) \\sim Ueq, Uanis(C30A) \\sim Ueq, Uanis(C31A) \\sim Ueq, Uanis(C32A) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02 5. Rigid body (RIGU) restrains O2, C23, C24, C25, C26, C27, C28, C29, C30, C31, C32, C17 with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001 C17, O2A, C23A, C24A, C25A, C26A, C27A, C28A, C29A, C30A, C31A, C32A with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001 6. Others Sof(H17A)=Sof(O2A)=Sof(C23A)=Sof(H23A)=Sof(C24A)=Sof(H24D)=Sof(H24E)= Sof(H24F)=Sof(C25A)=Sof(H25C)=Sof(H25D)=Sof(C26A)=Sof(H26A)=Sof(C27A)= Sof(H27D)=Sof(H27E)=Sof(H27F)=Sof(C28A)=Sof(C29A)=Sof(H29C)=Sof(H29D)= Sof(C30A)=Sof(H30A)=Sof(C31A)=Sof(H31D)=Sof(H31E)=Sof(H31F)=Sof(C32A)= Sof(H32D)=Sof(H32E)=Sof(H32F)=1-FVAR(1) Sof(O2)=Sof(H17)=Sof(C23)=Sof(H23)=Sof(C24)=Sof(H24A)=Sof(H24B)=Sof(H24C)= Sof(C25)=Sof(H25A)=Sof(H25B)=Sof(C26)=Sof(H26)=Sof(C27)=Sof(H27A)=Sof(H27B)= Sof(H27C)=Sof(C28)=Sof(C29)=Sof(H29A)=Sof(H29B)=Sof(C30)=Sof(H30)=Sof(C31)= Sof(H31A)=Sof(H31B)=Sof(H31C)=Sof(C32)=Sof(H32A)=Sof(H32B)=Sof(H32C)=FVAR(1) 7.a Ternary CH refined with riding coordinates: C2(H2), C6(H6), C9(H9), C17(H17), C17(H17A), C23(H23), C26(H26), C30(H30), C23A(H23A), C26A(H26A), C30A(H30A) 7.b Secondary CH2 refined with riding coordinates: C3(H3A,H3B), C4(H4A,H4B), C7(H7A,H7B), C8(H8A,H8B), C12(H12A,H12B), C15(H15A, H15B), C16(H16A,H16B), C25(H25A,H25B), C25A(H25C,H25D) 7.c Aromatic/amide H refined with riding coordinates: C11(H11) 7.d X=CH2 refined with riding coordinates: C29(H29A,H29B), C29A(H29C,H29D) 7.e Idealised Me refined as rotating group: C18(H18A,H18B,H18C), C19(H19A,H19B,H19C), C20(H20A,H20B,H20C), C21(H21A,H21B, H21C), C22(H22A,H22B,H22C), C24(H24A,H24B,H24C), C27(H27A,H27B,H27C), C31(H31A, H31B,H31C), C32(H32A,H32B,H32C), C24A(H24D,H24E,H24F), C27A(H27D,H27E,H27F), C31A(H31D,H31E,H31F), C32A(H32D,H32E,H32F) 7.f Idealised tetrahedral OH refined as rotating group: O1(H1) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_fab_file ; 0 0 3 5.4144 -18.9526 0 0 6 -0.8117 -3.3777 0 1 0 8.0222 0.0668 0 1 1 -3.5676 -5.6608 0 1 2 2.4799 9.0670 0 1 3 1.4690 -9.0788 0 1 4 0.5958 -1.5295 0 1 5 1.6315 -0.8620 0 1 6 -0.5251 -1.6512 0 1 7 -0.9932 -1.3149 0 1 8 0.7242 -0.2910 0 2 0 -21.2219 0.0089 0 2 1 -10.1410 -9.5970 0 2 2 9.7945 13.2769 0 2 3 -2.9955 0.1949 0 2 4 0.5041 -2.3291 0 2 5 1.8704 -1.3528 0 2 6 -1.2762 0.4419 0 2 7 -1.5966 -2.1060 0 2 8 0.6935 -1.2392 0 3 0 51.3004 -0.0180 0 3 1 -21.3398 -12.6896 0 3 2 7.8766 -0.8907 0 3 3 -3.0592 -5.2107 0 3 4 0.7065 0.6644 0 3 5 -0.8893 0.2382 0 3 6 -2.6752 -0.3133 0 3 7 -0.6197 -0.4907 0 3 8 -0.4984 -1.7032 0 4 0 163.8481 0.0138 0 4 1 -31.8673 -15.2119 0 4 2 -5.3421 -4.3969 0 4 3 -3.0503 -5.4434 0 4 4 3.7698 1.8675 0 4 5 -0.9064 0.9849 0 4 6 -1.8992 -2.3689 0 4 7 -0.3647 0.4315 0 4 8 -0.0773 -0.8541 0 5 0 135.6128 0.0022 0 5 1 -17.0473 1.7084 0 5 2 -4.1102 5.0179 0 5 3 -3.2716 2.3623 0 5 4 4.0585 -1.2854 0 5 5 0.0256 0.2996 0 5 6 0.3146 -3.0736 0 5 7 -0.3636 0.4111 0 5 8 0.2492 0.0986 0 6 0 13.0713 -0.0103 0 6 1 10.4257 9.7376 0 6 2 4.3939 1.2682 0 6 3 -3.2931 1.6812 0 6 4 -0.0703 -1.9931 0 6 5 -1.7107 0.9762 0 6 6 2.5653 -1.4168 0 6 7 0.4012 0.8720 0 6 8 -1.5584 0.6006 0 7 0 -27.7494 0.0020 0 7 1 8.8152 -7.6537 0 7 2 -1.4425 -5.5643 0 7 3 -2.4396 -3.9239 0 7 4 -0.4252 0.4695 0 7 5 -1.6906 0.2627 0 7 6 3.3469 0.8217 0 7 7 -0.3485 0.7857 0 7 8 -2.2460 0.4395 0 8 0 -3.4212 -0.0001 0 8 1 -8.4471 -9.5276 0 8 2 -3.9558 -0.7222 0 8 3 0.4471 -4.0620 0 8 4 1.7767 0.7780 0 8 5 0.1606 -2.7185 0 8 6 0.5749 0.8394 0 8 7 -2.3758 0.2684 0 8 8 -0.6537 -0.4252 0 9 0 3.1494 -0.0022 0 9 1 -5.6945 2.3162 0 9 2 3.9463 0.6553 0 9 3 1.6335 -1.6044 0 9 4 0.7012 0.6936 0 9 5 -0.7268 -2.1541 0 9 6 -1.1776 -0.2155 0 9 7 -1.4706 0.2764 0 9 8 0.3406 -0.9417 0 10 0 1.0614 0.0024 0 10 1 4.3229 1.5095 0 10 2 3.8918 -3.6722 0 10 3 0.4220 -0.1028 0 10 4 -0.0608 1.7680 0 10 5 -2.1742 0.7579 0 10 6 2.2847 0.7797 0 10 7 1.2776 0.7569 0 10 8 0.7015 -1.4448 0 11 0 0.4561 0.0008 0 11 1 3.3164 -0.3294 0 11 2 0.5635 -3.7234 0 11 3 0.1124 1.1917 0 11 4 0.2190 1.3399 0 11 5 -1.1857 1.2856 0 11 6 4.3477 2.3520 0 11 7 -0.2928 1.5147 0 11 8 1.4352 -2.3053 0 12 0 -1.6555 -0.0001 0 12 1 -0.4550 -0.3610 0 12 2 4.3715 -1.5160 0 12 3 0.4259 1.6867 0 12 4 -0.4845 0.5295 0 12 5 0.3949 0.7892 0 12 6 1.2112 1.4061 0 12 7 -3.6652 1.2373 0 12 8 1.1249 -1.9110 0 13 0 2.9538 0.0009 0 13 1 -0.4006 -2.8242 0 13 2 6.8109 0.9158 0 13 3 0.8001 -0.4528 0 13 4 0.7253 0.8432 0 13 5 0.5594 -0.9432 0 13 6 -1.3592 -0.4485 0 13 7 -1.0699 0.1163 0 14 0 5.3824 0.0007 0 14 1 2.3087 -0.6761 0 14 2 3.3708 1.4103 0 14 3 0.9806 -2.6680 0 14 4 2.0499 1.8611 0 14 5 -0.0583 -3.4611 0 14 6 -1.1068 -0.8151 0 14 7 3.0396 0.2256 0 15 0 -0.9250 -0.0000 0 15 1 2.8943 -0.6490 0 15 2 0.1483 -0.7659 0 15 3 0.1672 -0.6493 0 15 4 0.2025 1.7495 0 15 5 0.8912 -1.6412 0 15 6 -0.2427 -0.3881 0 15 7 0.9231 0.7191 0 16 0 -4.9223 -0.0003 0 16 1 0.1633 -3.9528 0 16 2 0.2293 -0.5478 0 16 3 -0.1333 0.9520 0 16 4 -1.2189 -2.6100 0 16 5 2.8805 2.4604 0 16 6 0.5235 -0.2491 0 16 7 -1.8174 0.8725 0 17 0 -1.7918 0.0001 0 17 1 0.0682 -1.6495 0 17 2 0.1529 -0.3477 0 17 3 0.6522 -1.0753 0 17 4 -0.1045 -5.6966 0 17 5 3.1046 2.4832 0 17 6 0.4870 -0.9758 0 17 7 0.0848 2.0596 0 18 0 1.2663 -0.0001 0 18 1 0.0338 1.0048 0 18 2 -1.6379 -2.5556 0 18 3 0.8866 -0.0470 0 18 4 0.3179 -1.4521 0 18 5 2.0437 0.8675 0 18 6 -0.2442 -1.2609 0 18 7 1.3726 2.9301 0 19 0 -0.1919 -0.0003 0 19 1 -3.2537 0.5398 0 19 2 -1.0782 -1.7151 0 19 3 0.1335 2.7997 0 19 4 -0.7923 1.2839 0 19 5 1.2728 1.4170 0 19 6 -0.5281 0.2497 0 19 7 0.0721 1.8691 0 20 0 -0.9792 -0.0001 0 20 1 -3.4105 0.8709 0 20 2 1.3644 0.8679 0 20 3 -0.6094 1.3467 0 20 4 0.3360 -1.2534 0 20 5 0.5623 1.5710 0 20 6 -0.5938 0.1960 0 21 0 1.1334 -0.0002 0 21 1 -1.0921 0.6176 0 21 2 1.3275 0.3733 0 21 3 -0.3457 -0.5829 0 21 4 2.2894 0.3325 0 21 5 -0.0168 0.7117 0 21 6 -0.6048 -2.3991 0 22 0 1.3506 -0.0002 0 22 1 -0.5750 0.2670 0 22 2 0.2789 -1.1482 0 22 3 0.6110 -0.5007 0 22 4 -0.7744 4.0058 0 22 5 0.2450 0.6074 0 22 6 -0.3634 -2.8821 0 23 0 -0.2766 -0.0002 0 23 1 0.0227 1.0066 0 23 2 0.6125 -0.7702 0 23 3 0.6689 -0.6793 0 23 4 -4.3427 2.0094 0 23 5 1.3068 -0.4701 0 23 6 -0.4607 -1.2022 0 24 0 -0.7548 0.0000 0 24 1 0.0431 0.2558 0 24 2 1.3268 0.3762 0 24 3 -0.8610 0.0772 0 24 4 -2.0214 -0.5738 0 24 5 2.2364 -2.3057 0 24 6 -0.6272 -0.4592 0 25 0 -0.0414 0.0001 0 25 1 -1.3329 -0.7898 0 25 2 1.7957 0.1286 0 25 3 -1.7086 1.5367 0 25 4 0.2939 0.2699 0 25 5 2.8520 -1.5488 0 26 0 0.8984 -0.0001 0 26 1 -1.8737 0.0336 0 26 2 1.2780 -0.4395 0 26 3 0.3390 1.3174 0 26 4 -1.0682 -0.1492 0 26 5 2.9830 0.5315 0 27 0 0.3869 0.0001 0 27 1 -1.0619 0.1908 0 27 2 -0.4326 0.1158 0 27 3 2.2283 0.0521 0 27 4 -1.6084 -1.9797 0 27 5 1.6559 0.8265 0 28 0 -0.9188 -0.0000 0 28 1 0.4502 -1.5631 0 28 2 -1.5250 -0.2760 0 28 3 0.6557 -0.4520 0 28 4 -0.8962 -1.4346 0 29 0 -0.4304 -0.0002 0 29 1 0.3615 -2.3586 0 29 2 -1.6534 -1.8112 0 29 3 -1.6489 0.1873 0 29 4 -0.7814 0.3027 0 30 0 0.7711 0.0002 0 30 1 -0.8017 -1.1451 0 30 2 -2.2549 -2.3935 0 30 3 -1.8916 0.6860 0 30 4 -0.5217 0.4547 0 31 0 0.3946 0.0000 0 31 1 1.5934 -0.3455 0 31 2 -2.6883 -2.7115 0 31 3 -1.0584 0.1840 0 32 0 -0.9975 -0.0001 0 32 1 4.4823 -0.8386 0 32 2 -1.5500 -2.9220 0 33 0 -1.5340 0.0004 0 33 1 2.4438 -1.1031 0 33 2 -0.1778 -1.6040 1 1 0 -26.1490 0.0267 1 1 1 -2.1485 -1.9330 1 1 2 13.6555 4.2451 1 1 3 -1.8849 0.0261 1 1 4 2.1549 0.1684 1 1 5 -0.8107 -4.1897 1 1 6 -0.8542 0.3312 1 1 7 0.5213 -1.8350 1 1 8 0.1230 -1.0912 1 2 0 -13.0926 -0.0149 1 2 1 -20.4606 7.9623 1 2 2 10.0700 4.9606 1 2 3 2.7836 0.4554 1 2 4 0.3342 0.2623 1 2 5 -1.4728 -3.2955 1 2 6 -1.3610 1.0431 1 2 7 -1.4317 -0.5988 1 2 8 0.0671 -1.0967 1 3 0 87.7973 -0.0032 1 3 1 -22.9664 4.6463 1 3 2 -0.6504 -2.5511 1 3 3 8.8349 -3.7315 1 3 4 0.8254 1.8441 1 3 5 -0.8272 -0.4771 1 3 6 -0.4922 -0.3793 1 3 7 -0.7376 0.6567 1 3 8 0.1595 -1.0861 1 4 0 137.5492 0.0076 1 4 1 -12.6173 -3.8070 1 4 2 -6.9821 1.3593 1 4 3 4.4554 -1.0716 1 4 4 2.3583 0.2322 1 4 5 0.5842 0.3152 1 4 6 0.3314 -1.7529 1 4 7 0.9526 0.7621 1 4 8 0.7620 -0.7356 1 5 0 54.3901 -0.0065 1 5 1 -2.4893 3.1680 1 5 2 -0.5539 4.2136 1 5 3 1.0203 1.7151 1 5 4 1.2361 -3.1678 1 5 5 -0.6367 0.9668 1 5 6 0.6581 -1.2453 1 5 7 1.1312 0.7866 1 5 8 -0.3620 0.4312 1 6 0 -27.3101 -0.0013 1 6 1 -2.5467 4.8394 1 6 2 -0.5549 -4.6310 1 6 3 4.3749 -1.1137 1 6 4 0.2946 -1.5163 1 6 5 -1.8349 2.1266 1 6 6 1.8031 0.9598 1 6 7 -0.0381 0.2983 1 6 8 -2.1339 1.2912 1 7 0 -28.4183 0.0021 1 7 1 -9.0713 -1.9396 1 7 2 -8.1925 -6.9635 1 7 3 5.5877 -3.7390 1 7 4 1.5033 1.8704 1 7 5 -0.6294 0.1324 1 7 6 1.1052 1.7611 1 7 7 -1.3684 -0.1846 1 7 8 -1.9936 0.4804 1 8 0 -8.0390 -0.0019 1 8 1 -6.0676 -0.6741 1 8 2 -4.1690 -1.5042 1 8 3 4.0711 -2.3523 1 8 4 1.2596 0.9609 1 8 5 0.2926 -1.5388 1 8 6 -0.9965 -0.0646 1 8 7 -1.4179 0.0223 1 8 8 -1.0539 -0.2509 1 9 0 2.4382 0.0018 1 9 1 2.3464 2.6750 1 9 2 0.6437 -2.1967 1 9 3 2.7114 0.4936 1 9 4 -0.9217 -0.5404 1 9 5 -0.0695 0.9144 1 9 6 1.0814 -0.8397 1 9 7 0.6317 -0.3076 1 9 8 -0.4508 -0.2002 1 10 0 0.8756 0.0006 1 10 1 2.4127 3.9501 1 10 2 -3.8213 -3.9215 1 10 3 0.9482 1.1645 1 10 4 -1.5600 -0.3003 1 10 5 -0.2974 1.6951 1 10 6 4.8181 0.6969 1 10 7 1.6811 -1.0867 1 10 8 0.7190 -1.4212 1 11 0 -9.3437 -0.0014 1 11 1 -0.3548 2.0911 1 11 2 -3.3234 -0.5814 1 11 3 -0.1396 1.1857 1 11 4 -0.5827 -0.1713 1 11 5 0.0430 -0.0837 1 11 6 3.9172 1.2531 1 11 7 -0.3881 -1.1917 1 11 8 1.6696 -2.4378 1 12 0 -6.1372 0.0003 1 12 1 -0.1792 -2.9983 1 12 2 1.5733 1.9295 1 12 3 -0.0483 1.9900 1 12 4 0.5725 0.0546 1 12 5 0.3650 -0.1516 1 12 6 0.7432 0.0141 1 12 7 -0.0884 -0.7768 1 12 8 1.0560 -1.1011 1 13 0 4.4977 -0.0004 1 13 1 -0.0077 -1.0997 1 13 2 1.5881 0.0898 1 13 3 0.1633 -0.1678 1 13 4 1.4854 0.2602 1 13 5 0.2707 -0.5489 1 13 6 -0.8613 -0.6666 1 13 7 4.1324 0.1327 1 14 0 2.3862 -0.0007 1 14 1 -0.5073 2.2702 1 14 2 -0.0258 -2.4788 1 14 3 -0.2175 -1.8932 1 14 4 1.2110 0.4239 1 14 5 1.5065 -0.9315 1 14 6 -0.9838 0.0150 1 14 7 3.6057 0.7976 1 15 0 -4.3258 0.0001 1 15 1 -2.0056 -1.9234 1 15 2 -0.6560 -0.9976 1 15 3 -0.9266 0.8132 1 15 4 0.3766 -0.4077 1 15 5 4.0205 1.3239 1 15 6 0.1842 0.8436 1 15 7 -2.3113 0.0300 1 16 0 -3.7709 0.0005 1 16 1 -1.4573 -4.0651 1 16 2 -0.5374 0.7354 1 16 3 -0.9787 0.6515 1 16 4 0.5996 -2.1976 1 16 5 4.2614 2.2755 1 16 6 0.9491 0.5676 1 16 7 -4.0081 -1.1331 1 17 0 -0.3783 0.0003 1 17 1 1.9430 -2.1361 1 17 2 0.2760 -1.0888 1 17 3 -0.6165 -1.6350 1 17 4 0.8652 -0.5879 1 17 5 3.0279 0.9154 1 17 6 -0.4738 -0.4345 1 17 7 -1.4784 -1.6226 1 18 0 -0.8010 0.0001 1 18 1 1.6980 -0.8920 1 18 2 -0.1886 -0.9601 1 18 3 -0.5351 0.2550 1 18 4 -0.1277 1.5294 1 18 5 2.9846 1.4489 1 18 6 -2.3729 -0.3631 1 18 7 -1.1546 -1.4602 1 19 0 -2.0908 0.0007 1 19 1 -1.4755 1.6900 1 19 2 -0.8899 0.6863 1 19 3 -0.2147 0.6694 1 19 4 0.2548 -1.4707 1 19 5 2.2306 2.4483 1 19 6 -2.3562 0.1556 1 19 7 -1.5669 -0.5780 1 20 0 -0.4226 0.0000 1 20 1 -2.6727 2.7568 1 20 2 -0.4615 -0.4860 1 20 3 0.6228 -1.2894 1 20 4 2.7297 -2.3405 1 20 5 0.2987 0.7450 1 20 6 -0.6399 -1.2764 1 21 0 -0.2725 -0.0003 1 21 1 -2.2663 0.6825 1 21 2 -0.4142 -0.8192 1 21 3 1.0525 -0.5988 1 21 4 1.6251 2.3245 1 21 5 -0.5867 -0.9621 1 21 6 0.3085 -3.3011 1 22 0 -2.2591 0.0004 1 22 1 -0.8270 0.0426 1 22 2 -0.4417 0.6490 1 22 3 0.3017 -0.8954 1 22 4 -2.7278 3.4086 1 22 5 -0.1559 -0.4977 1 22 6 -0.4511 -3.1968 1 23 0 -1.9208 -0.0003 1 23 1 -0.2809 0.1959 1 23 2 -0.2053 0.4739 1 23 3 -1.0434 -1.9648 1 23 4 -3.1125 -0.1717 1 23 5 1.0030 -0.4120 1 23 6 -0.8290 -1.6205 1 24 0 -0.3519 -0.0002 1 24 1 -1.2322 -0.6181 1 24 2 -0.5446 -1.3898 1 24 3 -1.6944 0.1349 1 24 4 -0.8560 -1.6750 1 24 5 2.4937 -1.2481 1 25 0 0.3920 0.0002 1 25 1 -0.8426 -0.0141 1 25 2 -0.2409 -3.0006 1 25 3 -0.9259 1.0458 1 25 4 0.0101 -0.5760 1 25 5 3.3647 -0.4760 1 26 0 0.3533 -0.0003 1 26 1 -0.2224 1.1630 1 26 2 0.6792 -1.8132 1 26 3 0.3359 -0.9517 1 26 4 1.0836 -0.3136 1 26 5 2.3054 1.0925 1 27 0 -0.1563 0.0001 1 27 1 -0.0378 -0.4502 1 27 2 0.1296 0.9282 1 27 3 0.4086 -1.4023 1 27 4 1.1200 -1.4491 1 27 5 0.1848 0.9870 1 28 0 0.0379 -0.0000 1 28 1 0.6029 -2.4194 1 28 2 -0.8932 0.9124 1 28 3 0.0333 -0.6563 1 28 4 -0.5506 -1.5727 1 29 0 0.5844 -0.0002 1 29 1 -0.6614 -0.6002 1 29 2 -0.9693 -0.7722 1 29 3 0.7880 -1.5410 1 29 4 -0.5859 -0.3215 1 30 0 1.0978 0.0002 1 30 1 -1.2722 1.6869 1 30 2 -1.4593 -1.4633 1 30 3 1.4087 -2.5843 1 31 0 1.9145 -0.0004 1 31 1 2.1559 0.5460 1 31 2 -1.7955 -1.9581 1 31 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-0.0005 21 10 1 0.8581 0.6652 21 10 2 -0.3911 -0.3789 21 10 3 -1.0172 -1.0865 21 10 4 -0.9600 -0.3788 21 10 5 -0.3766 0.6291 21 11 0 0.6282 -0.0002 21 11 1 0.0454 -0.0645 21 11 2 -0.4269 0.7657 21 11 3 -0.7148 0.7627 21 11 4 -0.1429 0.5049 21 12 0 -1.0845 0.0001 21 12 1 -0.9743 -1.8670 21 12 2 -1.4297 0.4570 21 12 3 -0.0835 1.6452 21 12 4 -2.0619 0.4469 21 13 0 -0.9450 0.0000 21 13 1 -1.0864 -2.1847 21 13 2 -2.7247 -0.0231 21 13 3 0.6376 0.7516 21 13 4 -2.5778 -0.1049 21 14 0 0.4192 0.0001 21 14 1 0.3301 -0.5224 21 14 2 -2.0058 0.0385 21 14 3 0.9143 0.3969 21 15 0 -0.3390 0.0002 21 15 1 0.6672 0.5611 21 15 2 0.3525 0.1742 21 15 3 0.2836 0.7425 21 16 0 -0.4319 0.0001 21 16 1 0.2318 0.0888 21 16 2 1.3280 -0.3032 21 17 0 0.4846 -0.0004 21 17 1 0.4233 -0.1769 21 17 2 0.2392 -0.3871 21 18 0 0.1879 -0.0005 22 1 0 2.3276 0.0003 22 1 1 -1.2712 -0.2666 22 1 2 -1.1339 0.6807 22 1 3 1.1386 0.3441 22 1 4 -0.4069 -2.3495 22 1 5 0.5631 -0.9678 22 1 6 1.4980 -0.2105 22 2 0 1.0406 0.0003 22 2 1 -0.1105 -0.6304 22 2 2 -0.4655 -0.9605 22 2 3 1.5318 0.8333 22 2 4 0.5167 0.5582 22 2 5 -0.3476 -1.3651 22 2 6 2.9556 0.9598 22 3 0 -0.3452 -0.0003 22 3 1 0.4781 -0.8497 22 3 2 -0.1274 -1.6679 22 3 3 0.8165 -0.9073 22 3 4 0.5044 0.0071 22 3 5 -0.9610 -1.2494 22 3 6 0.2555 0.5063 22 4 0 0.3904 0.0002 22 4 1 0.4357 0.4659 22 4 2 0.5667 -0.1671 22 4 3 -0.1280 -2.8590 22 4 4 1.2452 -2.3124 22 4 5 -0.0948 0.3506 22 4 6 -1.6989 -0.0597 22 5 0 1.6754 0.0002 22 5 1 1.9664 1.6712 22 5 2 1.0914 -0.4689 22 5 3 -1.3929 -1.8794 22 5 4 -0.1967 -2.4114 22 5 5 0.1015 0.4230 22 6 0 0.9130 -0.0002 22 6 1 1.5112 0.5525 22 6 2 -0.0235 -0.9283 22 6 3 -1.6121 0.6907 22 6 4 -1.6494 -1.4430 22 6 5 -0.7970 -1.6952 22 7 0 -0.0507 0.0003 22 7 1 0.1793 -0.8281 22 7 2 -0.9159 -0.3342 22 7 3 -0.1087 1.2728 22 7 4 -0.4865 -0.2333 22 7 5 -0.3482 -1.9862 22 8 0 0.2923 0.0003 22 8 1 1.6004 -0.6923 22 8 2 -0.3866 -0.6546 22 8 3 0.6056 -0.1599 22 8 4 -0.4248 0.7287 22 8 5 0.4293 0.0735 22 9 0 0.4193 -0.0001 22 9 1 2.5798 -0.4521 22 9 2 -0.5060 -0.6219 22 9 3 0.0249 -0.8883 22 9 4 -1.4294 0.4937 22 9 5 0.0053 0.9852 22 10 0 0.1491 0.0002 22 10 1 1.9271 -1.1080 22 10 2 -1.1320 -0.3711 22 10 3 0.3209 0.1402 22 10 4 -0.6449 0.5913 22 11 0 -0.7095 0.0002 22 11 1 0.8852 -1.9876 22 11 2 -1.2263 -0.5577 22 11 3 1.4896 1.5076 22 11 4 -0.1325 1.3622 22 12 0 -0.9978 -0.0001 22 12 1 -0.5016 -2.3477 22 12 2 -1.8758 0.0653 22 12 3 1.4112 1.2834 22 12 4 -0.5955 0.9732 22 13 0 0.9603 0.0000 22 13 1 0.0196 -1.7791 22 13 2 -2.1755 0.6657 22 13 3 0.1973 0.0711 22 14 0 1.8184 -0.0001 22 14 1 1.2584 -0.5594 22 14 2 -0.5957 0.8972 22 14 3 -0.1481 -0.0617 22 15 0 0.4627 -0.0005 22 15 1 0.3237 0.0254 22 15 2 0.8906 0.7987 22 16 0 0.1994 -0.0004 22 16 1 -0.4326 -0.1835 22 17 0 0.5547 -0.0004 23 1 0 0.2526 -0.0000 23 1 1 -1.4688 0.0164 23 1 2 0.5177 -1.3829 23 1 3 1.0872 1.5941 23 1 4 1.7189 -2.0711 23 1 5 -2.1080 -0.3975 23 1 6 1.6915 0.3959 23 2 0 -1.5669 -0.0004 23 2 1 -0.7816 -0.1844 23 2 2 2.2969 -2.4058 23 2 3 0.4521 0.9362 23 2 4 2.3730 -1.1765 23 2 5 -2.0192 0.0501 23 2 6 1.5037 0.6509 23 3 0 -1.8826 -0.0005 23 3 1 -0.7570 -0.2541 23 3 2 1.0813 -0.8196 23 3 3 -0.9445 -2.7013 23 3 4 3.1466 -2.7630 23 3 5 -0.9405 0.3245 23 4 0 0.0314 -0.0003 23 4 1 0.6449 1.1256 23 4 2 -0.1220 0.9625 23 4 3 -1.6712 -2.5252 23 4 4 1.5767 -1.8136 23 4 5 0.0727 1.2516 23 5 0 0.9839 -0.0003 23 5 1 2.1040 0.9344 23 5 2 -0.0711 0.3225 23 5 3 -0.9497 0.2557 23 5 4 -0.4410 -0.0352 23 5 5 -0.3311 1.1940 23 6 0 0.0780 0.0001 23 6 1 0.6569 -0.5456 23 6 2 -0.6036 -0.7728 23 6 3 0.1812 0.3164 23 6 4 0.6637 0.3753 23 6 5 -1.0512 0.0358 23 7 0 0.0245 0.0001 23 7 1 0.1383 -0.3252 23 7 2 -0.1523 -0.7610 23 7 3 0.2285 -0.3140 23 7 4 1.3820 1.3051 23 7 5 -0.4790 0.0001 23 8 0 0.6966 -0.0002 23 8 1 1.0427 0.3699 23 8 2 1.1301 -0.0376 23 8 3 -0.1954 0.1107 23 8 4 -0.5987 1.1490 23 9 0 0.1967 0.0002 23 9 1 0.4477 0.2481 23 9 2 0.4036 -0.3506 23 9 3 0.1860 -0.3127 23 9 4 -1.3705 -0.2975 23 10 0 -0.3734 0.0003 23 10 1 0.3061 0.0708 23 10 2 -0.6525 -1.6131 23 10 3 1.4672 -0.3218 23 10 4 -0.3357 0.1961 23 11 0 -0.2716 -0.0002 23 11 1 0.2512 -0.0191 23 11 2 -0.3205 -0.8895 23 11 3 2.1983 0.8426 23 11 4 -0.1120 1.1108 23 12 0 0.3104 -0.0001 23 12 1 -0.6354 0.0327 23 12 2 -0.4738 0.5102 23 12 3 0.8946 0.7572 23 13 0 1.0683 0.0001 23 13 1 0.1629 0.2606 23 13 2 -0.8825 0.3271 23 13 3 -0.4441 -0.1017 23 14 0 0.6104 -0.0001 23 14 1 0.9307 0.2352 23 14 2 -0.3568 0.4880 23 15 0 -0.2389 0.0000 23 15 1 -0.0352 -0.0573 24 1 0 -0.9780 0.0003 24 1 1 -0.4497 0.3519 24 1 2 2.1388 -2.8989 24 1 3 -0.6274 1.5058 24 1 4 0.2779 -0.8197 24 1 5 -2.5902 0.6270 24 2 0 -1.3082 0.0002 24 2 1 -0.2830 -0.0373 24 2 2 2.1666 -2.0786 24 2 3 -0.8684 -1.0295 24 2 4 1.1210 -2.5860 24 2 5 -0.2983 1.6222 24 3 0 -1.0938 0.0002 24 3 1 -0.0855 0.0487 24 3 2 -1.1928 0.3191 24 3 3 -2.3934 -1.9210 24 3 4 0.2903 -1.8992 24 3 5 0.9647 1.7544 24 4 0 -0.5576 0.0001 24 4 1 0.6899 -0.1314 24 4 2 -2.2351 1.3769 24 4 3 -1.9404 0.5898 24 4 4 -1.9253 0.7847 24 4 5 0.9372 2.1050 24 5 0 0.1116 0.0001 24 5 1 0.4869 -1.2485 24 5 2 -1.2831 0.1586 24 5 3 0.8111 0.1237 24 5 4 -0.4461 0.6621 24 5 5 0.0221 1.8868 24 6 0 -0.1876 -0.0001 24 6 1 -0.2208 -0.8107 24 6 2 -0.6258 -0.8544 24 6 3 0.9043 -1.1974 24 6 4 1.9633 0.4277 24 6 5 -0.7110 0.8871 24 7 0 -0.4784 -0.0002 24 7 1 0.2716 0.7297 24 7 2 1.2990 0.1085 24 7 3 -1.0830 0.4819 24 7 4 0.6971 1.1764 24 8 0 -0.1886 -0.0000 24 8 1 -0.5680 1.7751 24 8 2 2.3571 0.7820 24 8 3 -1.0537 0.1321 24 8 4 -1.0891 -0.3622 24 9 0 0.0418 -0.0000 24 9 1 -1.5032 2.4776 24 9 2 0.6928 -0.4893 24 9 3 0.1596 -2.4146 24 9 4 -0.5568 -1.4539 24 10 0 0.7775 -0.0002 24 10 1 0.4991 2.1056 24 10 2 -0.0813 -0.6760 24 10 3 0.8793 -1.8669 24 11 0 0.9977 -0.0001 24 11 1 1.2256 1.5680 24 11 2 0.3014 0.7379 24 11 3 0.8540 0.0780 24 12 0 0.0239 0.0000 24 12 1 -0.3786 2.0956 24 12 2 -0.5879 0.2159 24 12 3 0.0359 0.1643 24 13 0 -0.5358 0.0001 24 13 1 -0.2277 1.8289 24 13 2 -1.2263 -0.9019 24 14 0 -0.5207 0.0002 24 14 1 0.5282 0.3776 25 1 0 0.7302 0.0001 25 1 1 0.8905 -0.6416 25 1 2 1.8318 -2.6157 25 1 3 -0.0942 0.8699 25 1 4 -0.3733 -1.7783 25 1 5 -0.2471 0.1099 25 2 0 1.0774 0.0002 25 2 1 0.1840 -0.2184 25 2 2 1.0682 -1.2445 25 2 3 -0.2386 -0.2019 25 2 4 0.1726 -2.5030 25 2 5 1.6272 1.7916 25 3 0 -0.4243 0.0002 25 3 1 -0.4192 -0.4742 25 3 2 -1.8301 0.6584 25 3 3 -2.5979 1.3697 25 3 4 -1.8511 0.0146 25 3 5 1.5836 2.1014 25 4 0 -0.4141 0.0002 25 4 1 -0.3205 -1.6169 25 4 2 -2.1075 1.3757 25 4 3 -1.3909 1.0366 25 4 4 -1.7506 0.4410 25 4 5 1.0762 1.7052 25 5 0 0.6602 -0.0000 25 5 1 -0.4143 -1.6718 25 5 2 -1.1270 0.3640 25 5 3 0.9023 -1.5498 25 5 4 0.9535 -1.0956 25 6 0 -0.3093 0.0001 25 6 1 0.0355 -0.4761 25 6 2 0.0903 -0.2326 25 6 3 -0.5230 -0.6781 25 6 4 1.2036 -0.1163 25 7 0 -0.9460 0.0003 25 7 1 0.3520 0.9119 25 7 2 1.6640 0.2561 25 7 3 -1.5494 0.2556 25 7 4 -0.4859 0.5266 25 8 0 -0.3073 -0.0001 25 8 1 -1.4468 2.3966 25 8 2 1.1834 0.1916 25 8 3 -0.2311 -2.5713 25 8 4 -0.7566 -0.7645 25 9 0 0.4008 -0.0001 25 9 1 -1.2695 2.0906 25 9 2 -0.3356 0.2144 25 9 3 0.1637 -3.7244 25 10 0 1.2046 0.0002 25 10 1 1.8513 0.5134 25 10 2 -0.4155 1.2547 25 10 3 -0.1594 -1.5178 25 11 0 0.5612 -0.0001 25 11 1 1.6017 1.4348 25 11 2 -0.6527 1.1419 25 12 0 -0.7959 -0.0001 25 12 1 -0.9151 3.0448 25 12 2 -1.2852 -0.4542 25 13 0 -0.5621 0.0001 25 13 1 -0.6970 1.8565 26 1 0 1.7895 -0.0002 26 1 1 0.2905 -0.7629 26 1 2 1.9974 -1.0283 26 1 3 2.8065 1.0544 26 1 4 2.1900 -2.1792 26 1 5 0.4801 -0.4279 26 2 0 0.8756 -0.0003 26 2 1 -1.0150 0.2574 26 2 2 1.3491 -0.3887 26 2 3 1.0742 1.3533 26 2 4 0.9420 -0.9085 26 2 5 0.6987 1.4224 26 3 0 -0.4960 -0.0002 26 3 1 -0.7037 -0.2931 26 3 2 -0.7222 0.8174 26 3 3 -1.7509 1.4583 26 3 4 -0.4093 0.1857 26 3 5 0.3471 1.3418 26 4 0 0.3663 -0.0002 26 4 1 0.0617 -0.7185 26 4 2 -0.8601 1.3746 26 4 3 -0.7579 -0.1074 26 4 4 0.7113 -1.4474 26 5 0 0.4922 -0.0002 26 5 1 -0.6060 -0.6887 26 5 2 0.0024 0.2467 26 5 3 0.0956 -0.6663 26 5 4 1.2421 -1.7415 26 6 0 -0.4785 0.0002 26 6 1 -0.3929 -0.4363 26 6 2 0.7989 -1.0678 26 6 3 -0.5617 -0.2775 26 6 4 0.2337 -0.0002 26 7 0 -0.2725 -0.0001 26 7 1 -0.5802 0.8698 26 7 2 0.9253 -1.3346 26 7 3 0.3147 -1.7841 26 8 0 -0.4208 -0.0003 26 8 1 -2.8586 1.0794 26 8 2 0.2212 -0.3543 26 8 3 1.0767 -2.9405 26 9 0 -0.5044 0.0002 26 9 1 -2.1869 -0.9707 26 9 2 -0.2295 0.9942 26 9 3 0.2465 -1.6593 26 10 0 0.1911 -0.0000 26 10 1 0.7846 -0.9202 26 10 2 -0.4338 1.2077 26 11 0 -0.2366 -0.0001 26 11 1 0.2473 1.7729 26 11 2 -0.7470 0.4075 26 12 0 -0.6082 0.0003 26 12 1 -1.1811 2.2648 27 1 0 -0.1088 0.0001 27 1 1 -0.5352 0.4344 27 1 2 1.7787 0.4451 27 1 3 3.0877 0.2999 27 1 4 2.1432 -0.5834 27 1 5 -0.0857 -0.0674 27 2 0 -0.5118 -0.0001 27 2 1 -0.6870 0.5285 27 2 2 0.8994 -0.1531 27 2 3 0.8701 -0.1780 27 2 4 0.2411 0.3127 27 3 0 -0.2235 0.0001 27 3 1 1.1519 0.3530 27 3 2 -0.2224 0.2139 27 3 3 -0.3127 -0.0539 27 3 4 0.5669 -0.4792 27 4 0 -0.2771 0.0000 27 4 1 0.6123 0.4465 27 4 2 0.0027 0.4818 27 4 3 0.6233 0.5011 27 4 4 1.1083 -1.5448 27 5 0 -0.8802 -0.0001 27 5 1 -1.2293 -0.2098 27 5 2 0.5962 -0.6877 27 5 3 0.9928 -0.1261 27 5 4 0.5555 -0.8241 27 6 0 -0.4057 -0.0001 27 6 1 -0.5801 0.0724 27 6 2 0.6839 -2.0648 27 6 3 1.1567 -1.6030 27 7 0 -0.1840 -0.0000 27 7 1 -1.3028 0.5652 27 7 2 0.8296 -1.5567 27 7 3 1.5382 -1.7309 27 8 0 -1.2742 0.0003 27 8 1 -4.0440 -1.0409 27 8 2 0.9633 0.2581 27 8 3 0.8791 -0.6802 27 9 0 -1.1750 -0.0001 27 9 1 -3.0403 -1.9300 27 9 2 0.5007 0.7630 27 10 0 -0.2753 0.0000 27 10 1 -0.3064 -0.1063 27 11 0 -0.3298 0.0009 28 1 0 -0.9245 0.0000 28 1 1 0.4592 0.7332 28 1 2 0.2017 1.0545 28 1 3 -0.0079 -0.6122 28 1 4 -0.3591 -0.0516 28 2 0 0.4364 0.0002 28 2 1 1.5783 -0.4291 28 2 2 0.0796 -0.6482 28 2 3 -0.1396 -0.7212 28 2 4 -0.5504 -0.0780 28 3 0 0.3307 0.0002 28 3 1 2.0373 0.0306 28 3 2 -0.3562 -0.6771 28 3 3 1.0520 0.6979 28 3 4 0.4612 -0.5986 28 4 0 -0.9535 0.0001 28 4 1 -0.2167 0.2515 28 4 2 -0.4624 0.2735 28 4 3 1.9659 0.6614 28 5 0 -1.2132 0.0000 28 5 1 -0.7186 0.1050 28 5 2 -0.4222 -0.1699 28 5 3 1.7801 -1.2583 28 6 0 -0.4553 0.0002 28 6 1 0.8962 0.3518 28 6 2 -0.0131 -1.0209 28 6 3 1.3082 -1.3032 28 7 0 -0.2202 0.0005 28 7 1 -0.3463 -0.5959 28 7 2 0.8595 -0.2083 28 8 0 -0.6045 0.0000 28 8 1 -2.5127 -1.5206 28 8 2 0.7974 0.6240 28 9 0 -0.4488 -0.0003 28 9 1 -1.4325 -0.6102 29 1 0 0.7231 -0.0000 29 1 1 2.0811 -0.5339 29 1 2 -0.4430 1.1591 29 1 3 -2.3858 0.9905 29 1 4 -0.7139 -0.6653 29 2 0 1.3154 -0.0002 29 2 1 2.1943 -1.2162 29 2 2 -0.0448 -1.2281 29 2 3 -0.6792 1.7006 29 2 4 -0.0704 -0.4866 29 3 0 0.5512 -0.0002 29 3 1 0.5006 -0.2751 29 3 2 -0.7578 -0.4933 29 3 3 1.2200 1.6077 29 4 0 -0.1548 0.0000 29 4 1 -0.9581 0.4893 29 4 2 -1.2888 1.3931 29 4 3 1.4065 -0.1949 29 5 0 -0.8614 -0.0001 29 5 1 0.3186 0.6920 29 5 2 -1.1061 0.8711 29 5 3 0.6784 -0.7725 29 6 0 -0.2864 -0.0002 29 6 1 1.7602 -0.1688 29 6 2 -0.2113 -0.0328 29 7 0 1.0067 -0.0007 29 7 1 0.7396 -0.9605 29 8 0 0.6736 -0.0012 30 1 0 0.2153 0.0001 30 1 1 1.6809 -0.2152 30 1 2 -0.1832 1.0302 30 1 3 -2.3971 2.6402 30 2 0 -0.6690 -0.0002 30 2 1 0.8584 -0.1188 30 2 2 0.0632 -1.2461 30 2 3 -0.6077 2.4555 30 3 0 0.4213 0.0001 30 3 1 -0.6206 0.7797 30 3 2 -0.3977 0.3835 30 3 3 0.4470 0.6363 30 4 0 0.2949 0.0002 30 4 1 -1.0120 1.6577 30 4 2 -0.6744 1.5200 30 5 0 -1.1925 -0.0002 30 5 1 0.1547 0.8663 30 5 2 -0.3662 0.3734 30 6 0 0.0261 -0.0011 30 6 1 0.9301 -0.3618 31 1 0 -2.7991 0.0002 31 1 1 0.3151 2.0799 31 1 2 -0.4833 0.7755 31 1 3 -1.1557 1.6138 31 2 0 -2.4111 0.0001 31 2 1 0.7808 0.9240 31 2 2 0.3520 -0.6035 31 3 0 0.4649 0.0000 31 3 1 -0.1731 1.3815 31 3 2 0.3284 0.5506 31 4 0 -0.2639 0.0005 31 4 1 -0.6708 1.4609 31 5 0 -1.4591 0.0004 32 1 0 -3.8131 0.0000 32 1 1 0.9728 1.8316 32 1 2 -0.6195 0.3402 32 2 0 -1.5119 -0.0009 32 2 1 1.6278 -0.0840 32 3 0 0.6563 -0.0007 32 3 1 0.0858 0.3906 33 1 0 -2.0170 -0.0004 33 1 1 1.8415 -0.3301 0 0 0 0.0 0.0 ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' 'x-y, x, z+2/3' '-y, x-y, z+1/3' '-x, -y, z' '-x+y, -x, z+2/3' 'y, -x+y, z+1/3' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.34009(6) 0.64286(5) 0.4511(2) 0.0600(4) Uani 1 1 d . . . . . H1 H 0.328542 0.646008 0.353451 0.090 Uiso 1 1 calc R U . . . O2 O 0.4598(7) 0.2864(7) 0.762(3) 0.121(5) Uani 0.325(13) 1 d D U P A 1 C1 C 0.38689(8) 0.60760(8) 0.3279(3) 0.0486(5) Uani 1 1 d . . . . . C2 C 0.34301(8) 0.59993(7) 0.4416(3) 0.0483(5) Uani 1 1 d . . . . . H2 H 0.314180 0.575152 0.379374 0.058 Uiso 1 1 calc R U . . . C3 C 0.34332(9) 0.58445(8) 0.6401(3) 0.0552(6) Uani 1 1 d . . . . . H3A H 0.315351 0.580792 0.705413 0.066 Uiso 1 1 calc R U . . . H3B H 0.371398 0.608934 0.704248 0.066 Uiso 1 1 calc R U . . . C4 C 0.34346(9) 0.53738(8) 0.6469(3) 0.0559(6) Uani 1 1 d . . . . . H4A H 0.313956 0.512450 0.592502 0.067 Uiso 1 1 calc R U . . . H4B H 0.344389 0.529022 0.776958 0.067 Uiso 1 1 calc R U . . . C5 C 0.38636(7) 0.53919(8) 0.5406(3) 0.0461(5) Uani 1 1 d . . . . . C6 C 0.38906(7) 0.56019(7) 0.3408(3) 0.0427(5) Uani 1 1 d . . . . . H6 H 0.359928 0.536195 0.277727 0.051 Uiso 1 1 calc R U . . . C7 C 0.42908(8) 0.56057(9) 0.2316(3) 0.0579(6) Uani 1 1 d . . . . . H7A H 0.458889 0.578703 0.299388 0.069 Uiso 1 1 calc R U . . . H7B H 0.432331 0.575786 0.110860 0.069 Uiso 1 1 calc R U . . . C8 C 0.41873(9) 0.51001(9) 0.2027(3) 0.0630(6) Uani 1 1 d . . . . . H8A H 0.444449 0.510566 0.130586 0.076 Uiso 1 1 calc R U . . . H8B H 0.389495 0.492482 0.130871 0.076 Uiso 1 1 calc R U . . . C9 C 0.41352(8) 0.48429(8) 0.3873(3) 0.0528(6) Uani 1 1 d . . . . . H9 H 0.445205 0.500640 0.445760 0.063 Uiso 1 1 calc R U . . . C10 C 0.38099(8) 0.48931(7) 0.5217(3) 0.0468(5) Uani 1 1 d . . . . . C11 C 0.35128(9) 0.45282(9) 0.6334(4) 0.0649(7) Uani 1 1 d . . . . . H11 H 0.330259 0.457313 0.708079 0.078 Uiso 1 1 calc R U . . . C12 C 0.34924(9) 0.40502(9) 0.6475(4) 0.0643(7) Uani 1 1 d . . . . . H12A H 0.320976 0.380833 0.583378 0.077 Uiso 1 1 calc R U . . . H12B H 0.346993 0.395857 0.778375 0.077 Uiso 1 1 calc R U . . . C13 C 0.39368(8) 0.40770(8) 0.5601(3) 0.0520(5) Uani 1 1 d . . . . . C14 C 0.40053(9) 0.43142(8) 0.3647(3) 0.0565(6) Uani 1 1 d . . . . . C15 C 0.43964(10) 0.42443(10) 0.2798(4) 0.0720(8) Uani 1 1 d . . . . . H15A H 0.470845 0.448760 0.323701 0.086 Uiso 1 1 calc R U . . . H15B H 0.438995 0.425587 0.143846 0.086 Uiso 1 1 calc R U . . . C16 C 0.42805(10) 0.37446(10) 0.3481(4) 0.0761(8) Uani 1 1 d . . . . . H16A H 0.456880 0.375168 0.390924 0.091 Uiso 1 1 calc R U . . . H16B H 0.414295 0.351433 0.246920 0.091 Uiso 1 1 calc R U . . . C17 C 0.39205(9) 0.36066(9) 0.5110(3) 0.0619(6) Uani 1 1 d D . . . . H17 H 0.361056 0.342107 0.448627 0.074 Uiso 0.325(13) 1 calc R U P A 1 H17A H 0.360131 0.338364 0.462436 0.074 Uiso 0.675(13) 1 calc R U P A 2 C18 C 0.43216(9) 0.65195(8) 0.3898(4) 0.0691(7) Uani 1 1 d . . . . . H18A H 0.429417 0.679662 0.364934 0.104 Uiso 1 1 calc R U . . . H18B H 0.458893 0.654278 0.321891 0.104 Uiso 1 1 calc R U . . . H18C H 0.436860 0.650005 0.521826 0.104 Uiso 1 1 calc R U . . . C19 C 0.37784(9) 0.61417(9) 0.1194(3) 0.0633(6) Uani 1 1 d . . . . . H19A H 0.348978 0.586629 0.077527 0.095 Uiso 1 1 calc R U . . . H19B H 0.404178 0.617870 0.044525 0.095 Uiso 1 1 calc R U . . . H19C H 0.374771 0.642078 0.106852 0.095 Uiso 1 1 calc R U . . . C20 C 0.43135(9) 0.56857(9) 0.6599(3) 0.0635(6) Uani 1 1 d . . . . . H20A H 0.434183 0.598815 0.690262 0.095 Uiso 1 1 calc R U . . . H20B H 0.458974 0.573707 0.590457 0.095 Uiso 1 1 calc R U . . . H20C H 0.429015 0.551565 0.773464 0.095 Uiso 1 1 calc R U . . . C21 C 0.43611(10) 0.43720(9) 0.6882(3) 0.0680(7) Uani 1 1 d . . . . . H21A H 0.439741 0.468297 0.705526 0.102 Uiso 1 1 calc R U . . . H21B H 0.464568 0.440357 0.632279 0.102 Uiso 1 1 calc R U . . . H21C H 0.430800 0.421570 0.807565 0.102 Uiso 1 1 calc R U . . . C22 C 0.35598(10) 0.40548(10) 0.2453(4) 0.0775(8) Uani 1 1 d . . . . . H22A H 0.331789 0.411597 0.293182 0.116 Uiso 1 1 calc R U . . . H22B H 0.344546 0.371783 0.248828 0.116 Uiso 1 1 calc R U . . . H22C H 0.363358 0.416634 0.118140 0.116 Uiso 1 1 calc R U . . . C23 C 0.3909(8) 0.3250(7) 0.668(3) 0.066(4) Uani 0.325(13) 1 d D U P A 1 H23 H 0.420881 0.343405 0.736758 0.079 Uiso 0.325(13) 1 calc R U P A 1 C24 C 0.3536(7) 0.3114(9) 0.809(3) 0.079(5) Uani 0.325(13) 1 d D U P A 1 H24A H 0.354240 0.339558 0.856001 0.119 Uiso 0.325(13) 1 calc R U P A 1 H24B H 0.358967 0.295096 0.910053 0.119 Uiso 0.325(13) 1 calc R U P A 1 H24C H 0.322985 0.290690 0.753156 0.119 Uiso 0.325(13) 1 calc R U P A 1 C25 C 0.3939(11) 0.2826(10) 0.582(4) 0.085(4) Uani 0.325(13) 1 d D U P A 1 H25A H 0.362667 0.259669 0.533601 0.102 Uiso 0.325(13) 1 calc R U P A 1 H25B H 0.415763 0.294368 0.476556 0.102 Uiso 0.325(13) 1 calc R U P A 1 C26 C 0.4101(8) 0.2565(7) 0.715(4) 0.088(4) Uani 0.325(13) 1 d D U P A 1 H26 H 0.391743 0.250160 0.831041 0.105 Uiso 0.325(13) 1 calc R U P A 1 C27 C 0.4729(8) 0.2807(10) 0.949(3) 0.137(8) Uani 0.325(13) 1 d D U P A 1 H27A H 0.500391 0.276670 0.944468 0.206 Uiso 0.325(13) 1 calc R U P A 1 H27B H 0.446788 0.253046 1.006410 0.206 Uiso 0.325(13) 1 calc R U P A 1 H27C H 0.480287 0.308491 1.022388 0.206 Uiso 0.325(13) 1 calc R U P A 1 C28 C 0.3981(8) 0.2076(6) 0.629(3) 0.091(4) Uani 0.325(13) 1 d D U P A 1 C29 C 0.3789(11) 0.1661(7) 0.741(4) 0.118(6) Uani 0.325(13) 1 d D U P A 1 H29A H 0.378852 0.138997 0.697664 0.142 Uiso 0.325(13) 1 calc R U P A 1 H29B H 0.366178 0.165849 0.858751 0.142 Uiso 0.325(13) 1 calc R U P A 1 C30 C 0.4183(6) 0.2094(6) 0.445(2) 0.080(3) Uani 0.325(13) 1 d D U P A 1 H30 H 0.416080 0.233187 0.366398 0.096 Uiso 0.325(13) 1 calc R U P A 1 C31 C 0.4680(5) 0.2248(9) 0.482(3) 0.149(7) Uani 0.325(13) 1 d D U P A 1 H31A H 0.485241 0.258664 0.502823 0.223 Uiso 0.325(13) 1 calc R U P A 1 H31B H 0.481381 0.217222 0.376185 0.223 Uiso 0.325(13) 1 calc R U P A 1 H31C H 0.470167 0.208695 0.591331 0.223 Uiso 0.325(13) 1 calc R U P A 1 C32 C 0.3852(6) 0.1559(6) 0.354(3) 0.146(6) Uani 0.325(13) 1 d D U P A 1 H32A H 0.368989 0.133294 0.452623 0.219 Uiso 0.325(13) 1 calc R U P A 1 H32B H 0.405137 0.146976 0.285786 0.219 Uiso 0.325(13) 1 calc R U P A 1 H32C H 0.362076 0.156249 0.270119 0.219 Uiso 0.325(13) 1 calc R U P A 1 O2A O 0.4679(2) 0.2978(2) 0.7222(11) 0.0827(16) Uani 0.675(13) 1 d D U P A 2 C23A C 0.4037(4) 0.3349(3) 0.6707(13) 0.0637(18) Uani 0.675(13) 1 d D U P A 2 H23A H 0.436740 0.355529 0.712282 0.076 Uiso 0.675(13) 1 calc R U P A 2 C24A C 0.3713(4) 0.3227(4) 0.8336(13) 0.083(3) Uani 0.675(13) 1 d D U P A 2 H24D H 0.379188 0.351267 0.902652 0.124 Uiso 0.675(13) 1 calc R U P A 2 H24E H 0.374751 0.300770 0.913594 0.124 Uiso 0.675(13) 1 calc R U P A 2 H24F H 0.338872 0.308299 0.790403 0.124 Uiso 0.675(13) 1 calc R U P A 2 C25A C 0.3986(5) 0.2884(4) 0.5856(14) 0.071(2) Uani 0.675(13) 1 d D U P A 2 H25C H 0.364952 0.265991 0.564592 0.086 Uiso 0.675(13) 1 calc R U P A 2 H25D H 0.414443 0.295784 0.464640 0.086 Uiso 0.675(13) 1 calc R U P A 2 C26A C 0.4191(3) 0.2650(3) 0.7078(14) 0.0675(16) Uani 0.675(13) 1 d D U P A 2 H26A H 0.404645 0.259332 0.832787 0.081 Uiso 0.675(13) 1 calc R U P A 2 C27A C 0.4918(3) 0.2900(4) 0.8736(13) 0.117(3) Uani 0.675(13) 1 d D U P A 2 H27D H 0.489008 0.259147 0.860392 0.176 Uiso 0.675(13) 1 calc R U P A 2 H27E H 0.477566 0.291327 0.990052 0.176 Uiso 0.675(13) 1 calc R U P A 2 H27F H 0.524893 0.314217 0.872532 0.176 Uiso 0.675(13) 1 calc R U P A 2 C28A C 0.4117(4) 0.2184(3) 0.6296(13) 0.0836(19) Uani 0.675(13) 1 d D U P A 2 C29A C 0.3803(6) 0.1778(3) 0.727(2) 0.147(5) Uani 0.675(13) 1 d D U P A 2 H29C H 0.372229 0.147823 0.680058 0.176 Uiso 0.675(13) 1 calc R U P A 2 H29D H 0.367248 0.180371 0.839589 0.176 Uiso 0.675(13) 1 calc R U P A 2 C30A C 0.4349(4) 0.2202(4) 0.4536(13) 0.109(3) Uani 0.675(13) 1 d D U P A 2 H30A H 0.453152 0.253762 0.415222 0.131 Uiso 0.675(13) 1 calc R U P A 2 C31A C 0.4678(4) 0.2028(4) 0.4677(19) 0.156(4) Uani 0.675(13) 1 d D U P A 2 H31D H 0.493916 0.223578 0.547768 0.234 Uiso 0.675(13) 1 calc R U P A 2 H31E H 0.479760 0.202073 0.345218 0.234 Uiso 0.675(13) 1 calc R U P A 2 H31F H 0.451767 0.171188 0.519675 0.234 Uiso 0.675(13) 1 calc R U P A 2 C32A C 0.3934(3) 0.1913(5) 0.2923(13) 0.200(5) Uani 0.675(13) 1 d D U P A 2 H32D H 0.377248 0.208710 0.265402 0.300 Uiso 0.675(13) 1 calc R U P A 2 H32E H 0.370837 0.160076 0.338112 0.300 Uiso 0.675(13) 1 calc R U P A 2 H32F H 0.408140 0.188363 0.179966 0.300 Uiso 0.675(13) 1 calc R U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0918(12) 0.0674(10) 0.0445(9) -0.0100(8) -0.0102(8) 0.0576(9) O2 0.111(7) 0.111(9) 0.115(7) 0.033(6) -0.016(6) 0.037(6) C1 0.0615(13) 0.0616(13) 0.0381(11) -0.0010(10) 0.0007(10) 0.0422(12) C2 0.0638(13) 0.0489(12) 0.0423(11) -0.0120(10) -0.0073(10) 0.0356(11) C3 0.0791(16) 0.0692(14) 0.0383(11) -0.0035(11) 0.0085(11) 0.0528(13) C4 0.0816(16) 0.0739(15) 0.0301(11) 0.0006(10) 0.0105(11) 0.0523(13) C5 0.0615(13) 0.0637(13) 0.0291(9) -0.0037(9) 0.0029(10) 0.0433(11) C6 0.0521(12) 0.0582(12) 0.0289(10) -0.0028(9) -0.0045(9) 0.0360(10) C7 0.0744(15) 0.0842(16) 0.0353(11) 0.0102(11) 0.0042(11) 0.0548(14) C8 0.0878(17) 0.0915(18) 0.0380(12) 0.0071(12) 0.0118(12) 0.0661(15) C9 0.0723(14) 0.0730(15) 0.0365(11) -0.0035(11) -0.0019(11) 0.0538(13) C10 0.0597(13) 0.0606(13) 0.0342(10) -0.0016(10) -0.0031(10) 0.0406(11) C11 0.0767(16) 0.0746(16) 0.0610(15) 0.0016(13) 0.0115(13) 0.0510(14) C12 0.0864(17) 0.0663(15) 0.0546(14) 0.0096(12) 0.0127(13) 0.0489(14) C13 0.0671(14) 0.0615(13) 0.0439(12) -0.0074(11) -0.0057(11) 0.0445(12) C14 0.0780(16) 0.0703(15) 0.0430(12) -0.0115(12) -0.0068(12) 0.0533(13) C15 0.110(2) 0.0946(19) 0.0443(13) -0.0059(13) 0.0019(14) 0.0762(18) C16 0.108(2) 0.0960(19) 0.0642(16) -0.0117(15) -0.0027(16) 0.0806(18) C17 0.0785(16) 0.0667(14) 0.0564(13) -0.0157(11) -0.0166(13) 0.0483(13) C18 0.0696(16) 0.0623(15) 0.0766(17) -0.0048(14) -0.0058(14) 0.0339(13) C19 0.0918(17) 0.0763(16) 0.0430(12) 0.0067(12) -0.0003(13) 0.0578(15) C20 0.0861(17) 0.0753(16) 0.0457(13) -0.0080(12) -0.0147(12) 0.0528(14) C21 0.104(2) 0.0730(16) 0.0451(13) -0.0044(12) -0.0176(14) 0.0577(15) C22 0.110(2) 0.0931(19) 0.0610(16) -0.0258(15) -0.0337(16) 0.0747(18) C23 0.072(8) 0.072(7) 0.060(5) -0.011(4) -0.021(4) 0.040(6) C24 0.088(10) 0.070(10) 0.094(9) 0.008(7) 0.005(7) 0.049(8) C25 0.099(9) 0.076(7) 0.098(8) 0.006(6) 0.007(6) 0.057(7) C26 0.096(7) 0.084(6) 0.099(7) 0.010(5) 0.006(6) 0.057(5) C27 0.140(14) 0.153(16) 0.120(9) 0.029(10) -0.023(9) 0.073(12) C28 0.102(9) 0.083(6) 0.110(6) 0.019(4) 0.016(6) 0.061(6) C29 0.143(13) 0.089(8) 0.125(10) 0.028(8) 0.023(9) 0.060(10) C30 0.082(6) 0.071(6) 0.104(6) 0.009(5) 0.004(5) 0.050(5) C31 0.084(6) 0.199(16) 0.171(14) 0.017(13) 0.004(6) 0.076(7) C32 0.182(11) 0.093(8) 0.144(11) -0.020(7) -0.025(10) 0.054(7) O2A 0.082(3) 0.059(2) 0.106(4) 0.012(2) -0.015(2) 0.035(2) C23A 0.082(5) 0.055(3) 0.066(2) -0.011(2) -0.019(3) 0.043(3) C24A 0.114(7) 0.079(5) 0.066(3) -0.004(3) -0.008(4) 0.057(5) C25A 0.106(5) 0.062(3) 0.065(3) -0.012(3) -0.027(3) 0.056(4) C26A 0.081(3) 0.052(2) 0.076(3) 0.006(2) -0.013(3) 0.038(2) C27A 0.111(5) 0.119(6) 0.126(6) 0.009(5) -0.039(5) 0.062(5) C28A 0.100(5) 0.066(3) 0.102(4) -0.003(3) -0.011(3) 0.055(3) C29A 0.184(8) 0.064(4) 0.197(10) 0.020(5) 0.063(8) 0.066(5) C30A 0.110(6) 0.115(6) 0.113(4) -0.015(4) -0.002(4) 0.065(5) C31A 0.184(7) 0.170(7) 0.179(7) 0.022(6) 0.043(5) 0.136(6) C32A 0.186(7) 0.227(13) 0.121(6) -0.033(7) -0.034(5) 0.054(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u 4 -4 0 59.39 4.4 1 4 0 7.6 2.8 4 -5 0 7.3 3.1 5 -1 0 7.2 2.9 -1 -4 0 13 3.6 -4 5 0 2.4 1.7 3 -5 0 235.08 11.7 -2 -3 0 222.18 12 5 -2 0 211.38 11.3 5 -2 0 231.78 11.6 2 -5 0 241.68 12.4 5 -3 0 259.07 12 5 -3 0 215.08 12.2 1 5 0 3368.76 156.78 5 -6 0 3540.15 156.28 -1 -5 0 3457.95 156.88 6 -1 0 3443.76 156.38 -5 6 0 3609.44 156.28 4 -6 0 1418.86 67.79 2 4 0 1677.43 69.19 -6 2 0 1449.35 67.59 -4 6 0 1378.76 67.59 6 -2 0 1558.04 67.69 6 -2 0 1473.35 67.59 3 -6 0 910.31 43.2 -6 3 0 841.12 42.5 -6 3 0 902.11 42.7 3 3 0 997 43.6 6 -3 0 931.01 42.8 -3 6 0 952.4 43.2 6 -3 0 1001.4 42.8 -6 4 0 8028 361.46 6 -4 0 8200.58 361.56 6 0 0 5925.41 263.17 0 6 0 5841.82 263.57 6 -7 0 349.17 17.1 1 6 0 323.27 17.8 -6 7 0 327.27 16.8 -1 -6 0 331.87 17.8 7 -1 0 344.67 17.4 -7 2 0 1111.89 47.5 5 -7 0 988.9 47.4 -5 7 0 992.2 47.3 -2 -5 0 997.5 48.1 7 -2 0 1041.6 47.5 3 4 0 3761.82 175.88 -7 3 0 3593.54 174.98 -7 3 0 4047.5 175.18 4 -7 0 3863.31 175.58 7 -3 0 4012.9 175.28 -3 -4 0 3782.32 175.98 7 -3 0 4186.88 175.38 -4 7 0 4038.4 175.58 3 -7 0 82.79 7.5 -7 4 0 94.49 6.4 -7 4 0 90.19 6.5 4 3 0 103.29 8.9 7 -4 0 91.29 6.8 -4 -3 0 88.19 7.6 -3 7 0 79.29 7 7 -4 0 84.29 6.5 5 2 0 1046.3 49.4 -7 5 0 1036.8 48.5 -7 5 0 1119.39 48.5 2 -7 0 1080.09 49.5 -5 -2 0 1032.7 49.3 7 -5 0 1081.89 48.7 -2 7 0 1022.5 49.3 1 -7 0 593.74 30.7 -7 6 0 633.84 29.7 7 -6 0 649.04 29.9 -1 7 0 650.03 30.7 0 -7 0 915.41 39.4 -7 7 0 762.12 36.8 7 0 0 757.22 37.5 7 -7 0 777.62 37 0 7 0 764.42 37.9 7 -8 0 351.16 17.6 1 7 0 323.97 18.4 -7 8 0 345.27 17.3 8 -1 0 338.67 17.9 -8 2 0 1070.99 50.49 2 6 0 1050.19 51.09 6 -8 0 1085.59 50.49 -2 -6 0 1091.29 51.29 8 -2 0 1124.99 50.49 -6 8 0 1110.79 50.29 5 -8 0 2109.59 98.79 -8 3 0 2105.59 98.39 3 5 0 2114.29 99.29 -8 3 0 2267.17 98.49 8 -3 0 2200.98 98.59 -5 8 0 2081.89 98.69 8 -3 0 2362.06 98.69 -8 4 0 467.05 21.8 4 4 0 467.05 23 -8 4 0 440.56 21.7 4 -8 0 457.85 22.6 8 -4 0 409.26 21.8 -4 8 0 468.45 22.5 8 -4 0 439.56 21.9 -8 5 0 273.37 13.9 5 3 0 269.47 15.1 -8 5 0 290.87 14 3 -8 0 282.77 15.2 -5 -3 0 258.87 15.1 -3 8 0 253.67 14.6 8 -5 0 245.28 14.1 8 -5 0 284.97 14.2 -8 6 0 33.9 4.3 -8 6 0 29.9 4.4 6 2 0 37.2 5.2 2 -8 0 31.5 5.1 -2 8 0 25.9 4.9 -6 -2 0 27.9 4.8 8 -6 0 40.1 4.8 1 -8 0 6294.57 274.37 -8 7 0 5937.01 272.97 8 -7 0 6103.99 273.27 8 0 0 1550.84 68.19 -8 8 0 1442.26 67.29 8 -8 0 1480.25 67.59 0 8 0 1429.66 68.59 1 8 0 800.52 40.1 8 -9 0 832.12 39.2 -8 9 0 837.32 39 9 -1 0 830.12 39.5 -1 -8 0 838.42 40.3 7 -9 0 4837.22 206.28 -9 2 0 4583.34 206.08 2 7 0 4608.44 206.98 -9 2 0 4115.49 205.78 -7 9 0 4874.21 206.08 9 -2 0 4521.65 206.08 6 -9 0 57.69 6.5 -9 3 0 50.49 5.7 -9 3 0 60.79 6.3 3 6 0 87.79 9.2 -6 9 0 57.59 6 9 -3 0 59.19 6.5 -3 -6 0 90.69 11.9 4 5 0 294.87 17.1 5 -9 0 257.77 15.1 -9 4 0 287.67 14.6 -9 4 0 251.07 14.4 -5 9 0 272.47 15 9 -4 0 311.87 14.8 9 -4 0 261.57 14.6 -9 5 0 1615.44 70.99 5 4 0 1490.15 72.09 -9 5 0 1603.64 70.99 4 -9 0 1548.45 71.89 9 -5 0 1520.15 71.09 -5 -4 0 1575.84 72.19 9 -5 0 1579.04 71.19 -4 9 0 1536.55 71.79 -9 6 0 3814.32 167.48 -9 6 0 3833.82 167.58 6 3 0 3722.83 168.68 3 -9 0 3670.73 168.58 9 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49 -10 6 0 499.25 23.2 -10 6 0 458.75 23 4 -10 0 479.25 24.4 10 -6 0 466.55 23.3 10 -6 0 474.95 23.4 -4 10 0 463.85 24.1 -6 -4 0 460.15 24.5 -10 7 0 4386.26 187.48 3 -10 0 4099.59 188.78 -10 7 0 4345.27 187.48 7 3 0 4117.49 188.68 10 -7 0 4338.17 187.78 -3 10 0 3975.6 188.58 -7 -3 0 3982.6 188.58 -10 8 0 19.8 4.1 8 2 0 17.5 4.3 -10 8 0 21.8 4.3 2 -10 0 21 4.8 -8 -2 0 14.7 4.8 -2 10 0 39.5 10.2 10 -8 0 17 4.7 -10 9 0 1011 47.3 -1 10 0 1032.5 48.9 10 -9 0 1010.3 47.7 0 -10 0 113.49 14.7 -10 10 0 56.79 6.2 10 0 0 79.09 8.5 10 -10 0 65.69 7 0 10 0 69.49 8 10 -11 0 669.83 32.9 1 10 0 658.63 34 -10 11 0 685.93 32.6 -1 -10 0 664.43 34.3 11 -1 0 685.03 33.4 2 9 0 180.88 12.7 9 -11 0 183.28 11.8 -11 2 0 199.98 12 -11 2 0 183.88 11.6 -2 -9 0 177.28 12.9 11 -2 0 178.48 11.9 -9 11 0 170.38 11 3 8 0 302.07 18.1 -11 3 0 316.47 17.1 8 -11 0 304.17 17.3 -11 3 0 318.37 16.9 -8 11 0 304.37 16.8 11 -3 0 339.17 17.5 7 -11 0 300.57 16.7 4 7 0 280.97 17.2 -11 4 0 287.87 15.7 -11 4 0 308.37 16.2 11 -4 0 291.77 16.2 -7 11 0 295.07 16.2 5 6 0 2420.56 108.99 -11 5 0 2450.65 107.39 6 -11 0 2217.98 108.19 -11 5 0 2328.77 107.39 11 -5 0 2493.05 107.79 -6 11 0 2392.86 108.19 -5 -6 0 2258.67 108.69 11 -5 0 2385.86 107.69 5 -11 0 1156.78 54.69 -11 6 0 1165.78 53.49 -11 6 0 1144.29 53.49 6 5 0 1101.19 54.89 -5 11 0 1206.78 54.59 11 -6 0 1215.18 53.79 -6 -5 0 1141.39 54.99 11 -6 0 1115.19 53.69 -11 7 0 2599.34 115.29 4 -11 0 2606.64 116.69 -11 7 0 2671.63 115.29 -7 -4 0 2588.84 116.69 11 -7 0 2260.97 115.29 -4 11 0 2571.34 116.49 8 3 0 1241.18 61.29 -11 8 0 1287.87 59.89 -11 8 0 1375.36 59.99 -8 -3 0 1305.87 61.39 -3 11 0 1282.27 61.39 11 -8 0 1318.67 60.39 -11 9 0 7.8 3.9 9 2 0 4.9 4 -11 9 0 8.5 3.6 2 -11 0 13.5 7 -2 11 0 17.3 6.8 11 -9 0 6.5 4.5 -9 -2 0 8.2 4 1 -11 0 1386.96 66.99 -11 10 0 1438.16 65.09 11 -10 0 1462.45 65.59 -1 11 0 1363.26 66.69 -11 11 0 271.87 14.6 11 0 0 263.07 15.9 0 -11 0 240.98 16.4 0 11 0 258.87 16.5 11 -11 0 261.77 15.1 11 -12 0 799.02 37.4 -1 -11 0 759.62 38.8 12 -1 0 740.53 37.7 -11 12 0 757.32 36.8 -12 2 0 29.6 5.7 2 10 0 12.7 4.7 10 -12 0 32.5 5.9 -12 2 0 37.2 6.2 -2 -10 0 61.79 12.7 -10 12 0 32 5.6 12 -2 0 30.3 5.5 -12 3 0 823.72 42.3 3 9 0 1032.3 45.8 9 -12 0 835.72 42.8 -12 3 0 954.3 42.8 -3 -9 0 847.32 43.9 -9 12 0 867.21 42.4 12 -3 0 894.51 42.7 8 -12 0 95.79 8.8 -12 4 0 93.19 8 4 8 0 105.49 11.9 -12 4 0 91.99 8.4 12 -4 0 83.09 8.4 -4 -8 0 157.38 15.6 -8 12 0 88.29 8 -12 5 0 106.39 8.6 7 -12 0 108.69 9.6 -12 5 0 115.49 8.1 12 -5 0 101.69 8.8 -7 12 0 103.19 8.7 -5 -7 0 132.39 12.4 12 -5 0 98.69 8.8 -12 6 0 307.87 16 6 -12 0 302.67 17.3 6 6 0 301.67 17.6 -12 6 0 297.47 15.8 12 -6 0 299.17 16.1 -6 12 0 292.67 16.7 12 -6 0 250.67 16 5 -12 0 378.86 22.3 7 5 0 395.06 22.5 -12 7 0 432.06 21 -12 7 0 409.66 20.9 12 -7 0 424.56 21.6 12 -7 0 428.86 21.4 -5 12 0 424.66 22.3 4 -12 0 59.89 7.1 -12 8 0 50.19 6.2 -12 8 0 67.69 6.7 8 4 0 50.99 6.5 -4 12 0 62.79 7.3 12 -8 0 86.79 8 -8 -4 0 78.59 8.5 -12 9 0 783.52 36.5 9 3 0 776.42 38.1 3 -12 0 777.42 38.3 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896.61 43.7 -5 -8 0 900.51 45.1 6 7 0 2440.26 110.79 -13 6 0 2391.16 108.89 -13 6 0 2313.77 108.79 7 -13 0 2420.56 110.19 -6 -7 0 2410.96 110.69 -7 13 0 2324.27 109.79 13 -6 0 2405.46 109.19 13 -6 0 2451.35 109.39 -13 7 0 4999.5 228.28 6 -13 0 5214.68 229.88 -13 7 0 4976.6 228.18 -7 -6 0 5018 230.08 -6 13 0 5088.29 229.48 13 -7 0 5124.39 228.68 13 -7 0 5186.08 228.78 8 5 0 892.41 42.6 -13 8 0 830.42 40.5 5 -13 0 839.22 42.2 -13 8 0 858.51 40.5 -5 13 0 874.51 42 -8 -5 0 858.41 42.4 13 -8 0 832.92 41.2 -13 9 0 78.49 7.6 4 -13 0 82.89 9.8 -13 9 0 88.99 8.2 9 4 0 71.39 9 -9 -4 0 104.09 10.5 -4 13 0 73.09 8.5 13 -9 0 64.99 8.1 -13 10 0 172.88 11.5 -13 10 0 181.38 11.8 3 -13 0 189.48 14.1 10 3 0 194.78 13.7 -10 -3 0 198.78 13.7 13 -10 0 175.68 12.6 -3 13 0 189.48 13.6 -13 11 0 135.39 9.9 2 -13 0 143.09 12.7 -13 11 0 137.39 10.4 11 2 0 156.98 11.8 13 -11 0 123.09 11.3 -2 13 0 161.78 12.5 -13 12 0 628.94 31.2 13 -12 0 651.13 32.1 -1 13 0 633.14 33.4 0 -13 0 560.54 31.2 13 0 0 567.24 30.2 -13 13 0 592.74 28.8 13 -13 0 569.14 29.5 0 13 0 579.74 31 -14 1 0 184.48 13.6 1 13 0 201.88 15.1 13 -14 0 190.58 13.8 -13 14 0 188.98 13.7 14 -1 0 193.58 14.5 -1 -13 0 205.98 15.8 -14 2 0 1269.17 63.99 12 -14 0 1317.97 64.09 -14 2 0 1570.34 65.09 14 -2 0 1362.46 64.49 -12 14 0 1298.17 63.89 -2 -12 0 1344.47 65.79 -14 3 0 1746.83 80.79 3 11 0 1709.13 82.19 11 -14 0 1754.92 80.89 -14 3 0 1703.33 80.59 -11 14 0 1712.53 80.39 14 -3 0 1755.12 80.89 -3 -11 0 1776.02 82.29 -14 4 0 215.58 13.5 10 -14 0 186.98 13.8 4 10 0 194.48 14.7 -14 4 0 197.08 13.1 -10 14 0 196.28 13.1 -4 -10 0 207.38 15.2 14 -4 0 200.38 13.7 9 -14 0 474.95 25.7 -14 5 0 497.15 24.7 -14 5 0 461.75 24.8 -9 14 0 457.05 25.1 -5 -9 0 496.55 26.9 14 -5 0 483.55 25.3 8 -14 0 4094.99 196.78 -14 6 0 4666.23 195.98 6 8 0 4410.16 197.88 -14 6 0 4300.77 195.78 -8 14 0 4366.56 196.78 14 -6 0 4612.74 196.38 14 -6 0 4099.69 196.08 -6 -8 0 4218.08 197.68 -14 7 0 6499.75 293.37 7 -14 0 6371.46 294.97 -14 7 0 6968 293.67 7 7 0 6548.64 295.47 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14 0 43.6 8.2 14 -15 0 32.7 7.6 -15 1 0 51.79 8 15 -1 0 37.7 8 -1 -14 0 29.7 8 -14 15 0 37 6.5 -15 2 0 139.29 11.4 -15 2 0 126.19 11.3 13 -15 0 99.09 11 15 -2 0 129.09 11.7 -13 15 0 136.59 10.4 -2 -13 0 148.99 13.4 3 12 0 133.19 14 12 -15 0 118.29 11.8 -15 3 0 98.69 9.9 -15 3 0 96.09 9.9 -12 15 0 102.69 9.3 -3 -12 0 109.69 12.5 15 -3 0 105.89 10.7 -15 4 0 2717.63 132.79 4 11 0 3288.87 137.19 11 -15 0 2671.33 133.39 15 -4 0 2614.44 133.09 -4 -11 0 3367.26 137.59 10 -15 0 23.2 7.1 -15 5 0 17.8 6.8 -15 5 0 16.3 5.6 5 10 0 34 8.5 -5 -10 0 16 5.4 15 -5 0 11.2 5.6 -10 15 0 16.8 6.4 9 -15 0 153.58 13 -15 6 0 146.59 11.5 -15 6 0 156.08 11.2 -9 15 0 146.89 11.8 15 -6 0 174.68 12 -6 -9 0 171.78 13.8 8 -15 0 780.02 39.2 -15 7 0 828.02 37.5 -15 7 0 774.62 37.6 7 8 0 795.02 39.9 15 -7 0 678.73 37.9 15 -7 0 800.82 38 -7 -8 0 779.62 39.9 -8 15 0 741.83 38.4 -15 8 0 3443.36 146.59 7 -15 0 3148.78 148.09 8 7 0 3166.78 148.49 -15 8 0 3261.77 146.39 15 -8 0 3212.38 146.89 -7 15 0 3233.38 147.79 15 -8 0 3253.37 146.79 -8 -7 0 3136.59 148.49 -15 9 0 1120.09 51.89 6 -15 0 1060.69 53.99 -15 9 0 1118.19 51.89 -9 -6 0 1138.49 54.29 15 -9 0 1102.09 52.69 -6 15 0 1076.09 53.59 10 5 0 25.3 7.1 -15 10 0 34.1 6.1 5 -15 0 34.7 7.9 -15 10 0 30 6.3 15 -10 0 24.6 7.1 -10 -5 0 34.3 8.2 -5 15 0 34 7.8 11 4 0 1489.35 69.49 -15 11 0 1431.06 67.09 4 -15 0 1449.15 69.69 -4 15 0 1403.46 69.19 -11 -4 0 1446.76 69.39 15 -11 0 1473.95 67.89 12 3 0 55.09 8.8 3 -15 0 57.69 9.2 -15 12 0 65.09 7.8 -15 12 0 59.19 7.7 -12 -3 0 53.59 9.3 -3 15 0 84.99 10.8 15 -12 0 56.59 8.7 2 -15 0 1705.23 81.49 13 2 0 1654.23 80.79 -15 13 0 1847.62 78.99 -15 13 0 1674.03 78.89 15 -13 0 1651.43 80.89 -15 14 0 491.45 25.5 -1 15 0 519.25 28.3 15 -14 0 474.85 28 15 0 0 3.5 5.3 0 -15 0 14.3 9.7 -15 15 0 1.5 4.6 -15 0 0 6.7 4.8 0 15 0 3.3 5.6 15 -15 0 8.2 5.6 15 -16 0 85.99 9.5 1 15 0 81.09 10.7 -16 1 0 92.69 10.5 -16 1 0 104.69 11.1 -15 16 0 76.79 8.6 -1 -15 0 122.79 14.7 16 -1 0 84.69 10.1 -16 2 0 74.89 9 14 -16 0 76.69 9.1 2 14 0 78.99 10.2 -16 2 0 79.29 9.5 -14 16 0 95.79 9.5 16 -2 0 88.29 10.9 -2 -14 0 49.6 7.8 13 -16 0 100.89 11.2 -16 3 0 92.29 10.4 3 13 0 141.29 16.8 -16 3 0 83.49 9.5 -3 -13 0 110.39 14.3 16 -3 0 84.79 10.1 -13 16 0 103.69 10.4 -16 4 0 -0.5 4.6 -16 4 0 8.5 5.3 4 12 0 -4.4 10.9 -12 16 0 -3.9 4 -4 -12 0 4.2 5 16 -4 0 -2.8 5.1 11 -16 0 2951.4 130.69 5 11 0 2780.72 131.59 -16 5 0 2745.33 129.59 -16 5 0 2870.91 129.59 -11 16 0 2907.01 130.09 16 -5 0 2764.62 129.89 10 -16 0 1392.56 66.59 -16 6 0 1341.47 65.19 -16 6 0 1472.95 65.39 -10 16 0 1389.36 66.09 16 -6 0 1364.46 65.69 9 -16 0 438.46 24.8 -16 7 0 431.96 23.1 7 9 0 530.25 28.8 -16 7 0 431.56 22.9 -7 -9 0 402.86 25.3 16 -7 0 450.55 24 16 -7 0 425.26 23.7 -9 16 0 397.86 25.2 8 -16 0 325.57 20.2 8 8 0 319.97 20.6 -16 8 0 308.97 18.2 -16 8 0 311.77 18 16 -8 0 301.07 18.5 -8 -8 0 341.17 21 16 -8 0 355.66 19.1 -16 9 0 960.3 44.1 9 7 0 929.71 46.7 7 -16 0 879.21 46.1 -16 9 0 926.41 44 16 -9 0 920.41 44.6 -9 -7 0 916.91 46.6 -7 16 0 917.51 47.5 16 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303.17 18.8 -10 18 0 319.17 19.6 -18 9 0 219.68 13.2 -18 9 0 203.58 13.6 9 9 0 192.58 16.1 9 -18 0 177.38 15.3 -9 -9 0 221.48 16.7 18 -9 0 211.78 14.7 18 -9 0 202.28 14.3 -9 18 0 204.18 15 10 8 0 43 11.4 -18 10 0 29.2 6 -18 10 0 38.4 6.5 18 -10 0 19.8 6.7 -8 18 0 44.1 8.7 -10 -8 0 40.3 8.6 11 7 0 312.27 20.3 -18 11 0 321.97 17.3 -18 11 0 311.37 17.1 -7 18 0 273.27 19.1 -11 -7 0 285.17 20 18 -11 0 296.67 18.4 6 -18 0 417.26 25.8 -18 12 0 443.86 22.4 12 6 0 408.76 25.1 -18 12 0 433.36 22.3 -12 -6 0 424.56 25.5 18 -12 0 408.46 23.7 -6 18 0 410.46 24.8 13 5 0 15.2 6.3 5 -18 0 9 5.7 -18 13 0 9.8 4.7 -18 13 0 4.6 4.7 -13 -5 0 17.6 7.5 18 -13 0 5.3 5.9 -5 18 0 15.3 7.5 4 -18 0 76.69 11.4 -18 14 0 69.49 8 14 4 0 106.79 13 -18 14 0 89.69 8.9 -14 -4 0 79.69 10.9 -4 18 0 120.09 13.6 18 -14 0 97.09 10.7 3 -18 0 138.29 14.5 -18 15 0 132.59 10.5 -18 15 0 137.79 11 15 3 0 147.79 13.9 -3 18 0 133.09 13.9 18 -15 0 123.09 12.7 -15 -3 0 195.58 23.4 2 -18 0 513.35 31 16 2 0 520.55 30.2 -18 16 0 533.85 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92.89 10.2 -6 -13 0 106.79 13.4 19 -6 0 80.59 9.9 -19 7 0 169.78 12.5 7 12 0 184.18 18.3 -19 7 0 138.49 12.4 12 -19 0 142.89 14.2 19 -7 0 153.78 13.6 -7 -12 0 225.38 19.4 -12 19 0 176.98 13.5 -19 8 0 4.7 5.2 11 -19 0 -2.5 5.6 8 11 0 10.3 9 -19 8 0 2 4.7 -8 -11 0 5.6 9 -11 19 0 10.1 6.1 19 -8 0 0.2 5.2 9 10 0 9.2 7.5 -19 9 0 8.3 5 10 -19 0 7 5.6 -19 9 0 8.8 5.2 19 -9 0 -5.7 5.2 -9 -10 0 4.4 6.3 -10 19 0 -3.2 4.9 19 -9 0 5.9 5.3 -19 10 0 6.4 4.5 9 -19 0 3.1 6.1 -19 10 0 -2.3 4.7 10 9 0 -1.1 5.8 -10 -9 0 8.1 6.2 19 -10 0 -1 5.3 -9 19 0 6.7 6 19 -10 0 -8.1 5.1 11 8 0 277.47 21.3 8 -19 0 228.48 17.9 -19 11 0 222.88 14.7 -19 11 0 221.28 14.3 -8 19 0 233.48 16.8 19 -11 0 240.48 16 -11 -8 0 300.97 21.6 -19 12 0 87.19 8.6 12 7 0 65.19 10.4 -19 12 0 89.09 8.6 7 -19 0 65.29 10.6 -7 19 0 92.39 11.8 -12 -7 0 71.69 9.6 19 -12 0 77.99 9.8 6 -19 0 244.38 18.7 -19 13 0 221.58 14.7 13 6 0 236.18 18.1 -19 13 0 244.08 14.8 -13 -6 0 252.57 18 -6 19 0 247.38 17.9 19 -13 0 247.28 16.8 -19 14 0 74.89 8.7 -19 14 0 98.09 9.7 14 5 0 84.29 12.4 5 -19 0 102.79 13.7 -5 19 0 76.99 11 19 -14 0 70.79 9.6 -14 -5 0 126.59 14.4 -19 15 0 53.99 7.8 15 4 0 55.89 9.4 -19 15 0 71.69 8.4 -4 19 0 54.69 10 19 -15 0 66.39 9.7 -15 -4 0 54.79 10.2 -19 16 0 19.9 6.2 -19 16 0 20.8 6.1 16 3 0 13.6 6.8 -3 19 0 14.7 8.3 19 -16 0 12.3 7.2 17 2 0 349.87 22.3 -19 17 0 335.77 19 -19 17 0 310.07 19.2 2 -19 0 328.87 25.4 19 -17 0 325.17 21.1 -2 19 0 327.87 22.6 -19 18 0 21.7 6.2 1 -19 0 28.5 12 -19 18 0 28.5 7.2 -18 -1 0 22.2 7.4 -1 19 0 37.8 9.6 19 -18 0 24.3 8 0 -19 0 21.9 9.7 19 0 0 21.1 8.1 -19 19 0 23 6.3 19 -19 0 34.4 8.9 0 19 0 24.8 8.5 -19 0 0 29.9 8.5 -19 0 0 17.7 7.3 -20 1 0 -6.8 5.4 -20 1 0 -1.3 6.5 19 -20 0 -1.3 7.4 1 19 0 4.7 7.8 -1 -19 0 -2.3 7.6 -19 20 0 1.4 5.2 20 -1 0 11.7 8.1 2 18 0 456.15 28.8 18 -20 0 442.26 26.6 -20 2 0 437.46 26.5 -20 2 0 461.95 26.6 -2 -18 0 449.86 29.1 20 -2 0 467.55 27.5 -18 20 0 448.56 24.9 -20 3 0 1051.09 48.9 -20 3 0 988.2 48.6 17 -20 0 966.7 48.8 -17 20 0 919.81 47.4 -3 -17 0 923.01 50.99 20 -3 0 927.41 49.2 -20 4 0 1261.97 58.29 16 -20 0 1092.39 58.39 4 16 0 1196.38 60.69 -20 4 0 1222.78 57.99 -4 -16 0 1242.28 61.19 20 -4 0 1162.68 58.79 -16 20 0 1148.89 57.49 15 -20 0 251.07 18.8 5 15 0 326.27 24.6 -20 5 0 252.87 17.5 -20 5 0 252.57 17.4 -15 20 0 235.68 16.9 -5 -15 0 266.57 20.5 20 -5 0 254.97 18.2 14 -20 0 5.6 6 -20 6 0 14.5 6.2 -20 6 0 20.7 6.5 6 14 0 12.7 9.7 20 -6 0 22.5 7 -14 20 0 16.9 5.8 -6 -14 0 0 8 -20 7 0 21 6.5 13 -20 0 16.6 7.2 7 13 0 5.8 14.4 -20 7 0 25 6.9 -7 -13 0 15.2 7.1 -13 20 0 22.8 6.7 20 -7 0 20.9 7.5 12 -20 0 236.48 17.8 -20 8 0 230.18 15.4 8 12 0 279.57 21.8 -20 8 0 217.48 15 -12 20 0 228.88 16.2 20 -8 0 226.58 16.2 -20 9 0 225.78 14.6 9 11 0 288.97 21.7 -20 9 0 210.48 14.9 11 -20 0 243.08 17.6 20 -9 0 228.58 15.9 -9 -11 0 206.18 17.9 -11 20 0 207.48 16.2 10 -20 0 17.1 6.7 -20 10 0 12.6 5.2 -20 10 0 14.9 5.4 10 10 0 15.3 8.5 -10 20 0 4.8 6.6 -10 -10 0 10.5 6.7 20 -10 0 6.7 5.8 20 -10 0 21 6.8 -20 11 0 35 6.7 9 -20 0 11.5 6.9 11 9 0 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26.1 6.9 -20 19 0 37.8 7.7 1 -20 0 28 9.2 -19 -1 0 39.4 9.1 20 -19 0 32.9 8.7 -1 20 0 28 8 0 -20 0 272.97 22.2 20 0 0 240.68 19.8 -20 20 0 252.77 16.5 -20 20 0 258.87 17.1 -20 0 0 247.58 19.1 0 20 0 221.68 20.7 -20 0 0 257.77 19.4 20 -20 0 269.67 19.6 1 20 0 273.67 22.2 -21 1 0 272.77 20.2 -21 1 0 271.17 19.5 20 -21 0 258.07 19.9 -20 21 0 261.67 17.4 21 -1 0 281.07 21.3 -1 -20 0 267.27 25.5 -21 2 0 25.8 8.4 -21 2 0 34.5 8.2 19 -21 0 24 8.5 2 19 0 37.1 11.4 -2 -19 0 32.9 9.2 -19 21 0 28.5 7.5 21 -2 0 26.2 9.4 -21 3 0 336.07 21.4 18 -21 0 316.47 22.2 -21 3 0 370.86 22.1 3 18 0 291.97 23.9 -18 21 0 332.47 20.3 21 -3 0 345.47 22.8 -21 4 0 432.66 26.4 17 -21 0 473.75 27.6 -21 4 0 433.56 26.4 -17 21 0 456.35 25.8 -4 -17 0 450.95 29.8 21 -4 0 508.75 28.1 5 16 0 421.46 26.7 16 -21 0 393.46 24.5 -21 5 0 364.06 23.3 -21 5 0 369.76 23.1 -5 -16 0 481.25 30.5 -16 21 0 359.46 22.8 21 -5 0 394.86 24.6 6 15 0 -1.5 7.4 15 -21 0 4.4 7.2 -21 6 0 13.4 6.4 -21 6 0 5.8 6.1 21 -6 0 11.1 7 -15 21 0 15.9 6.2 -6 -15 0 7.2 8.2 -21 7 0 451.55 26.5 -21 7 0 496.05 26.4 7 14 0 471.15 29.7 14 -21 0 514.55 28.8 21 -7 0 486.05 27.7 -14 21 0 460.85 27 -21 8 0 1199.18 58.89 8 13 0 1170.58 61.89 13 -21 0 1272.77 61.29 -21 8 0 1178.28 58.69 21 -8 0 1248.08 59.99 -13 21 0 1287.67 60.29 -21 9 0 374.46 21.4 9 12 0 349.07 24.3 -21 9 0 343.07 20.8 12 -21 0 375.56 24 -9 -12 0 371.26 24.5 21 -9 0 339.17 22.1 -12 21 0 395.16 22.9 10 11 0 74.29 12.1 11 -21 0 45.8 8.6 -21 10 0 52.89 8.3 -21 10 0 51.29 8 21 -10 0 44 8.3 -10 -11 0 54.69 11.5 -11 21 0 81.09 11.2 11 10 0 123.89 15.3 10 -21 0 107.09 12.6 -21 11 0 100.19 10.2 -21 11 0 88.19 9.6 -11 -10 0 177.48 23.7 -10 21 0 133.59 14.6 21 -11 0 113.69 12.2 -21 12 0 -2 4.7 -21 12 0 0.8 4.7 12 9 0 -4.5 6.7 9 -21 0 1 6.4 -9 21 0 0.2 6.3 -12 -9 0 -3.6 6.2 21 -12 0 -6.4 5.6 8 -21 0 301.97 21.4 13 8 0 300.37 21.3 -21 13 0 291.37 17.2 -21 13 0 288.07 17.2 -8 21 0 276.87 20.2 -13 -8 0 312.57 21.4 21 -13 0 282.27 18.8 -21 14 0 479.95 25.7 -21 14 0 499.45 25.6 14 7 0 489.75 29.6 7 -21 0 465.15 29.6 -7 21 0 488.05 29.2 -14 -7 0 510.35 29.7 21 -14 0 488.65 27.7 -21 15 0 561.34 28.4 15 6 0 544.55 32 6 -21 0 550.84 32.9 -21 15 0 564.44 28.5 -6 21 0 530.95 32 21 -15 0 534.65 30.2 -15 -6 0 564.54 32.2 16 5 0 13.4 7.1 -21 16 0 17.2 5.8 5 -21 0 25.6 8.4 -21 16 0 10.8 5.7 21 -16 0 8.9 7.3 -5 21 0 11.5 7.8 -16 -5 0 20.3 8.1 4 -21 0 385.66 27.1 -21 17 0 411.26 23.1 17 4 0 399.46 26.7 -21 17 0 426.46 23.1 -17 -4 0 434.36 27 -4 21 0 470.45 27.7 21 -17 0 437.86 25.4 -21 18 0 414.36 22.7 -21 18 0 393.86 22.9 3 -21 0 381.06 27 18 3 0 439.56 27 -3 21 0 424.26 27.2 21 -18 0 423.16 25.2 -21 19 0 14.6 6 19 2 0 3.1 7.3 -21 19 0 20.3 6.4 2 -21 0 23.4 9.1 21 -19 0 12 8.1 -19 -2 0 12.6 6.7 -2 21 0 21.7 8.1 -21 20 0 181.58 14.2 20 1 0 201.58 22.5 -21 20 0 207.18 15.3 1 -21 0 209.58 20 -20 -1 0 200.98 17.2 21 -20 0 216.58 17.8 -1 21 0 177.18 19.1 -21 21 0 8.7 5.9 21 0 0 6.4 7.8 -21 21 0 1.6 6.4 0 -21 0 19.3 9.6 21 -21 0 5.4 8.1 0 21 0 -7.4 7.8 -21 0 0 18.4 8.4 -21 0 0 4.8 7.6 -22 1 0 305.47 22.4 1 21 0 294.57 24.7 21 -22 0 321.57 22.5 -22 1 0 332.27 22.6 22 -1 0 329.57 23.6 -1 -21 0 310.87 25.1 -21 22 0 313.27 19.8 2 20 0 0.3 8.1 20 -22 0 10.4 7.9 -22 2 0 5.9 7.5 -22 2 0 4.8 6.7 -20 22 0 -1.8 5.7 22 -2 0 5 8.1 -2 -20 0 0.3 9.7 3 19 0 138.09 16.1 19 -22 0 167.38 15.5 -22 3 0 123.19 13.7 -22 3 0 139.49 14.4 22 -3 0 135.59 15.9 -3 -19 0 136.09 15.7 -19 22 0 145.69 12.8 4 18 0 53.59 12.5 -22 4 0 58.49 10.2 -22 4 0 47.3 9.1 18 -22 0 62.99 11.7 22 -4 0 54.59 11.2 -4 -18 0 29.1 10.4 -18 22 0 69.79 10.3 -22 5 0 200.98 16.4 17 -22 0 202.78 17.7 -22 5 0 227.88 16.6 22 -5 0 211.08 17.8 -17 22 0 207.18 15.7 -5 -17 0 274.27 24.1 16 -22 0 42.8 10.4 -22 6 0 30.5 7.4 -22 6 0 39.9 8.4 6 16 0 23.5 8.2 -6 -16 0 16.9 8.6 -16 22 0 35.1 8.4 22 -6 0 30.8 8.3 15 -22 0 11 7.3 7 15 0 9.2 7 -22 7 0 2 5.6 -22 7 0 9.9 5.9 22 -7 0 10.7 7.9 -15 22 0 2.6 5.9 -7 -15 0 14.4 8.5 -22 8 0 27.8 7.2 8 14 0 34.3 10.2 -22 8 0 20.8 6.7 14 -22 0 10.5 7.4 -8 -14 0 13.5 8.3 22 -8 0 30.1 8.4 -14 22 0 15.1 6.6 -22 9 0 160.98 13.2 13 -22 0 184.58 16.6 -22 9 0 160.98 13.4 9 13 0 171.98 16.8 22 -9 0 145.59 14.3 -9 -13 0 184.58 17.1 -13 22 0 177.48 14.8 10 12 0 18 9.1 12 -22 0 17.2 7.6 -22 10 0 24.4 6.6 -22 10 0 31.7 7.1 22 -10 0 14.7 7 -12 22 0 21.2 7 -10 -12 0 22.2 8.1 11 -22 0 8.4 6.9 -22 11 0 2.3 5.5 11 11 0 -0.8 6.9 -22 11 0 -1.1 4.9 22 -11 0 1.5 6.1 22 -11 0 -14.4 5 -11 22 0 11.2 6.1 -11 -11 0 -10.3 8.6 12 10 0 58.99 10.6 10 -22 0 61.29 11.7 -22 12 0 97.49 9.9 -22 12 0 82.29 9 -10 22 0 113.59 13.9 22 -12 0 61.19 9.8 -12 -10 0 85.99 13.1 -22 13 0 29.3 6.4 -22 13 0 27.7 6.2 9 -22 0 39.1 10.6 13 9 0 48 10.7 -13 -9 0 27.2 9.2 -9 22 0 17.8 7.1 22 -13 0 15.3 6.6 -22 14 0 62.99 8.1 -22 14 0 62.29 8 14 8 0 42.3 10.1 8 -22 0 25.2 9 22 -14 0 43.4 8.4 -14 -8 0 48.5 10.5 -8 22 0 60.79 11.3 7 -22 0 139.59 17 -22 15 0 98.99 9.9 -22 15 0 99.29 9.8 15 7 0 128.89 15.9 -7 22 0 113.59 14.3 -15 -7 0 135.69 15.7 22 -15 0 114.69 12.9 -22 16 0 156.38 12.2 -22 16 0 171.68 12 6 -22 0 161.48 17 16 6 0 141.89 16.3 22 -16 0 161.28 14.7 -6 22 0 158.58 16 -16 -6 0 168.78 16.1 5 -22 0 20.7 9 -22 17 0 14.4 5.7 -22 17 0 31.4 6.5 17 5 0 18 8.2 22 -17 0 24.6 7.8 -17 -5 0 5.2 7.1 -5 22 0 22.3 8.4 -22 18 0 494.95 27 18 4 0 533.75 31.4 -22 18 0 514.35 26.9 4 -22 0 511.85 32.1 -4 22 0 510.65 31.5 -18 -4 0 429.16 38 22 -18 0 542.25 29.5 -22 19 0 402.66 22.3 19 3 0 364.76 25.9 3 -22 0 386.36 27.1 -22 19 0 395.96 22 22 -19 0 406.16 25.2 -3 22 0 390.36 26.9 2 -22 0 32.4 13.2 -22 20 0 24.4 6.7 20 2 0 40.9 11.2 -22 20 0 34.8 7.5 -20 -2 0 36.5 9.5 -2 22 0 36.6 9.7 22 -20 0 20.7 9 -22 21 0 24.4 7.3 21 1 0 27 10.4 -22 21 0 38.6 7.3 1 -22 0 19.1 10.1 -21 -1 0 24.7 9.5 -21 -1 0 20.2 10.3 22 -21 0 41.8 9.6 -1 22 0 31.5 11.1 22 0 0 405.46 28 0 -22 0 404.46 29.3 -22 22 0 396.96 23.7 -22 22 0 419.36 23.4 -22 0 0 419.46 26.9 22 -22 0 409.46 26.5 -22 0 0 375.96 26.4 0 22 0 383.36 28.8 -23 1 0 97.29 13.2 1 22 0 78.69 15.1 22 -23 0 125.99 15.6 -1 -22 0 93.99 14.9 -22 23 0 103.89 12.2 23 -1 0 89.79 13.8 -23 2 0 9.4 8.2 -23 2 0 2.9 8.2 2 21 0 5.2 10 21 -23 0 2.7 8.7 -2 -21 0 24.9 11.5 23 -2 0 11.7 9.6 -21 23 0 7.2 6.7 -23 3 0 41.4 9.9 -23 3 0 52.49 10.1 20 -23 0 48.9 10.7 3 20 0 53.89 14.2 23 -3 0 49.3 11.2 -20 23 0 47 8.9 -23 4 0 49.3 9.7 19 -23 0 60.49 10.9 4 19 0 60.69 13.1 -23 4 0 55.79 10.3 -19 23 0 79.69 11 23 -4 0 77.99 12.1 -4 -19 0 79.49 23 -23 5 0 414.26 25 5 18 0 384.96 28 -23 5 0 358.86 24.1 18 -23 0 422.26 26.3 -5 -18 0 515.05 33.6 23 -5 0 374.26 25.9 -18 23 0 406.16 24.1 17 -23 0 41.8 9.5 -23 6 0 35.8 8.7 -23 6 0 47.5 9.2 -6 -17 0 20.3 9.6 23 -6 0 37.4 9.6 -17 23 0 35.3 8.2 7 16 0 247.78 22 16 -23 0 285.87 20.9 -23 7 0 285.37 18.9 -23 7 0 279.97 18.8 23 -7 0 264.77 20.1 -7 -16 0 267.97 22.6 -16 23 0 280.57 19.1 15 -23 0 253.57 19.9 -23 8 0 255.47 17.5 8 15 0 262.87 21.7 -23 8 0 259.97 17.6 -15 23 0 258.17 18.4 -8 -15 0 227.88 21.3 23 -8 0 255.97 19.1 14 -23 0 386.26 26.1 9 14 0 400.96 27.1 -23 9 0 382.96 22.8 -23 9 0 403.26 23.2 -14 23 0 419.36 24.8 23 -9 0 398.06 24.5 -9 -14 0 368.16 26.7 -23 10 0 86.89 10.3 13 -23 0 74.49 12 10 13 0 120.09 16.6 -23 10 0 88.99 10.2 -10 -13 0 84.89 13.1 -13 23 0 68.79 10.4 23 -10 0 86.99 11 11 12 0 19 8.6 -23 11 0 15.4 6.2 -23 11 0 22.6 6.7 12 -23 0 10 7.1 -12 23 0 18.3 8.2 -11 -12 0 7.3 6.7 23 -11 0 17.3 7.3 -23 12 0 27.6 6.8 12 11 0 22.6 8.4 11 -23 0 42.9 11.2 -23 12 0 39.6 7.1 -11 23 0 16.5 7.5 23 -12 0 40.5 8.4 -12 -11 0 23 8.4 13 10 0 2.7 6.5 10 -23 0 -2.9 7 -23 13 0 -8.2 4.5 -23 13 0 0.1 4.8 23 -13 0 2.9 6 -10 23 0 3.1 6.8 -13 -10 0 -0.2 6.6 9 -23 0 151.88 16.9 -23 14 0 158.18 12 -23 14 0 153.58 11.9 14 9 0 149.79 16.9 -14 -9 0 165.08 16.9 23 -14 0 149.39 13.9 -9 23 0 162.08 15.7 15 8 0 95.99 15 -23 15 0 77.79 8.6 8 -23 0 66.69 11.8 -23 15 0 73.29 8.8 -15 -8 0 62.49 10.8 -8 23 0 89.39 12.2 23 -15 0 67.99 10.5 -23 16 0 1.4 4.5 7 -23 0 13.6 6.5 16 7 0 6.7 7.1 -23 16 0 -3.1 4.8 -7 23 0 4 7.3 -16 -7 0 0.5 7.9 23 -16 0 4.9 7 -23 17 0 13.2 5.7 6 -23 0 19.1 9.1 17 6 0 3 6.9 -23 17 0 10.8 5.6 -17 -6 0 24.1 8.3 -6 23 0 10.3 6.8 23 -17 0 7.9 7.5 18 5 0 70.39 12.8 5 -23 0 59.59 12.3 -23 18 0 81.29 9.5 -23 18 0 83.99 9.5 -5 23 0 78.49 13.9 23 -18 0 89.09 12.6 19 4 0 1.2 7.6 -23 19 0 4.1 5.2 4 -23 0 3.8 9.3 -23 19 0 5.7 5.6 -4 23 0 12.4 8.5 23 -19 0 1.4 7.3 20 3 0 7.2 8.4 3 -23 0 8.1 10.4 -23 20 0 9.2 5.4 -23 20 0 11 6 -3 23 0 16.8 8.8 23 -20 0 7.5 8.1 -20 -3 0 -8.5 6 -23 21 0 9.1 5.9 -23 21 0 6.3 6.5 2 -23 0 10 8.7 21 2 0 16.5 10.2 -2 23 0 8.3 8.9 -21 -2 0 21.9 9.8 23 -21 0 -0.3 8.2 -23 22 0 294.17 19.3 -23 22 0 299.97 20.5 1 -23 0 296.87 25.1 22 1 0 278.77 26.1 23 -22 0 269.97 22.1 -1 23 0 282.57 24.1 -22 -1 0 286.77 23.7 -22 -1 0 287.87 22.2 23 0 0 255.47 24 -23 23 0 290.27 19.1 -23 23 0 278.47 19.7 0 -23 0 292.97 26.3 23 -23 0 313.47 23.4 -23 0 0 292.07 23 -23 0 0 308.07 23 0 23 0 378.46 31.9 -24 1 0 89.29 14.4 23 -24 0 109.19 15.3 1 23 0 76.09 15.5 -24 1 0 74.29 12.4 -23 24 0 103.49 12.6 24 -1 0 78.39 14.1 -1 -23 0 45.4 14.2 -23 24 0 88.79 11.3 -24 2 0 58.49 12.5 2 22 0 56.69 13.9 -24 2 0 47 11.7 22 -24 0 55.39 11.8 -22 24 0 60.49 9.8 -2 -22 0 46.8 12.8 24 -2 0 57.19 12.3 21 -24 0 701.93 39.8 -24 3 0 738.03 38.8 -24 3 0 691.93 41.5 3 21 0 707.13 42.1 -3 -21 0 680.43 42 -21 24 0 639.24 39.8 24 -3 0 694.33 40 -24 4 0 454.15 32 20 -24 0 479.15 29.9 -24 4 0 476.95 28.8 -20 24 0 497.95 29.6 24 -4 0 465.55 30.3 -24 5 0 180.68 17.1 5 19 0 242.48 26.4 -24 5 0 199.18 16.6 19 -24 0 210.38 19.1 -5 -19 0 197.28 21.6 -19 24 0 202.68 16.5 24 -5 0 192.08 18.8 18 -24 0 4.6 8.4 -24 6 0 10.9 7.5 -24 6 0 3.9 7.6 6 18 0 7.8 8.3 24 -6 0 8.8 8.2 -18 24 0 9.9 6.7 -6 -18 0 1.9 9.1 -24 7 0 109.89 13.1 7 17 0 138.99 21.5 -24 7 0 140.99 14.2 17 -24 0 135.09 16.5 -17 24 0 124.09 13.4 -7 -17 0 187.58 22.9 24 -7 0 139.29 16.5 -24 8 0 55.39 9.2 16 -24 0 57.09 12.5 8 16 0 35.6 12.8 -24 8 0 43.1 8.9 24 -8 0 41.4 9.5 -16 24 0 56.19 10 -8 -16 0 35 9.5 -24 9 0 4.7 6.6 15 -24 0 -0.3 7.6 -24 9 0 4.7 6.3 9 15 0 6.6 11.8 -15 24 0 -0.5 7.5 24 -9 0 -5.3 6.9 -9 -15 0 6.4 8.2 -24 10 0 167.78 14.1 -24 10 0 149.79 13.3 14 -24 0 146.59 17.2 10 14 0 173.48 18 -14 24 0 158.08 15.4 -10 -14 0 223.28 23.1 24 -10 0 157.28 15.7 13 -24 0 249.78 21.1 -24 11 0 260.37 16.9 -24 11 0 228.48 16.8 11 13 0 267.47 22.1 -11 -13 0 278.87 24.7 24 -11 0 270.27 19.1 -13 24 0 257.57 19.4 12 -24 0 6.5 8.1 12 12 0 -4.3 7.3 -24 12 0 -10.6 5.1 -24 12 0 -3.7 5.2 -12 24 0 0.2 6.9 -12 -12 0 1.1 7.5 -24 13 0 5.6 5.5 11 -24 0 15.9 8.3 -24 13 0 5.7 5.9 13 11 0 12.3 10 24 -13 0 14.4 7.5 -11 24 0 18.3 8.8 -13 -11 0 10.2 8.6 14 10 0 91.49 14.7 -24 14 0 80.89 9.4 -24 14 0 82.59 9.3 10 -24 0 80.99 13 -10 24 0 53.89 10.3 -14 -10 0 78.19 14.5 24 -14 0 84.89 11.7 -24 15 0 183.68 12.7 -24 15 0 158.98 12.5 15 9 0 168.28 17.5 9 -24 0 170.88 18 -15 -9 0 169.78 17.4 24 -15 0 161.38 15 -9 24 0 144.89 16.6 -24 16 0 32 6.8 16 8 0 18.6 8.8 8 -24 0 28.6 11.5 -24 16 0 23.8 6.3 -16 -8 0 21.5 8 -8 24 0 28.1 9.9 24 -16 0 20.3 8.5 17 7 0 65.89 13.4 7 -24 0 82.89 14.7 -24 17 0 92.69 9.5 -24 17 0 64.69 9 -17 -7 0 82.89 14.2 -7 24 0 85.99 13 24 -17 0 63.39 11.2 18 6 0 71.59 13.3 -24 18 0 68.99 9 -24 18 0 101.49 10.1 6 -24 0 53.59 10.9 24 -18 0 85.39 12 -18 -6 0 55.29 10.6 -6 24 0 54.19 11.3 19 5 0 9.4 8.6 5 -24 0 20.2 10.3 -24 19 0 14.3 5.9 -24 19 0 2.4 5.7 -19 -5 0 6.3 7.6 -5 24 0 14.1 9.7 24 -19 0 1.6 7.5 -24 20 0 2.2 5.5 -24 20 0 4.4 5.8 4 -24 0 -13.4 7.5 20 4 0 10.6 8.5 24 -20 0 6.4 8.7 -4 24 0 -2.6 7.5 -24 21 0 75.99 9.7 3 -24 0 57.49 13.3 21 3 0 73.79 14.4 -24 21 0 74.79 11.2 -3 24 0 49.9 11.7 24 -21 0 87.59 13 -21 -3 0 51.19 11.5 2 -24 0 16.3 10.3 22 2 0 21.7 10.1 -24 22 0 25 8.6 -24 22 0 26.9 7.1 -22 -2 0 22.8 10.4 -2 24 0 30.3 15.6 24 -22 0 23.3 9.9 23 1 0 229.18 24.7 1 -24 0 170.98 21.1 -24 23 0 200.58 15.7 -24 23 0 168.78 14.8 -1 24 0 211.38 22.2 -23 -1 0 204.88 19.3 -23 -1 0 168.18 19.2 24 -23 0 229.48 20 -24 24 0 167.88 15.2 -24 24 0 158.38 14.7 0 -24 0 203.48 24.4 24 0 0 198.28 20.9 0 24 0 147.79 17.5 -24 0 0 168.08 18.2 -24 0 0 159.58 18.7 24 -24 0 187.78 19.3 -25 1 0 166.08 18.4 1 24 0 162.38 21.3 24 -25 0 185.88 18.7 -25 1 0 115.99 15.2 25 -1 0 146.79 19.4 -24 25 0 152.78 15.2 -1 -24 0 197.08 25.3 -24 25 0 146.59 13.9 2 23 0 -1.6 8.7 -25 2 0 11.9 9.5 -25 2 0 15.5 8.5 23 -25 0 4.7 10.2 -2 -23 0 -2.1 9.9 -23 25 0 8.9 6.5 25 -2 0 4.9 10 -25 3 0 61.59 11.6 22 -25 0 38.5 12.9 3 22 0 38.2 12.1 -25 3 0 55.89 10.6 -3 -22 0 69.29 15.2 -22 25 0 71.59 11.1 25 -3 0 60.49 12.4 -25 4 0 19 8.8 4 21 0 11.7 10.4 -25 4 0 12.8 8.4 21 -25 0 25.6 11.1 -21 25 0 16 7.4 -4 -21 0 24.3 11.7 25 -4 0 9.2 9 20 -25 0 1.1 9.4 -25 5 0 2.8 7.5 5 20 0 4.4 10.9 -25 5 0 -5.9 7.3 25 -5 0 9.8 10.2 -20 25 0 5.9 7.1 -25 6 0 215.28 18 -25 6 0 237.88 20.3 19 -25 0 246.28 20.8 6 19 0 224.58 23.1 25 -6 0 231.68 20.4 -6 -19 0 241.08 24.2 -19 25 0 233.28 19.9 7 18 0 209.38 22.1 18 -25 0 208.18 19.7 -25 7 0 220.88 17.6 25 -7 0 228.58 20 -7 -18 0 223.58 23 -25 8 0 251.97 19 8 17 0 274.77 26.7 -25 8 0 248.38 18.7 17 -25 0 259.77 21.8 25 -8 0 270.87 20.9 -8 -17 0 247.18 23.6 -17 25 0 262.57 19.7 -25 9 0 105.19 13 16 -25 0 117.99 16 -25 9 0 91.69 11.6 9 16 0 80.99 14.4 -16 25 0 108.99 14.1 25 -9 0 77.59 13.1 -9 -16 0 149.69 27.5 15 -25 0 26 10.7 -25 10 0 35.2 8.2 10 15 0 25.7 10.7 -25 10 0 29.4 8 -15 25 0 26.7 8.9 -10 -15 0 31.4 10.5 25 -10 0 44.2 10.6 -25 11 0 108.59 11.6 14 -25 0 90.39 15.4 11 14 0 89.09 16.3 -25 11 0 98.29 11.4 -11 -14 0 68.39 13.5 -14 25 0 89.49 12.8 25 -11 0 80.59 11.9 -25 12 0 6.3 5.9 13 -25 0 -10.3 7.2 12 13 0 -7.4 7.7 -25 12 0 3.5 5.8 -13 25 0 -3.4 6.3 -12 -13 0 -6.9 7.9 -25 13 0 85.19 10.2 13 12 0 142.49 21.2 -25 13 0 96.89 10.6 12 -25 0 95.99 14.5 -12 25 0 67.79 11.4 -13 -12 0 68.79 13 -25 14 0 30.4 7.3 11 -25 0 21.4 9.4 -25 14 0 42 7.5 14 11 0 22.7 11 -11 25 0 32.1 9.8 -14 -11 0 20.5 8.3 25 -14 0 25.3 8.6 -25 15 0 32.2 7.4 10 -25 0 30.5 10.6 -25 15 0 28.6 6.9 15 10 0 38 10.6 -15 -10 0 33 10.5 25 -15 0 19.3 8 -10 25 0 41.1 11.4 9 -25 0 65.49 11.5 -25 16 0 79.59 9.7 16 9 0 65.99 12.8 -25 16 0 93.79 10 25 -16 0 63.49 11 -9 25 0 96.49 15 -16 -9 0 77.99 14.2 17 8 0 9.5 9.7 8 -25 0 -0.2 6.7 -25 17 0 5.4 5.5 -8 25 0 5.1 7.4 -17 -8 0 0.7 7 25 -17 0 2.2 7.6 7 -25 0 123.49 17.7 -25 18 0 83.99 10.1 -25 18 0 124.79 13.4 18 7 0 95.09 13.8 25 -18 0 77.79 12.4 -18 -7 0 109.59 15.8 -7 25 0 80.39 12.5 -25 19 0 319.27 19.6 19 6 0 320.17 25.5 6 -25 0 341.17 26.6 -19 -6 0 321.67 24.7 25 -19 0 354.06 23.5 -6 25 0 336.77 25.2 20 5 0 179.78 20.6 5 -25 0 122.79 17.9 -20 -5 0 137.09 26 25 -20 0 152.78 16.8 -5 25 0 198.58 22.2 21 4 0 28.3 12.1 -25 21 0 15.3 6.6 4 -25 0 17.5 11.2 -4 25 0 16.4 9.4 25 -21 0 10.3 9.5 -25 22 0 117.59 11.7 3 -25 0 107.79 15.7 -25 22 0 139.79 15.8 22 3 0 152.68 19.1 25 -22 0 135.39 15.3 -22 -3 0 128.49 15.8 -3 25 0 105.09 15.4 -25 23 0 14.4 8.9 23 2 0 22.5 10.4 -25 23 0 11.3 6.5 2 -25 0 33.1 13.4 -23 -2 0 12.8 9.4 25 -23 0 12.4 9.5 -23 -2 0 16.6 10.1 -2 25 0 19.6 11.3 -25 24 0 508.35 29.5 24 1 0 519.85 37.9 -25 24 0 512.35 28.8 1 -25 0 553.84 36.2 25 -24 0 539.65 32.7 -1 25 0 528.95 35.7 -24 -1 0 484.15 32.7 -24 -1 0 517.05 33 0 -25 0 151.48 29.2 -25 25 0 81.79 10.9 -25 25 0 59.89 12.1 25 0 0 82.59 15.3 25 -25 0 81.29 14.9 0 25 0 102.79 18.4 -25 0 0 83.39 14.2 -25 0 0 62.59 12.5 1 25 0 98.79 16.1 25 -26 0 87.09 15.2 -26 1 0 80.89 13.7 26 -1 0 117.49 17.2 -25 26 0 80.39 11.9 -1 -25 0 81.49 15 -25 26 0 78.09 12 -26 2 0 62.59 12.8 2 24 0 91.59 17.6 24 -26 0 46.8 12.8 -26 2 0 61.49 11.7 -24 26 0 49.6 9.6 26 -2 0 54.89 13.2 -2 -24 0 75.09 16.7 -24 26 0 62.39 11 23 -26 0 -1.8 10 -26 3 0 13.2 9.5 -26 3 0 9.6 8.3 -3 -23 0 11.2 20.7 26 -3 0 11.4 10.3 -23 26 0 -0.4 6.6 -26 4 0 63.59 11.8 4 22 0 81.69 17.6 22 -26 0 70.59 13.4 -26 4 0 60.39 11.5 -4 -22 0 97.79 21.8 -22 26 0 60.09 10.7 26 -4 0 64.39 14.4 -26 5 0 17.8 8.6 5 21 0 10.6 11 -26 5 0 25.3 9.4 21 -26 0 2.7 8.7 -21 26 0 7.6 6.8 26 -5 0 5.5 9.3 -5 -21 0 8.6 10.6 -26 6 0 25.5 8.8 6 20 0 32.3 24.3 20 -26 0 35.5 11.1 -26 6 0 27.9 9.3 -6 -20 0 37 14.7 26 -6 0 35 10 -20 26 0 22.4 8.5 7 19 0 10.2 13.1 -26 7 0 4 7 -26 7 0 3.1 7 19 -26 0 0.6 9.6 -19 26 0 0.2 7.3 -7 -19 0 12.4 12 26 -7 0 -5.2 9.4 -26 8 0 189.28 16.2 8 18 0 178.98 21.1 18 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167.18 19.5 -10 26 0 198.68 18.6 26 -16 0 166.68 15.8 -16 -10 0 163.78 18.8 9 -26 0 -8.9 8.8 17 9 0 3.8 8.1 -26 17 0 2.3 7 -26 17 0 -8.4 5.9 -17 -9 0 14 9.9 -9 26 0 3 7.9 26 -17 0 -4.6 7.4 8 -26 0 6.3 10.3 18 8 0 13.3 9.9 -26 18 0 11.1 6.2 -8 26 0 18.9 9.2 -18 -8 0 19.9 9.8 26 -18 0 19.2 9.2 -26 19 0 244.28 15.9 7 -26 0 277.77 24 -26 19 0 222.98 17.4 19 7 0 218.08 22.2 -19 -7 0 249.08 21.5 -7 26 0 232.68 21.5 26 -19 0 244.88 20 20 6 0 115.79 16.2 -26 20 0 110.39 11.4 -26 20 0 110.89 11.4 6 -26 0 101.19 14.9 -6 26 0 130.29 18.3 -20 -6 0 126.39 16.3 26 -20 0 127.19 15.8 21 5 0 182.48 20 -26 21 0 145.69 12.9 -26 21 0 159.08 13.4 5 -26 0 187.18 21.2 -5 26 0 174.98 20.2 26 -21 0 152.98 17.1 -26 22 0 302.37 19.3 22 4 0 310.57 26 -26 22 0 304.67 19.3 26 -22 0 325.47 24.1 -4 26 0 338.97 26.9 3 -26 0 291.47 26.6 -26 23 0 251.87 17.9 -26 23 0 295.17 18.5 23 3 0 246.18 24.2 -3 26 0 280.07 25.6 -23 -3 0 259.87 23.1 26 -23 0 330.27 23.1 -26 24 0 66.59 9.9 -26 24 0 83.29 10.7 2 -26 0 65.49 14.4 24 2 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-13 2 2264.77 103.79 -13 5 2 2188.18 105.89 -8 14 -2 297.67 16.7 14 -6 -2 292.47 20.4 -6 -8 -2 290.17 19.2 6 8 2 316.57 19.5 8 -14 2 276.57 18.8 -14 6 2 301.07 20.2 -14 6 2 312.37 20.3 -8 15 -2 417.36 22 -7 -8 -2 421.76 24.3 15 -7 -2 404.56 25.4 7 8 2 425.76 24.5 -15 7 2 400.76 25 8 -15 2 413.76 22.8 -15 7 2 380.06 24.6 16 -8 -2 1161.88 58.49 -8 16 -2 1183.78 55.89 -8 -8 -2 1224.28 57.79 8 -16 2 1089.59 56.29 -16 8 2 1226.98 58.19 -16 8 2 1154.78 58.19 8 8 2 1149.08 57.69 -9 -8 -2 189.68 15.1 -8 17 -2 158.98 12.3 17 -9 -2 144.99 15.2 9 8 2 173.98 14.8 8 -17 2 181.28 13.9 -17 9 2 170.28 15.7 -17 9 2 152.08 14.9 -7 16 -2 188.68 13.1 16 -9 -2 165.68 15.8 -16 9 2 155.48 15.1 9 7 2 177.68 14.6 7 -16 2 165.28 13.6 -16 9 2 177.38 15.8 -6 15 -2 344.37 19.2 15 -9 -2 294.37 21.2 -15 9 2 317.47 20.8 -15 9 2 297.67 20.9 6 -15 2 315.27 19.3 -9 -5 -2 88.79 10 14 -9 -2 125.99 14.1 -5 14 -2 128.79 10.8 9 5 2 128.89 11.8 -14 9 2 124.49 13.4 -14 9 2 140.89 13.5 13 -9 -2 559.24 32.2 -4 13 -2 591.34 30.2 -9 -4 -2 581.74 30.4 9 4 2 590.04 30.7 -13 9 2 619.64 32.5 -13 9 2 581.24 32 4 -13 2 547.65 30.7 -3 12 -2 734.83 38.4 12 -9 -2 710.63 38.4 -9 -3 -2 750.42 36.6 9 3 2 725.13 36.7 -12 9 2 739.93 38.3 3 -12 2 736.33 37.2 -12 9 2 696.83 38.1 -9 -2 -2 1982.9 91.19 -2 11 -2 1972.9 91.99 9 2 2 1987 91.59 -11 9 2 1957.4 92.79 2 -11 2 1989.2 92.19 -1 10 -2 1322.47 62.79 -9 -1 -2 1344.67 61.59 -10 9 2 1298.07 63.59 1 -10 2 1325.67 63.09 9 1 2 1302.27 61.79 -9 0 -2 1277.57 58.19 0 9 -2 1265.17 59.89 9 -9 -2 1180.88 60.59 0 -9 2 1266.17 59.99 -9 9 2 1264.17 60.69 9 0 2 1252.67 58.49 -9 1 -2 3130.09 139.29 1 8 -2 3119.89 141.39 9 -1 2 3119.29 139.79 -1 -8 2 3202.38 141.69 -8 9 2 2882.01 141.59 -9 2 -2 808.32 40.6 2 7 -2 818.32 43.1 7 -9 -2 1012.6 46.6 -2 -7 2 827.92 43.4 -7 9 2 1048.4 46.5 9 -2 2 842.32 41.2 3 6 -2 300.17 18.8 6 -9 -2 293.27 19.6 -9 3 -2 315.77 15.3 -3 -6 2 392.56 21.7 9 -3 2 314.27 16.3 5 -9 -2 417.86 24 4 5 -2 447.26 23.7 -5 9 2 414.26 23.7 -4 -5 2 420.76 23.8 9 -4 2 403.86 20.2 5 4 -2 273.27 17.5 9 -5 2 279.67 13.9 -5 -4 2 285.37 17.8 -4 9 2 286.57 17.8 3 -9 -2 289.27 18.1 6 3 -2 270.47 17.6 -3 9 2 285.17 17.9 -6 -3 2 278.37 18.1 -6 -3 2 262.27 17.8 7 2 -2 5966.7 271.47 2 -9 -2 5910.31 271.37 -2 9 2 6062.29 271.67 1 -9 -2 440.66 25.8 -1 9 2 360.06 23 -8 -1 2 446.66 26 0 -9 -2 1282.77 60.29 -9 0 2 1192.58 60.29 -9 0 2 1230.68 60.29 9 -9 2 1264.47 56.69 -1 -9 -2 679.73 34.6 10 -1 -2 638.84 34.6 -10 1 2 640.24 34.8 1 9 2 657.23 34.5 -10 1 2 642.14 34.7 9 -10 2 678.63 31.1 11 -2 -2 450.15 26.3 2 9 2 441.36 26 -11 2 2 471.25 26.8 9 -11 2 479.75 23.1 -11 2 2 479.55 26.8 -9 12 -2 128.99 7.9 12 -3 -2 151.18 16.1 12 -3 -2 116.09 12.5 -3 -9 -2 120.59 12.3 9 -12 2 109.59 8.9 3 9 2 126.99 12.5 -12 3 2 121.29 13.5 -12 3 2 134.49 13.2 13 -4 -2 9.1 8.5 -4 -9 -2 14 6.4 13 -4 -2 13.6 7.2 9 -13 2 15.5 4.8 -13 4 2 21.6 8 -13 4 2 8.4 6.7 4 9 2 28.9 9.1 -9 14 -2 288.17 15.7 14 -5 -2 312.07 20.1 -5 -9 -2 275.77 18.8 -14 5 2 260.47 19.5 -14 5 2 295.17 19.8 9 -14 2 278.07 17.9 5 9 2 281.97 19.2 15 -6 -2 600.54 33.6 -9 15 -2 620.64 30.1 -6 -9 -2 606.04 32.8 6 9 2 597.74 33 -15 6 2 635.54 33.7 9 -15 2 611.14 30.8 -15 6 2 536.45 34.9 -9 16 -2 683.93 33.3 16 -7 -2 640.34 36.3 -7 -9 -2 669.63 35.8 9 -16 2 705.53 34.4 7 9 2 672.63 36.2 -16 7 2 645.64 36.3 -16 7 2 653.93 36.1 17 -8 -2 596.84 35.1 -8 -9 -2 625.84 34.5 -9 17 -2 619.94 32 -17 8 2 643.04 35 8 9 2 640.34 34.7 9 -17 2 637.84 33 -17 8 2 653.93 35.1 18 -9 -2 33.4 7.9 -9 18 -2 57.19 8.1 -9 -9 -2 49.6 9.1 9 9 2 37.2 8.8 -18 9 2 48.7 9.2 -18 9 2 41.3 9.2 9 -18 2 49.1 8.1 19 -10 -2 43.2 8.7 -10 -9 -2 63.29 10.1 -9 19 -2 56.89 8.6 -19 10 2 74.39 12.2 10 9 2 69.89 11.6 9 -19 2 64.29 9.9 -19 10 2 78.69 12.2 -8 18 -2 170.28 13.4 18 -10 -2 190.08 16.3 -18 10 2 190.48 15.8 8 -18 2 182.98 14.8 -18 10 2 177.98 16.4 10 8 2 189.08 15.7 -7 17 -2 281.27 17.5 17 -10 -2 256.27 20 10 7 2 275.67 19 7 -17 2 273.97 18.4 -17 10 2 306.17 20 -17 10 2 266.97 19.7 -6 16 -2 162.78 12.5 -16 10 2 144.29 15 -16 10 2 174.78 15.1 6 -16 2 151.88 13.4 -10 -5 -2 75.19 9.5 -5 15 -2 82.69 9.6 15 -10 -2 110.19 13.6 5 -15 2 81.79 9.8 -15 10 2 123.39 13.6 10 5 2 66.69 8.5 -15 10 2 74.69 10.2 14 -10 -2 505.15 30.5 -4 14 -2 528.55 28.8 -10 -4 -2 548.55 28.7 -14 10 2 561.84 30.5 10 4 2 542.75 28.9 -10 -3 -2 927.91 44.8 13 -10 -2 951 47.1 -3 13 -2 938.01 45.3 -13 10 2 899.11 46.3 -13 10 2 845.42 46.2 10 3 2 931.91 45.3 3 -13 2 918.71 45.8 12 -10 -2 197.38 17.1 -10 -2 -2 234.18 14.3 -2 12 -2 213.88 16.5 -12 10 2 186.88 16 10 2 2 208.58 14.2 2 -12 2 208.88 15.3 -10 -1 -2 210.68 12.9 -1 11 -2 184.38 14.4 11 -10 -2 279.37 24.6 10 1 2 189.38 13.1 1 -11 2 209.08 15 -11 10 2 162.48 15.2 0 10 -2 1.9 5.1 -10 0 -2 7.9 4.3 10 -10 -2 10.4 13.5 -10 10 2 0.1 8.4 0 -10 2 17.9 6.7 10 0 2 16.6 5.3 1 9 -2 614.34 32.7 9 -10 -2 623.34 34 -10 1 -2 670.33 30.5 -9 10 2 564.14 33.1 10 -1 2 659.93 31.1 -1 -9 2 640.14 33.3 2 8 -2 1783.32 79.89 8 -10 -2 1648.34 80.29 -10 2 -2 1696.63 76.89 -8 10 2 1602.74 79.89 10 -2 2 1661.43 77.49 -2 -8 2 1778.92 80.19 7 -10 -2 497.25 29.4 3 7 -2 547.55 28.9 -7 10 2 509.25 28.9 -3 -7 2 552.14 29.1 10 -3 2 565.44 26 6 -10 -2 156.48 13.8 4 6 -2 140.19 12.7 -4 -6 2 197.58 13.9 -6 10 2 156.18 13.1 10 -4 2 153.98 9.2 5 5 -2 445.66 24.3 -5 10 2 403.76 24 10 -5 2 423.96 20.2 6 4 -2 2498.15 114.39 4 -10 -2 2458.65 114.39 -4 10 2 2477.35 114.49 -6 -4 2 2438.36 114.49 -3 10 2 3934.71 180.38 -7 -3 2 3980 180.58 -7 -3 2 3950.6 180.48 2 -10 -2 1451.55 70.29 8 2 -2 1501.25 70.49 -2 10 2 1394.86 70.09 -8 -2 2 1486.45 70.59 -8 -2 2 1527.55 70.89 1 -10 -2 1309.07 63.99 -9 -1 2 1340.97 64.19 -1 10 2 1327.07 63.89 0 -10 -2 9.8 5.2 10 0 -2 7.7 6.5 10 -10 2 13.3 3.2 -10 0 2 0.7 6.2 0 10 2 9.7 6.4 -10 0 2 4.3 5.6 11 -1 -2 326.07 21 -11 1 2 342.47 21.4 10 -11 2 326.17 16.9 1 10 2 339.57 20.8 12 -2 -2 345.07 22.1 10 -12 2 363.26 18.4 2 10 2 348.17 21.8 -12 2 2 365.46 22.3 -3 -10 -2 414.76 26.4 13 -3 -2 570.34 30.3 -10 13 -2 491.25 23.1 3 10 2 455.75 26.7 10 -13 2 455.75 23.5 -13 3 2 414.16 26.8 -4 -10 -2 59.09 11.3 -10 14 -2 37.6 5 14 -4 -2 44.2 9.1 14 -4 -2 17.2 7.9 10 -14 2 32.1 5.7 4 10 2 30 7.7 -14 4 2 26.8 8.7 -14 4 2 29.5 7.5 -10 15 -2 1261.57 56.49 -5 -10 -2 1202.28 59.69 15 -5 -2 1227.88 60.39 15 -5 -2 1094.99 59.59 -15 5 2 1244.98 62.59 -15 5 2 1216.58 60.09 5 10 2 1221.98 59.99 10 -15 2 1219.08 57.39 -10 16 -2 278.37 15.6 16 -6 -2 278.17 19.8 -6 -10 -2 272.97 18.9 16 -6 -2 250.37 19.1 -16 6 2 265.77 19.4 6 10 2 266.67 19 -16 6 2 268.57 19.4 10 -16 2 272.97 16.6 17 -7 -2 386.96 25.4 -7 -10 -2 410.76 24.5 -10 17 -2 405.96 21.3 7 10 2 391.96 24.2 -17 7 2 379.46 24.7 -17 7 2 341.17 24.2 10 -17 2 418.16 22.5 -8 -10 -2 -1.2 6.2 18 -8 -2 8 8.2 -10 18 -2 11.7 5.1 -18 8 2 10.6 7.5 10 -18 2 14.4 6 8 10 2 9 6.9 -18 8 2 1.5 6.5 -10 19 -2 50.99 7.7 19 -9 -2 50.79 10.5 -9 -10 -2 35.2 8.5 10 -19 2 56.99 8.5 -19 9 2 51.99 9.3 -19 9 2 51.79 9.1 9 10 2 63.29 10.1 -10 20 -2 86.09 9.8 20 -10 -2 78.59 13.4 -10 -10 -2 66.79 11.6 -20 10 2 69.19 12.6 10 10 2 60.79 10.6 -20 10 2 70.29 13.3 10 -20 2 43.3 8.6 21 -11 -2 77.09 11.8 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11.6 -11 -2 -2 122.79 10.5 13 -11 -2 137.89 14.7 -13 11 2 110.69 12.9 2 -13 2 115.19 12.3 11 2 2 125.99 11.1 -1 12 -2 223.28 16.8 -11 -1 -2 188.68 12.8 12 -11 -2 164.08 16.1 11 1 2 200.78 13.3 1 -12 2 192.08 14.9 -12 11 2 184.98 15.4 11 -11 -2 583.24 34.2 0 11 -2 617.04 33.1 -11 0 -2 650.73 31.3 11 0 2 653.23 31.8 0 -11 2 647.84 33.7 10 -11 -2 346.07 22.1 -11 1 -2 350.26 18 1 10 -2 337.17 20.8 -1 -10 2 327.27 20.9 11 -1 2 345.77 18.6 9 -11 -2 448.16 27 2 9 -2 460.85 26.1 -11 2 -2 461.45 22.9 -9 11 2 487.85 26.7 11 -2 2 489.95 23.8 3 8 -2 74.49 9.8 8 -11 -2 71.59 11.3 -8 11 2 44.1 8.5 -3 -8 2 71.89 9.3 11 -3 2 61.89 6.8 7 -11 -2 1683.03 81.19 11 -4 2 1678.53 77.69 -4 -7 2 1734.63 81.09 -7 11 2 1751.62 81.19 5 6 -2 1539.15 75.09 6 -11 -2 1647.24 75.89 11 -5 2 1595.04 71.69 -6 11 2 1553.94 75.29 -5 -6 2 1580.34 75.39 6 5 -2 1202.68 58.09 5 -11 -2 1164.38 58.09 -6 -5 2 1207.28 58.29 7 4 -2 1117.79 63.39 4 -11 -2 1442.26 66.39 -4 11 2 1439.06 66.19 3 -11 -2 3007.6 142.99 -8 -3 2 3072.69 143.29 -8 -3 2 3188.98 143.29 -3 11 2 3157.68 143.09 9 2 -2 1936.21 92.69 2 -11 -2 1984.1 92.99 -9 -2 2 1935.01 92.89 -9 -2 2 2006.4 93.19 -2 11 2 1999.8 92.79 1 -11 -2 176.98 15.4 10 1 -2 201.58 15.6 -10 -1 2 213.68 15.9 -10 -1 2 219.88 16 -1 11 2 185.88 15.3 11 0 -2 659.93 33.9 0 -11 -2 636.94 33.7 11 -11 2 610.34 29.3 0 11 2 618.84 33.5 -11 0 2 643.04 34 -11 0 2 582.64 33.7 -1 -11 -2 466.65 26.8 12 -1 -2 368.56 23.5 -12 1 2 377.16 24 1 11 2 348.87 23.4 -12 1 2 423.96 24.3 11 -12 2 392.36 19.6 13 -2 -2 575.14 32 -2 -11 -2 618.04 32.2 -13 2 2 564.44 31.8 11 -13 2 548.95 28 -13 2 2 565.54 31.9 2 11 2 578.94 31.7 -3 -11 -2 959.2 49.2 14 -3 -2 989.1 49.3 3 11 2 988.3 49.4 -14 3 2 980 49.4 -14 3 2 977.9 49.6 11 -14 2 933.91 45.9 -11 15 -2 979.8 46.1 15 -4 -2 993.8 50.69 11 -15 2 1022.1 47.5 -15 4 2 1002.3 50.79 -15 4 2 970.2 51.19 16 -5 -2 191.78 16.5 -5 -11 -2 203.08 16.4 -11 16 -2 213.78 12.2 16 -5 -2 202.98 17.1 -16 5 2 184.18 16.5 11 -16 2 190.88 13.4 5 11 2 225.58 16.8 -16 5 2 208.08 17 17 -6 -2 618.54 35 17 -6 -2 624.54 35.8 -11 17 -2 613.84 31.1 -6 -11 -2 644.14 35 6 11 2 632.74 35.1 11 -17 2 647.84 32.6 -17 6 2 661.03 35.3 -17 6 2 620.84 35 -11 18 -2 44.8 7.1 18 -7 -2 34.4 8.3 -7 -11 -2 29.4 8.9 11 -18 2 58.29 8.7 -18 7 2 37.6 8.2 -18 7 2 45.6 10.5 7 11 2 31.3 9.9 -8 -11 -2 53.19 10.3 19 -8 -2 93.69 14.3 -11 19 -2 94.39 9.6 -19 8 2 90.19 13.6 -19 8 2 91.29 12.7 11 -19 2 94.39 11 8 11 2 119.29 14.9 -11 20 -2 0.5 4.9 -9 -11 -2 -1.6 6.7 20 -9 -2 -18 6.7 -20 9 2 -0.7 6.3 11 -20 2 0.7 5.5 -20 9 2 4.8 7.4 9 11 2 7.1 7.2 -11 21 -2 17.9 6.8 21 -10 -2 22.3 9.5 -10 -11 -2 16.2 8 11 -21 2 18.1 7.6 10 11 2 19.6 7.2 -21 10 2 8.1 7.8 -11 22 -2 162.78 13.8 22 -11 -2 174.58 17.3 -11 -11 -2 160.48 16.9 -22 11 2 155.78 17.2 11 -22 2 154.48 15.5 11 11 2 180.58 17.2 -11 23 -2 102.89 11.5 23 -12 -2 103.59 15.2 -12 -11 -2 155.58 18.4 -23 12 2 64.89 12.1 -23 12 2 88.99 13.5 11 -23 2 93.19 12.6 12 11 2 75.19 11.7 22 -12 -2 61.69 13.4 -10 22 -2 66.19 10.1 -12 -10 -2 54.79 11.5 -22 12 2 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-1 3 881.71 42.7 2 -1 -3 2546.95 117.09 1 1 3 2505.65 116.59 1 -2 3 2556.54 116.39 -2 1 3 2524.65 116.99 2 1 3 665.03 35.5 -3 2 3 721.93 36.5 1 -3 3 703.13 35.3 1 -3 3 700.03 35.7 2 -2 -3 1904.51 87.49 -2 0 -3 1813.62 86.39 -2 2 3 1908.11 87.29 0 -2 3 1816.32 86.79 2 0 3 1803.92 86.49 0 -2 3 1907.81 86.79 1 -2 -3 2705.93 122.19 -2 1 -3 2643.94 121.29 -1 -1 3 2727.03 121.89 2 -1 3 2638.84 121.39 -1 2 3 2515.65 121.79 -1 -1 3 2652.63 121.89 2 0 -3 1970.9 88.29 -2 2 -3 1941.61 87.19 2 -2 3 1829.22 87.09 0 2 3 1795.32 87.69 -2 0 3 1848.12 87.89 -2 3 -3 113.99 11.3 3 -1 -3 124.09 12.5 2 -3 3 125.09 11.8 -3 1 3 143.19 13.2 2 -3 3 123.89 11.3 4 -2 -3 1804.92 85.79 2 -4 3 1800.02 84.69 2 2 3 1840.72 85.19 2 -4 3 1830.52 84.39 -3 -2 -3 553.04 31.3 2 -5 3 665.53 31.7 -5 3 3 624.14 33.2 2 -5 3 614.14 31.6 3 2 3 594.84 31.8 4 -3 -3 61.49 9.5 -3 -1 -3 64.79 8.9 1 -4 3 68.79 8.5 -4 3 3 86.49 11.3 3 1 3 81.79 9.1 1 -4 3 81.19 9.2 -3 0 -3 525.15 27.7 0 -3 3 501.05 28 3 0 3 514.65 27.7 0 -3 3 532.45 28.1 2 -3 -3 105.99 11.1 -3 1 -3 113.59 11.1 -1 -2 3 134.89 12.4 -2 3 3 130.39 13.2 3 -1 3 106.19 11.7 -1 -2 3 145.79 13.1 2 1 -3 690.43 36.2 -3 2 -3 683.13 34.5 1 -3 -3 687.23 36.1 -2 -1 3 680.03 35.9 3 -2 3 701.63 35 -2 -1 3 731.23 36.2 -1 3 3 692.43 36.1 0 -3 -3 497.85 28.6 -3 3 -3 503.75 26.7 3 0 -3 537.95 28.4 0 3 3 499.25 28.2 -3 0 3 519.55 28.2 3 -3 3 515.45 27.1 -3 0 3 524.45 28.5 4 -1 -3 1570.14 74.69 3 -4 3 1623.94 73.39 1 3 3 1540.35 74.09 3 -4 3 1540.55 72.99 -4 1 3 1550.54 74.49 5 -2 -3 388.96 23.9 3 -5 3 404.66 22.1 -5 2 3 375.06 23.8 2 3 3 390.86 24.5 3 -5 3 406.56 22.1 6 -3 -3 2901.61 134.29 3 -6 3 2898.41 132.69 -6 3 3 2777.82 133.89 3 3 3 2971.5 133.29 -6 3 3 2848.22 133.99 3 -6 3 3010.8 132.69 -4 -3 -3 1416.46 75.59 7 -4 -3 1897.91 80.59 -7 4 3 1841.82 79.89 4 3 3 1480.45 75.99 3 -7 3 1493.15 75.49 3 -7 3 1506.05 75.69 -7 4 3 1785.92 79.59 6 -4 -3 303.77 21 -4 -2 -3 311.67 19 2 -6 3 331.87 19.2 4 2 3 297.67 19.2 -6 4 3 317.27 21 2 -6 3 314.87 18.9 5 -4 -3 786.62 40.8 -4 -1 -3 772.42 38.7 1 -5 3 772.62 39.2 -5 4 3 780.62 40.4 1 -5 3 776.42 39.1 4 1 3 778.52 38.9 4 -4 -3 357.96 22.9 -4 0 -3 355.36 21 0 -4 3 352.76 21.7 -4 4 3 393.66 23.1 0 -4 3 395.36 21.9 4 0 3 371.56 21.3 3 -4 -3 1489.85 72.79 -4 1 -3 1563.44 71.39 -1 -3 3 1547.35 72.39 -3 4 3 1472.95 72.69 4 -1 3 1523.25 71.49 -1 -3 3 1561.44 72.39 2 -4 -3 1763.92 85.29 -4 2 -3 1877.91 83.79 4 -2 3 1849.11 84.09 -2 -2 3 1830.22 85.29 -2 4 3 1781.12 85.39 -2 -2 3 1761.82 84.99 3 1 -3 86.49 10.9 -4 3 -3 88.49 9.1 1 -4 -3 50.99 8.5 -3 -1 3 100.39 11.4 -1 4 3 82.99 11.2 4 -3 3 82.29 8.8 -3 -1 3 108.29 11.6 0 -4 -3 359.26 22.2 -4 0 3 394.56 22.6 4 -4 3 351.06 20.5 0 4 3 368.16 22.4 5 -1 -3 368.46 22.8 4 -5 3 366.96 20.4 4 -5 3 373.66 20.9 -5 1 3 384.66 22.8 1 4 3 346.77 22 -5 1 3 368.56 22.9 6 -2 -3 2194.28 99.89 2 4 3 2134.89 99.09 -6 2 3 2107.09 99.59 4 -6 3 2128.09 97.59 4 -6 3 2050.29 97.69 7 -3 -3 143.89 14.3 3 4 3 135.49 14.6 4 -7 3 146.29 11.9 -7 3 3 192.88 18.4 -7 3 3 161.18 14.6 4 -7 3 123.49 11.8 8 -4 -3 977.2 45.6 -8 4 3 766.12 41.9 4 -8 3 790.32 40.1 4 -8 3 787.92 40 4 4 3 777.22 40.9 -5 -4 -3 733.73 38.8 -9 5 3 919.91 43.7 5 4 3 759.82 39.3 4 -9 3 752.02 38.8 -9 5 3 731.03 40.6 8 -5 -3 47.1 8.5 -5 -3 -3 49.99 7.9 -8 5 3 56.99 10.9 -8 5 3 38.3 8 5 3 3 44.2 8.5 3 -8 3 52.49 7.7 -5 -2 -3 177.18 14 7 -5 -3 191.78 16.7 -7 5 3 179.18 15.9 2 -7 3 182.48 14.3 5 2 3 195.38 14.3 2 -7 3 209.58 14.4 6 -5 -3 1446.96 69.99 -5 -1 -3 1449.65 67.99 1 -6 3 1442.06 68.79 1 -6 3 1451.65 68.79 5 1 3 1450.65 68.39 5 -5 -3 2598.64 121.69 -5 0 -3 2688.03 119.89 0 -5 3 2759.72 120.99 -5 5 3 2567.84 121.59 5 0 3 2536.75 119.89 0 -5 3 2576.64 120.79 4 -5 -3 373.36 23.9 -5 1 -3 381.66 21.4 -4 5 3 385.16 23.7 -1 -4 3 397.96 22.9 5 -1 3 383.76 21.5 -1 -4 3 388.96 22.5 3 -5 -3 370.76 23.6 -5 2 -3 395.96 21.1 -2 -3 3 402.36 23.2 -2 -3 3 399.86 23.2 5 -2 3 372.76 21.5 2 -5 -3 609.34 33.1 -5 3 -3 619.14 30.8 5 -3 3 618.84 31.3 -3 -2 3 621.64 33.2 -2 5 3 617.44 33.3 -3 -2 3 617.54 32.9 1 -5 -3 801.02 41.1 -4 -1 3 799.92 41.3 -1 5 3 748.93 40.7 5 -4 3 814.12 39.3 -4 -1 3 846.82 41.3 0 -5 -3 2604.14 122.09 5 0 -3 2690.23 122.79 5 -5 3 2606.64 120.29 5 -5 3 2631.14 120.59 -5 0 3 2594.44 122.49 0 5 3 2728.33 122.39 6 -1 -3 1617.64 76.09 -1 -5 -3 1583.34 75.09 1 5 3 1550.84 74.99 5 -6 3 1630.94 73.49 -6 1 3 1525.45 75.49 5 -6 3 1571.24 73.49 7 -2 -3 -9.6 6.4 2 5 3 -0.3 6.4 5 -7 3 1.4 5.1 -7 2 3 13 6.1 5 -7 3 11.4 5.4 -7 2 3 9.3 6.1 8 -3 -3 935.11 46.7 5 -8 3 930.41 44 3 5 3 901.31 45.4 5 -8 3 861.51 43.9 9 -4 -3 179.88 16.2 5 -9 3 195.38 15.3 -9 4 3 169.88 16.2 -9 4 3 287.57 24.1 10 -5 -3 23 7.7 -5 10 -3 47 7 5 5 3 34.8 7.5 -10 5 3 18.3 7 -10 5 3 9.6 6.5 5 -10 3 25.6 6.2 -6 -5 -3 805.12 41.9 -5 11 -3 863.31 40.8 11 -6 -3 815.82 43.8 -11 6 3 830.62 43.6 5 -11 3 826.12 41.3 6 5 3 834.12 42.2 10 -6 -3 819.52 44.8 -4 10 -3 878.31 42.1 -6 -4 -3 891.41 43.2 -10 6 3 876.61 45 -10 6 3 854.01 44.8 6 4 3 866.81 43.3 4 -10 3 832.62 44.5 -6 -3 -3 423.46 23 -3 9 -3 396.66 22.3 9 -6 -3 383.26 25.2 -9 6 3 506.05 29.3 3 -9 3 394.66 23.4 6 3 3 377.06 22.9 -9 6 3 392.86 25 -2 8 -3 83.79 9.9 8 -6 -3 84.09 12.7 -6 -2 -3 73.79 9.3 -8 6 3 64.79 11 2 -8 3 86.99 9.9 6 2 3 57.29 8.5 -6 -1 -3 2021.9 90.39 7 -6 -3 1917.31 92.39 -1 7 -3 1735.83 94.29 -7 6 3 1981.8 92.39 1 -7 3 1991.5 91.29 1 -7 3 1982.4 91.39 6 1 3 2011.7 90.89 -6 0 -3 1008.3 49.5 6 -6 -3 1018.4 51.99 0 6 -3 1044 50.59 -6 6 3 1015.5 51.89 0 -6 3 1090.19 51.19 6 0 3 1046.6 50.09 0 -6 3 1040.6 51.39 1 5 -3 1611.94 74.89 5 -6 -3 1557.54 75.99 -6 1 -3 1568.94 73.49 -1 -5 3 1598.74 75.19 6 -1 3 1620.54 73.99 -5 6 3 1542.65 75.79 -1 -5 3 1591.74 75.29 -6 2 -3 2255.97 99.29 -4 6 3 2131.69 101.59 -2 -4 3 2147.69 101.09 -2 -4 3 2130.69 101.19 6 -2 3 2168.18 99.59 -6 3 -3 3017.3 132.89 3 -6 -3 2962.8 135.49 6 -3 3 2904.71 133.19 -3 -3 3 2889.51 134.89 -3 6 3 2850.71 135.29 -3 -3 3 2953 135.19 2 -6 -3 295.57 20.4 -4 -2 3 315.67 20.5 6 -4 3 303.47 17.8 -4 -2 3 316.37 20.3 -2 6 3 310.07 20.3 1 -6 -3 1441.86 69.29 -1 6 3 1480.15 69.39 6 -5 3 1408.06 66.99 -5 -1 3 1432.16 69.29 0 -6 -3 1035.8 51.99 -6 0 3 1009.3 52.19 -6 0 3 1097.69 52.89 0 6 3 1041.2 52.09 6 -6 3 1048.3 49.9 6 -6 3 1069.69 49.8 7 -1 -3 503.45 29.5 -1 -6 -3 505.45 28.7 6 -7 3 527.75 26.4 6 -7 3 501.75 26.4 1 6 3 505.35 28.7 -7 1 3 530.25 29.5 -7 1 3 521.85 29.3 -2 -6 -3 927.91 45.8 8 -2 -3 901.81 46.7 2 6 3 883.41 45.6 -8 2 3 895.41 46.4 6 -8 3 896.51 43.8 -8 2 3 938.11 46.5 6 -8 3 904.51 43.7 -9 3 3 799.62 42.1 3 6 3 796.92 41.3 6 -9 3 805.12 41 -9 3 3 811.72 42.1 10 -4 -3 44.1 8.5 -10 4 3 51.89 9.1 4 6 3 41.2 7.6 6 -10 3 55.99 7.8 -10 4 3 67.69 11.7 -6 11 -3 851.91 40.5 -11 5 3 818.42 43.8 6 -11 3 822.02 41.3 -11 5 3 890.71 44.5 5 6 3 816.42 42.9 -6 12 -3 95.59 9.6 12 -6 -3 81.79 12.1 -12 6 3 111.59 13.9 -12 6 3 91.09 12.9 6 -12 3 74.69 9.3 -7 -6 -3 409.56 23.8 13 -7 -3 387.36 25.4 -6 13 -3 414.96 22.2 -13 7 3 402.36 26 -13 7 3 403.66 25.6 6 -13 3 400.36 23 7 6 3 407.06 24.2 12 -7 -3 302.97 21.5 -7 -5 -3 301.47 19.4 -5 12 -3 316.07 18.3 -12 7 3 303.77 21.5 -12 7 3 300.17 21.3 7 5 3 310.87 19.8 5 -12 3 323.57 19.4 11 -7 -3 147.49 15.5 -7 -4 -3 166.28 13.1 -4 11 -3 144.69 11.8 -11 7 3 145.09 15.4 7 4 3 153.18 13 -11 7 3 172.08 18.4 4 -11 3 138.59 12.7 -7 -3 -3 101.59 10.6 -3 10 -3 103.19 10.4 10 -7 -3 90.79 11.6 7 3 3 103.69 10.9 3 -10 3 94.69 11.4 -10 7 3 132.79 15 9 -7 -3 136.39 14.7 -7 -2 -3 112.69 11.2 -2 9 -3 141.39 11.5 7 2 3 113.39 11.6 -9 7 3 124.09 14 2 -9 3 149.88 12.8 8 -7 -3 894.01 46.6 -1 8 -3 949.51 45.3 -7 -1 -3 923.91 44.2 7 1 3 906.01 44.4 1 -8 3 884.91 45.2 -8 7 3 875.61 46.4 -7 0 -3 840.32 40.4 0 7 -3 778.82 47.4 7 -7 -3 818.02 43.5 7 0 3 854.71 41.1 0 -7 3 846.12 44.5 -7 7 3 834.32 43.4 0 -7 3 837.32 42.2 1 6 -3 546.95 28.1 -7 1 -3 514.35 26.3 6 -7 -3 496.75 29.4 -1 -6 3 505.75 28.7 -1 -6 3 507.65 28.5 7 -1 3 494.85 26.7 -7 2 -3 -2.9 4.7 2 5 -3 15.6 7.3 5 -7 -3 -2 5.9 7 -2 3 -1.2 5.1 -2 -5 3 6.8 6.1 -5 7 3 6.7 9.9 -2 -5 3 4.2 6.3 4 -7 -3 138.09 14.8 -7 3 -3 137.39 10.1 3 4 -3 170.68 14 7 -3 3 139.79 11.5 -3 -4 3 158.58 14 -3 -4 3 137.39 14 -4 7 3 132.09 14.3 4 3 -3 1422.56 68.99 3 -7 -3 1410.86 69.59 7 -4 3 1496.15 67.19 -3 7 3 1363.56 69.39 -4 -3 3 1519.65 69.89 2 -7 -3 181.38 16.2 5 2 -3 202.18 15.5 -5 -2 3 184.68 15.8 -2 7 3 180.48 15.7 7 -5 3 172.88 12.7 -5 -2 3 230.78 16.3 1 -7 -3 1983.3 92.89 7 -6 3 1925.11 90.19 -6 -1 3 1975.5 92.79 -6 -1 3 1997.4 93.19 0 -7 -3 874.21 43.9 7 0 -3 859.61 44.4 7 -7 3 849.81 41.1 7 -7 3 858.31 41.1 -7 0 3 863.21 44.4 0 7 3 865.21 43.9 -7 0 3 827.82 44.1 8 -1 -3 181.78 16.6 -1 -7 -3 208.38 15.9 -8 1 3 204.18 17.1 1 7 3 207.68 15.9 7 -8 3 163.88 12.4 -8 1 3 282.57 20.8 7 -8 3 194.08 12.8 9 -2 -3 550.74 33.5 -2 -7 -3 610.64 32.9 2 7 3 600.64 32.8 7 -9 3 685.63 35.4 7 -9 3 579.64 30.3 -9 2 3 609.24 33.3 -3 -7 -3 396.66 24.5 -10 3 3 423.46 25.7 3 7 3 413.06 24.4 7 -10 3 420.56 22.5 -4 -7 -3 422.66 25.7 11 -4 -3 475.65 29.1 7 -11 3 413.46 22.4 4 7 3 380.76 24.1 -11 4 3 389.06 25.3 -11 4 3 383.86 25.3 12 -5 -3 39.4 9.2 -7 12 -3 71.49 7.8 -12 5 3 65.59 10.4 7 -12 3 66.29 8.6 -12 5 3 84.89 14.2 5 7 3 56.79 8.7 -7 13 -3 514.85 27.1 13 -6 -3 624.34 34.9 7 -13 3 519.35 28.1 -13 6 3 501.55 31 6 7 3 532.15 30 14 -7 -3 182.88 16.6 -7 14 -3 174.18 12.3 -14 7 3 166.08 16.8 7 7 3 177.58 15.1 7 -14 3 168.78 13.5 -7 15 -3 580.74 30 15 -8 -3 593.84 33.9 -8 -7 -3 554.34 31.6 -15 8 3 606.04 34 7 -15 3 566.24 31 -8 -6 -3 178.38 14.1 14 -8 -3 202.08 17.1 -6 14 -3 179.58 12.8 -14 8 3 182.48 17.2 8 6 3 149.39 14.3 6 -14 3 156.88 13.7 -8 -5 -3 310.47 19.7 -5 13 -3 307.57 18.6 -13 8 3 297.97 21.7 5 -13 3 304.07 19.7 8 5 3 298.77 19.9 -13 8 3 382.16 25.3 12 -8 -3 299.87 26.2 -8 -4 -3 194.18 14.8 -4 12 -3 202.88 14.2 4 -12 3 189.88 15 -12 8 3 194.58 17.2 -12 8 3 300.07 26 8 4 3 197.28 15.2 11 -8 -3 194.88 17.9 -8 -3 -3 205.98 14.8 -3 11 -3 217.88 14.8 -11 8 3 189.88 17.2 3 -11 3 216.48 15.7 -11 8 3 289.07 21.7 8 3 3 188.38 14.7 -2 10 -3 335.67 19.6 -8 -2 -3 336.77 19.4 10 -8 -3 363.76 25.4 2 -10 3 309.37 22.1 8 2 3 307.47 19.5 -1 9 -3 670.03 33.3 -8 -1 -3 620.34 32 9 -8 -3 604.44 34.7 1 -9 3 606.54 33.4 -9 8 3 651.13 35.1 8 1 3 637.94 32.5 -8 0 -3 2628.74 117.49 0 8 -3 2692.03 119.19 8 -8 -3 2444.26 120.09 8 0 3 2568.14 117.99 0 -8 3 2524.65 119.09 -8 1 -3 202.68 13.4 1 7 -3 202.18 22.4 7 -8 -3 236.08 20.6 -7 8 3 240.48 20.7 -1 -7 3 198.48 16 8 -1 3 210.18 14.1 -1 -7 3 217.78 16 2 6 -3 959.8 46.4 -8 2 -3 974.3 44 6 -8 -3 875.81 47.3 -2 -6 3 929.51 46.7 8 -2 3 925.21 44.6 -6 8 3 909.91 47.2 -2 -6 3 887.11 46.4 3 5 -3 896.31 46.5 5 -8 -3 923.31 47.4 -8 3 -3 946.11 43.6 8 -3 3 933.01 44.5 -3 -5 3 935.71 47 4 4 -3 814.72 41.3 4 -8 -3 798.82 42.1 -4 8 3 783.32 41.9 -4 -4 3 820.62 41.6 8 -4 3 789.82 38.8 -4 -4 3 828.52 41.7 3 -8 -3 48.2 9.8 5 3 -3 68.49 10.3 -5 -3 3 61.29 9.4 8 -5 3 49.3 6.8 -5 -3 3 66.19 10.6 -3 8 3 32.2 8.2 2 -8 -3 51.79 9.5 -2 8 3 51.69 8 -6 -2 3 102.19 17.1 -6 -2 3 47.9 7.6 8 -6 3 76.79 7.6 7 1 -3 913.01 46 1 -8 -3 886.81 46.1 -7 -1 3 927.61 46.6 -1 8 3 901.41 46.1 8 -7 3 917.51 43.1 -7 -1 3 888.41 46.2 8 -7 3 885.41 42.7 0 -8 -3 2562.64 117.59 8 -8 3 2487.55 114.69 8 -8 3 2497.75 114.59 0 8 3 2535.95 117.49 9 -1 -3 8.9 7.2 -1 -8 -3 29.5 8.6 8 -9 3 24.4 5.6 -9 1 3 33.5 9.2 1 8 3 9.6 6.5 -9 1 3 19.9 9.5 -2 -8 -3 382.86 23.9 -10 2 3 387.36 24.3 8 -10 3 386.26 20.7 2 8 3 365.46 23.4 -10 2 3 410.36 24.7 11 -3 -3 580.04 34 -3 -8 -3 612.54 32.9 -11 3 3 589.34 33.9 -11 3 3 603.04 33.8 8 -11 3 628.84 30.4 3 8 3 575.04 32.7 12 -4 -3 -2.5 6.7 -4 -8 -3 11.1 6.1 4 8 3 0.3 5.9 -12 4 3 1.6 9.7 -12 4 3 4.1 6.6 8 -12 3 5.1 4.9 -5 -8 -3 109.39 12.1 13 -5 -3 128.19 14.7 -8 13 -3 97.99 8.7 -13 5 3 106.79 12.8 5 8 3 111.09 11.9 8 -13 3 99.29 10.1 -13 5 3 182.68 19.6 -8 14 -3 146.29 10.6 14 -6 -3 130.09 15.1 6 8 3 143.09 13.8 -14 6 3 174.58 18.8 8 -14 3 137.39 12 -14 6 3 173.48 19.9 15 -7 -3 135.79 16.1 -8 15 -3 88.49 9.1 7 8 3 95.99 11.4 -15 7 3 126.79 15.8 -15 7 3 92.89 11.6 8 -15 3 101.49 10.7 -8 16 -3 137.79 11.4 16 -8 -3 171.98 19.9 8 8 3 131.89 14.4 -16 8 3 160.78 16.3 -16 8 3 151.08 16 8 -16 3 145.69 13 -8 17 -3 10 5.6 17 -9 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29.9 8 -4 4 486.55 27.3 3 -8 -4 398.56 25.8 -5 -3 4 393.16 25.9 8 -5 4 394.16 23.2 -5 -3 4 447.66 27.6 2 -8 -4 572.04 32.5 8 -6 4 567.74 29.6 -2 8 4 562.34 32.2 -6 -2 4 516.85 35.1 -6 -2 4 541.55 32.6 1 -8 -4 281.27 19.8 -7 -1 4 340.27 24.1 8 -7 4 225.58 15.8 8 -7 4 244.88 16.6 -7 -1 4 213.98 19.5 -1 8 4 238.48 19 0 -8 -4 204.28 18.2 8 -8 4 244.48 15.9 -8 0 4 293.57 23.5 -8 0 4 220.28 19.2 8 -8 4 228.28 15.3 0 8 4 224.48 18.8 9 -1 -4 221.98 22.2 -1 -8 -4 171.48 16.5 -9 1 4 175.88 17.7 8 -9 4 160.28 13.6 8 -9 4 177.28 13.3 1 8 4 179.68 16.8 -9 1 4 172.18 17.7 -2 -8 -4 4.9 7.3 10 -2 -4 9.2 7.4 -10 2 4 5.3 14.8 2 8 4 11.8 7.4 8 -10 4 11.9 5.8 8 -10 4 2.5 5.7 -10 2 4 17.2 11.1 -3 -8 -4 131.79 15.1 11 -3 -4 149.09 17.2 3 8 4 139.19 15.1 -11 3 4 152.28 17 -11 3 4 112.89 14.1 8 -11 4 129.29 12.6 8 -11 4 165.28 13.1 12 -4 -4 524.35 33.1 8 -12 4 581.04 29.6 -12 4 4 552.14 33.2 -12 4 4 505.25 33 8 -12 4 529.05 29.4 4 8 4 539.05 31.7 13 -5 -4 249.18 21.3 8 -13 4 234.58 17.5 -13 5 4 257.27 21.5 8 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9 4 4 64.59 10.5 -9 -3 -4 250.47 17.9 12 -9 -4 248.58 21.7 -3 12 -4 258.07 17.9 3 -12 4 248.98 19 -12 9 4 228.68 21.3 9 3 4 265.77 18.7 -12 9 4 298.67 25.5 -2 11 -4 243.78 17.5 11 -9 -4 350.86 30.4 -9 -2 -4 240.38 16.8 -11 9 4 230.38 20.7 2 -11 4 226.38 18.2 2 -11 4 211.78 18.2 9 2 4 250.07 17.9 -1 10 -4 377.56 24 -9 -1 -4 393.66 23 10 -9 -4 371.66 26.9 9 1 4 405.26 24 -10 9 4 414.26 26.7 1 -10 4 393.66 24.8 1 -10 4 420.36 25.6 0 9 -4 759.62 41.8 9 -9 -4 967.8 48.1 -9 0 -4 798.92 40.3 -9 9 4 780.22 43.9 9 0 4 797.32 41.2 0 -9 4 775.72 42.6 8 -9 -4 184.08 18.9 -9 1 -4 142.69 12.8 9 -1 4 178.38 14.4 -8 9 4 197.98 21.5 -1 -8 4 168.78 16 -1 -8 4 169.78 16.1 7 -9 -4 38 9.4 -9 2 -4 26.8 6.5 -2 -7 4 34.4 9.3 -2 -7 4 40 9.9 9 -2 4 37.6 7.4 -7 9 4 47.4 11.4 -9 3 -4 97.49 9.4 6 -9 -4 98.89 12.3 -3 -6 4 139.79 15 9 -3 4 91.89 11 -6 9 4 96.29 13.2 -3 -6 4 116.29 13.5 5 -9 -4 229.68 19.5 9 -4 4 250.47 16.8 -5 9 4 225.28 19.7 -4 -5 4 281.37 20.3 -4 -5 4 284.57 20.1 4 -9 -4 679.43 37.2 -5 -4 4 586.74 33.6 -5 -4 4 515.25 33 9 -5 4 575.24 30.4 -4 9 4 570.34 33.7 3 -9 -4 298.57 22.1 9 -6 4 302.37 18.7 -3 9 4 303.87 21.9 -6 -3 4 303.17 22.1 -6 -3 4 323.07 25.3 2 -9 -4 39.7 10 9 -7 4 57.29 7.6 9 -7 4 43.8 7.5 -2 9 4 39.1 8.4 -7 -2 4 49.7 12.9 -7 -2 4 74.59 14 1 -9 -4 5.9 8 9 -8 4 17.1 6.4 9 -8 4 6.4 5.3 -8 -1 4 13.5 8.5 -8 -1 4 5.9 7.6 -1 9 4 11.6 7.9 0 -9 -4 798.92 42.1 -9 0 4 753.32 42.7 9 -9 4 763.62 38.9 0 9 4 780.02 42 9 -9 4 795.82 38.7 -9 0 4 760.72 42.5 -1 -9 -4 152.48 16.4 9 -10 4 149.19 12.8 -10 1 4 237.18 21.9 1 9 4 143.49 15.9 9 -10 4 161.28 13.2 -10 1 4 266.77 26.5 -2 -9 -4 147.69 16 11 -2 -4 133.69 15.7 9 -11 4 150.68 12.9 -11 2 4 161.58 17 9 -11 4 143.39 12.3 2 9 4 141.49 15.7 -11 2 4 159.78 17.4 -3 -9 -4 256.47 20 12 -3 -4 227.78 20.5 -12 3 4 211.28 20.9 9 -12 4 267.67 17.1 -12 3 4 229.68 20.8 9 -12 4 250.07 16.5 3 9 4 247.28 19.5 -4 -9 -4 147.99 15.7 13 -4 -4 127.19 16.8 9 -13 4 143.19 13 -13 4 4 122.09 16.6 9 -13 4 137.39 13.1 -13 4 4 106.79 14 4 9 4 169.68 16.2 14 -5 -4 54.59 12.3 -14 5 4 35.6 10.1 -14 5 4 27.8 10.6 9 -14 4 59.29 9.7 5 9 4 47 10.4 15 -6 -4 225.48 25 9 -15 4 201.38 16.1 -15 6 4 178.98 19.9 6 9 4 185.38 18.5 -15 6 4 270.97 27.3 16 -7 -4 249.68 25.7 9 -16 4 292.47 19.7 -16 7 4 272.97 23.9 7 9 4 247.88 21.3 -16 7 4 245.18 23.2 -8 -9 -4 122.89 16 17 -8 -4 145.09 19.5 8 9 4 148.59 17.8 -17 8 4 184.48 24.3 -17 8 4 83.89 13.6 9 -17 4 119.09 14.1 -9 -9 -4 13.4 9.1 18 -9 -4 -6.9 8.7 -18 9 4 12.7 11.2 9 9 4 18.4 9.3 -18 9 4 11.9 10 9 -18 4 16.3 9.1 19 -10 -4 91.69 22.1 -10 -9 -4 87.49 14.4 -9 19 -4 76.79 13.4 -19 10 4 67.89 14.6 -19 10 4 80.69 15.6 9 -19 4 58.29 12.3 10 9 4 70.39 13.6 18 -10 -4 48.2 16.4 -10 -8 -4 23.5 9.5 -8 18 -4 24.4 7.4 -18 10 4 13.1 11.4 10 8 4 30.5 10 8 -18 4 40.8 9.6 -18 10 4 28.1 12.6 17 -10 -4 177.38 20.5 -10 -7 -4 185.98 17.5 -7 17 -4 163.48 14.3 7 -17 4 193.38 17.1 10 7 4 176.08 18.3 -17 10 4 276.47 26.8 -17 10 4 179.08 20.6 -6 16 -4 57.99 9.9 16 -10 -4 23.2 11.6 -10 -6 -4 57.69 10.3 10 6 4 32.6 9.6 -16 10 4 30.8 11.5 6 -16 4 55.79 11.2 -16 10 4 30.2 12.8 -10 -5 -4 107.69 13.5 15 -10 -4 112.19 16.6 -5 15 -4 99.39 11.9 -15 10 4 115.49 16.9 -15 10 4 132.99 17.8 10 5 4 93.29 13.6 5 -15 4 93.09 13.5 14 -10 -4 15.3 12.6 -4 14 -4 22.5 7.1 -10 -4 -4 30.6 8.1 -14 10 4 18.5 9 -14 10 4 11.1 9.5 10 4 4 6.8 7 4 -14 4 23.3 7.9 -10 -3 -4 107.79 12.9 13 -10 -4 159.18 19.7 -3 13 -4 120.79 12.9 3 -13 4 126.39 14.6 -13 10 4 154.88 18.9 -13 10 4 95.29 14.5 10 3 4 117.09 13.6 -10 -2 -4 101.29 11.9 12 -10 -4 115.19 16.1 -2 12 -4 115.09 12.7 2 -12 4 145.49 15.2 10 2 4 131.49 14.3 -12 10 4 105.79 15.5 -1 11 -4 237.28 18.1 11 -10 -4 241.68 21.8 -10 -1 -4 227.08 16.8 10 1 4 249.97 17.8 1 -11 4 264.47 19.7 -11 10 4 349.67 26.4 1 -11 4 249.97 19.6 0 10 -4 316.87 21.4 -10 0 -4 311.17 19.5 10 0 4 319.97 20.4 0 -10 4 318.07 24.7 -10 10 4 294.07 23.6 0 -10 4 337.87 22.2 -10 1 -4 163.78 13 1 9 -4 189.98 15.9 9 -10 -4 151.38 17.5 -9 10 4 169.38 18.7 10 -1 4 164.98 14 -1 -9 4 174.18 16.6 -1 -9 4 168.78 16.4 2 8 -4 10.6 8 8 -10 -4 5 10.8 -10 2 -4 8.5 5 -2 -8 4 7.6 7.2 -8 10 4 6 7.9 -2 -8 4 11.4 7.6 10 -2 4 1.1 5.7 7 -10 -4 122.19 18 -10 3 -4 100.59 9.2 3 7 -4 79.59 10.7 -3 -7 4 67.89 10.5 10 -3 4 97.49 10.6 -3 -7 4 72.39 10.7 -7 10 4 68.29 11.7 4 6 -4 89.39 12.5 6 -10 -4 64.29 11.5 -6 10 4 96.69 14.6 10 -4 4 92.49 9.8 -4 -6 4 83.89 11.9 -4 -6 4 104.19 13.9 5 -10 -4 61.19 10.3 -5 10 4 56.79 10.1 -5 -5 4 71.69 12.1 10 -5 4 85.59 9.7 -5 -5 4 86.49 13.2 -4 10 4 367.06 26.7 -6 -4 4 285.67 22.9 10 -6 4 312.27 19.5 -6 -4 4 410.76 27.2 3 -10 -4 56.89 18.4 -7 -3 4 44.6 10 -3 10 4 53.09 13.2 10 -7 4 42.6 7.7 -7 -3 4 33.3 15.9 2 -10 -4 6 7.2 10 -8 4 9.4 5.8 -8 -2 4 15 8.4 -2 10 4 20.5 11.4 10 -8 4 10.7 5.7 -8 -2 4 25.4 8.3 1 -10 -4 386.96 26.4 10 -9 4 408.66 22.9 -1 10 4 492.25 30.2 10 -9 4 399.26 22.5 -9 -1 4 402.56 27.2 0 -10 -4 322.67 23 10 -10 4 294.07 18.9 10 -10 4 326.27 18.7 -10 0 4 327.87 23.7 -10 0 4 311.97 23.7 0 10 4 314.97 22.9 -1 -10 -4 143.49 16.2 -11 1 4 230.88 22.2 10 -11 4 145.39 12.3 -11 1 4 158.88 17.7 10 -11 4 140.79 12.1 1 10 4 122.89 15.1 -2 -10 -4 338.57 23.7 -12 2 4 326.57 24.7 10 -12 4 337.37 20 2 10 4 345.57 23.6 10 -12 4 307.17 19.4 -12 2 4 326.87 24.6 -3 -10 -4 171.08 17.8 13 -3 -4 289.97 25.7 10 -13 4 171.88 14.6 10 -13 4 179.88 14.5 -13 3 4 299.37 28.1 -13 3 4 274.47 25.2 3 10 4 189.48 18.3 -4 -10 -4 347.97 24.8 14 -4 -4 310.37 25.5 10 -14 4 320.27 21.2 10 -14 4 347.17 21.4 -14 4 4 413.96 31.1 4 10 4 357.96 25 -14 4 4 446.56 31.8 -5 -10 -4 34.8 10.2 15 -5 -4 65.79 13.5 -15 5 4 34.2 11 10 -15 4 47.2 8.5 -15 5 4 52.09 12.6 5 10 4 51.09 11.3 -16 6 4 362.46 27.2 -16 6 4 371.86 27.5 6 10 4 369.56 26.4 10 -16 4 388.06 23.3 17 -7 -4 90.89 25 7 10 4 69.89 13.2 -17 7 4 80.49 14.8 -17 7 4 152.48 22 10 -17 4 53.69 9.9 18 -8 -4 79.69 15.2 10 -18 4 106.69 13 8 10 4 134.89 17.2 -18 8 4 169.98 21.5 -18 8 4 146.49 18.7 19 -9 -4 186.98 22.6 -9 -10 -4 203.38 19.2 10 -19 4 197.78 17.7 -19 9 4 247.18 26.9 9 10 4 178.48 20 -19 9 4 188.18 21.4 -10 20 -4 206.78 15.7 -10 -10 -4 217.68 20.8 20 -10 -4 261.37 23.6 10 10 4 226.28 22 -20 10 4 219.78 22.7 -20 10 4 223.78 23.6 10 -20 4 215.58 19 -11 -10 -4 312.27 24.9 -10 21 -4 317.97 20.1 -21 11 4 307.37 27.2 10 -21 4 300.77 22.7 11 10 4 317.57 25.8 -21 11 4 305.27 26.8 -9 20 -4 47.8 9.5 -11 -9 -4 60.39 12.8 20 -11 -4 31 12.4 -20 11 4 27.1 13.2 -20 11 4 53.59 15.1 9 -20 4 58.79 11.9 -11 -8 -4 11.8 8.4 -8 19 -4 32.9 8.7 19 -11 -4 5.8 11.2 11 8 4 17.1 9.8 -19 11 4 14.8 11.3 -19 11 4 21.5 11.2 8 -19 4 1.4 7.7 -11 -7 -4 28.8 9.6 -7 18 -4 23.2 9.1 18 -11 -4 15.6 11.5 7 -18 4 24.7 8.5 -18 11 4 38 12 11 7 4 29.5 10.2 -18 11 4 28.5 11.9 -6 17 -4 113.59 13.2 -11 -6 -4 173.38 17.6 17 -11 -4 146.09 19.8 -17 11 4 107.39 16.7 6 -17 4 110.09 13.6 11 6 4 138.49 16.5 16 -11 -4 25.3 11.9 -11 -5 -4 53.79 10.3 -5 16 -4 47.4 8.9 11 5 4 40.5 9.6 5 -16 4 23.7 9.1 -16 11 4 30.7 10.5 -16 11 4 24 11.6 -4 15 -4 34.7 9.3 -11 -4 -4 39 8.6 15 -11 -4 23.7 12.4 11 4 4 28.7 9.7 -15 11 4 19.7 11.4 4 -15 4 32.4 9.5 -15 11 4 34.4 11.7 14 -11 -4 171.88 20.1 -3 14 -4 159.08 15.2 -11 -3 -4 195.08 15.4 -14 11 4 165.78 19.1 11 3 4 189.88 16.3 3 -14 4 193.48 17.3 -14 11 4 188.08 19.6 -11 -2 -4 246.88 17.6 13 -11 -4 329.87 31.7 -2 13 -4 246.68 18.5 -13 11 4 352.86 27.2 11 2 4 229.78 18.6 2 -13 4 243.88 19.9 12 -11 -4 49.2 11.9 -1 12 -4 66.89 10.5 -11 -1 -4 57.19 9 11 1 4 61.69 10.2 1 -12 4 52.39 11.7 -11 0 -4 8 5.7 11 -11 -4 2.3 9.1 0 11 -4 20.3 8.2 11 0 4 6.4 6.1 0 -11 4 6.7 7.4 0 -11 4 11.6 7.1 -11 11 4 10.8 9.2 1 10 -4 131.39 14.5 -11 1 -4 147.79 12.3 10 -11 -4 186.28 20.7 -10 11 4 143.19 16.1 11 -1 4 146.49 13.4 -1 -10 4 163.08 17 -1 -10 4 157.18 16.1 2 9 -4 150.38 14.5 9 -11 -4 135.39 16.7 -11 2 -4 130.89 11.1 -2 -9 4 178.68 18.2 -2 -9 4 157.28 16.2 -9 11 4 145.89 17.1 11 -2 4 145.69 12.8 8 -11 -4 115.19 13.6 3 8 -4 153.88 15.1 -11 3 -4 142.19 10.3 -3 -8 4 131.69 15.2 -8 11 4 145.89 16.7 11 -3 4 139.09 12.4 -3 -8 4 133.59 15.4 4 7 -4 264.87 19.1 -4 -7 4 212.18 18.6 -7 11 4 211.28 19.4 11 -4 4 225.88 15.3 -4 -7 4 219.68 19 6 -11 -4 96.19 12.8 5 6 -4 92.59 12.3 -5 -6 4 74.99 12 11 -5 4 109.29 10.6 -6 11 4 75.49 11.4 -5 -6 4 120.49 14.5 5 -11 -4 378.06 25.1 6 5 -4 351.06 23.8 -5 11 4 341.07 24.2 11 -6 4 349.77 20.4 -6 -5 4 350.06 24.8 7 4 -4 5.7 6.8 4 -11 -4 6.6 8 11 -7 4 15.8 6.3 -7 -4 4 21.2 8.8 -4 11 4 12.7 7.1 -7 -4 4 15 8.8 3 -11 -4 19.1 8.1 -8 -3 4 22.6 9.2 11 -8 4 22.4 6.2 -3 11 4 21.2 8.9 11 -8 4 20.6 5.8 2 -11 -4 243.08 20.3 -9 -2 4 371.66 30.5 11 -9 4 227.68 15.8 -9 -2 4 248.08 21.1 11 -9 4 238.48 15.6 -2 11 4 289.47 23.8 1 -11 -4 236.78 20.6 -10 -1 4 331.27 29.8 -10 -1 4 332.87 26.8 11 -10 4 242.08 15.9 -1 11 4 236.68 20.5 11 -10 4 237.08 15.8 0 -11 -4 9.7 7.9 -11 0 4 6.8 8.2 11 -11 4 8.5 6 -11 0 4 -10.2 7.6 11 -11 4 10.4 5.8 0 11 4 13.6 8.4 -1 -11 -4 299.67 22.8 11 -12 4 307.27 18.5 11 -12 4 290.57 18.4 -12 1 4 338.87 24.1 1 11 4 295.37 22.7 -2 -11 -4 274.27 21.3 -13 2 4 228.68 21.9 -13 2 4 263.07 22.4 11 -13 4 244.58 16.5 11 -13 4 266.67 16.6 2 11 4 236.28 20.6 -3 -11 -4 222.28 19.6 -14 3 4 185.38 20 -14 3 4 200.68 20.4 11 -14 4 202.48 15 3 11 4 206.68 19.3 11 -14 4 189.18 15.1 15 -4 -4 46.4 11.2 -4 -11 -4 66.79 11.5 -15 4 4 103.89 14.9 11 -15 4 104.89 11.3 4 11 4 109.59 15.3 -15 4 4 74.09 13.6 -5 -11 -4 -2.8 7.1 16 -5 -4 1.9 10.6 11 -16 4 18.8 7.6 5 11 4 26.1 8.6 -16 5 4 17.5 13.9 -16 5 4 1.7 9.6 -6 -11 -4 70.19 13.8 17 -6 -4 95.29 19.3 -17 6 4 42.2 12.7 -17 6 4 49.8 12.7 11 -17 4 39.8 8.7 6 11 4 39.5 11.6 18 -7 -4 154.58 20.8 -18 7 4 149.29 19.1 11 -18 4 145.99 15.1 -18 7 4 192.68 21.6 7 11 4 183.88 20.4 19 -8 -4 97.39 15.9 -19 8 4 115.59 17.2 11 -19 4 92.59 12.4 8 11 4 102.29 15.4 -19 8 4 174.88 29.4 20 -9 -4 22.7 12.6 -20 9 4 18 11.2 -20 9 4 8.2 10.5 9 11 4 8.8 10.5 11 -20 4 16.4 8.6 21 -10 -4 102.59 15 -11 21 -4 136.29 12.3 -10 -11 -4 140.39 17.6 10 11 4 105.19 15.8 11 -21 4 140.39 15.8 -21 10 4 112.09 16.8 -21 10 4 109.29 17.7 -11 22 -4 160.08 14.4 -11 -11 -4 186.08 20.1 22 -11 -4 183.48 22 11 -22 4 173.28 17.7 -22 11 4 153.38 18.9 11 11 4 213.78 21.6 -11 23 -4 95.49 12.1 23 -12 -4 90.79 17.5 -12 -11 -4 80.29 15.6 -23 12 4 88.89 16.6 12 11 4 83.79 14 11 -23 4 77.79 12.7 -10 22 -4 287.77 20.7 22 -12 -4 334.07 27.9 -12 -10 -4 340.97 25.5 12 10 4 292.47 25.4 -22 12 4 335.17 26.9 10 -22 4 291.77 23.2 -22 12 4 330.07 28.3 21 -12 -4 13.1 11.2 -12 -9 -4 37.4 12 -9 21 -4 38.3 9.5 -21 12 4 47.2 14.1 -21 12 4 41.7 13.9 9 -21 4 17.7 9.9 12 9 4 47.3 12.4 -12 -8 -4 9.8 8.2 20 -12 -4 2.3 10.5 -8 20 -4 20.2 8.1 -20 12 4 14.5 11.2 -20 12 4 2.6 10.7 8 -20 4 12.8 10 12 8 4 4.5 9.5 -7 19 -4 8.9 7.3 19 -12 -4 -4.6 9.8 -12 -7 -4 15.3 9.1 -19 12 4 8.3 11 12 7 4 -1 8.9 -19 12 4 29 10.2 7 -19 4 3.6 9.3 18 -12 -4 51.59 13 -12 -6 -4 45 10 6 -18 4 33.1 9.4 -18 12 4 70.39 14.9 -18 12 4 22.1 10.8 12 6 4 16 9.8 17 -12 -4 24.4 11.1 -12 -5 -4 37.3 9.2 -5 17 -4 29.7 8.6 -17 12 4 11.6 10.3 12 5 4 12.5 8.8 5 -17 4 33.4 10.1 -17 12 4 52.69 16.6 16 -12 -4 46 12.1 -12 -4 -4 79.99 11.6 -4 16 -4 99.09 13.2 -16 12 4 87.49 14.9 12 4 4 77.19 12.5 -16 12 4 89.89 15 4 -16 4 68.39 11.5 -3 15 -4 31.7 9 -12 -3 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10.4 12 -5 4 65.09 8.5 -7 12 4 109.59 21.8 -5 -7 4 68.49 11.3 6 -12 -4 79.79 12.3 -6 -6 4 65.49 11.5 12 -6 4 99.89 9.7 -6 12 4 75.49 12 -6 -6 4 54.89 10.9 5 -12 -4 173.18 18.4 7 5 -4 190.78 17.8 -7 -5 4 244.98 26.1 -7 -5 4 278.67 26.5 12 -7 4 153.68 12.9 -5 12 4 197.68 21.8 4 -12 -4 151.08 17.4 -4 12 4 141.59 15.4 -8 -4 4 160.88 17.7 -8 -4 4 175.08 17.6 12 -8 4 161.08 12.4 9 3 -4 284.47 21 3 -12 -4 264.17 21.2 -3 12 4 227.48 20.5 12 -9 4 260.27 16 -9 -3 4 277.37 33.5 -9 -3 4 247.88 21.3 12 -9 4 236.48 15.5 2 -12 -4 131.39 16.7 10 2 -4 128.99 15.7 -10 -2 4 168.88 24.7 -10 -2 4 152.08 17.6 -2 12 4 150.48 17.8 12 -10 4 95.79 10.7 12 -10 4 108.49 10.3 1 -12 -4 49 10.1 12 -11 4 55.19 7.8 -11 -1 4 63.39 13.3 -11 -1 4 57.59 11.6 12 -11 4 61.99 7.8 -1 12 4 46.2 11.3 0 -12 -4 152.08 17.6 -12 0 4 238.48 25 12 -12 4 133.69 12 12 -12 4 139.49 12.1 0 12 4 157.58 17.5 -12 0 4 179.08 20.2 -1 -12 -4 687.53 39.4 -13 1 4 650.23 39.9 12 -13 4 667.93 34.7 1 12 4 703.93 39.7 12 -13 4 718.63 34.8 -2 -12 -4 42 10.9 2 12 4 51.79 11.7 -14 2 4 55.29 13 12 -14 4 48.9 8 12 -14 4 55.89 8.6 -14 2 4 47.7 11.4 -3 -12 -4 23.1 10.2 -15 3 4 49.8 20.7 -15 3 4 29.1 15.3 3 12 4 18.7 10.5 12 -15 4 19.5 7.1 12 -15 4 19.9 6.6 -4 -12 -4 20.4 11 4 12 4 27 11.6 -16 4 4 14.7 9.4 12 -16 4 18.8 7 -16 4 4 20.8 11.2 17 -5 -4 101.89 14.6 -5 -12 -4 157.58 17.4 5 12 4 184.78 20.6 12 -17 4 146.79 13.8 -17 5 4 141.39 17.4 -17 5 4 140.69 16.7 -6 -12 -4 47.6 12.9 18 -6 -4 90.79 24.1 -18 6 4 48.9 13.6 -18 6 4 46.2 12.1 12 -18 4 55.79 9.7 6 12 4 62.59 13.8 19 -7 -4 206.88 22.9 -7 -12 -4 221.18 20.6 7 12 4 207.98 21.4 -19 7 4 234.88 22.9 -19 7 4 204.78 22.4 12 -19 4 189.88 17.4 -8 -12 -4 102.09 25.8 20 -8 -4 128.89 19.2 -20 8 4 94.59 17.6 -20 8 4 64.59 13.6 12 -20 4 66.69 11.2 8 12 4 87.59 15.2 21 -9 -4 119.19 28.7 12 -21 4 93.19 12.8 -21 9 4 72.69 13.9 9 12 4 80.09 16.2 -21 9 4 60.99 15.6 -12 22 -4 18.2 7.2 22 -10 -4 20.1 13.8 10 12 4 22.3 12.5 -22 10 4 17.5 10.8 12 -22 4 33.9 10.3 -22 10 4 9.1 11.9 -12 23 -4 109.29 12 -11 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18.1 -6 19 -4 92.09 12.8 -13 -6 -4 80.69 13.4 19 -13 -4 59.19 14.4 6 -19 4 87.09 15.2 -19 13 4 72.69 15.9 13 6 4 59.79 12.2 -19 13 4 44.7 11.5 -13 -5 -4 54.89 11.2 18 -13 -4 29.2 12.4 -18 13 4 61.79 14.8 5 -18 4 36.7 9.7 13 5 4 49.2 11.9 -18 13 4 33.6 11.2 -4 17 -4 42 10 -13 -4 -4 41.6 9.2 17 -13 -4 24.8 11.3 -17 13 4 10.6 9.8 4 -17 4 34 9.7 -17 13 4 37.6 12 13 4 4 27 9.4 16 -13 -4 32.1 11.3 -13 -3 -4 66.29 10.8 -3 16 -4 62.59 10.9 -16 13 4 85.49 19.4 -16 13 4 32.1 10.4 3 -16 4 52.59 11.2 13 3 4 97.99 13.2 15 -13 -4 65.99 13.2 -13 -2 -4 70.89 10.5 -2 15 -4 81.49 12.3 2 -15 4 58.79 11.2 -15 13 4 111.39 24.2 13 2 4 56.89 10.2 14 -13 -4 346.57 28.3 -13 -1 -4 403.26 23.1 -1 14 -4 394.06 25.5 -14 13 4 418.86 28.9 1 -14 4 391.56 26.6 13 1 4 403.36 24.4 0 13 -4 378.26 24.7 13 -13 -4 356.46 27.1 -13 0 -4 350.26 21.3 0 -13 4 381.26 25.8 -13 13 4 380.46 27.4 13 0 4 384.16 23.2 1 12 -4 671.93 37.9 12 -13 -4 653.53 39.8 -13 1 -4 692.33 34.2 13 -1 4 681.73 35.8 -1 -12 4 688.03 38.7 -12 13 4 681.33 39.7 2 11 -4 274.37 21.2 11 -13 -4 327.77 27.7 -13 2 -4 289.37 16.8 13 -2 4 280.67 18.4 -2 -11 4 260.87 21.8 -2 -11 4 287.47 22.5 10 -13 -4 203.88 19.6 3 10 -4 184.98 17.2 -10 13 4 181.78 19.4 -3 -10 4 164.48 18.5 13 -3 4 191.48 14.4 -3 -10 4 204.98 18.4 4 9 -4 147.29 15.8 9 -13 -4 118.69 15.4 -4 -9 4 163.18 17.6 -9 13 4 146.19 16.6 -4 -9 4 188.98 19.9 13 -4 4 138.99 12.6 8 -13 -4 263.57 22.2 5 8 -4 275.37 20.4 -5 -8 4 223.78 20.9 13 -5 4 276.67 16.9 -5 -8 4 266.77 21 -8 13 4 265.77 21.8 6 7 -4 136.59 15.6 7 -13 -4 134.69 15.7 -7 13 4 90.49 12.6 -6 -7 4 128.89 15 -6 -7 4 148.39 16.2 13 -6 4 124.19 11.2 6 -13 -4 17.4 9.4 7 6 -4 15.6 8.4 13 -7 4 18.5 5.6 -6 13 4 24.7 9.8 -7 -6 4 28.8 9.9 -7 -6 4 33 9.6 5 -13 -4 169.98 18 8 5 -4 153.88 16.9 -8 -5 4 238.28 25.7 13 -8 4 140.39 12.1 -8 -5 4 167.68 18 -5 13 4 200.98 20.4 9 4 -4 121.59 18.6 4 -13 -4 85.59 14.2 -9 -4 4 92.29 13.7 -9 -4 4 80.79 13.4 -4 13 4 68.09 11.3 13 -9 4 64.99 8.2 13 -9 4 80.39 8.4 3 -13 -4 104.29 13.6 10 3 -4 191.78 22 13 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12 4 13.3 11.8 25 -14 -4 4.8 11.5 -14 -11 -4 14.4 10.1 -25 14 4 4.8 11.4 11 -25 4 12.8 10.5 14 11 4 19 11.5 -25 14 4 3.9 11.8 -14 -10 -4 77.69 13.8 24 -14 -4 83.19 16.8 -24 14 4 73.39 16.6 -24 14 4 89.79 17.9 10 -24 4 55.99 11.7 -14 -9 -4 34.3 12 23 -14 -4 57.99 19.2 14 9 4 21 10.5 9 -23 4 29.6 10.5 -23 14 4 43.8 13.9 -23 14 4 44.7 15.3 -8 22 -4 51.49 11 -14 -8 -4 40.3 11.3 22 -14 -4 33.1 15.3 -22 14 4 36.2 14 8 -22 4 36.5 11.5 14 8 4 31.7 11.7 -22 14 4 24.2 12.8 -7 21 -4 17.4 8.5 21 -14 -4 16.5 13.6 -14 -7 -4 18.7 9.9 -21 14 4 4.5 10.7 -21 14 4 6.7 11.8 14 7 4 14.2 10.3 7 -21 4 9.1 9.3 -6 20 -4 84.89 13.2 20 -14 -4 121.39 20.1 -14 -6 -4 86.49 13.7 -20 14 4 108.99 18.1 6 -20 4 95.29 15 -20 14 4 75.99 15 14 6 4 103.29 15.5 -14 -5 -4 -3.5 7.7 -5 19 -4 13.6 8.6 19 -14 -4 18.4 13.5 -19 14 4 18.2 11.8 14 5 4 28.5 10.1 -19 14 4 1.8 9.3 5 -19 4 17.4 10.8 18 -14 -4 20.4 15.4 -4 18 -4 37.6 16.2 -14 -4 -4 25.9 8.9 4 -18 4 42.8 12.1 -18 14 4 55.09 14.2 14 4 4 32.7 10.6 -18 14 4 31 11.3 -3 17 -4 162.68 16.9 17 -14 -4 213.98 22.9 -14 -3 -4 156.48 16.1 -17 14 4 191.48 21.5 -17 14 4 215.48 22.6 14 3 4 172.38 17.9 3 -17 4 201.18 19.7 -2 16 -4 298.27 21.9 -14 -2 -4 277.47 19.7 16 -14 -4 332.67 26.5 2 -16 4 280.47 22.8 -16 14 4 291.87 25.1 14 2 4 281.77 21.4 -14 -1 -4 155.68 14.1 15 -14 -4 138.09 17.1 -1 15 -4 158.58 16.5 -15 14 4 191.78 20.2 1 -15 4 180.58 19.3 14 1 4 150.48 16.1 -14 0 -4 89.49 10.2 0 14 -4 62.09 11.9 14 0 4 81.09 11.7 -14 14 4 70.59 16.9 0 -14 4 70.19 11.2 -14 1 -4 123.59 11.6 13 -14 -4 111.29 15.6 1 13 -4 145.29 15.5 14 -1 4 127.39 13.2 -13 14 4 168.38 20.4 -1 -13 4 116.99 14.3 12 -14 -4 57.69 12.8 2 12 -4 60.09 11.3 -2 -12 4 41.8 9.3 14 -2 4 43.6 8.7 -12 14 4 41.9 12.6 -14 3 -4 191.48 12 11 -14 -4 186.68 20 3 11 -4 198.88 18.2 -3 -11 4 197.68 19.3 14 -3 4 183.28 14.6 -11 14 4 302.37 30.5 -3 -11 4 201.88 19.9 4 10 -4 377.26 24.8 10 -14 -4 419.36 30.7 -4 -10 4 318.27 24.8 14 -4 4 339.77 20.7 -4 -10 4 347.27 25.7 5 9 -4 36.7 10.1 9 -14 -4 56.09 15.1 -9 14 4 46 10.5 14 -5 4 41.5 7.5 -5 -9 4 34.6 10.8 -5 -9 4 51.69 11.5 8 -14 -4 62.99 13.6 6 8 -4 29 8.5 -6 -8 4 46.8 10.8 14 -6 4 52.19 7.5 -8 14 4 48.1 19.2 -6 -8 4 37.5 10.9 7 -14 -4 79.79 13.6 7 7 -4 47.1 10.2 -7 -7 4 45.2 11.4 -7 14 4 46.2 11.3 14 -7 4 66.09 7.9 -7 -7 4 64.69 12 6 -14 -4 252.17 29.2 8 6 -4 154.08 17.2 14 -8 4 139.19 12 -8 -6 4 185.28 22.8 -8 -6 4 199.68 20.7 -6 14 4 258.27 29.3 5 -14 -4 72.89 13.6 9 5 -4 121.69 23.9 -9 -5 4 42.5 10.1 14 -9 4 82.89 8.5 -5 14 4 62.49 12.5 -9 -5 4 78.69 14.1 4 -14 -4 23.3 10.5 10 4 -4 13.5 8.4 -10 -4 4 18.1 10.1 -4 14 4 39.2 12 14 -10 4 27.2 6.2 14 -10 4 18.2 5.3 -10 -4 4 18 9.4 3 -14 -4 210.78 20.6 11 3 -4 294.67 25.1 -3 14 4 187.68 19.4 -11 -3 4 203.48 23.8 -11 -3 4 208.08 20.6 14 -11 4 176.38 12.7 14 -11 4 187.38 13.3 2 -14 -4 38.1 10.7 12 2 -4 66.39 13.8 -12 -2 4 66.99 12.6 -2 14 4 87.99 17 14 -12 4 60.99 8 14 -12 4 57.09 7.4 -12 -2 4 52.29 11.5 1 -14 -4 397.56 28.4 14 -13 4 401.86 22 -13 -1 4 411.36 29 14 -13 4 419.26 22.5 -13 -1 4 408.46 29.3 0 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171.88 16.9 9 14 4 164.18 20.2 -23 9 4 179.68 22.1 24 -10 -4 57.29 14.5 -10 -14 -4 83.99 16.2 -24 10 4 76.39 15.9 10 14 4 68.69 16.2 -24 10 4 72.09 17.8 14 -24 4 52.79 11.6 25 -11 -4 12.3 13.3 -25 11 4 23.4 13.3 -25 11 4 45.1 15.9 11 14 4 31.1 12.2 14 -25 4 27.9 10.1 26 -12 -4 9.2 13.1 -26 12 4 23.1 13.5 -26 12 4 -22.4 10.8 14 -26 4 4.7 10.8 12 14 4 21.4 13 27 -13 -4 21.9 13.1 -13 -14 -4 24.3 9.8 -27 13 4 33.5 10.9 13 14 4 31.9 12.5 14 -27 4 38.8 11.1 -14 -14 -4 13 11.4 28 -14 -4 15.3 14.1 14 14 4 33.6 11.7 14 -28 4 23.9 10.7 -28 14 4 32.3 15.1 29 -15 -4 10.7 12.6 -15 -14 -4 20.8 12.7 15 14 4 -0.6 11 -29 15 4 9.6 11.1 14 -29 4 -5.1 9.8 -15 -13 -4 69.99 15.1 28 -15 -4 20.8 14.4 15 13 4 47 13.7 13 -28 4 43 12.7 -28 15 4 35.6 14.7 -15 -12 -4 2.2 9.6 27 -15 -4 -0.3 12.2 15 12 4 0.8 9.8 -27 15 4 0.5 11 12 -27 4 -7.7 8.8 -15 -11 -4 74.19 13.9 26 -15 -4 31 14.5 -26 15 4 54.69 16.6 11 -26 4 60.29 18.2 15 11 4 70.89 15.5 -15 -10 -4 41.5 11.5 25 -15 -4 28.7 14.2 10 -25 4 20.4 9.8 -25 15 4 32.3 15.2 15 10 4 37.4 13.4 -25 15 4 18.6 11.9 24 -15 -4 76.69 16 -15 -9 -4 100.99 15.3 -24 15 4 85.09 17.7 15 9 4 94.19 16.9 9 -24 4 109.29 17.2 -24 15 4 127.29 20.3 23 -15 -4 20.7 11.7 -15 -8 -4 8.5 8.7 15 8 4 26 10.4 -23 15 4 8.4 11 -23 15 4 19.5 13.5 8 -23 4 5.3 9.1 22 -15 -4 203.58 24.4 -15 -7 -4 262.77 21.3 -7 22 -4 250.87 19.9 15 7 4 237.38 21.9 7 -22 4 261.57 21.9 -22 15 4 248.38 25.6 -22 15 4 263.07 30.3 21 -15 -4 110.59 16.9 -15 -6 -4 116.39 15.2 -6 21 -4 118.19 14.4 6 -21 4 95.59 15.6 15 6 4 116.19 15.8 -21 15 4 133.39 20 -21 15 4 89.39 15.8 -15 -5 -4 279.37 21.2 20 -15 -4 254.27 26.2 -5 20 -4 282.87 21.4 -20 15 4 251.17 25.4 -20 15 4 237.28 25.7 5 -20 4 280.97 24 15 5 4 275.87 22.5 -15 -4 -4 14.7 8.6 -4 19 -4 38.5 10.6 19 -15 -4 -4.9 10.4 -19 15 4 -5.1 9.6 -19 15 4 32.9 13.1 4 -19 4 24 10.5 15 4 4 9.8 8.6 -3 18 -4 218.68 20.3 18 -15 -4 231.98 23.7 -15 -3 -4 178.08 17.2 15 3 4 194.88 19.1 -18 15 4 267.17 24.2 3 -18 4 243.58 21.5 -18 15 4 290.67 32.3 17 -15 -4 437.86 32.5 -15 -2 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11.3 -2 -8 5 95.69 15.3 -2 -8 5 78.29 13.6 -8 10 5 83.39 14.7 10 -2 5 95.59 12.3 7 -10 -5 373.86 29.2 -10 3 -5 381.26 22.8 10 -3 5 397.06 24.8 -3 -7 5 396.16 28.3 -3 -7 5 388.56 28.2 -7 10 5 397.06 29 6 -10 -5 137.79 17.8 -4 -6 5 120.29 15.1 10 -4 5 140.49 15.1 -6 10 5 242.38 31.1 -4 -6 5 134.29 16.7 5 -10 -5 127.59 18.7 -5 10 5 98.19 15.6 10 -5 5 112.29 13.2 -5 -5 5 139.99 17.4 -5 -5 5 101.39 14.9 4 -10 -5 215.88 21 10 -6 5 196.68 17.7 -4 10 5 180.48 21.3 -6 -4 5 200.58 21.3 -6 -4 5 222.38 21.8 3 -10 -5 110.89 13.7 10 -7 5 119.39 13.9 -3 10 5 90.39 13.7 10 -7 5 89.99 12.2 -7 -3 5 112.89 16.5 -7 -3 5 121.79 16.6 2 -10 -5 155.38 17.9 -2 10 5 182.38 21 10 -8 5 136.99 16 -8 -2 5 180.68 20.8 -8 -2 5 154.48 18.6 10 -8 5 166.98 15.3 1 -10 -5 318.27 25.8 10 -9 5 342.77 22.7 10 -9 5 315.87 22 -9 -1 5 323.87 27.2 -1 10 5 388.66 27.5 0 -10 -5 430.66 29.9 -10 0 5 443.06 31.5 10 -10 5 418.76 26 10 -10 5 429.16 26.4 0 10 5 431.96 30.6 -1 -10 -5 55.89 12.3 -11 1 5 49.9 12.2 1 10 5 38.2 12 -11 1 5 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12.2 9 10 5 41.9 13.1 -10 -10 -5 51.89 13.2 20 -10 -5 22.3 13.3 -20 10 5 47.2 13.7 10 -20 5 50.79 12.4 -20 10 5 50.99 26.4 10 10 5 70.19 14.5 -11 -10 -5 16.8 10.4 21 -11 -5 9.3 12.3 -21 11 5 4.3 11.2 10 -21 5 -0.8 7.9 -21 11 5 8.2 12.8 -11 -9 -5 61.39 13.3 20 -11 -5 42.2 16.9 11 9 5 65.89 13.8 -20 11 5 62.49 16.7 9 -20 5 59.49 12.6 -20 11 5 115.29 25.2 -11 -8 -5 61.99 13.6 19 -11 -5 60.99 15 -19 11 5 73.79 16.3 11 8 5 65.89 14.2 -19 11 5 81.79 23.1 8 -19 5 75.89 14.2 18 -11 -5 46.7 15.1 -11 -7 -5 40.5 11.6 7 -18 5 61.09 12.8 -18 11 5 33.5 13.8 -18 11 5 58.89 15.8 11 7 5 48.7 12.3 7 -18 5 36.4 11.4 -11 -6 -5 40.4 11.4 17 -11 -5 30.3 20.2 11 6 5 21.7 9.8 -17 11 5 21.4 12.1 6 -17 5 54.49 13.5 -17 11 5 32.7 13.6 6 -17 5 22.9 11.9 -11 -5 -5 123.19 15.3 16 -11 -5 72.19 14.4 -16 11 5 112.79 18 -16 11 5 156.18 23.1 5 -16 5 131.99 17.1 11 5 5 198.28 20.6 5 -16 5 159.48 18.4 -11 -4 -5 31.4 10.4 4 -15 5 15.7 10.4 -15 11 5 39.6 13.8 11 4 5 25.2 11.2 4 -15 5 19.1 12 14 -11 -5 51.19 13.8 -11 -3 -5 99.09 13.2 3 -14 5 65.69 13.4 -14 11 5 76.79 17 -14 11 5 81.59 20.5 3 -14 5 56.09 13.2 13 -11 -5 170.58 21.4 -11 -2 -5 190.68 17.6 -13 11 5 185.18 22 2 -13 5 177.58 20.3 2 -13 5 187.68 20.1 -13 11 5 208.48 23 11 2 5 202.68 19.1 -11 -1 -5 27.7 9.2 12 -11 -5 21.5 16.6 -12 11 5 20.6 12.5 1 -12 5 26.7 10.9 1 -12 5 42.2 12.1 11 1 5 30.1 10.6 11 -11 -5 298.97 35.6 -11 0 -5 186.58 16.4 0 -11 5 188.08 20.2 11 0 5 152.08 17.6 0 -11 5 199.08 24.3 -11 1 -5 56.59 9.6 10 -11 -5 84.09 16 11 -1 5 59.69 11.7 -1 -10 5 57.69 13.4 -10 11 5 63.29 13.6 -1 -10 5 68.29 13.7 9 -11 -5 74.39 14 -11 2 -5 91.09 10.7 11 -2 5 83.89 12.7 -9 11 5 51.19 13.8 -2 -9 5 73.79 13.4 -2 -9 5 75.39 14.1 -11 3 -5 538.35 29 8 -11 -5 560.84 35.8 -3 -8 5 569.74 35 -3 -8 5 513.45 34 11 -3 5 557.24 31.2 -8 11 5 495.75 35.1 7 -11 -5 38.5 12.7 11 -4 5 7.4 7.9 -4 -7 5 27.1 10.8 -7 11 5 39.8 21.7 -4 -7 5 17.8 9.8 6 -11 -5 38.2 11.3 -5 -6 5 60.29 13.6 11 -5 5 62.19 10.9 -6 11 5 74.29 15.1 -5 -6 5 52.09 12.8 5 -11 -5 73.59 14.2 -5 11 5 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14.6 13.6 -13 11 8 35.9 20.8 12 -11 -8 -6.4 13.6 -11 -1 -8 19.4 9.5 -12 11 8 14.4 17.2 1 -12 8 21.2 14.2 -12 11 8 14 22.5 11 1 8 16.7 13 1 -12 8 0 12.2 11 -11 -8 -10.7 13.1 0 -11 8 21 15.2 -11 11 8 33.9 18.8 11 0 8 4.6 13.3 -11 11 8 18.6 17.7 10 -11 -8 -1.3 13 -1 -10 8 2.6 13.2 -1 -10 8 17.9 14.8 -10 11 8 45.5 19.3 -10 11 8 37 18.5 11 -1 8 12.1 12.1 9 -11 -8 23.1 15.1 -9 11 8 3.9 16 -2 -9 8 11.8 14.3 -9 11 8 35.6 16.7 11 -2 8 27.9 15.3 -2 -9 8 9.7 14.3 8 -11 -8 -29.3 10.3 -8 11 8 -7.5 14.4 11 -3 8 28.1 13.5 -3 -8 8 -4.8 12.2 11 -3 8 12.9 11.1 -3 -8 8 13.6 15.9 -8 11 8 13.6 16 7 -11 -8 7.1 13 -4 -7 8 -2.2 14.6 -7 11 8 5.2 15.5 11 -4 8 8.1 11.7 11 -4 8 21.5 12.6 -4 -7 8 9.8 14 -7 11 8 33 18.2 6 -11 -8 48 16.1 11 -5 8 83.99 16.1 11 -5 8 98.19 19.1 -5 -6 8 93.89 21.2 -6 11 8 43.9 18.6 -5 -6 8 98.59 18.9 5 -11 -8 14.3 11.5 -6 -5 8 11.3 15.1 11 -6 8 7.5 11.6 11 -6 8 18.9 13 -6 -5 8 25.1 17.3 -5 11 8 -3.6 14.6 4 -11 -8 25.7 14.4 -7 -4 8 33.1 17.1 -4 11 8 1.7 16.1 11 -7 8 26.6 13.4 11 -7 8 8.6 11.3 -7 -4 8 16.2 15.9 3 -11 -8 -6.9 12.7 -8 -3 8 31.6 14.4 11 -8 8 19.3 11.4 -8 -3 8 51.29 18.5 11 -8 8 11.4 12 -3 11 8 53.19 17.2 2 -11 -8 8.7 13 -9 -2 8 -10.6 13.3 11 -9 8 -4.4 10 -2 11 8 15.3 15.7 -9 -2 8 3 15.1 11 -9 8 27.4 12.4 -10 -1 8 17.4 16.3 -10 -1 8 12.8 20.6 11 -10 8 19.6 11.9 -1 11 8 25.7 16.2 11 -10 8 22.4 13.2 0 -11 -8 -12.1 9.7 0 11 8 38.2 16.8 -11 0 8 14.9 16 11 -11 8 -3 11.4 -11 0 8 17.2 19.1 11 -11 8 0.7 12 -1 -11 -8 28.1 14.6 -12 1 8 -25.3 14.4 11 -12 8 -10.8 11.9 -12 1 8 6 15.9 1 11 8 27.6 17.2 11 -12 8 31.2 14.3 -2 -11 -8 29.8 15 11 -13 8 31.9 13.2 2 11 8 5 16.5 11 -13 8 28 15.3 -13 2 8 25.4 17.6 -13 2 8 22.7 18.3 -3 -11 -8 19.4 13.6 11 -14 8 16 12.4 -14 3 8 -7.3 17.2 -14 3 8 28.6 18.4 11 -14 8 5.4 16 3 11 8 11.8 16 13 -12 -8 25.5 14.5 -13 12 8 -1.4 14.9 -13 12 8 -4.7 24.1 1 -13 8 16 14.6 1 -13 8 -1.9 12.2 12 1 8 22.6 14.2 12 -12 -8 19.3 14 0 -12 8 5.6 12.4 -12 12 8 13 18.5 -12 12 8 3.1 15.6 12 0 8 14.2 12.5 11 -12 -8 30.1 14.2 -11 12 8 -5.5 15 12 -1 8 20.8 13.8 -1 -11 8 24.9 15.3 -1 -11 8 39.7 16.9 -11 12 8 -3.9 16.6 10 -12 -8 16.8 12.8 -10 12 8 25.3 18.3 12 -2 8 11.7 11.7 -10 12 8 13.4 19.3 -2 -10 8 19.1 16.1 -2 -10 8 1 13 9 -12 -8 7.9 11.3 -3 -9 8 4.4 16.3 12 -3 8 44.4 15.4 -9 12 8 -9.2 15.8 -3 -9 8 8.5 16.8 12 -3 8 25.8 13.5 -9 12 8 22.4 17.9 8 -12 -8 40.2 13.8 12 -4 8 30 13.1 -8 12 8 46.8 20 -8 12 8 33.9 17.9 -4 -8 8 43.4 15.9 -4 -8 8 14.8 15 12 -4 8 24.6 12.7 7 -12 -8 48.5 16.2 -5 -7 8 49.7 19.3 -5 -7 8 88.59 19.5 -7 12 8 47.6 18.4 12 -5 8 75.99 15.9 12 -5 8 87.79 16 6 -12 -8 22.3 13.6 -6 12 8 -28.7 17.6 -6 -6 8 14.1 16.3 12 -6 8 12.5 11.5 -6 -6 8 18.5 16.4 12 -6 8 37.3 13.4 5 -12 -8 8.5 15.5 12 -7 8 3.7 11.2 -7 -5 8 3.3 14.3 12 -7 8 28.9 14.1 -5 12 8 10.1 16 -7 -5 8 2.7 14.8 4 -12 -8 10.9 13.1 12 -8 8 29 13 -8 -4 8 7.8 16.5 -8 -4 8 21.4 17.1 -4 12 8 -2.1 14.5 12 -8 8 18.3 10.9 3 -12 -8 4.8 12.2 -9 -3 8 17.6 17.2 12 -9 8 9 10.6 -9 -3 8 -11.9 14.6 -3 12 8 24.1 14.2 12 -9 8 20.6 14.6 2 -12 -8 18.8 14.8 -2 12 8 53.39 19.9 -10 -2 8 18.1 19 -10 -2 8 31.1 17 12 -10 8 36.2 13.8 -1 12 8 9.3 16.6 12 -11 8 -7.6 12.6 12 -11 8 4.2 11.6 -11 -1 8 0.7 11.8 -11 -1 8 -2.6 14 -12 0 8 15.2 14.3 -12 0 8 13.3 17 12 -12 8 20.7 12.8 0 12 8 24.3 16.8 12 -12 8 4.2 11.7 -1 -12 -8 22.5 14.2 -13 1 8 8.4 15.9 12 -13 8 -0.3 11.7 12 -13 8 3.1 11.3 1 12 8 34.4 17.3 -13 1 8 20.6 15 12 -13 -8 18.6 14.3 -1 -12 8 28.8 12.9 -1 -12 8 5.4 16.2 -12 13 8 21.9 16.4 13 -1 8 23.7 13.7 -12 13 8 21.8 18.5 11 -13 -8 15.2 15.2 -2 -11 8 20.9 14.8 -11 13 8 54.59 26.8 -11 13 8 23.9 18.8 -2 -11 8 32.7 16.2 13 -2 8 19.4 13.9 10 -13 -8 6 14.6 -10 13 8 10.3 16.6 -10 13 8 10.2 17 13 -3 8 35 14 -3 -10 8 29.6 16.9 -3 -10 8 8.9 13.6 9 -13 -8 27 15.1 13 -4 8 18.8 12.5 -4 -9 8 8.7 14.5 -9 13 8 4.8 16.7 -9 13 8 12.9 17.8 -4 -9 8 26.1 17.7 13 -4 8 -3.3 12.2 8 -13 -8 58.99 18.1 -5 -8 8 43.5 19.7 -8 13 8 66.89 19.9 -5 -8 8 62.89 21.6 13 -5 8 86.39 16 13 -5 8 67.39 16.4 7 -13 -8 49.9 18.1 -7 13 8 70.59 21.3 -6 -7 8 70.19 20.3 -6 -7 8 16.8 15.9 13 -6 8 48.4 16 13 -6 8 50.19 14 6 -13 -8 27.4 13.4 -7 -6 8 20.4 15.1 -7 -6 8 27.1 16.9 13 -7 8 36.7 12.8 -6 13 8 40.2 19.3 5 -13 -8 4.6 14.1 13 -8 8 7.8 11.9 13 -8 8 12.6 10.5 -8 -5 8 33.4 17.2 -8 -5 8 24.8 15.7 4 -13 -8 14.2 14.3 -9 -4 8 -4.3 15.2 13 -9 8 -6.3 10.2 13 -9 8 -0.4 10.4 -9 -4 8 -12.1 16.5 -4 13 8 1.9 14.4 3 -13 -8 6.9 13.4 -10 -3 8 19.2 20.7 -10 -3 8 47.9 19 13 -10 8 33.2 12.9 -3 13 8 27.8 15.9 13 -10 8 32.8 13.6 2 -13 -8 11.4 14.9 -11 -2 8 1.6 15.7 13 -11 8 24.8 13.7 -11 -2 8 35.2 18.9 13 -11 8 23 12.1 -2 13 8 41.9 18 1 -13 -8 2.9 11.4 -12 -1 8 1.7 15.4 13 -12 8 7 12.2 -12 -1 8 -6.4 15.8 -1 13 8 24.8 17.4 13 -12 8 8.7 12 11 -14 -8 9.8 14 -3 -11 8 2.2 15.3 -11 14 8 24.9 17 -11 14 8 11.8 15.1 14 -3 8 7 11.8 -3 -11 8 32.4 15.7 10 -14 -8 -21.6 12.7 -10 14 8 -12.5 14.2 14 -4 8 -0.3 13.1 14 -4 8 20.1 10.6 -10 14 8 23.1 17.4 -4 -10 8 22.3 17.4 -4 -10 8 -11.5 11.6 9 -14 -8 -17.8 13.6 -5 -9 8 -7 13.2 14 -5 8 10.3 20 -5 -9 8 -13 14.4 14 -5 8 9 11.6 -9 14 8 39 19.8 8 -14 -8 11.7 14.7 -6 -8 8 14.1 14.8 -6 -8 8 7 15.2 14 -6 8 32.7 12.6 14 -6 8 20.7 12.2 -8 14 8 27.1 16.9 7 -14 -8 21.4 14.8 14 -7 8 11.2 12.4 14 -7 8 29 12.4 -7 14 8 22.4 18.1 -7 -7 8 4.9 16.7 -7 -7 8 2 13.4 6 -14 -8 39.1 15.7 14 -8 8 24.4 12.4 14 -8 8 47.9 14.9 -6 14 8 62.99 19 -8 -6 8 63.29 18.7 -8 -6 8 34.3 18.3 5 -14 -8 28.5 15.1 14 -9 8 6.1 11.8 -9 -5 8 -11.9 17 -9 -5 8 24.8 17.4 -5 14 8 11.2 13.9 14 -9 8 4 11 4 -14 -8 -2.3 14 -10 -4 8 -0.9 12 14 -10 8 29.2 12.9 14 -10 8 2.9 11 -10 -4 8 -11.8 15.7 3 -14 -8 8.2 14.2 -11 -3 8 42.9 18.8 -3 14 8 6.9 16.4 14 -11 8 4.9 10.2 14 -11 8 6.7 11.6 -11 -3 8 18.6 18.1 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 O1 H1 109.5 . . ? C26 O2 C27 115.5(16) . . ? C2 C1 C6 107.36(17) . . ? C2 C1 C19 107.72(18) . . ? C18 C1 C2 112.01(18) . . ? C18 C1 C6 114.39(18) . . ? C18 C1 C19 108.0(2) . . ? C19 C1 C6 107.07(17) . . ? O1 C2 C1 111.61(18) . . ? O1 C2 H2 108.4 . . ? O1 C2 C3 106.96(16) . . ? C1 C2 H2 108.4 . . ? C3 C2 C1 112.92(18) . . ? C3 C2 H2 108.4 . . ? C2 C3 H3A 109.3 . . ? C2 C3 H3B 109.3 . . ? C2 C3 C4 111.49(16) . . ? H3A C3 H3B 108.0 . . ? C4 C3 H3A 109.3 . . ? C4 C3 H3B 109.3 . . ? C3 C4 H4A 108.9 . . ? C3 C4 H4B 108.9 . . ? C3 C4 C5 113.25(19) . . ? H4A C4 H4B 107.7 . . ? C5 C4 H4A 108.9 . . ? C5 C4 H4B 108.9 . . ? C4 C5 C6 108.39(15) . . ? C10 C5 C4 111.84(18) . . ? C10 C5 C6 109.16(16) . . ? C20 C5 C4 107.74(17) . . ? C20 C5 C6 113.95(18) . . ? C20 C5 C10 105.81(16) . . ? C1 C6 H6 104.6 . . ? C5 C6 C1 117.24(15) . . ? C5 C6 H6 104.6 . . ? C7 C6 C1 114.78(18) . . ? C7 C6 C5 109.65(15) . . ? C7 C6 H6 104.6 . . ? C6 C7 H7A 109.7 . . ? C6 C7 H7B 109.7 . . ? C6 C7 C8 109.72(19) . . ? H7A C7 H7B 108.2 . . ? C8 C7 H7A 109.7 . . ? C8 C7 H7B 109.7 . . ? C7 C8 H8A 109.2 . . ? C7 C8 H8B 109.2 . . ? C7 C8 C9 112.24(19) . . ? H8A C8 H8B 107.9 . . ? C9 C8 H8A 109.2 . . ? C9 C8 H8B 109.2 . . ? C8 C9 H9 105.8 . . ? C8 C9 C14 114.07(18) . . ? C10 C9 C8 112.80(16) . . ? C10 C9 H9 105.8 . . ? C10 C9 C14 111.70(19) . . ? C14 C9 H9 105.8 . . ? C9 C10 C5 117.04(18) . . ? C11 C10 C5 121.55(19) . . ? C11 C10 C9 121.15(19) . . ? C10 C11 H11 117.3 . . ? C10 C11 C12 125.5(2) . . ? C12 C11 H11 117.3 . . ? C11 C12 H12A 109.5 . . ? C11 C12 H12B 109.5 . . ? C11 C12 C13 110.8(2) . . ? H12A C12 H12B 108.1 . . ? C13 C12 H12A 109.5 . . ? C13 C12 H12B 109.5 . . ? C12 C13 C14 106.95(17) . . ? C12 C13 C17 118.1(2) . . ? C17 C13 C14 102.17(17) . . ? C21 C13 C12 108.57(19) . . ? C21 C13 C14 111.55(19) . . ? C21 C13 C17 109.35(18) . . ? C13 C14 C9 110.15(17) . . ? C15 C14 C9 114.8(2) . . ? C15 C14 C13 102.00(17) . . ? C22 C14 C9 109.09(18) . . ? C22 C14 C13 111.7(2) . . ? C22 C14 C15 109.0(2) . . ? C14 C15 H15A 110.9 . . ? C14 C15 H15B 110.9 . . ? C14 C15 C16 104.2(2) . . ? H15A C15 H15B 108.9 . . ? C16 C15 H15A 110.9 . . ? C16 C15 H15B 110.9 . . ? C15 C16 H16A 110.3 . . ? C15 C16 H16B 110.3 . . ? C15 C16 C17 107.05(18) . . ? H16A C16 H16B 108.6 . . ? C17 C16 H16A 110.3 . . ? C17 C16 H16B 110.3 . . ? C13 C17 C16 103.7(2) . . ? C13 C17 H17 103.2 . . ? C13 C17 H17A 108.1 . . ? C13 C17 C23 122.3(8) . . ? C13 C17 C23A 117.6(4) . . ? C16 C17 H17 103.2 . . ? C16 C17 H17A 108.1 . . ? C16 C17 C23 118.5(8) . . ? C16 C17 C23A 110.7(4) . . ? C23 C17 H17 103.2 . . ? C23A C17 H17A 108.1 . . ? C1 C18 H18A 109.5 . . ? C1 C18 H18B 109.5 . . ? C1 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C1 C19 H19A 109.5 . . ? C1 C19 H19B 109.5 . . ? C1 C19 H19C 109.5 . . ? H19A C19 H19B 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C5 C20 H20A 109.5 . . ? C5 C20 H20B 109.5 . . ? C5 C20 H20C 109.5 . . ? H20A C20 H20B 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C13 C21 H21A 109.5 . . ? C13 C21 H21B 109.5 . . ? C13 C21 H21C 109.5 . . ? H21A C21 H21B 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C14 C22 H22A 109.5 . . ? C14 C22 H22B 109.5 . . ? C14 C22 H22C 109.5 . . ? H22A C22 H22B 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? C17 C23 H23 104.7 . . ? C24 C23 C17 114.7(16) . . ? C24 C23 H23 104.7 . . ? C24 C23 C25 114.5(17) . . ? C25 C23 C17 112.1(15) . . ? C25 C23 H23 104.7 . . ? C23 C24 H24A 109.5 . . ? C23 C24 H24B 109.5 . . ? C23 C24 H24C 109.5 . . ? H24A C24 H24B 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C23 C25 H25A 108.3 . . ? C23 C25 H25B 108.3 . . ? H25A C25 H25B 107.4 . . ? C26 C25 C23 116.0(18) . . ? C26 C25 H25A 108.3 . . ? C26 C25 H25B 108.3 . . ? O2 C26 C25 110.6(18) . . ? O2 C26 H26 107.5 . . ? O2 C26 C28 113.7(16) . . ? C25 C26 H26 107.5 . . ? C25 C26 C28 109.9(17) . . ? C28 C26 H26 107.5 . . ? O2 C27 H27A 109.5 . . ? O2 C27 H27B 109.5 . . ? O2 C27 H27C 109.5 . . ? H27A C27 H27B 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? C29 C28 C26 121.0(16) . . ? C29 C28 C30 121.6(16) . . ? C30 C28 C26 115.8(15) . . ? C28 C29 H29A 120.0 . . ? C28 C29 H29B 120.0 . . ? H29A C29 H29B 120.0 . . ? C28 C30 H30 109.7 . . ? C28 C30 C32 105.7(13) . . ? C31 C30 C28 104.2(15) . . ? C31 C30 H30 109.7 . . ? C31 C30 C32 117.4(15) . . ? C32 C30 H30 109.7 . . ? C30 C31 H31A 109.5 . . ? C30 C31 H31B 109.5 . . ? C30 C31 H31C 109.5 . . ? H31A C31 H31B 109.5 . . ? H31A C31 H31C 109.5 . . ? H31B C31 H31C 109.5 . . ? C30 C32 H32A 109.5 . . ? C30 C32 H32B 109.5 . . ? C30 C32 H32C 109.5 . . ? H32A C32 H32B 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? C26A O2A C27A 115.4(6) . . ? C17 C23A H23A 109.2 . . ? C24A C23A C17 112.7(7) . . ? C24A C23A H23A 109.2 . . ? C24A C23A C25A 109.3(8) . . ? C25A C23A C17 107.1(6) . . ? C25A C23A H23A 109.2 . . ? C23A C24A H24D 109.5 . . ? C23A C24A H24E 109.5 . . ? C23A C24A H24F 109.5 . . ? H24D C24A H24E 109.5 . . ? H24D C24A H24F 109.5 . . ? H24E C24A H24F 109.5 . . ? C23A C25A H25C 108.8 . . ? C23A C25A H25D 108.8 . . ? H25C C25A H25D 107.7 . . ? C26A C25A C23A 113.6(7) . . ? C26A C25A H25C 108.8 . . ? C26A C25A H25D 108.8 . . ? O2A C26A C25A 105.9(7) . . ? O2A C26A H26A 109.1 . . ? O2A C26A C28A 110.0(7) . . ? C25A C26A H26A 109.1 . . ? C28A C26A C25A 113.5(7) . . ? C28A C26A H26A 109.1 . . ? O2A C27A H27D 109.5 . . ? O2A C27A H27E 109.5 . . ? O2A C27A H27F 109.5 . . ? H27D C27A H27E 109.5 . . ? H27D C27A H27F 109.5 . . ? H27E C27A H27F 109.5 . . ? C29A C28A C26A 116.0(7) . . ? C29A C28A C30A 126.5(8) . . ? C30A C28A C26A 117.3(7) . . ? C28A C29A H29C 120.0 . . ? C28A C29A H29D 120.0 . . ? H29C C29A H29D 120.0 . . ? C28A C30A H30A 107.5 . . ? C28A C30A C32A 108.8(7) . . ? C31A C30A C28A 113.2(9) . . ? C31A C30A H30A 107.5 . . ? C31A C30A C32A 112.2(9) . . ? C32A C30A H30A 107.5 . . ? C30A C31A H31D 109.5 . . ? C30A C31A H31E 109.5 . . ? C30A C31A H31F 109.5 . . ? H31D C31A H31E 109.5 . . ? H31D C31A H31F 109.5 . . ? H31E C31A H31F 109.5 . . ? C30A C32A H32D 109.5 . . ? C30A C32A H32E 109.5 . . ? C30A C32A H32F 109.5 . . ? H32D C32A H32E 109.5 . . ? H32D C32A H32F 109.5 . . ? H32E C32A H32F 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 H1 0.8200 . ? O1 C2 1.439(2) . ? O2 C26 1.44(2) . ? O2 C27 1.442(16) . ? C1 C2 1.543(3) . ? C1 C6 1.572(3) . ? C1 C18 1.514(3) . ? C1 C19 1.549(3) . ? C2 H2 0.9800 . ? C2 C3 1.502(3) . ? C3 H3A 0.9700 . ? C3 H3B 0.9700 . ? C3 C4 1.525(3) . ? C4 H4A 0.9700 . ? C4 H4B 0.9700 . ? C4 C5 1.555(3) . ? C5 C6 1.561(3) . ? C5 C10 1.539(3) . ? C5 C20 1.536(3) . ? C6 H6 0.9800 . ? C6 C7 1.505(3) . ? C7 H7A 0.9700 . ? C7 H7B 0.9700 . ? C7 C8 1.510(3) . ? C8 H8A 0.9700 . ? C8 H8B 0.9700 . ? C8 C9 1.520(3) . ? C9 H9 0.9800 . ? C9 C10 1.490(3) . ? C9 C14 1.551(3) . ? C10 C11 1.347(3) . ? C11 H11 0.9300 . ? C11 C12 1.517(3) . ? C12 H12A 0.9700 . ? C12 H12B 0.9700 . ? C12 C13 1.528(3) . ? C13 C14 1.551(3) . ? C13 C17 1.535(3) . ? C13 C21 1.522(3) . ? C14 C15 1.517(3) . ? C14 C22 1.515(3) . ? C15 H15A 0.9700 . ? C15 H15B 0.9700 . ? C15 C16 1.543(4) . ? C16 H16A 0.9700 . ? C16 H16B 0.9700 . ? C16 C17 1.544(4) . ? C17 H17 0.9800 . ? C17 H17A 0.9800 . ? C17 C23 1.592(16) . ? C17 C23A 1.563(8) . ? C18 H18A 0.9600 . ? C18 H18B 0.9600 . ? C18 H18C 0.9600 . ? C19 H19A 0.9600 . ? C19 H19B 0.9600 . ? C19 H19C 0.9600 . ? C20 H20A 0.9600 . ? C20 H20B 0.9600 . ? C20 H20C 0.9600 . ? C21 H21A 0.9600 . ? C21 H21B 0.9600 . ? C21 H21C 0.9600 . ? C22 H22A 0.9600 . ? C22 H22B 0.9600 . ? C22 H22C 0.9600 . ? C23 H23 0.9800 . ? C23 C24 1.459(15) . ? C23 C25 1.547(17) . ? C24 H24A 0.9600 . ? C24 H24B 0.9600 . ? C24 H24C 0.9600 . ? C25 H25A 0.9700 . ? C25 H25B 0.9700 . ? C25 C26 1.523(18) . ? C26 H26 0.9800 . ? C26 C28 1.551(16) . ? C27 H27A 0.9600 . ? C27 H27B 0.9600 . ? C27 H27C 0.9600 . ? C28 C29 1.411(17) . ? C28 C30 1.458(16) . ? C29 H29A 0.9300 . ? C29 H29B 0.9300 . ? C30 H30 0.9800 . ? C30 C31 1.449(15) . ? C30 C32 1.644(17) . ? C31 H31A 0.9600 . ? C31 H31B 0.9600 . ? C31 H31C 0.9600 . ? C32 H32A 0.9600 . ? C32 H32B 0.9600 . ? C32 H32C 0.9600 . ? O2A C26A 1.395(9) . ? O2A C27A 1.421(8) . ? C23A H23A 0.9800 . ? C23A C24A 1.480(8) . ? C23A C25A 1.550(8) . ? C24A H24D 0.9600 . ? C24A H24E 0.9600 . ? C24A H24F 0.9600 . ? C25A H25C 0.9700 . ? C25A H25D 0.9700 . ? C25A C26A 1.511(7) . ? C26A H26A 0.9800 . ? C26A C28A 1.509(7) . ? C27A H27D 0.9600 . ? C27A H27E 0.9600 . ? C27A H27F 0.9600 . ? C28A C29A 1.379(9) . ? C28A C30A 1.447(9) . ? C29A H29C 0.9300 . ? C29A H29D 0.9300 . ? C30A H30A 0.9800 . ? C30A C31A 1.433(10) . ? C30A C32A 1.655(10) . ? C31A H31D 0.9600 . ? C31A H31E 0.9600 . ? C31A H31F 0.9600 . ? C32A H32D 0.9600 . ? C32A H32E 0.9600 . ? C32A H32F 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C2 C3 C4 176.73(19) . . . . ? O2 C26 C28 C29 98(3) . . . . ? O2 C26 C28 C30 -67(2) . . . . ? C1 C2 C3 C4 -60.1(3) . . . . ? C1 C6 C7 C8 -161.96(17) . . . . ? C2 C1 C6 C5 -51.1(2) . . . . ? C2 C1 C6 C7 178.02(17) . . . . ? C2 C3 C4 C5 57.4(3) . . . . ? C3 C4 C5 C6 -50.0(2) . . . . ? C3 C4 C5 C10 -170.42(17) . . . . ? C3 C4 C5 C20 73.7(2) . . . . ? C4 C5 C6 C1 49.1(2) . . . . ? C4 C5 C6 C7 -177.75(18) . . . . ? C4 C5 C10 C9 166.65(18) . . . . ? C4 C5 C10 C11 -19.2(3) . . . . ? C5 C6 C7 C8 63.6(2) . . . . ? C5 C10 C11 C12 -169.6(2) . . . . ? C6 C1 C2 O1 175.27(16) . . . . ? C6 C1 C2 C3 54.7(2) . . . . ? C6 C5 C10 C9 46.7(2) . . . . ? C6 C5 C10 C11 -139.1(2) . . . . ? C6 C7 C8 C9 -59.7(3) . . . . ? C7 C8 C9 C10 48.5(3) . . . . ? C7 C8 C9 C14 177.31(19) . . . . ? C8 C9 C10 C5 -43.4(3) . . . . ? C8 C9 C10 C11 142.4(2) . . . . ? C8 C9 C14 C13 -177.33(19) . . . . ? C8 C9 C14 C15 68.3(3) . . . . ? C8 C9 C14 C22 -54.4(3) . . . . ? C9 C10 C11 C12 4.3(4) . . . . ? C9 C14 C15 C16 156.6(2) . . . . ? C10 C5 C6 C1 171.10(17) . . . . ? C10 C5 C6 C7 -55.7(2) . . . . ? C10 C9 C14 C13 -47.9(2) . . . . ? C10 C9 C14 C15 -162.35(19) . . . . ? C10 C9 C14 C22 75.0(2) . . . . ? C10 C11 C12 C13 15.3(4) . . . . ? C11 C12 C13 C14 -48.8(3) . . . . ? C11 C12 C13 C17 -163.1(2) . . . . ? C11 C12 C13 C21 71.7(2) . . . . ? C12 C13 C14 C9 67.0(2) . . . . ? C12 C13 C14 C15 -170.8(2) . . . . ? C12 C13 C14 C22 -54.4(2) . . . . ? C12 C13 C17 C16 152.9(2) . . . . ? C12 C13 C17 C23 -69.6(10) . . . . ? C12 C13 C17 C23A -84.5(5) . . . . ? C13 C14 C15 C16 37.6(2) . . . . ? C13 C17 C23 C24 52.4(18) . . . . ? C13 C17 C23 C25 -174.8(14) . . . . ? C13 C17 C23A C24A 58.7(8) . . . . ? C13 C17 C23A C25A 178.9(7) . . . . ? C14 C9 C10 C5 -173.40(17) . . . . ? C14 C9 C10 C11 12.4(3) . . . . ? C14 C13 C17 C16 35.9(2) . . . . ? C14 C13 C17 C23 173.4(9) . . . . ? C14 C13 C17 C23A 158.5(5) . . . . ? C14 C15 C16 C17 -15.5(3) . . . . ? C15 C16 C17 C13 -13.1(3) . . . . ? C15 C16 C17 C23 -152.5(9) . . . . ? C15 C16 C17 C23A -140.1(4) . . . . ? C16 C17 C23 C24 -176.0(12) . . . . ? C16 C17 C23 C25 -43.2(19) . . . . ? C16 C17 C23A C24A 177.7(6) . . . . ? C16 C17 C23A C25A -62.1(8) . . . . ? C17 C13 C14 C9 -168.33(19) . . . . ? C17 C13 C14 C15 -46.0(2) . . . . ? C17 C13 C14 C22 70.3(2) . . . . ? C17 C23 C25 C26 160(2) . . . . ? C17 C23A C25A C26A 167.1(9) . . . . ? C18 C1 C2 O1 48.9(2) . . . . ? C18 C1 C2 C3 -71.6(2) . . . . ? C18 C1 C6 C5 73.8(2) . . . . ? C18 C1 C6 C7 -57.0(2) . . . . ? C19 C1 C2 O1 -69.7(2) . . . . ? C19 C1 C2 C3 169.75(19) . . . . ? C19 C1 C6 C5 -166.55(18) . . . . ? C19 C1 C6 C7 62.6(2) . . . . ? C20 C5 C6 C1 -70.9(2) . . . . ? C20 C5 C6 C7 62.3(2) . . . . ? C20 C5 C10 C9 -76.3(2) . . . . ? C20 C5 C10 C11 97.9(2) . . . . ? C21 C13 C14 C9 -51.6(2) . . . . ? C21 C13 C14 C15 70.7(2) . . . . ? C21 C13 C14 C22 -173.01(19) . . . . ? C21 C13 C17 C16 -82.3(2) . . . . ? C21 C13 C17 C23 55.1(10) . . . . ? C21 C13 C17 C23A 40.2(5) . . . . ? C22 C14 C15 C16 -80.7(2) . . . . ? C23 C25 C26 O2 -69(3) . . . . ? C23 C25 C26 C28 164(2) . . . . ? C24 C23 C25 C26 -67(3) . . . . ? C25 C26 C28 C29 -137(3) . . . . ? C25 C26 C28 C30 57(3) . . . . ? C26 C28 C30 C31 77(2) . . . . ? C26 C28 C30 C32 -158.8(17) . . . . ? C27 O2 C26 C25 146(2) . . . . ? C27 O2 C26 C28 -90(3) . . . . ? C29 C28 C30 C31 -89(3) . . . . ? C29 C28 C30 C32 36(3) . . . . ? O2A C26A C28A C29A 130.7(12) . . . . ? O2A C26A C28A C30A -54.2(11) . . . . ? C23A C25A C26A O2A -62.4(12) . . . . ? C23A C25A C26A C28A 176.9(9) . . . . ? C24A C23A C25A C26A -70.6(13) . . . . ? C25A C26A C28A C29A -110.9(14) . . . . ? C25A C26A C28A C30A 64.3(12) . . . . ? C26A C28A C30A C31A 119.8(10) . . . . ? C26A C28A C30A C32A -114.7(10) . . . . ? C27A O2A C26A C25A 161.6(8) . . . . ? C27A O2A C26A C28A -75.4(10) . . . . ? C29A C28A C30A C31A -65.6(16) . . . . ? C29A C28A C30A C32A 59.9(16) . . . . ? loop_ _twin_individual_id _twin_individual_mass_fraction_refined 1 1.8(15) 2 -0.8(15) loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 0.000 0.000 -0.474 2252.5 56.4 '1.05 Hexane' 2 0.090 0.491 0.629 14.7 0.0 ? 3 0.401 0.910 0.296 14.7 0.0 ? 4 0.491 0.401 -0.038 14.7 0.0 ? 5 0.509 0.599 -0.038 14.7 0.0 ? 6 0.599 0.090 0.296 14.7 0.0 ? 7 0.910 0.509 0.629 14.7 0.0 ?