#------------------------------------------------------------------------------ #$Date: 2024-11-22 01:30:57 +0200 (Fri, 22 Nov 2024) $ #$Revision: 296051 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/96/7249630.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7249630 loop_ _publ_author_name 'Nath, Jitendra' 'Baruah, Jubaraj B.' _publ_section_title ; Positional isomers of (E)-2-(anthracen-9-ylmethylene)-N-(aryl)hydrazinecarbothioamide, zinc complexes and polymorphic solvates ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D4CE00992D _journal_year 2024 _chemical_formula_sum 'C52 H50 N8 O4 S2 Zn' _chemical_formula_weight 980.49 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2019/1 _audit_update_record ; 2024-09-28 deposited with the CCDC. 2024-11-21 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 118.737(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 31.105(3) _cell_length_b 9.3163(10) _cell_length_c 19.108(2) _cell_measurement_reflns_used 9983 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 24.98 _cell_measurement_theta_min 2.31 _cell_volume 4855.2(9) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2014 (Sheldrick 2014)' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _diffrn_ambient_temperature 296(2) _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0424 _diffrn_reflns_av_unetI/netI 0.0219 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 36 _diffrn_reflns_limit_h_min -36 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 53670 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.047 _diffrn_reflns_theta_max 25.047 _diffrn_reflns_theta_min 2.156 _exptl_absorpt_coefficient_mu 0.646 _exptl_absorpt_correction_type none _exptl_absorpt_process_details none _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.341 _exptl_crystal_description Block _exptl_crystal_F_000 2048 _exptl_crystal_size_max 0.42 _exptl_crystal_size_mid 0.39 _exptl_crystal_size_min 0.32 _refine_diff_density_max 0.503 _refine_diff_density_min -0.345 _refine_diff_density_rms 0.056 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.188 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 306 _refine_ls_number_reflns 4283 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.188 _refine_ls_R_factor_all 0.0756 _refine_ls_R_factor_gt 0.0473 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0594P)^2^+9.9481P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1203 _refine_ls_wR_factor_ref 0.1543 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3260 _reflns_number_total 4283 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4ce00992d2.cif _cod_data_source_block 3OCH3_ZnATU _cod_original_cell_volume 4855.3(9) _cod_original_sg_symbol_H-M 'C 2/c' _cod_database_code 7249630 _shelx_shelxl_version_number 2019/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL ZN3OCH3_0m_a.res in C2/c ZN3OCH3_0m_a.res created by SHELXL-2019/1 at 14:36:34 on 27-Mar-2024 CELL 0.71073 31.1052 9.3163 19.1082 90 118.737 90 ZERR 4 0.0033 0.001 0.002 0 0.003 0 LATT 7 SYMM -X,+Y,0.5-Z SFAC C H N O S Zn UNIT 208 200 32 16 8 4 OMIT 2 0 0 OMIT -3 50.1 L.S. 30 ACTA BOND $H FMAP 2 PLAN 2 MORE -1 CONF TEMP 22.85 WGHT 0.059400 9.948100 FVAR 0.23541 ZN1 6 0.500000 0.820263 0.750000 10.50000 0.04306 0.04721 = 0.05486 0.00000 0.02177 0.00000 S1 5 0.427359 0.883091 0.741483 11.00000 0.04833 0.04897 = 0.06693 -0.01079 0.02833 0.00153 N2 3 0.411638 0.667182 0.632001 11.00000 0.04050 0.05333 = 0.05566 -0.00776 0.02519 -0.00199 N1 3 0.459685 0.694461 0.652514 11.00000 0.04149 0.04960 = 0.05555 -0.00132 0.02558 0.00197 N3 3 0.349108 0.727787 0.657988 11.00000 0.04345 0.05624 = 0.06188 -0.01169 0.03092 0.00010 AFIX 43 H3 2 0.341136 0.778806 0.687489 11.00000 -1.20000 AFIX 0 O2 4 0.302862 -0.080031 0.726944 11.00000 0.10741 0.06815 = 0.12857 -0.01214 0.07403 -0.00016 O1 4 0.178344 0.608364 0.524085 11.00000 0.04696 0.10601 = 0.11912 -0.01677 0.03076 -0.01055 C16 1 0.395700 0.747937 0.671282 11.00000 0.04411 0.04255 = 0.04722 0.00093 0.02311 0.00532 C14 1 0.450131 0.550157 0.536631 11.00000 0.04296 0.06056 = 0.05730 -0.00664 0.03095 0.00444 C17 1 0.311499 0.636290 0.603367 11.00000 0.04882 0.05210 = 0.05339 -0.00354 0.02613 -0.00536 C15 1 0.476088 0.639824 0.608293 11.00000 0.04536 0.05798 = 0.06225 -0.00709 0.03049 0.00056 AFIX 43 H15 2 0.508735 0.659592 0.623627 11.00000 -1.20000 AFIX 0 C22 1 0.264598 0.666090 0.591651 11.00000 0.04723 0.05652 = 0.06274 -0.00093 0.02807 -0.00215 AFIX 43 H22 2 0.259896 0.741322 0.619250 11.00000 -1.20000 AFIX 0 C13 1 0.442906 0.605883 0.463239 11.00000 0.04788 0.07112 = 0.06169 0.00597 0.03184 0.01640 N4 3 0.274634 0.147209 0.701905 11.00000 0.09395 0.07282 = 0.09467 -0.00548 0.04395 0.00524 C1 1 0.436290 0.408332 0.541919 11.00000 0.04902 0.06133 = 0.06734 -0.00824 0.03460 0.00160 C21 1 0.225313 0.585114 0.539647 11.00000 0.05039 0.07046 = 0.07658 -0.00121 0.02944 -0.00828 C8 1 0.420531 0.518113 0.393390 11.00000 0.05572 0.10588 = 0.05571 -0.00014 0.02838 0.02629 C6 1 0.414731 0.321162 0.472140 11.00000 0.05556 0.07830 = 0.08160 -0.02193 0.03487 -0.00309 C7 1 0.406906 0.378713 0.400147 11.00000 0.05874 0.09937 = 0.06849 -0.02678 0.02420 0.00681 AFIX 43 H7 2 0.391967 0.321996 0.354552 11.00000 -1.20000 AFIX 0 C18 1 0.318714 0.522048 0.563726 11.00000 0.06392 0.06588 = 0.09794 -0.02704 0.04922 -0.01495 AFIX 43 H18 2 0.349906 0.498887 0.572043 11.00000 -1.20000 AFIX 0 C2 1 0.445307 0.345013 0.615892 11.00000 0.08378 0.06501 = 0.08251 -0.00263 0.05425 0.00033 AFIX 43 H2 2 0.459584 0.399713 0.662312 11.00000 -1.20000 AFIX 0 C20 1 0.231809 0.473853 0.498310 11.00000 0.06627 0.08273 = 0.09475 -0.02724 0.03626 -0.02552 AFIX 43 H20 2 0.205118 0.420285 0.462081 11.00000 -1.20000 AFIX 0 C12 1 0.456506 0.749222 0.456124 11.00000 0.07029 0.08167 = 0.08543 0.01963 0.04913 0.01682 AFIX 43 H12 2 0.470807 0.808579 0.500703 11.00000 -1.20000 AFIX 0 C26 1 0.307913 0.045871 0.719182 11.00000 0.07978 0.08530 = 0.10370 -0.01823 0.04837 -0.00723 AFIX 43 H26 2 0.338313 0.074803 0.726034 11.00000 -1.20000 AFIX 0 C19 1 0.277986 0.443120 0.511193 11.00000 0.08686 0.08043 = 0.10966 -0.04219 0.05689 -0.02164 AFIX 43 H19 2 0.282314 0.366735 0.483861 11.00000 -1.20000 AFIX 0 C3 1 0.433336 0.206534 0.619229 11.00000 0.12247 0.07043 = 0.11887 0.00355 0.08173 -0.00668 AFIX 43 H3A 2 0.439848 0.166745 0.667984 11.00000 -1.20000 AFIX 0 C5 1 0.402316 0.175175 0.479253 11.00000 0.09138 0.07455 = 0.11870 -0.03806 0.05228 -0.02902 AFIX 43 H5 2 0.387952 0.116851 0.434250 11.00000 -1.20000 AFIX 0 C23 1 0.170174 0.712036 0.570137 11.00000 0.06074 0.11835 = 0.12268 -0.00406 0.04859 0.00675 AFIX 137 H23A 2 0.135814 0.716168 0.553953 11.00000 -1.50000 H23B 2 0.180990 0.804204 0.562280 11.00000 -1.50000 H23C 2 0.188155 0.686342 0.625544 11.00000 -1.50000 AFIX 0 C10 1 0.426268 0.708452 0.315217 11.00000 0.11990 0.16383 = 0.08016 0.04105 0.05991 0.04447 AFIX 43 H10 2 0.420963 0.743642 0.266153 11.00000 -1.20000 AFIX 0 C9 1 0.413069 0.575362 0.320109 11.00000 0.09669 0.14828 = 0.06162 0.01042 0.03917 0.03978 AFIX 43 H9 2 0.398635 0.518689 0.274449 11.00000 -1.20000 AFIX 0 C11 1 0.448438 0.798745 0.383674 11.00000 0.10070 0.10583 = 0.11970 0.04931 0.07075 0.03525 AFIX 43 H11 2 0.457457 0.891931 0.378945 11.00000 -1.20000 AFIX 0 C4 1 0.411288 0.122703 0.550168 11.00000 0.12155 0.07132 = 0.16008 -0.01451 0.08710 -0.02687 AFIX 43 H4 2 0.402664 0.028393 0.553566 11.00000 -1.20000 AFIX 0 C24 1 0.226522 0.113581 0.689478 11.00000 0.10597 0.13804 = 0.16545 -0.01094 0.08203 0.01788 AFIX 137 H24A 2 0.216248 0.022940 0.662567 11.00000 -1.50000 H24B 2 0.204013 0.187099 0.657473 11.00000 -1.50000 H24C 2 0.227066 0.108168 0.740069 11.00000 -1.50000 AFIX 0 C25 1 0.284751 0.296140 0.693737 11.00000 0.19187 0.07005 = 0.20354 0.01018 0.07829 0.00112 AFIX 137 H25A 2 0.287699 0.349673 0.738766 11.00000 -1.50000 H25B 2 0.258426 0.334805 0.645623 11.00000 -1.50000 H25C 2 0.314837 0.302703 0.691406 11.00000 -1.50000 AFIX 0 HKLF 4 REM ZN3OCH3_0m_a.res in C2/c REM wR2 = 0.1543, GooF = S = 1.188, Restrained GooF = 1.188 for all data REM R1 = 0.0473 for 3260 Fo > 4sig(Fo) and 0.0756 for all 4283 data REM 306 parameters refined using 0 restraints END WGHT 0.0594 9.9397 REM Highest difference peak 0.503, deepest hole -0.345, 1-sigma level 0.056 Q1 1 0.4257 0.7643 0.7401 11.00000 0.05 0.50 Q2 1 0.5000 0.9543 0.7500 10.50000 0.05 0.34 ; _shelx_res_checksum 65074 _shelx_hkl_file ; 2 0 0 -0.10 0.10 -2 0 0 0.10 0.10 2 0 0 -0.10 0.10 -2 0 0 -0.10 0.10 -4 0 0 1392.36 35.40 -4 0 0 1397.46 35.00 -4 0 0 1449.76 35.60 -4 0 0 1417.86 34.40 4 0 0 1386.36 34.50 4 0 0 1418.86 34.80 4 0 0 1431.66 35.20 -4 0 0 1436.96 35.30 -4 0 0 1468.05 34.90 -4 0 0 1400.16 34.80 4 0 0 1402.16 34.40 4 0 0 1341.47 35.00 4 0 0 1435.46 35.60 -4 0 0 1375.76 34.50 4 0 0 1397.16 35.40 6 0 0 6280.27 152.38 6 0 0 6465.75 152.78 6 0 0 6241.98 153.18 -6 0 0 6828.72 152.28 6 0 0 6599.84 152.18 -6 0 0 6331.47 153.08 -6 0 0 6952.70 154.28 -6 0 0 6281.47 153.68 -6 0 0 6381.66 152.68 6 0 0 6322.37 153.18 6 0 0 6389.36 153.88 -6 0 0 6457.25 153.48 -6 0 0 6226.68 152.78 8 0 0 6768.12 159.68 -8 0 0 6185.78 158.18 -8 0 0 6845.52 159.88 -8 0 0 6854.41 157.38 8 0 0 6767.82 158.28 -8 0 0 6670.53 158.08 8 0 0 6567.24 157.08 -8 0 0 6471.55 159.18 -8 0 0 6628.24 157.98 8 0 0 6542.85 158.68 8 0 0 6582.74 159.48 8 0 0 6627.64 158.78 -8 0 0 6592.24 157.48 -8 0 0 6627.14 158.98 -10 0 0 507.05 16.80 -10 0 0 526.25 18.10 -10 0 0 506.65 15.60 10 0 0 492.95 15.80 10 0 0 530.55 17.90 10 0 0 507.35 17.10 10 0 0 500.65 17.70 10 0 0 518.55 15.50 -10 0 0 502.55 15.80 -10 0 0 538.95 17.50 -10 0 0 519.35 17.70 -10 0 0 523.05 16.30 -10 0 0 503.05 16.40 10 0 0 484.05 16.80 12 0 0 1718.93 47.90 -12 0 0 1735.73 47.50 12 0 0 1713.53 47.90 12 0 0 1622.94 44.20 12 0 0 1683.43 45.20 12 0 0 1769.12 47.30 -12 0 0 1723.83 45.30 -12 0 0 1694.63 45.60 -12 0 0 1786.22 45.10 -12 0 0 1795.12 48.50 -12 0 0 1718.23 46.10 -12 0 0 1714.43 46.50 -12 0 0 1691.43 47.60 -14 0 0 515.15 19.40 -14 0 0 525.45 17.20 14 0 0 520.65 19.80 14 0 0 544.15 19.50 14 0 0 509.65 17.40 14 0 0 536.35 20.20 -14 0 0 528.55 18.30 14 0 0 484.45 16.50 -14 0 0 490.85 19.30 -14 0 0 505.15 17.30 -14 0 0 503.75 17.70 -14 0 0 523.05 20.20 -14 0 0 494.65 18.40 16 0 0 65.29 5.70 16 0 0 71.49 7.10 16 0 0 66.69 6.80 16 0 0 63.09 6.20 -16 0 0 73.89 6.40 -16 0 0 77.09 7.00 -16 0 0 60.69 6.20 -16 0 0 70.39 7.20 -16 0 0 65.99 5.40 -16 0 0 63.69 5.60 -16 0 0 59.39 5.20 16 0 0 63.59 5.00 -18 0 0 188.18 12.20 -18 0 0 159.58 10.60 -18 0 0 172.88 9.20 18 0 0 194.48 11.70 18 0 0 176.38 12.00 18 0 0 182.08 8.80 18 0 0 183.18 9.60 -18 0 0 176.78 9.70 -18 0 0 160.98 9.40 -18 0 0 180.18 10.40 -18 0 0 174.88 11.30 -20 0 0 9.00 2.70 -20 0 0 5.20 3.00 -20 0 0 4.50 2.10 -20 0 0 8.50 2.70 20 0 0 3.30 2.30 -20 0 0 3.20 2.50 20 0 0 5.20 3.20 20 0 0 5.20 3.10 -20 0 0 5.60 2.90 22 0 0 563.44 21.00 22 0 0 573.94 24.20 -22 0 0 517.55 19.90 -22 0 0 535.65 25.00 -22 0 0 561.64 24.60 -22 0 0 553.14 21.80 22 0 0 521.35 24.80 24 0 0 5.80 3.80 24 0 0 6.40 3.60 -24 0 0 6.90 3.90 -24 0 0 5.50 3.40 -24 0 0 10.60 3.80 24 0 0 10.70 3.70 26 0 0 218.18 12.50 -26 0 0 224.08 15.80 26 0 0 195.18 15.10 -26 0 0 206.88 16.50 26 0 0 177.48 15.80 28 0 0 38.70 7.80 28 0 0 37.80 7.30 -28 0 0 44.40 9.10 -28 0 0 47.60 9.20 30 0 0 24.20 5.50 30 0 0 2.90 5.60 -30 0 0 16.70 6.30 -30 0 0 14.40 6.40 32 0 0 -7.20 5.00 -32 0 0 7.20 5.70 -32 0 0 2.20 6.10 1 -1 0 580.74 16.10 -1 -1 0 668.13 17.00 -1 -1 0 591.04 16.20 -1 -1 0 592.34 15.20 -1 -1 0 561.64 16.00 1 -1 0 590.04 15.80 -1 -1 0 579.94 15.90 -1 -1 0 666.13 17.00 1 -1 0 677.13 15.60 1 -1 0 576.54 15.40 -1 -1 0 667.43 15.60 -1 -1 0 573.24 16.10 1 -1 0 567.74 16.40 -1 1 0 571.54 15.80 1 1 0 586.84 16.10 1 1 0 576.44 16.10 -1 1 0 584.04 16.20 1 1 0 678.33 17.00 -1 1 0 646.64 15.90 1 1 0 553.84 15.80 -1 1 0 672.13 16.60 -1 1 0 580.64 16.10 -1 1 0 580.14 16.40 -1 1 0 571.34 15.90 -3 -1 0 280.97 8.90 3 -1 0 270.77 9.30 -3 -1 0 276.97 9.10 3 -1 0 273.87 8.20 3 -1 0 277.67 9.30 -3 -1 0 287.87 9.20 -3 -1 0 283.17 8.40 -3 -1 0 281.87 9.00 3 -1 0 274.87 9.30 -3 -1 0 270.87 9.30 -3 -1 0 289.37 8.70 3 -1 0 276.27 8.30 3 -1 0 268.17 9.00 3 1 0 283.97 8.90 3 1 0 272.87 9.20 -3 1 0 273.27 9.10 -3 1 0 289.07 8.20 3 1 0 281.07 8.30 -3 1 0 286.47 9.40 3 1 0 283.37 9.20 3 1 0 278.17 9.00 -3 1 0 277.17 8.10 3 1 0 279.57 9.00 -3 1 0 275.37 9.20 3 1 0 283.47 8.60 -3 1 0 270.17 9.20 -3 1 0 278.47 9.30 5 -1 0 878.91 23.80 -5 -1 0 939.91 24.50 5 -1 0 964.20 25.80 -5 -1 0 918.41 25.00 -5 -1 0 920.31 24.70 5 -1 0 926.41 25.80 -5 -1 0 903.31 25.50 5 -1 0 890.51 24.10 -5 -1 0 946.91 25.40 -5 -1 0 905.51 25.50 5 -1 0 908.51 25.70 5 -1 0 964.40 25.90 5 1 0 944.31 24.40 -5 1 0 946.11 25.70 -5 1 0 943.61 25.80 5 1 0 933.81 24.90 5 1 0 909.01 25.20 -5 1 0 951.10 25.50 -5 1 0 953.60 24.30 5 1 0 943.21 24.60 -5 1 0 902.71 25.40 -5 1 0 933.41 25.80 5 1 0 951.00 25.60 -5 1 0 936.91 23.80 5 1 0 913.61 24.90 5 1 0 944.91 25.40 -7 -1 0 296.47 8.60 -7 -1 0 293.77 11.40 7 -1 0 290.27 9.60 -7 -1 0 303.87 8.70 7 -1 0 307.77 11.50 7 -1 0 307.67 11.50 -7 -1 0 315.97 11.00 -7 -1 0 312.27 11.10 -7 -1 0 295.37 11.40 -7 -1 0 307.27 10.40 -7 -1 0 296.47 10.60 7 -1 0 309.97 11.70 7 -1 0 294.57 11.50 7 -1 0 289.47 10.10 7 1 0 299.67 10.50 -7 1 0 305.27 11.70 -7 1 0 303.07 11.10 7 1 0 312.27 10.40 7 1 0 299.27 11.10 7 1 0 288.17 10.70 -7 1 0 295.97 11.20 -7 1 0 305.37 11.60 -7 1 0 294.37 9.40 -7 1 0 304.77 11.30 7 1 0 306.57 10.80 -7 1 0 305.47 10.40 7 1 0 312.27 11.40 9 -1 0 258.07 10.90 -9 -1 0 249.18 8.20 -9 -1 0 252.07 10.40 9 -1 0 245.68 9.00 -9 -1 0 261.47 8.40 9 -1 0 245.08 11.00 -9 -1 0 256.67 10.10 -9 -1 0 248.58 9.80 9 -1 0 235.78 9.70 -9 -1 0 258.47 10.40 -9 -1 0 245.58 10.90 9 -1 0 241.48 10.80 9 -1 0 257.87 11.10 -9 -1 0 259.17 11.00 9 1 0 252.37 10.10 9 1 0 260.67 9.90 -9 1 0 249.88 8.90 -9 1 0 248.48 10.50 9 1 0 257.87 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393.96 17.10 -13 3 0 411.36 18.20 13 3 0 408.26 16.70 13 3 0 389.86 15.50 -13 3 0 423.56 15.30 -13 3 0 394.16 14.10 13 3 0 397.26 16.90 15 -3 0 412.56 15.70 -15 -3 0 408.56 19.50 -15 -3 0 398.46 18.50 -15 -3 0 409.26 17.40 15 -3 0 383.86 19.30 15 -3 0 432.76 20.40 -15 -3 0 410.46 16.90 15 3 0 406.66 17.30 -15 3 0 395.46 19.10 15 3 0 426.96 16.50 -15 3 0 407.76 16.00 15 3 0 374.06 17.30 -15 3 0 403.46 19.30 15 3 0 410.26 16.80 -15 3 0 381.96 14.50 15 3 0 419.26 18.90 -17 -3 0 384.46 17.40 -17 -3 0 357.86 16.80 17 -3 0 390.66 15.40 -17 -3 0 368.86 19.30 -17 -3 0 362.86 17.90 17 -3 0 376.36 19.60 17 -3 0 381.66 19.80 17 3 0 427.06 17.70 17 3 0 365.16 16.40 -17 3 0 367.16 16.00 -17 3 0 377.16 19.30 -17 3 0 343.87 14.00 -17 3 0 350.26 18.70 17 3 0 370.66 15.90 17 3 0 383.36 18.40 -19 -3 0 139.79 12.20 -19 -3 0 145.49 10.90 19 -3 0 145.09 12.30 -19 -3 0 142.89 10.30 -19 -3 0 149.99 11.50 19 -3 0 132.79 11.90 19 -3 0 144.59 8.90 -19 3 0 135.49 11.80 19 3 0 132.19 11.50 19 3 0 143.39 10.40 -19 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4.10 4.60 26 -4 0 1.10 4.90 -26 -4 0 0.10 2.50 26 -4 0 -2.80 5.00 -26 -4 0 3.10 5.20 -26 -4 0 -4.20 3.50 26 4 0 -9.00 4.00 -26 4 0 -5.00 4.00 -26 4 0 -1.40 3.80 -26 4 0 -2.40 3.00 26 4 0 -1.50 3.90 28 -4 0 -10.60 5.10 -28 -4 0 4.60 3.40 28 -4 0 -10.50 5.40 -28 -4 0 -0.80 4.10 -28 4 0 -5.30 4.70 28 4 0 -7.60 4.60 28 4 0 0.10 4.50 -28 4 0 -6.00 3.90 -30 -4 0 -5.00 2.80 30 -4 0 9.00 4.30 30 -4 0 -14.00 7.00 30 4 0 -7.10 5.20 -30 4 0 -9.00 5.90 -30 4 0 -0.30 5.30 -1 -5 0 2.10 1.80 1 -5 0 -2.50 1.50 1 -5 0 0.80 1.80 -1 -5 0 -1.70 1.50 1 -5 0 1.60 1.60 -1 -5 0 -0.10 1.20 1 -5 0 0.30 1.80 -1 -5 0 0.50 1.50 -1 -5 0 0.90 1.50 1 5 0 1.60 1.50 1 5 0 -1.40 1.50 -1 5 0 -0.30 1.50 1 5 0 1.40 1.30 -1 5 0 -0.60 1.60 -1 5 0 -1.00 1.80 -1 5 0 0.90 2.00 1 5 0 3.00 1.10 -1 5 0 -2.00 1.20 -1 5 0 -3.10 1.50 1 5 0 0.70 1.70 -1 5 0 -0.90 1.50 -1 5 0 1.50 1.70 1 5 0 1.50 1.50 1 5 0 -2.60 1.70 -1 5 0 -1.80 1.40 1 5 0 -1.60 1.50 1 5 0 -1.20 1.40 -3 -5 0 609.74 23.30 3 -5 0 648.04 21.90 3 -5 0 728.33 24.00 -3 -5 0 641.44 24.00 3 -5 0 683.33 26.10 3 -5 0 704.33 21.90 -3 -5 0 610.34 22.90 -3 -5 0 592.14 24.10 -3 -5 0 589.74 20.40 3 -5 0 718.43 27.50 3 5 0 582.34 25.70 3 5 0 639.44 25.90 -3 5 0 662.93 25.20 3 5 0 635.54 21.20 3 5 0 629.94 24.40 3 5 0 622.64 21.20 -3 5 0 667.13 21.60 -3 5 0 657.03 23.80 -3 5 0 687.13 24.30 -3 5 0 719.13 23.80 3 5 0 613.44 23.90 3 5 0 634.84 24.70 3 5 0 618.44 21.10 -3 5 0 658.63 21.90 3 5 0 594.34 23.10 3 5 0 617.74 23.60 -3 5 0 648.24 25.60 -3 5 0 731.53 23.20 -3 5 0 696.03 22.80 -3 5 0 675.73 26.60 5 -5 0 121.19 7.20 -5 -5 0 128.49 10.00 -5 -5 0 127.59 8.90 -5 -5 0 124.39 7.40 -5 -5 0 119.59 9.40 5 -5 0 122.39 10.20 5 -5 0 122.39 7.40 5 -5 0 121.89 8.10 -5 -5 0 135.09 9.50 5 -5 0 128.89 10.50 -5 -5 0 126.29 9.50 -5 5 0 111.29 9.60 5 5 0 131.29 7.50 -5 5 0 128.19 9.40 5 5 0 134.49 9.30 -5 5 0 124.39 8.40 -5 5 0 114.09 7.70 -5 5 0 121.89 7.30 5 5 0 128.59 9.30 5 5 0 128.79 7.00 -5 5 0 117.69 9.10 -5 5 0 138.19 7.60 5 5 0 121.39 6.80 5 5 0 113.79 8.80 5 5 0 119.69 9.00 -5 5 0 123.09 7.40 5 5 0 113.89 9.90 -5 5 0 130.09 8.80 -5 5 0 126.09 9.50 5 5 0 119.29 9.10 -5 5 0 121.69 10.60 5 5 0 129.99 10.40 -7 -5 0 516.85 21.10 7 -5 0 513.85 23.20 -7 -5 0 537.45 21.50 -7 -5 0 498.85 22.80 -7 -5 0 528.45 21.00 7 -5 0 546.55 23.90 -7 -5 0 516.35 21.80 -7 -5 0 525.75 18.20 7 -5 0 516.45 17.40 7 -5 0 502.25 19.70 7 5 0 516.65 23.70 -7 5 0 520.35 22.10 7 5 0 511.95 17.70 -7 5 0 509.85 18.10 -7 5 0 513.15 17.20 7 5 0 530.45 22.80 7 5 0 545.15 16.50 -7 5 0 501.25 20.50 -7 5 0 543.15 18.10 7 5 0 498.75 15.90 -7 5 0 519.05 22.00 7 5 0 536.25 21.00 7 5 0 525.95 21.00 -7 5 0 494.45 19.00 -7 5 0 505.35 21.90 -7 5 0 532.75 24.10 7 5 0 532.15 21.30 -7 5 0 528.55 20.60 -9 -5 0 174.48 9.50 9 -5 0 150.98 12.00 -9 -5 0 165.98 10.80 -9 -5 0 169.78 11.90 -9 -5 0 171.68 11.60 9 -5 0 172.88 13.00 9 -5 0 173.98 10.20 9 -5 0 166.48 7.80 -9 -5 0 173.68 10.90 9 5 0 148.89 10.50 9 5 0 181.38 12.30 -9 5 0 154.98 11.50 -9 5 0 173.68 11.00 9 5 0 174.18 10.60 9 5 0 158.38 8.50 -9 5 0 159.28 7.80 -9 5 0 161.28 7.50 -9 5 0 177.18 8.70 -9 5 0 172.08 9.30 -9 5 0 156.18 9.00 -9 5 0 177.98 11.40 11 -5 0 6.00 3.50 -11 -5 0 4.00 2.80 -11 -5 0 1.50 2.10 11 -5 0 2.70 3.00 -11 -5 0 3.50 2.30 -11 -5 0 5.60 2.60 11 -5 0 0.90 1.70 -11 -5 0 6.30 2.80 11 5 0 4.40 2.20 -11 5 0 3.50 1.90 -11 5 0 3.50 2.50 11 5 0 3.80 2.40 -11 5 0 3.50 2.40 11 5 0 7.50 3.40 11 5 0 2.20 1.80 -11 5 0 4.70 1.30 -11 5 0 1.50 1.50 13 -5 0 -0.80 3.10 13 -5 0 0.10 2.20 -13 -5 0 1.60 3.10 -13 -5 0 -1.20 2.50 13 -5 0 0.20 2.40 -13 -5 0 3.50 1.50 -13 -5 0 1.20 2.40 -13 5 0 1.30 2.40 13 5 0 1.30 2.40 13 5 0 1.00 1.90 13 5 0 1.80 2.60 -13 5 0 0.20 1.60 -13 5 0 1.80 2.50 13 5 0 8.00 4.10 -15 -5 0 32.80 5.60 -15 -5 0 34.60 6.40 -15 -5 0 34.10 7.00 15 -5 0 33.80 4.90 15 -5 0 24.30 6.10 -15 -5 0 26.90 5.50 15 -5 0 23.60 5.90 -15 5 0 25.10 5.30 -15 5 0 24.80 4.00 -15 5 0 24.00 5.60 -15 5 0 29.00 4.60 15 5 0 30.30 5.70 15 5 0 40.60 5.50 15 5 0 31.80 6.30 -17 -5 0 164.88 11.20 -17 -5 0 180.08 14.00 -17 -5 0 172.58 13.40 17 -5 0 143.49 13.80 17 -5 0 167.08 14.50 17 -5 0 175.68 10.50 -17 5 0 172.58 14.00 17 5 0 182.78 12.80 -17 5 0 163.78 10.10 17 5 0 165.78 13.30 17 5 0 169.18 11.00 -17 5 0 141.29 12.40 -19 -5 0 266.67 18.50 -19 -5 0 240.88 14.80 19 -5 0 263.07 19.40 19 -5 0 258.47 13.90 -19 -5 0 232.68 16.30 19 -5 0 271.57 18.80 19 5 0 270.57 16.20 19 5 0 263.07 14.50 -19 5 0 267.87 17.70 -19 5 0 269.07 13.50 -19 5 0 260.07 17.60 19 5 0 275.87 17.80 21 -5 0 56.19 10.50 21 -5 0 78.09 10.90 -21 -5 0 76.99 8.50 -21 -5 0 79.09 10.20 -21 -5 0 69.89 11.30 21 5 0 76.59 10.30 21 5 0 55.09 8.20 21 5 0 68.19 8.80 -21 5 0 61.59 9.80 -21 5 0 56.19 9.20 -21 5 0 74.89 8.40 -23 -5 0 3.40 4.20 23 -5 0 15.60 6.80 23 -5 0 16.10 4.80 -23 -5 0 1.20 4.10 -23 5 0 7.00 4.90 23 5 0 8.30 4.50 -23 5 0 13.40 5.30 23 5 0 4.70 4.50 25 -5 0 2.90 5.10 25 -5 0 8.00 4.50 -25 -5 0 9.10 5.20 -25 -5 0 -5.10 3.60 25 5 0 2.60 4.30 -25 5 0 0.50 4.40 -25 5 0 -1.90 4.30 25 5 0 -3.90 4.00 27 -5 0 4.00 7.40 -27 -5 0 1.50 5.70 -27 -5 0 7.20 5.30 27 -5 0 10.70 7.30 27 5 0 6.80 4.80 27 5 0 -4.50 5.30 -27 5 0 16.50 6.50 -27 5 0 11.60 6.60 29 -5 0 -9.80 6.90 0 -6 0 79.69 9.20 0 -6 0 81.19 7.60 0 -6 0 98.49 7.70 0 -6 0 80.09 7.70 0 6 0 97.89 9.90 0 6 0 87.19 8.10 0 6 0 73.59 6.90 0 6 0 85.49 7.60 0 6 0 84.29 8.90 0 6 0 85.09 7.60 0 6 0 81.19 6.90 2 -6 0 176.88 10.70 -2 -6 0 142.69 10.40 2 -6 0 170.38 12.40 -2 -6 0 151.78 12.40 -2 -6 0 148.89 9.00 -2 -6 0 152.38 10.70 -2 -6 0 163.58 10.40 -2 6 0 176.58 11.30 -2 6 0 185.98 11.30 2 6 0 156.68 9.30 2 6 0 168.08 9.90 -2 6 0 177.28 12.90 2 6 0 158.48 9.60 2 6 0 155.28 12.30 2 6 0 155.88 11.20 -2 6 0 169.58 10.40 2 6 0 172.28 12.20 4 -6 0 210.18 11.30 -4 -6 0 194.28 10.10 4 -6 0 227.08 12.50 4 -6 0 209.68 14.80 4 -6 0 196.58 13.80 -4 -6 0 181.88 11.80 -4 -6 0 177.08 12.10 4 -6 0 215.98 11.10 -4 -6 0 186.98 13.00 -4 -6 0 213.58 12.70 4 6 0 197.88 10.20 4 6 0 194.28 10.30 -4 6 0 198.38 14.30 -4 6 0 211.18 11.10 4 6 0 190.78 13.90 -4 6 0 223.68 12.40 4 6 0 199.18 13.00 4 6 0 211.28 13.40 4 6 0 186.28 10.30 -4 6 0 200.58 11.80 -4 6 0 205.18 12.70 4 6 0 201.98 12.70 -4 6 0 217.48 11.70 6 -6 0 54.79 6.60 6 -6 0 35.80 6.50 -6 -6 0 54.89 6.90 6 -6 0 37.80 6.80 -6 -6 0 59.69 6.50 -6 -6 0 50.69 6.90 -6 -6 0 35.50 6.10 6 -6 0 50.09 5.50 -6 -6 0 54.19 5.70 -6 6 0 58.09 7.10 -6 6 0 44.20 5.10 -6 6 0 62.89 6.70 -6 6 0 54.79 7.20 6 6 0 52.39 5.20 -6 6 0 42.70 7.30 6 6 0 47.30 6.80 -6 6 0 55.19 6.40 6 6 0 47.10 5.20 6 6 0 65.49 7.70 6 6 0 57.39 8.20 -6 6 0 53.79 5.40 6 6 0 44.30 4.50 6 6 0 58.59 7.10 -8 -6 0 294.77 16.70 -8 -6 0 321.37 16.10 8 -6 0 310.57 18.70 8 -6 0 297.57 18.70 -8 -6 0 296.57 15.80 -8 -6 0 307.17 16.70 8 -6 0 301.17 12.90 -8 -6 0 286.57 13.10 8 -6 0 309.57 15.40 -8 6 0 306.97 19.00 8 6 0 289.37 11.50 -8 6 0 311.37 13.20 8 6 0 274.77 12.50 8 6 0 319.97 18.30 -8 6 0 282.67 12.40 -8 6 0 291.07 17.00 8 6 0 308.77 16.50 -8 6 0 304.57 15.70 8 6 0 307.97 16.00 -8 6 0 275.77 14.20 -8 6 0 279.07 12.80 8 6 0 278.77 15.60 -10 -6 0 142.79 11.00 10 -6 0 164.18 13.50 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2.60 16 6 0 -0.80 2.80 18 -6 0 3.90 4.80 18 -6 0 4.60 4.10 -18 -6 0 1.50 2.50 18 -6 0 3.70 3.50 -18 -6 0 1.50 3.90 -18 6 0 -0.80 3.10 -18 6 0 7.00 4.20 18 6 0 3.80 3.80 18 6 0 8.10 4.70 -20 -6 0 20.70 6.20 20 -6 0 10.90 7.00 20 -6 0 22.30 7.10 -20 -6 0 9.40 4.90 20 6 0 15.20 5.10 -20 6 0 11.80 5.80 -20 6 0 13.10 5.80 20 6 0 21.70 6.30 22 -6 0 139.89 15.40 -22 -6 0 117.19 13.80 -22 -6 0 129.79 12.70 22 -6 0 107.69 14.70 22 6 0 134.49 12.90 -22 6 0 134.19 14.80 -22 6 0 107.49 13.20 22 6 0 107.39 12.80 -24 -6 0 41.50 8.60 24 -6 0 42.90 10.50 -24 -6 0 52.19 9.90 -24 6 0 43.80 9.40 24 6 0 40.40 9.20 24 6 0 46.10 7.90 -24 6 0 34.10 8.90 -26 -6 0 1.80 4.70 26 -6 0 0.60 6.40 -26 -6 0 11.00 5.80 -26 6 0 14.40 6.30 26 6 0 2.90 4.90 26 6 0 0.60 4.70 1 -7 0 -1.90 2.00 1 -7 0 -0.70 2.80 -1 -7 0 -1.40 2.40 -1 -7 0 -0.20 2.10 1 -7 0 -3.20 1.90 1 -7 0 -4.90 2.00 -1 -7 0 -1.90 1.90 -1 -7 0 -3.30 2.20 1 7 0 -2.50 1.40 -1 7 0 2.90 1.80 -1 7 0 -0.60 1.10 -1 7 0 0.50 1.70 -1 7 0 -3.80 2.20 1 7 0 -1.80 2.40 3 -7 0 7.00 3.20 -3 -7 0 5.00 2.80 3 -7 0 2.50 2.90 3 -7 0 4.40 3.90 3 -7 0 5.60 3.40 3 -7 0 6.10 2.90 -3 -7 0 1.80 2.20 -3 -7 0 1.50 2.20 -3 -7 0 2.90 2.00 3 7 0 2.80 2.50 3 7 0 8.00 2.50 -3 7 0 -1.70 2.80 -3 7 0 3.30 3.70 -3 7 0 3.60 2.70 3 7 0 0.60 1.80 -3 7 0 8.60 3.50 -3 7 0 3.40 2.90 3 7 0 1.20 2.60 3 7 0 0.00 2.30 -5 -7 0 44.90 5.90 5 -7 0 51.49 8.30 5 -7 0 46.10 6.30 -5 -7 0 65.89 7.40 5 -7 0 54.59 7.30 5 -7 0 45.80 8.00 -5 -7 0 50.89 6.80 -5 -7 0 35.60 6.50 5 -7 0 63.79 6.90 5 7 0 57.19 5.60 -5 7 0 51.49 8.90 -5 7 0 48.80 7.60 -5 7 0 50.29 5.90 -5 7 0 51.29 6.30 -5 7 0 52.49 6.60 5 7 0 43.20 7.10 5 7 0 58.79 7.90 5 7 0 45.40 8.50 -5 7 0 72.59 9.70 -7 -7 0 10.50 4.50 7 -7 0 12.10 3.60 7 -7 0 7.00 2.70 -7 -7 0 10.90 2.30 -7 -7 0 7.00 3.20 7 -7 0 6.70 3.40 -7 -7 0 8.00 3.40 7 7 0 7.30 2.40 -7 7 0 7.70 2.70 7 7 0 1.90 2.90 7 7 0 6.10 3.50 -7 7 0 2.10 3.20 -7 7 0 3.50 3.10 7 7 0 3.40 3.30 -7 7 0 6.80 3.00 -7 7 0 8.90 3.90 9 -7 0 2.70 2.40 9 -7 0 -2.90 2.40 9 -7 0 1.10 3.20 -9 -7 0 -2.30 2.70 9 -7 0 -1.50 2.10 -9 -7 0 -1.40 2.30 9 7 0 3.70 2.70 -9 7 0 -1.10 1.80 -9 7 0 -3.40 1.70 -9 7 0 1.00 3.00 -9 7 0 -2.00 2.60 9 7 0 2.80 3.50 -9 7 0 0.40 2.70 -11 -7 0 30.90 5.90 11 -7 0 37.20 5.80 11 -7 0 36.90 8.20 -11 -7 0 34.10 6.90 11 -7 0 31.40 7.30 -11 -7 0 40.50 7.50 11 7 0 29.60 6.10 -11 7 0 34.80 8.10 -11 7 0 34.10 6.20 11 7 0 45.80 8.50 -11 7 0 28.60 6.40 11 7 0 33.20 6.00 -13 -7 0 26.20 6.00 13 -7 0 45.20 9.30 -13 -7 0 25.00 6.10 13 -7 0 26.60 7.40 13 -7 0 31.70 6.50 13 7 0 33.70 6.30 13 7 0 24.50 5.50 -13 7 0 34.30 6.50 -13 7 0 25.60 7.30 -13 7 0 30.80 6.90 13 7 0 29.30 6.90 -15 -7 0 -1.00 1.80 15 -7 0 1.60 2.80 15 -7 0 -3.60 3.80 -15 7 0 -2.10 3.30 15 7 0 -4.00 3.00 15 7 0 -0.30 2.30 -15 7 0 1.80 3.20 -15 7 0 1.10 3.10 15 7 0 -1.30 2.70 -17 -7 0 3.90 3.70 17 -7 0 3.50 4.60 -17 -7 0 -4.50 3.20 17 -7 0 6.30 5.00 -17 7 0 4.70 4.20 -17 7 0 1.50 2.10 17 7 0 0.70 2.90 17 7 0 9.50 4.40 -19 -7 0 1.80 5.00 19 -7 0 -11.20 4.70 -19 -7 0 10.60 4.80 19 -7 0 -0.10 4.30 19 7 0 8.70 4.70 19 7 0 9.40 5.20 -19 7 0 -1.60 2.90 -19 7 0 0.00 4.90 -21 -7 0 11.50 5.40 21 -7 0 19.80 5.30 21 -7 0 19.00 6.70 -21 7 0 21.70 7.20 21 7 0 3.60 5.10 -21 7 0 19.90 4.80 21 7 0 2.50 4.70 -23 -7 0 5.80 5.90 23 -7 0 10.40 4.90 -23 -7 0 1.50 4.40 23 -7 0 -6.40 5.90 23 7 0 -7.10 3.90 23 7 0 -0.30 5.60 -23 7 0 0.40 4.10 -23 7 0 -2.10 4.20 -25 -7 0 9.00 3.40 25 -7 0 6.80 7.00 25 -7 0 -1.30 5.80 -25 -7 0 -3.10 4.80 25 7 0 -7.20 4.40 -25 7 0 2.60 5.30 -25 7 0 7.80 4.10 0 -8 0 3.00 3.60 0 -8 0 1.20 3.10 0 -8 0 8.00 3.30 0 -8 0 4.80 3.50 0 8 0 3.70 2.90 0 8 0 0.50 3.00 0 8 0 2.40 4.30 0 8 0 1.80 3.00 2 -8 0 16.30 4.80 2 -8 0 11.20 3.80 -2 -8 0 6.40 3.80 2 -8 0 7.00 3.60 2 -8 0 14.30 4.80 -2 -8 0 12.00 4.70 -2 -8 0 12.20 4.50 2 8 0 7.20 4.10 -2 8 0 12.70 4.80 -2 8 0 6.20 4.20 2 8 0 10.60 3.50 -2 8 0 14.10 4.30 2 8 0 4.20 2.80 2 8 0 3.80 3.90 -2 8 0 10.50 5.10 2 8 0 10.40 3.10 -4 -8 0 168.08 12.50 4 -8 0 200.38 16.60 -4 -8 0 140.29 12.50 -4 -8 0 152.58 12.90 4 -8 0 178.58 12.90 4 -8 0 162.88 12.10 4 8 0 159.48 14.70 -4 8 0 186.48 15.60 4 8 0 144.69 10.20 4 8 0 157.28 13.00 -4 8 0 179.68 14.80 4 8 0 154.38 13.70 -4 8 0 171.68 13.30 -4 8 0 179.48 11.90 -6 -8 0 96.29 11.10 -6 -8 0 106.89 9.90 -6 -8 0 102.09 10.20 6 -8 0 118.59 12.80 6 -8 0 109.19 10.40 6 -8 0 98.99 13.10 -6 8 0 104.09 11.40 -6 8 0 113.59 9.70 -6 8 0 111.89 13.10 6 8 0 123.09 11.60 6 8 0 93.59 10.10 -6 8 0 103.19 9.90 -6 8 0 91.49 12.50 6 8 0 115.29 12.10 8 -8 0 101.89 12.90 8 -8 0 108.39 10.50 -8 -8 0 97.09 10.60 -8 -8 0 78.89 9.70 8 -8 0 99.09 12.10 -8 -8 0 82.19 9.70 8 8 0 104.59 10.20 -8 8 0 99.39 11.10 8 8 0 97.69 10.90 -8 8 0 87.39 8.70 8 8 0 102.29 11.20 -8 8 0 85.49 11.70 -10 -8 0 39.30 7.90 -10 -8 0 23.90 6.30 10 -8 0 34.70 8.70 10 -8 0 26.00 7.10 -10 -8 0 28.10 6.10 10 8 0 22.70 5.80 -10 8 0 26.30 6.30 -10 8 0 20.70 6.40 -10 8 0 28.90 7.20 10 8 0 37.70 8.90 10 8 0 27.20 5.80 -12 -8 0 6.40 3.40 12 -8 0 -5.20 4.20 -12 -8 0 -5.60 2.50 -12 8 0 -0.50 2.20 -12 8 0 0.40 3.30 12 8 0 3.20 3.40 -12 8 0 -1.30 3.20 12 8 0 -7.00 3.10 12 8 0 -3.30 3.40 -14 -8 0 1.90 3.20 14 -8 0 -5.40 4.40 -14 -8 0 0.20 3.70 14 -8 0 -3.00 3.80 14 -8 0 12.70 4.60 14 8 0 5.70 5.10 14 8 0 1.80 4.90 14 8 0 8.40 4.00 -14 8 0 9.20 4.90 -14 8 0 -1.90 3.60 -14 8 0 3.30 3.20 -16 -8 0 3.30 4.40 16 -8 0 0.30 5.90 -16 -8 0 5.60 5.10 16 -8 0 20.60 6.30 -16 8 0 2.20 4.00 16 8 0 5.00 4.50 -16 8 0 4.30 5.10 -16 8 0 6.00 4.60 16 8 0 5.70 3.90 -18 -8 0 21.00 6.20 18 -8 0 12.30 7.50 -18 -8 0 27.10 8.50 18 -8 0 37.90 9.00 -18 8 0 21.80 7.50 18 8 0 22.90 6.40 -18 8 0 23.80 7.30 -18 8 0 28.30 8.30 18 8 0 30.10 7.70 -20 -8 0 59.09 9.70 -20 -8 0 67.39 12.20 20 -8 0 63.29 12.60 20 -8 0 45.50 12.90 20 8 0 53.69 10.50 -20 8 0 56.99 11.80 20 8 0 40.70 7.90 -20 8 0 66.89 11.50 -20 8 0 47.20 10.80 22 -8 0 40.20 9.00 -22 -8 0 53.69 11.40 22 -8 0 54.99 12.10 -22 -8 0 57.19 10.70 -22 8 0 50.99 10.20 22 8 0 52.29 11.10 -22 8 0 44.20 10.40 -22 8 0 37.30 10.00 22 8 0 27.10 7.50 -1 -9 0 3.60 3.70 -1 -9 0 4.50 4.40 1 -9 0 -5.80 3.40 -1 -9 0 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21.90 3.60 20 4 -4 17.00 3.00 20 4 -4 20.80 5.00 -20 4 4 17.40 5.00 20 4 -4 23.60 5.10 -20 4 4 20.30 5.60 -18 -4 4 93.89 9.30 -18 -4 4 90.49 8.90 18 -4 -4 101.09 8.60 18 -4 -4 86.09 9.80 -18 -4 4 87.49 9.60 18 -4 -4 99.09 10.20 18 4 -4 85.59 5.70 -18 4 4 82.99 8.80 -18 4 4 95.19 5.80 18 4 -4 93.09 8.90 -18 4 4 89.59 10.00 -18 4 4 109.09 10.30 18 4 -4 92.49 8.50 18 4 -4 88.59 9.30 -16 -4 4 87.29 8.50 -16 -4 4 83.39 8.80 -16 -4 4 81.69 8.40 16 -4 -4 98.29 8.10 -16 -4 4 101.69 6.00 16 -4 -4 90.79 9.50 16 -4 -4 85.39 9.20 16 4 -4 84.49 7.80 16 4 -4 88.89 8.60 -16 4 4 74.49 8.50 -16 4 4 87.89 9.40 -16 4 4 91.89 9.10 -16 4 4 95.49 8.70 16 4 -4 74.29 7.40 16 4 -4 82.49 7.70 16 4 -4 93.19 5.40 14 -4 -4 293.27 16.90 14 -4 -4 330.37 10.90 -14 -4 4 283.57 10.00 -14 -4 4 303.87 15.50 14 -4 -4 276.87 16.70 -14 -4 4 300.87 15.40 -14 -4 4 301.17 16.60 14 -4 -4 310.57 14.90 14 -4 -4 311.07 14.80 -14 -4 4 309.27 12.00 -14 -4 4 311.47 16.00 14 4 -4 305.57 10.10 14 4 -4 324.07 16.50 14 4 -4 304.47 10.90 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35.20 3.90 6 4 -4 26.30 3.80 -6 4 4 26.80 4.20 6 4 -4 27.20 4.50 6 4 -4 26.20 4.40 -6 4 4 19.90 4.10 6 4 -4 25.80 4.00 -4 -4 4 194.38 9.50 4 -4 -4 182.58 11.80 -4 -4 4 196.78 10.90 4 -4 -4 210.78 10.80 4 -4 -4 187.78 12.30 4 -4 -4 199.68 10.20 -4 -4 4 202.48 10.20 -4 -4 4 187.68 10.90 -4 -4 4 197.18 10.30 4 -4 -4 207.88 11.30 -4 -4 4 199.08 10.70 -4 -4 4 200.98 9.90 -4 4 4 181.38 11.70 4 4 -4 202.38 9.70 -4 4 4 203.58 7.90 4 4 -4 196.78 10.50 4 4 -4 199.98 11.10 4 4 -4 193.68 9.90 4 4 -4 201.18 9.60 -4 4 4 193.38 7.20 4 4 -4 223.38 11.30 -4 4 4 188.48 10.40 -4 4 4 193.48 12.50 -4 4 4 207.88 10.80 4 4 -4 200.98 9.80 -4 4 4 224.88 13.00 4 4 -4 215.78 10.70 -4 4 4 192.18 12.00 4 4 -4 206.28 10.70 4 4 -4 205.48 10.70 -4 4 4 185.78 9.60 -2 -4 4 13.90 2.30 -2 -4 4 9.10 2.50 2 -4 -4 10.40 2.50 -2 -4 4 10.30 2.80 -2 -4 4 11.20 2.60 -2 -4 4 5.00 2.10 2 -4 -4 13.30 2.90 -2 -4 4 11.00 2.60 -2 -4 4 8.60 2.40 2 -4 -4 10.10 2.50 2 -4 -4 7.90 2.70 2 -4 -4 12.20 2.30 2 -4 -4 8.20 3.10 2 4 -4 11.90 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4 2.80 1.30 -10 4 -4 4.90 1.40 10 4 4 8.30 3.20 -10 4 -4 8.30 1.80 10 4 4 5.40 2.60 12 -4 4 143.49 12.40 -12 -4 -4 159.58 12.10 -12 -4 -4 152.18 12.00 12 -4 4 155.28 12.10 12 -4 4 161.08 13.00 -12 -4 -4 149.49 10.30 12 -4 4 154.98 7.60 -12 -4 -4 151.18 9.00 -12 4 -4 170.98 10.80 12 4 4 150.88 10.50 12 4 4 170.88 12.40 -12 4 -4 163.98 12.30 12 4 4 167.18 11.60 -14 -4 -4 214.58 14.20 14 -4 4 219.28 14.80 -14 -4 -4 204.08 14.20 14 -4 4 199.18 15.40 -14 -4 -4 218.98 11.60 14 -4 4 224.08 15.30 -14 4 -4 200.88 12.80 -14 4 -4 219.48 15.70 -14 4 -4 218.38 15.10 14 4 4 203.48 14.30 14 4 4 226.08 13.10 14 4 4 210.08 13.60 -16 -4 -4 24.70 6.20 16 -4 4 23.60 6.30 -16 -4 -4 39.40 7.00 16 -4 4 28.90 6.50 -16 4 -4 29.60 5.90 16 4 4 30.60 6.50 -16 4 -4 22.60 5.60 -16 4 -4 34.40 6.70 16 4 4 22.70 5.50 -18 -4 -4 -3.10 3.50 18 -4 4 4.30 4.80 -18 -4 -4 2.00 3.50 18 -4 4 -5.50 3.60 18 -4 4 -3.50 2.90 -18 4 -4 1.40 4.00 18 4 4 -2.00 2.80 -18 4 -4 1.80 2.60 18 4 4 2.10 2.80 -18 4 -4 -2.80 2.90 18 4 4 -2.30 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6.30 2.80 -29 5 4 -1.60 5.20 29 5 -4 -2.50 3.30 -29 5 4 -6.00 4.40 27 -5 -4 -5.50 4.00 -27 -5 4 4.10 4.10 27 -5 -4 -0.40 4.50 -27 -5 4 -4.90 1.80 -27 -5 4 -1.90 4.70 -27 5 4 -6.60 2.80 27 5 -4 -1.70 4.10 27 5 -4 -4.50 3.10 -27 5 4 -4.80 4.60 27 5 -4 -8.80 3.40 -25 -5 4 108.79 12.20 -25 -5 4 73.19 11.80 25 -5 -4 95.19 13.50 25 -5 -4 96.79 11.40 25 -5 -4 87.99 12.90 -25 -5 4 90.09 12.00 -25 5 4 69.59 11.70 25 5 -4 93.59 10.90 -25 5 4 95.99 12.70 25 5 -4 80.09 10.00 25 5 -4 98.39 11.90 -25 5 4 73.29 10.80 23 -5 -4 104.39 12.00 -23 -5 4 124.09 11.40 -23 -5 4 92.39 10.90 23 -5 -4 112.59 9.80 23 -5 -4 92.69 11.50 -23 -5 4 94.29 11.80 23 5 -4 103.89 11.70 23 5 -4 80.69 10.30 -23 5 4 74.99 10.60 23 5 -4 103.29 11.20 -23 5 4 102.29 12.10 -21 -5 4 289.37 17.00 -21 -5 4 279.77 19.10 21 -5 -4 294.17 16.20 21 -5 -4 295.07 20.60 -21 -5 4 281.17 17.50 21 -5 -4 275.57 18.70 -21 5 4 284.87 17.50 -21 5 4 261.17 18.50 21 5 -4 267.47 18.00 21 5 -4 289.57 17.10 -21 5 4 277.77 19.90 21 5 -4 295.17 17.50 19 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2 10 111.89 9.60 -20 2 10 129.79 9.70 20 2 -10 134.09 9.90 -20 2 10 131.99 7.50 18 -2 -10 207.38 12.70 -18 -2 10 190.68 13.90 18 -2 -10 208.28 13.30 -18 -2 10 210.78 11.80 -18 -2 10 205.08 10.60 -18 -2 10 217.18 13.80 18 -2 -10 201.98 11.20 -18 2 10 211.38 11.80 -18 2 10 217.68 14.10 -18 2 10 210.38 9.80 -18 2 10 199.18 12.60 18 2 -10 209.58 13.00 -18 2 10 202.98 11.70 -18 2 10 204.28 11.20 18 2 -10 209.68 12.20 -18 2 10 206.58 13.10 18 2 -10 191.58 11.70 18 2 -10 201.68 10.40 16 -2 -10 8.80 3.50 -16 -2 10 6.40 3.40 -16 -2 10 7.50 2.70 16 -2 -10 5.60 2.60 16 -2 -10 7.90 2.50 16 -2 -10 3.40 2.60 16 -2 -10 2.30 1.80 -16 -2 10 8.20 2.50 16 -2 -10 7.50 2.90 -16 -2 10 -0.40 2.30 16 2 -10 3.90 1.80 -16 2 10 2.80 2.60 -16 2 10 4.10 2.20 16 2 -10 4.30 2.80 -16 2 10 9.80 3.20 -16 2 10 5.80 2.20 -16 2 10 1.40 2.10 16 2 -10 6.20 2.50 16 2 -10 5.50 2.40 -16 2 10 4.40 2.80 -16 2 10 4.70 1.90 14 -2 -10 126.09 8.30 -14 -2 10 125.49 10.40 14 -2 -10 116.69 8.90 14 -2 -10 105.69 6.50 14 -2 -10 103.19 6.50 -14 -2 10 117.59 9.70 -14 -2 10 98.89 7.80 -14 -2 10 113.69 8.20 14 -2 -10 105.59 8.70 14 -2 -10 100.89 8.80 -14 -2 10 114.29 6.10 14 -2 -10 107.49 8.20 -14 2 10 111.69 8.10 -14 2 10 97.29 8.10 14 2 -10 119.29 6.10 -14 2 10 108.89 9.00 14 2 -10 120.09 9.20 -14 2 10 118.19 9.70 -14 2 10 105.89 8.70 14 2 -10 102.09 8.20 14 2 -10 113.99 7.90 -14 2 10 125.39 8.30 12 -2 -10 35.70 4.20 -12 -2 10 35.80 5.80 -12 -2 10 39.90 4.90 12 -2 -10 44.30 5.00 -12 -2 10 48.50 6.00 12 -2 -10 44.60 5.80 12 -2 -10 48.40 5.80 -12 -2 10 47.00 5.70 12 -2 -10 39.20 5.40 12 -2 -10 33.60 5.50 12 -2 -10 46.20 5.00 -12 -2 10 43.80 3.50 -12 2 10 41.70 6.20 -12 2 10 41.00 5.40 -12 2 10 45.20 4.90 12 2 -10 36.20 7.60 -12 2 10 48.70 6.10 12 2 -10 37.10 3.40 12 2 -10 44.80 5.80 12 2 -10 38.80 5.40 -12 2 10 36.40 4.90 -12 2 10 39.70 5.10 -10 -2 10 2.10 1.40 10 -2 -10 2.10 2.00 10 -2 -10 3.00 1.80 -10 -2 10 1.00 1.80 10 -2 -10 2.20 2.00 10 -2 -10 0.60 2.00 -10 -2 10 2.10 2.00 -10 -2 10 1.00 1.90 -10 -2 10 5.60 2.40 10 -2 -10 4.00 1.40 -10 -2 10 0.70 1.70 10 -2 -10 1.00 1.60 10 -2 -10 4.30 2.20 10 -2 -10 3.60 1.60 10 2 -10 1.90 1.80 -10 2 10 1.70 2.00 -10 2 10 2.40 2.00 -10 2 10 3.40 1.90 10 2 -10 1.80 1.90 10 2 -10 2.30 1.50 -10 2 10 1.60 1.60 -10 2 10 1.80 1.70 10 2 -10 3.20 1.70 10 2 -10 2.60 1.90 -8 -2 10 296.97 12.40 -8 -2 10 322.97 15.80 8 -2 -10 309.67 14.40 -8 -2 10 293.97 14.60 8 -2 -10 300.07 14.20 -8 -2 10 321.07 15.20 8 -2 -10 320.17 12.40 -8 -2 10 296.47 12.30 8 -2 -10 287.57 12.70 8 -2 -10 295.57 12.60 8 -2 -10 291.57 15.00 -8 -2 10 324.27 16.30 8 -2 -10 315.37 14.40 8 -2 -10 277.37 15.00 -8 2 10 291.27 14.80 8 2 -10 322.97 12.40 8 2 -10 309.47 12.30 -8 2 10 317.27 13.60 8 2 -10 305.07 15.80 8 2 -10 296.17 15.50 -8 2 10 302.07 14.20 -8 2 10 317.67 13.70 -8 2 10 311.67 14.30 -8 2 10 316.07 15.40 -8 2 10 310.37 14.10 8 2 -10 306.17 14.70 8 2 -10 299.97 14.60 6 -2 -10 74.79 7.10 -6 -2 10 61.29 6.50 6 -2 -10 77.79 7.20 6 -2 -10 85.69 6.10 6 -2 -10 75.69 5.90 -6 -2 10 80.39 5.70 6 -2 -10 88.89 6.80 6 -2 -10 70.19 7.30 -6 -2 10 73.99 7.40 -6 2 10 72.79 6.50 -6 2 10 66.19 6.50 -6 2 10 65.29 5.60 -6 2 10 71.09 6.90 6 2 -10 95.29 8.30 -6 2 10 74.29 6.30 -6 2 10 82.19 6.10 -6 2 10 63.59 6.70 6 2 -10 89.99 7.40 4 -2 -10 9.00 2.80 -4 -2 10 8.20 2.70 4 -2 -10 12.50 2.30 -4 -2 10 10.20 2.70 -4 -2 10 3.90 2.40 4 -2 -10 12.80 3.00 -4 -2 10 6.80 3.00 4 -2 -10 14.90 3.60 -4 -2 10 8.80 1.90 4 -2 -10 9.50 3.20 4 -2 -10 11.50 2.80 -4 2 10 12.60 3.30 -4 2 10 5.50 2.90 -4 2 10 6.30 2.40 -4 2 10 13.10 2.60 -4 2 10 7.40 2.80 4 2 -10 7.90 1.70 4 2 -10 11.90 2.80 -4 2 10 8.70 2.20 4 2 -10 8.00 2.50 4 2 -10 13.40 3.30 4 2 -10 10.40 3.00 4 2 -10 7.30 2.70 -4 2 10 8.80 2.70 -2 -2 10 16.10 3.80 -2 -2 10 13.20 2.10 2 -2 -10 13.00 3.50 2 -2 -10 16.00 3.10 2 -2 -10 14.90 3.60 2 -2 -10 18.00 3.80 -2 -2 10 10.60 3.10 2 -2 -10 20.20 4.10 -2 -2 10 14.60 3.70 2 -2 -10 15.00 3.20 -2 -2 10 14.70 3.60 -2 2 10 18.60 3.90 2 2 -10 18.20 3.70 -2 2 10 15.30 3.10 -2 2 10 15.20 3.40 2 2 -10 16.50 2.30 -2 2 10 16.60 3.10 2 2 -10 10.20 3.70 -2 2 10 11.50 3.50 -2 2 10 14.70 3.30 2 2 -10 21.50 4.40 2 2 -10 10.10 3.30 0 -2 10 167.28 10.30 0 -2 -10 175.48 9.30 0 -2 10 161.58 11.50 0 -2 -10 163.38 10.50 0 -2 -10 177.18 9.90 0 -2 10 159.08 10.80 0 -2 -10 190.48 11.60 0 -2 -10 148.39 10.00 0 -2 -10 169.28 11.10 0 -2 10 174.78 12.00 0 -2 10 171.28 7.70 0 2 -10 170.98 10.20 0 2 10 152.78 11.00 0 2 10 148.29 9.00 0 2 -10 154.18 7.20 0 2 10 167.88 10.50 0 2 10 164.18 11.40 0 2 -10 166.48 6.10 0 2 10 163.18 8.60 0 2 10 165.78 9.90 0 2 -10 148.69 10.10 0 2 -10 157.58 11.10 -2 -2 -10 181.18 11.10 2 -2 10 187.58 9.00 -2 -2 -10 185.98 12.20 -2 -2 -10 180.08 11.80 -2 -2 -10 170.88 9.90 -2 -2 -10 172.08 9.30 -2 -2 -10 173.88 9.70 2 -2 10 174.08 12.20 -2 -2 -10 181.88 11.20 2 -2 10 189.68 12.40 2 -2 10 196.48 12.70 2 -2 10 161.28 10.50 -2 2 -10 156.48 8.30 2 2 10 181.98 11.70 -2 2 -10 206.38 11.00 2 2 10 210.28 13.10 2 2 10 175.18 9.80 -2 2 -10 182.78 12.30 2 2 10 192.28 11.30 2 2 10 178.48 10.80 -4 -2 -10 29.30 5.50 -4 -2 -10 24.80 4.70 -4 -2 -10 31.40 4.50 -4 -2 -10 21.50 4.80 4 -2 10 29.30 5.70 -4 -2 -10 31.20 5.40 4 -2 10 28.80 5.30 4 -2 10 29.90 4.60 4 -2 10 24.60 4.30 -4 -2 -10 25.00 4.30 4 2 10 35.80 4.60 4 2 10 25.50 4.60 4 2 10 20.30 4.40 -4 2 -10 35.90 5.10 -4 2 -10 38.70 6.60 4 2 10 18.30 4.60 -4 2 -10 33.20 6.10 -4 2 -10 22.30 3.70 -6 -2 -10 52.59 5.90 -6 -2 -10 46.60 5.20 -6 -2 -10 58.89 7.20 -6 -2 -10 43.40 6.60 6 -2 10 48.90 6.80 -6 -2 -10 55.39 6.80 6 -2 10 31.50 6.20 6 -2 10 42.00 7.40 6 2 10 37.30 5.00 -6 2 -10 42.70 6.80 6 2 10 35.50 6.30 6 2 10 52.49 6.70 -6 2 -10 53.69 7.50 6 2 10 38.30 6.00 -6 2 -10 51.09 6.00 -8 -2 -10 19.90 5.20 -8 -2 -10 31.90 6.50 8 -2 10 26.50 5.60 8 -2 10 25.00 5.30 -8 -2 -10 25.80 4.30 8 -2 10 28.10 6.30 -8 -2 -10 32.10 4.50 8 2 10 26.50 6.20 -8 2 -10 27.20 6.00 -8 2 -10 25.30 5.70 8 2 10 24.00 4.10 8 2 10 22.10 4.50 -8 2 -10 21.00 4.20 -10 -2 -10 42.00 8.00 10 -2 10 38.10 7.40 10 -2 10 35.80 7.30 10 -2 10 38.30 6.30 -10 -2 -10 46.60 7.50 -10 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2 -21 4.30 5.90 -8 2 21 -7.80 5.70 8 2 -21 -1.70 2.60 6 -2 -21 12.10 4.30 -6 -2 21 7.70 8.00 -6 -2 21 -4.10 3.80 -6 -2 21 -5.90 4.70 6 2 -21 6.70 4.50 6 2 -21 0.50 4.60 -6 2 21 2.10 5.30 25 -3 -21 27.80 6.90 25 -3 -21 36.20 9.30 -25 -3 21 21.50 6.80 25 3 -21 21.90 6.60 -25 3 21 26.40 9.20 25 3 -21 25.50 10.90 25 3 -21 25.50 6.20 23 -3 -21 -3.40 3.80 -23 -3 21 -2.00 6.80 -23 -3 21 4.40 6.00 23 -3 -21 -2.00 5.90 23 3 -21 2.80 4.80 -23 3 21 9.60 5.90 23 3 -21 6.10 7.50 23 3 -21 15.30 4.90 21 -3 -21 1.40 5.10 21 -3 -21 -5.60 4.80 -21 -3 21 -4.70 4.80 -21 -3 21 4.60 5.30 -21 3 21 -1.40 4.40 21 3 -21 -4.50 3.60 -19 -3 21 -5.60 5.70 -19 -3 21 -7.90 3.70 19 -3 -21 4.60 4.80 19 -3 -21 -5.40 5.10 19 3 -21 2.90 7.50 -19 3 21 -7.50 4.70 19 3 -21 -2.20 3.60 17 -3 -21 6.10 5.40 -17 -3 21 -4.00 4.80 17 -3 -21 -5.30 3.30 -17 -3 21 -3.80 4.40 -17 3 21 9.80 4.90 17 3 -21 -10.90 5.50 -17 3 21 12.30 5.50 17 3 -21 -0.70 3.70 -15 -3 21 2.70 4.30 15 -3 -21 -2.00 5.60 15 -3 -21 5.90 3.40 -15 -3 21 -2.60 5.10 15 3 -21 -0.30 3.30 -15 3 21 -8.70 3.80 -15 3 21 -7.10 4.40 15 3 -21 -0.10 6.30 13 -3 -21 -4.20 3.80 -13 -3 21 -3.10 4.60 13 -3 -21 -8.30 5.50 -13 -3 21 0.70 4.40 -13 3 21 -2.30 3.50 -13 3 21 -9.10 5.60 13 3 -21 -4.40 3.20 13 3 -21 -0.50 5.50 11 -3 -21 1.80 4.50 -11 -3 21 -5.10 4.50 11 3 -21 5.00 2.90 11 3 -21 -2.10 4.20 -11 3 21 -9.40 7.80 -11 3 21 6.90 4.30 -9 -3 21 -5.00 4.40 9 -3 -21 -0.40 4.10 -9 -3 21 9.20 4.70 9 3 -21 -3.30 4.00 -9 3 21 -8.60 7.40 9 3 -21 4.60 4.90 -20 -4 21 0.70 5.50 20 -4 -21 9.80 7.60 -20 4 21 11.30 6.30 20 4 -21 16.50 7.60 20 4 -21 7.60 6.10 -18 -4 21 -1.20 5.30 -18 -4 21 5.90 3.70 18 -4 -21 2.50 4.90 18 -4 -21 1.30 4.70 -18 4 21 0.20 6.20 18 4 -21 8.30 3.70 18 4 -21 -4.50 6.50 16 -4 -21 7.70 6.20 16 -4 -21 6.50 5.10 -16 -4 21 8.30 4.50 16 4 -21 5.00 4.80 -16 4 21 14.20 4.50 -16 4 21 6.70 8.70 16 4 -21 2.50 6.10 -14 -4 21 -3.40 5.70 14 -4 -21 7.20 5.40 14 4 -21 5.20 7.40 24 0 -22 -3.00 3.70 24 0 -22 -3.30 4.80 -24 0 22 -2.50 4.70 -22 0 22 -9.00 4.80 22 0 -22 -0.50 3.80 -22 0 22 -2.10 3.80 22 0 -22 -11.60 4.60 20 0 -22 -0.40 5.50 -20 0 22 7.90 5.80 20 0 -22 -5.40 4.40 20 0 -22 -6.80 9.50 -20 0 22 -2.80 5.50 18 0 -22 47.90 10.90 -18 0 22 24.60 6.00 -18 0 22 32.90 9.20 18 0 -22 32.00 6.90 -16 0 22 9.40 6.30 16 0 -22 19.80 7.10 16 0 -22 11.00 9.10 14 0 -22 10.20 6.90 14 0 -22 8.40 4.20 -14 0 22 6.60 6.20 -12 0 22 -4.60 4.60 12 0 -22 -9.70 7.10 12 0 -22 -0.70 4.30 10 0 -22 4.40 6.60 10 0 -22 -2.90 4.50 -10 0 22 7.20 7.60 -23 -1 22 -2.90 5.20 -23 -1 22 -2.20 4.40 23 -1 -22 3.30 5.00 -23 1 22 -7.50 3.20 -23 1 22 -0.40 4.80 23 1 -22 -5.50 3.20 23 1 -22 -0.80 8.30 -21 -1 22 -1.70 4.60 -21 -1 22 5.00 5.20 21 -1 -22 -5.00 4.10 21 -1 -22 -5.10 5.90 -21 1 22 -6.30 4.70 21 1 -22 -0.90 3.60 21 1 -22 -8.20 8.00 -21 1 22 3.20 3.50 -19 -1 22 -4.00 4.80 -19 -1 22 5.50 4.40 19 -1 -22 -1.70 5.40 -19 1 22 -4.10 4.20 19 1 -22 -5.70 7.70 19 1 -22 7.80 5.70 -17 -1 22 4.00 4.60 -17 -1 22 14.80 4.40 17 -1 -22 5.60 4.90 -17 1 22 10.10 5.80 17 1 -22 4.30 4.80 17 1 -22 9.90 7.60 -15 -1 22 15.30 5.60 15 -1 -22 14.10 5.70 -15 -1 22 9.10 6.50 15 1 -22 10.90 6.20 -15 1 22 16.60 6.40 13 -1 -22 -9.40 5.80 -13 -1 22 4.50 5.20 13 -1 -22 -0.70 5.20 -13 -1 22 5.60 4.00 13 1 -22 5.00 3.80 -13 1 22 -17.00 7.10 -13 1 22 7.70 4.10 13 1 -22 -1.70 7.60 -11 -1 22 1.80 4.20 11 -1 -22 1.50 6.80 -11 -1 22 -0.20 4.90 11 -1 -22 -0.20 3.70 -11 1 22 -7.30 4.20 11 1 -22 -7.40 3.20 -11 1 22 5.00 6.10 11 1 -22 -5.00 6.10 22 -2 -22 -5.10 4.80 -22 2 22 -3.40 4.50 22 2 -22 -5.40 4.10 22 2 -22 -8.60 6.30 20 -2 -22 0.10 4.90 20 -2 -22 7.10 4.40 -20 -2 22 -4.90 4.80 -20 -2 22 -8.20 4.40 20 2 -22 17.60 7.10 20 2 -22 -10.80 5.10 -20 2 22 2.00 4.60 -18 -2 22 2.00 5.90 -18 -2 22 -6.10 4.40 18 -2 -22 -1.90 5.90 -18 2 22 -2.60 4.10 18 2 -22 10.50 4.60 18 2 -22 -11.30 7.90 -16 -2 22 -2.40 5.90 -16 -2 22 9.60 6.90 16 -2 -22 5.60 5.30 16 2 -22 -0.20 6.20 -16 2 22 1.60 3.20 -14 -2 22 -2.80 3.80 -14 -2 22 0.70 4.30 14 2 -22 7.50 5.00 14 2 -22 -5.90 6.40 -14 2 22 -10.20 4.20 -14 2 22 -14.00 6.50 12 -2 -22 0.20 4.40 -12 2 22 8.30 6.50 12 2 -22 -3.60 3.40 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 30265 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn1 Zn 0.500000 0.82026(6) 0.750000 0.0491(2) Uani 1 2 d S T P . . S1 S 0.42736(3) 0.88309(10) 0.74148(6) 0.0545(3) Uani 1 1 d . . . . . N2 N 0.41164(10) 0.6672(3) 0.63200(18) 0.0490(7) Uani 1 1 d . . . . . N1 N 0.45969(10) 0.6945(3) 0.65251(17) 0.0479(7) Uani 1 1 d . . . . . N3 N 0.34911(10) 0.7278(3) 0.65799(18) 0.0515(7) Uani 1 1 d . . . . . H3 H 0.341136 0.778806 0.687489 0.062 Uiso 1 1 calc R U . . . O2 O 0.30286(14) -0.0800(4) 0.7269(2) 0.0942(11) Uani 1 1 d . . . . . O1 O 0.17834(11) 0.6084(4) 0.5241(2) 0.0945(11) Uani 1 1 d . . . . . C16 C 0.39570(12) 0.7479(4) 0.6713(2) 0.0442(8) Uani 1 1 d . . . . . C14 C 0.45013(12) 0.5502(4) 0.5366(2) 0.0508(9) Uani 1 1 d . . . . . C17 C 0.31150(13) 0.6363(4) 0.6034(2) 0.0508(8) Uani 1 1 d . . . . . C15 C 0.47609(13) 0.6398(4) 0.6083(2) 0.0533(9) Uani 1 1 d . . . . . H15 H 0.508735 0.659592 0.623627 0.064 Uiso 1 1 calc R U . . . C22 C 0.26460(13) 0.6661(4) 0.5917(2) 0.0548(9) Uani 1 1 d . . . . . H22 H 0.259896 0.741322 0.619250 0.066 Uiso 1 1 calc R U . . . C13 C 0.44291(14) 0.6059(5) 0.4632(2) 0.0579(10) Uani 1 1 d . . . . . N4 N 0.27463(17) 0.1472(5) 0.7019(3) 0.0877(12) Uani 1 1 d . . . . . C1 C 0.43629(13) 0.4083(4) 0.5419(2) 0.0565(9) Uani 1 1 d . . . . . C21 C 0.22531(15) 0.5851(5) 0.5396(3) 0.0663(11) Uani 1 1 d . . . . . C8 C 0.42053(15) 0.5181(6) 0.3934(2) 0.0718(13) Uani 1 1 d . . . . . C6 C 0.41473(15) 0.3212(5) 0.4721(3) 0.0710(12) Uani 1 1 d . . . . . C7 C 0.40691(16) 0.3787(6) 0.4001(3) 0.0782(14) Uani 1 1 d . . . . . H7 H 0.391967 0.321996 0.354552 0.094 Uiso 1 1 calc R U . . . C18 C 0.31871(16) 0.5220(5) 0.5637(3) 0.0716(12) Uani 1 1 d . . . . . H18 H 0.349906 0.498887 0.572043 0.086 Uiso 1 1 calc R U . . . C2 C 0.44531(17) 0.3450(5) 0.6159(3) 0.0711(12) Uani 1 1 d . . . . . H2 H 0.459584 0.399713 0.662312 0.085 Uiso 1 1 calc R U . . . C20 C 0.23181(17) 0.4739(5) 0.4983(3) 0.0823(14) Uani 1 1 d . . . . . H20 H 0.205118 0.420285 0.462081 0.099 Uiso 1 1 calc R U . . . C12 C 0.45651(16) 0.7492(5) 0.4561(3) 0.0743(12) Uani 1 1 d . . . . . H12 H 0.470807 0.808579 0.500703 0.089 Uiso 1 1 calc R U . . . C26 C 0.3079(2) 0.0459(6) 0.7192(3) 0.0878(14) Uani 1 1 d . . . . . H26 H 0.338313 0.074803 0.726034 0.105 Uiso 1 1 calc R U . . . C19 C 0.27799(19) 0.4431(6) 0.5112(3) 0.0883(15) Uani 1 1 d . . . . . H19 H 0.282314 0.366735 0.483861 0.106 Uiso 1 1 calc R U . . . C3 C 0.4333(2) 0.2065(6) 0.6192(4) 0.0940(16) Uani 1 1 d . . . . . H3A H 0.439848 0.166745 0.667984 0.113 Uiso 1 1 calc R U . . . C5 C 0.4023(2) 0.1752(6) 0.4793(4) 0.0941(17) Uani 1 1 d . . . . . H5 H 0.387952 0.116851 0.434250 0.113 Uiso 1 1 calc R U . . . C23 C 0.17017(18) 0.7120(7) 0.5701(4) 0.0987(17) Uani 1 1 d . . . . . H23A H 0.135814 0.716168 0.553953 0.148 Uiso 1 1 calc R U . . . H23B H 0.180990 0.804204 0.562280 0.148 Uiso 1 1 calc R U . . . H23C H 0.188155 0.686342 0.625544 0.148 Uiso 1 1 calc R U . . . C10 C 0.4263(3) 0.7085(10) 0.3152(4) 0.116(2) Uani 1 1 d . . . . . H10 H 0.420963 0.743642 0.266153 0.140 Uiso 1 1 calc R U . . . C9 C 0.4131(2) 0.5754(9) 0.3201(3) 0.1017(19) Uani 1 1 d . . . . . H9 H 0.398635 0.518689 0.274449 0.122 Uiso 1 1 calc R U . . . C11 C 0.4484(2) 0.7987(7) 0.3837(4) 0.1013(19) Uani 1 1 d . . . . . H11 H 0.457457 0.891931 0.378945 0.122 Uiso 1 1 calc R U . . . C4 C 0.4113(2) 0.1227(6) 0.5502(5) 0.110(2) Uani 1 1 d . . . . . H4 H 0.402664 0.028393 0.553566 0.131 Uiso 1 1 calc R U . . . C24 C 0.2265(2) 0.1136(8) 0.6895(5) 0.129(2) Uani 1 1 d . . . . . H24A H 0.216248 0.022940 0.662567 0.194 Uiso 1 1 calc R U . . . H24B H 0.204013 0.187099 0.657473 0.194 Uiso 1 1 calc R U . . . H24C H 0.227066 0.108168 0.740069 0.194 Uiso 1 1 calc R U . . . C25 C 0.2848(3) 0.2961(7) 0.6937(6) 0.162(3) Uani 1 1 d . . . . . H25A H 0.287699 0.349673 0.738766 0.243 Uiso 1 1 calc R U . . . H25B H 0.258426 0.334805 0.645623 0.243 Uiso 1 1 calc R U . . . H25C H 0.314837 0.302703 0.691406 0.243 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn1 0.0431(3) 0.0472(4) 0.0549(4) 0.000 0.0218(3) 0.000 S1 0.0483(5) 0.0490(5) 0.0669(6) -0.0108(4) 0.0283(5) 0.0015(4) N2 0.0405(15) 0.0533(17) 0.0557(17) -0.0078(14) 0.0252(14) -0.0020(13) N1 0.0415(15) 0.0496(17) 0.0556(17) -0.0013(14) 0.0256(14) 0.0020(13) N3 0.0434(16) 0.0562(18) 0.0619(19) -0.0117(15) 0.0309(14) 0.0001(14) O2 0.107(3) 0.068(2) 0.129(3) -0.012(2) 0.074(2) 0.000(2) O1 0.0470(17) 0.106(3) 0.119(3) -0.017(2) 0.0308(18) -0.0105(17) C16 0.0441(18) 0.0426(19) 0.0472(19) 0.0009(15) 0.0231(16) 0.0053(15) C14 0.0430(18) 0.061(2) 0.057(2) -0.0066(18) 0.0309(17) 0.0044(17) C17 0.049(2) 0.052(2) 0.053(2) -0.0035(17) 0.0261(17) -0.0054(16) C15 0.0454(19) 0.058(2) 0.062(2) -0.0071(18) 0.0305(18) 0.0006(17) C22 0.047(2) 0.057(2) 0.063(2) -0.0009(18) 0.0281(18) -0.0022(17) C13 0.048(2) 0.071(3) 0.062(2) 0.006(2) 0.0318(19) 0.0164(19) N4 0.094(3) 0.073(3) 0.095(3) -0.005(2) 0.044(3) 0.005(2) C1 0.049(2) 0.061(2) 0.067(2) -0.0082(19) 0.0346(19) 0.0016(18) C21 0.050(2) 0.070(3) 0.077(3) -0.001(2) 0.029(2) -0.008(2) C8 0.056(2) 0.106(4) 0.056(2) 0.000(2) 0.028(2) 0.026(2) C6 0.056(2) 0.078(3) 0.082(3) -0.022(2) 0.035(2) -0.003(2) C7 0.059(3) 0.099(4) 0.068(3) -0.027(3) 0.024(2) 0.007(3) C18 0.064(2) 0.066(3) 0.098(3) -0.027(2) 0.049(2) -0.015(2) C2 0.084(3) 0.065(3) 0.083(3) -0.003(2) 0.054(3) 0.000(2) C20 0.066(3) 0.083(3) 0.095(3) -0.027(3) 0.036(3) -0.026(2) C12 0.070(3) 0.082(3) 0.085(3) 0.020(3) 0.049(3) 0.017(2) C26 0.080(3) 0.085(4) 0.104(4) -0.018(3) 0.048(3) -0.007(3) C19 0.087(3) 0.080(3) 0.110(4) -0.042(3) 0.057(3) -0.022(3) C3 0.122(5) 0.070(3) 0.119(4) 0.004(3) 0.082(4) -0.007(3) C5 0.091(4) 0.075(3) 0.119(5) -0.038(3) 0.052(4) -0.029(3) C23 0.061(3) 0.118(5) 0.123(5) -0.004(4) 0.049(3) 0.007(3) C10 0.120(5) 0.164(7) 0.080(4) 0.041(5) 0.060(4) 0.044(5) C9 0.097(4) 0.148(6) 0.062(3) 0.010(4) 0.039(3) 0.040(4) C11 0.101(4) 0.106(4) 0.120(5) 0.049(4) 0.071(4) 0.035(3) C4 0.122(5) 0.071(4) 0.160(6) -0.015(4) 0.087(5) -0.027(3) C24 0.106(5) 0.138(6) 0.165(7) -0.011(5) 0.082(5) 0.018(4) C25 0.192(9) 0.070(4) 0.204(9) 0.010(5) 0.078(7) 0.001(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Zn1 N1 109.95(16) . 2_656 ? N1 Zn1 S1 111.60(8) . 2_656 ? N1 Zn1 S1 85.92(8) 2_656 2_656 ? N1 Zn1 S1 85.92(8) . . ? N1 Zn1 S1 111.59(8) 2_656 . ? S1 Zn1 S1 150.02(6) 2_656 . ? C16 S1 Zn1 92.48(11) . . ? C16 N2 N1 112.8(3) . . ? C15 N1 N2 117.4(3) . . ? C15 N1 Zn1 124.3(2) . . ? N2 N1 Zn1 118.2(2) . . ? C16 N3 C17 130.5(3) . . ? C16 N3 H3 114.8 . . ? C17 N3 H3 114.8 . . ? C21 O1 C23 118.0(4) . . ? N2 C16 N3 118.3(3) . . ? N2 C16 S1 128.2(3) . . ? N3 C16 S1 113.4(2) . . ? C1 C14 C13 120.6(4) . . ? C1 C14 C15 121.1(3) . . ? C13 C14 C15 118.1(4) . . ? C18 C17 C22 119.8(3) . . ? C18 C17 N3 124.8(3) . . ? C22 C17 N3 115.3(3) . . ? N1 C15 C14 128.6(3) . . ? N1 C15 H15 115.7 . . ? C14 C15 H15 115.7 . . ? C21 C22 C17 120.4(4) . . ? C21 C22 H22 119.8 . . ? C17 C22 H22 119.8 . . ? C14 C13 C12 121.8(4) . . ? C14 C13 C8 119.5(4) . . ? C12 C13 C8 118.7(4) . . ? C26 N4 C24 121.1(5) . . ? C26 N4 C25 121.8(6) . . ? C24 N4 C25 117.1(6) . . ? C14 C1 C6 119.4(4) . . ? C14 C1 C2 122.5(4) . . ? C6 C1 C2 118.1(4) . . ? O1 C21 C22 124.0(4) . . ? O1 C21 C20 115.7(4) . . ? C22 C21 C20 120.3(4) . . ? C7 C8 C9 122.2(5) . . ? C7 C8 C13 118.7(4) . . ? C9 C8 C13 119.0(5) . . ? C7 C6 C1 119.2(4) . . ? C7 C6 C5 122.2(5) . . ? C1 C6 C5 118.5(5) . . ? C6 C7 C8 122.5(4) . . ? C6 C7 H7 118.7 . . ? C8 C7 H7 118.7 . . ? C17 C18 C19 118.1(4) . . ? C17 C18 H18 121.0 . . ? C19 C18 H18 121.0 . . ? C3 C2 C1 120.8(5) . . ? C3 C2 H2 119.6 . . ? C1 C2 H2 119.6 . . ? C19 C20 C21 119.1(4) . . ? C19 C20 H20 120.4 . . ? C21 C20 H20 120.4 . . ? C11 C12 C13 119.7(5) . . ? C11 C12 H12 120.2 . . ? C13 C12 H12 120.2 . . ? O2 C26 N4 126.5(5) . . ? O2 C26 H26 116.7 . . ? N4 C26 H26 116.7 . . ? C20 C19 C18 122.3(4) . . ? C20 C19 H19 118.9 . . ? C18 C19 H19 118.9 . . ? C2 C3 C4 120.7(6) . . ? C2 C3 H3A 119.7 . . ? C4 C3 H3A 119.7 . . ? C4 C5 C6 120.4(5) . . ? C4 C5 H5 119.8 . . ? C6 C5 H5 119.8 . . ? O1 C23 H23A 109.5 . . ? O1 C23 H23B 109.5 . . ? H23A C23 H23B 109.5 . . ? O1 C23 H23C 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? C9 C10 C11 121.2(6) . . ? C9 C10 H10 119.4 . . ? C11 C10 H10 119.4 . . ? C10 C9 C8 121.1(6) . . ? C10 C9 H9 119.5 . . ? C8 C9 H9 119.5 . . ? C12 C11 C10 120.3(6) . . ? C12 C11 H11 119.9 . . ? C10 C11 H11 119.9 . . ? C5 C4 C3 121.4(5) . . ? C5 C4 H4 119.3 . . ? C3 C4 H4 119.3 . . ? N4 C24 H24A 109.5 . . ? N4 C24 H24B 109.5 . . ? H24A C24 H24B 109.5 . . ? N4 C24 H24C 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? N4 C25 H25A 109.5 . . ? N4 C25 H25B 109.5 . . ? H25A C25 H25B 109.5 . . ? N4 C25 H25C 109.5 . . ? H25A C25 H25C 109.5 . . ? H25B C25 H25C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zn1 N1 2.042(3) . ? Zn1 N1 2.042(3) 2_656 ? Zn1 S1 2.2629(9) 2_656 ? Zn1 S1 2.2629(9) . ? S1 C16 1.756(3) . ? N2 C16 1.316(4) . ? N2 N1 1.374(4) . ? N1 C15 1.284(4) . ? N3 C16 1.359(4) . ? N3 C17 1.418(5) . ? N3 H3 0.8600 . ? O2 C26 1.202(6) . ? O1 C21 1.361(5) . ? O1 C23 1.410(6) . ? C14 C1 1.408(5) . ? C14 C13 1.408(5) . ? C14 C15 1.470(5) . ? C17 C18 1.386(5) . ? C17 C22 1.393(5) . ? C15 H15 0.9300 . ? C22 C21 1.372(5) . ? C22 H22 0.9300 . ? C13 C12 1.427(6) . ? C13 C8 1.429(6) . ? N4 C26 1.320(6) . ? N4 C24 1.433(7) . ? N4 C25 1.448(7) . ? C1 C6 1.424(6) . ? C1 C2 1.429(6) . ? C21 C20 1.376(6) . ? C8 C7 1.391(7) . ? C8 C9 1.409(7) . ? C6 C7 1.385(7) . ? C6 C5 1.438(7) . ? C7 H7 0.9300 . ? C18 C19 1.389(6) . ? C18 H18 0.9300 . ? C2 C3 1.353(6) . ? C2 H2 0.9300 . ? C20 C19 1.366(6) . ? C20 H20 0.9300 . ? C12 C11 1.363(7) . ? C12 H12 0.9300 . ? C26 H26 0.9300 . ? C19 H19 0.9300 . ? C3 C4 1.397(8) . ? C3 H3A 0.9300 . ? C5 C4 1.338(8) . ? C5 H5 0.9300 . ? C23 H23A 0.9600 . ? C23 H23B 0.9600 . ? C23 H23C 0.9600 . ? C10 C9 1.323(9) . ? C10 C11 1.424(9) . ? C10 H10 0.9300 . ? C9 H9 0.9300 . ? C11 H11 0.9300 . ? C4 H4 0.9300 . ? C24 H24A 0.9600 . ? C24 H24B 0.9600 . ? C24 H24C 0.9600 . ? C25 H25A 0.9600 . ? C25 H25B 0.9600 . ? C25 H25C 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C16 N2 N1 C15 -168.3(3) . . . . ? C16 N2 N1 Zn1 11.1(4) . . . . ? N1 N2 C16 N3 -178.0(3) . . . . ? N1 N2 C16 S1 1.8(5) . . . . ? C17 N3 C16 N2 -4.2(6) . . . . ? C17 N3 C16 S1 176.0(3) . . . . ? Zn1 S1 C16 N2 -11.1(3) . . . . ? Zn1 S1 C16 N3 168.7(2) . . . . ? C16 N3 C17 C18 15.9(6) . . . . ? C16 N3 C17 C22 -165.3(4) . . . . ? N2 N1 C15 C14 0.3(6) . . . . ? Zn1 N1 C15 C14 -179.0(3) . . . . ? C1 C14 C15 N1 -69.9(5) . . . . ? C13 C14 C15 N1 115.0(4) . . . . ? C18 C17 C22 C21 -1.6(6) . . . . ? N3 C17 C22 C21 179.5(4) . . . . ? C1 C14 C13 C12 179.9(3) . . . . ? C15 C14 C13 C12 -5.0(5) . . . . ? C1 C14 C13 C8 1.1(5) . . . . ? C15 C14 C13 C8 176.1(3) . . . . ? C13 C14 C1 C6 -0.1(5) . . . . ? C15 C14 C1 C6 -175.0(3) . . . . ? C13 C14 C1 C2 176.6(4) . . . . ? C15 C14 C1 C2 1.7(5) . . . . ? C23 O1 C21 C22 -6.9(7) . . . . ? C23 O1 C21 C20 174.2(5) . . . . ? C17 C22 C21 O1 -179.1(4) . . . . ? C17 C22 C21 C20 -0.2(7) . . . . ? C14 C13 C8 C7 -0.7(5) . . . . ? C12 C13 C8 C7 -179.5(4) . . . . ? C14 C13 C8 C9 179.4(4) . . . . ? C12 C13 C8 C9 0.6(6) . . . . ? C14 C1 C6 C7 -1.3(6) . . . . ? C2 C1 C6 C7 -178.2(4) . . . . ? C14 C1 C6 C5 178.0(4) . . . . ? C2 C1 C6 C5 1.1(6) . . . . ? C1 C6 C7 C8 1.8(6) . . . . ? C5 C6 C7 C8 -177.5(4) . . . . ? C9 C8 C7 C6 179.1(4) . . . . ? C13 C8 C7 C6 -0.8(6) . . . . ? C22 C17 C18 C19 1.9(7) . . . . ? N3 C17 C18 C19 -179.3(4) . . . . ? C14 C1 C2 C3 -177.2(4) . . . . ? C6 C1 C2 C3 -0.5(6) . . . . ? O1 C21 C20 C19 -179.5(5) . . . . ? C22 C21 C20 C19 1.5(8) . . . . ? C14 C13 C12 C11 -179.5(4) . . . . ? C8 C13 C12 C11 -0.7(6) . . . . ? C24 N4 C26 O2 -0.6(9) . . . . ? C25 N4 C26 O2 -179.8(7) . . . . ? C21 C20 C19 C18 -1.1(9) . . . . ? C17 C18 C19 C20 -0.6(8) . . . . ? C1 C2 C3 C4 -0.8(8) . . . . ? C7 C6 C5 C4 178.7(5) . . . . ? C1 C6 C5 C4 -0.5(8) . . . . ? C11 C10 C9 C8 0.0(10) . . . . ? C7 C8 C9 C10 179.9(5) . . . . ? C13 C8 C9 C10 -0.2(8) . . . . ? C13 C12 C11 C10 0.4(7) . . . . ? C9 C10 C11 C12 0.0(9) . . . . ? C6 C5 C4 C3 -0.8(10) . . . . ? C2 C3 C4 C5 1.5(10) . . . . ?