#------------------------------------------------------------------------------ #$Date: 2024-12-03 01:34:10 +0200 (Tue, 03 Dec 2024) $ #$Revision: 296183 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/96/7249654.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7249654 loop_ _publ_author_name 'Baraboshkin, Nikita' 'Zelenov, Victor Petrovich' 'Fedyanin, Ivan V.' 'Samigullina, Aida I.' 'Klenov, Michael S.' _publ_section_title ; Cocrystals of [1,2,5]oxadiazolo[3,4-c]cinnoline 5-oxides and 1,5-dioxides: step-by-step development of crystal engineering of energetic materials ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D4CE01081G _journal_year 2024 _chemical_formula_moiety '2(C8 H3 N5 O5), C6 N6 O6' _chemical_formula_sum 'C22 H6 N16 O16' _chemical_formula_weight 750.43 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_method 'Modified SHELXL output' _audit_update_record ; 2024-11-25 deposited with the CCDC. 2024-12-02 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 92.843(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 6.51400(10) _cell_length_b 32.5430(8) _cell_length_c 12.9337(3) _cell_measurement_reflns_used 5068 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 78.1240 _cell_measurement_theta_min 5.4120 _cell_volume 2738.38(10) _computing_cell_refinement 'CrysAlisPro 1.171.43.104a (Rigaku OD, 2023)' _computing_data_collection 'CrysAlisPro system (CCD 43.103a 64-bit (release 20-12-2023))' _computing_data_reduction 'CrysAlisPro 1.171.43.104a (Rigaku OD, 2023)' _computing_molecular_graphics 'SHELXTL (Sheldrick, 2008)' _computing_publication_material 'SHELXTL (Sheldrick, 2008)' _computing_structure_refinement 'ShelXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100(2) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.992 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -74.00 30.00 0.50 1.40 -- -44.13 84.00 25.00 208 2 \w -16.00 20.00 0.50 1.40 -- 44.13 -84.00 -94.00 72 3 \w -98.00 -73.00 0.50 6.00 -- -96.00 84.00 25.00 50 4 \w 61.00 89.00 0.50 6.00 -- 117.50 -84.00 -94.00 56 5 \w 137.00 176.00 0.50 6.00 -- 117.50 84.00 25.00 78 6 \w 103.00 130.00 0.50 6.00 -- 117.50 84.00 25.00 54 7 \w -42.00 18.00 0.50 1.40 -- -44.13 38.00 150.00 120 8 \w -32.00 27.00 0.50 1.40 -- 44.13 -19.00 -90.00 118 9 \w 17.00 113.00 0.50 1.40 -- 44.13 77.00 0.00 192 10 \w -141.00 -82.00 0.50 6.00 -- -96.00 -84.00 -94.00 118 11 \w 72.00 98.00 0.50 6.00 -- 117.50 -95.00 -30.00 52 12 \w 111.00 139.00 0.50 6.00 -- 117.50 30.00 -60.00 56 13 \w 45.00 70.00 0.50 6.00 -- 117.50 -77.00 60.00 50 14 \w 139.00 178.00 0.50 6.00 -- 117.50 15.00 -90.00 78 15 \w 47.00 91.00 0.50 6.00 -- 117.50 -77.00 30.00 88 16 \w 45.00 70.00 0.50 6.00 -- 117.50 -61.00 -30.00 50 17 \w 97.00 145.00 0.50 6.00 -- 117.50 61.00 -30.00 96 18 \w 46.00 88.00 0.50 6.00 -- 117.50 -77.00 -30.00 84 19 \w 87.00 130.00 0.50 6.00 -- 117.50 15.00-150.00 86 20 \w 141.00 177.00 0.50 6.00 -- 117.50 15.00-150.00 72 21 \w 122.00 148.00 0.50 6.00 -- 117.50 30.00 120.00 52 22 \w 94.00 121.00 0.50 6.00 -- 117.50 15.00 -90.00 54 23 \w 98.00 152.00 0.50 6.00 -- 117.50 45.00 -30.00 108 24 \w 128.00 154.00 0.50 6.00 -- 117.50 125.00 120.00 52 25 \w 98.00 144.00 0.50 6.00 -- 117.50 45.00 -90.00 92 26 \w 88.00 114.00 0.50 6.00 -- 117.50 15.00 0.00 52 27 \w 146.00 178.00 0.50 6.00 -- 117.50 15.00 0.00 64 28 \w 46.00 90.00 0.50 6.00 -- 117.50 -77.00-150.00 88 29 \w 99.00 173.00 0.50 6.00 -- 117.50 45.00-180.00 148 30 \w 74.00 105.00 0.50 6.00 -- 117.50 -77.00 -90.00 62 31 \w 61.00 93.00 0.50 6.00 -- 117.50-125.00 0.00 64 32 \w 45.00 70.00 0.50 6.00 -- 117.50 -61.00 30.00 50 33 \w 46.00 83.00 0.50 6.00 -- 117.50 -77.00-180.00 74 34 \w 47.00 111.00 0.50 6.00 -- 117.50-125.00 150.00 128 35 \w 70.00 96.00 0.50 6.00 -- 117.50 -81.00 171.11 52 36 \w 103.00 146.00 0.50 6.00 -- 117.50 -81.00 171.11 86 37 \w 69.00 109.00 0.50 6.00 -- 117.50-125.00-150.00 80 38 \w 45.00 147.00 0.50 6.00 -- 117.50 -83.00 134.53 204 39 \w 59.00 99.00 0.50 6.00 -- 117.50 -95.00-180.00 80 40 \w 48.00 75.00 0.50 6.00 -- 117.50-125.00 -30.00 54 41 \w 50.00 76.00 0.50 6.00 -- 117.50-125.00 30.00 52 42 \w 105.00 131.00 0.50 6.00 -- 117.50 45.00-150.00 52 43 \w 125.00 163.00 0.50 6.00 -- 117.50 30.00-150.00 76 44 \w 97.00 124.00 0.50 6.00 -- 117.50 61.00 150.00 54 45 \w 136.00 176.00 0.50 6.00 -- 117.50 61.00 150.00 80 46 \w 119.00 145.00 0.50 6.00 -- 117.50 77.00 -60.00 52 47 \w 81.00 107.00 0.50 6.00 -- 117.50 -82.00 -15.10 52 48 \w 89.00 115.00 0.50 6.00 -- 117.50 -84.00-152.74 52 49 \w 77.00 103.00 0.50 6.00 -- 117.50 8.00 99.67 52 50 \w 108.00 147.00 0.50 6.00 -- 117.50 -84.00 -94.00 78 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0678983000 _diffrn_orient_matrix_UB_12 0.0342481000 _diffrn_orient_matrix_UB_13 -0.0765163000 _diffrn_orient_matrix_UB_21 0.0972122000 _diffrn_orient_matrix_UB_22 -0.0236141000 _diffrn_orient_matrix_UB_23 -0.0884653000 _diffrn_orient_matrix_UB_31 -0.2048956000 _diffrn_orient_matrix_UB_32 -0.0225881000 _diffrn_orient_matrix_UB_33 -0.0234659000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0204 _diffrn_reflns_av_unetI/netI 0.0188 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.992 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 41 _diffrn_reflns_limit_k_min -40 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_number 30352 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.992 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 80.811 _diffrn_reflns_theta_min 2.716 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 1.404 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.587 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.43.104a (Rigaku Oxford Diffraction, 2023) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.820 _exptl_crystal_description prism _exptl_crystal_F_000 1512 _exptl_crystal_size_max 0.280 _exptl_crystal_size_mid 0.120 _exptl_crystal_size_min 0.050 _refine_diff_density_max 0.985 _refine_diff_density_min -0.694 _refine_diff_density_rms 0.087 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.058 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 814 _refine_ls_number_reflns 5983 _refine_ls_number_restraints 649 _refine_ls_restrained_S_all 1.102 _refine_ls_R_factor_all 0.0962 _refine_ls_R_factor_gt 0.0935 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1100P)^2^+6.0000P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2444 _refine_ls_wR_factor_ref 0.2462 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5635 _reflns_number_total 5983 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4ce01081g2.cif _cod_data_source_block z482101_g _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 7249654 _publ_contact_name 'Aida I. Samigullina' _publ_contact_email s_aida_88@mail.ru _shelx_shelxl_version_number 2019/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.695 _shelx_estimated_absorpt_t_max 0.933 _shelx_res_file ; TITL z482101_g_a.res in P2(1)/n 030_085.res created by SHELXL-2019/3 at 11:13:37 on 25-Nov-2024 REM Old TITL Z482101_g in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.249, Rweak 0.101, Alpha 0.058, Orientation as input REM Formula found by SHELXT: C44A N3 O9 CELL 1.54184 6.514 32.543 12.9337 90 92.843 90 ZERR 4 0.0001 0.0008 0.0003 0 0.002 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H N O UNIT 88 24 64 64 DELU 0.006 C54A > O52A DELU 0.006 C54B > O52B DELU 0.006 C54C > O52C ISOR 0.006 C54A > O52A ISOR 0.006 C54B > O52B ISOR 0.006 C54C > O52C SUMP 1 0.00001 1 2 1 3 1 4 L.S. 15 PLAN 20 SIZE 0.05 0.12 0.28 TEMP -173 CONF BOND $H list 4 MORE -1 fmap 2 53 acta OMIT -1 3 3 OMIT 2 4 2 OMIT 1 5 1 WGHT 0.110000 6.000000 FVAR 0.43040 0.57669 0.24756 0.17576 O2 4 0.458108 0.300674 -0.231888 11.00000 0.05777 0.04457 = 0.05128 -0.00044 0.00164 0.01996 O1 4 0.536308 0.348756 -0.353830 11.00000 0.04913 0.05178 = 0.05712 -0.00526 0.01769 0.00690 O6 4 -0.273946 0.366978 -0.108468 11.00000 0.05028 0.05256 = 0.06382 0.01270 0.02678 0.00291 O29 4 -0.038694 0.171699 0.557866 11.00000 0.04552 0.06376 = 0.07547 -0.01575 0.01814 -0.01025 O30 4 0.193155 0.140529 0.653886 11.00000 0.07794 0.04779 = 0.05330 0.00679 0.01069 -0.01677 N1 3 0.414796 0.338546 -0.289648 11.00000 0.04398 0.03932 = 0.04387 -0.00698 0.00442 0.00842 N6 3 -0.111325 0.361179 -0.153785 11.00000 0.04549 0.03848 = 0.04690 0.00659 0.01459 0.00089 PART 1 O21 4 1.003737 0.293524 0.617710 11.00000 0.04879 0.06921 = 0.09088 -0.03608 -0.00048 -0.00488 PART 0 O10 4 -0.267017 0.506509 -0.425363 11.00000 0.08879 0.05070 = 0.06975 0.02071 0.01363 0.02313 O9 4 -0.468957 0.481496 -0.313306 11.00000 0.05881 0.05525 = 0.09084 0.01123 0.01706 0.02148 PART 1 O26 4 0.177443 0.280751 0.344093 11.00000 0.09919 0.05567 = 0.05273 -0.00482 -0.03287 0.01517 PART 0 N29 3 0.134514 0.168902 0.598196 11.00000 0.04651 0.04749 = 0.04382 -0.01028 0.01375 -0.00840 PART 1 O22 4 0.949369 0.336441 0.475744 11.00000 0.08882 0.05654 = 0.09793 -0.03022 0.04802 -0.03878 PART 0 N5 3 0.003455 0.329937 -0.126256 11.00000 0.05978 0.03877 = 0.05406 0.01282 0.01719 0.00877 PART 1 N21 3 0.889316 0.302265 0.543382 11.00000 0.05377 0.04801 = 0.07350 -0.02788 0.02326 -0.01452 N26 3 0.348730 0.284090 0.390152 11.00000 0.07863 0.03613 = 0.03693 -0.00050 -0.00578 0.00542 PART 0 N9 3 -0.309135 0.481047 -0.360238 11.00000 0.06251 0.03931 = 0.06011 0.00549 0.01121 0.01435 C12 1 0.117278 0.387305 -0.287395 11.00000 0.03686 0.02947 = 0.03541 -0.00349 0.00529 -0.00003 N3 3 0.304041 0.294450 -0.164251 11.00000 0.06427 0.04756 = 0.05002 0.00563 0.00790 0.01657 C27 1 0.387624 0.256929 0.477160 11.00000 0.04956 0.03115 = 0.03070 -0.00503 0.00228 0.00552 C7 1 -0.064856 0.390500 -0.234600 11.00000 0.03799 0.03048 = 0.03825 0.00127 0.00842 -0.00060 C28 1 0.237307 0.228636 0.498398 11.00000 0.03968 0.03789 = 0.03693 -0.01008 -0.00019 0.00362 AFIX 43 H28 2 0.109159 0.227874 0.460038 11.00000 -1.20000 AFIX 0 C13 1 0.243254 0.353079 -0.255765 11.00000 0.03799 0.03308 = 0.03730 -0.00491 0.00273 0.00291 C32 1 0.574397 0.258346 0.534973 11.00000 0.04153 0.03152 = 0.03757 -0.01045 0.00763 -0.00038 PART 1 C33 1 0.711605 0.289464 0.503034 11.00000 0.05035 0.03441 = 0.04735 -0.01502 0.01500 -0.00452 PART 0 C4 1 0.179784 0.325947 -0.179611 11.00000 0.05121 0.03543 = 0.04141 0.00147 0.00420 0.00610 C29 1 0.283095 0.201624 0.578063 11.00000 0.04394 0.03539 = 0.03343 -0.00610 0.00769 -0.00250 C31 1 0.612245 0.231071 0.615645 11.00000 0.04405 0.04013 = 0.03947 -0.00706 -0.00404 0.00069 AFIX 43 H31 2 0.737867 0.232321 0.656094 11.00000 -1.20000 AFIX 0 C9 1 -0.160982 0.448219 -0.334947 11.00000 0.04850 0.03288 = 0.04697 0.00167 0.00685 0.00693 PART 1 N25 3 0.478871 0.310819 0.356754 11.00000 0.11146 0.04255 = 0.04225 0.00242 0.00686 0.00022 PART 0 C8 1 -0.205859 0.421241 -0.257117 11.00000 0.03921 0.03464 = 0.04708 -0.00097 0.00850 0.00330 AFIX 43 H8 2 -0.328300 0.423701 -0.220637 11.00000 -1.20000 AFIX 0 C30 1 0.465430 0.201931 0.636929 11.00000 0.05433 0.03864 = 0.03347 -0.00196 -0.00011 -0.00094 AFIX 43 H30 2 0.489820 0.182527 0.691027 11.00000 -1.20000 AFIX 0 C11 1 0.157496 0.415493 -0.364786 11.00000 0.04594 0.03919 = 0.04367 0.00255 0.01620 0.00242 AFIX 43 H11 2 0.280548 0.413489 -0.400934 11.00000 -1.20000 AFIX 0 C10 1 0.018397 0.446241 -0.388684 11.00000 0.06476 0.03564 = 0.04702 0.00836 0.01661 0.00674 AFIX 43 H10 2 0.044385 0.465792 -0.440990 11.00000 -1.20000 AFIX 0 PART 1 C24 1 0.661425 0.313897 0.416980 11.00000 0.09296 0.03644 = 0.04955 -0.00584 0.02657 -0.00657 N23 3 0.800380 0.341599 0.399227 11.00000 0.12742 0.05503 = 0.06963 -0.00957 0.03731 -0.02827 C54A 1 0.589322 0.448723 0.082423 21.00000 0.06514 0.04193 = 0.04966 -0.00104 0.00550 0.01954 O41A 4 0.247590 0.422757 -0.071786 21.00000 0.09052 0.06156 = 0.04518 -0.01010 -0.01995 0.02551 N46A 3 0.450313 0.410541 0.379674 21.00000 0.06902 0.05336 = 0.05068 -0.01041 0.00366 0.01795 C55A 1 0.401815 0.428266 0.096521 21.00000 0.05717 0.04215 = 0.04821 -0.01208 -0.01144 0.01848 C45A 1 0.484593 0.420869 0.282052 21.00000 0.05596 0.04159 = 0.03971 -0.00685 0.00865 0.01710 N51A 3 0.895260 0.475641 0.141177 21.00000 0.05724 0.05235 = 0.09079 -0.01738 0.00689 0.01176 O46A 4 0.320491 0.393172 0.425246 21.00000 0.11455 0.06874 = 0.06010 0.00799 0.04069 0.02155 O42A 4 0.110411 0.396471 0.079304 21.00000 0.06730 0.06643 = 0.08142 -0.00918 -0.00602 0.00730 C44A 1 0.344994 0.413677 0.192352 21.00000 0.04577 0.03945 = 0.06230 -0.00790 0.00384 0.00837 C50A 1 0.723328 0.454535 0.171432 21.00000 0.04630 0.03519 = 0.06433 -0.01002 0.00628 0.01141 C49A 1 0.671854 0.440184 0.272596 21.00000 0.04656 0.03816 = 0.05688 -0.01984 -0.00857 0.01664 O47A 4 0.617750 0.424769 0.436459 21.00000 0.10003 0.08044 = 0.07055 -0.02597 -0.04141 0.03260 N53A 3 0.657928 0.462843 -0.008460 21.00000 0.09473 0.06814 = 0.06717 0.00383 0.00476 0.02272 N41A 3 0.258370 0.417270 0.024724 21.00000 0.06488 0.05178 = 0.05181 -0.00837 -0.01281 0.01750 O51A 4 1.042965 0.486307 0.187584 21.00000 0.05662 0.05434 = 0.13491 -0.03763 -0.00454 0.00306 N43A 3 0.163050 0.394180 0.182043 21.00000 0.05873 0.05527 = 0.06743 -0.00798 -0.00067 0.00574 N48A 3 0.771799 0.444172 0.363541 21.00000 0.08223 0.06915 = 0.07636 -0.01993 -0.02064 0.01997 O52A 4 0.856308 0.480090 0.035803 21.00000 0.11181 0.09737 = 0.10015 0.01645 0.02685 -0.00133 PART 2 SAME 0.002 C54A > O52A C54B 1 0.610293 0.448851 0.111801 31.00000 0.06927 0.05741 = 0.06823 0.00290 0.01253 0.00816 O41B 4 0.443266 0.453112 -0.112659 31.00000 0.14573 0.12985 = 0.10018 0.01510 0.03514 0.01787 N46B 3 0.176607 0.391119 0.289826 31.00000 0.06026 0.04908 = 0.07281 -0.00700 0.00942 0.02092 C55B 1 0.427341 0.433737 0.062597 31.00000 0.07224 0.06839 = 0.07509 -0.00537 0.00331 0.00703 C45B 1 0.309501 0.408324 0.227343 31.00000 0.07322 0.06078 = 0.07119 -0.00432 0.00547 0.01880 N51B 3 0.825214 0.460054 0.253052 31.00000 0.07938 0.07783 = 0.09066 -0.00649 0.00158 0.00575 O46B 4 0.024218 0.370581 0.280690 31.00000 0.15526 0.20234 = 0.19986 -0.00442 -0.00975 -0.08881 O42B 4 0.175949 0.415450 -0.043619 31.00000 0.08550 0.07799 = 0.08236 -0.01325 -0.01859 0.01431 C44B 1 0.276918 0.413298 0.115838 31.00000 0.06993 0.06371 = 0.07222 -0.00377 0.00406 0.00804 C50B 1 0.637833 0.443000 0.220685 31.00000 0.07642 0.07094 = 0.07214 -0.00256 0.00484 0.00709 C49B 1 0.484615 0.422893 0.279871 31.00000 0.07495 0.06879 = 0.06499 0.00102 0.00752 0.00851 O47B 4 0.268013 0.394585 0.386660 31.00000 0.08018 0.05659 = 0.07640 0.00941 0.01683 0.01212 N53B 3 0.759093 0.470754 0.066666 31.00000 0.07601 0.07631 = 0.08880 0.00507 0.01854 -0.00293 N41B 3 0.366492 0.435326 -0.037263 31.00000 0.07285 0.05231 = 0.07260 -0.00682 0.00141 0.02287 O51B 4 0.910743 0.461390 0.333937 31.00000 0.10717 0.09831 = 0.11668 -0.01524 -0.03185 0.02666 N43B 3 0.116347 0.403627 0.050880 31.00000 0.08107 0.08443 = 0.09473 -0.00501 -0.00255 0.00088 N48B 3 0.479517 0.415724 0.380336 31.00000 0.07676 0.07649 = 0.06954 -0.00550 0.00211 0.00513 O52B 4 0.895681 0.475916 0.162328 31.00000 0.07966 0.08572 = 0.10926 -0.00563 0.01118 -0.00279 PART 3 SAME 0.002 C54A > O52A C54C 1 0.714220 0.451239 0.208834 41.00000 0.03417 0.02772 = 0.04601 -0.00778 0.00261 0.00283 O41C 4 0.876812 0.483924 0.007458 41.00000 0.07859 0.06786 = 0.07969 -0.00148 0.03127 -0.01650 N46C 3 0.134059 0.399213 0.147705 41.00000 0.05385 0.05388 = 0.05674 -0.00244 0.00206 -0.00120 C55C 1 0.630688 0.450613 0.106059 41.00000 0.03473 0.02486 = 0.04010 -0.00190 0.00781 0.01055 C45C 1 0.322224 0.415349 0.160188 41.00000 0.03887 0.03293 = 0.04159 -0.00363 0.00528 0.01063 N51C 3 0.704918 0.436563 0.380575 41.00000 0.06068 0.05351 = 0.05812 -0.00738 -0.00691 0.00318 O46C 4 0.016612 0.390233 0.077164 41.00000 0.09302 0.12278 = 0.09982 -0.01120 -0.02915 -0.02274 O42C 4 0.562379 0.457487 -0.058710 41.00000 0.06547 0.05756 = 0.04384 0.00149 -0.00550 0.01203 C44C 1 0.441392 0.432685 0.078397 41.00000 0.04030 0.03520 = 0.03333 -0.00837 -0.00021 0.01095 C50C 1 0.595427 0.433159 0.286268 41.00000 0.04191 0.03520 = 0.04048 -0.00301 0.00538 0.00717 C49C 1 0.397141 0.414757 0.262066 41.00000 0.03701 0.02523 = 0.03762 0.00234 0.01190 0.01071 O47C 4 0.086150 0.386911 0.244456 41.00000 0.05517 0.05810 = 0.07179 0.00286 0.01789 -0.01092 N53C 3 0.897771 0.467504 0.242271 41.00000 0.04410 0.03578 = 0.06082 -0.01548 0.00016 0.00556 N41C 3 0.709647 0.465746 0.020902 41.00000 0.04366 0.03196 = 0.04240 0.00234 0.00544 0.01159 O51C 4 0.666727 0.425850 0.463074 41.00000 0.08418 0.08841 = 0.05736 -0.00163 -0.02910 -0.00230 N43C 3 0.398176 0.436989 -0.023856 41.00000 0.05857 0.03779 = 0.03844 -0.00291 -0.00226 0.01501 N48C 3 0.264718 0.397518 0.323039 41.00000 0.04743 0.03474 = 0.04761 -0.00061 0.01568 0.00623 O52C 4 0.883924 0.455643 0.353585 41.00000 0.05524 0.05591 = 0.06534 -0.00834 -0.01084 0.00942 HKLF 4 REM z482101_g_a.res in P2(1)/n REM wR2 = 0.2462, GooF = S = 1.058, Restrained GooF = 1.102 for all data REM R1 = 0.0935 for 5635 Fo > 4sig(Fo) and 0.0962 for all 5983 data REM 814 parameters refined using 649 restraints END WGHT 0.1576 4.5903 REM Highest difference peak 0.985, deepest hole -0.694, 1-sigma level 0.087 Q1 1 0.5362 0.4144 0.4804 11.00000 0.05 0.99 Q2 1 0.9914 0.4845 0.0962 11.00000 0.05 0.68 Q3 1 0.3626 0.4384 -0.1012 11.00000 0.05 0.64 Q4 1 0.9909 0.4757 0.2697 11.00000 0.05 0.63 Q5 1 0.7387 0.4798 -0.0542 11.00000 0.05 0.62 Q6 1 0.0878 0.4009 -0.0036 11.00000 0.05 0.56 Q7 1 0.1929 0.3984 0.2646 11.00000 0.05 0.53 Q8 1 0.4993 0.4415 -0.0188 11.00000 0.05 0.52 Q9 1 0.2147 0.3964 0.3624 11.00000 0.05 0.52 Q10 1 0.6763 0.4383 0.4252 11.00000 0.05 0.51 Q11 1 0.9287 0.4784 0.2147 11.00000 0.05 0.39 Q12 1 0.3239 0.3990 0.3373 11.00000 0.05 0.39 Q13 1 0.8182 0.2189 0.7276 11.00000 0.05 0.36 Q14 1 0.8582 0.4615 0.2846 11.00000 0.05 0.34 Q15 1 0.5081 0.4399 0.0818 11.00000 0.05 0.33 Q16 1 0.3592 0.4184 0.2441 11.00000 0.05 0.31 Q17 1 0.7955 0.2425 0.6591 11.00000 0.05 0.30 Q18 1 -0.0592 0.1818 0.5010 11.00000 0.05 0.30 Q19 1 0.9217 0.2618 0.6456 11.00000 0.05 0.29 Q20 1 0.8165 0.4424 0.4434 11.00000 0.05 0.27 ; _shelx_res_checksum 15301 _shelx_hkl_file ; 0 0 1 0.15 0.09 0 0 -1 0.15 0.14 0 0 2 11.38 0.46 0 0 3 0.76 0.37 0 0 4 4027.82 95.16 0 0 5 3.17 0.54 0 0 6 2.43 0.56 0 0 -6 1.99 0.45 0 0 7 0.44 0.54 0 0 -7 0.20 0.39 0 0 -8 535.10 13.09 0 0 8 570.79 13.96 0 0 -8 542.06 14.11 0 0 -9 4.55 0.52 0 0 9 5.90 1.11 0 0 -9 4.04 0.92 0 0 -10 50.57 1.64 0 0 10 49.01 2.49 0 0 -10 50.80 1.67 0 0 -10 50.96 1.77 0 0 -10 49.08 1.76 0 0 -10 48.51 2.57 0 0 11 1.14 0.64 0 0 -11 1.22 0.47 0 0 -11 0.94 0.60 0 0 -11 0.87 0.61 0 0 -11 1.00 0.64 0 0 -11 0.82 0.80 0 0 -11 1.06 0.60 0 0 -12 19.88 1.06 0 0 -12 18.94 0.99 0 0 -12 18.26 1.08 0 0 12 18.85 1.12 0 0 -12 18.96 1.02 0 0 -13 1.08 0.49 0 0 -13 2.03 0.53 0 0 -13 1.11 0.57 0 0 -13 1.54 0.56 0 0 -13 0.35 0.58 0 0 13 1.50 0.64 0 0 -14 10.11 0.71 0 0 -14 11.78 0.79 0 0 -14 11.65 0.75 0 0 14 9.88 0.76 0 0 -14 10.34 0.79 0 0 14 12.79 0.83 0 0 -15 1.14 0.42 0 0 -15 0.96 0.40 0 0 15 0.29 0.44 0 0 15 1.35 0.48 0 0 -15 0.51 0.37 0 0 16 2.87 0.34 0 1 1 98.28 2.38 0 -1 -1 96.77 2.51 0 1 2 2.28 0.24 0 -1 -2 2.21 0.37 0 1 3 1004.38 23.60 0 -1 3 984.15 23.63 0 -1 -3 976.80 23.95 0 -1 4 109.63 3.01 0 1 4 110.23 2.98 0 -1 5 15.68 0.85 0 1 5 15.01 0.82 0 -1 6 42.21 1.63 0 1 6 45.64 1.63 0 -1 7 0.98 0.56 0 1 7 0.99 0.54 0 1 -7 1.65 0.48 0 -1 8 3.91 0.88 0 1 8 5.29 0.87 0 1 -8 3.90 0.40 0 1 -8 3.65 0.75 0 1 9 65.64 2.71 0 -1 9 63.31 2.71 0 1 -9 63.91 1.90 0 1 -10 0.15 0.47 0 -1 -10 0.41 0.45 0 1 -10 0.60 0.49 0 -1 -10 0.97 0.47 0 1 -10 0.73 0.47 0 1 -10 0.40 0.67 0 1 -10 0.35 0.48 0 -1 -10 0.24 0.49 0 1 -10 0.82 0.38 0 1 10 -0.08 0.84 0 -1 10 1.04 0.84 0 1 11 69.35 2.41 0 -1 11 73.84 2.44 0 -1 -11 75.69 2.37 0 -1 11 70.09 3.30 0 1 -11 79.12 2.32 0 -1 -11 73.85 2.40 0 -1 -11 73.49 2.40 0 1 -11 76.37 2.41 0 1 -11 73.97 2.40 0 1 -11 73.25 3.52 0 1 -11 71.82 2.39 0 -1 -11 73.73 2.42 0 -1 12 3.70 0.71 0 1 -12 3.23 0.65 0 -1 -12 3.12 0.65 0 1 -12 2.76 0.63 0 1 -12 3.04 0.56 0 1 -12 4.14 0.67 0 -1 -12 3.27 0.70 0 -1 12 3.51 0.73 0 1 12 4.05 0.74 0 1 -12 3.29 0.62 0 -1 -12 3.89 0.64 0 1 -13 2.06 0.53 0 -1 -13 1.59 0.52 0 1 -13 2.05 0.58 0 -1 -13 2.03 0.59 0 1 -13 1.97 0.51 0 -1 -13 2.27 0.63 0 1 -13 2.41 0.66 0 -1 13 1.20 0.65 0 1 13 2.50 0.68 0 1 -13 3.01 0.58 0 -1 -13 2.58 0.58 0 1 14 24.97 1.12 0 1 -14 24.17 1.01 0 1 -14 24.55 1.07 0 -1 -14 24.18 1.11 0 1 -14 22.44 1.08 0 1 -14 24.65 1.07 0 -1 -14 25.60 1.08 0 1 -14 25.29 1.14 0 -1 -14 25.24 1.14 0 -1 14 23.87 1.15 0 1 14 25.72 1.16 0 -1 -15 5.51 0.53 0 1 -15 4.82 0.52 0 -1 -15 4.43 0.49 0 1 -15 4.95 0.51 0 1 -15 4.96 0.48 0 1 15 4.35 0.52 0 -1 15 5.08 0.57 0 1 15 5.33 0.57 0 1 16 4.42 0.38 0 1 -16 5.07 0.34 0 2 0 1.65 0.15 0 2 1 5.22 0.19 0 -2 -1 6.48 0.35 0 2 2 1294.71 30.54 0 -2 -2 1282.13 30.82 0 2 3 4255.90 100.89 0 -2 -3 4331.64 101.29 0 2 4 35.83 1.23 0 -2 4 39.23 1.31 0 -2 -4 36.74 1.60 0 2 5 91.95 2.72 0 -2 5 97.04 2.79 0 2 -6 203.39 5.75 0 -2 6 217.34 5.72 0 2 6 211.56 5.64 0 2 -7 21.91 1.27 0 -2 7 21.39 1.24 0 2 7 23.33 1.24 0 2 -8 290.61 8.18 0 -2 8 304.33 8.09 0 2 8 297.99 8.02 0 2 -8 289.92 7.23 0 2 -9 161.15 5.44 0 2 -9 174.53 4.43 0 2 9 164.59 5.29 0 -2 9 169.78 5.38 0 2 -10 0.23 0.46 0 -2 -10 0.03 0.43 0 -2 -10 0.08 0.45 0 2 -10 0.84 0.39 0 2 10 0.50 0.79 0 -2 10 0.18 0.82 0 2 -10 0.51 0.48 0 2 -10 0.26 0.47 0 -2 -10 0.12 0.46 0 2 -10 0.90 0.65 0 -2 -10 0.24 0.50 0 2 -10 0.53 0.48 0 2 -11 0.51 0.55 0 -2 -11 1.48 0.61 0 2 11 0.86 0.61 0 -2 11 0.76 0.61 0 -2 11 1.01 0.98 0 2 -11 1.60 0.47 0 -2 -11 1.04 0.56 0 2 11 1.30 0.66 0 2 -11 1.50 0.56 0 -2 -11 1.04 0.55 0 2 -11 0.77 0.56 0 2 -11 0.47 0.79 0 2 -12 0.80 0.62 0 -2 -12 0.64 0.62 0 -2 12 0.68 0.61 0 -2 -12 0.79 0.50 0 -2 -12 1.72 0.58 0 2 -12 0.88 0.55 0 -2 -12 1.14 0.58 0 2 -12 0.99 0.59 0 2 12 2.15 0.70 0 2 -12 0.86 0.57 0 2 -12 1.46 0.49 0 -2 -13 1.57 0.48 0 2 -13 1.76 0.57 0 -2 -13 1.59 0.56 0 2 -13 2.10 0.49 0 -2 -13 1.86 0.60 0 2 -13 2.01 0.60 0 2 13 2.33 0.65 0 -2 13 2.06 0.65 0 2 -13 2.65 0.57 0 -2 -13 2.25 0.55 0 2 14 2.08 0.57 0 2 -14 1.34 0.44 0 2 -14 1.95 0.46 0 2 -14 0.96 0.50 0 -2 -14 1.05 0.52 0 2 -14 1.62 0.51 0 -2 -14 1.27 0.50 0 -2 -14 1.23 0.56 0 2 -14 1.85 0.55 0 2 14 1.33 0.59 0 -2 14 1.92 0.60 0 -2 -15 11.13 0.67 0 2 -15 11.01 0.67 0 -2 -15 12.51 0.66 0 2 -15 11.93 0.65 0 2 -15 12.26 0.66 0 2 15 12.13 0.70 0 -2 15 11.91 0.71 0 2 16 1.33 0.31 0 2 -16 1.53 0.27 0 3 0 0.94 0.18 0 -3 0 0.34 0.07 0 -3 -1 33.40 1.06 0 -3 -2 304.64 7.73 0 3 2 310.10 7.41 0 -3 -3 2529.09 60.05 0 3 3 2521.10 59.61 0 -3 -4 2296.08 54.84 0 -3 4 2305.56 54.37 0 3 4 2277.62 54.27 0 -3 -5 253.49 6.98 0 3 -5 243.43 6.44 0 -3 -5 241.99 6.42 0 3 5 249.83 6.31 0 -3 5 245.94 6.39 0 -3 -6 16.16 0.99 0 3 -6 17.08 1.02 0 -3 6 20.00 1.09 0 3 6 17.60 1.00 0 -3 -7 8.43 0.81 0 3 -7 8.88 0.84 0 -3 7 9.76 0.91 0 3 7 8.51 0.83 0 3 -8 107.45 3.73 0 -3 -8 111.30 3.76 0 -3 -8 110.18 2.89 0 3 -8 106.12 2.88 0 -3 8 114.30 3.69 0 3 8 103.81 3.55 0 3 -9 94.67 3.66 0 -3 -9 99.73 3.73 0 -3 9 105.23 3.68 0 3 9 103.39 3.58 0 3 -9 98.04 2.70 0 -3 -9 92.75 2.68 0 3 -10 31.24 1.31 0 -3 -10 30.75 1.34 0 -3 10 33.60 1.37 0 -3 -10 33.23 1.23 0 3 -10 31.77 1.21 0 3 10 28.68 1.88 0 -3 10 28.77 1.94 0 -3 -10 31.17 1.28 0 -3 -10 34.13 1.26 0 3 10 33.66 1.40 0 3 -10 34.25 1.25 0 -3 -10 31.49 1.32 0 -3 -10 32.65 1.33 0 3 -10 32.36 1.32 0 -3 -10 32.43 2.03 0 3 -10 32.20 2.04 0 3 -11 0.42 0.54 0 -3 -11 0.63 0.57 0 -3 11 0.73 0.58 0 -3 -11 0.79 0.43 0 3 -11 0.41 0.43 0 -3 11 1.65 1.06 0 -3 -11 0.96 0.53 0 3 11 0.79 0.61 0 -3 -11 0.62 0.55 0 3 -11 1.44 0.57 0 3 -11 0.67 0.53 0 -3 -11 0.47 0.79 0 3 -11 0.82 0.74 0 -3 12 11.13 0.92 0 -3 -12 13.34 0.83 0 3 -12 13.19 0.91 0 3 -12 12.68 0.89 0 -3 -12 12.11 0.88 0 3 -12 13.45 0.94 0 -3 -12 12.63 0.93 0 -3 -12 13.89 0.89 0 3 -12 14.03 0.89 0 3 -12 12.20 0.80 0 -3 -12 13.48 0.84 0 3 12 12.39 0.95 0 -3 -13 7.82 0.65 0 -3 -13 8.89 0.77 0 3 -13 8.39 0.74 0 3 -13 8.33 0.76 0 -3 -13 9.52 0.80 0 -3 -13 8.79 0.71 0 3 -13 8.90 0.73 0 -3 13 8.40 0.80 0 3 13 9.38 0.82 0 -3 -13 7.37 0.65 0 3 -13 7.27 0.66 0 -3 -14 28.07 1.18 0 3 -14 28.81 1.19 0 3 -14 30.37 1.15 0 -3 -14 29.62 1.24 0 3 -14 31.31 1.24 0 -3 14 32.36 1.30 0 3 14 33.48 1.32 0 3 -14 31.24 1.27 0 3 -14 29.94 1.20 0 -3 -14 32.39 1.22 0 -3 14 26.88 1.20 0 3 14 31.65 1.25 0 -3 -15 0.69 0.34 0 3 -15 0.41 0.33 0 3 -15 0.76 0.40 0 -3 15 0.71 0.43 0 3 -15 0.72 0.37 0 -3 -15 0.91 0.37 0 3 15 0.94 0.40 0 -3 15 0.49 0.41 0 3 -15 1.14 0.41 0 3 -16 0.24 0.22 0 -3 16 0.24 0.27 0 3 16 0.50 0.27 0 -4 0 216.26 5.14 0 4 0 214.08 5.34 0 -4 1 1612.58 38.32 0 4 -1 1638.32 38.45 0 4 2 2226.36 52.66 0 -4 -2 2257.83 53.05 0 4 3 1809.53 42.97 0 -4 -3 1835.89 43.46 0 4 4 53.37 1.64 0 -4 4 55.30 1.75 0 -4 -4 53.88 2.09 0 4 5 50.38 1.67 0 -4 5 53.23 1.78 0 4 -5 47.09 1.72 0 -4 -5 49.67 1.76 0 -4 -5 51.18 2.17 0 4 -6 691.32 17.24 0 -4 -6 687.07 17.24 0 -4 6 708.83 17.21 0 4 6 698.51 17.07 0 4 -7 37.80 1.75 0 -4 -7 34.97 1.71 0 -4 7 39.96 1.75 0 4 7 39.21 1.66 0 4 -8 1.05 0.53 0 -4 -8 1.77 0.59 0 -4 -8 2.30 0.34 0 4 -8 2.46 0.35 0 -4 8 1.51 0.68 0 4 8 2.33 0.67 0 4 -9 2.23 0.77 0 -4 -9 1.89 0.73 0 4 9 3.10 0.87 0 -4 -9 2.01 0.39 0 4 -9 2.01 0.40 0 -4 9 2.03 0.90 0 4 -10 9.92 0.75 0 -4 -10 7.48 0.72 0 -4 10 9.26 0.77 0 -4 -10 10.37 0.65 0 4 -10 8.82 0.61 0 -4 10 10.19 1.22 0 -4 -10 9.86 0.71 0 4 -10 8.58 1.15 0 -4 -10 8.35 1.13 0 -4 -10 10.26 0.75 0 4 -10 8.41 0.69 0 -4 -10 9.79 0.69 0 4 10 9.20 0.78 0 4 -10 9.46 0.68 0 4 -11 15.78 0.94 0 -4 -11 15.42 0.92 0 4 -11 13.62 0.94 0 -4 -11 15.93 1.00 0 -4 11 16.24 1.01 0 -4 -11 15.13 0.87 0 4 -11 18.02 1.68 0 -4 -11 15.86 1.62 0 4 11 15.01 1.02 0 -4 -11 14.55 0.83 0 -4 11 16.62 1.64 0 4 -11 15.76 0.85 0 4 -11 15.16 0.94 0 -4 -11 16.35 0.97 0 4 -12 1.28 0.60 0 -4 -12 0.24 0.60 0 -4 12 0.65 0.62 0 -4 -12 1.00 0.48 0 -4 -12 0.52 0.54 0 4 -12 1.15 0.58 0 -4 -12 0.81 0.57 0 4 12 1.16 0.67 0 4 -12 1.22 0.49 0 -4 -12 1.19 0.48 0 4 -12 1.12 0.58 0 -4 13 0.30 0.55 0 -4 -13 0.32 0.40 0 -4 -13 0.82 0.51 0 4 -13 0.87 0.52 0 4 -13 0.90 0.56 0 -4 -13 1.16 0.55 0 -4 -13 1.08 0.50 0 4 -13 0.74 0.50 0 -4 13 0.56 0.57 0 4 13 1.09 0.62 0 -4 -13 1.20 0.45 0 4 -13 0.77 0.43 0 -4 -14 1.26 0.43 0 4 -14 1.55 0.43 0 4 -14 1.06 0.42 0 4 -14 1.23 0.49 0 -4 -14 1.22 0.52 0 -4 14 1.18 0.52 0 4 14 1.18 0.52 0 4 -14 0.16 0.50 0 4 14 1.02 0.56 0 -4 14 1.08 0.54 0 4 -14 0.94 0.47 0 -4 -14 1.34 0.48 0 -4 -15 0.70 0.37 0 -4 -15 0.91 0.33 0 4 -15 0.88 0.33 0 4 -15 0.44 0.36 0 4 -15 1.16 0.41 0 -4 -15 0.39 0.36 0 4 -15 0.55 0.36 0 4 15 0.75 0.42 0 -4 15 0.75 0.39 0 -4 15 0.54 0.43 0 -4 16 0.57 0.27 0 4 16 0.61 0.27 0 4 -16 0.52 0.23 0 5 0 0.67 0.28 0 -5 0 3.46 0.17 0 5 -1 730.28 17.47 0 -5 1 726.25 17.30 0 -5 -2 1393.46 33.29 0 5 2 1390.67 32.85 0 -5 -3 208.13 5.70 0 5 3 211.98 5.21 0 -5 -4 1.47 0.54 0 5 4 1.91 0.37 0 -5 4 2.12 0.43 0 -5 -5 70.44 2.76 0 -5 5 78.17 2.36 0 5 5 70.88 2.20 0 -5 -5 75.01 2.34 0 5 -5 71.20 2.32 0 -5 -6 454.06 12.45 0 5 6 468.76 11.61 0 -5 6 473.37 11.77 0 -5 -6 456.84 11.75 0 5 -6 463.56 11.77 0 5 7 50.70 1.95 0 -5 7 46.42 2.02 0 5 -7 50.53 2.06 0 -5 -7 49.94 2.04 0 5 8 3.08 0.72 0 -5 -8 3.07 0.35 0 5 -8 2.73 0.35 0 -5 8 2.61 0.78 0 -5 -8 2.51 0.65 0 5 -8 2.67 0.68 0 5 9 40.47 2.04 0 -5 9 43.47 2.20 0 -5 -9 42.28 1.38 0 5 -9 42.52 1.38 0 -5 -9 39.93 2.14 0 5 -9 36.86 2.10 0 5 -10 0.32 0.47 0 -5 -10 0.16 0.50 0 -5 10 0.19 0.50 0 5 -10 0.45 0.37 0 -5 10 0.83 0.88 0 -5 -10 0.21 0.34 0 -5 -10 0.64 0.47 0 -5 -10 -0.51 0.69 0 5 -10 0.10 0.60 0 -5 -10 0.09 0.46 0 5 -10 0.53 0.44 0 5 -10 0.35 0.45 0 5 10 0.45 0.54 0 -5 -10 -0.02 0.47 0 5 -11 24.99 1.16 0 -5 -11 23.00 1.12 0 -5 -11 23.20 1.20 0 5 -11 20.61 1.13 0 -5 11 23.66 1.19 0 -5 -11 23.94 1.08 0 -5 -11 24.24 1.95 0 5 -11 24.79 1.94 0 5 11 23.52 1.21 0 -5 11 24.22 1.92 0 5 -11 22.99 1.05 0 -5 -11 24.27 1.07 0 -5 -11 24.33 1.19 0 5 -11 21.86 1.13 0 -5 -12 63.30 2.24 0 5 -12 69.60 2.25 0 -5 12 64.92 2.27 0 -5 -12 64.26 2.11 0 -5 -12 67.62 2.19 0 5 -12 66.01 2.22 0 -5 -12 67.77 2.25 0 5 12 63.63 2.27 0 5 -12 68.30 2.15 0 -5 -12 68.36 2.16 0 5 -12 63.58 2.19 0 5 -13 0.46 0.56 0 -5 -13 0.55 0.57 0 -5 13 0.34 0.57 0 -5 -13 0.24 0.42 0 5 -13 0.68 0.49 0 -5 -13 0.74 0.48 0 5 -13 0.86 0.51 0 -5 -13 0.92 0.53 0 5 -13 0.24 0.51 0 5 13 0.88 0.60 0 -5 13 0.55 0.59 0 5 -13 -0.25 0.43 0 -5 -13 0.62 0.42 0 -5 -14 2.15 0.45 0 5 -14 1.54 0.42 0 5 -14 1.89 0.43 0 5 -14 2.32 0.51 0 -5 -14 2.24 0.51 0 5 14 1.02 0.49 0 -5 14 1.70 0.50 0 5 -14 2.25 0.52 0 5 14 2.25 0.56 0 -5 14 2.35 0.55 0 5 -14 1.84 0.46 0 -5 -14 1.81 0.46 0 -5 -15 4.93 0.45 0 -5 -15 5.38 0.46 0 5 -15 5.54 0.46 0 5 -15 4.90 0.49 0 5 -15 4.29 0.50 0 5 -15 5.27 0.47 0 -5 15 4.16 0.49 0 5 15 4.72 0.50 0 -5 15 4.99 0.53 0 -5 16 6.14 0.38 0 5 16 5.99 0.38 0 5 -16 6.53 0.37 0 6 0 25.22 1.00 0 -6 0 27.91 0.75 0 6 -1 1229.28 29.82 0 -6 1 1236.76 29.62 0 -6 -1 1256.63 29.53 0 6 -1 1257.70 29.53 0 -6 2 134.59 3.49 0 -6 -3 79.80 2.55 0 6 3 74.10 2.01 0 -6 -4 1063.67 25.57 0 6 4 1048.25 24.86 0 -6 -4 1019.50 25.01 0 6 -4 1041.67 25.02 0 -6 -5 52.61 2.29 0 -6 5 54.95 1.89 0 6 5 51.26 1.73 0 6 -5 53.39 1.85 0 -6 -5 52.48 1.83 0 -6 -6 100.76 3.70 0 -6 6 97.80 3.09 0 6 6 98.08 2.94 0 6 -6 93.83 3.06 0 -6 -6 95.07 3.05 0 6 7 409.66 10.49 0 -6 7 410.10 10.68 0 6 -7 402.87 10.70 0 -6 -7 412.56 10.70 0 6 8 71.20 2.59 0 6 -8 67.09 2.74 0 -6 -8 65.63 2.71 0 -6 -8 65.69 1.92 0 6 -8 66.77 1.92 0 -6 -9 1.59 0.69 0 6 -9 2.45 0.73 0 -6 9 2.69 0.90 0 6 -9 3.03 0.40 0 -6 -9 2.68 0.38 0 6 -10 6.96 0.64 0 -6 -10 6.82 0.65 0 6 -10 6.67 0.68 0 -6 -10 5.67 0.69 0 -6 10 6.61 0.68 0 -6 -10 7.12 0.59 0 -6 -10 5.60 1.02 0 6 -10 7.48 1.08 0 -6 -10 6.70 0.66 0 6 -10 6.38 0.55 0 -6 -10 6.83 0.55 0 -6 10 5.78 1.13 0 6 10 7.87 0.75 0 6 -11 0.48 0.53 0 -6 -11 0.42 0.52 0 -6 -11 0.89 0.61 0 6 -11 0.64 0.56 0 -6 11 0.35 0.59 0 -6 -11 0.42 0.47 0 -6 -11 0.12 0.75 0 6 -11 0.12 0.73 0 6 11 0.48 0.62 0 -6 -11 0.63 0.46 0 6 -11 0.92 0.43 0 -6 11 -0.43 1.01 0 -6 -11 0.34 0.55 0 -6 -12 12.74 0.95 0 6 -12 11.92 0.88 0 -6 12 14.00 0.98 0 -6 -12 11.96 0.81 0 -6 -12 13.73 0.89 0 6 -12 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1.30 0 -7 -12 1.56 0.64 0 7 -12 1.77 0.62 0 -7 12 1.78 0.62 0 -7 -12 2.03 0.50 0 -7 -12 1.94 0.57 0 -7 -12 1.29 0.57 0 7 -12 1.55 0.57 0 7 12 1.15 0.63 0 -7 -12 1.66 0.50 0 7 -12 2.13 0.52 0 7 -12 2.00 0.58 0 -7 13 19.21 1.04 0 -7 -13 15.67 0.83 0 -7 -13 19.17 1.00 0 7 -13 16.58 0.94 0 7 -13 16.95 0.95 0 -7 -13 18.87 0.94 0 7 -13 16.17 0.95 0 7 13 18.76 1.02 0 7 -13 16.28 0.88 0 -7 -13 16.45 0.89 0 7 -14 5.18 0.51 0 -7 -14 4.39 0.50 0 7 -14 5.01 0.57 0 -7 -14 4.62 0.53 0 7 -14 4.30 0.53 0 7 -14 4.64 0.58 0 -7 14 5.44 0.65 0 7 14 4.55 0.58 0 -7 14 4.29 0.55 0 -7 15 9.15 0.59 0 7 15 9.65 0.59 0 7 -15 9.72 0.61 0 7 -15 9.07 0.58 0 7 -15 9.30 0.61 0 -7 15 9.21 0.64 0 -7 -15 9.01 0.53 0 7 -16 0.13 0.21 0 7 16 0.12 0.20 0 7 -16 0.27 0.21 0 8 0 4893.88 115.26 0 -8 0 4872.09 114.86 0 8 -1 974.41 23.65 0 -8 1 995.47 23.37 0 8 -1 980.01 23.25 0 -8 -1 981.36 23.24 0 -8 2 76.71 2.15 0 -8 -2 76.76 2.05 0 8 -2 76.29 2.04 0 -8 -3 37.95 1.67 0 -8 3 38.96 1.36 0 -8 -3 41.98 1.30 0 8 -3 38.86 1.28 0 -8 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2.78 0.64 0 -8 12 2.97 0.67 0 -8 -12 2.96 0.54 0 -8 -12 3.41 0.63 0 8 -12 3.78 0.62 0 8 12 2.58 0.69 0 8 -12 3.14 0.53 0 -8 -12 3.82 0.55 0 8 -12 3.01 0.63 0 -8 -12 2.44 0.63 0 -8 -13 7.66 0.64 0 8 -13 7.20 0.61 0 8 -13 7.11 0.69 0 8 -13 7.21 0.69 0 -8 -13 7.74 0.71 0 8 -13 5.86 0.68 0 8 13 7.54 0.74 0 -8 -13 7.34 0.66 0 -8 13 8.48 0.76 0 -8 -14 3.92 0.51 0 8 -14 5.51 0.52 0 -8 -14 4.24 0.49 0 8 -14 4.40 0.54 0 -8 14 4.97 0.62 0 8 -14 5.73 0.59 0 -8 -14 4.94 0.52 0 -8 14 4.51 0.55 0 8 14 4.50 0.54 0 -8 15 3.60 0.42 0 8 15 3.61 0.43 0 -8 15 4.22 0.49 0 8 -15 3.72 0.43 0 8 -15 3.30 0.44 0 8 -15 4.09 0.43 0 -8 -15 3.26 0.37 0 8 -16 0.83 0.20 0 8 -16 1.08 0.22 0 -9 0 3.67 0.28 0 9 0 3.32 0.52 0 9 -1 353.44 8.57 0 -9 -1 358.85 8.56 0 -9 1 371.79 8.73 0 9 1 361.72 9.13 0 9 -1 366.29 9.06 0 9 -2 908.20 21.42 0 -9 -2 900.08 21.41 0 -9 2 884.62 21.53 0 9 -3 74.34 2.14 0 -9 -3 76.28 2.14 0 -9 3 72.46 2.22 0 -9 -4 1472.62 35.48 0 9 -4 1484.00 35.49 0 -9 4 1497.95 35.56 0 -9 -4 1483.43 36.15 0 9 -5 275.85 7.19 0 -9 -5 276.72 7.17 0 -9 5 273.72 7.23 0 -9 -5 269.19 7.85 0 -9 -6 59.06 2.77 0 -9 -6 57.66 2.17 0 9 -6 60.49 2.23 0 -9 -7 45.55 2.55 0 -9 -7 43.22 1.33 0 9 -7 45.60 1.34 0 9 -7 42.14 1.97 0 -9 -7 43.83 1.98 0 -9 -8 15.28 0.69 0 9 -8 15.22 0.68 0 -9 8 16.14 1.32 0 9 -8 14.35 1.21 0 -9 -8 12.64 1.13 0 9 -9 36.75 1.25 0 -9 9 35.34 2.08 0 -9 -9 34.55 1.23 0 -9 -9 33.21 2.00 0 9 -9 32.46 1.99 0 -9 -10 0.47 0.48 0 9 -10 0.63 0.50 0 -9 -10 0.98 0.57 0 -9 10 0.94 0.55 0 -9 -10 0.80 0.42 0 -9 -10 0.63 0.65 0 9 -10 0.74 0.68 0 -9 -10 0.99 0.53 0 -9 -10 0.80 0.39 0 9 -10 1.00 0.40 0 -9 10 0.20 0.93 0 9 10 1.12 0.60 0 9 -11 19.12 1.04 0 -9 -11 20.82 1.06 0 9 -11 19.83 1.08 0 -9 11 21.82 1.14 0 -9 -11 19.72 0.98 0 -9 -11 18.34 1.70 0 9 -11 20.19 1.80 0 9 11 22.01 1.16 0 -9 11 21.47 1.89 0 -9 -11 20.82 0.98 0 9 -11 20.86 0.98 0 -9 -11 20.03 1.10 0 9 -12 39.65 1.58 0 -9 12 44.35 1.69 0 -9 -12 38.76 1.46 0 -9 -12 43.16 1.57 0 9 -12 39.71 1.57 0 9 12 39.69 1.63 0 -9 -12 42.14 1.63 0 9 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64.00 1.88 0 10 -8 65.64 1.89 0 -10 -8 64.86 2.71 0 10 -8 63.05 2.74 0 -10 -9 14.71 0.74 0 10 -9 16.29 0.77 0 -10 9 16.01 1.49 0 -10 -9 14.60 1.33 0 10 -9 14.28 1.34 0 -10 -10 0.27 0.48 0 10 -10 0.73 0.53 0 -10 10 0.03 0.52 0 -10 -10 0.51 0.44 0 -10 -10 0.94 0.72 0 10 -10 0.11 0.61 0 -10 -10 -0.10 0.51 0 -10 -10 0.54 0.38 0 10 -10 1.64 0.41 0 -10 10 1.04 0.92 0 10 10 -0.03 0.56 0 10 -11 10.74 0.80 0 -10 -11 9.36 0.75 0 10 -11 11.31 0.84 0 -10 11 10.34 0.85 0 -10 -11 10.15 0.70 0 10 -11 7.10 1.17 0 -10 -11 7.72 1.18 0 10 11 9.52 0.85 0 -10 -11 8.35 0.78 0 -10 11 10.78 1.47 0 10 -11 10.32 0.69 0 -10 -11 9.84 0.70 0 -10 12 1.25 0.62 0 10 -12 1.59 0.46 0 -10 -12 1.53 0.47 0 -10 -12 0.68 0.51 0 10 -12 0.63 0.52 0 -10 -12 0.60 0.54 0 -10 -12 0.87 0.43 0 10 -12 1.44 0.56 0 10 -13 1.58 0.53 0 -10 -13 1.51 0.47 0 -10 13 1.50 0.53 0 10 13 1.70 0.54 0 10 -13 1.81 0.54 0 -10 -13 1.84 0.53 0 -10 13 1.68 0.59 0 10 -13 1.58 0.42 0 -10 -13 1.58 0.44 0 10 -13 1.88 0.52 0 10 -14 27.11 1.08 0 10 -14 25.59 1.00 0 -10 -14 23.43 0.99 0 10 -14 28.14 1.10 0 -10 -14 26.11 0.99 0 10 14 25.72 1.03 0 -10 14 25.03 1.02 0 10 -15 8.31 0.54 0 10 -15 9.05 0.55 0 10 15 7.65 0.47 0 10 -16 4.68 0.26 0 11 0 2.59 0.52 0 -11 0 2.97 0.30 0 11 1 218.43 5.96 0 11 -1 224.84 5.88 0 -11 1 217.35 5.48 0 11 -2 141.62 4.00 0 -11 2 137.37 3.70 0 11 -2 137.76 3.54 0 -11 -2 140.36 3.53 0 -11 3 7.74 0.64 0 11 -3 7.30 0.48 0 -11 -3 7.54 0.49 0 -11 4 112.64 3.23 0 11 -4 103.72 3.09 0 -11 -4 107.37 3.09 0 -11 -5 105.78 3.91 0 -11 5 110.17 3.35 0 11 -5 104.87 3.24 0 -11 -5 105.87 3.23 0 -11 -6 93.39 3.82 0 -11 6 97.80 3.24 0 -11 -6 94.04 3.14 0 11 -6 98.23 3.20 0 -11 7 11.90 1.12 0 11 -7 13.83 1.07 0 -11 -7 12.20 1.02 0 -11 -7 13.87 1.50 0 -11 -7 13.69 0.60 0 11 -7 12.86 0.59 0 11 -8 75.81 3.08 0 -11 -8 77.13 3.07 0 11 -8 76.29 2.18 0 -11 -8 77.12 2.18 0 11 -9 29.53 1.87 0 -11 -9 27.08 1.81 0 11 -9 27.58 1.20 0 -11 -9 29.51 1.09 0 11 -9 28.65 1.08 0 11 -9 28.85 1.19 0 -11 -10 17.29 0.95 0 11 -10 17.39 0.95 0 11 -10 18.04 0.99 0 -11 10 18.23 1.02 0 -11 -10 17.24 0.89 0 11 -10 16.29 1.55 0 -11 -10 14.90 1.48 0 11 10 15.64 0.99 0 -11 -10 18.42 0.87 0 11 -10 17.83 0.86 0 -11 10 18.38 1.75 0 11 -10 17.80 0.92 0 -11 -10 16.79 1.00 0 11 -11 0.38 0.55 0 -11 11 0.35 0.58 0 -11 -11 0.05 0.42 0 -11 -11 0.40 0.51 0 11 11 0.55 0.59 0 -11 -11 -0.21 0.54 0 11 -11 -0.03 0.50 0 -11 -11 1.03 0.44 0 11 -11 1.24 0.44 0 11 -12 13.01 0.90 0 -11 -12 14.87 0.88 0 11 -12 13.51 0.89 0 -11 -12 13.76 0.80 0 11 -12 12.85 0.78 0 -11 12 14.12 0.95 0 -11 13 12.18 0.84 0 11 -13 10.44 0.74 0 -11 -13 10.52 0.68 0 11 -13 10.21 0.67 0 11 -13 11.20 0.79 0 11 13 9.49 0.71 0 -11 13 9.72 0.71 0 -11 -13 10.76 0.74 0 11 -14 18.70 0.90 0 11 -14 19.15 0.82 0 11 -14 20.40 0.92 0 11 14 18.96 0.85 0 -11 14 18.33 0.94 0 -11 -14 20.79 0.84 0 11 -15 15.84 0.68 0 11 -15 17.29 0.69 0 12 0 182.80 4.95 0 -12 0 174.98 4.39 0 12 -1 43.96 1.68 0 12 1 42.47 1.75 0 -12 1 42.63 1.35 0 -12 2 587.42 14.15 0 12 -2 581.00 14.49 0 12 -2 575.05 13.94 0 -12 -2 584.38 13.92 0 -12 3 528.85 12.90 0 -12 -3 523.39 12.72 0 12 -3 516.88 12.74 0 -12 4 309.48 8.15 0 -12 -4 311.60 8.01 0 12 -4 323.48 8.05 0 -12 5 22.55 1.26 0 -12 -5 19.72 1.56 0 -12 -5 23.39 1.15 0 12 -5 23.40 1.17 0 -12 6 133.49 4.04 0 -12 -6 124.41 3.89 0 12 -6 125.20 3.93 0 -12 7 1.79 0.74 0 -12 -7 1.37 0.28 0 -12 -7 0.80 0.82 0 -12 -7 1.16 0.50 0 12 -7 1.34 0.55 0 12 -8 101.64 2.70 0 -12 8 98.89 3.71 0 -12 -8 95.13 2.67 0 12 -8 98.22 3.65 0 -12 -8 95.93 3.61 0 -12 -8 97.36 4.39 0 -12 -9 0.77 0.36 0 12 -9 0.86 0.35 0 12 -9 0.63 0.43 0 -12 -9 0.45 0.45 0 12 -9 0.69 0.49 0 -12 -9 0.84 0.51 0 12 9 0.16 0.55 0 12 -9 0.84 0.69 0 -12 -9 0.64 0.57 0 12 -10 8.80 1.17 0 -12 -10 7.65 1.10 0 12 -10 7.92 0.75 0 -12 10 8.27 0.78 0 -12 -10 8.03 0.63 0 12 10 6.98 0.76 0 -12 -10 7.87 0.62 0 12 -10 6.95 0.59 0 12 -10 8.08 0.70 0 -12 -10 7.63 0.74 0 12 -10 8.47 0.71 0 -12 -10 8.74 0.73 0 -12 11 27.87 1.29 0 -12 -11 25.26 1.08 0 12 -11 23.55 1.06 0 -12 -11 24.26 1.15 0 12 -11 23.27 1.16 0 -12 -11 22.68 1.06 0 12 -11 26.64 1.23 0 12 -11 23.16 1.10 0 12 -11 26.91 1.21 0 12 -12 36.97 1.49 0 -12 -12 37.15 1.45 0 12 -12 37.66 1.48 0 -12 12 39.53 1.58 0 12 -12 37.35 1.38 0 -12 -12 37.97 1.40 0 -12 13 4.37 0.66 0 12 13 5.22 0.59 0 12 -13 4.96 0.62 0 -12 -13 4.84 0.61 0 -12 -13 5.12 0.51 0 12 -13 4.52 0.50 0 12 -13 5.12 0.61 0 12 14 8.69 0.57 0 12 -14 8.39 0.63 0 -12 -14 9.05 0.58 0 12 -14 9.96 0.65 0 12 -14 8.45 0.62 0 12 -15 2.24 0.36 0 12 -15 2.21 0.34 0 -12 -15 1.82 0.33 0 -13 0 1.16 0.29 0 13 0 0.51 0.46 0 -13 1 100.87 2.77 0 13 1 103.74 3.29 0 13 -1 101.10 3.17 0 -13 2 246.32 5.60 0 -13 -2 225.61 5.22 0 13 2 233.98 6.17 0 13 -2 249.74 6.01 0 13 -3 52.43 1.64 0 -13 -3 49.88 1.60 0 -13 3 52.76 1.84 0 13 -4 281.76 7.12 0 -13 -4 271.98 7.08 0 -13 4 272.09 7.26 0 13 -5 64.56 2.24 0 -13 -5 63.58 2.21 0 -13 5 61.92 2.33 0 -13 6 77.01 2.81 0 -13 -6 71.97 2.65 0 13 -6 78.12 2.74 0 -13 -6 76.28 3.46 0 -13 -7 38.68 1.22 0 -13 7 41.96 2.05 0 -13 -7 37.41 1.85 0 13 -7 35.85 1.86 0 -13 -7 38.95 2.48 0 -13 8 5.35 1.05 0 -13 -8 5.03 0.45 0 -13 -8 4.85 0.81 0 13 -8 5.36 0.84 0 -13 -8 4.49 1.19 0 -13 -9 7.26 0.54 0 -13 9 8.94 1.33 0 13 -9 8.69 0.58 0 -13 -9 7.87 0.70 0 -13 9 7.12 0.65 0 13 -9 8.12 0.66 0 13 -9 7.58 0.70 0 -13 -9 8.63 0.64 0 -13 -9 7.22 1.01 0 13 -9 8.98 1.10 0 13 -10 3.43 0.63 0 -13 10 4.69 0.69 0 13 -10 3.73 0.50 0 -13 -10 3.66 0.49 0 13 -10 3.57 0.60 0 -13 -10 3.68 0.60 0 13 -10 3.56 0.62 0 -13 -10 4.27 0.94 0 -13 -10 3.81 0.54 0 13 -11 50.60 1.73 0 13 -11 51.84 1.85 0 -13 -11 48.86 1.70 0 13 -11 50.18 1.71 0 13 -11 51.02 1.86 0 -13 -11 51.22 1.81 0 13 -11 53.95 1.86 0 -13 11 53.90 1.92 0 13 12 2.16 0.55 0 -13 12 1.89 0.52 0 13 -12 2.24 0.55 0 -13 -12 1.58 0.60 0 -13 -12 1.55 0.45 0 13 -12 1.71 0.44 0 13 -12 0.74 0.56 0 -13 12 1.27 0.61 0 13 13 8.58 0.66 0 13 -13 10.36 0.76 0 -13 -13 10.20 0.73 0 13 -13 10.23 0.63 0 -13 13 10.80 0.81 0 13 -13 10.45 0.75 0 13 14 1.01 0.36 0 -13 14 0.92 0.45 0 -13 14 1.10 0.46 0 -13 -14 0.76 0.38 0 13 -14 0.66 0.40 0 13 -14 0.53 0.37 0 13 -15 3.97 0.37 0 -13 15 4.50 0.42 0 13 -15 4.13 0.37 0 14 0 382.89 9.95 0 -14 1 95.73 2.70 0 14 -1 101.60 3.16 0 14 1 97.55 3.24 0 -14 2 47.34 1.68 0 14 -2 50.06 1.98 0 -14 -2 52.21 2.23 0 14 2 49.75 2.14 0 -14 -3 471.37 11.59 0 -14 3 482.27 11.88 0 14 -4 455.99 11.46 0 -14 -4 459.86 11.43 0 -14 4 463.36 11.66 0 -14 -5 226.41 6.32 0 14 -5 240.53 6.41 0 -14 5 241.50 6.56 0 -14 6 0.73 0.67 0 -14 -6 0.52 0.41 0 14 -6 0.49 0.46 0 -14 7 1.17 0.75 0 -14 -7 0.64 0.50 0 14 -7 0.81 0.52 0 -14 -7 1.60 0.87 0 -14 -8 125.58 3.38 0 -14 8 133.00 4.60 0 14 -8 130.43 4.47 0 -14 -8 125.34 4.40 0 -14 -8 129.71 5.31 0 -14 9 1.36 0.55 0 -14 9 1.22 0.97 0 -14 -9 0.99 0.37 0 -14 -9 0.85 0.49 0 14 -9 1.08 0.49 0 14 -9 0.56 0.51 0 -14 -9 1.55 0.66 0 -14 10 30.32 1.34 0 14 -10 29.33 1.26 0 14 -10 28.24 1.20 0 14 -10 29.94 1.30 0 -14 -10 28.57 1.13 0 14 -10 27.62 1.12 0 -14 10 28.27 2.15 0 -14 11 82.25 2.54 0 14 -11 75.95 2.44 0 14 -11 78.21 2.43 0 14 -11 76.63 2.45 0 -14 -11 75.98 2.41 0 14 -11 75.64 2.31 0 -14 -11 73.91 2.29 0 14 -11 75.15 2.29 0 -14 12 13.11 0.91 0 -14 -12 11.97 0.83 0 14 12 11.85 0.77 0 14 -12 12.58 0.84 0 14 -12 13.62 0.88 0 -14 13 52.66 1.78 0 -14 -13 48.99 1.61 0 14 -13 53.79 1.72 0 14 -13 52.23 1.70 0 14 -14 3.64 0.43 0 -14 14 4.47 0.49 0 14 -14 3.96 0.46 0 -14 -14 3.60 0.40 0 -14 14 3.89 0.51 0 -14 15 10.26 0.51 0 14 -15 9.77 0.48 0 14 -15 9.84 0.48 0 15 0 3.10 0.64 0 15 -1 47.34 1.92 0 15 1 44.57 1.99 0 -15 1 47.86 1.55 0 -15 -2 169.80 5.15 0 15 2 164.87 5.01 0 15 -2 159.17 4.76 0 -15 2 162.70 4.42 0 -15 3 208.05 5.62 0 -15 4 469.67 11.83 0 -15 -4 460.77 11.53 0 -15 5 30.05 1.55 0 -15 -5 27.64 1.31 0 -15 6 50.25 2.21 0 -15 -6 44.20 1.93 0 -15 7 12.81 1.26 0 -15 -7 11.41 1.41 0 -15 -7 12.65 1.03 0 -15 8 82.31 3.46 0 -15 -8 81.75 4.08 0 -15 9 13.26 0.85 0 15 -9 14.88 0.87 0 -15 9 13.18 0.82 0 -15 -9 12.96 0.92 0 15 -9 12.45 0.86 0 -15 9 13.16 1.56 0 -15 -9 12.35 0.69 0 -15 -10 48.91 1.67 0 -15 10 56.10 2.98 0 -15 -10 52.19 1.86 0 15 -10 53.73 1.83 0 -15 10 50.35 1.74 0 15 -10 54.05 1.88 0 15 -10 53.58 1.77 0 -15 11 5.31 0.73 0 -15 -11 4.83 0.51 0 15 -11 4.75 0.64 0 -15 -11 5.80 0.75 0 15 -11 4.76 0.69 0 15 -11 4.77 0.63 0 15 -11 4.88 0.67 0 -15 -12 15.70 0.92 0 -15 12 20.44 1.06 0 15 -12 17.26 0.94 0 15 -12 18.84 0.99 0 -15 -13 3.45 0.54 0 -15 13 3.98 0.59 0 15 -13 3.91 0.54 0 15 -13 3.54 0.54 0 -15 14 0.98 0.40 0 15 -14 0.50 0.34 0 15 -14 1.16 0.37 0 -15 -14 0.77 0.36 0 -15 14 0.95 0.41 0 -15 -14 0.86 0.33 0 15 -15 3.78 0.31 0 15 -15 3.61 0.31 0 16 0 697.76 17.52 0 -16 1 430.22 10.76 0 16 -1 439.15 11.32 0 16 1 450.80 11.48 0 -16 2 53.56 1.83 0 -16 -2 51.74 2.37 0 16 2 54.65 2.33 0 -16 3 124.08 3.65 0 -16 -3 120.15 4.29 0 16 3 122.53 4.21 0 -16 4 14.23 1.02 0 -16 5 11.52 1.03 0 -16 6 243.44 7.05 0 -16 7 59.40 2.64 0 -16 -7 48.88 3.00 0 16 -8 97.42 2.86 0 -16 8 93.46 3.84 0 16 -8 97.83 2.84 0 -16 8 95.70 2.76 0 -16 -8 96.73 2.87 0 -16 8 93.51 2.71 0 -16 -8 93.23 4.49 0 -16 9 11.84 0.84 0 16 -9 11.84 0.81 0 -16 9 12.67 0.82 0 16 -9 12.28 0.86 0 -16 -9 12.09 0.91 0 -16 9 13.72 1.56 0 -16 -10 1.08 0.64 0 -16 10 0.80 0.59 0 16 -10 0.27 0.51 0 16 -10 0.38 0.55 0 16 -10 1.12 0.56 0 16 -11 35.22 1.33 0 16 -11 37.98 1.49 0 -16 11 37.39 1.53 0 16 -11 35.61 1.43 0 -16 -11 36.81 1.45 0 16 -12 1.53 0.50 0 -16 12 0.83 0.55 0 16 -12 0.63 0.49 0 -16 -12 0.83 0.53 0 16 -13 9.14 0.66 0 -16 13 9.92 0.73 0 16 -13 10.89 0.71 0 -16 -13 10.42 0.64 0 16 -14 0.52 0.33 0 -16 14 0.28 0.36 0 -16 14 0.42 0.38 0 16 -14 0.40 0.32 0 16 -14 0.28 0.32 0 -16 -14 0.59 0.33 0 16 -15 3.13 0.25 0 -16 15 3.48 0.29 0 16 -15 3.03 0.27 0 17 0 1.24 0.57 0 -17 1 7.08 0.58 0 17 -1 6.41 0.77 0 -17 2 0.55 0.45 0 17 2 0.54 0.61 0 -17 -2 0.86 0.67 0 -17 3 1.70 0.55 0 17 3 2.13 0.71 0 -17 -3 3.68 0.81 0 -17 4 10.74 0.93 0 17 4 11.94 1.25 0 -17 5 152.78 4.73 0 -17 6 21.65 1.52 0 -17 7 13.69 1.37 0 -17 -8 113.17 3.38 0 -17 8 119.48 4.48 0 17 -8 119.39 3.36 0 -17 8 114.37 3.27 0 17 -8 120.25 3.39 0 -17 8 118.17 3.24 0 17 -9 67.32 2.19 0 -17 9 65.13 3.24 0 -17 9 65.64 2.11 0 -17 -9 62.96 2.18 0 -17 9 67.44 2.07 0 17 -9 68.52 2.16 0 -17 10 7.07 0.72 0 17 -10 5.68 0.71 0 -17 -10 3.89 0.73 0 17 -10 5.70 0.67 0 17 -10 4.90 0.67 0 17 -11 6.37 0.70 0 17 -11 5.96 0.63 0 17 -11 6.41 0.67 0 -17 -11 6.75 0.73 0 -17 12 4.49 0.62 0 -17 -12 3.29 0.57 0 17 -12 3.79 0.56 0 17 -12 3.79 0.52 0 17 -13 18.76 0.87 0 17 -13 18.89 0.89 0 -17 13 21.56 0.97 0 -17 -13 18.60 0.85 0 -17 -13 19.29 0.82 0 17 -14 0.62 0.32 0 -17 14 0.87 0.36 0 -17 14 0.91 0.35 0 -17 -14 0.54 0.28 0 17 -14 0.66 0.30 0 17 -14 0.11 0.29 0 17 -15 1.87 0.20 0 17 -15 1.32 0.18 0 18 0 2.27 0.62 0 18 1 3.87 0.74 0 18 -1 4.29 0.71 0 -18 2 11.32 0.81 0 18 2 10.83 1.07 0 -18 -2 10.37 1.14 0 -18 3 4.51 0.68 0 18 3 4.31 0.81 0 -18 -3 4.31 0.88 0 -18 4 17.63 1.20 0 -18 -4 17.86 1.57 0 18 4 17.96 1.49 0 -18 5 42.12 2.03 0 -18 6 70.43 2.93 0 18 -7 14.32 0.82 0 18 -7 14.18 0.84 0 -18 7 15.02 1.43 0 -18 7 13.08 0.78 0 -18 -8 28.15 1.30 0 -18 8 29.38 1.22 0 -18 8 28.28 1.19 0 18 -8 25.97 1.21 0 18 -8 31.36 1.28 0 -18 -8 27.22 2.41 0 -18 8 29.71 2.09 0 18 -8 29.25 1.24 0 18 -9 1.06 0.51 0 -18 9 0.45 0.98 0 18 -9 0.44 0.47 0 -18 9 0.99 0.60 0 -18 -9 1.01 0.61 0 -18 9 1.23 0.57 0 18 -10 198.23 5.25 0 18 -10 191.56 5.11 0 -18 -10 189.79 5.19 0 18 -10 201.60 5.23 0 18 -11 3.01 0.58 0 18 -11 3.13 0.54 0 18 -11 3.00 0.53 0 -18 -11 2.40 0.60 0 18 -12 1.13 0.45 0 -18 -12 1.92 0.51 0 -18 -12 0.50 0.47 0 18 -12 0.85 0.46 0 18 -13 1.12 0.41 0 18 -13 1.67 0.42 0 -18 13 0.67 0.44 0 -18 -13 1.15 0.41 0 18 -14 0.19 0.27 0 18 -14 0.49 0.30 0 -18 14 0.37 0.33 0 -18 14 0.42 0.31 0 18 -14 0.51 0.27 0 19 0 1.45 0.61 0 19 -1 635.19 16.22 0 19 1 638.07 16.38 0 -19 -1 639.56 16.74 0 19 2 89.57 3.41 0 -19 -2 90.67 3.61 0 -19 2 88.34 2.79 0 19 3 47.58 2.37 0 -19 -3 47.09 2.51 0 -19 3 44.13 1.87 0 19 4 29.07 1.92 0 -19 -4 26.54 2.02 0 -19 4 32.19 1.63 0 19 5 14.79 1.55 0 -19 5 17.60 1.33 0 -19 6 22.12 1.58 0 19 -7 47.91 1.68 0 -19 7 47.41 2.49 0 -19 7 47.79 1.60 0 -19 7 46.49 1.56 0 19 -7 46.17 1.62 0 19 -7 45.83 1.65 0 -19 -7 45.88 1.69 0 -19 7 47.68 1.57 0 -19 8 32.94 1.29 0 -19 8 29.36 2.09 0 19 -8 30.12 1.31 0 19 -8 31.90 1.34 0 -19 -8 31.57 1.37 0 19 -8 32.71 1.31 0 -19 8 32.59 1.27 0 -19 -9 23.31 1.17 0 -19 9 24.84 1.10 0 19 -9 26.35 1.14 0 19 -9 21.89 1.12 0 -19 9 22.63 1.91 0 19 -10 1.68 0.59 0 19 -10 2.47 0.58 0 19 -10 2.38 0.57 0 -19 -10 2.32 0.64 0 -19 10 1.90 0.64 0 19 -11 19.08 0.88 0 19 -11 21.11 1.03 0 -19 -11 19.06 0.97 0 -19 -11 18.19 0.97 0 19 -11 19.41 0.96 0 19 -12 5.61 0.55 0 -19 -12 4.53 0.55 0 -19 -12 4.65 0.56 0 19 -12 4.60 0.54 0 19 -13 1.70 0.41 0 19 -13 1.51 0.37 0 -19 -13 1.72 0.39 0 -19 13 2.02 0.48 0 19 -14 0.57 0.27 0 -19 14 0.81 0.28 0 19 -14 0.35 0.25 0 20 0 104.62 3.65 0 -20 -1 51.07 2.56 0 20 -1 49.69 2.20 0 20 1 53.01 2.36 0 20 2 42.50 2.19 0 -20 -2 43.56 2.40 0 -20 3 401.23 10.46 0 20 3 400.21 11.20 0 -20 -3 411.07 11.57 0 -20 4 10.64 1.01 0 -20 -4 10.21 1.38 0 -20 5 125.90 4.29 0 20 5 129.28 4.90 0 -20 -5 128.16 5.14 0 -20 6 9.11 1.17 0 20 6 7.86 1.30 0 -20 7 29.25 1.13 0 -20 7 29.29 1.14 0 20 -7 26.96 1.15 0 20 -7 26.76 1.20 0 -20 -7 25.73 1.09 0 -20 7 25.15 1.89 0 20 -7 27.08 1.19 0 -20 -7 26.73 1.25 0 -20 7 28.00 1.16 0 -20 -7 26.21 1.23 0 -20 -7 25.99 1.13 0 -20 8 3.30 0.60 0 20 -8 2.09 0.51 0 20 -8 2.06 0.51 0 -20 8 2.01 1.04 0 20 -8 2.31 0.56 0 -20 -8 1.78 0.45 0 -20 -8 2.22 0.65 0 -20 -8 1.56 0.45 0 -20 -8 1.67 0.59 0 -20 8 2.05 0.59 0 -20 9 9.05 0.74 0 20 -9 7.40 0.68 0 -20 -9 8.95 0.81 0 -20 -9 8.51 0.79 0 -20 -9 6.95 0.62 0 20 -9 7.53 0.72 0 20 -10 47.37 1.68 0 -20 10 43.94 1.67 0 -20 -10 44.24 1.64 0 20 -10 42.10 1.53 0 -20 -10 43.45 1.64 0 20 -10 45.67 1.63 0 20 -11 7.40 0.64 0 -20 -11 7.49 0.68 0 20 -11 7.48 0.67 0 20 -11 7.23 0.59 0 -20 -11 5.96 0.64 0 20 -12 6.06 0.56 0 -20 -12 5.34 0.54 0 20 -12 6.05 0.55 0 20 -13 5.42 0.48 0 -20 -13 4.75 0.41 0 20 -13 5.32 0.46 0 20 -14 0.19 0.23 0 20 -14 0.35 0.23 0 21 0 2.13 0.71 0 -21 -1 23.63 1.73 0 21 -1 21.93 1.42 0 21 1 24.12 1.56 0 21 2 404.26 11.09 0 -21 -2 398.71 11.48 0 21 3 130.06 4.64 0 -21 -3 128.70 4.94 0 -21 -4 29.69 2.17 0 21 4 29.81 2.00 0 -21 4 28.70 1.61 0 -21 -5 129.49 5.33 0 -21 5 138.63 4.56 0 -21 6 18.21 0.88 0 -21 6 18.40 1.51 0 21 -6 16.35 0.87 0 -21 -6 16.63 1.83 0 -21 -6 17.54 1.00 0 21 -6 15.95 0.90 0 -21 7 7.04 0.68 0 21 -7 5.39 0.63 0 21 -7 5.97 0.66 0 -21 -7 4.99 0.55 0 -21 7 5.45 1.18 0 21 -7 4.26 0.61 0 -21 7 4.38 0.63 0 -21 -7 6.36 0.77 0 -21 7 5.20 0.66 0 -21 -7 5.28 0.60 0 -21 -7 4.72 0.70 0 -21 8 1.38 0.58 0 21 -8 0.33 0.47 0 -21 -8 0.94 0.41 0 -21 8 1.50 0.98 0 21 -8 1.37 0.53 0 -21 -8 1.30 0.63 0 21 -8 0.90 0.49 0 -21 -8 1.72 0.47 0 -21 -8 1.27 0.60 0 -21 8 0.95 0.56 0 21 -9 44.07 1.60 0 -21 -9 38.08 1.43 0 -21 -9 39.92 1.57 0 21 -9 41.39 1.53 0 -21 9 42.04 1.51 0 -21 -9 39.62 1.57 0 -21 -10 22.92 1.14 0 -21 10 25.99 1.19 0 21 -10 24.20 1.14 0 -21 -10 22.55 1.12 0 21 -10 21.99 1.03 0 21 -10 24.19 1.11 0 -21 -11 1.05 0.49 0 21 -11 0.57 0.46 0 21 -11 0.75 0.43 0 21 -11 1.19 0.44 0 -21 -11 1.06 0.48 0 -21 11 0.99 0.51 0 -21 -12 0.66 0.40 0 21 -12 0.13 0.37 0 21 -12 0.29 0.40 0 21 -13 5.11 0.43 0 21 -13 4.89 0.44 0 21 -14 5.46 0.31 0 21 -14 6.38 0.33 0 -22 0 286.40 8.70 0 -22 -1 1.69 0.85 0 22 -1 2.13 0.68 0 -22 -2 19.84 1.73 0 -22 -3 52.93 2.89 0 -22 -4 198.50 6.93 0 -22 5 30.80 1.85 0 -22 5 33.33 1.21 0 -22 5 31.13 1.19 0 -22 5 31.00 1.21 0 -22 -6 86.32 4.21 0 -22 -6 80.55 2.54 0 -22 -6 81.93 2.46 0 -22 -6 80.14 2.51 0 -22 -6 83.79 2.45 0 -22 6 81.14 2.41 0 -22 -6 76.75 2.40 0 22 -6 81.20 2.48 0 22 -6 83.47 2.53 0 -22 6 82.06 3.38 0 -22 6 84.81 2.43 0 22 -7 7.73 0.72 0 -22 -7 8.87 0.66 0 -22 7 9.88 0.74 0 -22 -7 9.05 0.86 0 -22 -7 8.57 0.69 0 -22 -7 8.54 0.83 0 22 -7 9.41 0.74 0 22 -7 8.80 0.71 0 22 -8 9.33 0.72 0 -22 8 8.78 0.74 0 -22 8 8.14 0.73 0 -22 -8 7.44 0.61 0 22 -8 9.47 0.75 0 -22 -8 9.07 0.79 0 -22 -8 7.25 0.63 0 22 -8 7.65 0.71 0 -22 -8 8.71 0.81 0 22 -9 42.87 1.58 0 -22 -9 38.97 1.55 0 22 -9 44.04 1.57 0 -22 9 42.37 1.52 0 -22 -9 40.30 1.57 0 22 -10 4.44 0.62 0 -22 10 5.09 0.65 0 -22 -10 5.02 0.63 0 22 -10 4.68 0.57 0 22 -10 4.92 0.59 0 22 -11 4.36 0.54 0 22 -11 4.59 0.52 0 -22 11 4.30 0.57 0 22 -11 4.35 0.46 0 -22 -11 4.33 0.53 0 22 -12 7.22 0.54 0 22 -12 8.12 0.57 0 -22 -12 7.07 0.51 0 -22 12 7.31 0.61 0 22 -13 4.68 0.39 0 22 -13 5.29 0.42 0 22 -14 1.71 0.18 0 -23 0 1.54 0.85 0 -23 -1 161.15 5.78 0 -23 -2 1.29 0.88 0 -23 -3 7.52 1.26 0 -23 -4 47.09 2.87 0 23 -5 11.58 0.77 0 -23 -5 10.41 0.70 0 -23 5 9.57 0.69 0 -23 5 8.90 0.68 0 -23 -5 10.32 0.71 0 -23 -5 8.93 0.74 0 -23 -5 12.01 1.56 0 -23 5 11.15 0.73 0 -23 -5 8.56 0.72 0 23 -6 13.00 0.85 0 -23 -6 12.99 0.78 0 -23 6 12.07 0.79 0 -23 -6 12.46 0.78 0 -23 6 14.95 0.84 0 -23 -6 12.41 0.83 0 23 -6 11.41 0.78 0 -23 -6 12.69 1.68 0 -23 6 13.75 0.83 0 -23 -6 11.90 0.85 0 -23 -7 3.54 0.52 0 23 -7 3.98 0.60 0 -23 -7 4.04 0.64 0 23 -7 4.29 0.57 0 -23 -7 4.49 0.56 0 -23 -7 3.58 0.67 0 -23 -7 4.21 1.22 0 23 -7 4.61 0.64 0 -23 -8 10.98 0.69 0 -23 8 11.86 0.82 0 23 -8 11.80 0.82 0 -23 8 12.19 0.81 0 -23 -8 10.96 0.72 0 -23 -8 11.38 0.84 0 23 -8 10.09 0.76 0 23 -8 10.57 0.75 0 23 -9 10.29 0.78 0 -23 -9 10.29 0.80 0 -23 9 9.68 0.77 0 23 -9 10.42 0.73 0 -23 10 0.79 0.49 0 23 -10 0.05 0.47 0 -23 -10 0.68 0.50 0 23 -10 0.18 0.44 0 23 -10 0.92 0.42 0 -23 -11 0.07 0.38 0 23 -11 0.43 0.42 0 23 -11 0.09 0.38 0 -23 -11 0.02 0.41 0 -23 11 -0.15 0.46 0 23 -11 0.16 0.36 0 23 -12 12.25 0.66 0 -23 12 12.93 0.71 0 23 -12 12.86 0.66 0 23 -13 17.91 0.66 0 -23 13 17.31 0.72 0 23 -13 16.93 0.65 0 -24 0 27.95 2.04 0 -24 -1 81.26 3.73 0 -24 -2 111.60 4.64 0 -24 -3 61.73 3.31 0 -24 -4 9.00 0.74 0 -24 4 9.82 0.69 0 -24 -4 10.09 1.49 0 -24 -4 10.74 0.73 0 -24 4 9.16 0.68 0 -24 4 10.88 0.73 0 -24 5 109.15 3.04 0 -24 5 103.76 2.97 0 -24 -5 106.18 3.06 0 -24 -5 106.28 3.10 0 -24 -5 113.70 4.93 0 24 -5 109.28 3.15 0 -24 5 105.16 2.99 0 -24 6 8.94 0.72 0 -24 6 9.47 0.74 0 24 -6 8.90 0.69 0 24 -6 9.57 0.75 0 -24 -6 7.94 0.77 0 -24 -6 7.43 1.43 0 -24 -6 8.57 0.67 0 -24 6 9.92 0.74 0 -24 -7 0.98 0.57 0 -24 -7 0.91 0.44 0 24 -7 -0.22 0.51 0 24 -7 0.61 0.49 0 24 -7 0.37 0.47 0 -24 8 0.89 0.57 0 24 -8 0.21 0.48 0 24 -8 0.68 0.45 0 -24 -8 0.22 0.39 0 -24 -8 0.53 0.53 0 -24 8 -0.12 0.55 0 24 -8 -0.12 0.45 0 24 -9 0.46 0.44 0 -24 -9 0.03 0.51 0 -24 9 0.05 0.54 0 24 -9 -0.03 0.49 0 -24 10 9.47 0.72 0 24 -10 10.19 0.71 0 24 -10 9.39 0.63 0 -24 -10 7.92 0.64 0 24 -10 9.48 0.66 0 24 -11 4.25 0.51 0 -24 11 4.52 0.54 0 -24 -11 3.27 0.45 0 -24 -11 4.71 0.49 0 24 -11 4.00 0.48 0 -24 12 6.79 0.53 0 24 -12 5.90 0.49 0 24 -12 6.74 0.47 0 24 -13 0.69 0.23 0 -24 13 0.90 0.28 0 24 -13 0.70 0.24 0 -25 0 1.23 0.89 0 -25 -1 80.09 3.79 0 -25 1 77.90 3.68 0 -25 2 1.97 0.52 0 -25 -2 1.96 0.94 0 -25 -3 74.71 3.77 0 -25 3 74.89 2.24 0 -25 3 71.78 2.16 0 -25 3 74.64 2.16 0 -25 -3 73.22 2.27 0 -25 4 7.53 0.66 0 -25 -4 6.56 0.64 0 -25 4 5.69 0.66 0 -25 4 6.52 0.68 0 -25 5 62.10 1.97 0 -25 -5 60.47 1.97 0 -25 5 60.36 1.91 0 -25 -5 58.33 1.99 0 25 -5 61.24 2.05 0 -25 5 60.91 1.92 0 -25 6 17.28 0.94 0 -25 6 16.30 0.92 0 25 -6 18.21 0.98 0 -25 -6 18.01 1.97 0 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6.48 0 -26 4 263.11 6.57 0 -26 5 29.53 1.23 0 -26 5 30.70 1.24 0 -26 -5 28.67 1.22 0 -26 5 31.75 1.28 0 26 -5 32.13 1.33 0 -26 6 84.21 2.54 0 26 -6 86.98 2.60 0 -26 6 88.61 2.55 0 -26 -6 83.74 2.54 0 -26 -6 83.55 2.58 0 26 -6 87.75 2.65 0 -26 6 84.23 2.57 0 -26 7 0.30 0.55 0 26 -7 0.89 0.52 0 -26 7 0.69 0.59 0 -26 -7 0.51 0.41 0 -26 -7 0.13 0.52 0 26 -7 0.45 0.47 0 26 -7 0.84 0.46 0 26 -8 0.03 0.47 0 26 -8 0.27 0.41 0 -26 -8 0.02 0.49 0 -26 -9 0.46 0.45 0 26 -9 0.29 0.46 0 26 -9 0.63 0.42 0 -26 9 1.07 0.48 0 -26 10 4.23 0.53 0 26 -10 4.23 0.48 0 26 -10 5.21 0.54 0 26 -10 4.19 0.46 0 -26 -10 4.30 0.51 0 -26 11 1.33 0.40 0 26 -11 0.70 0.37 0 26 -11 0.80 0.35 0 26 -11 0.55 0.33 0 -26 -11 0.33 0.34 0 26 -12 0.50 0.29 0 -26 12 0.43 0.32 0 26 -12 0.23 0.26 0 -27 0 1.87 1.03 0 -27 0 1.62 0.54 0 -27 1 7.74 0.68 0 -27 -1 7.75 0.65 0 -27 -1 9.91 1.45 0 -27 1 7.71 1.28 0 -27 2 73.42 2.12 0 -27 2 73.70 2.23 0 -27 -2 73.15 2.13 0 -27 2 75.54 3.64 0 -27 -2 72.55 3.73 0 -27 -2 72.66 2.26 0 -27 2 68.46 2.10 0 -27 3 147.01 3.91 0 -27 -3 149.82 5.90 0 -27 3 145.77 3.90 0 -27 -3 147.02 4.03 0 -27 4 133.47 3.69 0 -27 4 137.24 3.68 0 -27 -4 133.73 3.76 0 -27 4 136.40 3.76 0 -27 -4 138.72 5.74 0 -27 5 76.56 2.34 0 -27 -5 70.43 2.28 0 -27 5 75.01 2.28 0 27 -5 76.31 2.41 0 -27 5 75.64 2.28 0 27 -6 13.92 0.83 0 -27 6 14.50 0.88 0 -27 6 13.22 0.83 0 -27 -6 12.57 0.76 0 -27 6 13.02 0.85 0 27 -6 15.36 0.90 0 -27 7 41.94 1.50 0 27 -7 38.36 1.46 0 -27 7 40.18 1.47 0 27 -7 39.93 1.51 0 27 -7 41.74 1.55 0 27 -8 1.30 0.51 0 27 -8 1.30 0.44 0 27 -9 1.27 0.46 0 27 -9 1.43 0.42 0 -27 9 1.17 0.46 0 27 -10 6.86 0.49 0 27 -10 6.55 0.52 0 27 -10 7.85 0.57 0 -27 -10 7.16 0.58 0 -27 10 8.12 0.59 0 27 -11 3.32 0.38 0 27 -11 4.02 0.40 0 27 -11 4.27 0.42 0 -27 11 3.81 0.44 0 -27 -11 4.01 0.41 0 27 -12 9.66 0.44 0 -27 12 8.76 0.46 0 27 -12 8.73 0.42 0 -28 0 40.46 2.69 0 -28 0 42.34 1.50 0 -28 1 15.68 1.75 0 -28 -1 16.91 1.82 0 -28 -1 17.55 0.89 0 -28 1 16.56 0.92 0 -28 2 3.09 0.51 0 -28 2 3.54 0.60 0 -28 -2 3.35 0.52 0 -28 2 3.18 0.99 0 -28 -2 2.31 1.02 0 -28 -2 3.51 0.54 0 -28 2 2.81 0.51 0 -28 3 39.69 1.43 0 -28 -3 37.97 2.81 0 -28 -3 37.23 1.46 0 -28 3 39.25 1.42 0 -28 4 29.21 1.24 0 -28 4 25.06 1.14 0 -28 -4 25.30 1.15 0 -28 4 27.43 1.17 0 -28 5 72.83 2.21 0 -28 -5 70.64 2.21 0 -28 5 70.54 2.19 0 -28 5 71.51 2.26 0 28 -5 72.91 2.32 0 -28 6 3.57 0.61 0 -28 -6 2.25 0.46 0 28 -6 2.49 0.52 0 28 -6 2.56 0.51 0 -28 6 3.47 0.60 0 28 -7 2.55 0.56 0 -28 7 2.77 0.60 0 -28 7 3.15 0.60 0 28 -7 2.08 0.50 0 28 -7 3.51 0.54 0 28 -8 8.17 0.63 0 28 -8 8.85 0.70 0 -28 -9 3.51 0.51 0 28 -9 3.21 0.46 0 -28 9 2.52 0.48 0 28 -9 3.08 0.50 0 28 -10 7.16 0.46 0 28 -10 8.34 0.57 0 28 -10 7.44 0.51 0 -28 10 7.12 0.55 0 28 -11 5.65 0.40 0 28 -11 5.85 0.43 0 -28 -11 5.59 0.43 0 -28 11 5.66 0.44 0 28 -12 16.80 0.54 0 28 -12 15.23 0.55 0 -29 0 1.61 0.54 0 -29 0 1.39 1.00 0 -29 1 140.70 5.46 0 -29 -1 143.05 5.58 0 -29 1 135.19 3.69 0 -29 -1 130.27 3.63 0 -29 2 60.71 1.85 0 -29 2 57.16 1.82 0 -29 2 59.02 3.28 0 -29 -2 57.65 3.36 0 -29 2 63.72 1.99 0 -29 -2 58.96 1.85 0 -29 3 570.99 13.63 0 -29 -3 549.40 13.72 0 -29 3 554.90 13.60 0 -29 4 45.56 1.62 0 -29 4 44.14 1.53 0 29 -4 44.59 1.66 0 -29 4 45.03 1.53 0 -29 -4 40.11 1.52 0 -29 5 59.01 1.87 0 -29 -5 53.70 1.83 0 -29 5 60.43 1.88 0 -29 5 56.43 1.91 0 29 -5 58.56 1.97 0 29 -5 57.95 1.91 0 29 -6 2.07 0.48 0 -29 6 1.63 0.55 0 -29 6 2.63 0.58 0 29 -6 2.21 0.52 0 29 -7 31.06 1.28 0 29 -7 31.62 1.26 0 29 -7 31.01 1.23 0 -29 7 31.88 1.25 0 -29 7 31.55 1.26 0 -29 -8 7.86 0.66 0 29 -8 10.11 0.68 0 29 -8 9.32 0.64 0 29 -9 17.15 0.82 0 29 -9 16.55 0.78 0 -29 9 18.90 0.84 0 -29 -9 16.51 0.84 0 29 -10 9.34 0.54 0 29 -10 10.57 0.58 0 29 -11 6.95 0.41 0 29 -11 6.71 0.39 0 -29 -11 6.82 0.42 0 -30 0 13.01 0.84 0 -30 1 32.97 1.36 0 -30 -1 37.80 1.36 0 -30 2 111.85 3.15 0 -30 -2 108.50 3.02 0 -30 2 110.95 3.00 0 -30 2 105.53 2.97 0 -30 -3 25.68 1.15 0 -30 3 23.80 1.07 0 -30 3 25.74 1.10 0 -30 4 3.88 0.60 0 -30 4 4.78 0.67 0 30 -4 2.73 0.57 0 -30 -4 2.78 0.54 0 -30 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11.32 0.75 0 31 -6 9.64 0.71 0 31 -7 22.57 0.96 0 31 -7 24.66 1.02 0 -31 -7 23.29 1.03 0 31 -7 21.95 0.97 0 31 -8 8.36 0.59 0 31 -8 8.48 0.56 0 -31 -8 8.39 0.61 0 31 -9 48.72 1.42 0 31 -9 48.90 1.45 0 -31 -9 46.35 1.48 0 31 -10 2.57 0.30 0 31 -10 2.38 0.31 0 31 -10 2.83 0.33 0 31 -11 0.93 0.16 0 -31 -11 1.22 0.17 0 -32 0 508.25 12.47 0 -32 1 48.48 1.69 0 -32 -1 45.21 1.59 0 -32 2 53.74 1.85 0 -32 2 56.55 1.88 0 -32 -2 54.84 1.76 0 -32 3 28.29 1.11 0 -32 -3 28.21 1.17 0 -32 4 3.55 0.56 0 32 -4 3.73 0.56 0 -32 4 4.72 0.58 0 32 -4 3.71 0.51 0 -32 -4 3.43 0.53 0 -32 5 18.75 0.90 0 32 -5 20.12 0.92 0 -32 5 20.05 0.91 0 32 -5 20.02 0.96 0 -32 -5 17.72 0.93 0 -32 -6 0.75 0.41 0 32 -6 0.66 0.42 0 32 -6 0.02 0.43 0 32 -6 0.52 0.40 0 32 -7 0.98 0.37 0 32 -7 1.03 0.42 0 -32 -7 -0.11 0.40 0 32 -8 0.45 0.32 0 32 -8 0.43 0.36 0 -32 -8 0.81 0.38 0 32 -9 0.22 0.27 0 32 -9 0.55 0.31 0 -32 -9 0.46 0.33 0 32 -10 3.85 0.27 0 -32 -10 3.21 0.31 0 32 -10 3.52 0.29 0 -33 0 3.40 0.71 0 -33 -1 181.38 4.90 0 -33 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125.33 3.38 1 -25 -5 124.90 3.50 -1 -25 5 120.73 3.42 1 -25 -5 128.79 5.42 1 -25 -5 125.12 3.53 -1 -25 5 115.56 3.40 1 25 -5 122.75 3.41 1 25 -5 119.08 3.44 1 -25 -4 178.73 4.67 1 -25 -4 182.99 4.79 -1 -25 4 174.04 4.65 1 -25 -4 184.54 4.82 -1 -25 4 171.14 4.65 1 -25 -4 176.31 6.66 -1 -25 4 175.04 4.73 -1 -25 4 170.90 4.73 -1 -25 3 150.93 4.09 -1 25 3 154.19 5.69 -1 -25 3 148.77 5.33 1 -25 -3 148.07 4.00 1 -25 -3 156.24 4.14 -1 -25 3 145.31 3.93 -1 -25 3 142.42 3.94 -1 -25 2 86.22 3.67 -1 25 2 88.61 3.87 1 -25 -2 82.80 2.45 1 -25 -2 85.63 2.56 -1 -25 2 78.95 2.48 -1 -25 1 10.89 1.34 -1 25 1 11.15 1.36 1 -25 -1 10.71 0.70 1 -25 -1 9.30 0.72 -1 -25 1 9.36 0.73 -1 -25 0 11.04 1.41 -1 25 0 13.65 1.42 1 -25 0 14.30 1.60 1 -25 0 11.67 0.79 1 -25 0 12.49 0.75 -1 25 -1 127.26 4.71 -1 -25 -1 120.97 4.84 1 -25 2 0.52 0.43 -1 25 -2 0.31 0.46 1 -25 2 0.67 0.40 -1 -25 -2 0.62 0.43 1 -25 2 0.90 0.44 -1 -25 -2 0.37 0.77 1 -25 3 82.12 2.40 1 -25 3 82.75 2.37 -1 -25 -3 87.16 4.02 -1 -25 -3 85.31 2.58 1 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21.37 1.11 -1 27 -6 20.06 1.08 -1 27 -6 19.65 1.01 -1 -27 -6 21.89 1.12 1 -27 6 22.00 1.00 -1 -27 -6 21.53 1.11 1 -27 6 20.57 0.99 -1 -27 -7 2.29 0.56 1 -27 7 2.03 0.52 -1 27 -7 2.83 0.57 -1 27 -7 1.65 0.49 -1 -27 -7 2.05 0.60 1 -27 8 12.88 0.76 -1 -27 -8 10.97 0.79 -1 27 -8 10.20 0.71 1 -27 8 10.81 0.76 -1 -27 -9 2.46 0.51 -1 27 -9 2.52 0.46 1 -27 9 3.28 0.54 -1 27 -10 0.41 0.36 -1 -27 -10 0.02 0.37 -1 27 -10 0.60 0.39 1 -27 10 0.21 0.40 -1 27 -11 7.08 0.46 -1 -27 -11 7.36 0.48 -1 27 -11 7.71 0.50 1 -27 11 7.04 0.51 -1 27 -11 6.57 0.42 -1 27 -12 0.26 0.22 1 28 -12 3.19 0.22 1 -28 -12 3.84 0.23 1 28 -11 2.30 0.30 1 -28 -11 2.12 0.33 1 28 -10 0.05 0.32 1 28 -10 0.21 0.29 1 28 -9 0.72 0.38 1 28 -9 0.52 0.33 1 28 -8 17.55 0.85 1 28 -8 15.73 0.78 1 -28 -8 14.92 0.80 1 28 -7 36.97 1.31 1 28 -7 35.95 1.35 1 28 -7 32.87 1.26 1 -28 -7 34.15 1.33 1 28 -6 30.70 1.23 1 28 -6 32.15 1.23 1 -28 -6 32.19 1.30 1 -28 -6 31.28 1.15 1 -28 -5 0.69 0.42 1 -28 -5 -0.03 0.46 1 28 -5 0.68 0.41 1 28 -5 0.33 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1.58 -4 -19 -3 50.76 1.75 4 -19 3 51.12 1.72 4 -19 3 43.20 2.15 -4 -19 -3 49.84 1.93 -4 -19 -3 51.23 1.75 -4 -19 -3 48.16 1.81 -4 -19 -3 49.14 1.82 4 -19 3 52.83 1.65 -4 19 -3 47.92 1.74 -4 -19 -4 2.49 0.74 4 -19 4 2.88 0.60 4 -19 4 2.75 0.59 -4 -19 -4 2.95 0.68 -4 -19 -4 5.18 0.75 -4 -19 -4 3.41 0.61 -4 -19 -4 2.18 0.59 -4 -19 -5 34.50 1.48 4 -19 5 33.39 1.31 4 -19 5 33.07 1.25 -4 19 -5 29.44 1.22 -4 -19 -5 35.81 1.40 -4 -19 -5 35.93 1.45 -4 -19 -5 34.78 1.28 -4 -19 -5 35.76 1.60 4 -19 6 18.94 0.87 -4 -19 -6 13.92 0.87 -4 -19 -6 16.05 0.91 4 -19 6 19.51 0.88 -4 -19 -6 17.56 1.07 -4 -19 -6 17.08 1.11 -4 -19 -6 16.15 1.08 -4 -19 -7 3.34 0.68 4 -19 7 2.75 0.50 -4 -19 -7 3.11 0.64 -4 -19 -7 2.97 0.61 -4 -19 -7 3.33 0.57 -4 19 -7 3.29 0.62 -4 -19 -7 4.05 0.70 4 -19 7 2.85 0.51 -4 -19 -8 26.12 1.17 -4 -19 -8 28.08 1.22 -4 -19 -8 27.53 1.15 -4 19 -8 27.29 1.16 4 -19 8 27.06 0.98 -4 -19 -8 28.23 1.19 4 -19 8 25.96 0.99 -4 -19 -9 1.60 0.52 -4 19 -9 0.91 0.51 4 -19 9 1.49 0.38 -4 -19 -9 1.18 0.46 -4 19 -10 1.49 0.35 -4 -19 -10 1.01 0.42 4 -19 10 1.00 0.34 -4 19 -10 1.20 0.31 -4 19 -10 1.42 0.43 -4 -19 -11 2.77 0.37 -4 19 -11 1.95 0.34 -4 19 -11 2.34 0.37 -4 -20 12 1.83 0.29 4 -20 -12 1.87 0.24 4 -20 -12 2.26 0.27 4 -20 -11 0.50 0.33 4 -20 -11 0.54 0.29 -4 -20 11 0.76 0.24 -4 -20 11 0.89 0.39 -4 -20 10 8.00 0.55 -4 -20 10 7.26 0.47 4 -20 -10 7.61 0.58 4 -20 -9 7.70 0.61 -4 -20 9 7.50 0.54 -4 -20 9 7.93 0.59 -4 -20 9 7.73 0.65 4 -20 -9 7.15 0.64 4 -20 -8 5.51 0.61 -4 -20 8 6.41 0.58 -4 -20 8 5.67 0.67 4 -20 -8 6.55 0.68 -4 -20 8 5.14 0.57 4 -20 -7 62.73 2.03 -4 -20 7 61.28 1.99 -4 -20 7 63.59 2.13 4 -20 -7 60.50 2.06 -4 -20 7 57.98 2.00 4 -20 -6 28.82 1.26 -4 -20 6 27.42 1.21 -4 -20 6 28.10 1.27 -4 -20 6 31.07 1.40 4 -20 -6 31.94 1.34 -4 -20 6 30.25 1.33 -4 -20 5 8.02 0.78 -4 -20 5 8.13 0.77 -4 -20 5 7.40 0.82 4 -20 -5 7.08 0.74 4 -20 -5 7.73 0.72 -4 -20 4 7.09 0.78 -4 -20 4 8.76 0.84 4 -20 -4 6.92 0.72 -4 -20 4 9.24 0.88 -4 20 4 6.39 0.61 -4 -20 4 6.80 0.85 4 -20 -4 7.21 0.68 4 -20 -3 83.56 2.55 4 -20 -3 82.04 2.52 -4 20 3 79.42 2.66 -4 -20 3 86.71 2.75 -4 20 3 88.72 2.42 -4 -20 3 76.72 2.49 4 -20 -3 83.52 2.59 -4 -20 3 88.12 2.69 -4 -20 3 81.22 2.69 -4 -20 3 86.93 2.76 -4 -20 2 23.53 1.20 -4 -20 2 24.12 1.13 -4 20 2 25.34 1.22 -4 -20 2 24.21 1.25 4 -20 -2 22.22 1.09 -4 -20 2 22.47 1.10 -4 20 2 23.84 0.99 4 -20 -2 23.46 1.08 4 -20 -2 22.14 1.03 -4 -20 1 19.62 1.14 -4 20 1 17.83 1.05 -4 -20 1 19.34 1.12 -4 -20 1 18.55 1.06 4 -20 -1 20.38 0.99 -4 -20 1 18.28 1.02 4 -20 -1 18.99 0.96 -4 20 1 18.07 0.88 -4 -20 1 19.87 1.04 -4 -20 0 2.95 0.55 -4 -20 0 3.00 0.61 -4 20 0 3.19 0.64 4 -20 0 3.03 0.51 4 -20 0 2.86 0.50 -4 -20 0 4.10 0.70 4 -20 0 1.60 0.89 -4 -20 0 4.01 0.64 -4 -20 -1 6.72 0.76 -4 20 -1 6.40 0.73 -4 -20 -1 5.79 0.73 -4 -20 -1 7.41 0.77 -4 -20 -1 6.21 0.73 4 -20 1 6.54 0.59 4 -20 2 30.76 1.27 -4 -20 -2 30.45 1.11 -4 -20 -2 31.44 1.37 -4 -20 -2 30.65 1.38 -4 -20 -2 28.75 1.24 -4 -20 -2 31.16 1.34 -4 -20 -2 31.86 1.43 -4 20 -2 30.82 1.25 -4 -20 -3 2.53 0.68 -4 -20 -3 2.42 0.70 -4 -20 -3 2.45 0.64 4 -20 3 2.13 0.60 4 -20 3 2.85 0.59 -4 -20 -3 2.73 0.71 -4 20 -3 1.74 0.56 -4 -20 -3 2.32 0.61 -4 -20 -3 2.51 0.56 4 -20 4 169.29 4.39 -4 -20 -4 171.79 4.60 -4 -20 -4 164.04 4.56 -4 -20 -4 167.37 4.53 -4 -20 -4 165.09 4.37 4 -20 4 170.08 4.48 -4 -20 -5 180.87 4.83 4 -20 5 173.26 4.66 4 -20 5 181.56 4.58 -4 -20 -5 170.70 4.70 -4 -20 -5 179.00 5.00 -4 -20 -5 176.43 4.74 4 -20 5 185.11 4.57 -4 -20 -5 173.36 4.58 -4 20 -5 168.19 4.60 4 -20 6 16.36 0.82 4 -20 6 18.47 0.84 -4 -20 -6 17.03 0.99 -4 -20 -6 16.46 1.05 -4 -20 -6 17.19 1.02 -4 -20 -6 17.02 0.88 -4 -20 -7 3.68 0.57 -4 -20 -7 5.10 0.67 -4 -20 -7 4.25 0.67 4 -20 7 3.87 0.51 -4 -20 -7 4.78 0.66 4 -20 7 4.63 0.53 -4 20 -7 3.84 0.63 4 -20 8 31.40 1.10 -4 -20 -8 33.57 1.29 -4 20 -8 35.82 1.31 -4 -20 -8 31.58 1.29 -4 -20 -8 33.51 1.31 4 -20 8 30.62 1.09 -4 20 -9 21.49 0.93 -4 -20 -9 20.40 0.94 4 -20 9 18.39 0.75 -4 -20 -9 20.05 0.84 -4 -20 -10 9.63 0.58 -4 20 -10 7.44 0.40 -4 -20 -10 9.00 0.57 -4 20 -10 9.48 0.58 4 -20 10 7.88 0.47 -4 20 -10 6.98 0.45 -4 20 -11 0.42 0.29 -4 -20 -11 0.34 0.30 -4 20 -11 0.29 0.28 4 -21 -12 0.63 0.19 4 -21 -12 0.42 0.17 -4 -21 12 0.16 0.20 4 -21 -11 2.44 0.35 -4 -21 11 2.41 0.40 -4 -21 10 3.91 0.42 -4 -21 10 3.04 0.35 4 -21 -10 3.20 0.46 4 -21 -10 3.56 0.42 -4 -21 9 4.58 0.44 4 -21 -9 5.78 0.57 -4 -21 9 5.36 0.55 -4 -21 9 4.83 0.51 4 -21 -9 4.71 0.52 -4 -21 8 5.79 0.55 -4 -21 8 5.25 0.57 -4 -21 8 5.56 0.66 4 -21 -8 6.11 0.60 4 -21 -8 5.61 0.63 -4 -21 7 1.81 0.52 -4 -21 7 1.95 0.56 -4 -21 7 1.03 0.57 4 -21 -7 1.54 0.51 4 -21 -7 2.50 0.56 -4 -21 6 165.68 4.54 -4 -21 6 161.82 4.47 -4 -21 6 169.07 4.60 -4 -21 6 167.86 4.67 4 -21 -6 171.48 4.56 4 -21 -6 167.90 4.60 -4 -21 5 110.60 3.22 -4 -21 5 109.50 3.18 -4 -21 5 107.51 3.25 4 -21 -5 106.32 3.19 4 -21 -5 105.83 3.14 4 -21 -4 140.96 3.98 -4 -21 4 148.55 4.17 -4 -21 4 140.82 4.08 -4 -21 4 143.80 4.09 -4 -21 4 141.59 4.17 4 -21 -4 143.55 4.05 4 -21 -4 150.53 4.03 4 -21 -3 27.94 1.20 4 -21 -3 25.33 1.14 -4 21 3 25.57 1.29 -4 -21 3 25.28 1.31 -4 -21 3 28.88 1.30 -4 -21 3 27.76 1.34 -4 -21 3 25.28 1.13 4 -21 -3 27.43 1.22 -4 -21 3 25.82 1.34 -4 21 2 2.07 0.61 -4 -21 2 2.46 0.57 4 -21 -2 1.50 0.47 -4 -21 2 1.80 0.50 -4 -21 2 2.52 0.62 -4 -21 2 1.63 0.69 4 -21 -2 2.08 0.53 4 -21 -2 1.18 0.49 4 -21 -1 4.74 0.61 4 -21 -1 5.03 0.58 4 -21 -1 4.70 0.52 -4 21 1 4.47 0.68 -4 -21 1 5.56 0.75 -4 -21 1 5.64 0.71 -4 -21 1 4.76 0.63 -4 -21 1 6.17 0.68 -4 -21 1 5.91 0.77 -4 -21 0 32.58 1.34 -4 -21 0 33.63 1.46 -4 21 0 32.39 1.44 -4 -21 0 34.03 1.46 4 -21 0 31.26 1.30 4 -21 0 29.79 2.29 -4 -21 0 31.40 1.39 4 -21 0 33.74 1.29 4 -21 1 2.88 0.52 -4 -21 -1 3.52 0.69 -4 21 -1 2.35 0.60 -4 -21 -1 2.92 0.63 -4 -21 -1 3.69 0.66 -4 -21 -1 3.33 0.65 4 -21 2 73.64 2.24 -4 21 -2 68.03 2.22 -4 -21 -2 65.98 2.02 -4 -21 -2 72.05 2.30 -4 -21 -2 72.21 2.21 -4 -21 -2 72.20 2.42 -4 -21 -2 75.93 2.37 -4 -21 -2 69.09 2.35 -4 -21 -3 14.27 0.95 -4 -21 -3 13.81 0.95 -4 -21 -3 14.15 0.94 4 -21 3 14.43 0.86 4 -21 3 13.57 0.81 -4 -21 -3 12.01 0.77 -4 -21 -3 13.55 0.88 -4 -21 -3 14.37 1.02 -4 21 -3 12.03 0.83 4 -21 4 72.60 2.19 4 -21 4 72.82 2.10 -4 -21 -4 69.59 2.23 -4 -21 -4 65.46 2.06 -4 -21 -4 64.60 2.21 -4 -21 -4 69.38 2.26 4 -21 5 7.20 0.69 4 -21 5 8.04 0.67 -4 -21 -5 7.80 0.81 4 -21 5 7.42 0.66 -4 -21 -5 6.60 0.68 -4 21 -5 6.24 0.60 -4 -21 -5 7.72 0.86 -4 -21 -5 6.21 0.70 4 -21 6 2.17 0.50 -4 -21 -6 2.50 0.65 4 -21 6 2.22 0.49 -4 -21 -6 2.02 0.63 -4 -21 -6 2.00 0.55 -4 -21 -6 1.53 0.63 -4 21 -7 19.63 0.98 -4 -21 -7 20.46 1.06 4 -21 7 18.90 0.83 -4 -21 -7 18.85 0.99 4 -21 7 18.50 0.83 -4 -21 -7 18.31 1.02 -4 -21 -7 19.88 0.89 -4 21 -8 46.27 1.50 4 -21 8 42.06 1.32 -4 -21 -8 43.06 1.52 -4 -21 -8 41.59 1.52 4 -21 8 40.19 1.31 -4 -21 -9 5.94 0.57 -4 21 -9 5.40 0.54 4 -21 9 4.56 0.42 -4 21 -9 4.60 0.42 -4 21 -10 5.73 0.48 -4 -21 -10 6.63 0.48 -4 21 -10 4.53 0.31 4 -21 10 5.90 0.39 -4 21 -10 4.46 0.36 -4 21 -11 10.72 0.48 -4 21 -11 10.12 0.44 4 -22 -11 9.84 0.50 -4 -22 11 9.42 0.52 -4 -22 10 0.34 0.32 4 -22 -10 0.20 0.34 4 -22 -10 0.01 0.31 -4 -22 10 0.51 0.45 4 -22 -9 4.83 0.49 -4 -22 9 5.00 0.43 4 -22 -9 5.09 0.53 -4 -22 9 5.37 0.54 -4 -22 9 5.35 0.48 4 -22 -9 4.49 0.50 -4 -22 8 2.12 0.43 -4 -22 8 2.09 0.46 -4 -22 8 2.87 0.56 4 -22 -8 3.38 0.54 4 -22 -8 3.01 0.50 4 -22 -8 2.42 0.50 -4 -22 7 14.87 0.83 -4 -22 7 14.06 0.85 -4 -22 7 14.25 0.93 4 -22 -7 13.65 0.87 4 -22 -7 13.43 0.83 4 -22 -6 55.53 1.91 -4 -22 6 59.97 1.99 -4 -22 6 57.02 1.87 -4 -22 6 56.73 1.92 -4 -22 6 56.61 2.03 4 -22 -6 57.54 1.97 4 -22 -6 55.64 1.91 -4 -22 5 0.93 0.66 -4 -22 5 0.34 0.55 -4 -22 5 0.59 0.58 4 -22 -5 0.81 0.51 4 -22 -5 0.47 0.56 4 -22 -5 1.79 0.60 4 -22 -4 37.78 1.48 4 -22 -4 38.01 1.47 -4 22 4 37.52 1.59 -4 -22 4 37.47 1.57 -4 -22 4 37.76 1.56 -4 -22 4 42.20 1.68 -4 -22 4 39.45 1.64 4 -22 -4 37.45 1.51 4 -22 -3 1.46 0.54 4 -22 -3 1.10 0.51 4 -22 -3 1.01 0.48 -4 22 3 1.62 0.62 -4 -22 3 2.20 0.62 -4 -22 3 1.04 0.63 -4 -22 3 0.90 0.47 -4 -22 3 1.93 0.67 -4 -22 3 1.20 0.68 -4 -22 2 73.50 2.29 4 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2.94 -4 -22 -4 110.38 3.34 4 -22 4 108.26 3.06 4 -22 5 78.30 2.26 -4 -22 -5 76.23 2.35 4 -22 5 78.44 2.35 -4 -22 -5 77.69 2.28 -4 -22 -5 79.36 2.42 4 -22 5 80.21 2.25 -4 -22 -6 37.55 1.54 -4 -22 -6 40.70 1.44 4 -22 6 38.17 1.27 4 -22 6 37.03 1.27 -4 -22 -6 39.20 1.32 -4 -22 -7 24.34 1.12 4 -22 7 24.18 0.93 4 -22 7 22.71 0.92 -4 -22 -7 24.20 1.06 -4 -22 -7 23.13 0.97 -4 22 -7 23.46 1.05 4 -22 8 0.79 0.41 4 -22 8 0.65 0.40 -4 22 -8 1.10 0.50 -4 -22 -8 0.99 0.46 -4 22 -9 0.22 0.30 4 -22 9 0.65 0.34 4 -22 9 0.26 0.32 -4 22 -9 0.71 0.41 4 -22 10 4.03 0.33 -4 -22 -10 4.62 0.42 -4 22 -10 4.88 0.42 -4 22 -11 0.54 0.21 4 -23 -11 3.57 0.32 -4 -23 11 3.94 0.36 4 -23 -11 3.31 0.30 -4 -23 10 6.62 0.44 4 -23 -10 6.31 0.47 4 -23 -10 6.14 0.43 4 -23 -9 1.43 0.41 4 -23 -9 1.63 0.39 -4 -23 9 0.56 0.29 -4 -23 9 1.83 0.42 -4 -23 9 1.28 0.38 4 -23 -9 1.26 0.39 4 -23 -8 5.15 0.56 -4 -23 8 5.40 0.51 -4 -23 8 6.02 0.51 4 -23 -8 6.34 0.59 -4 -23 8 6.07 0.63 -4 -23 8 5.34 0.57 4 -23 -8 6.02 0.56 -4 -23 7 95.75 2.77 -4 -23 7 94.93 2.74 -4 -23 7 96.66 2.89 4 -23 -7 97.44 2.85 4 -23 -7 96.28 2.81 4 -23 -6 0.14 0.45 -4 -23 6 0.38 0.55 -4 -23 6 0.19 0.47 -4 -23 6 0.36 0.57 -4 -23 6 1.16 0.52 4 -23 -6 0.24 0.48 -4 -23 5 109.13 3.27 -4 -23 5 115.57 3.29 4 -23 -5 112.68 3.25 4 -23 -5 115.06 3.31 -4 -23 5 115.82 3.36 4 -23 -5 111.00 3.24 4 -23 -4 89.35 2.73 -4 23 4 94.00 2.91 -4 -23 4 90.18 2.84 -4 -23 4 89.53 2.82 4 -23 -4 92.39 2.76 -4 -23 4 88.46 2.88 -4 -23 4 96.83 2.92 4 -23 -4 94.09 2.81 4 -23 -3 26.79 1.22 4 -23 -3 28.07 1.18 -4 23 3 26.93 1.32 -4 -23 3 26.59 1.29 -4 -23 3 26.69 1.34 -4 -23 3 27.59 1.23 4 -23 -3 28.47 1.22 -4 -23 3 30.96 1.44 -4 -23 3 27.90 1.35 -4 23 2 3.71 0.69 -4 -23 2 2.50 0.69 4 -23 -2 3.00 0.58 4 -23 -2 3.77 0.58 -4 -23 2 3.28 0.66 -4 -23 2 2.60 0.53 4 -23 -2 3.19 0.51 4 -23 -1 5.19 0.60 -4 23 1 5.90 0.71 -4 -23 1 5.88 0.75 -4 -23 1 6.11 0.65 4 -23 -1 6.07 0.64 -4 -23 1 5.49 0.79 -4 -23 1 5.92 0.67 -4 -23 1 5.14 0.71 -4 -23 0 2.86 0.65 -4 23 0 3.40 0.62 4 -23 0 3.83 0.55 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34.91 1.30 -5 4 -5 35.11 1.23 -5 -4 -5 35.61 1.22 -5 -4 -5 38.66 1.47 5 -4 5 32.53 1.98 5 4 5 34.09 1.92 -5 -4 -5 35.00 1.40 -5 4 -5 38.41 1.52 -5 -4 -5 32.13 1.19 -5 -4 -5 34.44 1.26 -5 4 -6 9.43 0.69 -5 -4 -6 9.83 0.69 -5 -4 -6 11.35 0.70 -5 4 -6 10.71 0.69 -5 -4 -6 12.91 0.97 -5 4 -6 11.90 0.95 -5 4 -6 9.38 0.79 -5 -4 -6 12.52 0.76 -5 4 -6 10.22 0.78 -5 -4 -6 10.61 0.86 -5 4 -6 11.34 0.93 -5 -4 -6 11.33 0.74 -5 -4 -6 12.57 0.71 -5 -4 -7 49.11 1.56 -5 -4 -7 52.69 1.79 -5 -4 -7 50.65 1.64 -5 -4 -7 49.36 1.75 -5 4 -7 48.40 1.73 -5 4 -7 53.66 1.66 -5 4 -7 50.33 1.81 -5 4 -7 51.51 1.59 -5 -4 -7 49.05 1.57 -5 4 -7 53.86 1.85 -5 4 -8 3.37 0.50 -5 4 -8 2.61 0.47 -5 -4 -8 3.40 0.48 -5 -4 -8 2.36 0.43 -5 4 -8 3.91 0.42 -5 -4 -8 2.36 0.51 -5 4 -8 3.80 0.53 -5 -4 -8 2.81 0.61 -5 -4 -8 3.73 0.53 -5 4 -8 3.24 0.60 -5 4 -8 2.77 0.58 -5 4 -8 3.65 0.69 -5 4 -9 1.81 0.43 -5 -4 -9 1.74 0.42 -5 4 -9 1.69 0.33 -5 -4 -9 1.83 0.38 -5 4 -9 1.84 0.45 -5 -4 -9 2.00 0.46 -5 4 -9 1.36 0.53 -5 4 -9 1.93 0.60 -5 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10 2 1.00 0.41 -7 10 2 1.23 0.43 -7 10 2 1.02 0.36 -7 -10 2 1.41 0.36 -7 10 2 1.29 0.46 -7 10 1 12.78 0.75 -7 10 1 13.15 0.61 -7 -10 1 13.09 0.61 -7 -10 1 14.71 0.75 -7 10 1 12.44 0.66 -7 10 1 11.63 0.66 -7 10 0 4.63 0.48 -7 -10 0 5.77 0.58 -7 10 0 5.60 0.44 -7 -10 0 4.71 0.43 -7 10 -1 1.20 0.46 -7 10 -1 1.52 0.39 -7 10 -2 1.13 0.42 -7 10 -2 1.01 0.29 -7 10 -2 1.16 0.36 -7 10 -2 0.43 0.42 -7 10 -2 1.59 0.46 -7 10 -3 1.26 0.44 -7 10 -3 1.11 0.39 -7 10 -3 0.93 0.28 -7 10 -3 1.12 0.33 -7 -10 -3 0.80 0.30 -7 10 -3 0.99 0.38 -7 10 -4 0.25 0.39 -7 10 -4 0.36 0.29 -7 10 -4 0.42 0.26 -7 10 -4 0.55 0.35 -7 10 -4 0.58 0.32 -7 -10 -4 0.83 0.29 -7 10 -5 2.26 0.27 -7 10 -5 2.58 0.26 -7 10 -5 2.57 0.29 -7 10 -5 2.47 0.28 -7 10 -6 0.42 0.18 -7 10 -6 0.58 0.18 -7 10 -7 0.55 0.18 -7 -11 8 4.14 0.28 -7 -11 8 3.39 0.23 -7 -11 8 3.57 0.25 -7 11 7 4.58 0.26 -7 -11 7 5.14 0.37 -7 11 7 5.98 0.41 -7 -11 7 5.85 0.41 -7 -11 7 4.82 0.40 -7 -11 7 5.35 0.37 -7 11 6 3.10 0.42 -7 -11 6 3.03 0.35 -7 11 6 2.85 0.29 -7 11 6 3.02 0.34 -7 -11 6 3.55 0.40 -7 11 5 -0.29 0.32 -7 11 5 -0.36 0.40 -7 -11 5 0.14 0.31 -7 11 5 0.04 0.27 -7 -11 5 -0.20 0.39 -7 11 4 0.44 0.34 -7 -11 4 0.06 0.33 -7 -11 4 0.88 0.43 -7 11 4 0.56 0.30 -7 11 4 0.49 0.40 -7 11 3 4.98 0.51 -7 11 3 5.86 0.53 -7 -11 3 6.57 0.54 -7 11 3 6.56 0.43 -7 -11 2 18.67 0.84 -7 11 2 18.30 0.84 -7 11 2 16.42 0.77 -7 11 2 16.67 0.76 -7 -11 2 17.59 0.79 -7 11 2 18.30 0.69 -7 11 1 3.27 0.45 -7 11 1 4.31 0.40 -7 11 1 3.93 0.55 -7 -11 1 4.12 0.54 -7 11 0 14.48 0.69 -7 -11 0 16.41 0.76 -7 11 0 16.58 0.65 -7 11 -1 0.60 0.44 -7 11 -1 0.82 0.36 -7 11 -2 4.25 0.49 -7 11 -2 4.36 0.40 -7 11 -2 3.94 0.47 -7 11 -3 10.08 0.62 -7 11 -3 11.10 0.56 -7 11 -3 9.82 0.48 -7 -11 -3 10.44 0.47 -7 11 -3 10.00 0.55 -7 11 -4 0.15 0.33 -7 11 -4 0.16 0.27 -7 11 -4 0.16 0.37 -7 11 -4 0.65 0.30 -7 -11 -4 0.27 0.26 -7 11 -5 0.46 0.21 -7 11 -5 0.57 0.20 -7 11 -5 0.20 0.22 -7 11 -6 1.28 0.25 -7 11 -7 0.07 0.15 -7 -12 8 0.40 0.18 -7 -12 7 1.85 0.30 -7 12 7 2.15 0.32 -7 -12 7 2.31 0.33 -7 -12 7 2.28 0.33 -7 12 6 0.32 0.34 -7 -12 6 0.60 0.28 -7 12 6 0.30 0.26 -7 -12 6 -0.10 0.33 -7 12 6 0.18 0.20 -7 12 5 0.35 0.25 -7 12 5 0.67 0.38 -7 -12 5 0.01 0.30 -7 -12 5 0.17 0.37 -7 12 5 0.54 0.31 -7 12 4 2.82 0.31 -7 -12 4 3.25 0.39 -7 12 4 2.82 0.39 -7 -12 4 2.74 0.43 -7 12 4 2.90 0.45 -7 12 3 4.05 0.47 -7 12 3 5.00 0.49 -7 -12 3 5.18 0.49 -7 12 3 5.14 0.37 -7 -12 2 1.04 0.40 -7 -12 2 1.26 0.49 -7 12 2 0.69 0.44 -7 12 2 0.77 0.38 -7 12 2 1.27 0.31 -7 12 2 1.31 0.41 -7 12 1 6.40 0.41 -7 12 1 5.90 0.49 -7 12 0 4.81 0.53 -7 12 0 4.39 0.44 -7 12 0 4.15 0.41 -7 12 -1 4.73 0.51 -7 12 -1 4.83 0.41 -7 12 -2 11.27 0.63 -7 12 -2 11.73 0.61 -7 12 -2 10.95 0.52 -7 12 -3 5.89 0.47 -7 12 -3 6.22 0.39 -7 12 -3 5.83 0.46 -7 12 -3 5.97 0.52 7 -12 4 0.10 0.22 -7 12 -4 0.01 0.34 -7 12 -4 0.01 0.26 -7 12 -4 -0.03 0.26 -7 12 -4 0.09 0.21 -7 12 -5 0.52 0.19 -7 12 -5 0.60 0.21 -7 12 -6 1.60 0.24 -7 13 7 1.03 0.27 -7 -13 7 1.07 0.29 -7 -13 7 1.19 0.26 -7 13 6 2.26 0.35 -7 -13 6 2.53 0.35 -7 -13 6 2.82 0.31 -7 13 5 2.90 0.41 -7 13 5 2.30 0.33 -7 -13 5 2.69 0.40 -7 -13 5 3.12 0.35 -7 -13 4 1.82 0.34 -7 13 4 1.85 0.27 -7 13 4 1.73 0.39 -7 13 4 1.29 0.33 -7 -13 4 1.95 0.41 -7 -13 3 1.62 0.39 -7 13 3 1.70 0.28 -7 13 3 1.86 0.40 -7 13 3 1.54 0.40 -7 13 2 0.57 0.36 -7 13 2 0.45 0.36 -7 13 2 0.55 0.27 -7 13 2 0.29 0.42 -7 -13 2 0.96 0.44 -7 13 1 4.12 0.42 -7 -13 1 5.13 0.50 -7 13 0 -0.05 0.31 -7 13 0 -0.10 0.41 -7 13 -1 14.79 0.58 -7 13 -1 15.75 0.72 -7 13 -2 12.71 0.53 -7 13 -2 12.18 0.64 -7 13 -2 12.48 0.63 -7 13 -3 2.04 0.29 -7 13 -3 1.02 0.40 -7 13 -3 1.88 0.36 -7 13 -3 2.00 0.38 -7 13 -4 0.03 0.33 -7 13 -4 0.28 0.23 -7 13 -4 0.42 0.26 7 -13 4 0.12 0.21 -7 13 -5 0.46 0.18 -7 13 -5 0.16 0.26 -7 13 -6 0.82 0.21 -7 14 7 7.66 0.38 -7 -14 7 6.87 0.35 -7 -14 7 7.42 0.38 -7 -14 6 -0.26 0.25 -7 14 6 0.24 0.29 -7 -14 6 -0.11 0.28 -7 -14 6 -0.24 0.30 -7 -14 5 2.61 0.33 -7 -14 5 2.75 0.38 -7 14 5 2.08 0.38 -7 14 4 1.53 0.36 -7 -14 4 1.88 0.38 -7 14 4 1.46 0.33 -7 14 3 4.47 0.42 -7 14 3 3.83 0.44 -7 14 2 0.13 0.39 -7 14 2 -0.18 0.32 -7 14 2 0.01 0.34 -7 -14 2 0.37 0.42 -7 14 1 2.74 0.34 -7 14 1 2.26 0.38 -7 14 0 3.65 0.35 -7 14 0 4.43 0.49 -7 14 -1 2.59 0.32 7 -14 1 2.60 0.32 -7 14 -1 1.90 0.44 -7 14 -2 1.13 0.28 -7 14 -2 1.05 0.40 -7 14 -2 1.40 0.40 -7 14 -3 1.18 0.26 -7 14 -3 0.69 0.34 -7 14 -3 1.20 0.37 -7 14 -3 0.58 0.32 7 -14 4 2.28 0.25 -7 14 -4 2.72 0.29 -7 14 -5 0.13 0.15 -7 14 -5 0.45 0.24 -7 14 -6 4.74 0.25 -7 15 7 3.43 0.25 -7 -15 7 3.14 0.24 -7 -15 7 3.44 0.27 -7 -15 6 0.05 0.23 -7 -15 6 0.33 0.28 -7 15 6 0.16 0.26 -7 -15 6 0.11 0.27 -7 -15 5 1.81 0.33 -7 -15 5 1.88 0.30 -7 15 5 1.47 0.32 -7 -15 4 2.04 0.36 -7 15 4 1.97 0.35 -7 15 3 2.06 0.38 -7 -15 3 1.49 0.43 -7 15 3 2.23 0.35 -7 15 2 2.06 0.43 -7 -15 2 1.95 0.41 -7 15 2 1.50 0.32 -7 15 1 1.74 0.30 -7 15 0 0.71 0.39 -7 15 0 0.49 0.26 7 -15 0 0.23 0.29 -7 15 -1 3.72 0.46 -7 15 -1 4.15 0.32 7 -15 1 3.60 0.34 -7 15 -2 2.22 0.38 -7 15 -2 1.74 0.26 -7 15 -2 2.40 0.38 -7 15 -3 0.12 0.28 7 -15 3 0.23 0.25 -7 15 -3 0.34 0.21 -7 15 -4 6.31 0.31 -7 15 -4 6.91 0.44 -7 15 -5 3.24 0.27 -7 -16 7 0.04 0.17 -7 -16 6 23.66 0.73 -7 -16 6 22.89 0.74 -7 16 6 22.04 0.72 -7 -16 6 24.11 0.74 -7 -16 5 1.30 0.26 -7 -16 5 1.80 0.31 -7 16 5 1.66 0.29 -7 16 4 0.72 0.29 -7 16 3 2.25 0.37 -7 -16 3 2.25 0.40 -7 16 3 1.75 0.32 -7 16 2 1.55 0.40 -7 16 2 0.95 0.25 -7 16 1 15.65 0.54 -7 16 0 0.04 0.36 -7 16 0 0.29 0.23 7 -16 0 0.41 0.28 -7 16 -1 7.23 0.34 7 -16 1 6.63 0.39 -7 16 -2 4.85 0.40 -7 16 -2 4.36 0.39 -7 16 -3 1.51 0.28 7 -16 3 1.33 0.26 -7 16 -4 3.55 0.23 7 -16 4 3.01 0.23 -7 16 -5 0.05 0.19 -7 -17 6 3.86 0.26 -7 -17 6 3.52 0.27 -7 17 6 4.16 0.26 -7 -17 5 3.43 0.35 -7 17 5 2.56 0.28 -7 -17 5 3.18 0.29 -7 17 4 2.72 0.30 -7 -17 4 3.65 0.39 -7 17 3 0.84 0.26 -7 -17 3 0.98 0.36 -7 17 3 0.80 0.33 -7 17 2 5.69 0.45 7 -17 -1 0.44 0.29 7 -17 0 1.84 0.29 -7 17 0 1.90 0.37 7 -17 1 0.64 0.25 -7 17 -1 0.37 0.33 -7 17 -2 0.87 0.31 -7 17 -2 0.96 0.31 7 -17 3 1.35 0.24 -7 17 -3 1.88 0.26 -7 17 -4 0.41 0.24 -7 17 -5 0.80 0.16 -7 -18 6 -0.01 0.16 -7 -18 6 0.00 0.13 -7 -18 5 0.37 0.20 -7 18 5 0.17 0.18 -7 -18 5 0.12 0.27 -7 -18 4 1.96 0.33 -7 18 3 8.55 0.45 -7 18 2 0.47 0.32 7 -18 -1 3.01 0.32 -7 18 0 0.18 0.32 7 -18 0 0.13 0.25 -7 18 -1 2.70 0.34 7 -18 1 2.34 0.26 -7 18 -2 0.15 0.26 7 -18 2 -0.07 0.24 -7 18 -3 0.57 0.21 7 -18 3 0.54 0.21 -7 18 -4 8.02 0.34 -7 -19 5 0.14 0.20 -7 -19 5 0.33 0.16 -7 -19 5 0.18 0.19 -7 -19 4 3.41 0.31 7 -19 -3 0.91 0.25 -7 19 3 1.39 0.28 7 -19 -2 8.70 0.42 -7 19 2 9.17 0.48 7 -19 -1 9.79 0.44 7 -19 0 1.00 0.25 -7 19 0 2.12 0.33 7 -19 1 4.26 0.27 -7 19 -1 4.52 0.36 7 -19 2 8.10 0.38 -7 19 -2 10.39 0.42 7 -19 3 2.20 0.21 -7 19 -4 0.33 0.15 7 -20 -4 2.15 0.21 -7 -20 4 1.96 0.23 -7 20 3 0.87 0.24 7 -20 -3 0.82 0.22 -7 20 2 4.20 0.34 7 -20 -2 4.12 0.30 7 -20 -1 15.18 0.53 -7 20 0 9.00 0.44 7 -20 0 7.80 0.36 -7 20 -1 2.41 0.28 7 -20 1 1.93 0.25 7 -20 1 1.94 0.20 -7 20 -2 4.28 0.26 7 -20 2 3.96 0.26 -7 20 -3 0.20 0.17 -7 21 3 4.29 0.26 7 -21 -3 4.17 0.25 7 -21 -2 0.93 0.21 -7 21 1 4.28 0.32 7 -21 -1 2.93 0.26 -7 21 0 6.36 0.35 7 -21 0 5.45 0.28 -7 21 -1 0.87 0.23 -7 21 -1 1.06 0.22 7 -21 1 0.36 0.20 7 -21 2 0.24 0.16 7 -22 -2 1.67 0.18 7 -22 -1 0.15 0.15 -7 22 1 0.26 0.19 -7 22 0 12.35 0.41 -7 22 0 11.99 0.43 7 -22 1 5.28 0.24 -8 0 5 0.12 0.15 -8 0 4 7.02 0.31 -8 0 4 7.46 0.33 -8 0 3 0.21 0.21 -8 0 3 0.25 0.22 -8 0 3 -0.05 0.21 -8 0 2 13.91 0.52 -8 0 2 14.04 0.50 -8 0 1 0.14 0.23 -8 0 0 3.12 0.27 -8 0 -1 0.18 0.21 -8 0 -2 1.61 0.20 -8 0 -2 2.21 0.23 -8 0 -3 0.18 0.15 -8 0 -3 0.22 0.17 -8 1 5 1.47 0.16 -8 1 5 1.18 0.18 -8 1 4 2.23 0.23 -8 1 4 2.33 0.22 -8 -1 3 0.34 0.21 -8 1 3 0.68 0.22 -8 1 3 -0.20 0.23 -8 -1 3 0.35 0.22 -8 1 3 0.16 0.21 -8 1 2 3.79 0.29 -8 -1 2 4.14 0.28 -8 1 2 4.30 0.30 -8 -1 1 1.20 0.24 -8 1 1 0.88 0.24 -8 -1 0 0.21 0.22 -8 1 0 0.42 0.23 -8 -1 -1 4.23 0.28 -8 1 -1 4.25 0.29 -8 1 -2 -0.02 0.18 -8 -1 -2 0.22 0.19 -8 1 -3 0.15 0.15 -8 -1 -3 0.23 0.14 -8 -1 -3 0.18 0.16 -8 2 5 0.64 0.15 -8 2 5 0.44 0.15 -8 2 5 0.77 0.16 -8 2 4 0.20 0.18 -8 -2 4 -0.13 0.20 -8 2 4 0.10 0.19 -8 -2 3 3.56 0.33 -8 2 3 3.34 0.29 -8 -2 3 3.12 0.29 -8 -2 2 0.14 0.21 -8 2 2 0.16 0.22 -8 2 1 2.27 0.27 -8 -2 1 2.06 0.25 -8 2 0 1.32 0.26 -8 -2 0 1.80 0.23 -8 2 -1 1.83 0.23 -8 -2 -1 2.20 0.23 -8 2 -2 0.94 0.19 -8 -2 -2 1.40 0.21 -8 -2 -3 -0.10 0.14 -8 3 5 0.02 0.14 -8 3 5 0.23 0.13 -8 -3 5 0.17 0.13 -8 3 4 0.49 0.18 -8 -3 4 0.48 0.18 -8 -3 4 0.16 0.20 -8 -3 4 0.40 0.23 -8 3 3 0.24 0.20 -8 -3 3 0.24 0.21 -8 3 3 -0.04 0.22 -8 -3 3 -0.01 0.22 -8 -3 3 0.29 0.26 -8 3 2 2.11 0.25 -8 -3 2 1.94 0.24 -8 3 1 0.46 0.24 -8 3 0 2.63 0.28 -8 3 -1 1.51 0.22 -8 3 -2 0.76 0.19 -8 3 -3 2.12 0.20 -8 4 5 0.12 0.13 -8 4 4 0.13 0.17 -8 -4 4 0.29 0.17 -8 -4 4 0.02 0.19 -8 -4 4 0.26 0.22 -8 4 3 2.00 0.23 -8 -4 3 1.61 0.22 -8 -4 3 1.27 0.28 -8 4 3 1.25 0.23 -8 4 2 -0.03 0.22 -8 4 2 0.01 0.20 -8 -4 2 0.02 0.20 -8 4 1 0.04 0.23 -8 4 1 -0.03 0.22 -8 4 0 -0.09 0.24 -8 4 0 -0.06 0.22 -8 4 -1 1.33 0.23 -8 4 -1 1.04 0.20 -8 4 -2 2.29 0.22 -8 4 -2 1.72 0.20 -8 4 -3 -0.04 0.14 -8 -4 -3 0.07 0.14 -8 4 -3 0.17 0.16 -8 5 5 1.83 0.16 -8 5 4 1.94 0.21 -8 5 4 1.46 0.17 -8 -5 4 1.60 0.18 -8 -5 4 1.11 0.23 -8 -5 4 1.08 0.21 -8 5 3 1.36 0.22 -8 5 3 1.56 0.20 -8 -5 3 1.26 0.20 -8 5 3 1.02 0.22 -8 -5 3 1.07 0.27 -8 5 2 0.47 0.22 -8 5 1 -0.02 0.23 -8 5 1 0.12 0.22 -8 5 0 0.44 0.23 -8 5 0 0.23 0.21 -8 5 -1 1.40 0.22 -8 5 -1 0.50 0.20 -8 5 -2 0.77 0.19 -8 5 -3 0.34 0.15 -8 -5 -3 0.35 0.13 -8 6 4 2.65 0.21 -8 -6 4 1.99 0.22 -8 -6 4 2.16 0.24 -8 6 3 0.38 0.20 -8 6 3 1.14 0.21 -8 6 2 0.28 0.20 -8 6 1 3.37 0.25 -8 6 1 2.38 0.26 -8 6 0 0.05 0.20 -8 6 0 -0.10 0.19 -8 6 -1 2.06 0.22 -8 6 -1 2.74 0.23 -8 6 -1 2.55 0.26 -8 6 -2 2.40 0.21 -8 6 -3 -0.13 0.12 -8 -7 4 3.60 0.23 -8 -7 4 4.19 0.26 -8 7 3 2.09 0.21 -8 7 3 1.36 0.20 -8 7 2 0.16 0.20 -8 -7 2 0.08 0.25 -8 7 1 1.86 0.25 -8 7 1 2.39 0.23 -8 7 0 1.35 0.20 -8 7 0 2.50 0.23 -8 7 -1 -0.06 0.17 -8 7 -1 -0.26 0.20 -8 7 -1 0.10 0.18 -8 7 -2 0.38 0.17 -8 -8 4 0.30 0.18 -8 8 3 1.66 0.19 -8 8 2 0.46 0.18 -8 -8 2 0.66 0.24 -8 8 1 -0.22 0.21 -8 8 1 0.16 0.18 -8 8 0 0.44 0.19 -8 8 -1 0.82 0.17 -8 8 -1 1.20 0.21 -8 8 -1 1.54 0.19 -8 8 -2 0.25 0.15 -8 9 3 3.22 0.19 -8 9 2 0.63 0.17 -8 -9 2 0.63 0.22 -8 9 1 1.33 0.21 -8 9 1 2.18 0.20 -8 9 0 0.24 0.16 -8 9 -1 0.09 0.17 -8 9 -1 0.47 0.15 -8 9 -2 3.73 0.19 -8 -10 3 3.93 0.23 -8 -10 2 5.95 0.29 -8 10 1 0.44 0.18 -8 10 -1 0.66 0.16 -8 11 1 2.44 0.19 -8 11 0 0.34 0.12 0 0 0 0.00 0.00 TITL Z482101_g in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 1.54184 6.513969 32.543041 12.933746 90.0000 92.8435 90.0000 ZERR 3.00 0.000132 0.000799 0.000272 0.0000 0.0019 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N O UNIT 120.00 57.00 15.00 30.00 REM CrysAlisPro recorded range (K): Min=100.0; max=100.0; aver:100.0 TEMP -173 SIZE 0.05 0.12 0.28 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 17580 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O2 O 0.4581(4) 0.30067(8) -0.2319(2) 0.0512(7) Uani 1 1 d . . . . . O1 O 0.5363(4) 0.34876(9) -0.3538(2) 0.0522(7) Uani 1 1 d . . . . . O6 O -0.2739(4) 0.36698(9) -0.1085(2) 0.0548(7) Uani 1 1 d . . . . . O29 O -0.0387(4) 0.17170(10) 0.5579(3) 0.0611(8) Uani 1 1 d . . . . . O30 O 0.1932(5) 0.14053(9) 0.6539(2) 0.0594(8) Uani 1 1 d . . . . . N1 N 0.4148(5) 0.33855(9) -0.2896(2) 0.0423(7) Uani 1 1 d . . . . . N6 N -0.1113(5) 0.36118(9) -0.1538(2) 0.0432(7) Uani 1 1 d . . . . . O21 O 1.0037(5) 0.29352(11) 0.6177(3) 0.0698(10) Uani 1 1 d . . . A 1 O10 O -0.2670(6) 0.50651(10) -0.4254(3) 0.0694(9) Uani 1 1 d . . . . . O9 O -0.4690(5) 0.48150(10) -0.3133(3) 0.0679(9) Uani 1 1 d . . . . . O26 O 0.1774(6) 0.28075(10) 0.3441(2) 0.0704(10) Uani 1 1 d . . . A 1 N29 N 0.1345(5) 0.16890(10) 0.5982(2) 0.0456(7) Uani 1 1 d . . . . . O22 O 0.9494(6) 0.33644(10) 0.4757(3) 0.0797(12) Uani 1 1 d . . . A 1 N5 N 0.0035(5) 0.32994(10) -0.1263(3) 0.0504(8) Uani 1 1 d . . . . . N21 N 0.8893(6) 0.30227(11) 0.5434(3) 0.0578(9) Uani 1 1 d . . . A 1 N26 N 0.3487(6) 0.28409(10) 0.3902(2) 0.0508(8) Uani 1 1 d . . . A 1 N9 N -0.3091(6) 0.48105(10) -0.3602(3) 0.0537(8) Uani 1 1 d . . . . . C12 C 0.1173(5) 0.38730(9) -0.2874(2) 0.0338(6) Uani 1 1 d . . . . . N3 N 0.3040(6) 0.29445(11) -0.1643(3) 0.0538(8) Uani 1 1 d . . . . . C27 C 0.3876(6) 0.25693(10) 0.4772(2) 0.0371(7) Uani 1 1 d . . . . . C7 C -0.0649(5) 0.39050(10) -0.2346(3) 0.0354(7) Uani 1 1 d . . . . . C28 C 0.2373(5) 0.22864(10) 0.4984(3) 0.0382(7) Uani 1 1 d . . . . . H28 H 0.109159 0.227874 0.460038 0.046 Uiso 1 1 calc R U . . . C13 C 0.2433(5) 0.35308(10) -0.2558(3) 0.0361(7) Uani 1 1 d . . . . . C32 C 0.5744(5) 0.25835(10) 0.5350(3) 0.0367(7) Uani 1 1 d . . . . . C33 C 0.7116(6) 0.28946(11) 0.5030(3) 0.0436(8) Uani 1 1 d . . . A 1 C4 C 0.1798(6) 0.32595(11) -0.1796(3) 0.0426(8) Uani 1 1 d . . . . . C29 C 0.2831(5) 0.20162(10) 0.5781(2) 0.0374(7) Uani 1 1 d . . . . . C31 C 0.6122(6) 0.23107(11) 0.6156(3) 0.0414(7) Uani 1 1 d . . . . . H31 H 0.737867 0.232321 0.656094 0.050 Uiso 1 1 calc R U . . . C9 C -0.1610(6) 0.44822(11) -0.3349(3) 0.0426(8) Uani 1 1 d . . . . . N25 N 0.4789(8) 0.31082(11) 0.3568(3) 0.0653(11) Uani 1 1 d . . . A 1 C8 C -0.2059(5) 0.42124(10) -0.2571(3) 0.0401(7) Uani 1 1 d . . . . . H8 H -0.328300 0.423701 -0.220637 0.048 Uiso 1 1 calc R U . . . C30 C 0.4654(6) 0.20193(11) 0.6369(3) 0.0422(8) Uani 1 1 d . . . . . H30 H 0.489820 0.182527 0.691027 0.051 Uiso 1 1 calc R U . . . C11 C 0.1575(6) 0.41549(11) -0.3648(3) 0.0425(8) Uani 1 1 d . . . . . H11 H 0.280548 0.413489 -0.400934 0.051 Uiso 1 1 calc R U . . . C10 C 0.0184(7) 0.44624(11) -0.3887(3) 0.0487(9) Uani 1 1 d . . . . . H10 H 0.044385 0.465792 -0.440990 0.058 Uiso 1 1 calc R U . . . C24 C 0.6614(8) 0.31390(12) 0.4170(3) 0.0589(11) Uani 1 1 d . . . A 1 N23 N 0.8004(9) 0.34160(14) 0.3992(4) 0.0830(15) Uani 1 1 d . . . A 1 C54A C 0.5893(14) 0.4487(4) 0.0824(6) 0.0522(16) Uani 0.577(3) 1 d D U P B 1 O41A O 0.2476(11) 0.4228(2) -0.0718(4) 0.0665(16) Uani 0.577(3) 1 d D U P B 1 N46A N 0.4503(15) 0.4105(4) 0.3797(5) 0.0577(17) Uani 0.577(3) 1 d D U P B 1 C55A C 0.4018(12) 0.4283(3) 0.0965(6) 0.0496(15) Uani 0.577(3) 1 d D U P B 1 C45A C 0.4846(14) 0.4209(4) 0.2821(5) 0.0455(16) Uani 0.577(3) 1 d D U P B 1 N51A N 0.8953(14) 0.4756(4) 0.1412(7) 0.0667(18) Uani 0.577(3) 1 d D U P B 1 O46A O 0.3205(13) 0.3932(3) 0.4252(5) 0.080(2) Uani 0.577(3) 1 d D U P B 1 O42A O 0.1104(11) 0.3965(3) 0.0793(6) 0.0720(16) Uani 0.577(3) 1 d D U P B 1 C44A C 0.3450(12) 0.4137(3) 0.1924(7) 0.0491(15) Uani 0.577(3) 1 d D U P B 1 C50A C 0.7233(11) 0.4545(3) 0.1714(7) 0.0485(13) Uani 0.577(3) 1 d D U P B 1 C49A C 0.6719(11) 0.4402(2) 0.2726(6) 0.0476(13) Uani 0.577(3) 1 d D U P B 1 O47A O 0.6177(12) 0.4248(3) 0.4365(5) 0.0852(18) Uani 0.577(3) 1 d D U P B 1 N53A N 0.6579(14) 0.4628(3) -0.0085(6) 0.077(2) Uani 0.577(3) 1 d D U P B 1 N41A N 0.2584(10) 0.41727(19) 0.0247(5) 0.0567(13) Uani 0.577(3) 1 d D U P B 1 O51A O 1.0430(9) 0.48631(18) 0.1876(6) 0.0823(19) Uani 0.577(3) 1 d D U P B 1 N43A N 0.1630(11) 0.3942(2) 0.1820(6) 0.0606(16) Uani 0.577(3) 1 d D U P B 1 N48A N 0.7718(14) 0.4442(3) 0.3635(6) 0.0767(19) Uani 0.577(3) 1 d D U P B 1 O52A O 0.8563(16) 0.4801(4) 0.0358(8) 0.102(2) Uani 0.577(3) 1 d D U P B 1 C54B C 0.610(3) 0.4489(10) 0.1118(10) 0.065(4) Uani 0.248(3) 1 d D U P C 2 O41B O 0.443(3) 0.4531(6) -0.1127(8) 0.124(6) Uani 0.248(3) 1 d D U P C 2 N46B N 0.1766(16) 0.3911(4) 0.2898(7) 0.061(3) Uani 0.248(3) 1 d D U P C 2 C55B C 0.427(3) 0.4337(10) 0.0626(8) 0.072(4) Uani 0.248(3) 1 d D U P C 2 C45B C 0.310(2) 0.4083(7) 0.2273(7) 0.068(4) Uani 0.248(3) 1 d D U P C 2 N51B N 0.825(2) 0.4601(6) 0.2531(9) 0.083(4) Uani 0.248(3) 1 d D U P C 2 O46B O 0.024(3) 0.3706(9) 0.2807(12) 0.186(9) Uani 0.248(3) 1 d D U P C 2 O42B O 0.176(2) 0.4154(6) -0.0436(8) 0.083(4) Uani 0.248(3) 1 d D U P C 2 C44B C 0.2769(19) 0.4133(6) 0.1158(8) 0.069(3) Uani 0.248(3) 1 d D U P C 2 C50B C 0.638(2) 0.4430(7) 0.2207(9) 0.073(4) Uani 0.248(3) 1 d D U P C 2 C49B C 0.485(4) 0.4229(14) 0.2799(9) 0.069(5) Uani 0.248(3) 1 d D U P C 2 O47B O 0.268(2) 0.3946(6) 0.3867(8) 0.071(4) Uani 0.248(3) 1 d D U P C 2 N53B N 0.759(2) 0.4708(6) 0.0667(10) 0.080(4) Uani 0.248(3) 1 d D U P C 2 N41B N 0.366(2) 0.4353(7) -0.0373(7) 0.066(4) Uani 0.248(3) 1 d D U P C 2 O51B O 0.911(3) 0.4614(9) 0.3339(10) 0.109(6) Uani 0.248(3) 1 d D U P C 2 N43B N 0.116(3) 0.4036(10) 0.0509(9) 0.087(5) Uani 0.248(3) 1 d D U P C 2 N48B N 0.480(4) 0.4157(13) 0.3803(9) 0.074(5) Uani 0.248(3) 1 d D U P C 2 O52B O 0.896(3) 0.4759(11) 0.1623(11) 0.091(5) Uani 0.248(3) 1 d D U P C 2 C54C C 0.714(2) 0.4512(8) 0.2088(8) 0.036(3) Uani 0.176(3) 1 d D U P D 3 O41C O 0.877(3) 0.4839(11) 0.0075(11) 0.074(6) Uani 0.176(3) 1 d D U P D 3 N46C N 0.134(2) 0.3992(7) 0.1477(9) 0.055(4) Uani 0.176(3) 1 d D U P D 3 C55C C 0.631(3) 0.4506(10) 0.1061(8) 0.033(3) Uani 0.176(3) 1 d D U P D 3 C45C C 0.322(2) 0.4153(9) 0.1602(9) 0.038(3) Uani 0.176(3) 1 d D U P D 3 N51C N 0.705(3) 0.4366(9) 0.3806(8) 0.058(4) Uani 0.176(3) 1 d D U P D 3 O46C O 0.017(3) 0.3902(10) 0.0772(10) 0.106(8) Uani 0.176(3) 1 d D U P D 3 O42C O 0.5624(19) 0.4575(5) -0.0587(7) 0.056(3) Uani 0.176(3) 1 d D U P D 3 C44C C 0.441(3) 0.4327(10) 0.0784(8) 0.036(4) Uani 0.176(3) 1 d D U P D 3 C50C C 0.595(2) 0.4332(7) 0.2863(7) 0.039(3) Uani 0.176(3) 1 d D U P D 3 C49C C 0.3971(19) 0.4148(6) 0.2621(7) 0.033(3) Uani 0.176(3) 1 d D U P D 3 O47C O 0.0861(18) 0.3869(6) 0.2445(9) 0.061(3) Uani 0.176(3) 1 d D U P D 3 N53C N 0.8978(18) 0.4675(5) 0.2423(10) 0.047(3) Uani 0.176(3) 1 d D U P D 3 N41C N 0.710(2) 0.4657(7) 0.0209(8) 0.039(3) Uani 0.176(3) 1 d D U P D 3 O51C O 0.667(3) 0.4258(10) 0.4631(8) 0.078(6) Uani 0.176(3) 1 d D U P D 3 N43C N 0.398(3) 0.4370(8) -0.0239(8) 0.045(4) Uani 0.176(3) 1 d D U P D 3 N48C N 0.2647(19) 0.3975(5) 0.3230(8) 0.043(3) Uani 0.176(3) 1 d D U P D 3 O52C O 0.884(3) 0.4556(9) 0.3536(9) 0.059(4) Uani 0.176(3) 1 d D U P D 3 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O2 0.0578(16) 0.0446(14) 0.0513(15) -0.0004(11) 0.0016(12) 0.0200(12) O1 0.0491(15) 0.0518(15) 0.0571(16) -0.0053(12) 0.0177(12) 0.0069(12) O6 0.0503(15) 0.0526(16) 0.0638(17) 0.0127(13) 0.0268(13) 0.0029(12) O29 0.0455(15) 0.0638(18) 0.075(2) -0.0157(15) 0.0181(14) -0.0103(13) O30 0.078(2) 0.0478(16) 0.0533(16) 0.0068(13) 0.0107(14) -0.0168(14) N1 0.0440(15) 0.0393(15) 0.0439(15) -0.0070(12) 0.0044(12) 0.0084(12) N6 0.0455(16) 0.0385(15) 0.0469(16) 0.0066(12) 0.0146(13) 0.0009(12) O21 0.0488(16) 0.069(2) 0.091(2) -0.0361(18) -0.0005(16) -0.0049(14) O10 0.089(2) 0.0507(17) 0.070(2) 0.0207(15) 0.0136(17) 0.0231(16) O9 0.0588(18) 0.0553(18) 0.091(2) 0.0112(16) 0.0171(17) 0.0215(14) O26 0.099(3) 0.0557(18) 0.0527(17) -0.0048(14) -0.0329(17) 0.0152(17) N29 0.0465(17) 0.0475(17) 0.0438(16) -0.0103(13) 0.0138(13) -0.0084(13) O22 0.089(3) 0.0565(19) 0.098(3) -0.0302(18) 0.048(2) -0.0388(18) N5 0.0598(19) 0.0388(16) 0.0541(18) 0.0128(13) 0.0172(15) 0.0088(14) N21 0.0538(19) 0.0480(18) 0.073(2) -0.0279(17) 0.0233(18) -0.0145(15) N26 0.079(2) 0.0361(15) 0.0369(15) -0.0005(12) -0.0058(15) 0.0054(15) N9 0.063(2) 0.0393(16) 0.060(2) 0.0055(14) 0.0112(16) 0.0143(15) C12 0.0369(15) 0.0295(14) 0.0354(15) -0.0035(12) 0.0053(12) 0.0000(12) N3 0.064(2) 0.0476(18) 0.0500(18) 0.0056(14) 0.0079(16) 0.0166(15) C27 0.0496(18) 0.0311(15) 0.0307(15) -0.0050(12) 0.0023(13) 0.0055(13) C7 0.0380(16) 0.0305(15) 0.0382(16) 0.0013(12) 0.0084(13) -0.0006(12) C28 0.0397(16) 0.0379(16) 0.0369(16) -0.0101(13) -0.0002(13) 0.0036(13) C13 0.0380(16) 0.0331(15) 0.0373(16) -0.0049(12) 0.0027(13) 0.0029(12) C32 0.0415(16) 0.0315(15) 0.0376(16) -0.0104(12) 0.0076(13) -0.0004(12) C33 0.0503(19) 0.0344(16) 0.0473(19) -0.0150(14) 0.0150(15) -0.0045(14) C4 0.0512(19) 0.0354(17) 0.0414(17) 0.0015(14) 0.0042(15) 0.0061(14) C29 0.0439(17) 0.0354(16) 0.0334(15) -0.0061(12) 0.0077(13) -0.0025(13) C31 0.0441(18) 0.0401(18) 0.0395(17) -0.0071(14) -0.0040(14) 0.0007(14) C9 0.0485(19) 0.0329(16) 0.0470(19) 0.0017(14) 0.0069(15) 0.0069(14) N25 0.111(3) 0.0425(18) 0.0423(18) 0.0024(14) 0.007(2) 0.000(2) C8 0.0392(17) 0.0346(16) 0.0471(18) -0.0010(14) 0.0085(14) 0.0033(13) C30 0.054(2) 0.0386(17) 0.0335(16) -0.0020(13) -0.0001(14) -0.0009(15) C11 0.0459(18) 0.0392(17) 0.0437(18) 0.0025(14) 0.0162(15) 0.0024(14) C10 0.065(2) 0.0356(17) 0.047(2) 0.0084(15) 0.0166(17) 0.0067(16) C24 0.093(3) 0.0364(19) 0.050(2) -0.0058(16) 0.027(2) -0.007(2) N23 0.127(4) 0.055(2) 0.070(3) -0.010(2) 0.037(3) -0.028(3) C54A 0.065(4) 0.042(4) 0.050(3) -0.001(3) 0.006(3) 0.020(3) O41A 0.091(4) 0.062(4) 0.045(2) -0.010(2) -0.020(3) 0.026(3) N46A 0.069(4) 0.053(4) 0.051(3) -0.010(3) 0.004(2) 0.018(3) C55A 0.057(3) 0.042(4) 0.048(3) -0.012(3) -0.011(3) 0.018(3) C45A 0.056(3) 0.042(4) 0.040(2) -0.007(3) 0.009(2) 0.017(3) N51A 0.057(3) 0.052(4) 0.091(4) -0.017(3) 0.007(3) 0.012(3) O46A 0.115(5) 0.069(4) 0.060(4) 0.008(3) 0.041(4) 0.022(4) O42A 0.067(3) 0.066(4) 0.081(3) -0.009(3) -0.006(3) 0.007(3) C44A 0.046(3) 0.039(3) 0.062(3) -0.008(4) 0.004(3) 0.008(3) C50A 0.046(3) 0.035(3) 0.064(3) -0.010(3) 0.006(3) 0.011(2) C49A 0.047(3) 0.038(3) 0.057(3) -0.020(3) -0.009(2) 0.017(2) O47A 0.100(4) 0.080(4) 0.071(3) -0.026(3) -0.041(3) 0.033(3) N53A 0.095(4) 0.068(4) 0.067(3) 0.004(4) 0.005(3) 0.023(4) N41A 0.065(3) 0.052(3) 0.052(2) -0.008(2) -0.013(2) 0.017(2) O51A 0.057(3) 0.054(3) 0.135(5) -0.038(3) -0.005(3) 0.003(2) N43A 0.059(3) 0.055(3) 0.067(3) -0.008(3) -0.001(3) 0.006(3) N48A 0.082(4) 0.069(4) 0.076(3) -0.020(3) -0.021(3) 0.020(3) O52A 0.112(5) 0.097(5) 0.100(4) 0.016(4) 0.027(3) -0.001(4) C54B 0.069(6) 0.057(7) 0.068(5) 0.003(5) 0.013(4) 0.008(5) O41B 0.146(11) 0.130(11) 0.100(8) 0.015(8) 0.035(9) 0.018(8) N46B 0.060(5) 0.049(5) 0.073(5) -0.007(5) 0.009(4) 0.021(4) C55B 0.072(6) 0.068(7) 0.075(5) -0.005(5) 0.003(4) 0.007(5) C45B 0.073(6) 0.061(7) 0.071(4) -0.004(5) 0.005(4) 0.019(5) N51B 0.079(6) 0.078(7) 0.091(5) -0.006(5) 0.002(4) 0.006(5) O46B 0.155(11) 0.202(14) 0.200(13) -0.004(11) -0.010(8) -0.089(10) O42B 0.085(6) 0.078(7) 0.082(5) -0.013(5) -0.019(4) 0.014(5) C44B 0.070(5) 0.064(6) 0.072(4) -0.004(5) 0.004(4) 0.008(5) C50B 0.076(6) 0.071(7) 0.072(5) -0.003(5) 0.005(4) 0.007(5) C49B 0.075(6) 0.069(8) 0.065(5) 0.001(6) 0.008(4) 0.009(6) O47B 0.080(6) 0.057(6) 0.076(5) 0.009(5) 0.017(4) 0.012(5) N53B 0.076(6) 0.076(7) 0.089(5) 0.005(5) 0.019(5) -0.003(5) N41B 0.073(6) 0.052(6) 0.073(5) -0.007(5) 0.001(4) 0.023(5) O51B 0.107(10) 0.098(12) 0.117(7) -0.015(9) -0.032(8) 0.027(9) N43B 0.081(6) 0.084(8) 0.095(6) -0.005(6) -0.003(4) 0.001(5) N48B 0.077(6) 0.076(8) 0.070(5) -0.006(5) 0.002(4) 0.005(5) O52B 0.080(6) 0.086(8) 0.109(6) -0.006(6) 0.011(5) -0.003(5) C54C 0.034(5) 0.028(6) 0.046(4) -0.008(5) 0.003(4) 0.003(5) O41C 0.079(8) 0.068(11) 0.080(11) -0.001(9) 0.031(7) -0.016(8) N46C 0.054(5) 0.054(7) 0.057(5) -0.002(5) 0.002(4) -0.001(5) C55C 0.035(5) 0.025(6) 0.040(4) -0.002(5) 0.008(4) 0.011(5) C45C 0.039(5) 0.033(6) 0.042(4) -0.004(5) 0.005(4) 0.011(5) N51C 0.061(6) 0.054(7) 0.058(5) -0.007(5) -0.007(4) 0.003(5) O46C 0.093(11) 0.123(14) 0.100(8) -0.011(10) -0.029(9) -0.023(10) O42C 0.065(5) 0.058(6) 0.044(4) 0.001(5) -0.005(4) 0.012(5) C44C 0.040(6) 0.035(7) 0.033(4) -0.008(5) 0.000(4) 0.011(5) C50C 0.042(5) 0.035(6) 0.040(4) -0.003(5) 0.005(4) 0.007(5) C49C 0.037(5) 0.025(6) 0.038(4) 0.002(5) 0.012(4) 0.011(4) O47C 0.055(5) 0.058(6) 0.072(5) 0.003(5) 0.018(4) -0.011(5) N53C 0.044(5) 0.036(6) 0.061(5) -0.015(5) 0.000(4) 0.006(4) N41C 0.044(5) 0.032(6) 0.042(5) 0.002(5) 0.005(4) 0.012(4) O51C 0.084(11) 0.088(11) 0.057(6) -0.002(9) -0.029(7) -0.002(9) N43C 0.059(6) 0.038(6) 0.038(4) -0.003(5) -0.002(4) 0.015(5) N48C 0.047(5) 0.035(6) 0.048(4) -0.001(5) 0.016(4) 0.006(4) O52C 0.055(5) 0.056(7) 0.065(5) -0.008(5) -0.011(4) 0.009(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3 O2 N1 108.7(2) . . ? O1 N1 C13 136.2(3) . . ? O1 N1 O2 117.5(3) . . ? C13 N1 O2 106.3(3) . . ? O6 N6 N5 118.6(3) . . ? O6 N6 C7 116.6(3) . . ? N5 N6 C7 124.8(3) . . ? O30 N29 O29 124.3(3) . . ? O30 N29 C29 117.6(3) . . ? O29 N29 C29 118.2(3) . . ? N23 O22 N21 108.8(3) . . ? N6 N5 C4 114.8(3) . . ? O21 N21 C33 136.9(4) . . ? O21 N21 O22 118.2(4) . . ? C33 N21 O22 104.9(4) . . ? O26 N26 N25 118.9(3) . . ? O26 N26 C27 116.0(3) . . ? N25 N26 C27 125.1(4) . . ? O10 N9 O9 123.8(3) . . ? O10 N9 C9 118.7(3) . . ? O9 N9 C9 117.5(3) . . ? C11 C12 C7 119.7(3) . . ? C11 C12 C13 126.3(3) . . ? C7 C12 C13 113.9(3) . . ? C4 N3 O2 104.6(3) . . ? C28 C27 C32 121.5(3) . . ? C28 C27 N26 117.7(3) . . ? C32 C27 N26 120.8(3) . . ? C8 C7 C12 121.4(3) . . ? C8 C7 N6 117.8(3) . . ? C12 C7 N6 120.8(3) . . ? C29 C28 C27 116.4(3) . . ? C29 C28 H28 121.8 . . ? C27 C28 H28 121.8 . . ? N1 C13 C4 107.1(3) . . ? N1 C13 C12 132.3(3) . . ? C4 C13 C12 120.4(3) . . ? C31 C32 C27 120.0(3) . . ? C31 C32 C33 125.7(3) . . ? C27 C32 C33 114.2(3) . . ? N21 C33 C24 107.7(4) . . ? N21 C33 C32 131.5(4) . . ? C24 C33 C32 120.7(4) . . ? N3 C4 N5 121.4(3) . . ? N3 C4 C13 113.4(3) . . ? N5 C4 C13 125.2(3) . . ? C28 C29 C30 123.9(3) . . ? C28 C29 N29 118.4(3) . . ? C30 C29 N29 117.6(3) . . ? C32 C31 C30 119.4(3) . . ? C32 C31 H31 120.3 . . ? C30 C31 H31 120.3 . . ? C8 C9 C10 123.3(3) . . ? C8 C9 N9 117.8(3) . . ? C10 C9 N9 118.9(3) . . ? N26 N25 C24 114.5(3) . . ? C9 C8 C7 116.9(3) . . ? C9 C8 H8 121.5 . . ? C7 C8 H8 121.5 . . ? C29 C30 C31 118.7(3) . . ? C29 C30 H30 120.7 . . ? C31 C30 H30 120.7 . . ? C10 C11 C12 119.7(3) . . ? C10 C11 H11 120.1 . . ? C12 C11 H11 120.1 . . ? C11 C10 C9 118.8(3) . . ? C11 C10 H10 120.6 . . ? C9 C10 H10 120.6 . . ? N23 C24 N25 122.1(5) . . ? N23 C24 C33 113.4(5) . . ? N25 C24 C33 124.5(4) . . ? C24 N23 O22 105.2(4) . . ? N53A C54A C55A 126.6(8) . . ? N53A C54A C50A 116.1(8) . . ? C55A C54A C50A 117.3(7) . . ? O46A N46A C45A 137.7(8) . . ? O46A N46A O47A 117.4(7) . . ? C45A N46A O47A 104.9(7) . . ? N41A C55A C44A 108.7(7) . . ? N41A C55A C54A 128.2(8) . . ? C44A C55A C54A 123.0(7) . . ? N46A C45A C49A 112.8(7) . . ? N46A C45A C44A 125.8(7) . . ? C49A C45A C44A 121.4(7) . . ? O51A N51A O52A 125.8(9) . . ? O51A N51A C50A 131.5(9) . . ? O52A N51A C50A 102.6(8) . . ? N43A O42A N41A 112.0(6) . . ? N43A C44A C55A 110.1(7) . . ? N43A C44A C45A 131.8(7) . . ? C55A C44A C45A 118.1(7) . . ? N51A C50A C54A 108.0(8) . . ? N51A C50A C49A 130.0(7) . . ? C54A C50A C49A 122.0(7) . . ? N48A C49A C45A 111.3(8) . . ? N48A C49A C50A 130.4(8) . . ? C45A C49A C50A 118.2(7) . . ? N46A O47A N48A 109.6(5) . . ? C54A N53A O52A 96.4(7) . . ? O41A N41A C55A 130.9(7) . . ? O41A N41A O42A 124.3(6) . . ? C55A N41A O42A 104.8(6) . . ? C44A N43A O42A 104.5(7) . . ? C49A N48A O47A 101.3(7) . . ? N51A O52A N53A 116.8(8) . . ? N53B C54B C55B 126.4(9) . . ? N53B C54B C50B 116.0(8) . . ? C55B C54B C50B 117.5(7) . . ? O46B N46B C45B 137.1(9) . . ? O46B N46B O47B 117.3(8) . . ? C45B N46B O47B 104.7(7) . . ? N41B C55B C44B 108.3(7) . . ? N41B C55B C54B 128.8(8) . . ? C44B C55B C54B 122.8(7) . . ? N46B C45B C49B 113.0(7) . . ? N46B C45B C44B 125.3(7) . . ? C49B C45B C44B 121.7(8) . . ? O51B N51B O52B 125.9(10) . . ? O51B N51B C50B 131.5(10) . . ? O52B N51B C50B 102.6(8) . . ? N43B O42B N41B 111.8(6) . . ? N43B C44B C55B 110.3(7) . . ? N43B C44B C45B 131.5(8) . . ? C55B C44B C45B 118.1(7) . . ? N51B C50B C54B 108.1(8) . . ? N51B C50B C49B 130.0(8) . . ? C54B C50B C49B 121.9(7) . . ? N48B C49B C45B 111.2(8) . . ? N48B C49B C50B 130.7(8) . . ? C45B C49B C50B 118.0(7) . . ? N46B O47B N48B 109.7(6) . . ? C54B N53B O52B 96.4(7) . . ? O41B N41B C55B 131.1(8) . . ? O41B N41B O42B 123.6(7) . . ? C55B N41B O42B 105.0(6) . . ? C44B N43B O42B 104.3(7) . . ? C49B N48B O47B 101.3(7) . . ? N51B O52B N53B 116.8(8) . . ? N53C C54C C55C 126.7(8) . . ? N53C C54C C50C 116.0(8) . . ? C55C C54C C50C 117.3(7) . . ? O46C N46C C45C 137.4(9) . . ? O46C N46C O47C 117.4(8) . . ? C45C N46C O47C 104.8(7) . . ? N41C C55C C44C 108.4(7) . . ? N41C C55C C54C 128.8(8) . . ? C44C C55C C54C 122.8(7) . . ? N46C C45C C49C 112.8(8) . . ? N46C C45C C44C 125.7(7) . . ? C49C C45C C44C 121.5(8) . . ? O51C N51C O52C 126.1(10) . . ? O51C N51C C50C 131.3(10) . . ? O52C N51C C50C 102.6(8) . . ? N43C O42C N41C 111.9(6) . . ? N43C C44C C55C 110.3(7) . . ? N43C C44C C45C 131.4(8) . . ? C55C C44C C45C 118.2(7) . . ? N51C C50C C54C 108.2(8) . . ? N51C C50C C49C 129.8(8) . . ? C54C C50C C49C 122.1(7) . . ? N48C C49C C45C 111.4(8) . . ? N48C C49C C50C 130.5(8) . . ? C45C C49C C50C 118.1(7) . . ? N46C O47C N48C 109.8(6) . . ? C54C N53C O52C 96.4(7) . . ? O41C N41C C55C 131.3(8) . . ? O41C N41C O42C 123.7(7) . . ? C55C N41C O42C 105.0(6) . . ? C44C N43C O42C 104.3(7) . . ? C49C N48C O47C 101.2(7) . . ? N51C O52C N53C 116.8(8) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O2 N3 1.379(4) . ? O2 N1 1.461(4) . ? O1 N1 1.221(4) . ? O6 N6 1.250(4) . ? O29 N29 1.223(4) . ? O30 N29 1.221(5) . ? N1 C13 1.309(4) . ? N6 N5 1.301(4) . ? N6 C7 1.458(4) . ? O21 N21 1.220(5) . ? O10 N9 1.222(5) . ? O9 N9 1.231(5) . ? O26 N26 1.243(5) . ? N29 C29 1.471(4) . ? O22 N23 1.362(7) . ? O22 N21 1.480(5) . ? N5 C4 1.375(5) . ? N21 C33 1.314(5) . ? N26 N25 1.303(5) . ? N26 C27 1.443(4) . ? N9 C9 1.466(5) . ? C12 C11 1.392(5) . ? C12 C7 1.402(4) . ? C12 C13 1.431(4) . ? N3 C4 1.315(5) . ? C27 C28 1.382(5) . ? C27 C32 1.397(5) . ? C7 C8 1.379(5) . ? C28 C29 1.376(5) . ? C28 H28 0.9500 . ? C13 C4 1.400(5) . ? C32 C31 1.383(5) . ? C32 C33 1.425(5) . ? C33 C24 1.393(6) . ? C29 C30 1.379(5) . ? C31 C30 1.384(5) . ? C31 H31 0.9500 . ? C9 C8 1.378(5) . ? C9 C10 1.390(5) . ? N25 C24 1.392(7) . ? C8 H8 0.9500 . ? C30 H30 0.9500 . ? C11 C10 1.375(5) . ? C11 H11 0.9500 . ? C10 H10 0.9500 . ? C24 N23 1.306(6) . ? C54A N53A 1.358(10) . ? C54A C55A 1.411(10) . ? C54A C50A 1.422(10) . ? O41A N41A 1.259(8) . ? N46A O46A 1.196(9) . ? N46A C45A 1.336(9) . ? N46A O47A 1.365(10) . ? C55A N41A 1.333(8) . ? C55A C44A 1.394(11) . ? C45A C49A 1.383(11) . ? C45A C44A 1.457(10) . ? N51A O51A 1.162(9) . ? N51A O52A 1.381(14) . ? N51A C50A 1.387(11) . ? O42A N43A 1.358(10) . ? O42A N41A 1.397(10) . ? C44A N43A 1.345(9) . ? C50A C49A 1.444(10) . ? C49A N48A 1.322(9) . ? O47A N48A 1.546(12) . ? N53A O52A 1.496(13) . ? C54B N53B 1.358(10) . ? C54B C55B 1.411(10) . ? C54B C50B 1.424(10) . ? O41B N41B 1.259(8) . ? N46B O46B 1.198(10) . ? N46B C45B 1.336(9) . ? N46B O47B 1.364(10) . ? C55B N41B 1.333(8) . ? C55B C44B 1.394(11) . ? C45B C49B 1.382(11) . ? C45B C44B 1.456(10) . ? N51B O51B 1.161(9) . ? N51B O52B 1.381(14) . ? N51B C50B 1.387(11) . ? O42B N43B 1.356(10) . ? O42B N41B 1.398(10) . ? C44B N43B 1.346(10) . ? C50B C49B 1.444(10) . ? C49B N48B 1.322(10) . ? O47B N48B 1.546(12) . ? N53B O52B 1.497(13) . ? C54C N53C 1.358(10) . ? C54C C55C 1.411(10) . ? C54C C50C 1.423(10) . ? O41C N41C 1.259(8) . ? N46C O46C 1.197(10) . ? N46C C45C 1.336(9) . ? N46C O47C 1.365(10) . ? C55C N41C 1.333(8) . ? C55C C44C 1.395(11) . ? C45C C49C 1.382(11) . ? C45C C44C 1.456(10) . ? N51C O51C 1.161(9) . ? N51C O52C 1.381(14) . ? N51C C50C 1.387(11) . ? O42C N43C 1.357(10) . ? O42C N41C 1.398(10) . ? C44C N43C 1.346(10) . ? C50C C49C 1.444(10) . ? C49C N48C 1.322(10) . ? O47C N48C 1.545(12) . ? N53C O52C 1.498(13) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N3 O2 N1 O1 -179.7(3) . . . . ? N3 O2 N1 C13 0.1(4) . . . . ? O6 N6 N5 C4 -179.7(3) . . . . ? C7 N6 N5 C4 0.3(5) . . . . ? N23 O22 N21 O21 -178.9(4) . . . . ? N23 O22 N21 C33 0.2(4) . . . . ? N1 O2 N3 C4 -0.3(4) . . . . ? O26 N26 C27 C28 3.0(5) . . . . ? N25 N26 C27 C28 -176.1(3) . . . . ? O26 N26 C27 C32 -179.4(3) . . . . ? N25 N26 C27 C32 1.5(5) . . . . ? C11 C12 C7 C8 -0.4(5) . . . . ? C13 C12 C7 C8 -178.6(3) . . . . ? C11 C12 C7 N6 179.5(3) . . . . ? C13 C12 C7 N6 1.3(4) . . . . ? O6 N6 C7 C8 -2.2(5) . . . . ? N5 N6 C7 C8 177.8(4) . . . . ? O6 N6 C7 C12 177.9(3) . . . . ? N5 N6 C7 C12 -2.1(5) . . . . ? C32 C27 C28 C29 -1.1(5) . . . . ? N26 C27 C28 C29 176.5(3) . . . . ? O1 N1 C13 C4 180.0(4) . . . . ? O2 N1 C13 C4 0.2(4) . . . . ? O1 N1 C13 C12 4.9(7) . . . . ? O2 N1 C13 C12 -174.9(3) . . . . ? C11 C12 C13 N1 -2.6(6) . . . . ? C7 C12 C13 N1 175.5(4) . . . . ? C11 C12 C13 C4 -177.1(3) . . . . ? C7 C12 C13 C4 1.0(5) . . . . ? C28 C27 C32 C31 -0.1(5) . . . . ? N26 C27 C32 C31 -177.6(3) . . . . ? C28 C27 C32 C33 -179.8(3) . . . . ? N26 C27 C32 C33 2.8(4) . . . . ? O21 N21 C33 C24 178.3(4) . . . . ? O22 N21 C33 C24 -0.6(4) . . . . ? O21 N21 C33 C32 1.1(7) . . . . ? O22 N21 C33 C32 -177.8(3) . . . . ? C31 C32 C33 N21 -6.4(6) . . . . ? C27 C32 C33 N21 173.2(3) . . . . ? C31 C32 C33 C24 176.6(3) . . . . ? C27 C32 C33 C24 -3.7(5) . . . . ? O2 N3 C4 N5 178.8(3) . . . . ? O2 N3 C4 C13 0.5(4) . . . . ? N6 N5 C4 N3 -175.9(4) . . . . ? N6 N5 C4 C13 2.2(6) . . . . ? N1 C13 C4 N3 -0.5(4) . . . . ? C12 C13 C4 N3 175.3(3) . . . . ? N1 C13 C4 N5 -178.7(4) . . . . ? C12 C13 C4 N5 -2.9(6) . . . . ? C27 C28 C29 C30 1.0(5) . . . . ? C27 C28 C29 N29 -175.3(3) . . . . ? O30 N29 C29 C28 165.5(3) . . . . ? O29 N29 C29 C28 -14.1(5) . . . . ? O30 N29 C29 C30 -11.0(5) . . . . ? O29 N29 C29 C30 169.4(3) . . . . ? C27 C32 C31 C30 1.4(5) . . . . ? C33 C32 C31 C30 -179.0(3) . . . . ? O10 N9 C9 C8 176.3(4) . . . . ? O9 N9 C9 C8 -3.0(6) . . . . ? O10 N9 C9 C10 -2.5(6) . . . . ? O9 N9 C9 C10 178.3(4) . . . . ? O26 N26 N25 C24 176.5(3) . . . . ? C27 N26 N25 C24 -4.5(6) . . . . ? C10 C9 C8 C7 -1.4(6) . . . . ? N9 C9 C8 C7 179.8(3) . . . . ? C12 C7 C8 C9 1.0(5) . . . . ? N6 C7 C8 C9 -178.9(3) . . . . ? C28 C29 C30 C31 0.2(5) . . . . ? N29 C29 C30 C31 176.6(3) . . . . ? C32 C31 C30 C29 -1.4(5) . . . . ? C7 C12 C11 C10 0.1(5) . . . . ? C13 C12 C11 C10 178.1(4) . . . . ? C12 C11 C10 C9 -0.4(6) . . . . ? C8 C9 C10 C11 1.2(6) . . . . ? N9 C9 C10 C11 179.9(4) . . . . ? N26 N25 C24 N23 -174.1(4) . . . . ? N26 N25 C24 C33 3.4(6) . . . . ? N21 C33 C24 N23 0.8(5) . . . . ? C32 C33 C24 N23 178.4(4) . . . . ? N21 C33 C24 N25 -176.9(4) . . . . ? C32 C33 C24 N25 0.7(6) . . . . ? N25 C24 N23 O22 177.1(4) . . . . ? C33 C24 N23 O22 -0.7(5) . . . . ? N21 O22 N23 C24 0.3(5) . . . . ? N53A C54A C55A N41A 3(2) . . . . ? C50A C54A C55A N41A -175.8(10) . . . . ? N53A C54A C55A C44A 178.2(12) . . . . ? C50A C54A C55A C44A -0.4(17) . . . . ? O46A N46A C45A C49A -177.5(15) . . . . ? O47A N46A C45A C49A 2.0(15) . . . . ? O46A N46A C45A C44A 3(3) . . . . ? O47A N46A C45A C44A -177.5(13) . . . . ? N41A C55A C44A N43A -1.4(12) . . . . ? C54A C55A C44A N43A -177.6(10) . . . . ? N41A C55A C44A C45A 177.7(10) . . . . ? C54A C55A C44A C45A 1.5(17) . . . . ? N46A C45A C44A N43A -4(2) . . . . ? C49A C45A C44A N43A 176.4(11) . . . . ? N46A C45A C44A C55A 177.0(13) . . . . ? C49A C45A C44A C55A -2.4(18) . . . . ? O51A N51A C50A C54A -178.8(13) . . . . ? O52A N51A C50A C54A -1.7(13) . . . . ? O51A N51A C50A C49A 2(2) . . . . ? O52A N51A C50A C49A 179.3(10) . . . . ? N53A C54A C50A N51A 2.3(14) . . . . ? C55A C54A C50A N51A -179.0(10) . . . . ? N53A C54A C50A C49A -178.6(9) . . . . ? C55A C54A C50A C49A 0.1(15) . . . . ? N46A C45A C49A N48A -0.6(15) . . . . ? C44A C45A C49A N48A 178.9(11) . . . . ? N46A C45A C49A C50A -177.3(10) . . . . ? C44A C45A C49A C50A 2.2(17) . . . . ? N51A C50A C49A N48A 1.9(16) . . . . ? C54A C50A C49A N48A -177.0(10) . . . . ? N51A C50A C49A C45A 177.8(12) . . . . ? C54A C50A C49A C45A -1.1(14) . . . . ? O46A N46A O47A N48A 177.2(11) . . . . ? C45A N46A O47A N48A -2.4(13) . . . . ? C55A C54A N53A O52A 179.8(13) . . . . ? C50A C54A N53A O52A -1.7(13) . . . . ? C44A C55A N41A O41A -178.0(8) . . . . ? C54A C55A N41A O41A -2.0(17) . . . . ? C44A C55A N41A O42A 1.3(11) . . . . ? C54A C55A N41A O42A 177.3(11) . . . . ? N43A O42A N41A O41A 178.5(7) . . . . ? N43A O42A N41A C55A -0.9(10) . . . . ? C55A C44A N43A O42A 0.8(11) . . . . ? C45A C44A N43A O42A -178.1(13) . . . . ? N41A O42A N43A C44A 0.1(10) . . . . ? C45A C49A N48A O47A -0.8(11) . . . . ? C50A C49A N48A O47A 175.3(8) . . . . ? N46A O47A N48A C49A 2.1(11) . . . . ? O51A N51A O52A N53A 178.1(12) . . . . ? C50A N51A O52A N53A 0.7(16) . . . . ? C54A N53A O52A N51A 0.5(15) . . . . ? N53B C54B C55B N41B 4(6) . . . . ? C50B C54B C55B N41B -180(3) . . . . ? N53B C54B C55B C44B -177(3) . . . . ? C50B C54B C55B C44B -1(5) . . . . ? O46B N46B C45B C49B -168(3) . . . . ? O47B N46B C45B C49B 0(3) . . . . ? O46B N46B C45B C44B 14(4) . . . . ? O47B N46B C45B C44B -178(2) . . . . ? N41B C55B C44B N43B -3(4) . . . . ? C54B C55B C44B N43B 178(3) . . . . ? N41B C55B C44B C45B -179(2) . . . . ? C54B C55B C44B C45B 1(4) . . . . ? N46B C45B C44B N43B 2(4) . . . . ? C49B C45B C44B N43B -176(4) . . . . ? N46B C45B C44B C55B 177(2) . . . . ? C49B C45B C44B C55B -1(4) . . . . ? O51B N51B C50B C54B -178(4) . . . . ? O52B N51B C50B C54B 1(3) . . . . ? O51B N51B C50B C49B 3(6) . . . . ? O52B N51B C50B C49B -178(4) . . . . ? N53B C54B C50B N51B -4(4) . . . . ? C55B C54B C50B N51B -180(3) . . . . ? N53B C54B C50B C49B 175(3) . . . . ? C55B C54B C50B C49B -1(5) . . . . ? N46B C45B C49B N48B 1(5) . . . . ? C44B C45B C49B N48B 179(3) . . . . ? N46B C45B C49B C50B -179(3) . . . . ? C44B C45B C49B C50B -1(5) . . . . ? N51B C50B C49B N48B 1(8) . . . . ? C54B C50B C49B N48B -178(5) . . . . ? N51B C50B C49B C45B -180(3) . . . . ? C54B C50B C49B C45B 1(6) . . . . ? O46B N46B O47B N48B 170(3) . . . . ? C45B N46B O47B N48B -1(3) . . . . ? C55B C54B N53B O52B 179(4) . . . . ? C50B C54B N53B O52B 4(3) . . . . ? C44B C55B N41B O41B 174(3) . . . . ? C54B C55B N41B O41B -7(6) . . . . ? C44B C55B N41B O42B 0(3) . . . . ? C54B C55B N41B O42B 179(3) . . . . ? N43B O42B N41B O41B -172(3) . . . . ? N43B O42B N41B C55B 3(3) . . . . ? C55B C44B N43B O42B 4(3) . . . . ? C45B C44B N43B O42B -180(2) . . . . ? N41B O42B N43B C44B -5(3) . . . . ? C45B C49B N48B O47B -1(5) . . . . ? C50B C49B N48B O47B 178(4) . . . . ? N46B O47B N48B C49B 1(4) . . . . ? O51B N51B O52B N53B -180(3) . . . . ? C50B N51B O52B N53B 1(4) . . . . ? C54B N53B O52B N51B -3(4) . . . . ? N53C C54C C55C N41C -1(6) . . . . ? C50C C54C C55C N41C 179(3) . . . . ? N53C C54C C55C C44C 179(3) . . . . ? C50C C54C C55C C44C -1(5) . . . . ? O46C N46C C45C C49C -173(4) . . . . ? O47C N46C C45C C49C -1(3) . . . . ? O46C N46C C45C C44C 8(6) . . . . ? O47C N46C C45C C44C 180(3) . . . . ? N41C C55C C44C N43C -1(4) . . . . ? C54C C55C C44C N43C 179(3) . . . . ? N41C C55C C44C C45C -178(3) . . . . ? C54C C55C C44C C45C 2(5) . . . . ? N46C C45C C44C N43C 0(6) . . . . ? C49C C45C C44C N43C -179(3) . . . . ? N46C C45C C44C C55C 176(3) . . . . ? C49C C45C C44C C55C -3(5) . . . . ? O51C N51C C50C C54C -179(4) . . . . ? O52C N51C C50C C54C -1(3) . . . . ? O51C N51C C50C C49C 0(6) . . . . ? O52C N51C C50C C49C 178(3) . . . . ? N53C C54C C50C N51C -1(3) . . . . ? C55C C54C C50C N51C 179(3) . . . . ? N53C C54C C50C C49C 180(2) . . . . ? C55C C54C C50C C49C 0(4) . . . . ? N46C C45C C49C N48C 1(3) . . . . ? C44C C45C C49C N48C -180(3) . . . . ? N46C C45C C49C C50C -177(2) . . . . ? C44C C45C C49C C50C 2(4) . . . . ? N51C C50C C49C N48C 2(4) . . . . ? C54C C50C C49C N48C -178(2) . . . . ? N51C C50C C49C C45C -180(3) . . . . ? C54C C50C C49C C45C -1(4) . . . . ? O46C N46C O47C N48C 174(3) . . . . ? C45C N46C O47C N48C 1(3) . . . . ? C55C C54C N53C O52C -178(3) . . . . ? C50C C54C N53C O52C 2(3) . . . . ? C44C C55C N41C O41C -179(4) . . . . ? C54C C55C N41C O41C 1(6) . . . . ? C44C C55C N41C O42C 1(3) . . . . ? C54C C55C N41C O42C -179(3) . . . . ? N43C O42C N41C O41C 179(3) . . . . ? N43C O42C N41C C55C -1(3) . . . . ? C55C C44C N43C O42C 0(4) . . . . ? C45C C44C N43C O42C 176(3) . . . . ? N41C O42C N43C C44C 1(3) . . . . ? C45C C49C N48C O47C 0(2) . . . . ? C50C C49C N48C O47C 177(2) . . . . ? N46C O47C N48C C49C 0(2) . . . . ? O51C N51C O52C N53C -179(3) . . . . ? C50C N51C O52C N53C 3(4) . . . . ? C54C N53C O52C N51C -3(3) . . . . ?