#------------------------------------------------------------------------------ #$Date: 2024-12-05 01:32:01 +0200 (Thu, 05 Dec 2024) $ #$Revision: 296221 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/96/7249664.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7249664 loop_ _publ_author_name 'Kim, Seulgi' 'Ju, Kyunghye' 'Kim, Taehun' 'Park, In-Hyeok' _publ_section_title ; An unsymmetrically sandwiched bis(O3S2-macrocycle) lead(ii) complex via an endo/exo-coordination mode ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D4CE01045K _journal_year 2025 _chemical_formula_moiety '2(C40 H48 Cl O10 Pb S4), 2(Cl O4), C H2 Cl2, C N, C H3' _chemical_formula_sum 'C83 H101 Cl6 N O28 Pb2 S8' _chemical_formula_weight 2444.20 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2024-11-11 deposited with the CCDC. 2024-11-25 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 112.9730(10) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 15.4259(2) _cell_length_b 21.5068(3) _cell_length_c 15.6995(2) _cell_measurement_reflns_used 5277 _cell_measurement_temperature 173(2) _cell_measurement_theta_max 22.13 _cell_measurement_theta_min 2.36 _cell_volume 4795.40(12) _computing_cell_refinement 'Bruker APEX software' _computing_data_collection 'Bruker APEX software' _computing_data_reduction 'Bruker APEX software' _computing_molecular_graphics ORTEP _computing_publication_material CIFTAB _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXS-2013/1 (Sheldrick, 2013)' _diffrn_ambient_temperature 173(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'PHOTON detectors' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0726 _diffrn_reflns_av_unetI/netI 0.0599 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 26 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 42433 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.999 _diffrn_reflns_theta_min 1.570 _diffrn_source 'Microfocus X-ray sources' _exptl_absorpt_coefficient_mu 3.923 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_correction_T_min 0.5018 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.693 _exptl_crystal_description block _exptl_crystal_F_000 2448 _exptl_crystal_size_max 0.240 _exptl_crystal_size_mid 0.210 _exptl_crystal_size_min 0.150 _refine_diff_density_max 0.944 _refine_diff_density_min -1.139 _refine_diff_density_rms 0.115 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.031 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 605 _refine_ls_number_reflns 9419 _refine_ls_number_restraints 39 _refine_ls_restrained_S_all 1.032 _refine_ls_R_factor_all 0.0553 _refine_ls_R_factor_gt 0.0369 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0285P)^2^+2.7991P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0745 _refine_ls_wR_factor_ref 0.0807 _reflns_Friedel_coverage 0.000 _reflns_number_gt 7346 _reflns_number_total 9419 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4ce01045k2.cif _cod_data_source_block 1 _cod_depositor_comments ; The following automatic conversions were performed: data item '_exptl_absorpt_correction_type' value 'MULTI-SCAN' was changed to 'multi-scan' in accordance with the /home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 last updated on 2011-04-26. Automatic conversion script Id: cif_fix_values 8170 2020-07-09 18:12:32Z antanas ; _cod_original_cell_volume 4795.40(11) _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 7249664 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.453 _shelx_estimated_absorpt_t_max 0.591 _shelx_res_file ; TITL aaa in P2(1)/n aaa.res created by SHELXL-2018/3 at 23:04:38 on 11-Nov-2024 CELL 0.71073 15.4259 21.5068 15.6995 90.000 112.973 90.000 ZERR 2.00 0.0002 0.0003 0.0002 0.000 0.001 0.000 LATT 1 SYMM 0.5-X, 0.5+Y, 0.5-Z SFAC C H O S Cl Pb N UNIT 166 202 56 16 12 4 2 LIST 4 L.S. 9 BIND Pb1 O1 BIND Pb1 O2 BOND FMAP 2 PLAN 20 TEMP -100.000 SIZE 0.150 0.210 0.240 ACTA OMIT -1 52 WGHT 0.028500 2.799100 FVAR 0.06680 PB1 6 0.847439 0.612994 0.702851 11.00000 0.02289 0.02304 = 0.02123 -0.00038 0.00309 0.00261 CL1 5 0.885821 0.767758 0.867190 11.00000 0.03468 0.02587 = 0.02304 -0.00007 0.00205 -0.00105 CL2 5 0.785679 0.575442 0.390294 11.00000 0.04901 0.05498 = 0.04538 0.00823 0.02367 0.02222 S1 4 0.805568 0.480975 0.692289 11.00000 0.02532 0.02472 = 0.02324 -0.00020 0.00337 0.00188 S2 4 1.007141 0.541081 0.688681 11.00000 0.02945 0.02794 = 0.02493 -0.00079 0.01131 0.00193 S3 4 0.980075 0.568878 0.880630 11.00000 0.02033 0.02769 = 0.02004 0.00027 0.00252 -0.00187 S4 4 0.742223 0.576292 0.828059 11.00000 0.02322 0.03205 = 0.02170 -0.00244 0.00515 -0.00356 O1 3 0.653821 0.603955 0.581543 11.00000 0.02727 0.02299 = 0.02809 0.00091 0.00453 0.00730 O2 3 0.767368 0.710502 0.578011 11.00000 0.03148 0.03154 = 0.02692 0.00160 0.00425 0.00776 O3 3 0.965054 0.695164 0.641467 11.00000 0.03575 0.02272 = 0.04447 0.00076 0.01481 0.00401 O4 3 1.117079 0.658766 1.087246 11.00000 0.02484 0.03965 = 0.01892 -0.00074 0.00392 0.00062 O5 3 0.983923 0.662770 1.174614 11.00000 0.02680 0.03238 = 0.02619 0.00021 0.00899 -0.00235 O6 3 0.783651 0.640325 1.068328 11.00000 0.02710 0.05099 = 0.02265 -0.00359 0.00974 -0.01165 O7 3 0.926413 0.742843 0.958950 11.00000 0.06308 0.04056 = 0.02926 0.01148 -0.00090 -0.00119 O8 3 0.841274 0.718767 0.802339 11.00000 0.06128 0.03384 = 0.03747 -0.01709 0.01420 -0.01275 O9 3 0.957467 0.795739 0.843337 11.00000 0.05732 0.07479 = 0.05263 -0.00360 0.02239 -0.03072 O10 3 0.817425 0.813282 0.862542 11.00000 0.05726 0.05056 = 0.04203 -0.00645 0.00253 0.02491 O11 3 0.865573 0.595444 0.376055 11.00000 0.05124 0.26673 = 0.07764 0.06464 0.04221 0.03644 O12 3 0.704916 0.608271 0.329732 11.00000 0.04906 0.05614 = 0.04497 0.01022 0.01576 0.01857 O13 3 0.769197 0.510040 0.377299 11.00000 0.14887 0.05191 = 0.09380 -0.02734 -0.00167 0.03995 O14 3 0.802208 0.588992 0.485675 11.00000 0.07236 0.05288 = 0.03357 0.00606 0.02121 0.02135 C1 1 0.594236 0.563653 0.602593 11.00000 0.02264 0.03273 = 0.02124 -0.00456 0.00052 0.00109 C2 1 0.517505 0.583740 0.619753 11.00000 0.02636 0.04489 = 0.03141 -0.00842 0.00209 0.00552 AFIX 43 H2A 2 0.502814 0.626768 0.617374 11.00000 -1.20000 AFIX 0 C3 1 0.462159 0.540267 0.640511 11.00000 0.02515 0.06508 = 0.02535 -0.01097 0.00252 0.00105 AFIX 43 H3A 2 0.408927 0.553684 0.651796 11.00000 -1.20000 AFIX 0 C4 1 0.483817 0.477310 0.644955 11.00000 0.03236 0.06429 = 0.02359 0.00294 0.00211 -0.00518 AFIX 43 H4A 2 0.446240 0.447656 0.659799 11.00000 -1.20000 AFIX 0 C5 1 0.560844 0.458618 0.627435 11.00000 0.03107 0.04152 = 0.02130 -0.00023 -0.00300 -0.00243 AFIX 43 H5A 2 0.575943 0.415632 0.630518 11.00000 -1.20000 AFIX 0 C6 1 0.616759 0.500838 0.605472 11.00000 0.02514 0.03300 = 0.01491 -0.00392 -0.00217 0.00272 C7 1 0.699407 0.478270 0.585446 11.00000 0.02602 0.02340 = 0.02361 -0.00287 0.00140 0.00165 AFIX 23 H7B 2 0.707722 0.504970 0.537822 11.00000 -1.20000 H7C 2 0.687956 0.435148 0.561570 11.00000 -1.20000 AFIX 0 C8 1 0.892342 0.441077 0.660770 11.00000 0.02930 0.02387 = 0.03514 -0.00166 0.00744 0.00281 AFIX 23 H8B 2 0.941273 0.423895 0.717785 11.00000 -1.20000 H8C 2 0.861114 0.405506 0.620441 11.00000 -1.20000 AFIX 0 C9 1 0.940814 0.480064 0.611416 11.00000 0.03872 0.02535 = 0.02533 -0.00343 0.01081 0.00868 AFIX 23 H9B 2 0.893290 0.498437 0.554530 11.00000 -1.20000 H9C 2 0.983557 0.453631 0.593601 11.00000 -1.20000 AFIX 0 C10 1 1.050676 0.587831 0.616979 11.00000 0.03617 0.03547 = 0.02676 0.00014 0.01559 0.00258 AFIX 23 H10B 2 1.090896 0.562287 0.594612 11.00000 -1.20000 H10C 2 0.997370 0.604252 0.562699 11.00000 -1.20000 AFIX 0 C11 1 1.106503 0.640220 0.675605 11.00000 0.03674 0.02739 = 0.02469 0.00291 0.01625 -0.00274 C12 1 1.203484 0.636288 0.722232 11.00000 0.03429 0.04017 = 0.04695 0.00917 0.02045 -0.00107 AFIX 43 H12B 2 1.234949 0.599147 0.718090 11.00000 -1.20000 AFIX 0 C13 1 1.255190 0.685214 0.774504 11.00000 0.03234 0.05231 = 0.04555 0.00837 0.01029 -0.00814 AFIX 43 H13B 2 1.321529 0.681517 0.805813 11.00000 -1.20000 AFIX 0 C14 1 1.210719 0.739341 0.781300 11.00000 0.04672 0.03657 = 0.03388 0.00176 0.01593 -0.01188 AFIX 43 H14B 2 1.246636 0.773225 0.816319 11.00000 -1.20000 AFIX 0 C15 1 1.113800 0.744618 0.737288 11.00000 0.05016 0.03374 = 0.03002 0.00274 0.01920 -0.00237 AFIX 43 H15A 2 1.082805 0.781658 0.742747 11.00000 -1.20000 AFIX 0 C16 1 1.062652 0.695093 0.685158 11.00000 0.03319 0.03384 = 0.02616 0.00471 0.01355 -0.00079 C17 1 0.919678 0.754466 0.612996 11.00000 0.03553 0.02890 = 0.03713 0.00128 0.01233 0.00783 AFIX 23 H17A 2 0.957509 0.781269 0.589334 11.00000 -1.20000 H17B 2 0.912914 0.775716 0.666004 11.00000 -1.20000 AFIX 0 C18 1 0.825452 0.742528 0.538862 11.00000 0.04575 0.02926 = 0.02959 0.00640 0.01363 0.00773 AFIX 23 H18A 2 0.795545 0.782394 0.511203 11.00000 -1.20000 H18B 2 0.832218 0.716831 0.489497 11.00000 -1.20000 AFIX 0 C19 1 0.675584 0.698200 0.510395 11.00000 0.03750 0.03087 = 0.02924 0.00252 -0.00120 0.00465 AFIX 23 H19A 2 0.680178 0.671740 0.460724 11.00000 -1.20000 H19B 2 0.644711 0.737730 0.482307 11.00000 -1.20000 AFIX 0 C20 1 0.618440 0.665981 0.554743 11.00000 0.03477 0.02599 = 0.03961 0.00149 0.00699 0.01574 AFIX 23 H20A 2 0.621412 0.689600 0.609941 11.00000 -1.20000 H20B 2 0.551820 0.664056 0.510829 11.00000 -1.20000 AFIX 0 C21 1 1.185279 0.627254 1.070094 11.00000 0.01795 0.02983 = 0.02353 0.00314 0.00592 -0.00496 C22 1 1.272595 0.611106 1.137300 11.00000 0.02309 0.03666 = 0.02623 0.00830 0.00634 -0.00688 AFIX 43 H22A 2 1.289249 0.623968 1.199582 11.00000 -1.20000 AFIX 0 C23 1 1.335074 0.576325 1.113321 11.00000 0.01619 0.04768 = 0.03195 0.01362 0.00407 -0.00040 AFIX 43 H23A 2 1.394081 0.564708 1.159590 11.00000 -1.20000 AFIX 0 C24 1 1.312441 0.558345 1.022743 11.00000 0.02593 0.04323 = 0.03723 0.00409 0.01633 0.00127 AFIX 43 H24A 2 1.355142 0.533930 1.006703 11.00000 -1.20000 AFIX 0 C25 1 1.226154 0.576409 0.954950 11.00000 0.03034 0.04134 = 0.02234 0.00191 0.01171 -0.01011 AFIX 43 H25A 2 1.211053 0.565014 0.892314 11.00000 -1.20000 AFIX 0 C26 1 1.163013 0.610304 0.977461 11.00000 0.01863 0.02829 = 0.02417 0.00200 0.00782 -0.01109 C27 1 1.069508 0.630046 0.904359 11.00000 0.02875 0.02517 = 0.02095 0.00260 0.00666 -0.00764 AFIX 23 H27A 2 1.077963 0.640224 0.846581 11.00000 -1.20000 H27B 2 1.047400 0.668042 0.925330 11.00000 -1.20000 AFIX 0 C28 1 0.926802 0.583124 0.963558 11.00000 0.02807 0.02677 = 0.01933 -0.00132 0.00863 -0.00184 AFIX 23 H28A 2 0.969443 0.569212 1.026012 11.00000 -1.20000 H28B 2 0.914152 0.628054 0.966265 11.00000 -1.20000 AFIX 0 C29 1 0.835305 0.546517 0.931009 11.00000 0.02696 0.02520 = 0.02396 0.00582 0.00921 -0.00093 AFIX 23 H29A 2 0.812318 0.545623 0.981713 11.00000 -1.20000 H29B 2 0.848735 0.503098 0.919098 11.00000 -1.20000 AFIX 0 C30 1 0.703295 0.643175 0.875974 11.00000 0.02821 0.03574 = 0.02351 0.00156 0.00986 0.00061 AFIX 23 H30A 2 0.758719 0.667919 0.914939 11.00000 -1.20000 H30B 2 0.662400 0.670055 0.824908 11.00000 -1.20000 AFIX 0 C31 1 0.649772 0.622193 0.933327 11.00000 0.02723 0.03349 = 0.03330 -0.00400 0.01438 -0.00185 C32 1 0.555712 0.604839 0.890896 11.00000 0.03280 0.06539 = 0.03417 -0.00416 0.00994 -0.00337 AFIX 43 H32A 2 0.525659 0.606410 0.825354 11.00000 -1.20000 AFIX 0 C33 1 0.505252 0.585564 0.940928 11.00000 0.02643 0.09184 = 0.04692 -0.00786 0.00919 -0.01439 AFIX 43 H33A 2 0.441142 0.573688 0.910566 11.00000 -1.20000 AFIX 0 C34 1 0.548783 0.583636 1.035945 11.00000 0.03488 0.07201 = 0.04660 -0.00747 0.02684 -0.01421 AFIX 43 H34A 2 0.513717 0.570844 1.070956 11.00000 -1.20000 AFIX 0 C35 1 0.642194 0.599860 1.081496 11.00000 0.03313 0.05485 = 0.03497 -0.00194 0.01588 -0.00790 AFIX 43 H35A 2 0.671727 0.597102 1.146984 11.00000 -1.20000 AFIX 0 C36 1 0.692469 0.620325 1.030009 11.00000 0.02429 0.03736 = 0.03177 -0.00645 0.01155 -0.00548 C37 1 0.827556 0.645136 1.167373 11.00000 0.03179 0.06608 = 0.02318 -0.00481 0.01180 0.00028 AFIX 23 H37A 2 0.850806 0.603921 1.194895 11.00000 -1.20000 H37B 2 0.781673 0.660403 1.192395 11.00000 -1.20000 AFIX 0 C38 1 0.907313 0.689499 1.190050 11.00000 0.02511 0.06254 = 0.03318 -0.02300 0.00625 -0.00144 AFIX 23 H38A 2 0.885756 0.727251 1.151424 11.00000 -1.20000 H38B 2 0.928476 0.702110 1.255712 11.00000 -1.20000 AFIX 0 C39 1 1.053174 0.708536 1.184370 11.00000 0.03221 0.02515 = 0.02376 -0.00400 0.00822 -0.00495 AFIX 23 H39A 2 1.069951 0.730153 1.244368 11.00000 -1.20000 H39B 2 1.027623 0.739744 1.134391 11.00000 -1.20000 AFIX 0 C40 1 1.139343 0.679137 1.179930 11.00000 0.02413 0.02992 = 0.02005 0.00224 0.00227 -0.00387 AFIX 23 H40A 2 1.191520 0.709634 1.198155 11.00000 -1.20000 H40B 2 1.159374 0.643355 1.222901 11.00000 -1.20000 AFIX 0 ISOR 0.005 C1S PART 1 CL1S 5 0.735434 0.350955 0.451219 10.50000 0.07099 0.06166 = 0.04167 -0.00354 0.03016 0.01140 CL2S 5 0.923121 0.293314 0.540350 10.50000 0.13238 0.10446 = 0.05135 0.01397 0.03098 0.02164 C1S 1 0.810142 0.285243 0.478190 10.50000 0.03769 0.02200 = 0.01838 0.00058 0.01308 -0.01435 AFIX 23 H1SA 2 0.785258 0.255188 0.510772 10.50000 -1.20000 H1SB 2 0.803685 0.265671 0.418939 10.50000 -1.20000 AFIX 0 SIMU 0.005 N1S C2S C3S DELU 0.005 N1S C2S C3S ISOR 0.001 N1S C2S C3S PART 2 N1S 7 0.994719 0.299754 0.558822 10.50000 0.03448 0.04113 = 0.03544 -0.00017 0.01580 -0.00196 C2S 1 0.920129 0.297972 0.549621 10.50000 0.01913 0.01781 = 0.01814 -0.00156 0.00645 0.00049 C3S 1 0.798220 0.286328 0.526186 10.50000 0.02541 0.01946 = 0.02550 -0.00245 0.00840 -0.00405 AFIX 137 H3SA 2 0.769800 0.325929 0.532389 10.50000 -1.50000 H3SB 2 0.791939 0.256190 0.570249 10.50000 -1.50000 H3SC 2 0.766078 0.270480 0.463068 10.50000 -1.50000 PART 0 REM REM F:/On going works/x. PbSandwich/PbClO4_X-ray/aaa.hkl REM AFIX 0 HKLF 4 REM aaa in P2(1)/n REM wR2 = 0.0807, GooF = S = 1.031, Restrained GooF = 1.032 for all data REM R1 = 0.0369 for 7346 Fo > 4sig(Fo) and 0.0553 for all 9419 data REM 605 parameters refined using 39 restraints END WGHT 0.0285 2.7991 REM Highest difference peak 0.944, deepest hole -1.139, 1-sigma level 0.115 Q1 1 1.0020 0.2595 0.5635 11.00000 0.05 0.94 Q2 1 0.9030 0.2571 0.4953 11.00000 0.05 0.94 Q3 1 0.7779 0.5501 0.3383 11.00000 0.05 0.75 Q4 1 0.7800 0.3165 0.4965 11.00000 0.05 0.66 Q5 1 0.8779 0.6462 0.7473 11.00000 0.05 0.64 Q6 1 0.8338 0.5872 0.6565 11.00000 0.05 0.61 Q7 1 0.8261 0.6398 0.6437 11.00000 0.05 0.48 Q8 1 0.8776 0.2803 0.4223 11.00000 0.05 0.47 Q9 1 0.8133 0.3062 0.4406 11.00000 0.05 0.46 Q10 1 0.8377 0.5576 0.3182 11.00000 0.05 0.46 Q11 1 0.7875 0.5198 0.2901 11.00000 0.05 0.45 Q12 1 0.8723 0.5892 0.7587 11.00000 0.05 0.45 Q13 1 0.8324 0.5294 0.3893 11.00000 0.05 0.45 Q14 1 0.8546 0.6140 0.7909 11.00000 0.05 0.44 Q15 1 0.9593 0.5680 0.6756 11.00000 0.05 0.42 Q16 1 0.7336 0.5844 0.3362 11.00000 0.05 0.42 Q17 1 0.5826 0.5240 0.5783 11.00000 0.05 0.42 Q18 1 0.8244 0.5919 0.3832 11.00000 0.05 0.41 Q19 1 0.7575 0.6185 0.6279 11.00000 0.05 0.39 Q20 1 0.9076 0.2074 0.4980 11.00000 0.05 0.38 ; _shelx_res_checksum 2893 _shelx_hkl_file ; -1 0 0 -0.41 0.06 1 0 0 -0.38 0.06 1 0 0 -0.28 0.04 1 0 0 -0.37 0.06 -1 0 0 -0.21 0.08 2 0 0 205.84 9.28 2 0 0 222.85 9.43 2 0 0 204.28 10.00 3 0 0 -0.52 0.17 3 0 0 -0.29 0.28 3 0 0 -0.45 0.26 4 0 0 31.46 2.20 4 0 0 28.38 1.76 4 0 0 29.99 2.05 5 0 0 0.54 0.54 5 0 0 -0.06 0.30 5 0 0 0.27 0.60 6 0 0 286.16 14.76 6 0 0 291.65 13.41 6 0 0 311.65 14.06 7 0 0 -0.04 0.56 7 0 0 -0.42 0.37 7 0 0 0.83 0.78 8 0 0 2.73 0.79 8 0 0 1.87 1.02 8 0 0 1.53 0.91 9 0 0 0.19 0.62 -9 0 0 -0.12 0.84 9 0 0 1.26 1.08 9 0 0 -0.20 0.72 10 0 0 59.09 5.23 10 0 0 58.00 3.55 -10 0 0 47.61 4.83 10 0 0 55.53 4.42 11 0 0 0.13 1.08 11 0 0 0.35 1.23 11 0 0 -0.94 0.67 -11 0 0 0.22 1.18 12 0 0 21.21 2.40 12 0 0 17.17 3.03 -12 0 0 19.15 3.24 12 0 0 17.93 3.22 13 0 0 4.01 1.88 -13 0 0 -0.03 1.42 13 0 0 0.59 1.21 -14 0 0 25.23 4.10 14 0 0 24.47 3.77 14 0 0 21.26 3.94 15 0 0 0.07 1.80 -15 0 0 -2.22 1.84 15 0 0 3.70 2.45 -16 0 0 15.24 3.86 16 0 0 20.65 3.70 16 0 0 21.58 4.58 17 0 0 1.46 2.12 17 0 0 -0.15 2.40 -17 0 0 -1.19 2.36 18 0 0 -0.07 2.17 -18 0 0 -0.75 2.17 18 0 0 -1.22 2.37 0 -1 0 -0.03 0.03 0 1 0 -0.03 0.03 1 -1 0 296.95 12.41 -1 -1 0 295.52 12.43 1 -1 0 252.56 12.38 -1 -1 0 288.72 13.27 1 -1 0 283.80 13.26 1 1 0 269.30 12.41 1 1 0 285.19 13.26 -1 1 0 297.84 12.39 -1 1 0 292.70 13.26 1 1 0 300.03 12.39 2 -1 0 79.33 4.28 2 -1 0 85.02 4.00 2 -1 0 85.53 3.81 2 1 0 85.43 3.82 2 1 0 82.79 3.97 2 1 0 80.13 4.25 3 -1 0 215.18 9.58 3 -1 0 216.42 9.29 3 -1 0 196.38 10.16 3 1 0 213.30 9.28 3 1 0 208.00 9.54 3 1 0 200.79 10.13 4 -1 0 58.57 3.32 4 -1 0 54.83 3.49 4 -1 0 61.41 2.97 4 1 0 56.64 3.28 4 1 0 59.42 2.95 4 1 0 55.99 3.47 5 -1 0 45.69 3.05 5 -1 0 52.43 2.69 5 -1 0 46.29 3.25 5 1 0 45.96 3.21 5 1 0 47.78 3.10 5 1 0 52.63 2.73 6 -1 0 9.61 1.10 6 -1 0 9.79 1.51 6 -1 0 6.59 1.31 6 1 0 8.64 1.12 6 1 0 7.08 1.33 6 1 0 11.80 1.69 7 -1 0 74.89 4.93 7 -1 0 74.44 4.08 7 -1 0 76.74 4.78 7 1 0 79.39 4.24 7 1 0 76.14 4.75 7 1 0 80.83 4.98 8 -1 0 85.76 4.48 8 -1 0 71.66 5.05 8 -1 0 79.72 5.35 8 1 0 88.55 5.48 8 1 0 78.65 5.21 8 1 0 80.84 4.49 -8 1 0 89.39 5.38 9 -1 0 15.21 1.75 -9 -1 0 20.88 2.83 9 -1 0 14.85 2.43 9 -1 0 10.01 2.01 9 1 0 14.80 1.74 9 1 0 12.73 2.17 -9 1 0 13.68 2.34 9 1 0 17.12 2.60 10 -1 0 0.42 1.11 -10 -1 0 -0.72 0.91 10 -1 0 1.44 1.15 10 -1 0 1.51 0.77 10 1 0 -0.40 0.83 -10 1 0 1.07 1.19 10 1 0 0.27 1.04 10 1 0 0.57 0.76 11 -1 0 2.93 1.44 -11 -1 0 1.29 1.33 11 -1 0 0.69 1.27 11 -1 0 1.22 0.87 -11 1 0 3.15 1.47 11 1 0 2.39 1.01 11 1 0 1.78 1.44 11 1 0 0.76 1.32 12 -1 0 20.80 3.21 12 -1 0 21.41 2.43 -12 -1 0 17.35 3.15 12 -1 0 17.86 3.26 -12 1 0 13.37 2.93 12 1 0 25.48 2.56 12 1 0 26.66 3.59 12 1 0 17.61 3.25 -13 -1 0 38.99 5.07 13 -1 0 63.62 5.88 13 -1 0 48.28 5.55 13 1 0 65.20 5.90 -13 1 0 40.88 5.18 13 1 0 39.32 5.09 -14 -1 0 34.06 4.88 14 -1 0 34.53 4.96 14 -1 0 45.04 5.10 14 1 0 38.86 4.71 14 1 0 33.42 4.86 -14 1 0 37.32 5.03 15 -1 0 -1.51 1.26 -15 -1 0 0.47 1.82 15 -1 0 1.02 2.22 15 1 0 0.41 1.91 15 1 0 1.34 1.84 -15 1 0 -0.51 1.73 16 -1 0 -2.21 1.50 16 -1 0 -1.74 1.50 -16 -1 0 -2.05 2.04 -16 1 0 0.25 2.06 16 1 0 5.01 2.31 16 1 0 3.05 2.63 17 -1 0 17.72 4.24 -17 -1 0 19.32 4.34 17 -1 0 16.24 3.71 17 1 0 12.33 4.04 17 1 0 17.51 3.85 -17 1 0 15.12 3.91 -18 -1 0 11.09 3.59 18 -1 0 19.92 4.65 18 -1 0 5.71 2.66 -18 1 0 9.26 3.55 18 1 0 9.03 3.23 18 1 0 8.04 3.42 0 2 0 16.12 1.00 1 -2 0 533.30 22.90 1 -2 0 532.24 23.09 1 -2 0 511.82 24.52 -1 2 0 550.20 22.91 -1 2 0 538.09 23.10 1 2 0 513.35 24.54 1 2 0 532.10 22.88 1 2 0 546.42 23.12 2 -2 0 2.40 0.54 2 -2 0 3.29 0.53 2 -2 0 2.84 0.44 -2 2 0 4.13 0.58 2 2 0 4.05 0.67 2 2 0 3.17 0.49 2 2 0 2.94 0.45 3 -2 0 0.25 0.27 3 -2 0 0.35 0.43 3 -2 0 0.22 0.38 3 2 0 1.18 0.50 3 2 0 0.56 0.32 3 2 0 0.23 0.51 4 -2 0 110.22 5.25 4 -2 0 103.88 5.99 4 -2 0 119.49 5.70 4 2 0 115.88 6.02 4 2 0 107.33 5.23 4 2 0 115.05 5.64 5 -2 0 291.12 13.77 5 -2 0 306.61 13.32 5 -2 0 289.86 14.68 5 2 0 313.34 14.66 5 2 0 290.35 13.75 5 2 0 287.87 13.24 6 -2 0 73.35 4.79 6 -2 0 79.31 4.59 6 -2 0 75.94 3.97 -6 2 0 82.10 4.65 6 2 0 76.70 4.74 6 2 0 77.79 3.97 6 2 0 73.35 4.50 7 -2 0 85.44 5.37 7 -2 0 100.94 4.85 7 -2 0 89.38 5.72 -7 2 0 89.53 5.46 7 2 0 89.96 4.77 7 2 0 89.98 5.62 7 2 0 101.10 5.59 8 -2 0 2.57 1.16 8 -2 0 0.85 0.61 8 -2 0 1.38 0.94 8 2 0 1.05 0.96 8 2 0 0.54 0.86 8 2 0 1.42 0.71 -8 2 0 2.17 1.10 9 -2 0 169.18 8.27 9 -2 0 156.15 9.10 9 -2 0 177.16 9.75 9 2 0 168.72 9.51 -9 2 0 156.74 9.16 9 2 0 161.79 9.20 9 2 0 175.51 8.41 10 -2 0 -0.33 0.99 -10 -2 0 1.05 1.16 10 -2 0 0.60 0.74 10 -2 0 -1.45 0.71 -10 2 0 0.11 1.03 10 2 0 -0.48 0.66 10 2 0 0.34 1.04 10 2 0 -0.31 0.82 11 -2 0 77.28 5.50 11 -2 0 62.19 4.06 11 -2 0 77.79 5.46 -11 -2 0 65.89 6.04 -11 2 0 55.75 5.56 11 2 0 63.78 4.06 11 2 0 55.23 5.44 11 2 0 72.13 5.39 -12 -2 0 2.72 1.80 12 -2 0 2.25 1.72 12 -2 0 0.64 1.32 12 -2 0 2.42 1.15 12 2 0 1.52 0.98 -12 2 0 2.25 1.86 12 2 0 3.22 1.52 12 2 0 1.58 1.54 13 -2 0 -1.25 1.50 -13 -2 0 -0.42 1.43 13 -2 0 -0.42 1.44 13 2 0 -1.57 1.17 -13 2 0 -0.10 1.76 13 2 0 -0.19 1.38 14 -2 0 4.54 1.87 -14 -2 0 1.62 1.83 14 -2 0 4.83 2.21 14 2 0 4.75 2.01 -14 2 0 5.87 2.31 14 2 0 9.44 2.73 15 -2 0 89.51 8.65 15 -2 0 89.27 7.35 -15 -2 0 99.74 9.13 -15 2 0 89.06 8.55 15 2 0 115.67 7.69 15 2 0 95.42 9.01 -16 -2 0 1.40 2.36 16 -2 0 0.88 1.94 16 -2 0 -0.68 2.00 16 2 0 0.74 1.82 -16 2 0 -1.99 1.65 16 2 0 -2.64 1.84 -17 -2 0 5.90 2.96 17 -2 0 1.88 2.43 17 -2 0 7.70 3.19 17 2 0 1.38 2.32 17 2 0 7.20 2.89 -17 2 0 10.60 3.40 18 -2 0 5.12 2.70 18 -2 0 -0.47 2.33 -18 -2 0 2.64 2.81 -18 2 0 1.87 2.68 18 2 0 1.39 1.93 18 2 0 -2.83 1.73 0 3 0 -0.80 0.08 0 3 0 -0.92 0.18 1 -3 0 195.93 8.32 1 -3 0 177.53 9.10 1 3 0 190.04 8.29 1 3 0 187.33 8.60 -1 3 0 192.24 8.32 -1 3 0 193.46 8.59 2 -3 0 43.21 2.77 2 -3 0 47.29 2.52 2 -3 0 48.99 2.48 -2 3 0 46.99 2.48 2 3 0 46.90 2.43 2 3 0 50.10 2.57 -2 3 0 52.54 2.58 2 3 0 46.00 2.82 3 -3 0 46.07 2.45 3 -3 0 45.37 2.54 3 -3 0 40.15 2.77 3 3 0 46.70 2.53 3 3 0 47.74 2.46 -3 3 0 45.78 2.57 3 3 0 39.09 2.78 4 -3 0 210.16 9.66 4 -3 0 201.34 10.66 4 -3 0 213.68 9.94 -4 3 0 221.68 10.00 4 3 0 216.75 9.93 4 3 0 218.28 10.65 4 3 0 204.78 9.63 5 -3 0 31.45 2.55 5 -3 0 32.87 2.35 5 -3 0 30.79 1.98 -5 3 0 31.94 2.36 5 3 0 31.70 1.96 5 3 0 38.19 2.46 5 3 0 31.57 2.45 6 -3 0 10.73 1.62 6 -3 0 15.06 1.42 6 -3 0 12.25 1.81 6 3 0 14.82 1.35 -6 3 0 13.50 1.80 6 3 0 12.97 1.80 6 3 0 15.38 1.88 7 -3 0 39.08 3.59 7 -3 0 36.42 3.37 7 -3 0 33.16 2.32 7 3 0 36.71 2.30 -7 3 0 34.13 3.31 7 3 0 40.91 3.06 7 3 0 36.58 3.31 8 -3 0 124.69 6.89 8 -3 0 122.61 7.21 8 -3 0 116.92 6.03 8 3 0 118.62 7.04 8 3 0 117.82 6.84 -8 3 0 123.10 6.93 8 3 0 107.78 5.90 9 -3 0 30.06 2.31 9 -3 0 27.46 3.29 9 -3 0 31.50 3.51 -9 3 0 30.64 3.50 9 3 0 28.04 3.30 9 3 0 29.47 2.27 9 3 0 28.42 3.26 10 -3 0 0.17 1.20 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-3 0 22.82 5.20 18 -3 0 23.25 4.45 -18 3 0 21.26 4.93 18 3 0 20.19 4.10 18 3 0 18.56 4.90 0 4 0 438.07 18.32 0 4 0 415.09 18.90 1 -4 0 205.04 10.37 -1 4 0 221.77 9.36 1 4 0 208.56 9.76 1 4 0 212.89 9.32 -1 4 0 217.04 9.78 2 -4 0 208.60 11.23 2 -4 0 229.67 10.30 2 -4 0 235.23 10.56 2 4 0 233.38 10.27 -2 4 0 235.96 10.33 2 4 0 243.58 10.61 -2 4 0 230.08 10.55 2 4 0 226.40 11.31 3 -4 0 4.73 0.77 3 -4 0 5.68 1.05 3 -4 0 2.95 0.67 -3 4 0 5.98 0.89 3 4 0 3.19 0.69 3 4 0 4.17 0.96 -3 4 0 4.01 0.76 3 4 0 5.27 0.79 4 -4 0 102.22 6.10 4 -4 0 113.49 5.63 4 -4 0 105.46 5.44 4 4 0 111.97 5.59 4 4 0 107.69 5.43 -4 4 0 117.24 5.52 4 4 0 118.64 6.15 -4 4 0 112.08 5.65 5 -4 0 1.25 0.66 5 -4 0 0.34 0.55 5 -4 0 0.66 0.49 -5 4 0 0.86 0.62 5 4 0 -0.09 0.37 5 4 0 0.26 0.52 5 4 0 0.58 0.64 6 -4 0 237.34 12.68 6 -4 0 237.13 11.79 6 -4 0 249.09 11.39 6 4 0 252.91 12.57 6 4 0 250.20 11.85 -6 4 0 248.81 11.90 6 4 0 240.81 11.25 7 -4 0 2.34 1.01 7 -4 0 0.73 0.75 7 -4 0 -0.09 0.49 7 4 0 1.38 0.84 7 4 0 0.94 0.58 7 4 0 0.47 0.73 -7 4 0 0.35 0.79 8 -4 0 9.47 1.85 8 -4 0 8.73 1.37 8 -4 0 13.20 2.15 8 4 0 11.50 1.94 8 4 0 8.40 1.21 -8 4 0 11.81 2.01 8 4 0 7.25 1.72 9 -4 0 33.64 3.72 9 -4 0 34.10 2.48 9 -4 0 32.46 3.56 9 4 0 35.46 3.53 9 4 0 27.51 3.35 9 4 0 27.76 2.22 -9 4 0 31.30 3.54 10 -4 0 183.98 10.42 10 -4 0 208.02 11.12 10 -4 0 192.93 9.46 -10 -4 0 178.56 10.46 10 4 0 188.50 9.32 10 4 0 189.43 10.74 10 4 0 179.92 10.43 11 -4 0 11.84 2.51 11 -4 0 8.74 1.61 11 -4 0 9.34 2.40 -11 -4 0 10.78 2.48 11 4 0 12.15 2.53 11 4 0 7.68 1.96 11 4 0 8.32 1.59 -11 4 0 9.98 2.37 12 -4 0 32.25 4.28 -12 -4 0 30.44 4.16 12 -4 0 25.03 2.78 12 -4 0 25.32 3.64 12 4 0 25.29 3.60 12 4 0 35.41 4.31 12 4 0 27.23 2.87 -12 4 0 23.08 3.62 13 -4 0 0.26 1.53 13 -4 0 -0.33 1.40 -13 -4 0 -1.83 1.56 13 4 0 -1.12 1.53 -13 4 0 0.37 1.41 13 4 0 -0.06 0.90 13 4 0 -0.55 1.20 14 -4 0 50.37 5.53 14 -4 0 30.88 4.70 -14 -4 0 31.92 4.85 14 4 0 39.13 4.74 14 4 0 42.76 5.52 -14 4 0 34.32 4.85 15 -4 0 7.04 2.41 -15 -4 0 4.20 2.39 15 -4 0 7.25 2.74 15 4 0 9.44 2.78 15 4 0 7.68 2.67 -15 4 0 7.71 3.17 16 -4 0 41.02 5.82 -16 -4 0 43.43 6.10 16 -4 0 45.19 5.71 -16 4 0 35.10 5.51 16 4 0 58.64 6.05 16 4 0 48.79 6.55 17 -4 0 -0.95 2.00 -17 -4 0 3.58 2.66 17 -4 0 -0.29 2.25 17 4 0 2.24 2.30 -17 4 0 0.28 2.34 17 4 0 0.56 1.99 18 -4 0 -0.64 2.13 -18 -4 0 -2.25 2.23 18 -4 0 2.62 2.68 18 4 0 -1.62 2.08 -18 4 0 -0.69 2.29 18 4 0 0.40 1.83 0 5 0 0.00 0.16 0 5 0 -0.13 0.31 -1 5 0 9.95 1.18 1 5 0 9.74 0.65 1 5 0 9.72 1.17 -1 5 0 9.54 0.67 2 -5 0 37.24 2.01 2 -5 0 31.70 2.42 2 5 0 40.88 2.37 -2 5 0 34.09 1.99 -2 5 0 34.56 2.27 2 5 0 38.99 2.64 2 5 0 37.31 1.97 3 -5 0 280.30 12.54 3 -5 0 281.60 12.76 3 -5 0 248.42 13.64 3 5 0 282.47 12.78 3 5 0 281.04 13.73 3 5 0 270.32 12.48 -3 5 0 293.60 12.60 -3 5 0 286.61 12.79 4 -5 0 9.27 1.19 4 -5 0 8.37 1.40 4 -5 0 7.99 1.10 4 5 0 7.93 1.39 -4 5 0 9.17 1.21 -4 5 0 9.87 1.23 4 5 0 6.65 1.05 4 5 0 9.14 1.15 5 -5 0 5.01 1.01 5 -5 0 3.98 0.86 5 -5 0 3.22 1.08 5 5 0 5.60 1.21 5 5 0 3.41 0.84 -5 5 0 3.76 0.85 5 5 0 4.25 0.88 -5 5 0 4.13 0.98 6 -5 0 0.36 0.55 6 -5 0 0.92 0.59 6 -5 0 0.76 0.75 6 5 0 1.07 0.55 -6 5 0 1.16 0.57 6 5 0 -0.05 0.65 -6 5 0 0.49 0.66 6 5 0 2.24 0.92 7 -5 0 155.24 8.12 7 -5 0 171.98 9.44 7 -5 0 166.40 8.69 7 5 0 178.82 9.25 7 5 0 159.36 8.59 7 5 0 160.88 7.98 -7 5 0 171.25 8.76 8 -5 0 16.12 2.31 8 -5 0 18.64 1.98 8 -5 0 17.07 2.64 8 5 0 17.09 2.44 -8 5 0 14.13 2.21 8 5 0 15.92 2.30 8 5 0 13.38 1.61 9 -5 0 43.69 4.23 9 -5 0 40.40 4.22 9 -5 0 39.62 2.94 -9 5 0 50.36 4.55 9 5 0 39.94 2.70 9 5 0 36.39 3.84 9 5 0 42.22 4.18 10 -5 0 0.06 0.79 -10 -5 0 0.75 1.15 10 -5 0 0.86 1.03 10 -5 0 0.75 1.11 10 5 0 0.43 1.00 10 5 0 1.79 1.30 10 5 0 0.63 0.75 -10 5 0 1.20 1.18 11 -5 0 17.21 2.24 11 -5 0 12.12 2.56 -11 -5 0 12.93 2.74 11 -5 0 19.73 3.20 11 5 0 15.35 2.57 11 5 0 14.44 1.88 11 5 0 12.41 2.62 -11 5 0 13.21 2.63 12 -5 0 16.85 2.30 12 -5 0 19.08 3.17 12 -5 0 17.02 3.08 -12 -5 0 7.94 2.32 12 5 0 17.13 3.12 12 5 0 19.86 3.11 12 5 0 12.67 1.96 -12 5 0 13.00 2.81 13 -5 0 25.27 3.83 13 -5 0 25.28 4.08 -13 -5 0 24.21 3.94 -13 5 0 28.55 4.30 13 5 0 26.62 2.90 13 5 0 19.75 3.54 13 5 0 27.61 3.82 14 -5 0 12.67 3.03 -14 -5 0 11.68 3.43 14 -5 0 12.80 3.08 -14 5 0 14.39 3.28 14 5 0 15.53 3.03 14 5 0 11.90 3.26 15 -5 0 8.81 3.05 -15 -5 0 2.80 2.29 15 -5 0 6.53 2.35 15 5 0 2.72 2.02 -15 5 0 7.04 3.01 15 5 0 5.04 2.52 -16 -5 0 3.05 2.62 16 -5 0 2.06 2.25 16 -5 0 3.21 2.25 16 5 0 2.03 2.10 -16 5 0 2.32 2.23 16 5 0 1.88 2.19 17 -5 0 20.32 4.00 17 -5 0 9.98 3.56 -17 -5 0 16.95 4.45 17 5 0 19.85 3.95 -17 5 0 18.74 4.20 17 5 0 8.64 3.53 18 -5 0 9.13 3.19 -18 -5 0 1.93 3.14 18 -5 0 2.40 3.10 18 5 0 3.45 2.63 18 5 0 2.54 2.38 -18 5 0 1.38 2.36 0 6 0 490.93 22.01 0 6 0 541.03 22.91 1 6 0 408.45 17.37 1 6 0 396.88 18.12 -1 6 0 395.14 18.12 -1 6 0 404.43 17.36 2 -6 0 2.36 0.74 2 6 0 3.41 0.53 -2 6 0 1.71 0.66 -2 6 0 3.18 0.54 2 6 0 1.55 0.63 3 -6 0 102.81 4.77 3 -6 0 83.81 5.36 3 -6 0 96.45 5.03 3 6 0 95.76 4.69 3 6 0 90.77 4.98 -3 6 0 97.72 5.06 -3 6 0 96.32 4.76 3 6 0 90.47 5.47 4 -6 0 18.50 2.22 4 -6 0 20.18 1.94 4 -6 0 19.39 1.80 4 6 0 20.91 2.29 -4 6 0 18.58 1.91 4 6 0 18.72 1.90 -4 6 0 20.82 1.90 4 6 0 18.95 1.77 5 -6 0 225.79 10.33 5 -6 0 209.42 11.26 5 -6 0 205.97 10.19 -5 6 0 205.55 10.21 5 6 0 210.50 10.22 5 6 0 228.63 11.26 -5 6 0 217.16 10.31 5 6 0 209.65 10.16 6 -6 0 19.67 2.25 6 -6 0 18.54 2.04 6 -6 0 23.66 2.77 6 6 0 21.16 2.31 -6 6 0 25.23 2.28 -6 6 0 25.00 2.52 6 6 0 19.71 2.49 6 6 0 18.97 1.93 7 -6 0 84.57 4.89 7 -6 0 98.78 5.98 7 -6 0 79.65 5.16 -7 6 0 83.87 4.88 7 6 0 90.81 4.81 7 6 0 86.96 5.58 -7 6 0 88.72 5.29 7 6 0 89.93 5.31 8 -6 0 2.97 1.16 8 -6 0 3.93 1.10 8 -6 0 6.95 1.76 -8 6 0 3.49 1.23 8 6 0 5.39 1.51 -8 6 0 3.46 1.06 8 6 0 3.52 0.93 8 6 0 4.67 1.40 9 -6 0 19.27 2.26 9 -6 0 17.72 2.66 9 -6 0 20.02 2.95 9 6 0 22.33 2.97 9 6 0 19.02 2.74 9 6 0 27.53 2.37 -9 6 0 22.30 2.40 -9 6 0 25.35 3.10 10 -6 0 37.42 4.13 10 -6 0 32.44 4.10 10 -6 0 40.33 3.45 10 6 0 34.02 2.59 10 6 0 33.60 3.83 -10 6 0 35.17 3.99 10 6 0 37.51 4.13 -10 6 0 37.02 3.31 11 -6 0 36.11 3.38 -11 -6 0 33.75 4.20 11 -6 0 35.55 4.31 11 -6 0 32.45 4.07 11 6 0 38.27 2.75 11 6 0 27.42 3.72 11 6 0 35.24 3.98 -11 6 0 29.12 3.83 -11 6 0 33.01 3.19 12 -6 0 13.02 2.80 -12 -6 0 11.81 2.87 12 -6 0 11.32 2.68 12 -6 0 12.39 2.05 -12 6 0 13.91 2.11 12 6 0 11.98 2.76 12 6 0 19.04 3.06 -12 6 0 13.69 2.79 12 6 0 9.58 1.79 13 -6 0 17.84 3.40 13 -6 0 12.15 2.93 -13 -6 0 15.49 3.28 -13 6 0 11.65 2.89 13 6 0 13.39 2.95 13 6 0 16.72 2.32 13 6 0 20.27 3.33 14 -6 0 4.70 2.32 14 -6 0 2.97 2.12 -14 -6 0 1.00 1.88 -14 6 0 5.19 2.40 14 6 0 5.09 2.33 14 6 0 5.99 2.35 15 -6 0 24.98 4.13 -15 -6 0 21.92 4.27 15 -6 0 30.32 4.85 15 6 0 16.97 3.49 -15 6 0 12.95 3.63 15 6 0 24.16 4.30 16 -6 0 17.20 3.93 -16 -6 0 14.40 3.77 16 -6 0 12.76 3.16 -16 6 0 12.07 3.40 16 6 0 14.48 3.79 16 6 0 15.97 3.33 -17 -6 0 6.68 3.01 17 -6 0 2.58 2.49 17 -6 0 1.62 1.93 17 6 0 0.36 2.15 -17 6 0 4.14 2.76 17 6 0 5.44 2.55 18 -6 0 0.78 2.13 18 -6 0 0.89 2.82 -18 -6 0 -0.94 2.84 18 6 0 2.73 2.36 -18 6 0 1.46 2.78 18 6 0 1.27 3.03 0 7 0 0.04 0.19 0 7 0 -0.26 0.40 -1 7 0 0.11 0.44 -1 7 0 0.07 0.19 1 7 0 -0.04 0.43 1 7 0 0.70 0.25 2 7 0 234.73 10.31 -2 7 0 229.74 10.33 -2 7 0 225.23 10.99 2 7 0 234.44 11.01 3 -7 0 38.79 3.05 -3 7 0 42.34 2.81 -3 7 0 44.26 2.47 3 7 0 46.22 3.22 3 7 0 35.51 2.71 3 7 0 39.45 2.36 4 -7 0 39.20 3.04 4 -7 0 33.85 2.36 4 -7 0 40.17 2.67 4 7 0 35.89 2.38 4 7 0 32.91 2.54 -4 7 0 37.21 2.62 4 7 0 40.10 3.05 -4 7 0 37.53 2.46 5 -7 0 12.11 1.63 5 -7 0 12.08 1.61 5 -7 0 10.57 1.89 -5 7 0 10.59 1.52 5 7 0 14.50 1.73 -5 7 0 12.82 1.67 5 7 0 11.30 1.54 5 7 0 14.68 2.08 6 -7 0 140.01 7.50 6 -7 0 139.32 8.38 6 -7 0 153.99 7.55 6 7 0 140.92 8.18 -6 7 0 149.83 7.54 -6 7 0 138.92 7.53 6 7 0 153.33 7.60 6 7 0 144.58 7.40 7 -7 0 22.06 2.61 7 -7 0 23.53 2.98 7 -7 0 22.44 2.34 7 7 0 21.89 2.69 -7 7 0 22.11 2.36 -7 7 0 16.57 2.30 7 7 0 21.50 2.18 7 7 0 24.93 2.66 8 -7 0 73.48 5.15 8 -7 0 59.89 4.42 8 -7 0 65.19 4.16 8 7 0 65.29 4.74 8 7 0 70.73 4.60 -8 7 0 64.98 4.56 8 7 0 64.22 3.93 -8 7 0 66.60 4.18 9 -7 0 14.33 2.31 9 -7 0 14.08 2.58 9 -7 0 14.52 2.01 -9 7 0 11.83 1.88 9 7 0 10.16 2.09 9 7 0 12.79 1.66 9 7 0 15.99 2.42 -9 7 0 9.73 2.00 10 -7 0 3.92 1.63 10 -7 0 1.54 1.23 10 -7 0 4.03 1.27 10 7 0 3.07 0.97 10 7 0 1.87 1.43 -10 7 0 2.74 1.16 10 7 0 4.31 1.68 -10 7 0 2.89 1.48 -11 -7 0 -0.17 1.20 11 -7 0 0.17 1.18 11 -7 0 1.12 1.08 11 -7 0 1.77 1.37 11 7 0 2.66 0.99 -11 7 0 -0.88 1.08 -11 7 0 0.82 1.03 11 7 0 0.73 1.17 11 7 0 0.07 1.11 12 -7 0 42.87 4.96 -12 -7 0 32.02 4.34 12 -7 0 35.36 4.51 12 -7 0 38.33 3.70 12 7 0 40.90 4.45 12 7 0 30.97 4.26 12 7 0 36.31 3.25 -12 7 0 32.57 3.40 -12 7 0 25.97 3.90 13 -7 0 -2.07 1.47 13 -7 0 -0.08 1.58 -13 -7 0 -0.90 1.39 13 7 0 -1.15 0.73 13 7 0 -0.63 1.32 13 7 0 -1.05 1.38 -13 7 0 2.43 2.03 14 -7 0 20.63 3.91 -14 -7 0 12.22 3.25 14 -7 0 20.88 3.75 -14 7 0 22.21 3.87 14 7 0 21.95 3.55 14 7 0 18.81 3.74 15 -7 0 -1.84 1.30 15 -7 0 2.55 1.99 -15 -7 0 -0.74 2.08 15 7 0 -1.00 1.56 -15 7 0 1.01 1.68 15 7 0 -0.76 1.81 16 -7 0 6.17 3.06 16 -7 0 12.09 3.38 -16 -7 0 11.70 3.47 16 7 0 9.25 2.91 -16 7 0 1.69 2.50 16 7 0 10.53 3.29 17 -7 0 3.11 2.45 -17 -7 0 1.20 2.79 17 -7 0 0.45 1.90 17 7 0 0.69 2.50 -17 7 0 0.87 2.09 17 7 0 2.30 2.12 18 -7 0 10.33 3.91 -18 -7 0 10.51 4.13 18 -7 0 9.60 3.45 18 7 0 16.32 3.83 -18 7 0 13.45 3.94 18 7 0 9.06 3.91 0 8 0 77.52 3.51 0 8 0 76.93 4.47 1 8 0 267.91 12.83 1 8 0 277.71 11.82 -1 8 0 271.16 11.78 -1 8 0 263.48 12.84 2 8 0 159.96 7.36 -2 8 0 161.06 7.37 2 8 0 170.19 8.23 -2 8 0 158.92 8.17 3 -8 0 0.31 0.71 3 8 0 0.90 0.44 3 8 0 0.26 0.84 3 8 0 0.25 0.64 -3 8 0 0.10 0.38 -3 8 0 0.68 0.54 4 -8 0 327.57 17.43 4 -8 0 346.73 15.82 4 8 0 351.56 16.30 4 8 0 362.58 17.55 -4 8 0 360.61 16.34 -4 8 0 346.64 15.84 4 8 0 350.46 15.80 5 -8 0 46.76 3.19 5 -8 0 47.56 3.36 5 -8 0 57.73 4.15 5 8 0 55.88 3.31 -5 8 0 49.59 3.42 5 8 0 53.23 3.46 -5 8 0 52.64 3.33 5 8 0 53.28 3.99 6 -8 0 96.58 6.22 6 -8 0 85.65 5.27 6 -8 0 90.98 5.30 6 8 0 104.24 6.21 6 8 0 91.35 5.29 -6 8 0 95.41 5.41 6 8 0 93.25 5.29 -6 8 0 96.27 5.41 7 -8 0 27.35 2.85 7 -8 0 35.94 3.28 7 -8 0 29.49 3.57 -7 8 0 27.72 3.02 7 8 0 31.48 2.85 -7 8 0 28.19 2.84 7 8 0 36.41 3.32 7 8 0 33.57 3.47 8 -8 0 1.52 1.11 8 -8 0 1.33 0.90 8 -8 0 2.93 1.24 -8 8 0 1.71 1.04 8 8 0 0.84 1.14 8 8 0 1.39 1.16 -8 8 0 2.13 0.95 8 8 0 0.82 0.84 9 -8 0 30.18 3.47 9 -8 0 26.31 3.70 9 -8 0 35.88 3.32 -9 8 0 28.45 3.41 9 8 0 26.94 2.70 9 8 0 27.17 3.33 -9 8 0 31.62 3.08 9 8 0 33.90 3.73 10 -8 0 38.50 4.26 10 -8 0 39.68 3.75 10 -8 0 41.68 4.73 10 8 0 41.19 2.98 10 8 0 41.68 4.37 -10 8 0 36.69 4.18 -10 8 0 43.22 3.84 10 8 0 41.87 4.38 11 -8 0 25.37 3.61 11 -8 0 24.39 2.96 -11 -8 0 24.41 3.55 11 -8 0 22.99 3.62 -11 8 0 23.90 3.53 11 8 0 24.39 2.56 11 8 0 31.80 3.92 11 8 0 21.33 3.29 -11 8 0 30.02 3.23 12 -8 0 0.07 1.31 12 -8 0 0.61 1.57 12 -8 0 0.38 1.12 -12 -8 0 1.61 1.84 12 8 0 -0.54 1.36 12 8 0 1.56 0.97 -12 8 0 -0.95 1.14 -12 8 0 -0.87 0.99 12 8 0 2.28 1.74 13 -8 0 0.79 1.82 -13 -8 0 4.38 2.09 13 -8 0 1.42 1.76 13 8 0 1.46 1.69 -13 8 0 0.82 1.69 13 8 0 1.24 1.55 13 8 0 -1.15 0.69 14 -8 0 26.60 4.26 14 -8 0 19.58 3.92 -14 -8 0 25.91 4.44 14 8 0 26.85 4.40 -14 8 0 21.60 3.99 14 8 0 28.82 4.07 15 -8 0 17.21 3.88 -15 -8 0 12.63 3.60 15 -8 0 15.59 3.59 -15 8 0 8.84 3.12 15 8 0 11.42 2.87 15 8 0 22.53 4.26 16 -8 0 11.39 3.34 16 -8 0 12.19 3.54 -16 -8 0 19.90 4.30 16 8 0 15.59 3.41 16 8 0 14.32 3.81 -16 8 0 12.77 3.35 17 -8 0 1.11 2.40 -17 -8 0 1.23 2.83 17 -8 0 2.41 2.07 -17 8 0 1.76 2.69 17 8 0 -1.63 2.36 17 8 0 1.83 2.09 18 -8 0 -0.93 2.67 18 -8 0 -0.75 2.48 -18 -8 0 0.94 2.61 18 8 0 -1.26 1.89 18 8 0 -2.31 1.88 -18 8 0 1.69 2.31 0 9 0 0.01 0.19 0 9 0 1.06 0.76 1 9 0 23.08 2.38 -1 9 0 16.54 2.11 -1 9 0 21.50 1.15 1 9 0 22.09 1.21 -2 9 0 0.22 0.31 2 9 0 0.21 0.32 2 9 0 -0.24 0.65 -2 9 0 0.36 0.59 3 -9 0 361.04 18.21 -3 9 0 365.71 16.17 3 9 0 360.91 16.15 3 9 0 358.66 16.97 -3 9 0 352.17 16.98 3 9 0 380.73 18.30 4 -9 0 6.39 1.51 4 9 0 10.80 1.97 4 9 0 8.91 1.55 4 9 0 11.61 1.37 -4 9 0 11.44 1.37 -4 9 0 10.04 1.61 5 -9 0 0.06 0.73 5 -9 0 0.43 0.65 5 9 0 0.02 0.75 5 9 0 0.38 0.54 -5 9 0 1.38 0.79 5 9 0 1.35 1.12 -5 9 0 0.72 0.67 6 -9 0 21.60 2.50 6 -9 0 17.81 2.20 6 -9 0 21.57 2.99 6 9 0 21.87 2.31 -6 9 0 17.81 2.17 -6 9 0 21.23 2.48 6 9 0 22.15 2.85 6 9 0 20.08 2.31 7 -9 0 37.38 4.04 7 -9 0 34.35 3.20 7 -9 0 28.47 2.99 -7 9 0 33.05 3.21 7 9 0 28.03 3.00 7 9 0 34.45 3.10 -7 9 0 29.66 3.07 7 9 0 35.50 3.81 8 -9 0 0.93 1.28 8 -9 0 1.31 1.05 8 -9 0 0.44 0.87 -8 9 0 1.24 1.04 8 9 0 1.78 0.93 8 9 0 0.24 0.83 -8 9 0 0.97 0.94 8 9 0 -0.08 1.07 9 -9 0 178.51 10.46 9 -9 0 172.84 9.11 9 -9 0 167.35 9.39 9 9 0 162.90 8.72 -9 9 0 174.82 9.11 9 9 0 182.81 10.15 -9 9 0 157.76 9.33 9 9 0 167.71 9.40 10 -9 0 -1.06 0.83 10 -9 0 1.39 1.30 -10 -9 0 1.23 1.25 10 -9 0 0.09 1.28 10 9 0 1.01 1.25 10 9 0 2.61 1.44 10 9 0 0.12 0.88 -10 9 0 -0.23 0.82 -10 9 0 3.42 1.61 11 -9 0 10.59 2.38 11 -9 0 9.24 2.63 -11 -9 0 17.32 3.07 11 -9 0 14.14 2.29 11 9 0 6.97 2.22 -11 9 0 5.77 2.06 11 9 0 13.41 2.73 -11 9 0 9.46 1.95 11 9 0 9.80 1.74 12 -9 0 24.91 3.92 12 -9 0 25.02 3.15 12 -9 0 19.63 3.44 -12 -9 0 31.31 4.12 -12 9 0 27.31 3.19 12 9 0 25.20 3.74 12 9 0 18.40 2.42 12 9 0 26.00 3.64 -12 9 0 27.62 3.84 13 -9 0 60.39 6.37 13 -9 0 61.19 6.49 -13 -9 0 54.22 6.08 13 9 0 65.05 6.44 13 9 0 61.39 4.18 13 9 0 58.70 5.89 -13 9 0 65.58 6.42 14 -9 0 -0.04 1.93 -14 -9 0 -0.67 2.20 14 -9 0 1.01 1.96 14 9 0 0.64 1.67 14 9 0 0.67 1.93 -14 9 0 0.69 1.81 15 -9 0 1.46 2.32 15 -9 0 2.12 2.01 -15 -9 0 6.61 2.68 -15 9 0 4.43 2.35 15 9 0 1.85 1.66 15 9 0 0.96 1.78 -16 -9 0 4.80 3.09 16 -9 0 7.35 2.94 16 -9 0 5.98 3.13 16 9 0 3.50 2.68 16 9 0 8.70 2.89 -16 9 0 4.45 2.42 -17 -9 0 21.18 4.94 17 -9 0 16.86 3.83 17 -9 0 13.45 4.01 -17 9 0 14.40 3.90 17 9 0 22.58 4.16 17 9 0 26.83 5.18 0 10 0 158.34 8.77 0 10 0 177.34 7.50 -1 10 0 9.44 1.65 1 10 0 8.44 1.54 1 10 0 8.88 0.69 -1 10 0 9.46 0.65 -2 10 0 45.81 2.41 2 10 0 47.97 2.47 2 10 0 42.03 3.25 -2 10 0 52.69 3.52 3 10 0 -0.40 0.57 -3 10 0 -0.14 0.72 3 10 0 0.80 0.45 -3 10 0 -0.13 0.37 4 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100.69 6.46 -11 -10 0 100.52 7.09 11 -10 0 107.82 7.02 11 10 0 102.57 5.97 -11 10 0 87.85 6.66 11 10 0 101.87 6.97 11 10 0 115.00 7.47 -11 10 0 111.43 6.59 -12 -10 0 3.86 2.15 12 -10 0 12.20 2.93 12 -10 0 3.10 1.65 12 -10 0 3.02 1.70 12 10 0 4.49 1.41 -12 10 0 4.42 1.68 -12 10 0 4.64 2.00 12 10 0 5.33 2.03 12 10 0 5.21 2.06 13 -10 0 5.92 2.57 -13 -10 0 6.22 2.31 13 -10 0 3.26 1.83 13 10 0 5.44 1.49 13 10 0 4.97 1.96 13 10 0 1.01 1.77 -13 10 0 4.55 2.02 -14 -10 0 6.69 2.96 14 -10 0 11.61 3.15 14 -10 0 16.77 3.56 14 10 0 10.42 2.81 14 10 0 10.81 3.00 -14 10 0 9.04 2.85 15 -10 0 26.19 4.45 15 -10 0 19.78 3.99 -15 -10 0 16.45 3.89 15 10 0 19.93 3.55 -15 10 0 25.37 4.38 15 10 0 19.02 4.07 16 -10 0 8.47 2.94 -16 -10 0 16.23 4.07 16 10 0 9.27 3.19 -16 10 0 10.71 3.54 16 10 0 13.02 3.23 17 -10 0 14.63 3.93 -17 -10 0 23.05 5.01 17 10 0 14.45 3.65 -17 10 0 10.93 3.75 17 10 0 10.83 3.63 0 11 0 0.44 0.21 0 11 0 0.00 0.65 1 11 0 3.57 0.48 -1 11 0 4.87 1.28 -1 11 0 4.29 0.47 1 11 0 2.91 1.00 -2 11 0 58.81 2.89 2 11 0 58.80 2.96 2 11 0 57.81 3.98 -2 11 0 54.20 4.01 3 11 0 1.64 0.59 -3 11 0 2.21 0.60 -3 11 0 1.12 0.84 3 11 0 1.89 0.97 -4 11 0 37.37 2.36 4 11 0 32.61 3.75 4 11 0 37.62 3.52 -4 11 0 39.83 3.66 4 11 0 31.25 2.30 5 -11 0 12.57 2.34 5 11 0 14.77 2.16 5 11 0 13.36 1.69 5 11 0 15.29 2.63 -5 11 0 17.61 2.42 -5 11 0 18.02 1.94 6 -11 0 147.38 8.86 6 11 0 138.78 7.83 6 11 0 151.25 8.84 6 11 0 145.09 7.47 -6 11 0 132.49 7.39 -6 11 0 141.58 7.96 7 -11 0 3.46 1.53 7 11 0 6.41 1.52 -7 11 0 6.04 1.56 7 11 0 5.58 1.56 7 11 0 10.55 2.42 -7 11 0 9.70 1.76 8 -11 0 72.20 5.80 8 -11 0 67.97 4.80 -8 11 0 74.98 5.03 -8 11 0 73.80 4.93 8 11 0 70.31 4.84 8 11 0 85.28 5.86 8 11 0 72.18 4.78 9 -11 0 1.86 1.23 9 -11 0 -0.12 1.30 9 -11 0 -0.23 0.94 9 11 0 0.96 1.31 9 11 0 0.49 1.06 9 11 0 1.13 1.08 -9 11 0 0.98 1.12 -9 11 0 0.45 1.15 10 -11 0 -0.18 1.20 10 -11 0 2.06 1.40 -10 -11 0 4.91 1.84 10 -11 0 4.06 2.00 10 11 0 2.21 1.20 10 11 0 1.35 1.38 10 11 0 2.04 1.60 -10 11 0 1.92 1.28 -10 11 0 3.49 1.60 11 -11 0 1.03 1.20 -11 -11 0 2.87 1.76 11 -11 0 1.97 1.55 11 -11 0 2.09 1.96 11 11 0 1.82 1.22 -11 11 0 0.46 1.36 -11 11 0 1.16 1.31 11 11 0 1.23 1.66 11 11 0 1.79 1.51 12 -11 0 69.83 6.58 12 -11 0 70.31 5.25 12 -11 0 93.08 6.86 -12 -11 0 78.63 6.97 12 11 0 64.22 6.41 -12 11 0 69.85 6.41 12 11 0 78.22 6.86 12 11 0 67.61 4.71 13 -11 0 7.71 2.67 -13 -11 0 4.56 2.38 13 -11 0 4.84 2.27 13 11 0 3.75 2.16 13 11 0 6.72 2.34 13 11 0 7.00 1.67 -13 11 0 4.59 2.21 14 -11 0 29.50 4.60 -14 -11 0 12.24 3.29 14 -11 0 24.76 4.41 -14 11 0 20.09 3.68 14 11 0 27.06 4.22 14 11 0 25.63 3.92 15 -11 0 1.66 2.23 -15 -11 0 0.26 2.26 15 11 0 1.93 2.10 15 11 0 -1.40 1.85 -15 11 0 -0.54 1.96 16 -11 0 2.65 2.27 -16 -11 0 2.80 2.91 16 11 0 -0.43 1.62 16 11 0 -0.33 2.18 -16 11 0 1.04 2.41 -17 -11 0 3.93 2.82 17 -11 0 3.82 2.79 17 11 0 0.47 1.99 17 11 0 -0.04 2.06 -17 11 0 2.92 2.70 0 12 0 42.16 3.77 0 12 0 37.62 1.77 -1 12 0 67.96 4.33 1 12 0 53.96 4.00 -1 12 0 53.53 2.69 1 12 0 59.89 2.75 -2 12 0 0.07 0.75 2 12 0 -0.25 0.29 2 12 0 -0.11 0.72 -2 12 0 0.44 0.31 -3 12 0 50.81 2.83 -3 12 0 52.83 3.95 3 12 0 51.88 3.88 3 12 0 53.13 2.93 4 12 0 30.42 2.18 -4 12 0 33.19 2.22 4 12 0 35.69 3.91 -4 12 0 22.17 2.93 4 12 0 36.32 3.51 5 -12 0 181.19 10.74 -5 12 0 190.91 9.93 -5 12 0 178.01 8.91 5 12 0 185.16 9.78 5 12 0 191.11 10.77 5 12 0 175.49 8.91 6 -12 0 82.19 6.22 6 12 0 88.79 5.57 6 12 0 84.23 5.05 -6 12 0 90.32 5.13 -6 12 0 87.81 5.67 6 12 0 89.82 6.36 7 -12 0 0.74 1.31 7 12 0 1.02 1.15 -7 12 0 1.85 0.98 7 12 0 -0.17 0.79 -7 12 0 2.45 1.27 7 12 0 1.70 1.52 8 -12 0 3.94 1.81 8 12 0 2.70 1.31 -8 12 0 4.66 1.48 -8 12 0 3.28 1.46 8 12 0 4.77 1.44 8 12 0 4.52 1.75 9 -12 0 38.89 4.78 9 12 0 38.13 4.57 -9 12 0 43.60 4.22 9 12 0 38.65 3.76 9 12 0 37.02 3.96 -9 12 0 34.70 3.78 10 -12 0 35.55 4.70 -10 -12 0 28.02 3.67 10 12 0 29.85 3.72 10 12 0 28.95 3.29 -10 12 0 29.10 3.67 10 12 0 36.74 4.39 -10 12 0 32.97 3.68 -11 -12 0 26.52 3.77 11 -12 0 30.49 4.59 -11 12 0 25.36 3.30 11 12 0 25.91 3.57 -11 12 0 33.60 4.04 11 12 0 27.61 3.17 11 12 0 23.23 3.72 -12 -12 0 14.98 3.09 12 -12 0 10.85 3.20 -12 12 0 10.23 2.60 12 12 0 11.01 2.81 12 12 0 9.76 1.93 12 12 0 7.87 2.45 -13 -12 0 -0.23 1.82 13 -12 0 2.85 2.44 13 12 0 0.90 1.58 13 12 0 2.03 1.38 13 12 0 1.58 1.86 -13 12 0 -0.97 1.53 -14 -12 0 19.24 3.72 14 -12 0 20.57 4.05 14 12 0 20.89 3.67 14 12 0 14.67 3.33 -14 12 0 14.88 3.39 15 -12 0 15.06 3.88 -15 -12 0 8.26 3.08 15 12 0 8.60 2.58 -15 12 0 9.76 3.11 15 12 0 6.08 2.83 16 -12 0 10.13 3.64 -16 -12 0 5.10 3.01 16 12 0 1.79 2.55 -16 12 0 10.48 3.45 16 12 0 11.23 3.15 17 -12 0 12.53 3.92 -17 -12 0 15.11 4.46 17 12 0 15.95 4.31 -17 12 0 15.80 3.99 17 12 0 7.62 2.66 0 13 0 2.69 1.13 1 13 0 66.17 4.54 -1 13 0 68.62 4.62 1 13 0 60.75 2.96 2 13 0 3.92 1.33 2 13 0 3.24 0.65 -2 13 0 4.15 0.54 -2 13 0 5.18 1.46 3 13 0 72.40 4.97 -3 13 0 69.48 3.68 -3 13 0 75.81 5.11 3 13 0 76.87 3.86 4 13 0 -0.20 0.92 -4 13 0 0.97 0.62 4 13 0 -1.18 0.97 4 13 0 0.50 0.57 -4 13 0 0.45 0.98 -5 13 0 16.30 2.52 -5 13 0 14.16 1.77 5 13 0 13.28 2.75 5 13 0 15.77 1.86 5 13 0 14.43 2.36 6 -13 0 8.80 2.25 -6 13 0 5.64 1.58 6 13 0 5.81 2.18 -6 13 0 5.13 1.31 6 13 0 6.99 1.71 6 13 0 5.53 1.37 7 -13 0 146.47 9.75 7 13 0 159.12 9.80 7 13 0 162.21 8.80 -7 13 0 151.00 8.26 7 13 0 159.75 8.32 -7 13 0 155.65 8.96 8 -13 0 0.81 1.42 -8 13 0 1.30 1.31 8 13 0 3.19 1.32 8 13 0 1.38 1.80 8 13 0 1.35 1.32 -8 13 0 0.91 1.18 9 -13 0 24.54 3.90 -9 -13 0 29.63 3.45 9 13 0 25.22 3.15 9 13 0 22.13 3.54 -9 13 0 22.25 3.24 -9 13 0 25.20 3.26 9 13 0 23.01 3.03 -10 -13 0 8.63 2.28 10 -13 0 10.11 2.85 -10 13 0 12.20 2.40 10 13 0 15.20 2.39 10 13 0 15.08 3.00 -10 13 0 12.13 2.39 10 13 0 16.08 2.71 -11 -13 0 0.56 1.61 11 -13 0 5.86 2.35 11 13 0 4.27 1.94 11 13 0 2.61 1.63 -11 13 0 4.45 1.78 -11 13 0 0.67 1.45 11 13 0 5.32 1.57 -12 -13 0 -0.48 1.66 12 -13 0 2.46 1.96 12 13 0 -1.39 1.25 -12 13 0 0.83 1.51 12 13 0 -1.68 0.91 12 13 0 0.42 1.49 -13 -13 0 61.94 6.38 13 -13 0 58.32 6.80 13 13 0 55.41 4.32 13 13 0 58.83 6.29 -13 13 0 55.32 5.87 13 13 0 56.92 5.99 -14 -13 0 1.13 2.16 14 -13 0 0.75 1.97 14 13 0 0.42 1.80 -14 13 0 2.52 2.12 14 13 0 1.72 1.93 -15 -13 0 1.31 2.38 15 -13 0 2.43 2.46 -15 13 0 3.64 2.48 15 13 0 3.77 2.36 15 13 0 0.97 1.92 -16 -13 0 -1.62 2.37 16 -13 0 4.18 2.87 16 13 0 0.69 2.15 16 13 0 -0.15 2.25 -16 13 0 -0.05 2.21 0 14 0 46.48 4.35 1 14 0 27.28 1.45 -1 14 0 30.72 3.49 1 14 0 31.58 3.47 2 14 0 0.40 0.98 2 14 0 0.42 0.42 -2 14 0 1.00 1.01 -2 14 0 0.65 0.35 3 14 0 3.25 0.72 -3 14 0 2.54 0.58 -3 14 0 2.87 1.33 3 14 0 2.32 1.21 4 14 0 151.99 9.36 4 14 0 148.40 7.22 4 14 0 137.01 8.32 -4 14 0 162.54 8.77 -4 14 0 140.88 7.05 -5 14 0 62.63 5.48 5 14 0 57.28 5.16 -5 14 0 63.79 3.76 5 14 0 76.31 6.64 5 14 0 60.82 3.82 6 14 0 146.93 7.78 -6 14 0 154.90 7.80 6 14 0 144.44 9.45 -6 14 0 158.05 8.91 6 14 0 143.95 8.52 7 -14 0 -1.74 1.33 -7 14 0 0.58 1.03 7 14 0 0.61 1.01 7 14 0 1.75 1.31 7 14 0 0.55 1.55 -7 14 0 -0.50 0.84 8 -14 0 -0.08 1.72 -8 -14 0 -0.81 0.85 8 14 0 -1.06 1.34 -8 14 0 0.62 1.20 8 14 0 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15 0 1.40 1.20 -2 15 0 108.22 6.83 2 15 0 102.52 6.63 3 15 0 12.70 2.44 -3 15 0 14.37 2.63 3 15 0 17.73 1.57 4 15 0 21.32 3.01 -4 15 0 21.41 3.16 4 15 0 17.98 1.85 4 15 0 21.65 3.48 5 15 0 1.44 1.21 -5 15 0 5.61 1.87 5 15 0 5.27 1.17 5 15 0 6.57 2.25 6 15 0 12.01 1.86 6 15 0 10.67 2.22 -6 15 0 11.17 1.70 6 15 0 14.52 3.07 -6 15 0 11.95 2.57 -7 -15 0 23.22 2.73 7 15 0 23.77 3.86 7 15 0 20.74 3.08 -7 15 0 22.53 2.64 7 15 0 22.68 2.68 -7 15 0 25.40 3.56 -8 -15 0 57.78 4.38 8 -15 0 66.68 6.62 -8 15 0 58.54 4.27 8 15 0 58.72 4.33 8 15 0 62.97 5.51 8 15 0 69.50 6.63 -8 15 0 54.04 5.40 9 -15 0 20.43 3.83 -9 -15 0 15.74 2.61 9 15 0 9.79 2.37 -9 15 0 16.70 2.87 9 15 0 16.12 2.53 9 15 0 13.99 3.20 -9 15 0 23.39 2.89 10 -15 0 2.90 1.95 -10 -15 0 4.08 1.68 10 15 0 6.97 2.42 10 15 0 6.30 1.89 10 15 0 7.33 2.03 -10 15 0 7.70 2.23 -10 15 0 10.38 2.23 11 -15 0 1.05 2.20 -11 -15 0 3.13 1.73 -11 15 0 1.94 1.70 -11 15 0 2.54 1.71 11 15 0 4.41 1.75 11 15 0 3.65 1.79 11 15 0 -1.31 1.44 -12 -15 0 27.26 4.07 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-19 9.65 3.05 8 3 -19 9.42 2.80 7 -3 -19 -2.03 1.77 7 3 -19 0.94 2.29 6 -3 -19 -0.29 2.11 6 3 -19 0.89 2.10 5 -3 -19 1.80 2.06 5 3 -19 3.91 2.31 4 -3 -19 1.14 2.23 4 3 -19 3.76 2.38 3 -3 -19 9.55 3.07 3 3 -19 11.22 3.03 2 -3 -19 3.54 2.21 2 3 -19 5.73 2.50 1 -3 -19 2.14 2.40 1 3 -19 -0.57 1.86 0 -3 -19 11.52 3.24 0 3 -19 5.90 2.96 14 -4 -19 2.13 2.10 14 -4 -19 -3.68 2.29 14 4 -19 1.21 2.37 14 4 -19 2.59 2.28 13 -4 -19 2.67 2.34 13 -4 -19 3.14 3.04 13 4 -19 3.28 2.25 13 4 -19 4.51 2.26 12 -4 -19 0.83 1.95 12 -4 -19 -2.05 2.36 12 4 -19 -1.30 1.95 12 4 -19 1.03 2.07 11 -4 -19 8.85 3.02 11 -4 -19 11.25 3.50 11 4 -19 7.90 2.95 10 -4 -19 1.88 2.38 10 -4 -19 -1.64 2.36 10 4 -19 0.23 1.91 10 4 -19 2.98 2.46 9 -4 -19 3.46 2.20 9 -4 -19 0.06 1.90 9 4 -19 -0.54 1.87 9 4 -19 2.64 2.11 8 -4 -19 1.61 2.56 8 -4 -19 8.47 2.76 8 4 -19 1.68 2.32 8 4 -19 1.59 1.99 7 -4 -19 27.75 4.35 7 4 -19 15.07 3.44 6 -4 -19 -2.19 1.81 6 4 -19 3.60 2.57 5 -4 -19 7.85 2.55 5 4 -19 3.35 2.26 4 -4 -19 4.65 2.52 4 4 -19 1.12 2.04 3 -4 -19 3.83 2.39 3 4 -19 2.52 2.65 2 -4 -19 4.96 2.75 2 4 -19 3.73 2.66 1 -4 -19 15.19 3.67 1 4 -19 21.99 4.33 0 -4 -19 0.06 2.23 0 4 -19 1.76 2.28 14 -5 -19 21.08 4.79 14 -5 -19 11.73 3.24 14 5 -19 7.65 2.59 14 5 -19 10.35 3.24 13 -5 -19 -0.79 1.52 13 -5 -19 -0.84 2.13 13 5 -19 0.99 2.10 13 5 -19 1.75 2.18 12 -5 -19 8.62 3.49 12 -5 -19 5.59 2.53 12 5 -19 12.13 3.15 12 5 -19 10.63 2.93 11 -5 -19 1.75 2.40 11 -5 -19 2.89 2.39 11 5 -19 -0.20 2.29 11 5 -19 0.32 1.89 10 -5 -19 4.17 2.91 10 -5 -19 2.92 2.39 10 5 -19 2.21 2.10 10 5 -19 5.85 3.10 9 -5 -19 3.33 2.46 9 -5 -19 6.19 2.94 9 5 -19 10.82 2.84 9 5 -19 10.48 3.42 8 -5 -19 0.83 2.38 8 -5 -19 14.50 3.16 8 5 -19 11.63 2.81 8 5 -19 9.53 2.98 7 -5 -19 1.66 2.10 7 5 -19 -0.77 1.62 6 -5 -19 -0.07 1.99 6 5 -19 0.10 1.87 5 -5 -19 6.41 2.53 5 5 -19 1.41 2.45 4 -5 -19 16.74 3.47 4 5 -19 13.48 3.39 3 -5 -19 5.36 2.58 3 5 -19 3.04 2.36 2 -5 -19 1.57 2.39 2 5 -19 0.96 2.16 1 -5 -19 0.13 1.84 1 5 -19 2.66 2.41 14 -6 -19 3.52 3.27 14 -6 -19 0.45 1.76 14 6 -19 -2.15 2.14 14 6 -19 -0.32 1.62 13 -6 -19 3.91 3.22 13 -6 -19 -0.25 1.92 13 6 -19 -1.07 1.77 13 6 -19 2.61 2.53 12 -6 -19 23.46 5.16 12 -6 -19 20.74 3.67 12 6 -19 20.72 4.27 12 6 -19 14.66 3.32 11 -6 -19 7.70 3.66 11 -6 -19 7.58 2.77 11 6 -19 7.67 2.95 11 6 -19 2.71 2.09 10 -6 -19 10.75 3.74 10 -6 -19 10.92 3.05 10 6 -19 5.98 2.38 10 6 -19 6.53 2.77 9 -6 -19 1.30 2.31 9 -6 -19 0.94 2.17 9 6 -19 1.43 2.40 9 6 -19 3.11 1.97 8 -6 -19 5.30 2.60 8 -6 -19 0.56 2.42 8 6 -19 3.57 1.88 8 6 -19 1.08 2.07 7 -6 -19 -1.03 1.73 7 6 -19 3.91 2.41 6 -6 -19 26.12 4.05 6 6 -19 23.79 4.49 5 -6 -19 5.63 2.42 5 6 -19 1.80 2.53 4 -6 -19 -1.30 2.05 4 6 -19 1.07 2.47 3 -6 -19 0.13 1.97 3 6 -19 -0.58 1.86 2 -6 -19 21.55 4.00 2 6 -19 23.87 4.38 1 -6 -19 6.10 2.56 1 6 -19 3.21 2.31 13 -7 -19 7.73 2.85 13 -7 -19 12.16 4.10 13 7 -19 13.82 3.49 13 7 -19 17.50 3.49 12 -7 -19 1.70 3.32 12 -7 -19 2.04 2.07 12 7 -19 2.04 2.16 12 7 -19 -1.27 1.80 11 -7 -19 0.61 1.87 11 -7 -19 0.44 2.71 11 7 -19 -0.43 1.72 11 7 -19 -0.30 1.95 10 -7 -19 -1.02 1.79 10 -7 -19 -2.88 2.52 10 7 -19 1.93 2.42 10 7 -19 1.33 1.78 9 -7 -19 22.23 5.25 9 -7 -19 21.25 3.97 9 7 -19 20.19 4.39 9 7 -19 25.99 3.82 8 -7 -19 7.01 3.38 8 -7 -19 6.26 2.44 8 7 -19 9.78 3.10 8 7 -19 9.03 2.54 7 -7 -19 4.79 2.55 7 7 -19 8.63 3.07 6 -7 -19 -0.72 1.93 6 7 -19 2.28 2.18 5 -7 -19 10.07 3.01 5 7 -19 12.12 3.31 4 -7 -19 3.98 2.42 4 7 -19 0.45 2.35 3 -7 -19 40.66 5.17 3 7 -19 33.75 5.04 2 -7 -19 -0.94 1.95 2 7 -19 0.98 2.06 1 -7 -19 -0.82 2.01 1 7 -19 0.37 1.97 13 -8 -19 10.43 4.28 13 -8 -19 18.29 3.45 13 8 -19 6.87 2.77 13 8 -19 4.62 2.86 12 -8 -19 1.59 2.26 12 -8 -19 5.42 3.38 12 8 -19 5.17 2.35 12 8 -19 0.12 2.27 11 -8 -19 6.83 2.52 11 -8 -19 2.26 2.99 11 8 -19 8.64 3.10 11 8 -19 5.68 2.27 10 -8 -19 1.33 2.97 10 -8 -19 -3.32 1.54 10 8 -19 1.52 1.90 10 8 -19 1.62 2.35 9 -8 -19 3.52 2.29 9 -8 -19 2.06 3.11 9 8 -19 2.61 2.58 9 8 -19 2.06 1.69 8 -8 -19 7.20 3.53 8 -8 -19 5.19 2.55 8 8 -19 4.42 2.61 -8 8 19 6.98 3.10 7 -8 -19 13.37 3.32 7 8 -19 13.76 3.67 -7 8 19 9.18 3.61 6 -8 -19 8.40 2.82 6 8 -19 6.20 2.71 5 -8 -19 9.78 2.99 5 8 -19 6.46 2.81 4 -8 -19 3.69 2.44 4 8 -19 1.16 2.53 3 -8 -19 5.24 2.59 3 8 -19 1.92 2.26 2 -8 -19 8.31 2.74 2 8 -19 9.80 3.15 12 -9 -19 5.78 2.35 12 -9 -19 0.23 3.42 12 9 -19 1.24 2.09 12 9 -19 0.56 1.93 11 -9 -19 -1.46 2.98 11 -9 -19 0.38 1.82 11 9 -19 0.11 1.92 11 9 -19 3.23 2.95 10 -9 -19 5.48 3.39 10 -9 -19 15.70 3.42 10 9 -19 10.18 3.26 10 9 -19 15.73 3.23 9 -9 -19 -0.62 2.02 9 -9 -19 2.94 3.29 9 9 -19 3.51 2.52 -9 9 19 -1.92 2.42 9 9 -19 3.46 2.06 8 -9 -19 25.93 5.16 8 -9 -19 15.17 3.42 8 9 -19 20.18 4.23 -8 9 19 22.13 4.50 7 -9 -19 1.25 2.08 -7 9 19 1.03 2.51 7 9 -19 0.27 2.41 6 -9 -19 1.45 2.20 6 9 -19 2.91 2.35 5 -9 -19 -3.38 1.57 5 9 -19 -0.44 1.97 4 -9 -19 14.72 3.41 4 9 -19 19.15 4.00 3 -9 -19 -2.71 1.79 3 9 -19 -0.58 1.95 2 -9 -19 23.15 3.95 2 9 -19 11.36 3.38 11 -10 -19 5.17 3.35 11 10 -19 1.42 1.70 -11 10 19 3.20 2.60 11 10 -19 5.30 2.99 10 -10 -19 11.30 4.43 10 10 -19 5.39 2.86 -10 10 19 6.98 4.05 10 10 -19 7.05 2.39 9 -10 -19 -0.52 2.21 9 10 -19 0.71 1.82 -9 10 19 0.88 2.22 9 10 -19 -1.62 1.99 8 -10 -19 2.59 2.74 8 10 -19 1.70 2.19 -8 10 19 -0.11 2.41 -7 10 19 11.40 3.66 7 10 -19 16.36 3.93 6 10 -19 9.87 3.37 5 10 -19 1.67 2.43 4 10 -19 -0.57 1.86 3 10 -19 -0.91 2.27 10 -11 -19 -1.56 3.00 10 11 -19 -0.45 2.09 10 11 -19 0.43 2.03 -10 11 19 -1.54 2.66 9 -11 -19 11.59 4.35 9 11 -19 13.92 3.78 -9 11 19 12.44 4.19 9 11 -19 12.76 2.87 8 -11 -19 -0.43 2.78 8 11 -19 3.68 2.38 -8 11 19 1.26 2.73 7 -11 -19 8.00 4.14 7 11 -19 8.29 3.11 -7 11 19 11.00 3.92 6 11 -19 0.63 2.32 5 11 -19 14.94 3.61 8 12 -19 -1.39 2.16 -8 12 19 2.64 2.66 7 12 -19 4.10 2.51 -7 12 19 -0.02 2.77 13 0 -20 2.36 2.65 13 0 -20 0.72 2.01 12 0 -20 10.78 3.31 12 0 -20 9.58 3.21 11 0 -20 -1.76 1.67 11 0 -20 1.00 2.57 10 0 -20 4.64 3.03 10 0 -20 10.44 3.38 9 0 -20 0.96 2.42 9 0 -20 -3.10 1.52 8 0 -20 3.17 2.30 7 0 -20 2.23 2.50 6 0 -20 37.61 5.19 5 0 -20 1.75 2.25 4 0 -20 15.17 3.75 3 0 -20 1.26 2.19 13 -1 -20 8.60 3.50 13 -1 -20 4.65 2.78 13 1 -20 5.64 2.99 13 1 -20 9.90 3.33 12 -1 -20 0.63 2.57 12 -1 -20 4.08 2.76 12 1 -20 3.74 2.89 12 1 -20 4.82 2.42 11 -1 -20 1.33 2.35 11 -1 -20 -2.44 1.78 11 1 -20 1.11 2.51 11 1 -20 1.51 2.56 10 -1 -20 0.04 2.12 10 -1 -20 -2.23 2.35 10 1 -20 0.92 2.30 10 1 -20 0.76 1.96 9 -1 -20 12.79 3.44 9 -1 -20 5.37 2.94 9 1 -20 9.31 3.17 9 1 -20 19.03 3.95 8 -1 -20 9.29 3.19 8 1 -20 5.15 2.90 7 -1 -20 6.32 2.87 7 1 -20 11.94 3.26 6 -1 -20 -1.27 2.26 6 1 -20 0.33 1.98 5 -1 -20 4.68 2.87 5 1 -20 4.37 2.58 4 -1 -20 23.95 4.47 4 1 -20 21.10 4.21 3 -1 -20 35.25 4.96 3 1 -20 25.27 4.53 13 -2 -20 -2.14 2.10 13 -2 -20 -1.24 2.08 13 2 -20 3.70 2.45 13 2 -20 -0.63 2.15 12 -2 -20 -2.96 1.95 12 -2 -20 -1.62 1.95 12 2 -20 0.45 1.75 12 2 -20 -0.53 2.13 11 -2 -20 26.01 4.81 11 -2 -20 20.00 4.23 11 2 -20 22.06 4.55 11 2 -20 31.11 4.61 10 -2 -20 -0.76 2.51 10 -2 -20 2.57 2.64 10 2 -20 1.78 2.79 10 2 -20 4.51 2.56 9 -2 -20 -0.74 2.43 9 -2 -20 0.28 2.40 9 2 -20 -0.35 2.08 9 2 -20 0.03 2.09 8 -2 -20 -0.63 1.89 8 2 -20 1.85 2.48 7 -2 -20 3.68 2.68 7 2 -20 8.96 2.98 6 -2 -20 -2.23 1.59 6 2 -20 0.13 2.01 5 -2 -20 19.97 3.99 5 2 -20 29.27 4.63 4 -2 -20 1.46 2.13 4 2 -20 2.73 2.76 3 -2 -20 -0.41 2.22 3 2 -20 -0.33 2.00 12 -3 -20 7.61 3.01 12 -3 -20 8.01 3.61 12 3 -20 6.51 3.02 12 3 -20 3.89 2.48 11 -3 -20 -3.05 1.98 11 -3 -20 -1.97 1.89 11 3 -20 2.46 2.37 11 3 -20 -0.55 2.05 10 -3 -20 2.34 2.64 10 -3 -20 5.16 3.09 10 3 -20 2.64 2.87 10 3 -20 6.35 2.72 9 -3 -20 5.64 3.04 9 -3 -20 2.14 2.54 9 3 -20 6.39 2.90 9 3 -20 4.08 2.38 8 -3 -20 1.30 2.24 8 3 -20 -2.23 1.98 7 -3 -20 1.51 2.10 7 3 -20 2.16 2.21 6 -3 -20 -0.16 2.30 6 3 -20 1.69 2.38 5 -3 -20 -1.41 2.17 5 3 -20 -2.52 1.74 4 -3 -20 19.01 3.90 4 3 -20 21.93 4.26 3 -3 -20 3.21 2.24 3 3 -20 -0.52 2.46 12 -4 -20 10.31 3.56 12 -4 -20 9.31 3.01 12 4 -20 8.15 2.91 12 4 -20 7.06 3.13 11 -4 -20 3.15 2.54 11 -4 -20 9.39 3.57 11 4 -20 8.70 3.21 11 4 -20 3.29 2.47 10 -4 -20 8.56 3.24 10 -4 -20 12.18 3.54 10 4 -20 4.35 2.45 10 4 -20 11.97 3.83 9 -4 -20 -3.17 1.65 9 -4 -20 4.53 2.67 9 4 -20 0.95 2.02 9 4 -20 6.30 2.97 8 -4 -20 2.33 2.35 8 4 -20 1.71 2.53 7 -4 -20 1.52 2.03 7 4 -20 0.13 2.36 6 -4 -20 13.58 3.54 6 4 -20 11.14 3.52 5 -4 -20 3.54 2.62 5 4 -20 6.15 3.16 4 -4 -20 2.76 2.43 4 4 -20 0.69 2.19 3 -4 -20 4.41 2.59 3 4 -20 -0.31 2.08 12 -5 -20 1.28 2.26 12 -5 -20 1.21 2.84 12 5 -20 0.13 1.86 12 5 -20 1.24 2.29 11 -5 -20 1.36 2.98 11 -5 -20 2.29 2.18 11 5 -20 1.92 2.21 11 5 -20 -0.32 2.61 10 -5 -20 2.10 3.10 10 -5 -20 -0.11 1.86 10 5 -20 -2.03 2.09 10 5 -20 -0.24 1.88 9 -5 -20 2.46 2.14 9 -5 -20 1.83 2.83 9 5 -20 4.28 2.94 8 -5 -20 4.37 2.43 8 5 -20 4.87 2.77 7 -5 -20 6.13 2.70 7 5 -20 8.53 3.09 6 -5 -20 0.72 2.25 6 5 -20 -2.31 1.93 5 -5 -20 7.90 3.06 5 5 -20 8.42 3.16 4 -5 -20 -0.18 2.04 4 5 -20 -1.26 2.35 11 -6 -20 14.19 4.32 11 -6 -20 8.94 3.02 11 6 -20 4.99 2.43 11 6 -20 17.98 4.08 10 -6 -20 2.30 2.36 10 -6 -20 1.38 3.06 10 6 -20 -1.17 2.29 10 6 -20 1.90 2.09 9 -6 -20 8.20 3.13 9 -6 -20 1.56 3.02 9 6 -20 7.06 2.96 8 -6 -20 0.90 2.30 8 6 -20 1.07 2.47 7 -6 -20 14.04 3.66 7 6 -20 16.01 3.96 6 -6 -20 13.93 3.52 6 6 -20 4.73 3.09 5 -6 -20 6.46 2.81 5 6 -20 6.07 3.08 4 -6 -20 2.87 2.76 4 6 -20 1.50 2.19 10 -7 -20 0.91 2.36 10 -7 -20 14.06 4.22 10 7 -20 3.51 2.23 10 7 -20 4.71 2.77 9 -7 -20 8.52 2.88 9 -7 -20 9.00 3.92 9 7 -20 6.52 3.40 8 -7 -20 32.40 4.78 8 7 -20 25.10 4.61 7 -7 -20 0.96 2.01 7 7 -20 2.26 2.31 6 -7 -20 -1.98 1.93 6 7 -20 0.17 2.16 5 -7 -20 -0.76 2.01 5 7 -20 0.03 2.55 9 -8 -20 1.99 2.34 9 -8 -20 -1.40 2.63 9 8 -20 -1.32 2.04 8 -8 -20 4.48 2.44 -8 8 20 0.08 2.87 8 8 -20 -1.93 1.73 7 -8 -20 16.85 3.62 7 8 -20 19.40 4.03 6 -8 -20 12.97 3.07 6 8 -20 4.26 2.63 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 50288 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pb1 Pb 0.84744(2) 0.61299(2) 0.70285(2) 0.02408(6) Uani 1 1 d . . . . . Cl1 Cl 0.88582(8) 0.76776(6) 0.86719(8) 0.0307(3) Uani 1 1 d . . . . . Cl2 Cl 0.78568(10) 0.57544(7) 0.39029(10) 0.0482(4) Uani 1 1 d . . . . . S1 S 0.80557(8) 0.48097(6) 0.69229(8) 0.0263(3) Uani 1 1 d . . . . . S2 S 1.00714(8) 0.54108(6) 0.68868(8) 0.0272(3) Uani 1 1 d . . . . . S3 S 0.98007(8) 0.56888(6) 0.88063(8) 0.0243(3) Uani 1 1 d . . . . . S4 S 0.74222(8) 0.57629(6) 0.82806(8) 0.0268(3) Uani 1 1 d . . . . . O1 O 0.6538(2) 0.60395(14) 0.5815(2) 0.0280(8) Uani 1 1 d . . . . . O2 O 0.7674(2) 0.71050(15) 0.5780(2) 0.0322(8) Uani 1 1 d . . . . . O3 O 0.9651(2) 0.69516(15) 0.6415(2) 0.0346(8) Uani 1 1 d . . . . . O4 O 1.1171(2) 0.65877(16) 1.0872(2) 0.0292(8) Uani 1 1 d . . . . . O5 O 0.9839(2) 0.66277(15) 1.1746(2) 0.0289(8) Uani 1 1 d . . . . . O6 O 0.7837(2) 0.64032(17) 1.0683(2) 0.0336(8) Uani 1 1 d . . . . . O7 O 0.9264(3) 0.74284(18) 0.9590(2) 0.0501(11) Uani 1 1 d . . . . . O8 O 0.8413(3) 0.71877(17) 0.8023(2) 0.0458(10) Uani 1 1 d . . . . . O9 O 0.9575(3) 0.7957(2) 0.8433(3) 0.0613(12) Uani 1 1 d . . . . . O10 O 0.8174(3) 0.81328(19) 0.8625(3) 0.0551(11) Uani 1 1 d . . . . . O11 O 0.8656(3) 0.5954(4) 0.3761(4) 0.127(3) Uani 1 1 d . . . . . O12 O 0.7049(3) 0.60827(18) 0.3297(3) 0.0509(11) Uani 1 1 d . . . . . O13 O 0.7692(4) 0.5100(2) 0.3773(4) 0.113(2) Uani 1 1 d . . . . . O14 O 0.8022(3) 0.58899(19) 0.4857(2) 0.0528(11) Uani 1 1 d . . . . . C1 C 0.5942(3) 0.5637(2) 0.6026(3) 0.0280(11) Uani 1 1 d . . . . . C2 C 0.5175(3) 0.5837(3) 0.6198(3) 0.0370(13) Uani 1 1 d . . . . . H2A H 0.502814 0.626768 0.617374 0.044 Uiso 1 1 calc R U . . . C3 C 0.4622(4) 0.5403(3) 0.6405(3) 0.0408(14) Uani 1 1 d . . . . . H3A H 0.408927 0.553684 0.651796 0.049 Uiso 1 1 calc R U . . . C4 C 0.4838(4) 0.4773(3) 0.6450(3) 0.0428(14) Uani 1 1 d . . . . . H4A H 0.446240 0.447656 0.659799 0.051 Uiso 1 1 calc R U . . . C5 C 0.5608(3) 0.4586(3) 0.6274(3) 0.0354(13) Uani 1 1 d . . . . . H5A H 0.575943 0.415632 0.630518 0.042 Uiso 1 1 calc R U . . . C6 C 0.6168(3) 0.5008(2) 0.6055(3) 0.0274(11) Uani 1 1 d . . . . . C7 C 0.6994(3) 0.4783(2) 0.5854(3) 0.0269(11) Uani 1 1 d . . . . . H7B H 0.707722 0.504970 0.537822 0.032 Uiso 1 1 calc R U . . . H7C H 0.687956 0.435148 0.561570 0.032 Uiso 1 1 calc R U . . . C8 C 0.8923(3) 0.4411(2) 0.6608(3) 0.0310(12) Uani 1 1 d . . . . . H8B H 0.941273 0.423895 0.717785 0.037 Uiso 1 1 calc R U . . . H8C H 0.861114 0.405506 0.620441 0.037 Uiso 1 1 calc R U . . . C9 C 0.9408(3) 0.4801(2) 0.6114(3) 0.0303(12) Uani 1 1 d . . . . . H9B H 0.893290 0.498437 0.554530 0.036 Uiso 1 1 calc R U . . . H9C H 0.983557 0.453631 0.593601 0.036 Uiso 1 1 calc R U . . . C10 C 1.0507(3) 0.5878(2) 0.6170(3) 0.0318(12) Uani 1 1 d . . . . . H10B H 1.090896 0.562287 0.594612 0.038 Uiso 1 1 calc R U . . . H10C H 0.997370 0.604252 0.562699 0.038 Uiso 1 1 calc R U . . . C11 C 1.1065(3) 0.6402(2) 0.6756(3) 0.0283(11) Uani 1 1 d . . . . . C12 C 1.2035(4) 0.6363(3) 0.7222(4) 0.0391(13) Uani 1 1 d . . . . . H12B H 1.234949 0.599147 0.718090 0.047 Uiso 1 1 calc R U . . . C13 C 1.2552(4) 0.6852(3) 0.7745(4) 0.0449(15) Uani 1 1 d . . . . . H13B H 1.321529 0.681517 0.805813 0.054 Uiso 1 1 calc R U . . . C14 C 1.2107(4) 0.7393(3) 0.7813(4) 0.0390(13) Uani 1 1 d . . . . . H14B H 1.246636 0.773225 0.816319 0.047 Uiso 1 1 calc R U . . . C15 C 1.1138(4) 0.7446(3) 0.7373(3) 0.0369(13) Uani 1 1 d . . . . . H15A H 1.082805 0.781658 0.742747 0.044 Uiso 1 1 calc R U . . . C16 C 1.0627(3) 0.6951(2) 0.6852(3) 0.0305(12) Uani 1 1 d . . . . . C17 C 0.9197(3) 0.7545(2) 0.6130(4) 0.0344(12) Uani 1 1 d . . . . . H17A H 0.957509 0.781269 0.589334 0.041 Uiso 1 1 calc R U . . . H17B H 0.912914 0.775716 0.666004 0.041 Uiso 1 1 calc R U . . . C18 C 0.8255(4) 0.7425(2) 0.5389(3) 0.0352(13) Uani 1 1 d . . . . . H18A H 0.795545 0.782394 0.511203 0.042 Uiso 1 1 calc R U . . . H18B H 0.832218 0.716831 0.489497 0.042 Uiso 1 1 calc R U . . . C19 C 0.6756(3) 0.6982(2) 0.5104(3) 0.0369(13) Uani 1 1 d . . . . . H19A H 0.680178 0.671740 0.460724 0.044 Uiso 1 1 calc R U . . . H19B H 0.644711 0.737730 0.482307 0.044 Uiso 1 1 calc R U . . . C20 C 0.6184(3) 0.6660(2) 0.5547(4) 0.0358(13) Uani 1 1 d . . . . . H20A H 0.621412 0.689600 0.609941 0.043 Uiso 1 1 calc R U . . . H20B H 0.551820 0.664056 0.510829 0.043 Uiso 1 1 calc R U . . . C21 C 1.1853(3) 0.6273(2) 1.0701(3) 0.0244(11) Uani 1 1 d . . . . . C22 C 1.2726(3) 0.6111(2) 1.1373(3) 0.0297(11) Uani 1 1 d . . . . . H22A H 1.289249 0.623968 1.199582 0.036 Uiso 1 1 calc R U . . . C23 C 1.3351(3) 0.5763(3) 1.1133(3) 0.0336(13) Uani 1 1 d . . . . . H23A H 1.394081 0.564708 1.159590 0.040 Uiso 1 1 calc R U . . . C24 C 1.3124(3) 0.5583(2) 1.0227(3) 0.0342(13) Uani 1 1 d . . . . . H24A H 1.355142 0.533930 1.006703 0.041 Uiso 1 1 calc R U . . . C25 C 1.2262(3) 0.5764(2) 0.9550(3) 0.0309(12) Uani 1 1 d . . . . . H25A H 1.211053 0.565014 0.892314 0.037 Uiso 1 1 calc R U . . . C26 C 1.1630(3) 0.6103(2) 0.9775(3) 0.0239(10) Uani 1 1 d . . . . . C27 C 1.0695(3) 0.6300(2) 0.9044(3) 0.0259(11) Uani 1 1 d . . . . . H27A H 1.077963 0.640224 0.846581 0.031 Uiso 1 1 calc R U . . . H27B H 1.047400 0.668042 0.925330 0.031 Uiso 1 1 calc R U . . . C28 C 0.9268(3) 0.5831(2) 0.9636(3) 0.0249(11) Uani 1 1 d . . . . . H28A H 0.969443 0.569212 1.026012 0.030 Uiso 1 1 calc R U . . . H28B H 0.914152 0.628054 0.966265 0.030 Uiso 1 1 calc R U . . . C29 C 0.8353(3) 0.5465(2) 0.9310(3) 0.0256(11) Uani 1 1 d . . . . . H29A H 0.812318 0.545623 0.981713 0.031 Uiso 1 1 calc R U . . . H29B H 0.848735 0.503098 0.919098 0.031 Uiso 1 1 calc R U . . . C30 C 0.7033(3) 0.6432(2) 0.8760(3) 0.0292(11) Uani 1 1 d . . . . . H30A H 0.758719 0.667919 0.914939 0.035 Uiso 1 1 calc R U . . . H30B H 0.662400 0.670055 0.824908 0.035 Uiso 1 1 calc R U . . . C31 C 0.6498(3) 0.6222(2) 0.9333(3) 0.0305(12) Uani 1 1 d . . . . . C32 C 0.5557(4) 0.6048(3) 0.8909(4) 0.0451(15) Uani 1 1 d . . . . . H32A H 0.525659 0.606410 0.825354 0.054 Uiso 1 1 calc R U . . . C33 C 0.5053(4) 0.5856(3) 0.9409(4) 0.0566(18) Uani 1 1 d . . . . . H33A H 0.441142 0.573688 0.910566 0.068 Uiso 1 1 calc R U . . . C34 C 0.5488(4) 0.5836(3) 1.0359(4) 0.0478(16) Uani 1 1 d . . . . . H34A H 0.513717 0.570844 1.070956 0.057 Uiso 1 1 calc R U . . . C35 C 0.6422(4) 0.5999(3) 1.0815(4) 0.0402(14) Uani 1 1 d . . . . . H35A H 0.671727 0.597102 1.146984 0.048 Uiso 1 1 calc R U . . . C36 C 0.6925(3) 0.6203(2) 1.0300(3) 0.0310(12) Uani 1 1 d . . . . . C37 C 0.8276(3) 0.6451(3) 1.1674(3) 0.0400(14) Uani 1 1 d . . . . . H37A H 0.850806 0.603921 1.194895 0.048 Uiso 1 1 calc R U . . . H37B H 0.781673 0.660403 1.192395 0.048 Uiso 1 1 calc R U . . . C38 C 0.9073(3) 0.6895(3) 1.1900(4) 0.0419(15) Uani 1 1 d . . . . . H38A H 0.885756 0.727251 1.151424 0.050 Uiso 1 1 calc R U . . . H38B H 0.928476 0.702110 1.255712 0.050 Uiso 1 1 calc R U . . . C39 C 1.0532(3) 0.7085(2) 1.1844(3) 0.0279(11) Uani 1 1 d . . . . . H39A H 1.069951 0.730153 1.244368 0.033 Uiso 1 1 calc R U . . . H39B H 1.027623 0.739744 1.134391 0.033 Uiso 1 1 calc R U . . . C40 C 1.1393(3) 0.6791(2) 1.1799(3) 0.0267(11) Uani 1 1 d . . . . . H40A H 1.191520 0.709634 1.198155 0.032 Uiso 1 1 calc R U . . . H40B H 1.159374 0.643355 1.222901 0.032 Uiso 1 1 calc R U . . . Cl1S Cl 0.7354(2) 0.35096(16) 0.4512(2) 0.0556(8) Uani 0.5 1 d . . P A 1 Cl2S Cl 0.9231(8) 0.2933(5) 0.5404(7) 0.098(3) Uani 0.5 1 d . . P A 1 C1S C 0.8101(7) 0.2852(4) 0.4782(7) 0.025(2) Uani 0.5 1 d . U P A 1 H1SA H 0.785258 0.255188 0.510772 0.030 Uiso 0.5 1 calc R U P A 1 H1SB H 0.803685 0.265671 0.418939 0.030 Uiso 0.5 1 calc R U P A 1 N1S N 0.9947(7) 0.2998(4) 0.5588(7) 0.036(2) Uani 0.5 1 d . U P B 2 C2S C 0.9201(14) 0.2980(11) 0.5496(18) 0.019(2) Uani 0.5 1 d . U P B 2 C3S C 0.7982(6) 0.2863(4) 0.5262(7) 0.0239(19) Uani 0.5 1 d . U P B 2 H3SA H 0.769800 0.325929 0.532389 0.036 Uiso 0.5 1 calc R U P B 2 H3SB H 0.791939 0.256190 0.570249 0.036 Uiso 0.5 1 calc R U P B 2 H3SC H 0.766078 0.270480 0.463068 0.036 Uiso 0.5 1 calc R U P B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pb1 0.02289(10) 0.02304(11) 0.02123(10) -0.00038(8) 0.00309(7) 0.00261(8) Cl1 0.0347(7) 0.0259(7) 0.0230(6) -0.0001(5) 0.0021(5) -0.0011(5) Cl2 0.0490(8) 0.0550(11) 0.0454(9) 0.0082(7) 0.0237(7) 0.0222(7) S1 0.0253(6) 0.0247(7) 0.0232(6) -0.0002(5) 0.0034(5) 0.0019(5) S2 0.0294(6) 0.0279(8) 0.0249(6) -0.0008(5) 0.0113(6) 0.0019(5) S3 0.0203(6) 0.0277(7) 0.0200(6) 0.0003(5) 0.0025(5) -0.0019(5) S4 0.0232(6) 0.0320(8) 0.0217(6) -0.0024(5) 0.0051(5) -0.0036(5) O1 0.0273(17) 0.023(2) 0.0281(18) 0.0009(14) 0.0045(15) 0.0073(14) O2 0.0315(19) 0.032(2) 0.0269(18) 0.0016(15) 0.0043(16) 0.0078(15) O3 0.036(2) 0.023(2) 0.044(2) 0.0008(16) 0.0148(18) 0.0040(15) O4 0.0248(17) 0.040(2) 0.0189(17) -0.0007(15) 0.0039(14) 0.0006(15) O5 0.0268(17) 0.032(2) 0.0262(18) 0.0002(15) 0.0090(15) -0.0024(14) O6 0.0271(18) 0.051(2) 0.0226(18) -0.0036(16) 0.0097(16) -0.0117(16) O7 0.063(3) 0.041(3) 0.029(2) 0.0115(17) -0.001(2) -0.0012(19) O8 0.061(3) 0.034(2) 0.037(2) -0.0171(17) 0.014(2) -0.0128(18) O9 0.057(3) 0.075(3) 0.053(3) -0.004(2) 0.022(2) -0.031(2) O10 0.057(3) 0.051(3) 0.042(2) -0.006(2) 0.003(2) 0.025(2) O11 0.051(3) 0.267(8) 0.078(4) 0.065(4) 0.042(3) 0.036(4) O12 0.049(2) 0.056(3) 0.045(2) 0.010(2) 0.016(2) 0.019(2) O13 0.149(5) 0.052(4) 0.094(4) -0.027(3) -0.002(4) 0.040(3) O14 0.072(3) 0.053(3) 0.034(2) 0.0061(19) 0.021(2) 0.021(2) C1 0.023(2) 0.033(3) 0.021(3) -0.005(2) 0.001(2) 0.001(2) C2 0.026(3) 0.045(4) 0.031(3) -0.008(3) 0.002(2) 0.006(2) C3 0.025(3) 0.065(5) 0.025(3) -0.011(3) 0.003(2) 0.001(3) C4 0.032(3) 0.064(5) 0.024(3) 0.003(3) 0.002(2) -0.005(3) C5 0.031(3) 0.042(4) 0.021(3) 0.000(2) -0.003(2) -0.002(2) C6 0.025(3) 0.033(3) 0.015(2) -0.004(2) -0.002(2) 0.003(2) C7 0.026(2) 0.023(3) 0.024(3) -0.003(2) 0.001(2) 0.002(2) C8 0.029(3) 0.024(3) 0.035(3) -0.002(2) 0.007(2) 0.003(2) C9 0.039(3) 0.025(3) 0.025(3) -0.003(2) 0.011(2) 0.009(2) C10 0.036(3) 0.035(3) 0.027(3) 0.000(2) 0.016(2) 0.003(2) C11 0.037(3) 0.027(3) 0.025(3) 0.003(2) 0.016(2) -0.003(2) C12 0.034(3) 0.040(4) 0.047(3) 0.009(3) 0.020(3) -0.001(2) C13 0.032(3) 0.052(4) 0.046(4) 0.008(3) 0.010(3) -0.008(3) C14 0.047(3) 0.037(4) 0.034(3) 0.002(2) 0.016(3) -0.012(3) C15 0.050(3) 0.034(3) 0.030(3) 0.003(2) 0.019(3) -0.002(3) C16 0.033(3) 0.034(3) 0.026(3) 0.005(2) 0.014(2) -0.001(2) C17 0.036(3) 0.029(3) 0.037(3) 0.001(2) 0.012(3) 0.008(2) C18 0.046(3) 0.029(3) 0.030(3) 0.006(2) 0.014(3) 0.008(2) C19 0.038(3) 0.031(3) 0.029(3) 0.003(2) -0.001(2) 0.005(2) C20 0.035(3) 0.026(3) 0.040(3) 0.001(2) 0.007(3) 0.016(2) C21 0.018(2) 0.030(3) 0.024(3) 0.003(2) 0.006(2) -0.0050(19) C22 0.023(2) 0.037(3) 0.026(3) 0.008(2) 0.006(2) -0.007(2) C23 0.016(2) 0.048(4) 0.032(3) 0.014(2) 0.004(2) 0.000(2) C24 0.026(3) 0.043(4) 0.037(3) 0.004(3) 0.016(2) 0.001(2) C25 0.030(3) 0.041(3) 0.022(3) 0.002(2) 0.012(2) -0.010(2) C26 0.019(2) 0.028(3) 0.024(2) 0.002(2) 0.008(2) -0.011(2) C27 0.029(3) 0.025(3) 0.021(2) 0.003(2) 0.007(2) -0.008(2) C28 0.028(3) 0.027(3) 0.019(2) -0.001(2) 0.009(2) -0.002(2) C29 0.027(2) 0.025(3) 0.024(3) 0.006(2) 0.009(2) -0.001(2) C30 0.028(3) 0.036(3) 0.024(3) 0.002(2) 0.010(2) 0.001(2) C31 0.027(3) 0.033(3) 0.033(3) -0.004(2) 0.014(2) -0.002(2) C32 0.033(3) 0.065(5) 0.034(3) -0.004(3) 0.010(3) -0.003(3) C33 0.026(3) 0.092(5) 0.047(4) -0.008(3) 0.009(3) -0.014(3) C34 0.035(3) 0.072(5) 0.047(4) -0.007(3) 0.027(3) -0.014(3) C35 0.033(3) 0.055(4) 0.035(3) -0.002(3) 0.016(3) -0.008(3) C36 0.024(3) 0.037(3) 0.032(3) -0.006(2) 0.012(2) -0.005(2) C37 0.032(3) 0.066(4) 0.023(3) -0.005(3) 0.012(2) 0.000(3) C38 0.025(3) 0.063(4) 0.033(3) -0.023(3) 0.006(2) -0.001(3) C39 0.032(3) 0.025(3) 0.024(3) -0.004(2) 0.008(2) -0.005(2) C40 0.024(2) 0.030(3) 0.020(2) 0.002(2) 0.002(2) -0.004(2) Cl1S 0.071(2) 0.062(2) 0.0417(17) -0.0035(15) 0.0302(16) 0.0114(16) Cl2S 0.132(5) 0.104(5) 0.051(4) 0.014(3) 0.031(3) 0.022(4) C1S 0.038(4) 0.022(4) 0.018(4) 0.001(3) 0.013(3) -0.014(3) N1S 0.034(2) 0.041(3) 0.035(3) -0.0002(18) 0.0158(19) -0.0020(18) C2S 0.019(2) 0.018(3) 0.018(3) -0.0016(10) 0.0065(13) 0.0005(10) C3S 0.025(2) 0.019(3) 0.026(3) -0.0025(18) 0.0084(18) -0.0040(18) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O2 Pb1 O1 61.58(9) . . ? O2 Pb1 S3 150.35(7) . . ? O1 Pb1 S3 141.35(7) . . ? O2 Pb1 S1 131.58(7) . . ? O1 Pb1 S1 75.15(7) . . ? S3 Pb1 S1 78.04(3) . . ? O2 Pb1 S2 119.04(7) . . ? O1 Pb1 S2 126.39(7) . . ? S3 Pb1 S2 67.06(3) . . ? S1 Pb1 S2 70.19(3) . . ? O2 Pb1 S4 115.88(7) . . ? O1 Pb1 S4 74.65(7) . . ? S3 Pb1 S4 69.75(3) . . ? S1 Pb1 S4 68.11(3) . . ? S2 Pb1 S4 124.47(3) . . ? O10 Cl1 O9 109.3(3) . . ? O10 Cl1 O7 109.5(2) . . ? O9 Cl1 O7 110.0(2) . . ? O10 Cl1 O8 109.2(2) . . ? O9 Cl1 O8 109.1(2) . . ? O7 Cl1 O8 109.8(2) . . ? O11 Cl2 O12 109.6(3) . . ? O11 Cl2 O13 113.4(4) . . ? O12 Cl2 O13 109.4(3) . . ? O11 Cl2 O14 107.0(3) . . ? O12 Cl2 O14 110.2(2) . . ? O13 Cl2 O14 107.2(3) . . ? C8 S1 C7 103.1(2) . . ? C8 S1 Pb1 107.87(17) . . ? C7 S1 Pb1 100.54(16) . . ? C9 S2 C10 103.6(2) . . ? C9 S2 Pb1 99.11(16) . . ? C10 S2 Pb1 105.88(17) . . ? C28 S3 C27 104.4(2) . . ? C28 S3 Pb1 106.73(15) . . ? C27 S3 Pb1 98.79(15) . . ? C29 S4 C30 100.6(2) . . ? C29 S4 Pb1 103.13(15) . . ? C30 S4 Pb1 113.42(16) . . ? C1 O1 C20 115.8(4) . . ? C1 O1 Pb1 120.0(2) . . ? C20 O1 Pb1 108.1(3) . . ? C19 O2 C18 111.9(4) . . ? C19 O2 Pb1 114.9(3) . . ? C18 O2 Pb1 118.5(3) . . ? C16 O3 C17 117.1(4) . . ? C21 O4 C40 117.2(3) . . ? C39 O5 C38 110.1(4) . . ? C36 O6 C37 118.0(4) . . ? C2 C1 C6 121.3(5) . . ? C2 C1 O1 123.1(5) . . ? C6 C1 O1 115.6(4) . . ? C1 C2 C3 119.2(5) . . ? C2 C3 C4 120.7(5) . . ? C5 C4 C3 118.9(5) . . ? C4 C5 C6 121.8(5) . . ? C5 C6 C1 118.2(5) . . ? C5 C6 C7 120.0(5) . . ? C1 C6 C7 121.8(4) . . ? C6 C7 S1 109.0(3) . . ? C9 C8 S1 116.1(3) . . ? C8 C9 S2 108.7(3) . . ? C11 C10 S2 107.3(3) . . ? C12 C11 C16 117.5(5) . . ? C12 C11 C10 121.4(5) . . ? C16 C11 C10 121.0(4) . . ? C13 C12 C11 121.4(5) . . ? C14 C13 C12 120.1(5) . . ? C13 C14 C15 120.3(5) . . ? C14 C15 C16 119.1(5) . . ? C15 C16 O3 123.2(5) . . ? C15 C16 C11 121.6(5) . . ? O3 C16 C11 115.1(4) . . ? O3 C17 C18 107.4(4) . . ? O2 C18 C17 109.2(4) . . ? O2 C19 C20 109.6(4) . . ? O1 C20 C19 110.0(4) . . ? O4 C21 C22 124.5(4) . . ? O4 C21 C26 115.9(4) . . ? C22 C21 C26 119.5(4) . . ? C23 C22 C21 120.0(5) . . ? C24 C23 C22 120.6(4) . . ? C23 C24 C25 119.3(5) . . ? C26 C25 C24 120.9(5) . . ? C25 C26 C21 119.6(4) . . ? C25 C26 C27 121.2(4) . . ? C21 C26 C27 119.2(4) . . ? C26 C27 S3 111.8(3) . . ? C29 C28 S3 107.0(3) . . ? C28 C29 S4 115.2(3) . . ? C31 C30 S4 110.7(3) . . ? C32 C31 C36 118.2(5) . . ? C32 C31 C30 120.4(5) . . ? C36 C31 C30 121.4(4) . . ? C33 C32 C31 121.8(5) . . ? C32 C33 C34 119.0(5) . . ? C33 C34 C35 121.5(5) . . ? C34 C35 C36 119.0(5) . . ? O6 C36 C35 123.7(4) . . ? O6 C36 C31 115.9(4) . . ? C35 C36 C31 120.4(4) . . ? O6 C37 C38 107.6(4) . . ? O5 C38 C37 111.5(4) . . ? O5 C39 C40 110.3(4) . . ? O4 C40 C39 108.2(4) . . ? Cl2S C1S Cl1S 120.0(7) . . ? N1S C2S C3S 173(2) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pb1 O2 2.806(3) . ? Pb1 O1 2.854(3) . ? Pb1 S3 2.9015(11) . ? Pb1 S1 2.9022(13) . ? Pb1 S2 2.9897(12) . ? Pb1 S4 3.1003(12) . ? Cl1 O10 1.420(4) . ? Cl1 O9 1.431(4) . ? Cl1 O7 1.432(4) . ? Cl1 O8 1.440(3) . ? Cl2 O11 1.403(5) . ? Cl2 O12 1.425(4) . ? Cl2 O13 1.430(5) . ? Cl2 O14 1.447(4) . ? S1 C8 1.814(5) . ? S1 C7 1.832(4) . ? S2 C9 1.809(5) . ? S2 C10 1.822(5) . ? S3 C28 1.816(5) . ? S3 C27 1.836(4) . ? S4 C29 1.809(4) . ? S4 C30 1.830(5) . ? O1 C1 1.394(6) . ? O1 C20 1.441(5) . ? O2 C19 1.424(5) . ? O2 C18 1.444(6) . ? O3 C16 1.390(6) . ? O3 C17 1.439(6) . ? O4 C21 1.364(5) . ? O4 C40 1.427(5) . ? O5 C39 1.416(5) . ? O5 C38 1.418(6) . ? O6 C36 1.366(5) . ? O6 C37 1.437(6) . ? C1 C2 1.382(7) . ? C1 C6 1.391(7) . ? C2 C3 1.388(8) . ? C3 C4 1.390(8) . ? C4 C5 1.380(7) . ? C5 C6 1.385(7) . ? C6 C7 1.508(6) . ? C8 C9 1.521(7) . ? C10 C11 1.497(7) . ? C11 C12 1.388(7) . ? C11 C16 1.397(7) . ? C12 C13 1.381(8) . ? C13 C14 1.376(8) . ? C14 C15 1.385(7) . ? C15 C16 1.387(7) . ? C17 C18 1.488(7) . ? C19 C20 1.490(7) . ? C21 C22 1.392(6) . ? C21 C26 1.406(6) . ? C22 C23 1.383(7) . ? C23 C24 1.381(7) . ? C24 C25 1.396(7) . ? C25 C26 1.369(7) . ? C26 C27 1.512(6) . ? C28 C29 1.520(6) . ? C30 C31 1.509(6) . ? C31 C32 1.391(7) . ? C31 C36 1.400(7) . ? C32 C33 1.368(8) . ? C33 C34 1.377(8) . ? C34 C35 1.380(7) . ? C35 C36 1.392(7) . ? C37 C38 1.486(7) . ? C39 C40 1.498(6) . ? Cl1S C1S 1.767(10) . ? Cl2S C1S 1.641(14) . ? N1S C2S 1.10(2) . ? C2S C3S 1.79(2) . ?