#------------------------------------------------------------------------------ #$Date: 2024-12-17 04:09:21 +0200 (Tue, 17 Dec 2024) $ #$Revision: 296887 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/96/7249696.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7249696 loop_ _publ_author_name 'Sato, Kazuyuki' 'Kuroki, Tomohiro' 'Minami, Haruka' 'Sato, Azusa' 'Karuo, Yukiko' 'Tarui, Atsushi' 'Kawai, Kentaro' 'Omote, Masaaki' _publ_section_title ; Electrophilic aromatic substitution using fluorinated isoxazolines at the C5 position via C--F bond cleavage ; _journal_issue 53 _journal_name_full 'RSC Advances' _journal_page_first 39543 _journal_page_last 39549 _journal_paper_doi 10.1039/D4RA07102F _journal_volume 14 _journal_year 2024 _chemical_formula_moiety 'C23 H19 F2 N O' _chemical_formula_sum 'C23 H19 F2 N O' _chemical_formula_weight 363.39 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2024-04-10 _audit_creation_method ; Olex2 1.5-ac5-024 (compiled 2022.04.12 svn.rca3783a0 for Rigaku Oxford Diffraction, GUI svn.r6498) ; _audit_update_record ; 2024-04-19 deposited with the CCDC. 2024-12-11 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 94.7070(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 13.4568(2) _cell_length_b 16.4098(2) _cell_length_c 8.25210(10) _cell_measurement_reflns_used 13500 _cell_measurement_temperature 119.9(5) _cell_measurement_theta_max 77.1010 _cell_measurement_theta_min 4.2320 _cell_volume 1816.11(4) _computing_cell_refinement 'CrysAlisPro 1.171.42.84a (Rigaku OD, 2023)' _computing_data_collection 'CrysAlisPro 1.171.42.84a (Rigaku OD, 2023)' _computing_data_reduction 'CrysAlisPro 1.171.42.84a (Rigaku OD, 2023)' _computing_molecular_graphics 'Olex2 1.5-ac5-024 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5-ac5-024 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 119.9(5) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -68.00 31.00 0.50 0.23 -- -43.07 68.00 59.00 198 2 \w -117.00 -18.00 0.50 0.23 -- -43.07 -68.00 -74.00 198 3 \w -77.00 -30.00 0.50 0.90 -- -104.50 68.00 59.00 94 4 \w 88.00 178.00 0.50 0.90 -- 113.00 68.00 59.00 180 5 \w 39.00 87.00 0.50 0.90 -- 113.00 -68.00 -74.00 96 6 \w -39.00 34.00 0.50 0.23 -- -43.07 38.00-150.00 146 7 \w -25.00 38.00 0.50 0.23 -- -43.07 19.00 60.00 126 8 \w -66.00 -30.00 0.50 0.90 -- -104.50 61.00 -90.00 72 9 \w -174.00 -79.00 0.50 0.90 -- -104.50 -68.00 -74.00 190 10 \w -66.00 -30.00 0.50 0.90 -- -104.50 61.00 -60.00 72 11 \w 89.00 178.00 0.50 0.90 -- 113.00 30.00 120.00 178 12 \w 90.00 178.00 0.50 0.90 -- 113.00 95.00 135.61 176 13 \w 89.00 178.00 0.50 0.90 -- 113.00 30.00 150.00 178 14 \w 39.00 76.00 0.50 0.90 -- 113.00 -61.00 60.00 74 15 \w 39.00 76.00 0.50 0.90 -- 113.00 -61.00 -30.00 74 16 \w 39.00 106.00 0.50 0.90 -- 113.00 -77.00 60.00 134 17 \w 91.00 178.00 0.50 0.90 -- 113.00 45.00 90.00 174 18 \w 89.00 178.00 0.50 0.90 -- 113.00 30.00-180.00 178 19 \w 38.00 106.00 0.50 0.90 -- 113.00 -95.00 60.00 136 20 \w 40.00 108.00 0.50 0.90 -- 113.00-110.00 -68.53 136 21 \w 41.00 112.00 0.50 0.90 -- 113.00-125.00-180.00 142 22 \w 91.00 178.00 0.50 0.90 -- 113.00 45.00 -30.00 174 23 \w 39.00 106.00 0.50 0.90 -- 113.00 -77.00 90.00 134 24 \w 41.00 112.00 0.50 0.90 -- 113.00-125.00 -30.00 142 25 \w 39.00 106.00 0.50 0.90 -- 113.00 -77.00 -90.00 134 26 \w 39.00 106.00 0.50 0.90 -- 113.00 -77.00 0.00 134 27 \w 92.00 178.00 0.50 0.90 -- 113.00 51.00 -8.97 172 28 \w 39.00 106.00 0.50 0.90 -- 113.00 -77.00-180.00 134 29 \w 39.00 106.00 0.50 0.90 -- 113.00 -77.00 -30.00 134 30 \w 41.00 112.00 0.50 0.90 -- 113.00-125.00 -60.00 142 31 \w 39.00 76.00 0.50 0.90 -- 113.00 -61.00 120.00 74 32 \w 38.00 106.00 0.50 0.90 -- 113.00 -95.00 30.00 136 33 \w 38.00 106.00 0.50 0.90 -- 113.00 -95.00-150.00 136 34 \w 38.00 106.00 0.50 0.90 -- 113.00 -95.00 -90.00 136 35 \w 41.00 112.00 0.50 0.90 -- 113.00-125.00-120.00 142 36 \w 39.00 76.00 0.50 0.90 -- 113.00 -61.00 90.00 74 37 \w -117.00 -14.00 0.50 0.23 -- -43.07 -77.00-180.00 206 38 \w -117.00 -14.00 0.50 0.23 -- -43.07 -77.00 90.00 206 39 \w -39.00 34.00 0.50 0.23 -- -43.07 38.00 -60.00 146 40 \w -39.00 34.00 0.50 0.23 -- -43.07 38.00 150.00 146 41 \w -117.00 -20.00 0.50 0.23 -- -43.07 -57.00 0.00 194 42 \w 63.00 130.00 0.50 0.90 -- 113.00 15.00 -90.00 134 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy R, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0120160000 _diffrn_orient_matrix_UB_12 0.0717633000 _diffrn_orient_matrix_UB_13 -0.1171631000 _diffrn_orient_matrix_UB_21 0.1141753000 _diffrn_orient_matrix_UB_22 -0.0095551000 _diffrn_orient_matrix_UB_23 0.0230425000 _diffrn_orient_matrix_UB_31 -0.0037256000 _diffrn_orient_matrix_UB_32 -0.0597664000 _diffrn_orient_matrix_UB_33 -0.1443328000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0392 _diffrn_reflns_av_unetI/netI 0.0213 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_l_max 9 _diffrn_reflns_limit_l_min -10 _diffrn_reflns_number 31987 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 77.725 _diffrn_reflns_theta_min 3.295 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'PhotonJet R (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.783 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.68509 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.84a (Rigaku Oxford Diffraction, 2023) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.329 _exptl_crystal_description block _exptl_crystal_F_000 760 _exptl_crystal_recrystallization_method 'Re-crystallisation from solvent: hexane and ethylacetate' _exptl_crystal_size_max 0.12 _exptl_crystal_size_mid 0.081 _exptl_crystal_size_min 0.041 _refine_diff_density_max 0.409 _refine_diff_density_min -0.169 _refine_diff_density_rms 0.039 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.086 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 246 _refine_ls_number_reflns 3869 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.086 _refine_ls_R_factor_all 0.0479 _refine_ls_R_factor_gt 0.0450 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0419P)^2^+0.8909P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1061 _refine_ls_wR_factor_ref 0.1079 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3677 _reflns_number_total 3869 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL x-1335_auto_a.res in P2(1)/c x-1335_auto.res created by SHELXL-2018/3 at 10:18:37 on 10-Apr-2024 REM Old TITL X-1335_auto in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.117, Rweak 0.066, Alpha 0.020 REM 1.162 for 145 systematic absences, Orientation as input REM Formula found by SHELXT: C23 N O F25 CELL 1.54184 13.4568 16.4098 8.2521 90 94.707 90 ZERR 4 0.0002 0.0002 0.0001 0 0.001 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H F N O UNIT 92 76 8 4 4 L.S. 30 PLAN 1 SIZE 0.041 0.081 0.12 TEMP -153.2(5) fmap 2 acta REM REM REM WGHT 0.041900 0.890900 FVAR 3.88188 C1 1 0.327892 0.416805 0.735889 11.00000 0.02884 0.02477 = 0.02520 -0.00091 0.00103 0.00170 C2 1 0.299912 0.336025 0.766617 11.00000 0.03003 0.02462 = 0.03116 -0.00201 0.00434 -0.00008 C3 1 0.368823 0.286402 0.856130 11.00000 0.03673 0.02350 = 0.03493 0.00188 0.00692 0.00220 AFIX 43 H3 2 0.349596 0.232378 0.880679 11.00000 -1.20000 AFIX 0 C4 1 0.463812 0.312200 0.910782 11.00000 0.03324 0.02897 = 0.02898 -0.00098 0.00316 0.00671 C5 1 0.492482 0.390344 0.868789 11.00000 0.02780 0.03076 = 0.03227 -0.00158 -0.00099 0.00166 AFIX 43 H5 2 0.558500 0.408522 0.898471 11.00000 -1.20000 AFIX 0 C6 1 0.425208 0.441754 0.783907 11.00000 0.03052 0.02551 = 0.03087 0.00031 0.00004 -0.00106 AFIX 43 H6 2 0.445670 0.495232 0.757692 11.00000 -1.20000 AFIX 0 C7 1 0.170318 0.600772 0.669173 11.00000 0.02919 0.02717 = 0.02477 -0.00144 -0.00013 0.00016 C10 1 0.255575 0.476016 0.646897 11.00000 0.02493 0.02422 = 0.02799 0.00013 0.00108 -0.00166 C11 1 0.274895 0.567240 0.681486 11.00000 0.02832 0.02524 = 0.02940 -0.00030 -0.00127 -0.00137 C12 1 0.142699 0.686506 0.640586 11.00000 0.03031 0.02597 = 0.02776 -0.00080 0.00108 0.00220 C13 1 0.052581 0.705466 0.552456 11.00000 0.03332 0.02874 = 0.03907 0.00157 -0.00340 -0.00158 AFIX 43 H13 2 0.009315 0.663104 0.511847 11.00000 -1.20000 AFIX 0 C14 1 0.026524 0.786077 0.524487 11.00000 0.03665 0.03196 = 0.04707 0.00304 -0.00700 0.00362 AFIX 43 H14 2 -0.034722 0.798946 0.464420 11.00000 -1.20000 AFIX 0 C15 1 0.089245 0.848236 0.583580 11.00000 0.04565 0.02620 = 0.04575 0.00150 -0.00259 0.00423 AFIX 43 H15 2 0.070729 0.903476 0.564336 11.00000 -1.20000 AFIX 0 C16 1 0.178974 0.829862 0.670744 11.00000 0.04290 0.02683 = 0.04335 -0.00397 -0.00430 -0.00221 AFIX 43 H16 2 0.221841 0.872478 0.711380 11.00000 -1.20000 AFIX 0 C17 1 0.206036 0.749219 0.698500 11.00000 0.03393 0.03054 = 0.03687 -0.00237 -0.00434 0.00193 AFIX 43 H17 2 0.267856 0.736632 0.757095 11.00000 -1.20000 AFIX 0 C18 1 0.244485 0.461534 0.461947 11.00000 0.03207 0.02035 = 0.02863 0.00030 0.00174 -0.00150 C19 1 0.329249 0.451627 0.377416 11.00000 0.03402 0.02928 = 0.03380 0.00055 0.00441 -0.00057 AFIX 43 H19 2 0.393612 0.453543 0.433954 11.00000 -1.20000 AFIX 0 C20 1 0.319441 0.438943 0.210318 11.00000 0.04937 0.03385 = 0.03528 -0.00023 0.01422 0.00136 AFIX 43 H20 2 0.377274 0.432352 0.152888 11.00000 -1.20000 AFIX 0 C21 1 0.225706 0.435849 0.126892 11.00000 0.06175 0.02909 = 0.02798 -0.00184 0.00177 -0.00080 AFIX 43 H21 2 0.219324 0.427305 0.012650 11.00000 -1.20000 AFIX 0 C22 1 0.141857 0.445232 0.210551 11.00000 0.04591 0.02428 = 0.03280 -0.00069 -0.00599 -0.00121 AFIX 43 H22 2 0.077591 0.442720 0.153791 11.00000 -1.20000 AFIX 0 C23 1 0.150889 0.458339 0.377393 11.00000 0.03330 0.02232 = 0.03067 -0.00013 -0.00077 -0.00135 AFIX 43 H23 2 0.092774 0.465156 0.434025 11.00000 -1.20000 AFIX 0 C26 1 0.200426 0.299783 0.707215 11.00000 0.03451 0.02503 = 0.04993 0.00152 -0.00067 -0.00332 AFIX 137 H26A 2 0.148657 0.320823 0.772910 11.00000 -1.50000 H26B 2 0.203645 0.240311 0.717107 11.00000 -1.50000 H26C 2 0.184386 0.314687 0.593062 11.00000 -1.50000 AFIX 0 C27 1 0.534048 0.257288 1.012318 11.00000 0.03888 0.03552 = 0.04327 0.00643 0.00143 0.00918 AFIX 137 H27A 2 0.600917 0.261004 0.973955 11.00000 -1.50000 H27B 2 0.510350 0.200894 1.002529 11.00000 -1.50000 H27C 2 0.536490 0.274308 1.126409 11.00000 -1.50000 AFIX 0 F24 3 0.336534 0.602652 0.580861 11.00000 0.03151 0.02621 = 0.04884 0.00166 0.00770 -0.00377 F25 3 0.316022 0.582086 0.836360 11.00000 0.03976 0.03069 = 0.03699 -0.00746 -0.01237 0.00301 N8 4 0.107174 0.544540 0.692659 11.00000 0.03060 0.02673 = 0.03007 0.00027 0.00160 0.00396 O9 5 0.157404 0.468284 0.709137 11.00000 0.02654 0.02397 = 0.03208 0.00209 0.00328 0.00124 HKLF 4 REM x-1335_auto_a.res in P2(1)/c REM wR2 = 0.1079, GooF = S = 1.086, Restrained GooF = 1.086 for all data REM R1 = 0.0450 for 3677 Fo > 4sig(Fo) and 0.0479 for all 3869 data REM 246 parameters refined using 0 restraints END WGHT 0.0419 0.8910 REM Highest difference peak 0.409, deepest hole -0.169, 1-sigma level 0.039 Q1 1 0.1913 0.4150 -0.0078 11.00000 0.05 0.41 REM The information below was added by Olex2. REM REM R1 = 0.0450 for 3677 Fo > 4sig(Fo) and 0.0479 for all 32615 data REM 246 parameters refined using n/a restraints REM Highest difference peak 0.41, deepest hole -0.17 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0479 REM R1_gt = 0.0450 REM wR_ref = 0.1079 REM GOOF = 1.086 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 32615 REM Reflections_gt = 3677 REM Parameters = 246 REM Hole = -0.17 REM Peak = 0.41 REM Flack = n/a ; _cod_data_source_file d4ra07102f2.cif _cod_data_source_block x-1335_auto _cod_database_code 7249696 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C23 H19 F2 N O' _chemical_oxdiff_usercomment 5aI _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.969 _shelx_estimated_absorpt_t_min 0.912 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C3(H3), C5(H5), C6(H6), C13(H13), C14(H14), C15(H15), C16(H16), C17(H17), C19(H19), C20(H20), C21(H21), C22(H22), C23(H23) 2.b Idealised Me refined as rotating group: C26(H26A,H26B,H26C), C27(H27A,H27B,H27C) ; _olex2_exptl_crystal_mounting_method ; The crystal was mounted on a MiTeGEN Dual Thickness MicroLoops in perfluoropolyether oil ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.602 _oxdiff_exptl_absorpt_empirical_full_min 0.680 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.32789(10) 0.41680(8) 0.73589(17) 0.0263(3) Uani 1 1 d . . . . . C2 C 0.29991(11) 0.33603(9) 0.76662(18) 0.0285(3) Uani 1 1 d . . . . . C3 C 0.36882(12) 0.28640(9) 0.85613(19) 0.0315(3) Uani 1 1 d . . . . . H3 H 0.349596 0.232378 0.880679 0.038 Uiso 1 1 calc R U . . . C4 C 0.46381(11) 0.31220(9) 0.91078(18) 0.0304(3) Uani 1 1 d . . . . . C5 C 0.49248(11) 0.39034(9) 0.86879(18) 0.0305(3) Uani 1 1 d . . . . . H5 H 0.558500 0.408522 0.898471 0.037 Uiso 1 1 calc R U . . . C6 C 0.42521(11) 0.44175(9) 0.78391(18) 0.0291(3) Uani 1 1 d . . . . . H6 H 0.445670 0.495232 0.757692 0.035 Uiso 1 1 calc R U . . . C7 C 0.17032(11) 0.60077(9) 0.66917(16) 0.0272(3) Uani 1 1 d . . . . . C10 C 0.25558(10) 0.47602(8) 0.64690(17) 0.0258(3) Uani 1 1 d . . . . . C11 C 0.27489(11) 0.56724(9) 0.68149(17) 0.0279(3) Uani 1 1 d . . . . . C12 C 0.14270(11) 0.68651(9) 0.64059(17) 0.0281(3) Uani 1 1 d . . . . . C13 C 0.05258(12) 0.70547(9) 0.5525(2) 0.0341(3) Uani 1 1 d . . . . . H13 H 0.009315 0.663104 0.511847 0.041 Uiso 1 1 calc R U . . . C14 C 0.02652(13) 0.78608(10) 0.5245(2) 0.0391(4) Uani 1 1 d . . . . . H14 H -0.034722 0.798946 0.464420 0.047 Uiso 1 1 calc R U . . . C15 C 0.08924(13) 0.84824(10) 0.5836(2) 0.0395(4) Uani 1 1 d . . . . . H15 H 0.070729 0.903476 0.564336 0.047 Uiso 1 1 calc R U . . . C16 C 0.17897(13) 0.82986(10) 0.6707(2) 0.0381(4) Uani 1 1 d . . . . . H16 H 0.221841 0.872478 0.711380 0.046 Uiso 1 1 calc R U . . . C17 C 0.20604(12) 0.74922(9) 0.69850(19) 0.0342(3) Uani 1 1 d . . . . . H17 H 0.267856 0.736632 0.757095 0.041 Uiso 1 1 calc R U . . . C18 C 0.24449(11) 0.46153(8) 0.46195(17) 0.0271(3) Uani 1 1 d . . . . . C19 C 0.32925(12) 0.45163(9) 0.37742(19) 0.0323(3) Uani 1 1 d . . . . . H19 H 0.393612 0.453543 0.433954 0.039 Uiso 1 1 calc R U . . . C20 C 0.31944(13) 0.43894(10) 0.2103(2) 0.0389(4) Uani 1 1 d . . . . . H20 H 0.377274 0.432352 0.152888 0.047 Uiso 1 1 calc R U . . . C21 C 0.22571(14) 0.43585(10) 0.12689(19) 0.0397(4) Uani 1 1 d . . . . . H21 H 0.219324 0.427305 0.012650 0.048 Uiso 1 1 calc R U . . . C22 C 0.14186(13) 0.44523(9) 0.21055(19) 0.0348(3) Uani 1 1 d . . . . . H22 H 0.077591 0.442720 0.153791 0.042 Uiso 1 1 calc R U . . . C23 C 0.15089(11) 0.45834(8) 0.37739(18) 0.0289(3) Uani 1 1 d . . . . . H23 H 0.092774 0.465156 0.434025 0.035 Uiso 1 1 calc R U . . . C26 C 0.20043(12) 0.29978(9) 0.7072(2) 0.0367(4) Uani 1 1 d . . . . . H26A H 0.148657 0.320823 0.772910 0.055 Uiso 1 1 calc R U . . . H26B H 0.203645 0.240311 0.717107 0.055 Uiso 1 1 calc R U . . . H26C H 0.184386 0.314687 0.593062 0.055 Uiso 1 1 calc R U . . . C27 C 0.53405(13) 0.25729(10) 1.0123(2) 0.0393(4) Uani 1 1 d . . . . . H27A H 0.600917 0.261004 0.973955 0.059 Uiso 1 1 calc R U . . . H27B H 0.510350 0.200894 1.002529 0.059 Uiso 1 1 calc R U . . . H27C H 0.536490 0.274308 1.126409 0.059 Uiso 1 1 calc R U . . . F24 F 0.33653(6) 0.60265(5) 0.58086(12) 0.0353(2) Uani 1 1 d . . . . . F25 F 0.31602(7) 0.58209(5) 0.83636(11) 0.0367(2) Uani 1 1 d . . . . . N8 N 0.10717(9) 0.54454(7) 0.69266(15) 0.0292(3) Uani 1 1 d . . . . . O9 O 0.15740(7) 0.46828(6) 0.70914(12) 0.0275(2) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0288(7) 0.0248(7) 0.0252(6) -0.0009(5) 0.0010(5) 0.0017(5) C2 0.0300(7) 0.0246(7) 0.0312(7) -0.0020(5) 0.0043(6) -0.0001(5) C3 0.0367(8) 0.0235(7) 0.0349(7) 0.0019(6) 0.0069(6) 0.0022(6) C4 0.0332(7) 0.0290(7) 0.0290(7) -0.0010(6) 0.0032(6) 0.0067(6) C5 0.0278(7) 0.0308(7) 0.0323(7) -0.0016(6) -0.0010(6) 0.0017(6) C6 0.0305(7) 0.0255(7) 0.0309(7) 0.0003(5) 0.0000(6) -0.0011(5) C7 0.0292(7) 0.0272(7) 0.0248(6) -0.0014(5) -0.0001(5) 0.0002(5) C10 0.0249(7) 0.0242(7) 0.0280(7) 0.0001(5) 0.0011(5) -0.0017(5) C11 0.0283(7) 0.0252(7) 0.0294(7) -0.0003(5) -0.0013(5) -0.0014(5) C12 0.0303(7) 0.0260(7) 0.0278(7) -0.0008(5) 0.0011(5) 0.0022(5) C13 0.0333(8) 0.0287(7) 0.0391(8) 0.0016(6) -0.0034(6) -0.0016(6) C14 0.0367(8) 0.0320(8) 0.0471(9) 0.0030(7) -0.0070(7) 0.0036(6) C15 0.0456(9) 0.0262(7) 0.0457(9) 0.0015(7) -0.0026(7) 0.0042(7) C16 0.0429(9) 0.0268(7) 0.0433(9) -0.0040(6) -0.0043(7) -0.0022(6) C17 0.0339(8) 0.0305(8) 0.0369(8) -0.0024(6) -0.0043(6) 0.0019(6) C18 0.0321(7) 0.0204(6) 0.0286(7) 0.0003(5) 0.0017(6) -0.0015(5) C19 0.0340(8) 0.0293(7) 0.0338(8) 0.0006(6) 0.0044(6) -0.0006(6) C20 0.0494(10) 0.0339(8) 0.0353(8) -0.0002(6) 0.0142(7) 0.0014(7) C21 0.0618(11) 0.0291(8) 0.0280(7) -0.0018(6) 0.0018(7) -0.0008(7) C22 0.0459(9) 0.0243(7) 0.0328(8) -0.0007(6) -0.0060(6) -0.0012(6) C23 0.0333(7) 0.0223(6) 0.0307(7) -0.0001(5) -0.0008(6) -0.0014(5) C26 0.0345(8) 0.0250(7) 0.0499(9) 0.0015(6) -0.0007(7) -0.0033(6) C27 0.0389(9) 0.0355(8) 0.0433(9) 0.0064(7) 0.0014(7) 0.0092(7) F24 0.0315(4) 0.0262(4) 0.0488(5) 0.0017(4) 0.0077(4) -0.0038(3) F25 0.0398(5) 0.0307(5) 0.0370(5) -0.0075(4) -0.0124(4) 0.0030(4) N8 0.0306(6) 0.0267(6) 0.0301(6) 0.0003(5) 0.0016(5) 0.0040(5) O9 0.0265(5) 0.0240(5) 0.0321(5) 0.0021(4) 0.0033(4) 0.0012(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u _diffrn_refln_scale_group_code 0 0 -1 7.32911 19.9983 7 0 0 1 45.8381 9.7475 38 0 0 1 1.31252 17.038 41 0 0 -1 10.4206 24.4094 1 0 0 -2 175750 7224.81 7 0 0 2 169675 7216.63 38 0 0 -2 178061 7228.73 1 0 0 2 184977 7224.47 41 0 0 -3 -27.058 43.6129 7 0 0 3 12.307 19.6191 6 0 0 -3 -16.4526 54.6214 1 0 0 3 -10.8402 15.629 38 0 0 3 4.71392 42.9343 41 0 0 -4 10157.1 438.225 39 0 0 -4 10592.5 471.079 1 0 0 4 10463.2 456.23 41 0 0 -5 -27.9657 77.508 1 0 0 5 39.1146 55.195 41 0 0 -6 4566.76 213.762 3 0 0 6 5166.15 253.088 41 0 0 -6 5113.19 277.226 1 0 0 -7 94.4443 63.479 25 0 0 -7 2.3555 48.5613 3 0 0 -7 -12.1317 65.968 34 0 0 7 120.126 71.9811 2 0 0 -7 42.1556 95.9143 1 0 0 -7 111.48 84.7571 12 0 0 -7 79.5566 67.429 5 0 0 -7 17.4408 65.1699 20 0 0 -8 127.734 58.0768 3 0 0 -8 191.386 54.066 34 0 0 -8 334.965 65.193 15 0 0 -8 108.745 68.2403 5 0 0 -8 315.336 63.2345 12 0 0 -8 216.14 47.517 32 0 0 -8 151.528 62.1305 25 0 0 -9 -30.5711 50.8136 15 0 0 -9 5.30136 57.2726 5 0 0 -9 4.11192 46.4938 12 0 0 -9 67.3014 35.6677 32 0 0 -9 77.5489 40.7987 26 0 0 -9 48.3605 51.1173 25 0 0 -10 72.2392 40.1758 15 0 1 0 18.7897 8.82333 7 0 1 0 3.92369 9.90161 37 0 1 -1 25268.6 1072.93 1 0 -1 -1 26386 1068.32 39 0 -1 1 25656.2 1071.46 6 0 -1 -1 25439.7 1068.98 7 0 -1 1 26568.6 1073.02 41 0 -1 1 25483.9 1067.83 38 0 1 -2 212667 8742.86 1 0 -1 -2 213389 8731.72 39 0 1 -2 215198 8741.26 7 0 -1 2 205873 8735.31 6 0 -1 -2 214236 8736.6 7 0 -1 2 218383 8740.44 41 0 1 2 214798 8736.39 41 0 1 -2 221003 8740.64 37 0 -1 2 205660 8729.25 38 0 1 -3 149.406 59.6003 1 0 -1 -3 149.063 21.4913 39 0 -1 -3 44.7445 42.2855 7 0 1 -3 91.8208 51.5522 7 0 -1 3 112.957 29.2276 6 0 1 3 72.0181 38.4321 41 0 -1 3 133.298 49.3079 41 0 1 -3 134.756 45.4226 37 0 1 3 136.423 23.6339 38 0 1 -4 6379.13 308.709 7 0 -1 -4 6306.96 284.132 39 0 1 -4 7139.15 322.628 1 0 1 4 7439.27 306.959 41 0 -1 4 7297.89 311.626 41 0 1 -5 91.6405 79.6054 1 0 1 5 32.2023 49.1356 41 0 -1 5 67.711 59.7263 41 0 1 -6 63.3372 87.6562 1 0 -1 6 85.5399 59.9152 41 0 1 6 35.8938 53.4084 41 0 1 -6 51.6878 38.307 3 0 1 -7 348.343 76.4651 12 0 -1 -7 394.403 82.1434 12 0 1 -7 292.532 68.6459 5 0 -1 -7 319.603 66.6073 25 0 1 -7 225.005 65.3737 25 0 -1 -7 421.536 93.1925 20 0 1 -7 255.413 53.5553 3 0 1 7 216.972 77.9643 2 0 -1 -7 251.796 65.0629 29 0 1 -7 301.353 75.4011 34 0 -1 -7 310.637 62.2076 34 0 -1 -7 195.863 81.8704 32 0 -1 -8 116.167 62.2715 25 0 1 -8 159.396 61.4652 25 0 1 -8 123.984 60.9091 12 0 -1 -8 146.18 57.8351 12 0 1 -8 59.2092 68.2321 5 0 -1 -8 183.505 44.6601 20 0 1 -8 -26.0119 59.7876 3 0 -1 -8 292.901 56.1112 34 0 1 -8 110.792 49.7331 34 0 -1 -8 85.2682 50.2591 26 0 -1 -8 153.882 61.3153 15 0 -1 -8 210.376 64.2115 29 0 1 -8 156.256 63.9594 29 0 1 -8 195.534 48.2244 32 0 -1 -8 189.089 47.0347 32 0 -1 -9 621.514 61.167 29 0 1 -9 745.632 62.7769 29 0 1 -9 689.702 66.8943 5 0 1 -9 520.383 48.3502 32 0 -1 -9 582.414 46.6644 32 0 -1 -9 614.587 50.0004 26 0 1 -9 759.069 61.2881 25 0 1 -9 589.664 53.681 26 0 -1 -9 540.168 56.3328 12 0 1 -9 508.753 58.0116 12 0 -1 -9 631.188 58.0579 15 0 1 -9 598.283 62.2787 15 0 -1 -9 632 62.6992 25 0 -1 -10 177.285 40.8812 29 0 1 -10 212.307 42.7463 29 0 1 -10 158.258 41.2441 15 0 1 -10 103.509 32.741 26 0 2 0 68586.3 2828.39 37 0 2 0 68134.9 2826.37 7 0 -2 -1 4840.47 205.303 39 0 -2 -1 4784.29 203.482 40 0 -2 1 4982.26 210.783 41 0 -2 -1 4536.78 207.115 1 0 2 -1 4722.11 207.596 1 0 2 -1 4867.93 211.478 7 0 -2 -1 4987.52 204.889 6 0 -2 1 4668.28 209.829 6 0 2 -2 112000 4604.71 1 0 -2 -2 113186 4604.35 1 0 -2 -2 109578 4593.87 39 0 -2 2 106203 4599.7 6 0 -2 2 112622 4604.39 41 0 2 -2 117444 4604.83 37 0 2 -3 29422.3 1178.2 1 0 -2 -3 30185.9 1178.21 1 0 -2 -3 26047.8 1155.02 39 0 -2 3 28808.9 1174.72 41 0 2 3 29780 1165.5 41 0 2 -3 29072.5 1172.76 37 0 -2 3 26267.6 1162.8 6 0 2 -3 28606.4 1174.85 7 0 2 -4 6359.24 292.097 37 0 2 -4 6314.09 298.282 7 0 -2 4 5528.94 274.436 6 0 -2 -4 6671.48 304.645 1 0 2 -4 6637.69 306.131 1 0 -2 4 6795.7 299.379 41 0 2 4 6636.76 286.628 41 0 -2 -5 13147.3 581.841 1 0 2 -5 12985.5 582.634 1 0 2 5 12543.6 556.913 41 0 -2 5 12063.6 565.203 41 0 2 -6 54.6216 85.8816 1 0 -2 -6 71.229 84.0033 1 0 -2 6 209.597 66.7223 41 0 -2 -6 101.687 34.985 3 0 2 -6 183.994 38.5111 3 0 -2 -7 7251.06 289.351 29 0 -2 -7 6736.75 291.792 12 0 2 -7 6831.27 293.062 12 0 -2 -7 6805.81 289.741 5 0 2 -7 6927.43 289.996 5 0 2 -7 6649.81 287.794 25 0 -2 -7 6377.56 288.3 24 0 -2 7 5297.68 326.632 41 0 2 -7 5904.71 289.385 3 0 2 7 6134.86 329.306 2 0 -2 -7 6306.18 290.155 3 0 -2 7 6667.53 332.191 2 0 -2 -7 6574.79 286.816 34 0 2 -7 6077.2 287.639 34 0 -2 -7 6436.19 287.005 32 0 -2 -7 6157.27 290.822 30 0 -2 -7 6524.39 285.342 20 0 2 -8 178.285 59.0204 25 0 2 -8 169.468 61.1937 12 0 -2 -8 115.343 57.0228 12 0 -2 -8 96.0466 66.8495 5 0 2 -8 209.613 67.6063 5 0 -2 -8 156.44 49.2337 20 0 -2 -8 66.7056 56.099 3 0 2 -8 116.87 58.1926 3 0 -2 -8 119.52 62.6664 29 0 2 -8 169.392 63.9195 29 0 -2 -8 95.5418 56.7389 15 0 -2 -8 211.601 46.698 32 0 -2 -8 144.236 47.4441 26 0 -2 -8 167.724 56.2775 34 0 -2 -9 214.775 51.6104 29 0 2 -9 218.391 53.5683 29 0 -2 -9 209.908 45.1049 15 0 2 -9 160.508 55.2471 15 0 2 -9 201.803 55.7436 5 0 -2 -9 157.687 55.2002 5 0 -2 -9 118.449 37.5518 26 0 2 -9 185.838 45.7792 26 0 -2 -9 207.731 45.7664 12 0 2 -9 215.546 51.5405 12 0 -2 -9 188.724 35.3545 32 0 2 -9 192.405 37.707 32 0 2 -9 200.507 48.8835 25 0 2 -10 109.92 40.6476 15 0 2 -10 43.1659 30.3628 26 0 -2 -10 111.152 38.6834 29 0 2 -10 74.0524 38.9484 29 0 3 0 20.0007 24.2912 7 0 -3 0 22.2054 30.7215 41 0 3 0 39.0263 30.1868 37 0 -3 -1 79879.8 3285.49 40 0 -3 -1 80650 3288.86 6 0 -3 1 80533.1 3293.13 6 0 -3 -1 79270.4 3287.71 1 0 3 -1 76596.5 3287.76 1 0 3 -1 80172.1 3292.9 7 0 3 -2 949.867 68.9592 37 0 -3 2 796.333 61.4912 6 0 3 -2 757.776 68.9983 7 0 -3 -2 815.762 48.0558 39 0 3 -2 798.242 65.1434 1 0 -3 -2 838.489 63.3051 1 0 -3 2 696.938 66.5612 41 0 3 -3 14133 574.814 37 0 -3 3 12853.7 565.679 6 0 -3 -3 12443.4 553.751 39 0 3 -3 14673.4 579.269 1 0 -3 -3 14046.4 576.223 1 0 -3 3 14094.8 576.73 41 0 3 3 13098.1 561.396 41 0 3 -4 20923.4 842.846 37 0 3 4 19815.6 829.848 41 0 -3 4 20097.4 844.886 41 0 3 4 18829.4 823.638 38 0 3 -4 20559.2 847.383 7 0 -3 4 18242.4 826.743 6 0 -3 -4 19210.8 847.141 1 0 3 -4 20248.1 850.662 1 0 3 -5 -64.6105 74.164 1 0 -3 -5 -20.9211 74.1948 1 0 -3 5 66.7826 63.4754 41 0 3 5 8.19309 43.209 41 0 -3 -6 375.935 39.0805 29 0 3 -6 312.509 40.3421 12 0 3 -6 293.099 40.6311 5 0 -3 -6 294.924 39.3887 5 0 -3 -6 342.332 39.0863 25 0 3 -6 137.406 86.7047 1 0 -3 -6 213.892 90.5809 1 0 -3 -6 303.641 36.3704 20 0 -3 6 444.876 82.7048 41 0 3 -6 279.221 41.9791 3 0 -3 -6 348.895 43.8633 3 0 -3 -6 347.988 41.1283 35 0 -3 -6 402.957 36.6202 33 0 -3 -6 391.054 38.9058 34 0 -3 -7 74.4346 49.9736 30 0 -3 -7 35.5946 48.041 32 0 -3 -7 166.754 61.0721 15 0 3 -7 136.11 62.7452 5 0 -3 -7 110.529 61.7794 5 0 -3 -7 95.9287 57.5245 29 0 -3 -7 67.2685 50.692 26 0 3 -7 162.648 64.8156 12 0 -3 -7 125.325 59.7974 12 0 -3 -7 64.5457 58.0978 25 0 3 -7 172.128 57.3062 25 0 -3 -7 132.179 48.0149 24 0 3 -7 30.6825 64.6578 11 0 -3 -7 138.325 52.4655 20 0 3 -7 56.7334 47.453 3 0 -3 -7 59.9668 47.3718 3 0 -3 7 116.822 64.7051 2 0 3 7 7.33464 68.3903 2 0 -3 7 25.5627 81.1741 41 0 -3 -7 130.055 56.5336 34 0 3 -7 52.2983 57.0827 34 0 -3 -8 123.472 51.6078 20 0 -3 -8 23.2484 41.7884 32 0 -3 -8 94.0304 52.9562 15 0 -3 -8 -24.0473 65.9772 5 0 3 -8 -20.9561 67.1464 5 0 -3 -8 74.9979 59.4064 34 0 -3 -8 56.1609 44.434 26 0 3 -8 87.4068 64.5748 12 0 -3 -8 136.487 57.1036 12 0 -3 -8 68.1784 60.2124 29 0 3 -8 95.9686 64.8092 29 0 -3 -8 63.5718 64.2233 25 0 -3 -8 144.255 43.3926 24 0 3 -8 48.0441 56.3557 25 0 3 -9 75.3729 36.8337 32 0 -3 -9 100.796 32.7496 32 0 -3 9 36.2268 41.3525 27 0 -3 -9 50.8596 32.8779 26 0 3 -9 118.039 49.2998 12 0 3 -9 54.0607 44.1055 25 0 -3 -9 99.6198 38.631 15 0 3 -9 146.059 55.2538 15 0 3 -9 85.7834 49.3166 29 0 -3 -9 69.3256 47.508 29 0 -3 -9 60.1387 51.7309 5 0 3 -9 -7.18842 51.6193 5 0 -3 -10 339.511 38.6025 29 0 3 -10 240.661 41.076 29 0 3 -10 315.465 44.4784 15 0 3 -10 294.478 33.9125 26 0 -4 0 26621.9 1104.46 41 0 4 0 26071.6 1100.14 7 0 4 0 26711 1105.25 37 0 -4 1 288305 11593.7 6 0 4 -1 284606 11591.8 7 0 -4 -1 293149 11589.1 6 0 -4 -1 286295 11584 40 0 -4 -1 263250 11583.5 1 0 4 -1 278415 11584.4 1 0 -4 -2 281.118 47.0754 1 0 4 -2 354.501 48.2775 1 0 4 -2 261.904 58.7341 7 0 -4 2 267.284 53.4709 6 0 -4 -2 310.663 33.8661 6 0 -4 -2 316.271 30.5519 40 0 4 -2 369.959 55.2412 37 0 -4 3 19717.8 829.225 41 0 -4 -3 19282.7 825.594 1 0 4 -3 19459.7 827.111 1 0 -4 3 18676.3 820.396 6 0 4 -3 19460.2 827.062 37 0 4 4 11922.2 521.729 41 0 -4 4 11753.2 540.26 41 0 -4 -4 12504.5 543.381 1 0 4 -4 13115.5 547.672 1 0 4 -4 12350.5 544.409 7 0 -4 4 11434.2 525.676 6 0 4 -4 12221.2 537.615 37 0 4 -5 6593.23 322.598 37 0 4 -5 7076.23 340.822 1 0 -4 -5 6590.27 334.102 1 0 -4 5 6592.56 330.196 41 0 -4 -6 3821.4 170.855 33 0 -4 -6 3499.49 167.904 32 0 -4 -6 3969.33 168.991 30 0 4 -6 3554.92 172.509 13 0 -4 -6 3805.3 170.303 5 0 4 -6 4072 171.448 5 0 -4 -6 3926.8 169.979 29 0 -4 -6 3464.26 167.683 26 0 4 -6 4146.29 174.522 12 0 -4 -6 3831.93 171.955 12 0 -4 -6 3899 168.778 24 0 4 -6 3690.22 168.713 25 0 -4 -6 4030.76 170.722 25 0 4 -6 3679.56 175.253 11 0 -4 -6 3702.75 168.748 21 0 -4 -6 3955.95 170.062 20 0 -4 -6 3843.82 172.809 35 0 4 -6 3273.37 174.165 3 0 -4 -6 3458.13 173.982 3 0 -4 -6 3620.14 235.308 1 0 4 -6 3968.04 239.629 1 0 -4 6 3516.33 222.487 41 0 -4 -7 2188.44 109.379 29 0 4 -7 1790.89 111.332 13 0 -4 -7 1818.09 104.625 15 0 -4 -7 1963.84 110.461 5 0 4 -7 2014.51 110.944 5 0 4 -7 1961.05 105.723 25 0 -4 -7 2022.56 102.871 26 0 4 -7 2208.53 114.867 12 0 -4 -7 1989.89 110.127 12 0 4 -7 1900.08 117.715 11 0 -4 -7 2057.78 108.93 25 0 -4 -7 2140.4 103.821 24 0 -4 7 1588.2 146.756 41 0 -4 -7 2090.24 103.798 30 0 -4 -7 1891.35 107.525 34 0 -4 -7 1974.6 102.831 32 0 -4 -7 1938.56 108.404 33 0 4 -7 1653.75 106.809 3 0 4 7 1744.57 140.658 2 0 -4 7 1473.4 134.233 2 0 -4 -7 1782.27 106.512 3 0 -4 -7 2180.15 107.493 20 0 -4 -8 110.848 59.8016 20 0 -4 -8 50.0352 68.7484 34 0 -4 -8 76.5175 46.1265 30 0 -4 -8 13.1977 41.476 32 0 -4 -8 75.4561 42.3541 26 0 4 -8 80.8461 70.2946 12 0 -4 -8 74.9321 55.1874 12 0 -4 -8 94.489 47.6494 15 0 4 -8 95.7459 69.8663 29 0 -4 -8 105.876 62.8619 29 0 4 -8 -52.171 67.5297 5 0 -4 -8 35.1106 66.9243 5 0 -4 -8 29.495 46.8712 24 0 4 -8 83.3178 53.8267 25 0 -4 -8 90.8508 70.2233 25 0 -4 -9 1320.7 75.1882 34 0 -4 9 1111.49 73.8488 27 0 -4 -9 1348.42 76.8797 25 0 4 -9 1071.38 76.4497 12 0 -4 -9 1341.79 73.8778 29 0 4 -9 1421.19 76.0431 29 0 4 -9 1335.73 76.1513 5 0 -4 -9 1368.12 76.6362 5 0 -4 -9 1205.49 64.8186 24 0 4 -9 1017.31 67.8587 32 0 4 -10 268.566 47.7363 15 0 4 -10 274.766 36.3792 26 0 -4 -10 354.568 35.4704 29 0 4 -10 349.425 41.0616 29 0 5 0 61.4259 44.3119 37 0 -5 0 27.936 45.9216 6 0 5 0 54.4601 33.9999 7 0 -5 0 84.0054 44.8766 41 0 -5 1 903.916 70.7271 41 0 5 1 859.509 43.1954 2 0 -5 1 739.671 42.2379 2 0 5 1 1067.84 68.7239 37 0 -5 -1 948.088 64.4621 6 0 5 -1 1187.44 71.4971 7 0 -5 1 1020.52 75.1283 6 0 -5 -1 932.689 52.6681 40 0 -5 -2 7690.79 343.542 1 0 5 -2 7710.1 344.655 1 0 5 -2 7747.53 352.143 37 0 -5 2 8233.5 353.46 6 0 5 -2 8138.4 355.877 7 0 -5 -2 8168.15 340.847 6 0 -5 -2 7655.64 335.059 40 0 -5 3 17286 756.904 41 0 5 -3 17684.9 755.856 37 0 5 -3 17570.4 760.063 7 0 -5 3 16998.7 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134.942 51.77 30 -3 -4 -8 73.8139 55.7703 34 3 -4 8 29.1192 70.3372 22 -3 -4 -8 59.8482 57.5926 29 -3 -4 -8 91.3875 51.8552 24 -3 4 -8 79.222 56.9048 25 -3 -4 -9 1093.86 58.1629 20 -3 -4 -9 1046.34 64.9112 34 -3 4 -9 907.973 56.0135 25 -3 4 -9 1048.86 66.3998 5 -3 -4 -9 1058.84 66.703 5 -3 4 -9 1085.62 72.6812 29 -3 -4 -9 914.533 56.9894 29 -3 -4 -9 1046.89 57.1519 24 3 5 -10 204.158 39.4069 15 3 5 -10 228.254 31.9205 26 3 5 -10 192.419 30.182 32 3 5 -10 197.114 38.3356 12 3 -5 -10 178.56 34.0846 29 3 -5 -9 3335.26 156.774 26 3 5 -9 3609.05 160.247 26 3 5 -9 3531.47 162.918 15 3 -5 -9 3550.06 159.633 29 3 5 -9 3414.93 159.106 32 3 -5 -9 3437.73 157.418 32 3 5 -9 3595.96 155.758 29 3 5 -8 108.064 58.3985 3 3 -5 -8 39.5504 59.5215 3 3 -5 -8 41.4087 55.1102 19 -3 -5 8 177.086 64.2461 27 3 -5 -8 95.9904 65.7805 26 3 5 -8 25.8844 80.5766 13 3 5 -8 45.9486 82.1555 12 3 -5 -8 96.3543 82.5612 12 3 -5 -8 15.3193 73.2397 29 3 5 -8 -8.05729 64.127 29 3 5 -8 -61.054 82.2369 15 3 -5 -8 83.8896 64.9108 15 3 -5 -8 -21.6503 72.0833 25 3 -5 -8 -12.3204 65.6412 32 3 5 -7 2017.58 104.729 29 3 -5 -7 1855.75 109.227 29 3 -5 -7 1968.12 107.588 15 3 5 -7 1944.63 119.413 13 3 -5 -7 2013.58 107.301 25 -3 -5 7 1935.46 111.64 27 3 -5 -7 1981.05 106.19 26 3 -5 -7 2121.72 104.199 24 3 -5 -7 1890.89 116.555 12 3 5 -7 1985.05 116.056 12 3 5 -7 1916.79 105.147 3 3 -5 -7 1805.11 104.386 3 3 -5 -7 1937.95 106.415 32 3 -5 -7 1868.69 106.744 19 3 5 -7 1998.42 112.234 18 3 -5 -7 1985.29 109.109 34 3 -5 -7 2014.49 109.962 20 3 -5 -7 1843.23 99.9449 21 3 5 -7 1899.18 109.685 5 3 -5 -7 1905.68 107.788 5 3 -5 -6 3818.41 191.932 34 3 -5 -6 3435.9 189.764 35 3 -5 -6 3938.29 182.501 32 3 -5 -6 3761.51 186.014 30 3 -5 -6 3554.45 203.61 15 3 5 -6 3746.63 220.345 13 3 -5 -6 3787.82 205.116 25 3 5 -6 3576.47 210.809 25 -3 -5 6 3814.04 232.368 27 3 -5 -6 3802.67 190.509 26 3 -5 -6 3717.64 193.627 24 3 5 -6 3292.93 172.157 3 3 -5 -6 3732.76 173.736 3 3 -5 -6 3702.55 183.413 20 3 -5 -6 3899.85 174.767 21 3 -5 -6 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247.448 31.2735 32 3 -9 -8 85.1534 42.9883 32 3 9 -8 119.109 46.5918 18 3 -9 -8 55.5765 37.323 19 3 -9 -8 69.9458 38.0412 29 3 9 -8 60.9162 60.6048 13 3 9 -8 85.7343 57.0442 12 3 -9 -8 123.197 34.1978 26 -3 -9 8 166.494 55.0873 27 3 9 -8 68.3669 45.7656 15 3 9 -7 1668.54 104.914 15 3 9 -7 1802.92 134.192 13 3 -9 -7 1782.86 107.309 24 3 9 -7 1607.83 119.818 12 3 -9 -7 1622.39 95.9214 26 -3 -9 7 1717.99 127.352 27 -3 -9 7 1602.5 100.233 22 3 -9 -7 1680.16 105.494 32 3 -9 -7 1633.91 106.377 19 3 9 -7 1514.15 118.164 18 3 -9 -7 1677.83 96.637 34 3 -9 -7 1702.07 96.9178 29 3 -9 -7 1937.85 102.509 21 3 -9 -7 1703.12 107.42 20 3 -9 -6 665.456 59.63 29 3 -9 -6 516.276 57.5436 26 -3 -9 6 559.991 81.95 27 3 9 -6 795.043 79.2484 12 3 -9 -6 607.472 62.1353 21 3 -9 -6 622.526 64.5807 20 3 -9 -6 686.636 67.5659 24 -3 -9 6 684.109 74.1564 22 3 -9 -6 555.801 57.1181 16 3 -9 -6 664.092 64.5434 35 3 -9 -6 593.708 56.5201 34 3 -9 -6 625.566 66.4633 19 3 9 -6 600.917 79.2309 18 3 -9 -6 735.693 64.7968 32 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75.9848 41 -3 -9 -4 9930.9 409.312 28 3 -9 4 8417.72 448.006 6 -3 -9 -4 9555.48 405.843 24 -3 -9 -4 8963.46 404.59 23 -3 -9 -4 9260.42 408.811 8 -3 9 -4 9577.89 420.141 11 -3 -9 -4 9552.69 409.584 10 -3 -9 -4 9292.35 407.194 21 -3 -9 -4 9758.63 406.561 20 -3 -9 -4 10020.6 410.468 30 3 -9 4 9963.55 483.036 41 -3 9 -4 9298.9 411.301 17 -3 -9 -4 9757.47 406.59 34 -3 -9 -4 10091.4 411.249 35 -3 9 -5 2141.33 130.482 13 -3 -9 -5 2399.63 122.132 28 -3 9 -5 2333.24 133.799 17 -3 9 -5 2316.15 127.029 12 -3 -9 -5 2596.67 121.517 34 -3 -9 -5 2461.55 124.01 35 -3 -9 -5 2312.68 120 24 -3 -9 -5 2350.34 137.078 25 3 -9 5 2431.77 136.178 22 -3 -9 -5 2102.63 119.746 21 -3 -9 -5 2496.58 121.49 20 3 -9 5 1915.02 162.786 40 3 -9 5 1945.04 179.354 41 -3 9 -5 2550.9 131.983 18 -3 9 -5 2088.5 165.816 37 -3 9 -5 2310.93 132.749 11 -3 -9 -5 2306.51 117.361 10 3 -9 6 590.724 84.8033 22 -3 -9 -6 627.502 66.2778 35 -3 -9 -6 719.919 67.4704 20 -3 -9 -6 532.524 65.6758 21 -3 -9 -6 645.597 67.7743 33 -3 -9 -6 708.638 65.3269 34 -3 9 -6 638.689 74.1967 13 -3 9 -6 645.767 68.0221 12 -3 -9 -6 724.76 67.5797 30 -3 -9 -6 689.434 66.8159 24 -3 -9 -6 781.344 59.674 25 -3 9 -6 615.285 63.6644 18 -3 9 -6 532.408 76.8252 17 -3 -9 -6 637.711 60.6143 28 -3 -9 -7 194.952 54.8324 33 -3 -9 -7 220.97 55.318 34 -3 -9 -7 313.574 56.4112 30 -3 -9 -7 266.506 56.0996 35 3 -9 7 199.173 71.2145 22 -3 9 -7 286.697 73.8583 11 -3 9 -7 152.641 59.5957 12 -3 9 -7 193.434 64.4637 13 -3 -9 -7 255.867 54.5469 25 -3 -9 -7 216.535 52.0911 28 3 -9 8 43.9677 54.3297 22 -3 9 -8 28.841 39.1163 29 -3 -9 -8 26.71 46.9674 20 -3 9 -8 34.262 38.4485 12 -3 -9 -8 33.1661 44.3903 24 -3 -9 -8 28.4207 33.6839 25 -3 -9 -8 4.72644 44.2791 34 -3 -9 -8 -32.1799 41.6379 30 3 -9 9 310.385 43.1832 27 -3 9 -9 268.541 36.134 15 3 10 -9 405.793 42.6027 12 3 10 -8 91.5345 64.7649 13 3 10 -8 60.071 55.1184 12 -3 -10 8 84.9017 55.2664 27 3 10 -8 111.968 45.8292 18 3 -10 -8 47.3582 35.7165 19 3 -10 -8 86.9746 40.7861 32 3 10 -8 98.5439 38.4289 15 -3 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10 -2 651.633 87.249 37 -3 -10 2 883.615 85.6391 41 3 10 -2 841.495 85.638 7 3 -10 -2 919.974 76.5764 40 3 10 -1 1281 109.974 37 -3 10 1 1196 100.038 37 -3 -10 1 1283.94 90.2998 41 3 -10 -1 1313.16 107.206 6 -3 -10 1 1433.12 111.732 6 3 10 -1 1100.92 90.8906 7 3 -10 -1 1081.28 89.484 40 3 -10 0 10516.2 493.504 6 -3 -10 0 10242.5 485.36 6 3 10 0 11228.9 492.082 37 -3 10 0 10611.7 488.936 37 3 -10 0 10459.4 481.203 40 -3 -10 -1 650.088 74.9788 6 3 -10 1 775.508 96.5582 6 -3 10 -1 708.672 88.4835 37 3 -10 1 652.967 80.1948 40 3 -10 2 1945.38 136.979 40 -3 10 -2 1834.22 114.635 38 -3 -10 -2 1960.29 98.6851 8 3 10 2 2066.78 139.084 37 -3 10 -2 2074.13 147.134 37 3 -10 2 1920.57 145.593 6 -3 -10 -3 6658.27 297.635 10 -3 10 -3 6726.65 299.627 11 -3 -10 -3 6427.76 297.904 8 3 -10 3 6755.6 300.154 22 3 -10 3 6408.23 345.388 6 -3 -10 -3 6976.83 294.478 30 -3 10 -3 6895.97 300.886 13 -3 -10 -3 7381.71 297.597 35 -3 -10 -3 7069.76 296.783 28 3 10 3 7045.44 344.488 37 -3 10 -3 5655.81 341.731 37 -3 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40.8027 25 3 -10 6 -2.43951 82.8 22 -3 10 -6 12.0235 79.5777 11 -3 -10 -6 82.8605 57.222 35 -3 -10 -6 98.8755 58.2288 33 -3 -10 -6 78.6746 54.4821 34 -3 10 -6 73.2452 54.3604 18 -3 -10 -6 -30.4097 59.5905 21 -3 -10 -6 33.3883 59.5079 20 -3 -10 -7 1383.54 79.0344 25 3 -10 7 1636.25 102.394 22 -3 -10 -7 1611.18 88.9564 20 -3 -10 -7 1626.7 88.6958 30 -3 10 -7 1596.97 94.8516 13 -3 -10 -7 1651.42 86.5536 34 -3 -10 -7 1767.17 88.9246 35 3 -10 7 1614.95 102.638 27 -3 -10 -7 1439.58 81.9369 28 -3 -10 -7 1530.3 88.6528 33 -3 10 -7 1464.43 89.7308 12 3 -10 8 1031.1 90.9827 22 -3 -10 -8 1111.42 74.9568 30 -3 10 -8 735.554 57.586 29 -3 10 -8 940.371 68.5655 13 -3 -10 -8 1006.73 73.6175 34 -3 10 -8 810.483 63.1761 12 3 -11 -8 348.751 50.0917 19 -3 -11 8 433.559 86.9448 27 3 -11 -8 378.9 59.9941 32 3 11 -8 511.72 99.2057 13 3 11 -8 381.012 85.1852 12 3 -11 -7 5246.28 225.283 32 -3 -11 7 4699.16 227.327 22 3 -11 -7 4610.38 219.996 26 -3 -11 7 5597.77 236.046 27 3 -11 -7 5455.92 224.595 21 3 11 -7 4906.53 232.665 18 3 -11 -7 5222.31 225.754 19 3 11 -7 5456.76 231.235 12 3 11 -6 604.832 105.699 13 3 11 -6 589.992 86.3551 12 3 -11 -6 563.359 54.5063 26 -3 -11 6 665.369 100.757 27 -3 -11 6 621.816 82.5742 22 3 -11 -6 543.892 50.9528 23 3 -11 -6 748.441 71.8033 21 3 -11 -6 664.079 65.6801 35 3 -11 -6 674.241 71.7053 32 3 -11 -6 681.501 58.907 16 3 11 -6 562.436 97.4102 18 3 -11 -6 620.041 74.0069 19 3 -11 -5 672.932 57.6918 26 -3 -11 5 650.682 82.7465 27 3 11 -5 530.444 85.4989 13 3 11 -5 693.959 73.0126 12 3 -11 -5 574.703 64.9623 19 3 -11 -5 549.69 64.9797 24 3 -11 -5 528.885 58.2638 23 -3 -11 5 547.248 78.7858 22 3 -11 -5 659.957 58.1735 20 3 -11 -5 619.525 64.0496 21 3 -11 -5 547.989 62.9688 32 3 -11 -5 608.299 61.869 35 3 -11 -5 657.159 64.0101 30 3 -11 -5 635.457 53.4762 14 3 -11 -5 665.976 61.6126 16 3 -11 -4 1981.93 136.156 35 3 -11 -4 2088.07 115.246 36 3 -11 -4 2177.18 117.693 32 3 -11 -4 2337.59 136.301 30 3 11 -4 1686.93 163.433 7 -3 -11 4 2045.5 172.227 6 -3 -11 4 1810.06 153.913 41 3 -11 -4 2321.38 131.026 14 3 11 -4 2002.7 142.901 13 3 -11 -4 2024.77 131.82 26 3 -11 -4 2006.27 119.559 24 3 11 -4 2308.45 140.848 12 3 -11 -4 2242.98 121.862 23 -3 -11 4 2109.37 132.885 22 -3 11 4 1877.77 155.682 38 3 -11 -4 2011.45 108.47 20 3 -11 -4 2223.65 121.227 16 3 11 -4 2016.99 152.245 37 3 11 -4 2126.98 131.924 18 3 -11 -3 3962.21 178.302 26 -3 -11 3 4452.92 237.754 27 3 -11 -3 3963.32 180.278 36 3 -11 -3 4015.15 177.892 35 -3 -11 3 4036 259.523 22 3 -11 -3 4108.89 215.347 23 -3 11 3 3882.31 236.378 38 3 11 -3 3792.39 187.51 13 3 -11 -3 4099.48 184.429 14 -3 -11 3 3488.69 220.35 41 3 -11 -3 3728.92 174.617 30 3 -11 -3 4372.68 223.023 16 3 11 -3 3738.57 231.452 7 -3 -11 3 3996.15 244.069 6 3 -11 -3 4578.08 229.589 19 3 11 -3 4505.89 244.179 18 3 11 -3 3898.69 236.412 37 3 -11 -2 8647.14 354.781 16 3 11 -2 7860.35 398.393 37 -3 11 2 7587.57 387.68 37 3 -11 -2 7564.18 378.402 40 3 -11 -2 8470.87 352.2 21 3 -11 -2 8379.74 352.809 23 -3 -11 2 7725.32 387.249 41 3 11 -2 7369.3 386.584 7 3 -11 -1 179.391 55.1934 40 3 11 -1 144.818 68.3861 37 -3 11 1 65.3814 55.7313 37 -3 -11 1 230.405 35.8354 8 3 -11 0 3184.94 185.925 40 3 11 0 3759.63 204.192 37 -3 11 0 3416.82 197.45 37 -3 -11 0 3168.9 155.076 8 3 -11 0 3535.77 204.471 6 -3 -11 0 3624.19 196.671 6 3 -11 1 5295.36 286.346 6 -3 -11 -1 5317.23 267.649 6 -3 11 -1 5307.55 265.802 38 3 -11 1 5232.5 273.26 40 -3 11 -1 5299.26 281.576 37 -3 11 -2 16.7146 72.162 37 3 11 2 29.5037 71.2697 37 -3 11 -2 104.009 36.6564 13 -3 -11 -2 86.1023 29.6747 23 3 -11 2 83.5405 81.257 6 3 -11 2 59.3121 70.8884 40 -3 -11 -2 86.7323 35.2293 35 -3 -11 -2 81.1919 28.763 31 -3 -11 -2 105.038 39.779 8 -3 -11 -3 108.105 97.6506 35 -3 -11 -3 67.8208 34.0153 34 -3 -11 -3 23.4554 118.26 30 -3 -11 -3 180.695 115.402 31 3 -11 3 156.089 92.8383 6 -3 11 -3 126.061 78.7288 37 3 11 3 -46.6944 69.7687 37 -3 -11 -3 52.4124 90.5497 28 3 -11 3 75.3902 44.1381 27 -3 11 -3 112.596 108.229 13 -3 -11 -3 53.6319 31.776 24 -3 -11 -3 59.4844 114.933 23 3 -11 3 173.963 131.447 22 -3 11 -3 406.033 164.136 11 -3 -11 -3 92.3239 44.7237 8 3 -11 3 58.3721 71.3614 40 -3 -11 -3 76.9822 32.8676 16 -3 -11 -3 92.0934 47.4663 20 -3 -11 -3 143.564 101.569 21 3 -11 4 -45.3749 75.4993 40 3 11 4 -25.0842 70.8512 37 -3 -11 -4 -19.9584 57.5275 35 -3 -11 -4 -21.1484 54.9836 30 3 -11 4 -118.748 89.7271 6 -3 -11 -4 50.2236 53.5349 28 -3 -11 -4 57.5262 56.5261 34 3 -11 4 67.3138 62.0832 27 -3 11 -4 -9.65903 66.969 13 -3 -11 -4 43.3919 48.6841 24 -3 -11 -4 79.6655 49.8329 23 3 -11 4 11.9012 69.1036 22 -3 11 -4 -11.9192 68.0835 11 -3 -11 -4 93.693 51.6715 20 -3 -11 -4 -36.5872 50.1893 21 -3 11 -4 70.9108 68.2679 18 -3 -11 -4 -9.96544 37.1852 8 -3 -11 -4 7.77669 58.4476 19 3 -11 5 94.4874 62.203 27 -3 11 -5 114.624 62.5806 12 -3 -11 -5 161.861 57.1082 30 -3 -11 -5 4.1949 46.9996 24 -3 -11 -5 53.2151 54.7506 35 -3 11 -5 -2.46575 72.93 11 -3 -11 -5 15.7762 47.9539 34 -3 -11 -5 92.0869 55.102 33 -3 11 -5 36.0398 56.0585 17 -3 11 -5 84.0144 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405.179 37 -4 7 0 8886.56 399.839 37 4 -7 0 9125.99 411.758 6 -4 -7 0 9642.62 407.205 6 4 -7 1 8292.7 371.502 6 -4 -7 -1 8336.26 355.49 6 -4 7 -1 8113.15 363.388 37 4 7 1 7665.1 345.064 7 4 7 1 7251.63 343.487 2 4 -7 1 7562.17 343.948 2 -4 -7 -1 8293.81 364.617 39 -4 7 -1 7709.62 350.766 38 -4 7 -2 16012 693.154 37 -4 -7 -2 16055.7 686.598 39 4 -7 2 16958.4 693.591 40 -4 7 -2 15058.6 668.72 38 4 -7 2 16191.2 693.038 6 -4 -7 -2 15431.9 668.787 6 4 7 2 14958.2 671.709 2 4 -7 2 15660.9 672.293 2 4 -7 3 9564.29 445.858 41 -4 7 -3 8704.84 435.156 37 4 -7 3 9811.08 435.87 40 -4 -7 -3 9016.54 422.521 39 4 7 3 9627.37 417.584 2 4 -7 3 8915.21 414.347 2 4 -7 3 9245.92 430.93 6 4 -7 4 20152.2 852.192 40 -4 -7 -4 19548.3 805.342 10 4 -7 4 18701.8 830.479 2 -4 7 -4 18578.6 853.357 37 4 -7 4 19246.7 859.733 41 -4 -7 -4 18800 804.234 8 4 -7 5 5325.22 293.836 40 4 -7 5 4553.23 280.234 2 -4 -7 -5 5751.03 253.801 35 -4 -7 -5 5588.54 253.26 34 -4 -7 -5 5747.67 253.768 30 -4 7 -5 5455.72 258.381 13 -4 -7 -5 5827.28 252.524 28 -4 7 -5 5454.61 271.315 12 -4 -7 -5 5653.14 255.33 33 -4 -7 -5 5513.64 252.161 25 -4 -7 -5 5825.09 253.66 24 4 -7 5 5624.18 269.186 22 -4 -7 -5 5574.1 251.86 21 -4 7 -5 5298.32 268.502 18 -4 7 -5 5377.93 260.875 17 -4 7 -5 5395.07 261.367 11 -4 -7 -5 5765.25 247.884 10 4 -7 5 5489.66 309.7 41 -4 -7 -6 8458.11 354.657 30 -4 7 -6 8119.23 358.953 13 -4 7 -6 7462.48 354.023 12 -4 -7 -6 8213.67 352.52 5 -4 -7 -6 7980.59 356.265 28 -4 -7 -6 8541.72 355.384 25 4 -7 6 8576.9 366.177 22 -4 -7 -6 7558.58 352.299 10 -4 7 -6 8202.37 363.117 11 -4 -7 -6 8465.63 355.474 20 -4 7 -6 8467.73 365.002 17 -4 -7 -6 8481.4 357.296 33 -4 -7 -6 8464.42 354.728 35 -4 -7 -7 1251.24 95.3433 24 -4 -7 -7 1324.57 92.9835 25 -4 -7 -7 1215.16 76.3338 5 -4 7 -7 1212.72 76.5811 5 4 -7 7 1214.32 113.888 22 -4 7 -7 1197.91 108.793 11 -4 7 -7 949.675 76.0943 12 -4 -7 -7 1380.06 89.5825 30 -4 7 -7 1277.07 83.4433 13 -4 7 -7 1271.13 116.1 17 -4 -7 -7 1355.3 95.4658 20 -4 -7 -7 1227.17 86.0071 28 4 -7 8 1647.1 96.9897 22 -4 -7 -8 1666.44 87.0377 25 -4 -7 -8 1727.96 87.3322 24 -4 7 -8 1435.6 91.8236 11 -4 -7 -8 1758.53 89.6273 34 -4 -7 -8 1554.13 83.4485 30 -4 -7 -8 1718.86 87.8451 20 -4 7 -9 46.9563 38.9341 29 -4 -7 -9 136.654 33.2401 25 -4 -7 -9 107.69 33.6009 24 -4 -7 -9 112.389 38.6526 34 -4 -7 -9 123.229 32.9753 20 4 -7 9 149.433 56.1523 27 4 -8 -9 373.978 45.7991 29 4 8 -9 311.339 44.9253 32 4 8 -9 312.846 41.9067 26 4 8 -9 389.854 48.281 15 4 8 -9 326.262 51.7261 12 4 -8 -9 291.425 43.8245 32 4 -8 -8 2972.21 136.847 19 4 8 -8 2582.42 140.449 18 4 8 -8 2604.99 148.448 13 4 8 -8 2912.57 138.628 15 4 -8 -8 3104.02 137.558 29 -4 -8 8 2920.18 141.214 27 4 -8 -8 2945.13 135.965 26 4 -8 -8 3155.27 139.346 32 4 8 -8 2882.58 144.301 12 4 -8 -7 60.8593 67.896 32 4 8 -7 51.993 72.3915 18 4 -8 -7 -8.94712 64.8103 19 -4 -8 7 96.2513 72.5963 27 4 -8 -7 61.6916 55.7215 26 4 -8 -7 58.6416 46.1154 21 4 8 -7 12.0292 81.1165 12 4 8 -7 -47.613 95.1979 13 4 8 -7 31.3435 60.5698 15 4 -8 -7 27.4323 41.2608 16 4 -8 -7 5.97206 58.2029 29 4 -8 -6 1651.38 90.0569 24 4 8 -6 1307.3 94.3325 12 4 -8 -6 1424.59 87.7994 29 4 -8 -6 1457.37 92.2764 19 4 8 -6 1134.5 101.881 18 4 -8 -6 1444.51 82.9108 34 4 -8 -6 1241.22 85.3155 35 4 -8 -6 1271.06 85.1354 16 4 -8 -6 1437.72 89.7734 20 4 -8 -6 1489.75 83.8068 21 -4 -8 6 1413.21 101.01 27 4 -8 -6 1315.91 85.3059 26 4 -8 -5 1458.24 100.055 30 4 -8 -5 1451.27 107.134 29 -4 -8 5 1144.34 123.104 6 4 8 -5 1467.03 142.95 7 4 8 -5 1599 123.078 18 -4 -8 5 1666.83 116.525 27 4 -8 -5 1600.75 97.0045 26 4 8 -5 1314.01 105.352 12 4 -8 -5 1547.51 101.707 24 4 -8 -5 1613.48 129.957 23 -4 -8 5 1472.2 158.018 22 4 -8 -5 1689.83 101.889 21 4 -8 -5 1261.58 99.873 20 -4 8 5 1375.28 118.22 41 -4 -8 5 1442.86 129.769 41 4 -8 -5 1517.76 108.549 34 4 -8 -5 1330.56 121.022 35 -4 8 5 1092.52 114.687 38 4 -8 -5 1479 105.214 16 4 -8 -5 1384.89 106.327 14 4 8 -5 1506.4 129.369 13 -4 -8 4 271.634 75.8548 6 4 8 -4 141.902 84.092 7 -4 -8 4 176.791 68.752 41 -4 8 4 209.749 67.9851 38 4 8 -4 58.1536 47.1606 37 4 8 -3 24200 1009.37 7 -4 -8 3 23476.1 1009.27 6 -4 -8 3 22263.9 996.83 41 4 -8 -3 22649.9 994.709 40 -4 8 3 23918.7 1003.05 38 4 8 -3 22396.2 995.251 37 4 8 -2 4385.65 232.98 7 -4 -8 2 4988.8 244.729 6 -4 -8 2 4404.63 223.024 41 -4 8 2 4846.88 236.222 38 4 -8 -2 4673.14 228.239 40 4 8 -2 4509.25 229.059 37 -4 8 2 4152.61 216.81 37 -4 -8 1 448.834 73.8133 6 4 8 -1 344.635 59.6483 7 -4 -8 1 358.308 46.0129 41 -4 8 1 370.087 55.7298 37 -4 8 1 304.864 64.6333 38 4 8 -1 282.1 59.3412 37 4 -8 -1 361.419 60.5556 40 4 8 0 9099.34 437.873 7 4 8 0 10432.2 454.778 37 -4 8 0 9778.06 449.623 37 -4 -8 0 10278.8 452.957 6 4 -8 0 10075.6 451.242 40 -4 8 0 10461.7 448.753 38 4 8 1 1393.41 108.171 37 -4 8 -1 1092.46 98.5496 37 4 -8 1 1236.3 114.209 6 -4 -8 -1 1215.59 90.3734 6 -4 8 -1 1317.26 90.2065 38 -4 8 -2 12919.8 584.746 37 4 -8 2 12605.7 584.55 6 -4 -8 -2 12877.1 560.564 6 4 -8 2 13849.6 585.578 40 -4 8 -2 12599.3 559.78 38 -4 -8 -3 4934.96 221.309 10 -4 -8 -3 5105.87 221.524 8 4 -8 3 5081.95 265.761 40 -4 8 -3 4832.52 265.033 37 4 -8 3 4815 260.236 6 -4 -8 -4 348.921 38.2653 35 -4 -8 -4 318.866 38.8916 33 -4 -8 -4 313.477 37.3257 34 -4 8 -4 191.143 96.8768 37 -4 -8 -4 310.291 37.2916 28 -4 8 -4 255.823 40.7153 13 -4 8 -4 284.536 39.5608 12 -4 -8 -4 277.143 35.3961 24 -4 -8 -4 286.061 37.7401 8 4 -8 4 307.732 45.4962 22 -4 -8 -4 286.607 37.3272 20 -4 -8 -4 229.906 34.3104 21 -4 8 -4 236.832 41.1201 17 4 -8 4 140.679 82.7912 40 4 -8 4 240.199 106.51 41 -4 -8 -4 329.689 41.7247 10 -4 8 -4 249.569 44.5447 11 -4 8 -5 23525.4 1040.86 18 -4 -8 -5 25961.7 1037.42 33 -4 -8 -5 24727 1036.69 28 -4 8 -5 23421.3 1040.15 13 -4 -8 -5 24993.1 1035.3 30 -4 8 -5 23628 1039.37 12 -4 -8 -5 24809.3 1035.36 34 -4 -8 -5 25527.5 1036.67 35 -4 -8 -5 24228.6 1036.78 25 -4 -8 -5 26424.9 1036.18 24 4 -8 5 25309.4 1043.81 22 -4 -8 -5 23252.5 1034.58 21 -4 -8 -5 25571.4 1035.16 20 4 -8 5 23778.1 1088.92 40 -4 8 -5 24944 1042.33 17 -4 -8 -5 24518.8 1036.74 10 4 -8 5 23891.7 1103.41 41 -4 -8 -6 9283.14 391.828 25 -4 -8 -6 9450.85 392.875 30 -4 8 -6 9312.87 398.158 13 -4 8 -6 8508.67 392.57 12 4 -8 6 9697.78 404.707 22 -4 -8 -6 9257.51 392.569 35 -4 -8 -6 9627.41 393.864 34 -4 8 -6 8934.47 400.619 11 -4 -8 -6 8400.76 389.919 10 -4 -8 -6 9235.51 395.372 33 -4 8 -6 9227.01 401.823 17 -4 -8 -6 8981.91 393.521 28 4 -8 7 1919.86 119.913 22 -4 -8 -7 1953.89 104.509 20 -4 -8 -7 1827.55 104.26 28 -4 -8 -7 1953.25 102.904 30 -4 8 -7 1909.07 116.572 11 -4 -8 -7 1908.7 103.377 24 -4 -8 -7 1964.71 103.26 25 -4 8 -7 1663.76 106.397 12 -4 8 -7 1818.09 111.812 13 -4 -8 -8 92.5544 44.427 24 -4 -8 -8 72.7216 39.1533 25 -4 -8 -8 110.741 45.6573 20 -4 -8 -8 94.6419 39.242 30 -4 8 -8 8.39273 51.3897 11 4 -8 8 44.7555 55.9275 22 -4 -8 -9 283.597 34.8737 34 -4 -8 -9 231.635 31.9722 24 4 -8 9 237.893 50.4004 27 4 9 -9 167.718 31.104 26 4 -9 -9 112.394 35.6648 32 4 9 -9 210.604 41.7866 32 4 9 -9 247.438 49.6955 12 4 -9 -8 313.668 43.1117 29 4 -9 -8 221.159 39.0832 26 -4 -9 8 181.543 52.5468 27 4 -9 -8 242.852 47.5347 32 4 9 -8 311.07 52.2158 18 4 -9 -8 323.046 43.8252 19 4 9 -8 212.454 43.6983 15 4 9 -8 271.96 55.8014 12 4 9 -8 320.747 66.8903 13 4 -9 -7 70.9391 58.3163 21 4 9 -7 94.0246 84.2263 18 4 -9 -7 87.5218 64.5195 19 4 -9 -7 -51.2422 64.8834 29 4 -9 -7 -23.5149 59.9632 32 4 9 -7 3.76685 72.2433 12 4 9 -7 71.3202 88.0005 13 4 -9 -7 17.9287 59.0503 26 -4 -9 7 76.9892 79.2957 27 4 9 -7 -28.8195 66.5556 15 4 -9 -7 52.6018 50.7318 16 -4 -9 6 1971.07 119.857 27 4 -9 -6 1827.07 103.013 26 4 -9 -6 1939.03 103.267 29 4 9 -6 2066.85 114.073 12 -4 -9 6 1722.87 109.405 22 4 -9 -6 1768.84 95.6723 23 4 -9 -6 1925.29 102.265 21 4 -9 -6 1904.84 103.481 35 4 9 -6 1990.57 121.963 18 4 -9 -6 2070.74 109.935 19 4 -9 -6 1917.7 103.858 16 4 9 -6 1746.03 125.595 13 4 -9 -5 201.777 61.5307 30 4 -9 -5 133.322 62.4072 16 4 -9 -5 212.896 65.8673 14 4 -9 -5 150.675 89.7748 29 -4 -9 5 192.12 76.9002 27 4 -9 -5 309.7 62.1578 26 4 9 -5 134.831 78.2804 18 4 9 -5 283.635 83.9999 13 4 9 -5 242.355 71.6651 12 -4 -9 5 89.8066 99.4375 22 4 -9 -5 277.291 89.4237 23 4 -9 -5 250.185 62.3585 21 4 -9 -5 220.281 69.7922 20 -4 9 5 -36.2214 65.8624 38 4 -9 -5 212.934 92.7445 35 -4 -9 5 97.7574 84.2653 6 4 9 -5 272.784 101.553 7 -4 -9 5 190.436 93.7264 41 4 -9 -4 1368.62 73.2747 36 4 -9 -4 1484.43 74.7649 35 4 -9 -4 1581.64 96.0018 32 4 -9 -4 1343.48 75.2224 30 4 -9 -4 1246.08 73.5099 29 4 -9 -4 1458.37 76.4453 14 4 9 -4 1463.59 102.606 13 4 -9 -4 1376.7 75.4715 26 -4 -9 4 1707.97 117.139 27 4 -9 -4 1503.22 90.0825 24 -4 -9 4 1417.47 86.3616 22 4 -9 -4 1481.57 77.0547 23 4 -9 -4 1327.88 74.4536 20 4 -9 -4 1510.01 76.9574 21 4 -9 -4 1718.04 102.148 19 4 9 -4 1480.38 118.349 18 4 9 -4 1083.15 104.181 37 -4 9 4 1377.7 129.281 38 -4 -9 4 1286.85 124.819 41 4 9 -4 1394.07 77.7829 12 4 -9 -4 1436.11 82.7645 16 -4 -9 4 1400.51 145.147 6 4 9 -4 1633.66 167.789 7 -4 -9 3 249.607 77.4984 6 4 9 -3 187.852 68.6297 7 4 -9 -3 136.777 50.0366 40 -4 -9 3 126.981 57.5191 41 4 9 -3 199.5 58.6407 37 -4 9 3 118.889 66.0464 38 4 9 -2 2360.32 144.272 37 4 9 -2 2340.73 143.828 7 -4 -9 2 2044.5 131.737 41 4 -9 -2 2153.87 136.003 40 -4 9 2 2410.76 148.512 38 4 9 -1 3868.33 205.804 7 -4 -9 1 3882.69 217.894 6 4 9 -1 3990.55 214.455 37 -4 9 1 3928.55 207.669 37 -4 -9 1 3876.32 196.365 41 4 -9 -1 4234.98 212.244 40 -4 9 1 4522.36 217.334 38 4 9 0 9336.81 445.999 7 4 -9 0 10060 461.667 40 -4 9 0 10259.3 458.962 38 -4 -9 0 10871.3 464.855 6 4 9 0 10591.1 466.734 37 -4 9 0 9962.55 461.874 37 4 -9 1 183.247 61.3747 40 -4 -9 -1 263.641 59.1052 6 4 -9 1 133.856 71.4257 6 -4 9 -1 80.2977 61.7352 37 -4 9 -1 205.867 52.3638 38 4 9 1 238.353 66.1667 37 -4 -9 -2 4753.04 209.081 10 -4 -9 -2 4716.22 209.758 8 -4 9 -2 4560.01 225.664 38 4 -9 2 4619.21 254.343 6 -4 9 -2 4635.36 251.995 37 -4 -9 -3 9732.73 418.682 10 -4 -9 -3 9721.74 418.691 8 -4 9 -3 9416.6 465.589 37 4 -9 3 10613.7 469.239 40 4 -9 3 9529.89 462.78 6 -4 -9 -4 60.1797 70.739 33 -4 -9 -4 159.917 103.527 34 -4 -9 -4 120.853 80.2437 30 -4 -9 -4 112.739 77.5745 28 -4 -9 -4 16.2832 111.941 35 -4 9 -4 157.524 90.5591 13 -4 -9 -4 70.4695 39.1582 25 -4 -9 -4 135.748 108.192 24 -4 9 -4 -35.2513 70.9823 37 4 -9 4 72.1535 96.1374 22 -4 9 -4 196.52 94.2985 11 -4 -9 -4 145.669 43.6352 10 -4 -9 -4 33.2041 92.5873 20 -4 -9 -4 169.387 114.826 21 -4 9 -4 193.88 160.809 17 4 -9 4 -8.47026 68.9083 40 -4 -9 -4 126.931 54.136 8 -4 9 -5 6730.97 298.677 13 -4 -9 -5 6399.62 292.315 28 -4 -9 -5 6799.76 293.153 33 -4 9 -5 6478.79 293.024 12 -4 -9 -5 6775.93 291.754 34 -4 -9 -5 7087.18 292.99 35 -4 -9 -5 6978.3 291.725 24 -4 -9 -5 6436.29 288.776 25 4 -9 5 6580.45 346.613 40 -4 9 -5 6435.25 300.411 11 -4 -9 -5 6478.07 290.515 10 -4 -9 -5 6500.47 291.092 21 -4 -9 -5 7028.14 291.973 20 -4 9 -5 6506.09 298.682 17 -4 9 -5 6782.04 296.311 18 -4 -9 -5 6259.18 288.598 8 4 -9 6 54.2337 77.8521 22 -4 -9 -6 129.727 50.5865 35 -4 -9 -6 126.036 57.2936 24 -4 -9 -6 50.1579 48.3835 25 -4 -9 -6 22.5798 57.6835 30 -4 9 -6 17.2984 63.1705 13 -4 9 -6 73.3271 54.0829 12 -4 -9 -6 36.8049 55.924 34 -4 -9 -6 54.5847 52.0958 28 -4 9 -6 79.0568 69.4483 17 -4 9 -6 71.1732 48.7962 18 -4 -9 -7 3957.95 172.525 34 -4 -9 -7 3889.51 171.755 35 -4 -9 -7 3791.47 171.524 28 -4 9 -7 3702 176.081 13 -4 9 -7 3874.8 182.571 11 -4 -9 -7 3619.65 168.744 25 -4 9 -7 3166.05 170.225 12 -4 -9 -7 4055.15 172.303 30 4 -9 7 4057.24 185.186 22 4 -9 8 389.429 73.9902 22 -4 -9 -8 351.983 60.6944 34 -4 9 -8 334.691 53.8781 29 -4 -9 -8 441.574 63.1759 20 -4 9 -8 406.842 71.5277 11 -4 -9 -8 342.319 54.8748 30 -4 -9 -8 317.795 60.5054 24 -4 -9 -8 351.601 40.5503 25 4 10 -9 154.383 23.6791 32 -4 -10 8 626.01 64.7056 27 4 -10 -8 596.88 52.2269 19 4 10 -8 572.723 60.3589 18 4 -10 -8 731.006 57.146 32 4 10 -8 571.465 81.0808 13 4 10 -8 561.929 68.3272 12 4 -10 -7 164.76 44.854 21 4 10 -7 143.002 69.1503 18 4 -10 -7 137.305 51.5797 19 4 -10 -7 94.6001 41.6979 16 4 -10 -7 182.681 46.7872 29 4 10 -7 100.051 61.0989 12 4 -10 -7 135.124 45.2577 26 -4 -10 7 113.352 65.4908 27 4 -10 -7 224.392 52.6815 32 -4 -10 6 704.997 77.3008 22 4 -10 -6 846.886 59.2054 23 4 -10 -6 848.71 66.7896 21 4 -10 -6 740.899 65.5353 35 4 -10 -6 946.911 73.3338 32 4 -10 -6 764.051 64.5664 29 4 10 -6 891.991 80.506 12 4 10 -6 680.44 96.2771 13 4 -10 -6 1009.93 75.3459 19 4 10 -6 908.774 91.3347 18 4 -10 -6 840.428 66.1942 26 -4 -10 6 824.753 89.516 27 4 -10 -6 762.481 66.1232 16 -4 -10 5 1971.71 118.861 27 4 -10 -5 1882.39 102.435 26 4 10 -5 1823.49 109.088 12 -4 -10 5 1656.04 112.568 22 4 -10 -5 1828.78 100.973 23 4 -10 -5 1876.22 102.397 21 4 -10 -5 1925.7 105.814 16 4 -10 -5 1892 100.153 35 4 -10 -5 1671.55 99.1388 29 4 -10 -5 1909.18 98.6535 14 4 10 -5 1862.43 123.776 13 4 -10 -4 6316.21 336.242 29 4 -10 -4 7419.6 327.378 30 4 -10 -4 7749.57 330.828 14 4 10 -4 7481.88 341.012 13 4 10 -4 6386.47 364.66 37 4 -10 -4 7493.14 328.336 26 -4 -10 4 7742.83 344.596 27 -4 10 4 7203.62 370.773 38 4 10 -4 7525.85 333.168 12 4 10 -4 7607.04 384.047 7 -4 -10 4 7686.31 381.299 6 4 -10 -4 7842.93 329.53 23 -4 -10 4 7648.09 338.775 22 4 -10 -4 8008.9 329.241 21 4 -10 -4 6984.23 335.473 20 4 10 -4 7596.98 347.414 18 4 -10 -4 8114.6 335.649 19 4 -10 -4 7669.83 337.614 35 4 -10 -4 7257.12 336.123 36 4 -10 -4 7631.2 331.566 16 -4 -10 4 6013.87 363.352 41 4 -10 -3 308.233 34.2777 26 4 -10 -3 218.097 36.414 19 -4 -10 3 238.724 43.584 22 4 -10 -3 329.315 36.9076 23 4 -10 -3 268.826 36.5763 21 4 10 -3 345.005 71.9138 37 -4 10 3 301.308 86.0427 38 -4 -10 3 144.006 62.7224 41 4 10 -3 280.265 44.6186 18 4 -10 -3 273.248 34.356 36 -4 -10 3 455.093 99.1299 6 4 10 -3 236.619 74.9598 7 4 -10 -3 313.243 36.5122 14 4 -10 -3 322.818 36.6444 32 -4 -10 2 781.554 50.7656 8 4 -10 -2 774.975 78.9915 40 4 10 -2 774.39 85.0096 7 -4 -10 2 838.032 77.6957 41 4 10 -2 662.893 86.134 37 4 -10 -1 5896.81 280.747 40 -4 10 1 6382.84 290.914 38 4 10 -1 5802.2 287.609 37 -4 10 1 5300.99 278.407 37 4 10 -1 5352.85 272.628 7 -4 -10 1 5530.21 247.257 8 -4 -10 1 5658.25 288.545 6 -4 10 0 1021.06 94.141 38 4 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2309.98 123.134 12 -4 -12 -4 2133.4 109.296 34 -4 -12 -4 2379.93 118.343 35 -4 -12 -4 2040.56 106.514 24 -4 -12 -4 2084.24 109.841 23 4 -12 4 2166.76 125.464 22 -4 12 -4 2383.89 126.962 11 -4 -12 -4 2205.44 112.952 8 -4 -12 -4 2262.62 114.505 30 -4 12 -4 2283.81 128.651 18 -4 -12 -4 2112.51 110.591 21 -4 -12 -4 2037.78 110.161 20 -4 -12 -5 1984.51 104.227 24 -4 12 -5 1927.84 117.438 12 4 -12 5 1901.51 115.634 27 4 -12 5 2055.58 139.463 22 -4 12 -5 2024.45 135.326 11 -4 -12 -5 1911.25 117.107 35 -4 -12 -5 2067.62 106.391 34 -4 -12 -5 2192.79 118.499 30 -4 12 -5 2004.41 124.312 18 -4 -12 -5 2074.43 116.461 28 -4 -12 -5 2108.3 109.946 21 -4 -12 -5 1964.63 109.301 20 -4 -12 -6 661.345 57.3317 20 -4 12 -6 671.578 75.7577 11 -4 -12 -6 693.067 54.8082 34 -4 -12 -6 739.936 58.6988 35 -4 -12 -6 730.272 60.3334 30 -4 12 -6 666.051 61.1492 18 -4 -12 -6 685.214 54.5074 24 -4 12 -6 635.8 60.7869 12 -4 12 -6 767.121 72.5572 13 -4 -12 -6 659.927 56.7657 28 4 -12 6 698.221 67.9807 27 4 -12 7 267.813 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26 4 -13 -5 3155.63 150.332 16 4 13 -5 3141.02 171.473 18 4 13 -4 755.054 89.9455 18 4 -13 -4 777.066 70.7181 19 4 -13 -4 640.358 56.3879 35 4 -13 -4 676.536 53.8514 31 -4 -13 4 710.371 84.843 27 4 -13 -4 565.229 59.8837 26 4 -13 -4 706.828 61.578 36 -4 -13 4 722.706 87.3138 22 4 -13 -4 600.825 66.2658 23 4 13 -4 701.408 67.9442 12 4 13 -4 767.33 83.4701 13 4 -13 -4 724.897 61.9814 14 4 -13 -4 607.658 68.7994 16 -4 -13 3 18460.6 776.487 27 4 -13 -3 18804.3 771.727 19 4 13 -3 18070.8 777.736 18 4 -13 -3 18561.1 769.462 31 -4 -13 3 18161.7 777.751 22 4 -13 -3 19785.7 770.921 21 4 -13 -3 18560.8 771.146 32 4 13 -3 18557.2 771.032 12 4 13 -3 17263.3 773.673 13 4 -13 -3 18678.5 771.317 14 4 -13 -3 18082.2 769.707 36 4 -13 -3 16718.2 765.513 35 -4 -13 2 1691.41 104.465 27 4 -13 -2 1579.98 94.1559 14 4 13 -2 1326.37 133.779 37 4 -13 -2 1451.19 90.2386 23 4 -13 -2 1499.77 94.7015 21 -4 -13 2 1365.79 87.0915 31 -4 13 2 1491.8 137.407 38 -4 -13 2 1569.72 141.7 6 4 -13 -2 1486.19 91.5046 36 4 13 -2 1511.13 101.941 18 4 -13 -2 1565.99 92.2078 19 4 -13 -2 1394.5 93.5753 16 -4 -13 1 16097.7 776.566 6 4 -13 -1 18302.1 728.335 16 4 -13 -1 16732.6 725.973 36 -4 -13 1 16864.7 732.447 22 4 -13 -1 17389.6 725.494 23 4 -13 -1 17522.9 728.471 19 4 -13 -1 16769.1 726.222 21 -4 13 1 17095.1 779.079 38 -4 -13 1 16926.6 726.212 31 4 -13 -1 17860.9 728.593 14 -4 -13 1 17004.9 732.13 27 4 13 -1 15532.3 777.244 37 -4 -13 0 7382.04 364.607 6 -4 -13 0 7239.71 318.017 31 -4 -13 0 7269.64 332.232 27 -4 -13 0 7542.29 330.578 22 4 -13 0 7258.31 324.051 23 4 -13 0 6445.21 352.896 40 -4 13 0 6968.07 359.777 38 4 -13 0 7642.79 326.753 16 -4 13 0 6595.62 363.704 37 4 13 0 7527.12 376.862 37 -4 -13 0 6709.93 316.156 23 -4 -13 0 7442.97 318.896 8 4 -13 0 7179.05 317.863 36 -4 -13 -1 1784.76 107.062 31 -4 13 -1 1918.47 120.761 13 -4 -13 -1 1654.06 108.549 28 -4 -13 -1 1721.29 136.962 27 -4 -13 -1 1842.69 106.338 23 -4 -13 -1 1916.48 120.157 22 4 -13 1 1819.52 147.055 40 4 -13 1 1879.47 125.036 16 -4 -13 -1 2019.54 111.144 35 4 -13 1 1965.12 108.084 36 -4 -13 -1 2148.12 107.748 8 -4 13 -1 1632.15 156.691 37 -4 -13 -2 2030.97 113.092 31 -4 -13 -2 2054.1 105.995 30 -4 13 -2 2184.17 122.528 13 -4 -13 -2 2119.45 113.973 23 -4 -13 -2 2004.7 111.666 27 -4 13 -2 2046.85 115.334 11 4 -13 2 2216.99 118.069 22 4 -13 2 1655.13 150.813 40 -4 -13 -2 2393.89 119.018 35 -4 -13 -2 2242.55 115.641 33 -4 -13 -2 2082.94 113.935 8 4 13 2 2091.19 162.92 37 4 -13 2 2045.6 108.221 36 -4 13 -2 2000.28 163.083 37 -4 13 -3 1054.42 82.5571 11 -4 -13 -3 988.5 73.9435 23 4 -13 3 1014.77 84.8827 22 -4 -13 -3 1177.08 75.7828 8 -4 -13 -3 979.046 71.0436 30 -4 13 -3 1185.91 91.4138 13 -4 -13 -3 1077.01 79.2337 33 -4 -13 -3 1152.65 79.7871 28 -4 -13 -3 1010.46 81.1902 35 4 -13 4 2799.22 149.839 27 -4 13 -4 3387.12 160.696 12 -4 -13 -4 3080.95 145.204 20 -4 -13 -4 3084.31 146.961 21 -4 -13 -4 3024.22 142.271 24 4 -13 4 2966.86 162.176 22 -4 -13 -4 3454.44 155.546 35 -4 -13 -4 3049.33 144.781 34 -4 13 -4 3388.53 167.348 18 -4 -13 -4 3239.05 149.571 30 -4 13 -4 3306.77 166.968 13 -4 13 -4 3275.18 162.243 11 -4 -13 -4 3336.78 154.942 28 -4 -13 -5 114.078 50.4746 28 -4 -13 -5 69.6211 47.2696 20 4 -13 5 131.654 60.6755 27 -4 -13 -5 61.8923 43.4217 24 -4 13 -5 75.7831 57.4079 12 -4 13 -5 -14.7501 69.5579 13 4 -13 5 97.8596 71.381 22 -4 -13 -5 85.2791 51.0825 30 -4 -13 -5 145.054 47.0405 34 -4 13 -5 159.865 65.1658 18 -4 13 -5 122.833 68.6662 11 -4 -13 -5 125.65 52.979 35 4 -13 6 2184.72 117.813 27 -4 13 -6 2153.55 115.312 12 -4 -13 -6 2481.72 111.817 20 -4 -13 -6 2376.46 109.848 24 -4 -13 -6 2206.62 112.108 28 -4 -13 -6 2237.54 108.867 34 -4 -13 -6 2548.29 114.899 35 -4 -13 -6 2514.3 116.28 33 -4 13 -6 2423.26 124.657 13 -4 -13 -6 2547.62 114.728 30 -4 13 -6 2423.84 117.546 18 -4 13 -6 2398.02 124.569 11 -4 -13 -7 68.4791 33.487 24 -4 -13 -7 89.1733 34.3949 20 4 -13 7 46.2803 45.1268 27 -4 13 -7 18.584 48.1562 13 4 -13 7 20.7555 53.1399 22 -4 -13 -7 -11.0281 38.2234 33 4 14 -7 230.86 58.1916 13 4 14 -7 88.4924 40.1294 12 -4 -14 7 188.197 49.6142 27 4 -14 -7 177.042 36.6789 21 4 -14 -7 136.033 38.3647 19 4 14 -7 216.368 56.4789 18 -4 -14 7 171.893 36.3956 22 4 14 -6 3266.47 156.72 12 4 -14 -6 3942.89 156.176 21 4 14 -6 3423.62 168.032 13 -4 -14 6 3346.76 161.842 22 4 -14 -6 3271.95 150.937 23 4 -14 -6 3332.62 153.458 16 -4 -14 5 1025.73 87.8056 22 4 -14 -5 1201.23 71.6666 23 4 -14 -5 1039.26 66.6061 35 4 -14 -5 1201.29 78.1351 19 4 14 -5 1130.94 96.0998 18 4 -14 -5 1065.63 63.3647 36 4 14 -5 1076.53 77.3627 12 4 14 -5 1240.61 90.989 13 4 -14 -5 1132.19 75.9177 32 4 -14 -5 1080.1 74.2883 16 -4 -14 4 4048.77 199.854 27 4 14 -4 3746.5 190.738 13 -4 -14 4 3806.4 202.086 22 4 -14 -4 4150.02 186.724 23 4 -14 -4 3416.15 173.276 35 4 -14 -4 4088.48 189.006 19 4 14 -4 4040.9 205.851 18 4 -14 -4 3903.47 173.751 31 4 14 -4 3759.36 182.689 12 4 -14 -4 3937.56 187.871 16 4 -14 -4 4000.26 178.864 36 4 14 -3 942.712 72.8702 12 -4 -14 3 998.917 93.2779 22 4 -14 -3 732.625 60.3387 35 4 -14 -3 945.205 74.65 19 4 14 -3 857.702 86.6123 18 4 -14 -3 873.133 68.0356 31 4 -14 -3 950.758 72.238 14 4 -14 -3 880.992 75.8977 21 -4 -14 3 931.923 84.8222 27 4 -14 -3 888.927 71.2467 36 4 -14 -2 139.721 56.8417 36 -4 -14 2 183.675 48.3892 31 4 -14 -2 149.827 55.3037 31 -4 -14 2 234.654 66.1591 27 4 -14 -2 229.927 55.4566 19 4 14 -2 143.766 64.2405 18 4 -14 -2 204.544 59.5639 16 4 -14 -2 267.794 59.4504 14 4 -14 -2 175.516 61.8665 21 -4 -14 2 170.749 74.411 22 4 -14 -2 165.921 54.6069 23 -4 -14 1 1202.64 95.9051 22 4 -14 -1 1114.93 77.618 23 -4 -14 1 1367.82 89.783 27 4 -14 -1 1139.71 82.5858 36 4 -14 -1 1194.51 84.6942 21 -4 -14 1 1082.44 79.0438 31 4 -14 -1 1228.46 82.8455 16 -4 -14 0 553.652 72.9237 35 4 -14 0 457.017 62.5073 36 4 -14 0 448.91 62.8221 21 4 -14 0 563.284 60.752 16 -4 -14 0 520.823 65.06 27 -4 -14 0 558.612 73.4132 22 -4 -14 0 501.511 62.0781 23 4 -14 0 540.669 56.6426 23 -4 -14 0 561.701 63.954 31 -4 -14 -1 1390.18 90.5606 31 -4 14 -1 1353.89 89.9499 13 4 -14 1 1383.77 85.8218 36 4 -14 1 1386.89 85.0124 16 -4 -14 -1 1592.37 95.7769 35 -4 -14 -1 1281.84 93.75 22 -4 -14 -1 1458.4 89.8888 23 -4 -14 -1 1408.31 91.2573 28 -4 -14 -1 1222.87 84.8382 27 -4 -14 -1 1416 92.496 33 4 -14 2 1107.49 82.9738 22 -4 -14 -2 1160.44 85.0656 35 4 -14 2 1126.87 73.4817 36 -4 -14 -2 1137.6 80.8904 23 -4 14 -2 1249.11 89.1456 13 -4 -14 -2 1190.45 82.4799 33 -4 14 -3 80.7872 80.1836 18 -4 -14 -3 5.48053 58.3657 28 -4 -14 -3 50.1317 42.8508 30 4 -14 3 63.1132 62.0472 22 -4 -14 -3 46.2953 51.283 23 -4 14 -3 55.2983 70.2135 13 -4 14 -3 29.9411 56.5279 11 -4 -14 -3 -26.9484 62.7505 35 -4 -14 -4 1826.54 98.0834 20 -4 -14 -4 2035.52 104.375 21 -4 14 -4 2129.58 119.472 12 4 -14 4 1845.31 120.317 22 -4 -14 -4 1785.46 109.841 35 -4 14 -4 1909.59 121.213 18 -4 -14 -4 2036.57 108.862 28 -4 14 -4 2085.35 123.195 13 -4 14 -4 2007.61 121.983 11 -4 -14 -4 1915.24 106.103 30 -4 -14 -5 225.893 34.2106 24 4 -14 5 188.695 64.0446 22 -4 14 -5 186.64 59.9574 11 -4 -14 -5 210.695 45.567 28 -4 14 -5 184.28 58.9958 18 -4 -14 -5 230.254 44.7528 30 4 -14 5 236.058 46.8295 27 -4 -14 -5 238.574 48.9732 35 -4 14 -5 304.168 52.7125 12 -4 14 -5 203.075 63.9307 13 -4 -14 -5 166.346 37.2913 20 -4 14 -6 1677.58 94.7747 18 -4 -14 -6 1767.28 90.9045 30 -4 14 -6 1547.47 91.9502 12 -4 14 -6 1647.82 107.066 11 -4 -14 -6 1556.3 81.0177 20 -4 -14 -6 1696.34 94.2333 33 -4 -14 -6 1621.06 85.3243 28 -4 -14 -6 1787.92 92.9236 35 -4 14 -7 55.1775 39.1184 13 4 -14 7 88.7732 43.7974 22 -4 -15 6 1328.1 100.659 22 4 -15 -6 1271.66 77.1291 16 4 15 -6 1276.22 116.081 18 4 15 -6 1170.59 85.8866 12 4 15 -6 1173.44 110.197 13 4 15 -6 1123.38 89.1411 42 4 -15 -6 1432.92 85.582 21 -4 -15 5 -1.64668 56.9726 27 4 -15 -5 15.2013 42.6054 16 4 15 -5 30.0824 66.0731 18 4 -15 -5 38.2917 47.8179 19 4 15 -5 71.0485 57.5053 13 4 15 -5 53.8129 46.7981 12 -4 -15 5 37.7472 60.8346 22 4 -15 -5 72.332 40.8742 23 -4 -15 4 257.847 72.0868 22 4 -15 -4 197.803 50.8155 23 4 -15 -4 136.142 42.6304 35 4 -15 -4 152.414 45.3605 36 -4 -15 4 339.407 66.4911 27 4 -15 -4 221.498 53.4995 16 4 -15 -4 210.98 54.914 19 4 15 -4 221.133 73.4102 18 4 -15 -4 248.622 43.0271 31 4 15 -4 218.087 62.9033 13 4 15 -4 206.792 55.2978 12 4 -15 -4 222.628 57.6872 21 4 15 -3 1107.63 83.9942 12 4 -15 -3 1337.97 92.8168 23 -4 -15 3 1235.64 107.573 27 4 -15 -3 1192.1 92.1449 36 4 -15 -3 1309.42 85.5913 31 4 15 -3 1238.9 109.893 18 4 -15 -3 1251.2 96.9587 19 4 -15 -3 1285.72 99.4914 21 -4 -15 2 1286.95 103.149 22 4 -15 -2 1195.3 84.3326 23 4 -15 -2 1241.42 86.7661 36 -4 -15 2 1201.87 91.5466 27 4 -15 -2 1290.91 90.078 16 4 -15 -2 1160.38 83.8021 19 4 -15 -2 1394.74 90.0967 21 4 15 -2 1399.04 91.2915 18 4 -15 -2 1260.2 85.8163 31 4 -15 -1 358.01 60.0904 36 -4 -15 1 310.911 61.5117 27 4 -15 -1 235.296 61.8528 31 -4 -15 1 159.502 53.7845 31 -4 -15 1 272.914 72.5983 22 4 -15 -1 300.341 54.6999 23 4 -15 -1 380.867 60.9981 16 4 -15 -1 282.765 60.9344 21 -4 -15 0 1150.89 90.8471 35 4 -15 0 1106.97 81.6811 36 -4 -15 0 1130.23 82.6089 31 -4 -15 0 1243.58 91.1622 22 4 -15 0 1302.51 75.9173 23 4 -15 0 1121.62 80.6911 21 -4 -15 0 1116.91 78.8267 27 4 -15 0 1196.58 80.2955 16 -4 -15 -1 2502.71 135.65 35 -4 -15 -1 2334.59 123.818 27 -4 -15 -1 2581.96 132.554 28 4 -15 1 2389.85 125.641 21 4 -15 1 2702.41 127.492 36 -4 15 -1 2498.7 129.213 13 -4 -15 -1 2612.3 131.379 33 -4 15 -2 132.887 63.6737 13 4 -15 2 144.678 45.7619 36 -4 -15 -2 49.3672 71.3574 35 4 -15 2 79.6892 48.1451 21 -4 -15 -2 76.9852 63.5238 23 4 -15 2 245.317 55.9831 22 -4 -15 -3 4233.66 182.927 28 -4 15 -3 4337.31 191.391 13 -4 -15 -3 3497.21 170.606 30 4 -15 3 3580.19 178.41 31 4 -15 3 3789.96 187.879 22 -4 15 -3 4341.32 194.009 18 -4 15 -3 3572.32 181.497 11 -4 -15 -3 4060.75 183.574 35 -4 15 -4 509.283 67.5232 13 -4 15 -4 605.853 65.3582 12 -4 -15 -4 456.783 57.279 35 -4 -15 -4 387.264 44.1248 30 4 -15 4 512.535 64.8041 22 -4 15 -4 437.058 58.3559 11 -4 -15 -4 447.761 54.1424 28 -4 15 -5 2193.05 114.087 12 -4 -15 -5 2272.07 112.011 33 -4 -15 -5 2273.35 109.692 28 -4 15 -5 2481.53 122.133 13 -4 15 -5 2368.89 119.322 18 -4 -15 -5 2216.37 106.239 30 -4 -15 -5 2357.45 112.142 35 -4 15 -5 2247.89 115.451 11 4 -15 5 2311.68 119.702 22 -4 -15 -6 2240.21 95.9265 35 -4 15 -6 2064.36 99.4047 18 -4 -15 -6 2164.34 93.2057 30 -4 -15 -6 2078.21 96.9756 33 4 -15 6 2073.66 104.366 22 -4 -15 -6 1887.51 92.4299 28 -4 15 -6 1761.79 96.195 12 -4 -16 6 288.468 52.9292 27 -4 -16 6 327.946 49.8134 22 4 -16 -6 331.962 41.5387 21 4 16 -6 406.058 66.9062 18 4 16 -6 354.799 43.4562 42 4 -16 -5 406.514 54.9574 16 -4 -16 5 348.099 79.3725 22 4 -16 -5 381.523 51.6861 23 4 16 -5 332.156 48.3696 12 4 16 -5 299.54 57.1639 13 4 16 -5 493.475 86.5599 18 -4 -16 5 387.764 69.5378 27 4 16 -4 5598.77 250.157 18 -4 -16 4 5019.31 244.702 27 -4 -16 4 5927.28 250.045 22 4 -16 -4 5779.24 242.03 23 4 -16 -4 5514.06 242.872 16 4 -16 -4 6116.48 242.661 21 4 16 -4 4896.47 239.64 12 4 -16 -3 53.3213 49.9249 23 -4 -16 3 90.7176 55.9064 27 4 -16 -3 -6.81835 52.3885 21 4 -16 -3 42.8077 43.5016 31 4 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235.676 50.4619 21 -4 16 -2 276.254 62.9802 13 4 -16 2 344.294 65.1502 22 4 -16 2 193.301 53.9116 31 -4 -16 -2 328.391 62.4497 35 -4 16 -3 540.599 70.4503 18 -4 -16 -3 470.877 57.3104 28 -4 -16 -3 500.163 59.3566 35 -4 16 -3 469.052 63.143 13 4 -16 3 435.297 46.9496 31 4 -16 3 429.197 56.6378 22 -4 16 -4 331.597 45.4126 11 4 -16 4 519.961 56.8935 22 -4 -16 -4 442.84 52.4845 35 -4 16 -4 428.529 60.9981 13 -4 16 -4 464.823 59.0787 12 -4 -16 -4 437.604 49.6438 28 -4 16 -5 406.292 76.571 13 -4 16 -5 425.408 66.5213 12 -4 -16 -5 427.584 56.2445 28 -4 -16 -5 423.256 59.04 35 -4 16 -5 461.714 73.6223 18 4 -16 5 509.145 75.7678 22 -4 -16 -5 428.965 55.9563 33 4 -17 -5 915.942 52.7423 23 4 -17 -5 960.131 56.7807 21 -4 -17 5 740.855 58.6843 27 -4 -17 5 806.245 64.8956 22 4 17 -5 905.445 69.6293 18 4 17 -4 38.762 67.1884 18 -4 -17 4 139.243 34.1999 28 4 -17 -4 127.856 58.7186 21 -4 -17 4 138.783 74.8688 22 4 -17 -4 208.899 55.2354 23 4 -17 -4 45.5421 56.1986 16 -4 -17 4 36.3121 54.4299 27 -4 -17 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530.227 38 5 -11 1 11220.5 543.392 40 5 11 1 12282.5 551.386 37 -5 11 -1 11075.9 542.29 37 -5 -11 -1 11636.2 529.979 6 -5 -11 -1 11155.1 501.863 31 -5 -11 -1 11451.4 489.699 30 -5 -11 -2 2053.59 138.961 30 -5 11 -2 2135.46 127.575 13 -5 11 -2 1757.52 148.146 37 -5 -11 -2 1623.24 111.422 23 -5 -11 -2 2016.61 115.346 33 5 -11 2 1896.17 166.409 22 -5 11 -2 1982.03 146.601 11 -5 -11 -2 2111.19 111.834 8 -5 -11 -2 1739.66 152.48 27 -5 -11 -2 1952.81 114.828 28 -5 -11 -2 1863.22 121.337 35 5 -11 2 1856.1 149.002 40 -5 -11 -2 1871.33 123.163 20 -5 -11 -3 3185.9 143.534 30 -5 11 -3 2960.77 154.344 13 -5 -11 -3 2930 144.535 28 -5 -11 -3 3116.4 144.698 33 -5 -11 -3 2634.48 140.502 23 5 -11 3 2726.73 189.396 40 -5 11 -3 2851.91 151.213 11 -5 -11 -3 2988.93 142.68 8 5 11 3 2663.39 190.052 37 -5 11 -3 2502.69 187.586 37 -5 -11 -3 2671.69 144.376 34 -5 -11 -3 2925.86 144.386 35 5 -11 3 2752.33 151.187 22 -5 -11 -3 2943.92 143.871 20 -5 -11 -4 3193.19 153.148 30 -5 11 -4 3186.07 154.148 12 -5 -11 -4 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4 5 1222.91 127.569 2 7 -4 5 935.301 118.142 2 -7 4 -5 1104.9 114.972 39 -7 -4 -5 1385.8 80.5631 33 -7 -4 -5 1245.71 82.205 20 -7 4 -5 1341.25 90.5435 11 -7 -4 -5 1190.22 78.3473 10 -7 4 -5 1162.71 94.4243 17 -7 4 -6 3483.58 177.134 11 -7 -4 -6 3733.16 176.526 10 -7 -4 -6 4050.66 175.866 34 -7 -4 -6 3813.24 175.794 33 -7 -4 -6 3699.46 174.21 20 -7 -4 -6 3750.57 171.811 30 -7 -4 -6 3958.52 177.903 24 -7 -4 -6 3892.52 183.141 4 -7 4 -6 3469.21 181.363 4 -7 4 -6 3693.25 185.417 17 -7 4 -7 1801.86 113.735 17 -7 -4 -7 1971.05 100.158 34 -7 -4 -7 1714.96 96.8108 10 -7 4 -7 1800.85 104.007 11 -7 -4 -7 1905.36 95.6638 30 -7 -4 -7 1933.63 105.771 5 -7 4 -7 2037.7 106.086 5 -7 -4 -7 2051.25 102.962 24 -7 -4 -7 1979.52 106.349 25 -7 -4 -7 1931.73 99.1561 20 -7 -4 -8 525.587 46.476 34 -7 -4 -8 594.879 51.5595 24 -7 -4 -8 418.78 61.4013 25 7 -4 8 489.232 69.1093 22 -7 -4 -8 512.348 41.2672 20 -7 -4 -8 484.131 54.774 5 -7 4 -8 486.082 54.3024 5 7 -5 -9 538.662 49.9461 32 7 5 -9 505.113 46.2069 32 7 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2031.65 110.348 9 7 -5 -6 2045.85 109.879 9 7 -5 -6 2192.09 111.004 32 7 -5 -5 2234.23 133.637 12 7 -5 -5 2493.73 126.658 32 7 -5 -5 2583.08 120.714 9 7 5 -5 2298.05 118.205 9 7 5 -5 1987.48 169.277 7 7 -5 -5 2076.4 166.414 29 -7 5 5 2154.78 159.695 41 7 5 -5 2212.4 148.671 42 -7 -5 5 2045.36 159.39 41 7 -5 -5 2370.34 151.784 26 -7 5 5 1936.92 157.912 38 7 5 -5 2068.26 160.919 1 7 -5 -5 2161.41 161.983 1 7 5 -5 2060.94 206.385 13 7 5 -5 2176.02 184.916 18 7 -5 -5 2292.4 156.487 19 7 -5 -4 2272.38 114.005 29 7 -5 -4 2482.99 116.308 9 7 5 -4 2278.09 115.262 9 7 -5 -4 2361.61 115.514 19 -7 5 4 2456.63 166.013 38 7 -5 -4 2428.18 114.027 26 -7 -5 4 2526.21 156.11 41 7 5 -4 2545.88 159.871 1 7 -5 -4 2333.69 156.414 1 7 5 -4 2204.14 123.633 13 -7 -5 4 2056.22 153.487 38 7 5 -3 4559.13 244.792 7 7 5 -3 4308.33 233.008 1 7 -5 -3 4835.09 236.41 1 -7 5 3 4494.22 243.688 38 7 -5 -3 4317.09 241.444 40 -7 -5 3 4151.3 239.631 38 -7 -5 3 4271.14 225.607 41 7 5 -2 17011.6 715.429 7 7 5 -2 15550.1 702.028 1 7 -5 -2 16860.9 705.274 1 7 -5 -2 15726.4 712.453 40 -7 -5 2 14926.7 689.11 41 -7 -5 2 16832.9 718.768 38 -7 5 1 8996.93 394.229 39 -7 5 1 9177.72 410.802 38 7 -5 -1 8930.7 410.913 40 -7 -5 1 9226.55 409.125 39 7 5 -1 7619.48 384.536 37 -7 -5 1 9298.02 419.436 38 7 5 -1 8713.91 399.054 1 7 -5 -1 9336.25 402.24 1 7 5 -1 8271.27 404.88 2 7 -5 -1 8640.98 406.891 2 -7 5 0 954.317 85.1161 39 7 -5 0 963.476 95.7293 40 -7 -5 0 1070.84 99.0202 39 -7 -5 0 1059.31 105.255 38 -7 5 0 831.157 89.44 38 7 5 0 830 89.1573 2 7 -5 0 745.858 84.798 2 -7 5 -1 9350.43 422.639 38 7 -5 1 9653.21 433.868 40 7 5 1 8799.84 427.764 2 7 -5 1 9219.45 429.313 2 7 -5 2 18244.1 775.699 40 -7 -5 -2 17972.9 775.716 39 7 5 2 17359.4 773.619 2 7 -5 2 17086.7 771.243 2 -7 -5 -2 17332.8 736.436 10 -7 -5 -3 -6.70046 57.2843 39 7 -5 3 -33.1682 55.7002 40 7 5 3 7.10496 69.2806 2 7 -5 3 61.5746 65.5684 2 -7 -5 -4 2040.14 156.002 30 -7 5 -4 2042.24 120.384 13 -7 -5 -4 2204.35 138.363 28 -7 -5 -4 2195.81 139.941 34 -7 -5 -4 2185.9 142.153 24 -7 5 -4 2133.08 144.224 17 -7 5 -4 2208.88 170.437 11 -7 -5 -4 2157.88 110.749 10 7 5 4 1869.04 164.627 2 7 -5 4 1811.94 164.135 2 -7 -5 -4 2307.12 153.669 4 -7 5 -4 2076.7 154.484 4 -7 -5 -4 2054.2 142.294 33 -7 5 -4 2340.86 158.707 39 7 -5 4 1983.71 147.723 40 -7 -5 -4 2076.54 154.31 39 -7 -5 -4 2133.46 136.765 20 -7 -5 -5 9894.36 427.813 4 -7 5 -5 9292.13 426.521 4 -7 -5 -5 10356.1 424.688 30 -7 5 -5 9406.92 424.829 13 -7 -5 -5 9973.64 427.352 28 -7 5 -5 9849.6 428.925 11 -7 -5 -5 10213.4 427.845 10 -7 -5 -5 10114.2 425.32 20 -7 -5 -5 10130.6 425.707 34 -7 -5 -5 10172.2 424.462 33 -7 5 -5 9249.31 469.966 39 7 5 5 9359.23 477.689 2 7 -5 5 8772.49 472.299 2 -7 -5 -6 1697.3 97.1171 34 -7 -5 -6 1596.88 91.8271 30 -7 -5 -6 1586.19 94.3364 33 -7 -5 -6 1553.02 92.3757 10 -7 5 -6 1634.99 101.357 11 -7 -5 -6 1745.53 96.2656 20 -7 -5 -6 1573.15 101.933 4 -7 5 -6 1574.35 100.62 4 -7 -5 -6 1704.47 100.117 24 -7 -5 -7 662.152 60.1409 24 -7 -5 -7 543.547 49.6122 30 -7 -5 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219.577 41 7 6 -4 3702.47 175.939 9 7 -6 -4 3808.04 176.1 9 -7 6 3 10475.4 466.887 38 7 -6 -3 9678.4 462.854 40 -7 -6 3 9790.69 463.428 38 -7 -6 3 9590.19 444.844 41 7 6 -3 9318.84 449.192 1 7 -6 -3 10061.3 453.033 1 7 -6 -3 9375.76 415.171 9 7 -6 -2 288.683 70.7816 40 -7 -6 2 356.079 79.8163 38 7 -6 -2 339.055 62.7443 1 7 6 -2 294.18 60.7206 1 7 6 -2 411.478 82.3423 7 -7 -6 2 286.194 47.2279 41 7 6 -1 4136.34 213.88 1 7 -6 -1 4257.62 214.773 1 7 6 -1 4167.99 223.809 2 7 -6 -1 3917.3 220.276 2 -7 6 1 4438.83 229.118 38 -7 6 1 4071.45 210.539 39 -7 -6 1 4755.12 231.043 39 7 6 -1 4002.65 206.787 37 -7 -6 1 4748.8 240.628 38 7 6 0 5523.5 297.73 2 7 -6 0 5935.99 298.901 2 -7 6 0 6491.68 303.543 38 7 -6 0 6285.91 308.569 40 -7 -6 0 6267.37 307.862 39 7 6 0 6490.09 296.509 37 7 6 1 3070.82 180.469 2 7 -6 1 3321.87 183.149 2 7 -6 1 3594.4 191.201 40 -7 6 -1 3445.52 179.026 38 -7 6 -1 2832.13 174.022 37 7 6 2 62.5728 58.5895 2 7 -6 2 42.8095 60.3538 2 -7 6 -2 107.701 56.4011 37 -7 -6 -2 111.227 32.156 10 -7 -6 -2 141.284 62.9783 39 7 -6 2 27.2299 58.8295 40 7 -6 3 7769.73 389.418 40 -7 -6 -3 7411.12 385.934 39 -7 6 -3 8162.5 349.047 17 -7 -6 -3 8248.98 346.078 28 -7 6 -3 8241.93 348.528 11 -7 -6 -3 8004.95 344.561 24 7 6 3 7393.88 387.651 2 7 -6 3 7493.74 386.085 2 -7 -6 -4 960.828 118.132 28 -7 6 -4 1085.7 89.7209 13 -7 -6 -4 939.307 97.7732 4 -7 6 -4 1060.34 106.783 4 -7 -6 -4 885.067 106.211 24 -7 -6 -4 864.981 122.134 20 7 6 4 971.565 110.576 2 7 -6 4 864.878 107.085 2 -7 -6 -4 1041.27 102.968 39 7 -6 4 977.928 102.834 40 -7 6 -4 809.667 106.104 39 -7 -6 -4 1009.19 127.84 34 -7 -6 -4 1024.79 76.6931 33 -7 -6 -4 1001.18 121.421 30 -7 6 -4 1155.59 141.199 17 -7 6 -4 1017.08 120.916 11 -7 -6 -4 1002.51 73.7013 10 -7 -6 -5 3339.41 162.908 28 -7 -6 -5 3498.63 161.866 20 -7 -6 -5 3236.55 162.286 25 -7 -6 -5 3503.71 163.327 24 -7 6 -5 3453 168.006 11 -7 -6 -5 3463.08 161.449 10 -7 -6 -5 3115.62 156.889 8 -7 -6 -5 3403.33 161.313 30 -7 -6 -5 3319.54 162.014 4 -7 6 -5 3339.95 162.947 4 -7 -6 -5 3484.46 160.172 33 -7 6 -5 3286.58 169.663 17 -7 6 -5 3342.08 161.84 13 -7 -6 -5 3266.48 162.141 34 -7 6 -6 -32.8172 85.5327 17 -7 6 -6 149.286 67.2797 11 -7 -6 -6 40.2728 44.3047 10 -7 -6 -6 4.88167 53.0947 33 -7 -6 -6 82.9607 66.3579 34 -7 -6 -6 86.6643 56.1537 30 -7 -6 -6 -5.76268 65.3365 20 -7 -6 -6 1.56663 69.2086 25 -7 -6 -6 61.6289 55.2896 5 -7 6 -6 114.108 55.8731 5 -7 6 -6 83.9811 44.5146 13 -7 -6 -6 92.101 59.502 4 -7 6 -6 -17.4168 57.6965 4 -7 -6 -7 146.373 46.9014 20 -7 -6 -7 142.546 48.6205 34 7 -6 7 181.176 67.4609 22 -7 -6 -7 160.723 32.8095 10 -7 6 -7 146.02 50.958 11 -7 -6 -7 191.333 45.1878 5 -7 6 -7 217.209 46.4968 5 -7 -6 -7 198.372 41.4886 30 -7 -6 -7 182.172 50.2662 24 -7 -6 -7 229 52.8494 25 -7 6 -8 102.118 47.9647 5 7 -6 8 186.319 83.9954 22 -7 -6 -8 203.242 54.2984 34 -7 -6 -8 219.756 54.1836 24 -7 -6 -8 160.318 58.0228 25 -7 -6 -8 152.283 52.8272 20 7 7 -9 64.7433 32.2205 32 7 -7 -9 71.778 37.4462 26 7 -7 -9 19.9881 33.0122 19 7 -7 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1319.96 116.564 13 -7 7 5 1293.21 118.585 41 7 7 -5 1374.31 91.9938 42 -7 -7 5 1238.02 123.221 41 7 -7 -5 1477.4 97.8641 16 7 -7 -5 1604.52 83.8038 3 7 -7 -5 1505.83 82.7466 9 7 -7 -5 1391.03 89.5919 32 7 -7 -4 270.972 91.2111 29 7 -7 -4 364.251 46.1979 9 7 -7 -4 474.422 84.926 26 -7 -7 4 233.232 163.123 27 -7 -7 4 473.569 101.45 6 7 7 -4 652.389 107.259 7 7 -7 -4 385.633 120.286 32 7 7 -4 300.419 140.06 13 7 -7 -4 289.492 82.1689 1 7 -7 -4 350.714 44.4407 21 7 -7 -4 438.626 87.344 16 -7 -7 4 442.711 96.1761 41 7 -7 -4 411.394 108.117 19 7 7 -4 295.261 118.782 18 -7 7 4 371.407 89.8783 38 7 -7 -3 152.992 71.8053 40 7 -7 -3 86.7886 50.8449 1 7 7 -3 15.7209 76.4412 7 -7 -7 3 49.733 46.7017 41 7 -7 -3 66.7015 28.7545 26 -7 7 3 54.9609 72.6076 38 7 7 -3 113.129 43.1783 18 7 -7 -3 59.2846 32.0196 16 7 -7 -3 62.4271 32.836 29 7 7 -2 1244.21 116.582 7 7 -7 -2 1326.14 114.09 40 7 -7 -2 1298.48 99.0697 1 7 7 -1 174.856 66.6543 7 -7 7 1 101.306 45.3935 39 7 -7 -1 88.5822 65.3287 40 -7 7 1 65.0674 62.6042 38 7 7 -1 65.6683 43.0501 37 7 7 -1 -36.5145 51.8153 1 7 -7 -1 -22.8131 46.7399 1 -7 7 0 24794.6 1022.86 38 7 -7 0 26112.2 1032.59 40 -7 -7 0 25698.2 1031.71 39 7 7 0 23863.5 1016.25 37 7 7 0 22593.2 1006.96 1 7 -7 0 22987.9 1007.42 1 7 7 0 21224.5 1012.16 2 7 -7 0 23101.2 1014.71 2 -7 7 -1 2188.46 144.54 37 -7 -7 -1 2470.45 146.214 6 -7 -7 -1 2633.34 118.669 10 7 7 1 2122.87 146.427 2 7 -7 1 2274.57 145.257 2 7 -7 1 2580.68 162.421 40 -7 7 -1 2497.9 147.958 38 -7 -7 -2 13501.3 578.673 10 7 -7 2 14094.5 625.182 40 -7 -7 -2 14606.2 624.911 39 7 -7 2 13130.9 611.03 2 -7 7 -2 13371.5 617.76 37 -7 7 -3 1686.86 144.566 17 -7 -7 -3 1535.56 82.9248 33 -7 7 -3 1512.01 119.29 13 7 -7 3 1466.45 141.561 40 -7 -7 -3 1619.9 141.178 39 -7 -7 -3 1812.43 138.969 28 -7 -7 -3 1706.15 175.256 30 7 -7 3 1124.12 115.638 2 -7 -7 -3 1638.86 83.2244 24 -7 -7 -4 39.0065 58.0905 33 -7 -7 -4 43.7775 60.1746 24 -7 7 -4 54.9741 68.4975 17 -7 7 -4 75.729 70.7253 13 -7 -7 -4 39.2284 59.4906 30 -7 -7 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931.947 124.134 18 9 -8 -5 1088.98 82.0937 19 -9 -8 4 1870.25 111.345 27 9 -8 -4 1840.04 100.439 32 9 -8 -4 1819.12 111.765 14 9 8 -4 2031.03 133.938 18 9 -8 -4 1943.83 105.091 19 9 8 -4 1887.66 113.879 42 9 -8 -4 1919.45 109.055 26 9 -8 -4 1782.78 111.579 16 9 -8 -3 22596.6 938.572 26 9 8 -3 25011.6 1006.24 7 9 8 -3 23349 949.707 18 9 -8 -3 20920 934.061 19 -9 -8 3 22642.8 939.957 22 9 -8 -3 21153.3 931.946 21 9 -8 -3 22880.7 939.869 16 -9 8 3 21932.1 999.123 38 9 8 -3 22985.1 943.059 42 -9 -8 3 23215.7 941.8 27 9 -8 -2 206.925 71.1727 26 -9 -8 2 118.231 81.7151 27 -9 8 2 252.691 97.8316 38 -9 -8 2 317.304 125.791 22 9 -8 -2 241.867 82.3451 21 -9 8 2 121.867 65.3744 17 9 -8 -2 -7.65645 103.215 16 9 -8 -2 280.084 95.8461 40 -9 -8 2 349.705 105.007 6 9 8 -2 97.1729 102.231 7 9 8 -2 75.7853 71.1279 42 9 8 -2 342.751 156.695 18 9 8 -1 9159.05 448.016 7 -9 -8 1 9651.37 397.025 8 -9 8 1 8952.81 399.607 11 9 8 -1 9343.43 419.112 42 -9 8 1 8633.21 448.689 38 -9 -8 1 8663.5 445.118 6 9 -8 -1 8927.02 403.03 14 -9 -8 1 9415.49 418.253 27 -9 8 1 9091.28 397.337 17 -9 -8 0 479.442 84.6054 6 9 8 0 286.134 80.1458 7 -9 -8 0 624.052 139.318 27 -9 -8 0 375.438 51.37 10 -9 8 0 270.957 102.55 11 -9 -8 0 400.42 62.9942 8 -9 8 0 348.517 82.7057 38 9 8 0 408.36 94.7855 42 -9 8 0 401.842 69.6959 17 9 -8 0 148.57 88.376 40 -9 8 0 309.031 69.07 39 9 -8 0 392.03 71.9296 14 9 8 1 632.148 104.646 42 -9 -8 -1 535.17 54.9938 10 -9 8 -1 602.099 79.4385 11 9 8 1 510.254 83.9951 37 -9 8 -1 713.036 112.757 17 -9 -8 -1 558.732 82.8857 27 9 -8 1 472.88 99.5814 40 -9 8 -1 643.152 94.078 39 -9 -8 -1 640.786 65.7346 28 -9 -8 -2 2368.5 132.504 24 9 8 2 2539.48 179.098 37 -9 -8 -2 2889.2 138.294 10 -9 8 -2 3272.08 147.571 11 -9 8 -2 2586.46 179.935 39 9 -8 2 2805.75 189.57 40 -9 -8 -2 2538.18 181.968 39 -9 8 -2 2891.31 144.314 17 -9 -8 -2 2802.78 135.744 28 -9 -8 -3 35.6048 47.3393 10 -9 -8 -3 73.2953 50.8954 28 -9 8 -3 100.433 63.6063 17 -9 -8 -3 121.219 41.4565 33 -9 -8 -3 71.1864 45.5819 24 -9 8 -3 103.317 60.6974 13 -9 -8 -3 2.30056 46.495 8 9 -8 4 319.778 72.4914 22 -9 8 -4 212.615 76.6169 11 -9 -8 -4 240.373 59.7409 28 -9 8 -4 271.442 76.1916 17 -9 -8 -4 169.651 44.7569 33 -9 -8 -4 223.943 67.116 34 -9 -8 -4 220.334 52.901 24 -9 -8 -4 219.287 67.2833 30 -9 8 -4 292.054 63.556 13 -9 -8 -4 220.818 51.4758 8 -9 8 -5 94.4678 54.0325 13 -9 -8 -5 66.729 52.2103 25 -9 -8 -5 71.2269 50.0221 24 -9 -8 -5 -19.0087 52.9203 28 -9 -8 -5 14.9817 41.6598 33 -9 -8 -5 94.7424 56.1161 34 -9 -8 -5 53.495 45.2213 10 -9 8 -5 128.633 63.7482 11 -9 -8 -5 -34.6053 55.3132 20 -9 -8 -5 -30.4502 53.0588 30 9 -8 5 -20.6873 66.9221 22 -9 -8 -5 53.3856 40.0361 8 -9 8 -5 18.3999 64.9403 17 9 -8 6 407.057 66.2843 22 -9 -8 -6 402.366 43.9925 10 -9 8 -6 376.478 57.0796 11 -9 8 -6 388.009 64.5537 17 -9 -8 -6 452.398 48.3507 24 -9 -8 -6 434.401 49.6023 25 -9 -8 -6 548.25 48.2891 30 -9 -8 -6 484.984 52.6946 28 -9 -8 -6 382.334 50.9455 20 -9 -8 -6 407.242 51.1392 34 -9 -8 -7 473.84 40.2559 34 -9 -8 -7 375.919 38.9778 20 -9 -8 -7 344.452 33.8498 30 -9 8 -7 396.832 39.5973 11 -9 -8 -7 426.304 39.8885 24 -9 -8 -7 383.948 39.6433 25 9 -8 7 270.631 40.1335 27 9 -9 -8 55.3887 28.799 19 9 9 -7 519.329 99.856 18 9 -9 -7 558.668 70.4963 19 9 -9 -7 656.239 58.9214 32 9 -9 -7 717.255 71.8866 26 9 -9 -7 549.008 66.2395 16 9 -9 -6 1523.15 86.7405 14 9 9 -6 1449 85.7503 42 -9 -9 6 1351.72 86.1991 27 9 -9 -6 1627.74 86.331 32 9 -9 -6 1746.1 90.3115 19 9 -9 -6 1657.37 92.7564 26 9 -9 -6 1588.5 84.1951 23 9 -9 -5 665.974 83.6209 14 9 -9 -5 636.199 84.7145 16 9 9 -5 607.409 85.876 42 9 -9 -5 634.654 80.9538 23 9 -9 -5 713.239 74.6998 32 9 9 -5 588.986 118.491 18 9 -9 -5 700.041 81.7213 19 9 -9 -5 772.55 83.9466 26 -9 -9 5 645.037 86.2196 27 9 9 -4 5128.79 249.625 18 9 -9 -4 4957.42 227.004 19 9 -9 -4 5120.92 225.201 32 9 -9 -4 4654.13 220.889 21 9 -9 -4 5247.66 233.499 14 9 -9 -4 5186.13 233.416 16 -9 -9 4 5115.57 234.134 27 -9 -9 4 4890.32 229.739 22 9 9 -4 5202.27 236.025 42 9 -9 -4 5299.78 232.317 26 -9 -9 3 1303.47 88.1982 22 9 -9 -3 1162 85.9334 26 9 -9 -3 1216.23 75.434 32 -9 -9 3 1205.84 91.7417 27 9 -9 -3 1090.67 74.4537 21 9 9 -3 1288.13 107.518 18 9 -9 -3 1163.55 75.0571 19 9 -9 -3 1223.84 89.8154 14 9 -9 -3 1212.16 86.2484 16 -9 -9 2 2212.74 123.487 27 9 9 -2 2061.62 160.659 7 9 -9 -2 1932.91 115.771 26 -9 -9 2 1979.66 158.735 6 9 9 -2 2246.36 124.292 42 -9 -9 2 2137.96 123.091 22 9 -9 -2 2111.07 113.349 16 9 9 -2 1933.4 128.796 18 9 -9 -2 2096.72 117.951 14 9 -9 -2 1790.21 155.846 40 -9 9 2 1959.74 163.172 38 -9 9 2 2107.33 109.8 11 9 -9 -2 2032.42 109.374 21 -9 9 1 3104.58 162.63 11 -9 9 1 3220.5 168.135 17 -9 -9 1 3851.89 172.518 27 -9 -9 1 3189.4 210.325 6 9 -9 -1 3336.95 217 40 -9 9 1 2978.36 210.259 38 9 9 -1 3553.68 171.594 42 -9 -9 1 3507.43 159.756 8 9 9 -1 3327.07 214.977 7 9 -9 -1 3327.13 165.111 14 -9 9 0 5384.5 237.685 11 -9 9 0 5163.88 236.501 17 -9 -9 0 5488.18 236.064 8 -9 -9 0 4829.22 277.898 6 9 9 0 5282.31 240.682 42 -9 -9 0 5230.76 240.582 27 9 -9 0 4939.83 234.403 14 -9 9 0 4398.48 278.462 38 9 -9 0 5146.75 293.615 40 9 9 1 254.856 58.7823 42 -9 -9 -1 215.854 49.7801 28 9 9 1 181.687 72.6511 37 -9 9 -1 216.315 58.7243 17 9 -9 1 210.39 83.7234 40 -9 9 -1 192.364 72.3961 39 -9 -9 -1 274.994 50.4425 8 -9 -9 -1 198.257 47.3527 10 -9 9 -1 283.833 63.7893 11 -9 -9 -2 10724.8 455.231 28 -9 -9 -2 10644 457.342 30 -9 -9 -2 10403.7 458.288 10 -9 9 -2 10807.9 461.327 11 -9 9 -2 10451.6 459.459 17 -9 -9 -2 10716.9 460.176 8 -9 9 -3 24.5188 62.3574 13 9 -9 3 124.232 57.7282 22 -9 -9 -3 61.2185 48.2847 10 -9 9 -3 -2.28482 66.4565 11 -9 -9 -3 36.0975 49.69 8 -9 -9 -3 22.0312 57.7622 20 -9 -9 -3 15.6449 40.5452 33 -9 -9 -3 115.645 52.0184 28 -9 -9 -3 14.6272 41.2588 24 -9 9 -3 41.9788 62.496 17 9 -9 4 6914.63 313.391 22 -9 9 -4 6997.25 314.747 17 -9 -9 -4 6980.11 307.659 8 -9 -9 -4 6916.15 307.871 30 -9 9 -4 7405.05 312.848 13 -9 -9 -4 7241.96 308.464 28 -9 -9 -4 6505.03 300.007 33 -9 -9 -4 7035.53 307.904 20 -9 -9 -4 6791.59 300.47 24 9 -9 5 1535.91 99.4568 22 -9 9 -5 1613.25 98.0312 17 -9 -9 -5 1528 83.3201 8 -9 -9 -5 1605.59 90.2339 28 -9 9 -5 1548.15 89.9513 13 -9 -9 -5 1463.5 83.0388 24 -9 -9 -5 1463.1 86.1949 25 -9 -9 -5 1560.6 81.797 33 -9 -9 -5 1634.49 89.5505 30 -9 -9 -5 1616.67 87.5587 10 -9 9 -5 1672.31 99.2579 11 -9 9 -6 2239.07 118.305 11 -9 -9 -6 2388.19 112.633 20 -9 -9 -6 2217.03 112.08 34 -9 -9 -6 2277.98 109.792 30 -9 -9 -6 2080.92 112.631 28 -9 9 -6 2267.59 121.652 17 9 -9 6 2285.32 124.197 22 -9 -9 -6 2249.15 107.225 24 -9 -9 -6 2152.17 107.176 25 -9 -9 -7 158.431 31.197 24 -9 -9 -7 126.384 34.5997 20 -9 -9 -7 139.681 34.0482 34 9 -10 -7 424.997 56.3876 16 9 -10 -7 482.373 55.4301 32 9 -10 -7 575.765 57.8404 19 9 10 -6 1632.01 89.1484 42 9 10 -6 1780.72 116.951 18 9 -10 -6 1837.54 92.3734 19 9 -10 -6 1746.74 88.8931 32 -9 -10 6 1569.23 90.376 27 9 -10 -6 1914.12 95.5159 26 9 -10 -6 1529.01 87.5802 14 9 -10 -6 1664.65 87.2879 23 9 -10 -5 358.333 56.7227 23 9 -10 -5 372.617 48.6759 21 9 10 -5 507.584 65.7216 42 9 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653.284 75.1662 22 -9 10 -4 735.981 80.505 11 -9 10 -4 631.939 74.1265 17 -9 -10 -4 527.626 62.0508 25 -9 -10 -4 561.35 56.1143 24 -9 -10 -4 762.279 67.3817 20 -9 10 -4 755.589 73.9916 13 -9 -10 -4 747.297 65.9809 28 -9 -10 -4 566.487 55.5468 33 -9 -10 -4 673.507 66.3941 34 -9 -10 -4 740.177 60.7856 8 9 -10 5 -17.9942 54.5398 22 -9 -10 -5 39.8547 34.7765 33 -9 -10 -5 -37.186 33.229 8 -9 10 -5 45.5292 54.5592 17 -9 -10 -5 64.9169 48.146 30 -9 -10 -5 68.2392 34.9843 24 -9 -10 -5 11.4151 38.4101 25 -9 -10 -5 7.76344 46.2334 28 -9 10 -5 62.0871 47.8895 13 -9 -10 -5 18.1507 46.2444 20 -9 10 -6 453.065 77.5319 17 -9 10 -6 580.606 77.5302 11 -9 -10 -6 711.591 62.1091 30 9 -10 6 514.693 84.0462 22 -9 -10 -6 460.554 56.4734 24 -9 -10 -6 579.995 57.2664 25 9 -11 -7 546.326 46.545 16 9 -11 -7 494.202 48.4925 19 9 -11 -6 341.559 50.9134 19 9 11 -6 457.04 89.6387 18 9 -11 -6 351.603 46.6418 32 9 -11 -6 331.868 42.4279 14 -9 -11 6 361.359 49.4702 27 9 -11 -6 300.595 42.5789 23 9 11 -6 297.505 46.0318 42 9 -11 -5 20.9274 48.1334 23 9 11 -5 103.349 54.3122 42 9 -11 -5 1.09914 36.2597 36 9 -11 -5 -9.57689 53.696 16 9 -11 -5 76.0265 49.5207 14 -9 -11 5 113.897 55.1897 27 9 -11 -5 60.3035 53.02 26 9 -11 -5 45.6785 42.9889 32 9 11 -5 -44.9304 76.8298 18 9 -11 -5 51.6701 45.3707 19 9 -11 -5 34.5061 33.8945 21 -9 -11 4 97.2003 74.7163 22 9 -11 -4 67.0184 57.799 21 9 11 -4 54.7875 70.5697 42 9 -11 -4 83.7151 59.342 36 -9 -11 4 -34.5968 71.7271 27 9 -11 -4 36.1709 62.8505 26 9 -11 -4 58.2652 61.9568 16 9 -11 -4 113.215 62.7808 14 9 11 -4 -16.518 90.5713 18 9 -11 -4 20.7836 58.2915 19 9 -11 -4 150.633 60.3367 32 9 -11 -3 2293.56 121.712 21 9 11 -3 2711.11 143.706 42 9 -11 -3 2387.12 136.717 14 -9 -11 3 2425.82 139.362 27 -9 -11 3 2302.01 134.781 22 9 -11 -3 2599.64 133.564 23 9 11 -3 2540.29 146.72 18 9 -11 -3 2354.28 118.292 19 9 -11 -3 2470.91 130.083 16 9 11 -2 61.2855 69.0475 42 9 -11 -2 78.2176 53.5816 21 9 -11 -2 25.6721 50.3745 16 9 -11 -2 83.3975 62.4511 14 9 -11 -2 12.7267 56.6645 23 -9 -11 2 141.521 70.9943 27 9 11 -2 53.8457 68.0326 18 -9 -11 1 285.56 46.1501 8 -9 -11 1 374.521 72.2439 27 9 -11 -1 257.506 48.4615 16 9 -11 -1 387.612 61.2312 14 9 -11 -1 378.903 56.9771 23 9 11 -1 314.813 66.1564 42 -9 11 1 364.471 54.2317 11 -9 -11 0 697.285 61.743 8 9 -11 0 606.283 57.9125 23 9 -11 0 676.094 62.5691 14 -9 11 0 665.953 67.054 11 9 11 0 713.769 71.7453 42 -9 -11 -1 -20.2735 48.1747 8 -9 -11 -1 -18.3873 39.4425 33 -9 11 -1 49.9909 59.7025 11 -9 -11 -1 -62.4714 67.2857 27 -9 -11 -1 85.6107 45.2274 28 -9 -11 -1 42.2919 54.6133 30 -9 11 -2 1169.29 90.6768 11 -9 11 -2 826.748 71.2858 17 -9 -11 -2 909.874 77.5334 8 -9 -11 -2 861.366 61.6995 33 -9 11 -2 1040.22 94.8356 13 -9 -11 -2 746.509 69.4173 20 -9 -11 -2 846.39 69.1178 28 -9 -11 -2 951.19 76.4413 30 9 -11 3 28.3195 62.75 22 -9 11 -3 115.442 75.617 11 -9 11 -3 -38.3835 73.6572 17 -9 -11 -3 103.162 54.2902 33 -9 -11 -3 162.262 62.5914 34 -9 -11 -3 58.9206 62.6217 30 -9 -11 -3 99.2799 63.5743 20 -9 -11 -3 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-2 3 891.578 52.2815 17 16 -2 -3 708.572 49.2945 14 16 2 -2 147.651 57.8071 9 16 -2 -2 260.598 57.5714 9 -16 -2 2 174.078 51.6473 17 -16 2 2 184.043 57.7977 17 -16 -2 2 170.159 57.0335 4 -16 2 2 162.212 59.8823 4 -16 2 2 161.589 54.599 11 16 2 -1 181.371 69.4333 9 16 -2 -1 18.9001 66.1423 9 -16 2 1 32.8295 69.5875 17 -16 -2 1 126.394 71.8084 4 -16 2 1 -48.8156 71.8776 4 -16 2 1 30.1763 65.2513 11 16 2 0 7.62033 63.4859 9 16 -2 0 65.4915 60.4378 9 -16 2 0 101.361 59.9426 11 -16 2 0 95.7486 64.9553 17 -16 -2 0 35.5546 64.0503 4 -16 2 0 86.4755 66.4043 4 -16 -2 -1 773.211 56.8043 30 -16 -2 -1 1009.84 65.5006 4 -16 2 -1 1040.83 66.3695 4 16 2 1 973.927 64.767 9 16 -2 1 1000.99 65.5846 9 -16 -2 -1 951.455 58.492 8 -16 2 -1 994.205 63.2945 17 -16 2 -2 1733.52 84.153 17 -16 -2 -2 1735.89 89.3359 4 -16 2 -2 1716.93 90.1351 4 -16 3 4 110.126 30.178 17 -16 3 4 117.462 28.9304 11 -16 -3 3 77.887 40.0191 4 -16 3 3 6.04493 40.0005 4 -16 3 3 33.7382 44.1788 17 16 3 -3 77.6837 38.0588 9 16 -3 -3 54.3413 36.6182 9 -16 -3 2 2701.11 128.732 4 -16 3 2 2836.28 130.308 4 -16 3 2 2927.68 130.554 11 16 3 -2 2470.22 130.414 9 16 -3 -2 2840.68 130.681 9 -16 -3 1 580.62 66.0133 4 -16 3 1 716.002 66.7713 4 -16 3 1 668.282 65.8382 11 16 3 -1 611.228 67.833 9 16 -3 -1 539.41 66.4752 9 16 3 0 257.473 59.1536 9 16 -3 0 398.622 55.1777 9 -16 3 0 337.657 53.6949 11 -16 3 0 506.283 59.4222 17 -16 -3 0 376.99 55.6665 4 -16 3 0 419.053 59.2574 4 16 3 1 187.653 42.189 9 16 -3 1 99.1601 40.0049 9 -16 -3 -1 137.613 36.7235 30 -16 3 -1 155.837 35.7219 11 -16 -3 -1 159.502 42.181 4 -16 3 -1 61.923 44.3931 4 -16 3 -1 166.21 45.3815 17 -16 -3 -2 3.17753 39.0531 4 -16 3 -2 30.2014 39.7609 4 -16 3 -2 31.1524 39.8351 17 -16 4 3 5153.96 205.795 11 -16 4 3 5263.18 206.337 17 -16 -4 3 4458.05 200.894 4 -16 4 3 4368.17 201.482 4 16 4 -2 149.739 51.7883 42 -16 4 2 173.555 46.0947 17 -16 -4 2 131.845 40.0185 4 -16 4 2 261.959 40.6016 4 16 4 -2 137.363 38.5776 9 16 -4 -2 117.497 36.5503 9 -16 4 1 -33.6812 45.1544 11 -16 4 1 28.553 48.0857 17 16 4 -1 50.6185 45.9761 9 16 -4 -1 99.5431 44.4927 9 -16 -4 1 152.469 45.2163 4 -16 4 1 35.1759 43.762 4 16 4 0 214.073 43.2135 9 16 -4 0 156.207 39.2065 9 -16 4 0 108.936 42.9985 11 -16 -4 0 102.676 41.7886 4 -16 4 0 95.1213 42.8037 4 -16 4 -1 149.353 47.6625 17 -16 4 -1 125.545 36.1905 11 -16 -4 -1 85.3149 36.1172 4 -16 4 -1 113.086 38.9401 4 -16 -4 -1 95.5106 36.8228 30 -16 4 -2 188.251 34.2151 17 -16 5 3 39.9811 36.229 11 16 -5 -3 8.4045 33.8117 23 -16 5 3 40.3065 36.815 17 -16 5 2 720.598 56.0008 11 -16 5 2 597.168 54.9698 17 16 -5 -2 543.053 44.9444 23 -16 5 1 2082.12 91.7571 17 -16 5 1 1554.08 81.5174 4 -16 5 0 546.111 54.011 17 -16 -5 0 438.158 48.206 30 -16 5 0 457.528 49.5232 11 -16 5 0 496.005 39.213 13 -16 5 -1 897.459 56.8218 11 -16 -5 -1 851.365 54.8078 30 -16 -5 -1 805.104 55.7718 20 -16 6 2 57.0425 40.6635 11 -16 6 2 -3.73566 39.3814 17 -16 6 1 314.064 49.422 11 -16 6 1 283.842 49.2266 17 -16 -6 0 93.0562 41.3521 30 -16 6 0 44.2264 45.8347 17 -16 -6 0 81.6091 33.9151 34 -16 6 0 81.6714 44.8322 11 -16 -6 -1 417.15 33.5037 20 -16 -6 -1 362.385 33.0465 30 -16 6 -1 442.255 38.2764 17 -16 -7 1 39.4619 26.7339 30 -16 7 1 36.8747 29.5334 11 -17 0 1 -4.2004 30.3012 4 -17 1 1 168.775 30.3857 4 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 C1 C10 121.26(12) . . ? C6 C1 C2 118.90(13) . . ? C6 C1 C10 119.81(12) . . ? C1 C2 C26 123.79(13) . . ? C3 C2 C1 117.91(13) . . ? C3 C2 C26 118.30(13) . . ? C4 C3 C2 123.21(14) . . ? C3 C4 C5 117.88(13) . . ? C3 C4 C27 121.13(14) . . ? C5 C4 C27 120.99(14) . . ? C6 C5 C4 120.29(14) . . ? C5 C6 C1 121.55(14) . . ? C12 C7 C11 125.67(13) . . ? N8 C7 C11 110.76(12) . . ? N8 C7 C12 123.53(13) . . ? C1 C10 C11 116.06(11) . . ? C1 C10 C18 112.71(11) . . ? C18 C10 C11 109.54(11) . . ? O9 C10 C1 109.62(11) . . ? O9 C10 C11 99.37(10) . . ? O9 C10 C18 108.54(11) . . ? C7 C11 C10 101.52(11) . . ? F24 C11 C7 114.73(12) . . ? F24 C11 C10 113.96(12) . . ? F24 C11 F25 105.95(11) . . ? F25 C11 C7 107.52(11) . . ? F25 C11 C10 113.19(11) . . ? C13 C12 C7 119.62(13) . . ? C17 C12 C7 120.79(13) . . ? C17 C12 C13 119.59(13) . . ? C14 C13 C12 119.82(14) . . ? C13 C14 C15 120.41(15) . . ? C14 C15 C16 120.09(15) . . ? C17 C16 C15 119.92(15) . . ? C16 C17 C12 120.17(14) . . ? C19 C18 C10 119.81(13) . . ? C23 C18 C10 120.90(13) . . ? C23 C18 C19 119.29(14) . . ? C20 C19 C18 119.91(15) . . ? C21 C20 C19 120.41(15) . . ? C22 C21 C20 119.70(15) . . ? C21 C22 C23 120.33(15) . . ? C22 C23 C18 120.36(14) . . ? C7 N8 O9 109.41(11) . . ? N8 O9 C10 109.02(10) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 C2 1.407(2) . ? C1 C6 1.398(2) . ? C1 C10 1.5209(19) . ? C2 C3 1.399(2) . ? C2 C26 1.509(2) . ? C3 C4 1.386(2) . ? C4 C5 1.391(2) . ? C4 C27 1.509(2) . ? C5 C6 1.385(2) . ? C7 C11 1.507(2) . ? C7 C12 1.4693(19) . ? C7 N8 1.2799(19) . ? C10 C11 1.5420(19) . ? C10 C18 1.5397(19) . ? C10 O9 1.4617(17) . ? C11 F24 1.3521(17) . ? C11 F25 1.3722(16) . ? C12 C13 1.397(2) . ? C12 C17 1.395(2) . ? C13 C14 1.383(2) . ? C14 C15 1.387(2) . ? C15 C16 1.387(2) . ? C16 C17 1.387(2) . ? C18 C19 1.395(2) . ? C18 C23 1.390(2) . ? C19 C20 1.390(2) . ? C20 C21 1.387(3) . ? C21 C22 1.379(2) . ? C22 C23 1.389(2) . ? N8 O9 1.4234(15) . ?